tuv sud south asia pvt. ltd. - ias: the international ... · tuv sud south asia pvt. ltd. a1,...

This is to attest that

TUV SUD SOUTH ASIA PVT. LTD. A1, INDUSTRIAL ESTATE OPPOSITE TO NIRMAN PARK

KANCHARAPALEM MAIN ROAD, VISAKHAPATNAM ANDHRA PRADESH 530007

INDIA

Testing Laboratory TL-703

has met the requirements of the IAS Accreditation Criteria for Testing Laboratories (AC89), has demonstrated compliance with ISO/IEC Standard 17025:2005, General requirements for the competence of testing and calibration laboratories, and

has been accredited, commencing May 30, 2016, for the test methods listed in the approved scope of accreditation. This certificate expires June 1, 2017.

(See laboratory’s scope of accreditation for fields of testing and accredited test methods.)

This accreditation certificate supersedes any IAS accreditation bearing an earlier effective date. The certificate becomes invalid upon suspension, cancellation or revocation of accreditation. See http://iasonline.org/More/search.html for current accreditation information, or contact IAS at 562-364-8201.

C.P. Ramani, P.E., C.B.O President

of 27 TL-703, TUV SUD South Asia PVT. LTD.

IAS Accreditation Number TL-703

Accredited Entity TUV SUD South Asia PVT. LTD.

Address A1, Industrial Estate Opposite to Nirman Park

Kancharapalem Main Road, Visakhapatnam

Andhra Pradesh 530007

India

Contact Name Dr. Shaik Ali

Telephone +91 0891-6567000

Effective Date of Scope May 30, 2016

Accreditation Standard ISO/IEC Standard 17025:2005

FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE Microbiology Fish and Marine

Products

Aerobic Plate Count Chapter 3, US FDA - BAM

IS 5402

ISO 4833 – 1

ISO 4833 – 2

Escherichia coli Chapter 4, US FDA - BAM

IS 5887 (P 1)

ISO 16649 – 2

ISO 16649 – 3

Enumeration of Fecal Coliforms Chapter 4, US FDA – BAM

Enumeration of Coliforms Chapter 4, US FDA - BAM

IS 5401 (P 1)

ISO 4832

ISO 4831

Shigella spp Chapter 6, US FDA - BAM

IS 5887 (P 7)

Staphylococcus aureus Chapter 12, US FDA - BAM

IS 5887 (P 8 / Sec 1)

IS 5887 (P 2)

ISO 6888 (P 1)

Salmonella spp IS 5887 (P 3)

Chapter 5, US FDA - BAM

ISO 6579

2013.01, AOAC

Yeast and Mold Count Chapter 18, US US FDA - BAM

IS 5403

Bacillus cereus Chapter 14, US FDA – BAM

IS 5887 (P 6)

ISO 7932

Listeria monocytogenes Chapter 10, US FDA - BAM

IS 14988 (P 1)

ISO 11290 - 1

ISO 11290 - 2

2004.02, AOAC

Enterobacteriaceae ISO 21528 - 2

Enterococci Chapter 10, APHA 5th Edition


FIELDS OF TESTING MATERIAL DETERMINANTS METHOD REFERENCE

Microbiology Fish and Marine Products

Clostridium perfringens Chapter 16, US FDA - BAM

IS 5887 (P 4)

ISO 7937

Vibrio cholerae Chapter 9, US FDA - BAM

IS 5887 (P 5)

ISO 21872 - 1

Vibrio parahaemolyticus Chapter 9, US FDA - BAM

IS 5887 (P 5)

ISO 21872 - 1

Vibrio vulnificus Chapter 9, US FDA - BAM

ISO 21872 - 2

Sulfite reducing bacteria / Sulphide spoilage spore formers

ISO 15213

Meat & Meat Products Aerobic plate count Chapter 3, US FDA - BAM

IS 5402

ISO 4833 - 1 & 2


IS 5887 (P 1)

Enumeration of Fecal Coliforms Chapter 4, US FDA - BAM


IS 5401 (P 1)


IS 5887 (P 8 / Sec 1)

IS 5887 (P 2)



2013.01, AOAC

Yeast and Mold count Chapter 18, US FDA - BAM

IS 5403


IS 14988 (P 1)

2004.02, Chapter 17, AOAC

Clostridium perfringens ISO 7937

IS 5887 (P 4)

Shigella spp IS 5887 (P 7)

Poultry & Poultry

Products

Aerobic plate count Chapter 3, US FDA - BAM

IS 5402 / ISO 4833 - 1 & 2


IS 5887 (P 1)



IS 5401 (P 1)


IS 5887 (P 8 / Sec 1)

IS 5887 (P 2)

Salmonella IS 5887 (P 3)





Microbiology Poultry & Poultry Products


IS 5403


IS 14988 (P 1)



IS 5887 (P 4)


Vegetables & Vegetables Products


IS 5402

ISO 4833 – 1 & 2

Escherichia Coli Chapter 4, US FDA - BAM

IS 5887 (P 1)

ISO 16649 - 2



IS 5401 (P 1)



IS 5887 (P 8 / Sec 1)

IS 5887 (P 2)




Vibrio cholerae Chapter 9, US FDA - BAM

IS 5887 (P 5)


IS 14988 (P 1)


Bacillus cereus Chapter 14, US FDA - BAM

IS 5887 (P 6)


IS 5403


IS 5887 (P 4)

Lactic acid bacteria ISO 15214

Flat sour spore formers Clause 25.6, Chapter 25, APHA 5th Edition

Other Specified Food

Items - Raw, Cooked Foods and Ready to

Eat Foods


IS 5402

ISO 4833 – 1 & 2


IS 5887 (P 1)



