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TRANSCRIPT
AP - O0\
ANNUAL MONITORING REPORT
YEARfS):
n?4
STATE OF NEW MEXICO DEPARTMENT OF HEALTH
SCIENTIFlU LAPCTtATORY DIVISION P.O. Bo:; 47C0 700 Camino de Salud, NE
Albuquerque, NM 87126-S700 [505]-841-2500 WATER CHI USTRY SECTION [5051-841-2555
May 26, 1994
Request ID No. 014374
E I S n E M E E E n L J a B B E I E a i
• A ! LYriCAL REPORT 3 S 0 Aicesdon ilo. WC-94-1188 • Distribution
( J User 70320 (}J Submitter 260 (20 SLD Files
To: R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Water Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700
Re: A water,Nonpres/No sianpL i .:Lr.:» '.•> j thie 1 ."v.3tory cn March 28, 1994
_ ^I ' . iOC A I i;±C t)ATA COLLECTION " """ LOCATION
0«:25-Mar-94 By: Ols . . . • - MW-9/5 At: 10:40 hrs. In/Near: SunlardPaik
ANALYTICAL RESULTS Analvsis VHue D. Lmt. Units
calcium 2.'..00 mG/L magnesium 107.00 mG/L potassium l>.00 mG/L sodium 1440.00 mG/L bicarbonate . 712.00 mG/L carbonate 0.C0 mG/L chloride 1199.00 mG/L fl u o r i d e 0.80 mG/L sulfate 2102.00 mG/L Ion Balance 96.20 % t o t a l diss resid 5730.00 mG/L
Kcviiweu By: C. Rachael Howell 05/18/94 Analyst, Water Chemistry Section
S X \ T E OF NEW MEXICO DEPARTMENT OF HEALTH
SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE
Albuquerque, NM 87196-4700 [505] -841-2500 AIR & HEAVY METALS SECTION [5051-841-2553
May 11, 1994 I ANALYTICAL REPORT • ^ T - T ^ n • • Q£ Submitter 260
S)No.St 014373 • SLD Accession No. IC-94-0046 B « SLD Files
Distribution
R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Air & Heavy Metals Section Scientific Laboratory Div. 700 Camino de Salud, NE Albuquerque, NM 87106
A water,Nonpres/No sample submitted to this laboratory on March 28, 1994
User: NM Energy & Min - Oil Conserv. , NM
DEMOGRAPHIC DATA COLLECTION LOCATION
On: 25-Mar-94 By: Ols . . . MW-9% o At: 10:40 hrs. In/Near: Sunland Park
ANALYTICAL RESULTS in mG/L Analvsis Value Analysis Value Analvsis Value
Aluminum 1.80 Copper < 0.10 S i l v e r < 0 .10 Barium < 0.10 I r o n 13.00 Strontium 5 .70 B e r y l l i u m < 0.10 Lead < 0.10 Ti n < 0.10 Boron 1.10 Magnesium 110.00 Vanadium < 0 .10 Cadmium < 0.10 Manganese 3 .90 Zinc < 0 .10 Calcium 350.00 Molybdenum < 0.10 Mercury < 0.0005 Chromium < 0 .10 Nicke l < 0.10 Selenium < 0.0050 Cobalt < 0.05 S i l i c o n 0.80
Laboratory Remarks; ICP by method 200.7 on 4/29/94 by RAH. Mercury by method 245.1 on 4/13/94 by SD. Selenium by method 270.2 on 4/8/94 by RAH.
Reviewed By: Jim F. Ashl Supervisor,
5/11/94 & Heavy Metals Section
Al * & HEAVY METALS ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E.. ALBUQUERQUE. NM 87106
Air & Heavy Metals Section - Telephone: (505) 841-2553 31 Request
1 ID No.:
SLD No.
Date Received
DJ
_U Priority Code»
TftttyT
2JUser Code #: I 7 I 0 I 3 I 2 I 0 I
6 I County: ~
cil EID-SLD
Facility Name:
c
8 IState
Sample U 1 I _ Gf <C Location: il 1 iW i i / \~* i I I I I i i ' i ' i
raj Collected By: JLL
First 0\l\ s\Qh ILlatalt.
On: W / O ^ / >S At:l l \ Q \ 9 \ Dl hrs. Data: (YY/MM/OO) Tima: a«w.«o«
XOOwn • '300 hr*.
