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L.Test Certificatef! H-.~--,--~--' -~~-"'~"--<:>->:.~--""'~=--"""""'~'.~ •.•••...,.•.•.•",."-,....,..,,...,.-.--.:> .. """'". -, , - " -
Certificate ID: 66497 (Reissued) Received: 10/1/19 Scan QR Code
Client Sample ID: Isolate Hemp Extractfor authenticity~.Lot Number: I1908I-044A ~r ..
Matrix: Concentrates/Extracts - Hemp Extract - R .~.~00." ~
r---"-'Authorization: Signature:
~~.Date:
Jon Podgorni, Lead Research Chemist 10/24/2019
The data contained within this report wascollected in accordance with the requirementsor ISO/IECI7025:2017. I attest that theinformation contained within the report hasbeen reviewed for accurncy and checkedagainst the quality control requirements foreach method, These results relate only to thetest article listed in this report. Reports maynot be reproduced except in their entirety.# 80585
CN: Cannabinoid Profile &: Potency {WI.·IO~17 &: WI-IO-17-01] Analyst: RAS Test Date: 1011612019=='--'~==r-- '=====z====-'.----~===_..--~--.--~- ..---==~~~~.-~====~~~~,~~~=o=~.=-~======~~~~~~==~~~The client sample was analyzed for plant-based cannabinoids by Liquid Chromatography (LC). Due to the unique precision and accuracy demandsof assay testing for highly purified materials, samples were prepared in class-A volumetric glassware and quantitated against a single pointcalibration function. Five replicate injections of cannabidiol (CBD) certified reference standard are averaged to derive the calibration function andverify injection precision less than 2% RSD. Relative percent difference (RPD) of the Laboratory Duplicate for this sample preparation batch wasless than 2%. Assay values exceeding 100.00% are scientifically valid and result from the unavoidable accumulation of uncertainty at every stage ofsampling and analysis. Reissued to add sample lot number.
66497~C1V
ID Weigl~t % Concentration (mg/g)- """"-
09-THC NO NOTHCY NO NO
CBO 102.47 1024.66CBOV 0.35 3.50CBG NO NOCBC NO NOCBN ND NDTHCA NO NOCBOA NO NOCBGA NO ND
OS-THC NO NOexo·THC NO NOTotal 102.82 1028.16
Max THC NO NOMaxCBO 102.47 1024.66
---"'~'~.---"'-"""""""-"'--'"'- =-';""-'"""-~.-----~.~ -~. ~' ..
1I
Cannabinoids (wt%) 102.5%0%
Limit of Quantitation (LOQ) = 0.05 wt%
Max THC (and Max CBD) are calculated values for total cannabinoids after heating, assuming complete decarboxylation of the acid to the neutralform. It is calculated based on the weight loss of the acid group during decarboxylation: Max THC = (0.877 x THCA) + THe. This calculationdoes not include other cannabinoid isomers (eg, D8-THC and exo-THC). ND =None detected above the limits of detection (LOD), which is half ofLOQ.
FM-I0-1O, Rev. 1, DCN:15-0003tt20 Fortune Blvd 0 IVJliIfol'd,MA 01 '757 0 61 '7~:Z7,1<3356
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MMInc .ct - Raw Materials - Need full canabinoid profile)Certificate ID: 66497 (Reissued)
!!j}Il.: HeavYJ}!etal AI!Cl(vsislWl;20,,13j ._ __ .. nn n •• =.._.=A=n=a='l~"=s=~=:J=F=D=====T=e=st=D=at=e=:=1,,"O~/=7=,/2=O=1",,=2nThis test method was performed in accordance with the requirements ofISO/IEC 17025. These results relate only to the test article listed in thisreport. Reports may not be reproduced except in their entirety.
66497·HM
S~mbo~l~ __ ~ Me~talAs ArsenicCd CadmiumHg MercuryPb Lead
Cone. 1 ().lglkg)
NONONONO
RL
50505050
Use Limits 2 (ug/kg)All Ingestion Status
------~---.-.---~---
200 1500200 500100 1500500 1000
PASSPASSPASSPASS
I) ND =None detected to Lowest Limits of Detection (LLD)2) MA Dept. of Public Health: Protocol for MMJ and MIPS, Exhibit 4(a) for all products.3)USP exposure limits based on daily oral dosing of Ig of concentrate for a 110 lb person.
,YBl: Microbiological Coniamin.~mt~ rU:1-!O-09j . . __An_alyst~ MJC .. n_ •• _. Test Da.~e: 19!2!2019This test method was performed in accordance with the requirements of ISOIlEe 17025. These results relate only to the test article listed in thisreport. Reports may not be reproduced except in their entirely.
~ S~2.~?Ol~_~._~ .. Analysis Results Units Limits* Status... --- -. -_.
AC Total Aerobic Bacterial Count <100 CFU/g 10,000 CFU/g PASS
CC Total Coliform Bacterial Count <100 CFUlg 100 CFU/g PASS
EB Total Bile Tolerant Gram Negative Count <loa CFUlg 100 CFU/g PASS
YM Total Yeast & Mold <100 CFUlg 1,000 CFU/g PASS
Note: All recorded Microbiological tests are within the established limits.