IS 5401 (P 1)



IS 5887 (P 8 / Sec 1)



Microbiology Other Specified Food Items - Raw, Cooked Foods and Ready to Eat Foods





IS 5403


IS 5887 (P 6)


IS 14988 (P 1)



IS 5887 (P 4)

Vibrio cholerae Chapter 9, US FDA – BAM

IS 5887 (P 5)

ISO 21872-1

Enterobacteriaceae ISO 21528 – 2

Drinking Water - Piped and Bore Well

Coliforms 9221 B, 9221 C, 9221 E, APHA

IS 1622

Escherichia coli 9221 B, 9221 E, APHA

IS 1622

Escherichia coli and coliforms by membrane filtration technique

IS 15185

ISO 9308 - 1

Enterococci IS 15186

ISO 7899 - 2

Pseudomonas aeruginosa ISO 16266

Clostridium perfringens Annex 3, EU 98/83/EC

Colony count @ 220C ISO 6222

Colony count @ 370C ISO 6222

Packaged Natural Mineral Water and Packaged Drinking Water

Escherichia coli IS 5887 (P 1)

IS 15185

ISO 9308 - 1

Coliform IS 5401 (P 1)

IS 15185

ISO 9308 - 1

Fecal Streptococci IS 5887 (P 2)

IS 15186

ISO 7899 - 2

Staphylococcus aureus IS 5887 (P 2)

Sulphite reducing anaerobes IS 13428

Pseudomonas aeruginosa IS 13428

Yeast and Mold Count IS 5403

Aerobic Microbial Count IS 5402 @ 22 deg C & 37 Deg C

Salmonella IS 5887 (P 3)

IS 15187

Shigella IS 5887 (P 7)

Vibrio choleraee IS 5887 (P 5)



Microbiology Packaged Natural Mineral Water and Packaged Drinking Water

Vibrio parahemolyticus IS 5887 (P 5)

Water for Processed Food Industry

Standard Plate Count IS 1622

Coliform IS 1622

Proteolytic & Lipolytic count Appendix A, IS 4251

Beverages - (Alcoholic /Non - Alcoholic)


IS 5402

ISO 4833 - 1


ISO 16649 - 2

Yeast and Mold Count Chapter 18, US FDA - BAM

IS 5403

ISO 21527 - 1


ISO 6579




IS 5887 (P 8 / Sec 1)

ISO 6888 - 1


IS 5401 (P 1)

IS 5401 (P 2)

ISO 4831

ISO 4832


Vibrio cholerae IS 5887 (P 5)

Flat Sour Spore Organism Clause 25.6, Chapter 25, APHA 5th Edition

Cereal, Pulses and Cereal Products


IS 5887 (P 2)

IS 5887 (P 8 / Sec 1)





IS 5403

Bacillus cereus ISO 7932

Chapter 14, US FDA – BAM

Faecal Streptococci IS 5887 (P 2)

Microbiology Cereal, Pulses and Cereal Products


IS 5402

ISO 4833 – 1 & 2


IS 5401 (P 1)

IS 5401 (P 2)

ISO 4832



Microbiology Coffee and Cocoa Products

Escherichia coli Cereal, Pulses and Cereal Products


ISO 16649 - 2

IS 5887 (P 1)


IS 5402 ISO 4833 – 1 & 2


IS 5887 (P 1)


IS 5401 (P 1)



IS 5887 (P 8 / Sec 1)

Salmonella spp Chapter 5, US FDA - BAM

IS 5887 (P 3)



IS 5403


ISO 7932


Chapter 16, US FDA – BAM

Fruit and Fruit Products

Total Plate Count Chapter 3, US FDA - BAM

IS 5402 ISO 4833 – 1 & 2

Coliform Count Chapter 4, US FDA - BAM

IS 5401 (P 1)

IS 5401 (P 2)

ISO 4832

ISO 4831


ISO 16649 - 2

IS 5887 (P 1)



IS 5887 (P 8 / Sec 1)

IS 5887 (P 2)




Vibrio cholerae IS 5887 (P 5)



IS 14988 (P 1)



IS 5887 (P 6)


IS 5403



Microbiology Fruit and Fruit Products


ISO 7937

IS 5887 (P 4)

Lactic acid bacteria ISO 15214

Incubation test @ 37 deg for 10 days & 55 deg for 7 days

IS 2860

Flat sour spore formers Clause 25.6, Chapter 25, APHA 5th Edition

Herbs, Spices and Condiments


IS 5402

ISO 4833 - 1


ISO 16649 - 2

IS 5887 (P 1)


IS 5401 (P 1)

ISO 4832



IS 5887 (P 3)


ISO 6579


IS 5403

ISO 21527 - 2


IS 5887 (P 6)

ISO 7932


ISO 7937

IS 5887 (P 4)


IS 5887 (P 8 / Sec 1)

ISO 6888 - 1


Sulfite reducing bacteria ISO 15213

Milk and Dairy Products


IS 5402

ISO 4833 - 1


ISO 16649 - 2

IS 5887 (P 1)


IS 5401 (P 1)

ISO 4832





Microbiology Milk and Dairy Products


IS 5887 (P 8 / Sec 1)

IS 5887 (P 2)

ISO 6888 - 1


IS 5887 (P 3)


ISO 6579


IS 5403

ISO 21527 – 1


IS 5887 (P 6)

ISO 7932


IS 14988 (P 1)


ISO 11290 - 1


ISO 7937

IS 5887 (P 4)


Tea Aerobic Plate Count Chapter 3, US FDA - BAM

IS 5402

ISO 4833 - 1


ISO 16649 - 2

IS 5887 (P 1)


IS 5401 (P 1)