_njCodes: . l l l l l l I I l - l l 1 i i i l l l l
12 Latitude (DDMMSS)
I I I I I I I i m0i» in Submitter WSS # Organization Longitude (OODMMSS) I*1***
I I I I I I I N I 13 Report 14l Phone #: To: Roger Anderson (505) 827-5812
Longitude (OODMMSS) I*1*** I I I I I I I N I
Addrra
New Mexico Oi l Conservation Division i c Sampling Information: « . «. ^ G r a t J S a m p l * PurpOM: r^Pomoo«it« (Comeout*
p. n. Rox ?nas • - Complianca n - Flow Proportioned n-Chock Q. Equal Aliquot S£Monitoring Sampla Split w/Permiftea • • Spatial Q . Chain of Custody
City, SUM Zip
Santa Fe, New Mexico 87504-2088
• - Complianca n - Flow Proportioned n-Chock Q. Equal Aliquot S£Monitoring Sampla Split w/Permiftea • • Spatial Q . Chain of Custody
Data: PH: **7i i , Conductivity: 3 umhos ^2. *£~ Tamparatura: 1181 Flald Notaa/ — 1 Samnla * :
Chlorina C, RasiduaJ: mg/l, Row:
17| Sample Source: U-Stream •-Lake •-Drain •-Pool •-WWTP
^S^Well; Depth: . T>Spring •-Distribution ••Point-of-Entry •-Other
J9J Sample Type: J^-Water, Q-SoB, Q-Food, 3-Wastewater, •-Other
20| Preeervation: n-VVNF Watar f « * Praaarvad; Filtarad j&WNN Watar Not Praaarvad; Not Filtared
' • • W f Watar Praaarvad with Nitric Add (HN03); Filtarad • WPN Watar Praaarvad wtth Nitric Add; Not Filtartd ' WNL Watar Not Praaarvad in Fiald; Plaaaa Add HN03 at Lab ^ICE Watar load
a**™ —
This form accompanies a alngta sampta consisting of: / -1 liter cubitainers (1 quart)
- 4 liter cubitainers (1 gallon)
111 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required.
• - (721) SDWA Group I + other parameter(s) marked below M - (704) ICAP Scan • - (720) SDWA Group I Only
• - Aluminum • - Arsenic • - Barium • - Cadmium • - Chromium • - Cobalt • - Copper • - Iron
Remarks:
• - Lead • - Manganese
Mercury - Molybdenum - Nickel Selenium
0 - Silver • - Uranium
• -Vanadium • -Zinc • -• -• -
•-zzzzz • - Z Z Z Z • -
S L D 8 9 1 2 - H M Form Naw 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY I
"STATE OF NEW MEXICO DEPARTMENT OF HEALTH SCIENTIFIC LABORATORY DIVISION
P.O. Box 4700 700 Camino de Salud, NE « Albuquerque, NM 87196-4700 [505]-841-2500 U ORGANIC CHEMISTRY SECTION [505]-841-2570
i^ 9 4 m 8 50
Request ID No. 028742
S ANALYTICAL REPORT •
• SLD Accession No. OR-94-0915 g
Distribution QUser 70320
Submitter 260 (x) SLD Files
To: Roger Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Organic Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700
Re: A water,Purgeable sample submitted to this laboratory on March 28, 1994
DEMOGRAPHIC DATA COLLECTION LOCATION
On: 25-Mar-94 At: 12:45 hrs.
By: Ols . . . In/Near: Sunland Park
MW-11
ANALYTICAL RESULTS: Aromatic & Halogenated Purgeable [EPA-601/21 Screen (754) Parameter Value Note POL Units
Benzene 127.00 10.00 ppb Toluene 2 .40 T 10.00 ppb Ethylbenzene 1.90 T 10.00 ppb p- & m-Xylene 8 .40 T 10.00 ppb o-Xylene 3 .00 T 10.00 ppb Isopropylbenzene 15 .30 10 . 00 ppb
See Laboratory Remarks for Additional Information Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit: T = Trace (< Detection Limit); U Evidentiary Seals: Not Sealed^|
P = Compound Present, but not quantified; Compound Identity Not Confirmed. Intact: No | ~ | , Yes|~| & Broken By: Date:
Laboratory Remarks: Foamy sample; unable to achieve a lower detection l i m i t
Reported compound i d e n t i t i e s were confirmed by GC/MS
Compound Note Value PQL (ppb) n-Propylbenze 29 10 1,2,4-Trimethylbenzene T 3.2 10 sec-Butylbenzene T 6.9 10 n-Butylbenzene T 6.3 10 Naphthlene 23 .7 10 Methylene c h l o r i d e 10.9 10 1,2-Dichloroethane T 2.7 10
(Continued on page 2.)