/Y!.!}}: 1Z!!.tl1(!I{!..n.~£ Bacteria!. ~J!J!t(lmif!.(1'!.~sJ~f'l.-lq....!ql . Analyst: ,LabAd~Y!.i.n Test Date: 1Q!}L?Ql ~~This test method was performed in accordance with the requirements ofISOIJEC 17025. These results relate only to the test article listed in thisreport. Reports may not be reproduced except in their entirety.
66497-MB2
Test ID66497-ECPT
66497-SPT
AnalZ's_is~~E. coli (0157)
Salmonella
Results
Negative
Negative
Units
NA
NA
Limits*.~~-~-~Non Detected
N on Detected
StatusPASS
PASS
Note: All recorded pathogenic bacteria tests passed.
FM-10-1O, Rev. 1, DCN:15-0003420 Fortune Blvd 0 Milford, IVliA01757 0 617-221.,3356
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MMlnc Certificate ID: 66497 (Reissued) ct - Raw Materials - Need full canabinoid profile)
!§L:'!!!~/j{;!~{~1nalJ!§is[yfl:l0r~lJl .m________ ____~n ~nalyst:_10S_ Test Date: lO/22/20~!The client sample was anlayzed for pesticides using Liquid Chromatography with Mass Spectrometric detection (LC/MS/MS). The method used forsample prep was based on the European method for pesticide analysis (EN 15662)_
66497-PST
~~~~._v_>_o~c~naJ2'~~=«~_~o_~,~~.C~~_~_ ~~~~ul.!. ~-~~.J:!.~~~_~,~_......l:!:g_.._.~_.Abamectin 71751-41-2 ND ppb 0.2
Azoxystrobin 131860-33-8 ND ppb 0.10
Bifenazate 149877-41-8 ND ppb 0.10
Bifenthrin 82657-04-3 ND ppb 0.20
Cyfluthrin 68359-37-5 ND ppb 0.50
Daminozide 1596-84-5 ND ppb 10.00
Etoxazole 153233-91-1 ND ppb 0.10
Fenoxycarb 72490-01-8 ND pp b O.10
Imazalil 35554-44-0 ND ppb 0.10
Imidacloprid 138261-41-3 ND ppb 0.10
Myclobutanil 88671-89-0 ND ppb 0.10
Paclobutrazol 76738-62-0 ND ppb 0.10
Piperonyl butoxide 51-03-6 ND ppb 0.10
Pyrethrin 8003-34-7 ND ppb 0.1
Spinosad 168316-95-8 ND ppb 0.1
Spiromesifen 283594-90-1 ND ppb 0.10
Spirotetramat 203313-25-1 ND ppb 0.10
Trifloxystrobin 141517-21-7 ND ppb 0.10
Limits ~(pd,_p~b"-)__ S!.~~lS~_.300
40000
5000
500
1000
10
1500
10
10
3000
9000
10
8000
1000
3000
12000
13000
30000
PASS
PASS
PASS
PASS
PASS
*PASS
PASS
PASS
PASS
PASS
PASS
PASS
PASS
PASS
*PASS
PASS
" Testing limits for ingestion established by the State of California: CCR, Title 16, Division 42, Chapter 5, Section 5313. ND indicates "nonedetected" above the lower limit of detection (LLD). Analytes marked with (*) indicate analytes for which no recovery was observed for a pre-spikedmatrix sample.
FM-IO-lO, Rev. 1, DCN:1S-0003020 Fortune Blvd 0 io/Wfoi'd, IV~A01'157 0 61 7,,221<i3§6
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MMTnc Certificate lD: 66497 (Reissued) .ct - Raw Materials - Need full canabinoid profile)
,VC: :4nq(vsiJu()I}::~~f!~~!(?J)i'g(!nicC()mjJ()'1ndUU~/-J_~-2S.1. Anqlyst: .CM/L Test Date: 10/2/2019The client sample was analyzed by Head-Space Gas Chromatography (I-JS-GC). The collected data was compared to data collected for certifiedreference standards at known concentrations.
66497 ..VC
COl1:pound CAS Amount I Limit 2 RL Status--~-
Propane 74-98-6 ND 1,000 ppm 100 PASS
Isobutane 75-28-5 ND 1,000 ppm 100 PASS
Butane 106-97-8 ND 1,000 ppm 100 PASS
Methanol 67-56-1 ND 3,000 ppm 100 PASS
Pentane 109-66-0 347 ppm 5,000 ppm 100 PASS
Ethanol 64-17-5 ND 5,000 ppm 100 *Acetone 67-64-1 ND 5,000 ppm 100 PASS
Isopropanol 67-63-0 ND 5,000 ppm 100 PASSAcetonitrile 75-05-8 ND 410 ppm 100 PASSHexane 110-54-3 ND 290 ppm 100 PASSHeptane 142-82-5 ND 5,000 ppm 100 PASS---~~---.
1) ND =Not detected at a level greater than the Reporting Limit (RL).2) In ppm, based on USP recommended limits for residual solvents, adopted by the Massachusetts Department of Public Health for cannabisconcentrates and extracts on 3/31/16. Butane/Propane limits are based on limits established for state of Colorado.(*) For ethanol, as many formulations contain flavorings based on ethanol extracts of natural products, no status has been assigned.
FM-IO-tO, Rev. 1, DCN:15-00031120Fortune Blvd 0 IvWfol'di, MA 01757 0 617-221··3356
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