ISO 4832



IS 5887 (P 8 / Sec 1)

ISO 6888 - 1


IS 5887 (P 3)


ISO 6579


IS 5403

ISO 21527 - 1

ISO 21527 - 2


ISO 7932



ISO 11290 – 1



Microbiology Tea Clostridium perfringens Chapter 16, US FDA - BAM

ISO 7937

IS 5887 (P 4)


Wet Chemical Fish and Marine Products

Total Solids / Moisture 952.08, Chapter 35, AOAC FSSAI Lab Manual 6 (Clause 2.2)

Total Fat 948.15, Chapter 35, AOAC

Total Nitrogen 940.25, Chapter 35, AOAC

Total Ash 938.08, Chapter 35, AOAC

Sodium Chloride 937.09, Chapter 35, AOAC FSSAI Lab Manual 6 (Clause 2.3)

Total Volatile Base Nitrogen LAB_P_SOP_129 FSSAI Lab Manual 6 (Clause 1.2)

Acid Insoluble Ash IS 14950 Annex F FSSAI Lab Manual 6 (Clause 2.4)

Polyphosphates IS 5960 (P 13) Clause 8

ISO 5553 FSSAI Lab Manual 6 (Clause 3.5)

Lead, Cadmium, Mercury &

Arsenic

Lab_P_SOP_36 / AAS

Meat And Poultry Products

Moisture 950.46, Chapter 39, AOAC

Crude fat 960.39, Chapter 39, AOACFSSAI Lab Manual 6 (Clause 2.1)

Salt 935.47, Chapter 39, AOAC FSSAI Lab Manual 6 (Clause 2.3)

Total ash 920.153, Chapter 39, AOACFSSAI Lab Manual 6

(Clause 2.4)

Nitrogen 928.08, Chapter 39, AOACFSSAI Lab Manual 6 (Clause 2.2)

Copper, Zinc, Tin, Mercury, Arsenic, Lead, Cadmium & Selenium

LAB_P_SOP_50 AAS

Drinking Water / Packaged Drinking Water / Mineral Water / Process Water (Council

Directive 98/83/EC)

Colour IS 3025 (P 4) Clause 2 2120 B of APHA

Total dissolved solids IS 3025 (P 16) 2540 C of APHA

Odour IS 3025 (P 5) 2150 B of APHA

Turbidity IS 3025 (P 10) 2130 B of APHA

Taste IS 3025 (P 8)

2160 C of APHA

Aluminium IS 3025 (P 55) Lab_P_SOP_37 / AAS

Boron IS 3025 (P 57) Lab_P_SOP_37 / AAS

Residual free chlorine IS 3025 (P 26) Clause 3 4500 Cl-B of APHA



Wet Chemical Drinking Water / Packaged Drinking Water / Mineral Water / Process Water (Council Directive 98/83/EC)

Hexavalent chromium IS 3025 (P 52) Clause 6 3500 Cr B of APHA

Nitrites IS 3025 (P 34) Clause 4 4500 NO2 B of APHA

pH value IS 3025 (P 11) Clause 2 4500 H+ B of APHA

Total hardness (as CaCO3) IS 3025 (P 21) Clause 5 2340 C of APHA

Copper (as Cu) IS 3025 (P 42) Lab_P_SOP_37 / AAS

Iron (as Fe) IS 3025 (P 53)

Lab_P_SOP_37 / AAS

Manganese (as Mn) IS 3025 (P 35) Lab_P_SOP_37 / AAS

Nitrate (as NO3) IS 3025 (P 34) Clause 3 4500 NO3 B of APHA

Flouride (as F) IS 3025 (P 60) Clause 5

4500 F- D of APHA

Zinc (as Zn) IS 3025 (P 49) Lab_P_SOP_37 / AAS

Nickel (as Ni) Annexure F of IS 13428

Lab_P_SOP_37 / AAS

Chloride (as Cl) IS 3025 (P 32) Clause 2 3114 C of APHA

Selenium (as Se) IS 3025 (P 56) Lab_P_SOP_37 / AAS

Sulphate (as SO4) IS 3025 (P 24) Clause 4

4500 SO4 E of APHA

Alkalinity (as CaCO3) IS 3025 (P 23) 2320 B of APHA

Total Solids IS 3025 (P 15)

Calcium (as Ca) IS 3025 (P 40) Clause 5 3500 Ca B of APHA

Phenolic compounds (as C6H5OH) IS 3025 (P 43) 5530 D of APHA

Mercury (as Hg) IS 3025 (P 48) Lab_P_SOP_37 / AAS

Cadmium (as Cd) IS 3025 (P 41)

Lab_P_SOP_37 / AAS

Arsenic (as As) IS 3025 (P 37) Lab_P_SOP_37 / AAS

Lead (as Pb) IS 3025 (P 47)

Lab_P_SOP_37 / AAS

Chromium (as Cr) Annexure J of IS 13428 Lab_P_SOP_37 / AAS

Barium (as Ba) Annexure F of IS 13428 Lab_P_SOP_37 / AAS

Magnesium (as Mg) IS 3025 (P 46) 3500 Mg B of APHA



Wet Chemical Drinking Water/ Packaged Drinking Water/Mineral Water/Process

Water (Council Directive 98/83/EC)