ANALYTICAL REPORT SLD Accession No. OR-94-0915 Continuation, Page 2 of 4
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: NM SCIENTIFIC LABORATORY DIVISION N/A
mL
Lab Code: N/A Case No. Ma t r i x : ( s o i l / w a t e r ) Water Sample w t / v o l : 5.0 (g/mL)_ Level: (low/med) Low % Moisture: not dec. N/A dec. N/A E x t r a c t i o n : (SepF/Cont/Sonc) N/A GPC Cleanup: (Y/N) No pH:
SAS No, Contract: N/A
N/A SDG No. N/A
Lab Sample ID: SLD Batch NO:
OR-94-915 127
Date Received: 3/28/94 Date Extracted: N/A Date Analyzed: 4/05/94 D i l u t i o n Factor: 10 CONCENTRATION UNITS: (ug/L or ug/Kg) : ug/L
This sample was analyzed f o r the f o l l o w i n g compounds
CAS NO. COMPOUND CONC. Q POL 67-64-1 Acetone U 50.0 71-43-2 Benzene 127 10.0 108-86-1 Bromobenzene U 10.0 74-97-5 Bromochloromethane U 10.0 75-27-4 B romod i c hioromethane U 10.0 75-25-2 Bromoform U 10.0 78-93-3 2-Butanone (MEK) U 50.0 104-51-8 n-Butylbenzene 6.3 J 10.0 135-98-8 sec-Butylbenzene 6 . 9 J 10.0 98-06-6 tert-Butylbenzene U 10 .0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 50.0 56-23-5 Carbon t e t r a c h l o r i d e U 10 . 0 108-90-7 Chlorobenzene U 10 . 0 67-66-3 Chloroform U 10 . 0 95-49-8 2-Chlorotoluene U 10 . 0 106-43-4 4-Chlorotoluene U 10 .0 96-12-8 1,2-Dibromo-3-chloropropane U 10.0 124-48-1 Dibromochloromethane U 10 . 0 106-93-4 1.2-Dibromoethane U 10 .0 74-95-3 Dibromomethane U 10 . 0 95-50-1 1,2-Dichlorobenzene U 10 .0 541-73-1 1.3-Dichlorobenzene U 10.0 106-46-7 1,4-Dichlorobenzene U 10.0 75-71-8 Dichlorodifluoromethane U 10.0 75-34-3 1,1-Dichloroethane U 10.0 107-06-2 1.2-Dichloroethane 2.7 J 10.0
(Continued on page 3.)
ANALYTICAL REPORT SLD Accession No. OR-94-0915 Continuation, Page 3 of 4
75-35-4 1,1- D i c h l o r o e t h e n e U 10 . 0 156-59-4 c i s - 1 , 2 - D i c h l o r o e t h e n e U 10.0 156-60-5 t r a n s - 1 . 2 - D i c h l o r o e t h e n e U 10.0 78-87-5 1,2-Dichloropropane U 10.0 142-28-9 1,3-Dichloropropane U 10.0 590-20-7 2,2-Dichloropropane U 10.0 563-58-6 1,1-Dichloropropene U 10.0 1006-01-5 c i s - 1 . 3 - D i c h l o r o p r o p e n e U 10.0 1006-02-6 t r a n s - 1 . 3 - D i c h l o r o p r o p e n e U 10.0 100-41-4 Ethylbenzene 1.9 J 10 .0 87-68-3 Hex a c h l o r o b u t a d i e n e U 10.0 98-82-8 Isopro p y l b e n z e n e 15 .3 10.0 99-87-6 4 - l s o p r o p y l t o l u e n e U 10 . 0 75-09-2 Methylene c h l o r i d e 10.9 10.0 90-12-0 1-Methylnaphthalene U 10.0 91-57-6 2-Methylnaphthalene U 10.0 91-20-3 Naphthalene U 10.0 103-65-1 n-Propylbenzene 29 10.0 100-42-5 Styre n e U 10.0 630-20-6 1.1.1.2-Tetrachloroethane U 10.0 79-34-5 1.1.2,2-Tetrachloroethane U 10.0 127-18-4 T e t r a c h l o r o e t h e n e U 10.0 109-99-9 T e t r a h y d r o f u r a n (THF) U 50 . 0 108-88-3 Toluene 2.4 J 10 . 0 87-61-5 1,2,3-Trichlorobenzene U 10 . 0 120-82-1 1,2,4-Trichlorobenzene U 10 .0 71-55-6 1 , 1 , 1 - T r i c h l o r o e t h a n e U 10.0 79-00-5 1 , 1 , 2 - T r i c h l o r o e t h a n e U 10 . 0 79-01-6 T r i c h l o r o e t h e n e U 10 . 0 75-69-4 T r i c h l o r o f l u o r o r n e t h a n e U 10.0 96-18-4 1 , 2 , 3 - T r i c h l o r o p r o p a n e U 10.0 95-63-6 1,2,4-Trimethylbenzene 3.2 J 10 . 0 108-67-8 1,3,5-Trimethylbenzene u 10.0 75-01-4 V i n y l c h l o r i d e u 10.0 95-47-6 o-Xylene 3 J 10.0 N/A p- & m-Xylene 8.4 J 10.0 N/A T o t a l Xylenes 11.4 J 20.0
* CONC = CONCENTRAION DETERMINED PQL = Practical Quantitation Limit (Approximately 10 times MDL)
* Q = Q u a l i f i e r D e f i n i t i o n s :
(Continued on page 4.)