Sodium (as Na) IS 3025 (P 45) Lab_P_SOP_37 / AAS

Silver (as Ag) Annex J IS 13428

Lab_P_SOP_37 / AAS

Molybdenum (as Mo) IS 3025 (P 2) Lab_P_SOP_37 / AAS

Mineral Oil IS 3025 (P 39) 5520 C of APHA

Anionic Surface Active Agents as MBAS

Annex K of IS 13428 5540 C of APHA

Sulphide as H2S IS 3025 (P 29) Clause 3

4500 S2- F of APHA

Antimony (as Sb) Annex G IS 13428 Lab_P_SOP_37 / AAS

Cyanide (as CN) IS 3025 (P 27) Clause 2 4500 CN- E of APHA

Borates (as B) Annex H of IS 13428

Chloramines as Cl2 4500 Cl -G APHA

Ammonia (as Total Ammonia –N)

IS 3025 (P 34) Clause 2 4500 –NH3 C of APHA

Oxidisability IS 3025 (P 58)

Dissolved oxygen IS 3025 (P 38) Clause 4

Total Organic Carbon (TOC) In-house method

Specific conductance IS 3025 (P 14) 2510 B of APHA

Milk (Raw and Pasteurized)/Curd/

Lassi/Condensed

Milk/Sweetened UHT Treated Condensed Milk

Total Milk Solids & Total Solids IS 1166 Append B IS 1479 Clause 4

IS 11622

IS 12333 Clause 8 990.20, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 1.3.3)

Titratable Acidity as Lactic Acid IS 1166 Append D

IS 11766 Clause 8 IS 1479 (P 1) Clause 14 947.05, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 9.5)

pH IS 4238 Append C



Wet Chemical Milk (Raw and Pasteurized)/Curd/ Lassi/Condensed Milk/Sweetened UHT Treated Condensed Milk

Total Fat IS 13688 Clause 5B IS 1479 (P 2) IS 11762 IS 1166 FSSAI Lab Manual 1 (Clause 1.3.4)

Total Ash IS 1479 (P 2) Clause 16 945.46, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 10.7)

Lactose IS 1479 (P 2) Clause 13

Sucrose IS 1166 Append C FSSAI Lab Manual 1 (Clause 9.4)

Crude Protein IS 1479 (P 2) Clause 8 IS 7219 FSSAI Lab Manual 1 (Clause

19.0)

Total Nitrogen IS 1479 (P 2) Clause 8 991.20,Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 19.0)

Solids-Not-Fat (SNF) 990.21,Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 15.2)

Titratable Acidity (as Acetic Acid) IS 12176 Append D FSSAI Lab Manual 1 (Clause 9.5)

Total Antibiotics as Beta Lactum Lab_P_SOP_238(Detection of

Antibiotic Residue in Milk and Milk Power) / Delvo Kit

Dry Milk Powder

(Milk Powder, Skim Milk Powder, Partly Skimmed Milk Powder, Infant Milk Substitute)

Moisture IS 11623

IS 14433 IS 16072 FSSAI Lab Manual 1 (Clause 10.2)

Total Solids IS 1165 IS 13334 (P 1)

IS 13334 (P 2) IS 14542 FSSAI Lab Manual 1 (Clause 10.2)

Sucrose IS 4079 Append C

FSSAI Lab Manual 1 (Clause 9.4)

Fat IS 11721

IS 14433 FSSAI Lab Manual 1 (Clause 10.3)

Total Ash IS 1165 Append A 930.30, Chapter 33, AOAC FSSAI Lab Manual 1 (Clause 10.7)



Wet Chemical Dry Milk Powder (Milk Powder, Skim Milk Powder, Partly Skimmed Milk Powder, Infant Milk Substitute)

Titratable Acidity as Lactic Acid IS 1165 Append B IS 11766 FSSAI Lab Manual 1 (Clause 10.4)

Protein / Milk Protein in MSNF IS 7219 930.29, Chapter 33, AOAC


Total Antibiotics as Beta Lactum Lab_P_SOP_238 (Detection of Antibiotic Residue in Milk and Milk Power)/ Delvo Kit

Cheese (Includes Natural & Processed Cheese) & Paneer

Moisture IS 2785 Append A IS 10484 Append A 926.08, Chapter 33, AOAC

Milk Fat IS 10484 Append B

Salt IS 2785 Append C

Titratable Acidity as Lactic Acid IS 10484 Append C 920.124, Chapter 33, AOAC19th

Edition

Ash 935.42, Chapter 33, AOAC

Total Nitrogen 2001.14, Chapter 33, AOAC

pH 943.02, Chapter 33, AOAC

Dairy Products Copper, Zinc, Tin, Mercury, Arsenic, Lead, Cadmium & Selenium

Lab_P_SOP_36 / AAS

Milk and Milk

Products

Aflatoxin M1 LAB_P_SOP_235

LC-MS/MS

Animal Feed / Pet Foods

Moisture IS 7874 (P 1) 934.01, Chapter 4, AOAC Clause 4

Crude Fat IS 7874 (P 1)

920.39, Chapter 4, AOAC Clause 7

Protien IS 7874 (P 1) 984.13, Chapter 4, AOAC Clause 5

Ash IS 7874 (P 1) 942.05, Chapter 4, AOAC Clause 9

Sugars 974.06, Chapter 4, AOAC

Crude Fibre IS 7874 (P 1) Clause 8

Animal Feeds Lead, Cadmium, Arsenic & Mercury

Lab_P_SOP_36 / AAS

Wheat Atta Moisture IS 1155 Append A


Total Ash IS 1155 Append B FSSAI Lab Manual 3 (Clause 8.3)



Wet Chemical Wheat Atta Gluten IS 1155 Append D FSSAI Lab Manual 3 (Clause 8.5)

Acid Insoluble Ash IS 1155 Append C FSSAI Lab Manual 3 (Clause 8.4)

Alcoholic Acidity IS 1155 Append F


Crude Fiber IS 1155 Append E FSSAI Lab Manual 3 (Clause 8.9)

Maida Gluten IS 1009 Append D


Moisture IS 1009 Append A


Ash IS 1009 Append B FSSAI Lab Manual 3 (Clause 8.3)

Acid insoluble ash IS 1009 Append C FSSAI Lab Manual 3 (Clause 8.4)

Alcoholic Acidity IS 1009 Append E FSSAI Lab Manual 3 (Clause 8.6)

Cereals, Pulses and By Products

Copper, Zinc, Tin, Mercury, Arsenic, Lead & Cadmium

Lab_P_SOP_36 / AAS

Spices and Condiments Pepper - Black, Kalimirchi

White (Whole, Powder)

Moisture IS 1797 Clause 9 FSSAI Lab Manual 10 (Clause 3.0) / IS 1798

Total ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0) / IS 1798

Non-volatile ether extract IS 1797 Clause 14

FSSAI Lab Manual 10 (Clause 9.0) / IS 1798

Volatile oil IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0) / IS 1798

Extraneous matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0) / IS 1798

Light Berries IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause

13.2) / IS 1798

Pinheads or broken berries IS 1798 Clause 4

Bulk density Lab_P_SOP_16 (Determination of Bulk Density)

FSSAI Lab Manual 10 (Clause

13.1)

Piperine 987. 07, Chapter 43, AOAC FSSAI Lab Manual 10 (Clause 13.3)

Turmeric – Haldi (Whole, Powder)

Moisture IS 1797 Clause 9 FSSAI Lab Manual 10 (Clause 3.0)



Wet Chemical Turmeric - Haldi (Whole, Powder)

Total Ash IS 1797 Clause 9 FSSAI Lab Manual 10 (Clause 4.0)

Acid Insoluble Ash IS 1797 Clause 9 FSSAI Lab Manual 10 (Clause 5.0)

Colouring power expressed as curcuminoid content

IS 3576 / IS 10925 Append B FSSAI Lab Manual 10 (Clause 15.4)

Total Starch IS 4706 Clause 9


15.5)

Test for Lead Chromate IS 3576 Annex A FSSAI Lab Manual 10 (Clause 15.6)

Extraneous Matter IS 3576 Clause 4.3 FSSAI Lab Manual 10 (Clause 2.0)

Defective rhizomes IS 3576 Clause 4.4

Cumin- Safed Zeera (Whole, Powder)



Acid Insoluble Ash IS 1797 Clause 8 FSSAI Lab Manual 10 (Clause

5.0)

Volatile oil Content IS 1797 Clause 15


Non Volatile Ether Extract IS 1797 Clause 14 FSSAI Lab Manual 10 (Clause 9.0)

Extraneous Matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause 2.0)

Broken Fruits (Dam Discoloured and Immature Seeds)

IS 2447 Clause 4

Cumin Black – Kalonji (Whole, Powder)


Total Ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause

4.0)

Cumin Black – Kalonji (Whole, Powder)

Acid Insoluble Ash IS 1797 Clause 8 FSSAI Lab Manual 10 (Clause 5.0)



Wet Chemical Cumin Black – Kalonji (Whole, Powder)

Volatile Oil Content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0)

Non Volatile Ether Extract IS 1797 Clause 14 FSSAI Lab Manual 10 (Clause 9.0)


Broken Fruits (Damaged,

Shrivelled, Discoloured and

Immature Seeds)

IS 1797 Clause 4

Edible seeds other than Cumin Black

IS 2447 Clause 4

Cardamom - Choti

Elachi , Large Cardamom - Badi Elachi (Whole, Seeds, Powder)

Moisture IS 1797 Clause 9




Extraneous Matter IS 1797 Clause 4 FSSAI Lab Manual 10 (Clause

2.0)

Chillies and

Capsicum (Whole, Powder)

Moisture IS 1797 Clause 9


Total ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0)

Acid insoluble ash IS 1797 Clause 8 FSSAI Lab Manual 10 (Clause 5.0)

Volatile oil content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0)

Extraneous matter IS 2322 Clause 5.4


Unripe and marked fruits IS 2322 Clause 5.5

Broken fruits, seed & fragments IS 2322 Clause 5.5

Crude fiber IS 1797 Clause 13 FSSAI Lab Manual 10 (Clause 11.0)

Non-volatile ether extract IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause

9.0)



Wet Chemical Chillies and Capsicum (Whole, Powder)

Colour 971.26, Chapter 43, AOAC / ASTA Colour

Cinnamon – Dalchini (Whole, Powder)



Acid Insoluble Ash IS 1797 Clause 18


5.0)



Cloves – Laung (Whole, Powder)

Moisture IS 1797 Clause 9 FSSAI Lab Manual 10 (Clause

3.0)

Total ash IS 1797 Clause 6 FSSAI Lab Manual 10 (Clause 4.0)

Acid insoluble ash IS 1797 Clause 18


Volatile oil IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0)

Crude fiber IS 1797 Clause 13 FSSAI Lab Manual 10 (Clause 11.0)

Extraneous matter IS 4404 FSSAI Lab Manual 10 (Clause

2.0)

Tendrils, Mother cloves IS 4404

Khokar cloves IS 4404

Headless cloves IS 4404

Coriander – Dhania (Whole, Powder)


Total ash IS 1797 Clause 6


Acid insoluble ash IS 1797 Clause 18 FSSAI Lab Manual 10 (Clause 5.0)



Wet Chemical Coriander – Dhania (Whole, Powder)

Volatile oil content IS 1797 Clause 15 FSSAI Lab Manual 10 (Clause 10.0)

Extraneous matter IS 1797 Clause 4


Split fruits IS 1797 Clause 4

Damaged / discolored fruits IS 1797 Clause 4.1

Spices and Condiments

Moisture IS:1797- 1985 FSSAI Lab Manual 10 (Clause

3.0)