ANALYTICAL REPORT SLD Accession No. OR-94-0915 Continuation, Page 4 of 4
B - I n d i c a t e s compound was detected i n the Lab Blank as w e l l as i n the sample.
D - I n d i c a t e s value taken from a secondary ( d i l u t e d ) sample a n a l y s i s . E - I n d i c a t e s compound concentration exceeded the range of the
standard curve. J - I n d i c a t e s an estimated value f o r t e n t a t i v e l y i d e n t i f i e d compounds,
or f o r compounds detected and i d e n t i f i e d but present a t a conc e n t r a t i o n less than the q u a n t i t a t i o n l i m i t .
N - I n d i c a t e s t h a t more than one peak was used f o r q u a n t i t a t i o n . U - I n d i c a t e s compound was analyzed f o r , but not detected above the
con c e n t r a t i o n l i s t e d ( Q u a n t i t a t i o n L i m i t ) .
QUALITY CONTROL SUMMARY FOR VOLATILES SCREEN
METHOD BLANK: A l a b o r a t o r y method blank was analyzed along w i t h t h i s sample t o assure the absence of i n t e r f e r i n g contaminants from l a b reagents, instruments, or the general l a b o r a t o r y environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported d e t e c t i o n l i m i t .
COMPOUND DETECTED No Compounds Detected
CONCENTRATION (PPB)
SURROGATE RECOVERIES: SURROGATE
Bromofluorobenzene 2 -Bromo-1-chloropropane
CONCENTRATION 25.0 ppb 25.0 ppb
RECOVERY 95.6 90.8
SPIKE RECOVERY: The % recoveries f o r compounds i n the batch spike were from 80% t o 120% w i t h the exception of the compounds l i s t e d below: COMPOUND CONCENTRATION % RECOVERY
No exceptions . ppb
Analyst: Patrick F. Analyst, Organic Chemistry
Reviewed By: 5k Richard F. Meyerhein 05/04/94 Supervisor, Organic Chemistry Section
ORGANIC CHEMISTRY ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION 700 CAMINO OE SALUD N.E.. ALBUQUERQUE, NM 87106
Organic Chemistry Section - Telephone. (505) 841-2S70 I3J Request User
Code* I 7 i a i 3 ; 2 | 0 i
Name? S f r J d z J i ^ ^ I t r
IDNc
^quest ID No.
IIIII IIII III 028742-C
SLD No.
Oate Received
ij&eUnty:
J J Priority Code#:
M i ( W f o r T . cwBO>SLD
7--^JSample Location;
ipJCollected By:
i i i I I I L J I L J I L
Rrat ILIaUlt... On: W / O J / Z T " At:I / I ^ ^iJThrs
Data: (W/MM/OO)
Latitude (DOMMSS)
, 1 „L ' j 1 1
Longitude (DOOMMSS)
< I » '» I I
11 (Codes:
Submitter J I L
13| Report" To: Roger Anders.on
WSS # - I I I I 1.1
Orgai nizatlon
MdiM*
141 Phone* ^ (505) 827-5812
New Mexico Oi l Conservation Division
City, SUM Z * P. 0. Prrc ?naa Santa Fe, New ffexico 87504-2088
^ D a t a : P H : 7 ' ^ ' Conductivity: umhoa® 7 / ' / *fc
12 i_J 2 0lgrtlO
UU Sample Purpoaa
• - Complianoa "-Chack
Storing Spacial
:TJ-o
S'toonitoring bj£ fFSpacial T f .
Sampling Information Grab Compoaita Q- Row Proportion* ff- Equal Aliquot
• samp pla Split w/Parmittaa Chain ot Cmtody
18|FlaWNotoa7 Tamparatura:
Chlorina C, Raaidual: mg/l, Row.
17| Sample Source •-Stream G-Lake •-Drain •-Pool •-WWTP
K-Well; Depth: . MJ-Spring
•-Distribution •-Point-of-Entry •-Other
U*((- MLHl
19J Sample Type: ^Water, Q-Soi Q-Food, 201 Pre—rvatton; 1 Q-NP No PraaarvHon; Sampla atorad at room tamparatura
Tglp-loa SampJa atorad in an tea bain (Not Prown) P-TS Sampla Praaarvad with Sodium TWoautfata to ramova chlorina rasiduai
•-P-HOJ SlJT^f^aaMvadwrmHydrecMorto jgC-Ottar ^ < f f _
• -Wastewater, TJ -Other, This form accompanies a alngta «ampl« consisting of:
>— septum vial(s) (volume - 7t> * I ) - glass jugs (volume - ) - (volume • )
211 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s) required. Whenever possible, list specific compounds suspected or required.
Volatile Screens; (753) Aliphatic Headspace (1 -5 Carbons) (754) Aromatic & Halogenated Purgeables (EPA 601 & 602)
j • (765) Mass Spectrometer Purgeables (EPA 624) • - (766) SDWATotaJ Trirjalwnethanes (EPA 501.1) Q - (774) SDWA VOCs I (8 Regulated +1 (EPA 502.2) • - (775) SDWA VOCs II [EDB & DBCP] (EPA 504)
g Other Specific Compounds or Classes:
• - ( )
SI j = Remarks:
SemivQlatile Screens; - (763) Acid Extractables - (751) Aliphatic Hydrocarbons - (755) Base/Neutral Extractables (EPA 625) - (756) Base/Neutral/Acid Extractables (EPA 8270) • (758) Herbicides, Chlorophenoxy Acid • (759) Herbicides, Triazines - (760) Organochlorine Pesticides • (761) Organophosphate Pesticides - (767) Polychlorinated Biphenyls (PCB's) - (764) Polynuclear Aromatic Hydrocarbons • (762) SDWA Pesticides & Herbicides
SLD8912-QR torn Naw 12/se This Form WBI NOT Be Returned With Your Results. Please RETAIN A COPYI
STATE OF NEW MEXICO DEPARTMENT OF HEALTH
* SCIENTIFIC LABORATORY DIVISION P.O. Box 47C0 700 Camino de Salud, NE
Albuquerque, NM 87196-4700 [505]-841-2500 WATZR CHEMISTRY SECTION [505]-841-2555
May 26, 1994
Request ID No. 028744
H K B E C l a E E E a a r S C B C r a H H B H M H H M H U I
\ /*JA TICAL REPORT \ * U ccisaij" fJo. WC-94-1191 m
Distribution QUser 70320
Submitter 260 (x) SLD Files
To: R. Anderson From: Water Chemistry Section NM Oil Consv. Div. Scientific Laboratory Div. State Land Office Bldg. 700 Camino de Salud, N.E. P.O. Box 2088 P.O. Box 4700 Santa Fe, NM 87504-2088 Albuquerque, NM 87196-4700
Re: A water,Nonpres/No sample submitted to tlar laboratory on March 28, 1994
DEMOGRAPHIC DAIA COLLECTION LOCATION
On: 25-Mar-94 By: Ols . . . V , MW-11 At: 12:45 hrs. In/Near: Sunlau! Prrl-
ANALYTICAL RESULTS Analvsis _ Value D. Lmt. Units
calcium 50.00 mG/L magnesium 60.00 mG/L potassium 15.00 mG/L sodium 1120.00 mG/L bicarbonate 1756.00 mG/L carbonate ' '0.00 mG/L chloride 863.00 mG/L fl u o r i d e 2.80 mG/L sulfate 3.80 mG/L Ion Balance U 6 . J % t o t a l diss ret i d 3798.00 mG/L
Reviewed By: C. Rachael Howell 05/18/94 Analyst, Water Chemistry Section
WATER CHEMISTRY ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION - 700 CAMINO DE SALUD. ALBUQUERQUE. NM 87106
Water Chemistry Section • Telephone: (505) 841 -2555
SLO No.
Date Received
E T
UJ
LlUser Code*: ' 7»° <2 '2 '° '
31 Request ^ I D No.:
PUcm Form O StieaatHwt
5 Facility Name:
6 I County:
Priority Code #:
pr i -or T . c*il EiO-SLO Coordinanr)
TJCTtyy / fl 8 [State
MM. - ^ S a m p l e U T . _ ) /
Location: IPMIIA/I I l \ I i i i i ' i ' J I L J I I L lOlCollected*/ T I
By: Utlll^ First | 3 (Oh
ILIalal t . On: ? < / / & 3 / ^ At:l / 1>1 V1 J> I hrs.