Total ash IS:1797- 1985 FSSAI Lab Manual 10 (Clause

4.0)

Acid insoluble ash IS:1797- 1985

Non-volatile ether extract IS:1797- 1985 FSSAI Lab Manual 10 (Clause

9.0)

Volatile oil IS:1797- 1985 FSSAI Lab Manual 10 (Clause 10.0)

Extraneous matter IS:1797- 1985



Lab_P_SOP_36 / AAS

Fruit and Vegetable Products (Canned Fruits and Vegetables)

Total soluble solids IS 13815 920.151, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 1.6)

pH IS 2860 Clause 8 / IS 3881 Annex D FSSAI Lab Manual 5 (Clause 2.3)

Protein IS 7219 920.152, Chapter 37, AOAC

Salt IS 2860 Clause 11/ IS 1797 Clause 16

Reducing Sugars IS 6287 Clause 8 FSSAI Lab Manual 5 (Clause 2.6)

Sucrose IS 6287 Clause 9 FSSAI Lab Manual 5 (Clause 2.6)

Titratable Acidity IS 2860 Clause 10


Drained weight / net weight IS 2860 Clause 7

Vitamin C 967.21 Chapter 45, AOAC

Wet Chemical Fruit and Vegetable Products (Pickles)

pH IS 2860 Clause 8 / IS 3881 Annex D

Protein IS 7219 920.152, Chapter 37, AOAC



Wet Chemical Fruit and Vegetable Products (Pickles)

Salt IS 2860 / IS 1797 Clause 16

Reducing Sugars IS 6287 Clause 8

Sucrose IS 6287 Clause 9

Titratable Acidity IS 2860

942.15, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 2.4)

Drained weight / Net weight IS 2860 FSSAI Lab Manual 5 (Clause 1.4)

Vitamin C 967.21, Chapter 45, AOAC

Sulphur di oxide 990.28, Chapter 47, AOAC

Fruit and Vegetable

Products (Jam, Jellies, Marmalades)

Total soluble solids IS 13815

920.151, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause

17.3)

pH IS 2860 Clause 8 / IS 3881 Annex D

Protein IS 7219




Titratable Acidity IS 2860 942.15, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 2.4)



Water Insoluble solids 922.10, Chapter 37, AOAC

Soluble solids 932.12, Chapter 37, AOAC


Fruit and Vegetable Products (Dehydrated and Frozen Fruits and Vegetables)

pH IS 2860 Clause 8 / IS 3881 Annex D FSSAI Lab Manual 5 (Clause 17.3)

Protein IS 7219


Salt IS 2860 / IS 1797



Titratable Acidity IS 2860 942.15, Chapter 37, AOAC


Water Insoluble solids 922.10, Chapter 37, AOAC

Soluble solids 932.12, Chapter 37, AOAC


Moisture Lab_P_SOP_247 FSSAI Lab Manual 5 (Clause 4.1)

Acid Insoluble Ash Lab_P_SOP_248 FSSAI Lab Manual 5 (Clause 17.4)



Wet Chemical Fruit and Vegetable Products (Dehydrated and Frozen Fruits and Vegetables)

Starch IS 4706 (P 2) Clause 9


Fruit and Vegetable

Products (Ketchup, Sauces, Culinary Paste)



pH IS 2860 / IS 3881 Annex D

Protein IS 7219


Salt IS 2860 / IS 1797 Clause 16



Titratable Acidity IS 2860 942.15, Chapter 37, AOAC FSSAI Lab Manual 5 (Clause 2.4)


Fill of container Lab_P_SOP_250 (Determination of percentage fill of container in fruit and vegetable products)

Acid Insoluble Ash Lab_P_SOP_248 Determination of Ash Insoluble in Ash in Fruits and Vegetable product

Fruit and Vegetable

Products (Fruit Juice / Beverages, Squash, Cordial, Crush, Carbonated Juices)



Fruit content Lab_P_SOP_244 FSSAI Lab Manual 5 (Clause 2.11)

pH IS 2860 / IS 3881 Annex D FSSAI Lab Manual 5 (Clause 2.3)

Reducing Sugars IS 6287 Clause 8 FSSAI Lab Manual 5 (Clause 2.6)

Sucrose IS 6287 Clause 9 FSSAI Lab Manual 5 (Clause 2.6)

Titratable Acidity 942.15, Chapter 37, AOAC / FSSAI Lab Manual 5 (Clause 2.4)


Alcoholic and Non - Alcoholic Beverages (including Carbonated Beverages)


Lab_P_SOP_36 / AAS



Wet Chemical Coffee (Roasted Coffee/R&G Coffee/Soluble Coffee Powder, Soluble Coffee - Chicory Powder, Roasted Coffee -

Chicory Powder, Instant Coffee - Chicory Mixture)

Total ash IS 3077 920.93, Chapter 30, AOAC Annex F FSSAI Lab Manual 4 (Clause 1.3)

Acid insoluble ash IS 3077 Annex G FSSAI Lab Manual 4 (Clause 1.5)

Water soluble ash IS 3077 Annex H FSSAI Lab Manual 4 (Clause 1.4)

Alkalinity of ash IS 3077 Annex J FSSAI Lab Manual 4 (Clause 1.6)

Ether Extract IS 3077 Annex M

920.97 Chapter 30, AOAC

Aqueous extract IS 3077 Annex K FSSAI Lab Manual 4 (Clause 1.7)

Moisture IS 3077 Annex E 979.12, Chapter 30, AOAC FSSAI Lab Manual 4 (Clause 1.2)

Acidity 920.92, Chapter 30, AOAC

Crude fiber 920.98, Chapter 30, AOAC

Total ash IS 612 FSSAI Lab Manual 4 (Clause 1.3)

Tea (Black Tea, Green Tea, Instant

Tea)

Total ash IS 13854 / IS 13860 FSSAI Lab Manual 4 (Clause 1.3)

Acid insoluble ash IS 13857 FSSAI Lab Manual 4 (Clause 1.5)

Water soluble ash IS 13855 FSSAI Lab Manual 4 (Clause 1.4)

Alkalinity of ash IS 13856 FSSAI Lab Manual 4 (Clause 1.6)

Moisture IS 13853 FSSAI Lab Manual 4 (Clause 1.2)

Water soluble Extract IS 13862 FSSAI Lab Manual 4 (Clause 1.7)

Total polyphenols as Gallic Acid ISO 14502

Crude fiber IS 10226 (P 1)


Total ash 920.100, Chapter 30, AOAC FSSAI Lab Manual 4 (Clause 1.3)

Acid insoluble ash IS 3633

Alkalinity of ash IS 3633

Coffee, Tea, Cocoa and By Products

Copper, Zinc, Tin, Mercury, Arsenic, Lead, Cadmium,

Selenium, Manganese, Chromium, Iron & Nickel

Lab_P_SOP_36 / AAS



Chemical (Analytical) Food & Agricultural Commodities

Pesticide Residues: 4-Bromo-2-Chlorophenol, Alachlor, Aldrin, Allethrins, Bendiocarb, Bifenthrin, Bioallethrin, Butachlor, Carbaryl, Captafol, Captan, Chlordane-cis & trans, Chlorfenopyr,

Chlorfenvinphos, Chlorobenzilate, Chlorothalonil, Chlorpyrifos-methyl, ethyl, Cyfluthrin-I,II,III,IV, Cypermethrin - I, II,

III, IV, Deltamethrin, Dichlorvos , Dicofol, Dieldrin, α-Endosulfan, β-Endosulfan, Endosulfan -

Sulphate, Endrin, Ethion, Ethofenprox, Etrimfos,Fenitrothion, Fenpropathrin, Fenvalerate-I,II, Esfenvalerate, Fluvalinate-I,II, Fluchloralin, Formothion, HCB,

Heptachlor, Heptachlor epoxide, Imazethapyr,Iprodione, Isodrin, Methoxychlor, Metolachlor, Mirex, o,p', p,p' – DDD, o,p', p,p' - DDE, o,p', p,p' – DDT, Oxyfluorfen, Parathion-ethyl, methyl, Pendimethalin,

Permethrin-I,II, Phorate, Pretilachlor, Propanil, Propetamphos, Pyrene, Pyrethrins, Tau-Fluvalinate, Tetraconazole, Tetrahydrophthalimide, Transfluthrin, Trifluralin, Vinconazolin, α-BHC, β-BHC, ϒ-

BHC, δ-BHC, λ-cyhalothrin

AOAC 20th Edition 2015 EN 15662 : 2009 LAB_P_SOP_50-Fish & Fish Products LAB_P_SOP_97-Dairy & Dairy Products LAB_P_SOP_137- Beverages

LAB_P_SOP_202- Cereals, Pulses & their Products LAB_P_SOP_207-Spices Condiments & their products

LAB_P_SOP_260 – Fruits & Vegetables LAB_P_SOP_287 – Simulant

Foods By GC-MS/MS Lab_P_SOP_198 – Fish & Fish Products GCMSMS




Pesticide Residues: 2,4 - D, 3,4-Dichloroaniline, 3-Hydroxy Carbofuran, Acephate, Acetamiprid, Aldicarb, Aldicarb sulfone, Aldicarb Sulfoxide, Anilophos, Atrazine, Benfuracarb, Benomyl, Bitertanol, Buprofezin,

Carbaryl, Carbendazim, Carbofuran, Carbosulfan, Carpropamid, Cartaphydrochloride,

Chlorimuron-ethyl, Chlormequatchloride, Clomazone, Clodinafop-propargyl, Cyhalofop-

butyl, Cymoxanil, Diazinon, Diclofop-methyl, Difenoconazole, Diflubenzuron, Dimethoate, Dimethomorph, Dithianon, Diuron, Dodine, Edifenphos, Ethephon, Ethion, Ethoxyquin,

Ethoxysulfuron, Fenamidone, Fenarimol, Fenazaquin, Fenobucarb, Fenoxy-prop-p-ethyl, Fenthion, Fenthion sulfone, Fenthion sulfoxide, Formothion, Flonicamid, Flufenacet, Fosetyl-Al, Glufosinate-ammonium,

Glyphosphate, Hexaconazole, Imidacloprid, Indoxacarb, Iprodione, Isoprothiolane, Isoproturon, Kitazin (Iprobenphos), Linuron, Lufenuron, Malaoxon, Malathion, Malic Hydrazide, Metalaxyl,

Metalaxyl-M, Metasulfuron-methyl, Methabenzthiazuron, Methamidophos, Methomyl, Methyl Chloro-phenoxy-acetic Acid (M.C.P.A.), Metribuzin, Monocrotophos, Myclobutanil,

Novaluron, O-methoate, Oxadiargyl, Oxadiazon, Oxydemeton methyl,

Paclobutrazole, Paraoxon, Paraoxon-methyl, Paraquat, Penconazole, Phenthoate, Phorate sulfone, Phorate sulfoxide,

Phosalone, Phosphamidon, Pirimiphos-methyl, Profenofos,

AOAC 20th Edition 2015 EN 15662 : 2009 LAB_P_SOP_50-Fish & Fish Products LAB_P_SOP_97-Dairy & Dairy Products LAB_P_SOP_137- Beverages