Data: (YY/MM/OO) ~ Tim*' 2 4 •"• c l o c*
rycodes: .1 1 I I I 1 1 1 1 " 1 1 1 I I I I I I I
12| Latitude (DDMMS.S)
I I I I I I I o ni0i« in Submitter WSS # Organization Longitude (DOOMMSS) <•!<••*•*
I I I I I I I II I I 131 Report To:
Nam*
Roger AAderson 14 Phone # : — 1 (305) C27-5S12
Longitude (DOOMMSS) <•!<••*•* I I I I I I I II I I
New Mexico O i l C o n s e r v a t i o n D i v i s i o n i c i Sampling information:
XT- Grab Sampla Purpoaa: 1ft. Compoarta g°"5°—
• - Compiianca r> Flow Proportioned n-Chaek r j - Equal Aliquot
JKfrMonrtoring Sampla Split w/Parmittee LTSpacial Q. Chain ot Custody
P. 0. 2088
i c i Sampling information: XT- Grab
Sampla Purpoaa: 1ft. Compoarta g°"5°— • - Compiianca r> Flow Proportioned n-Chaek r j - Equal Aliquot
JKfrMonrtoring Sampla Split w/Parmittee LTSpacial Q. Chain ot Custody
City, SUM Zip Santa F e , New Mexico 87504-•2088
i c i Sampling information: XT- Grab
Sampla Purpoaa: 1ft. Compoarta g°"5°— • - Compiianca r> Flow Proportioned n-Chaek r j - Equal Aliquot
JKfrMonrtoring Sampla Split w/Parmittee LTSpacial Q. Chain ot Custody
•^Data: PH: ~7*(?2-< Conductivity: U^j
17| Sample Source: •-Stream •-Lake •-Drain G-Pool ••WWTP
I9j Sample Type:^-WatBr, • -Wastewater, Q-Other_
2 / i i _ * j & Tamparatura: 2— umhoa i
18| Plaid Notaa/ Sampla # :
Chlorina C. Rasiduai: mg/), Row:
forVell; Depth: '•-Spring •-Distribution •-Point-of-Entry •-Other
tn~j* Uf.ll MUTU
20| Preservation: 1 — 0 - V M F Watar Not Praaarvad; Hltarad
^ W N N Watar Not Praaarvad; Not Rltarad Q- WPF Watar Praaarvad with Sulfuric Add (H2S04); Rltarad • - W P N Watar Praaarvad with Sulfuric Add: Not Rltarad Q-WNU Watar Not Praaarvad in Fiatd; Plaaaa Add H2S04 at Lab
ICE Watar lead Othar
• -So* . •-Food,
This form accompanies a single sampla consisting of: / -1 liter cubitainers (1 quart)
- 4 liter cubitainers (1 gallon)
2iJ Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required. Group AnaJyaaa: • - (854) SDWA Group II (Nitrate as N) • • (861) SDWA Group ill (Fluoride) • • (860) SDWA Complete Secondary
Q (859) SWQB SS Anion • Cation Group + O (868) SWQB NPS Anion, Cation, Physical + TSS Q (869) SWQB Nutrient Analysis Group +
^(867) Major Anions & Cations
Cations: • - Calcium (as Ca) • - Magnesium (asMg) ~ •-Potassium (as rQ ~ •-Sodium (as Na) " • - Total Hardness (as CaC03)~ Anions: • - Alkalinity (as CaC03) • - Bicarbonate (as HC03) • - Carbonate (as COS) ~ •-Chloride (as CQ •-Fluoride (as F) • - Sulfate (as S04) "
Ion Charge Balance
Remarks:
Phys ica l Parameters: •-Color •- Conductance <mcnit*>e»9nQ •-Odor • - P H ••Surfactants • - Total Dissolved Solids •-Turbidity O t h a r • -
o-• -• -
Surfaca and Waste Watar: • - Biological Oxygen Demand ••Total Suspended Solids • - Chemical Oxygen Demand • - Total Organic Carbon • • Cyanide Nutrients: • - Nitrate + Nitrite (as N) • - Ammonia (as N) •-Total Kjeldahl (as N) • - Nitrite (as N) • - Orthophosphate (as P) • - Total Phosphorus (as P)
S L D 8 9 1 2 - W C Form Maw 12/89 This Form WSJ NOT Be Returned With Your Results. Please RETAIN A COPYI
STATE OF NEW MEXICO . . . f DEPARTMENT OF HEALTH
SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE
Albuquerque, NM 87196-4700 [505]-841-2500 AIR & HEAVY METALS SECTION [505]-841-2553
August 12, 1994
Request ID No. 028743
ANALYTICAL REPORT | SLD Accession No. IC-94-0049 \
• Distribution (JUser 70320
Submitter 260 (20 SLD Files
To: R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Air & Heavy Metals Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700
Re: A wat not preserved sample submitted to this laboratory on March 28, 1994
DEMOGRAPHIC DATA COLLECTION LOCATION
On: 25-Mar-94 At: 12:45 hrs.
By: Ols . . . In/Near: Sunland Park
MW-11
ANALYTICAL RESULTS in mG/L Analvsis Value Analvsis Value Analvsis Value
Aluminum 12.00 Copper < 0.10 S i l v e r < 0.10 Barium 1.30 I r o n 15.00 S t r o n t i u m 3.20 B e r y l l i u m < 0.10 Lead < 0.10 T i n < 0.10 Boron 1.40 Magnesium 72.00 Vanadium < 0.10 Cadmium < 0.10 Manganese 0.89 Zinc < 0.10 Calcium 120.00 Molybdenum < 0.10 Mercury < 0.0005 Chromium < 0.10 N i c k e l < 0.10 Selenium < 0.0050 Cobal t < 0.05 S i l i c o n 10.00
Laboratory Remarks: Acidified and Digested at SLD ICP by method 200.7 on 7/27/94 by RAH. Mercury by method 245.1 on 4/13/94 by SD. Selenium by method 270.1 on 4/8/94 by RAH.
Reviewed By: JimF. Ashby 08/11/94 Supervisor, Air & Heavy Metals Section
AIR & HEAVY METALS ANALYTICAL REQUEST FORM
' V, SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E.. ALBUQUERQUE. NM 87106
Air & Heavy Metals Section - Telephone: (505) 841 -2553
SLD No.
Date Received:
User Code #: I 7 I 0 13 I 2 I 0 I
Request ID No.:
Plan Form C Priority Code #: <3> [ K ' l ' O l T .
c«iiSO-SL3
^NameT firJJ+J. ( f ^ i Z
-iisamDie Kil I / i I / Sampie K/1 I / / / Location: I/V{I1A/I \ l\ I i
6J County:
arm J I L J L _ L J I L
jOj Collected By: QdlllML
LkJJiiiL On: 9 9 / 0 3 ! ^ At:l / l ^ l / i f l h r s .
' Data: (YY/MM/DD)
T2I Latitude (DDMMSS) XOO om - 1500 hn.
111Codes:
Submitter J I I I " I L
wss# 13J Report
TO: Roger Anderson
OrganizatTorT 14 Phone #: — 1 (505) 827-5812
New Mexico Oil Conservation Division
City, SUM Zip
Santa Fe, New Mexico 87504-2088 Data: P H : *7» > 2- • Conductivity: ^ / ^ 2^ umho« ® ^ / , | Temparatura:
17J Sample Source: ' l ^ s a S f f a T '
Longitude (DODMMSS)
i I I '» I •
2 Digit IO
•icl Sampling Information:
Sampla Purpoaa: composita ! w ? « w • - Complianca H- Row Proportioned'
^n^Chack r j - Equal Aliquot Monitoring jsjr: Sampla Split w/Permirtee
••Spacial • • Chain of Custody Chlorina
C. Residual: mg/l, Row:
17| Sample Source: i_i-Stream G-Lake C-Drain G-Pool ---WWTP
^-Well; Depth: •-Spring •-Distribution •-Point-of-Entry •-Other:
MUb~ UII ML/-11
19] Sample Type: pa Water, -Wastewater, •-Other_
• -SoU. •-Food, 20
This form accompanies a single sample consisting of: -1 liter cubitainers (1 quart) - 4 liter cubitainers (1 gallon)
Preservation: • - WMF Watar Not Praaarvad; Rltarad
Watar Not Praaarvad; Not Rltarad Watar Praaarvad with Nitric Acid (HN03); Rltarad Watar Praaarvad wtth Nitric Add; Not Rltarad Watar Not Praaarvad in Raid; Plaaaa Add HN03 at Ub Watar toad
Q W N N • - W P F • - W P N
' Q J Othar.
211 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required.
(704) ICAP Scan (720) SDWA Group I Only
• - Aluminum • - Arsenic • - Barium • - Cadmium • - Chromium • - Cobalt • - Copper • - Iron
• - (721) SDWA Group I + other parameters) marked below
• -Lead •-Manganese ]Er Mercury • - Molybdenum • - Nickel
Selenium • -Silver • - Uranium
• - Vanadium • -Zinc • -• -• -• -• -• -
Remarks:
S L D 8 9 1 2 - H M Form Naw 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI
AIR & HEAVY M E T A L S ANALYT ICAL R E Q U E S T FORM
' ~* SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E., ALBUQUERQUE. NM 87106
Air & Heavy Metals Section - Telephone: (505) 841 -2553
SLD No.