LAB_P_SOP_202- Cereals, Pulses & their Products LAB_P_SOP_207-Spices Condiments & their products

LAB_P_SOP_260 – Fruits & Vegetables LAB_P_SOP_287 – Simulant

Foods By GC-MS/MS Lab_P_SOP_198 – Fish & Fish Products LCMSMS




Propargite, Propiconazole, Pyrazosulfuron ethyl, Quinolphos, Quizalofop-ethyl, Simazine, Spinosad-A, D, Sulfosulfuron, Tebuconazole, Thiamethoxam, Thiochlorprid, Thiodicarb, Thiometon, Thiophenatemethyl,

TNFA, TNFG, Triadimefon, Triadimenol, Triallate, Triazophos, Trichlorfon, Tricyclazole, Tridemorph, α-Naphthyl acetic

acid

Food and

Agricultural Commodities

Pesticide Residues:

Dithiocarbamates as CS2, Mancozeb, Metiram, & Propineb

LAB_P_SOP_210 GC-MS

Food and Agricultural Products, Animal

Feeds

Aflatoxins B1, B2, G1 & G2 Lab_P_SOP_225 LC-MS/MS

Food and Agricultural Commodities

Copper Oxychloride By AAS

Nut and Nut

Products, Cereals & Grains, Coffee

Aflatoxin B1, B2, G1 & G2 Lab_P_SOP_225

LC-MS/MS

Fish And Marine Products

Chloramphenicol LAB_P_SOP_43 LC-MS/MS

Sulfonamides: Sulfamethoxazole, Sulfadoxine, Sulfamerazine, Sulfadiazine, Sulfadimethoxine, Sulfapyridine, Sulfamethazine, Sulfachloropyridazine, Sulfamethoxypyridazine,

Sulfamethizole, Sulfathiazole

LAB_P_SOP_48 LC-MS/MS

Nitrofuran Metabolties: AHD, AMOZ, AOZ, SEM


Nitrofurans:

Furaltadone, Furazolidone, Nitrofurantoin, Nitrofurazone

LAB_P_SOP_96

LC-MS/MS

Dyes: Crystal violet, Leuco Crystal Violet, Malachite green, Leuco

Malachite Green


Tetracyclines & Epimers: Chlorotetracycline, 4-epi-Chlortetracycline, Oxyteracycline, 4-epi-Oxytetracycline, Tetracycline, 4-epi-Tetracycline




Chemical (Analytical) Fish And Marine Products

Fluoroquinolones: Ciprofloxacin, Danofloxacin, Difloxacin, Enrofloxacin, Flumequine, Oxolinic Acid, Sarafloxacin, Norfloxacin, Nalidixic acid


Antihelmintics : Emamectin benzoate, Ivermectin


Pesticide Residues: Aldrin, Carbaryl, Chlordane, Chlordane, Dieldrin, Endosulfan-

α, Endosulfan-β, Endosulfa-sulfate, Endrin, , Heptachlor, Heptachlorepoxide, Hexachlorobenzene, Lindane, Methoxychlor, o,p’, p,p’-DDD, o,p’, p,p’-DDE, o,p’, p,p’--DDT Pendimethalin, Quinolphos,

Trifluralin, α HCH, β HCH, γ-HCH, δ- HCH

LAB_P_SOP_50 GC-MS/MS

Polychlorobiphenyls: PCB28, PCB52, PCB101, PCB138, PCB153, PCB180


Ethoxyquin LAB_P_SOP_198 LCMSMS

Water (IS 14543:2004, IS

10500:1994, IS

13428:2005)

Pesticide Residues: Alachor, Aldrin, , Butachlor,

Methyl parathion, Chlordane,

Chlorpyrifos-methyl, Diledrin, o, p’,p,p’--DDT, o,p’,p,p’--DDE, o,p’, p,p’-DDD, Endosulfan-α, Endosulfan-β, Endosulfan sulfate, Ethion, Endrin, Heptachlor, Heptachlor epoxide, α-HCH, β-HCH, γ-HCH, δ-HCH,

Hexachlorobenzene , Parathion-methyl, ethyl, Phorate


2,4 – D, Atrazine, Carbaryl, Ethion, Isoproturon, Malaoxon, Malathion, Methyl paraoxon,

Monocrotophos, Pendimethalin, Phorate Sulfone, Phorate Sulfoxide, Quinolphos, Trifluralin

& Simazine


Polychlorobiphenyls (PCBs): PCB28, PCB52, PCB101, PCB138,

PCB153, PCB180




Chemical (Analytical) Water (IS 14543:2004, IS 10500:1994, IS 13428:2005) (Council Directive 98/83/EC)

Polyaromatic Hydrocarbons (PAHs) Acenaphthalene, Acenaphthene, Anthracene, Benz(a)anthracene, Benzo(a)pyrene, Benzo(b)fluoranthene, Benzo(g,h,i)perylene,

Benzo(k)fluoranthene, Chrysene, Di-benz(a,h)anthracene, Fluoranthrene, Fluorene, Indeno 1,2,3(c,d)pyrene, Naphthalene,

Phenanthrene & Pyrene


Water (Council

Directive 98/83/EC) (IS 14543:2004, IS 10500:1994, IS 13428:2005)

Volatile Organic Compounds

(VOCs): 1,2-dichloroethane, Acrylamide, Benzene, Trihalomethanes (Bromodichloromethane, Bromoform, Chloroform, Dibromochloromethane),

Epichlorohydrin, Tetrachloroethene, Trichloroethene & Vinyl Chloride

LAB_P_SOP_45

GC-MS/MS LC-MS/MS

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