Date Received: _U Priority
Code#: JJUser
Code *: l 7 I 0 I 3 I 2 | 0 | 31 Request
ID No.: PtaoaFormQ SMcMrrMr*
[t "l" oi "3" can EiD-SLC Coorainaior
TJCTtyT ~ ~ iSJStat
SJJ Perl Wlt 5 Facility
Name: ML f 6 County
/ffu - i J Sample K/i \ f _ 1 r
Location: I Tli W| i J>i ° i J L_J I I I—L
10 Collected By: u;llr<
First I P i l \ J \ O n On: ' 1 0 1 1 2 ^ At:l / \ 2 - \ O \ 0 1 hrs
| L | « f i t 'Date: (YY/MM/DD) Time: ^ l 1 " : ? ^ . -100om • I9O0nn.
Tf] Latitude (DDMMSSI
I I I I I I I 2 Digit ID
Longitude (OOOMMSS)
I I I 'I
111Codes:
J . l . l I Submitter WSS# Organization
13 Report To: Roger Anderson
14] Phone #: l~ 1 (505) 827-5812
New Mexico Oil Conservation Division
City, Slate Zip P. n. Rnv ?naa
Santa Fe_ New Mexico 87504-2088 — Data: P H : * 7 > 1 • Conductivity: 3 4> umhos ® T J '^""Temperature:
Sampla Purpoaa: • • Complianca
fc—Ttpling Information:
Grab Composite (Como
H- Check „ • Monitoring •-Special
f j - Row Proponioned v J j - Equal Aliquot .^f^&mple Split w/Permittee
G • Chain of Custody
181 Field Notee/ 1 Samala *:
Chlorine C, Residual: mg/l, Row:
17| Sample Source: •-Stream •-Lake •-Drain •-Pool n-WWTP
jS^Well; Depth: /U-Spring
J-Distribution •-Point-of-Entry •-Other
JL r Ul ML/- Is
19j Sample Type: Ijgj-Water, 2 -Wastewater, •-Other,
• -Soi. •-Food,
This form accompanies a single sampla consisting of: JK~ -1 liter cubitainers (1 quart)
- 4 liter cubitainers (1 gallon)
20| Preservation: ' — • - W N F Watar Not Praaarvad; Rltered
Water Not Praaarvad; Not Rltered Watar Praaarvad with Nitric Acid (HN03); Rltered Watar Praaarvad wtth Nitric Add; Not Rltered Watar Not Praaarvad in Raid; Please Add HN03 at Lab Watar load
n-WNN • - W P F • - W P N
^ W N L
Othar.
211 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required.
- (704) ICAP Scan -(720) SDWA Group I Only
• - Aluminum • - Arsenic • - Barium • - Cadmium • - Chromium • - Cobalt • - Copper • - Iron
• - >J21) SDWA Group I + other parameters) marked below
• -Lead • -Manganese J2[- Mercury • - Molybdenum n - Nickel M: Selenium
"LT'• Silver • - Uranium
• - Vanadium • - Zinc • -
• -• -• -• -
Remarks:
S L D 8912-HM Form New 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI
""STATE OF NEW MEXICO DEPARTMENT OF HEALTH
SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE
- C , o L , : : Altaquerque, NM 87196-4700 [505]-841-2500 il l . . l ORGANIC CHEMISTRY SECTION [505]-841-2570
-May4, 1994^ 8 50
Request ID No. 014378
g ANALYTICAL REPORT • • SLD Accession No. OR-94-0916 £
Distribution QUser 70320 Q$ Submitter 260 (x) SLD Files
To: Roger Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Organic Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, NE Albuquerque, NM 87106
Re: A water,Purgeable sample submitted to this laboratory on March 28, 1994
DEMOGRAPHIC DATA COLLECTION LOCATION
On: 25-Mar-94 At: 12:00 hrs.
By: Ols . . . In/Near: Sunland Park
MW-33
ANALYTICAL RESULTS: Parameter
Aromatic & Halogenated Purgeable [EPA-601/21 Screen {754} Value Note POL Units
0.00 Additional
N 10 Information
00 EPA 601/2 V o l a t i l e s (60) See Laboratory Remarks fo r
Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit; P = Compound Present, but not quantified; T = Trace (< Detection Limit); U = Compound Identity Not Confirmed. Evidentiary Seals: Not Sealed^; Intact: No | ~ | , Yes|~| & Broken By:
Laboratory Remarks:
ppb
Date:
Late e l u t i n g compound confirmed by GC/MS as Octanal, aldehyde.
a C8
This sample was f i r s t analyzed on 4/5/94 and the a n a l y t i c a l results were judged unacceptable by the analyst. The sample was re-analyzed on 4/6/94 y i e l d i n g the results on t h i s form.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: NM SCIENTIFIC LABORATORY DIVISION C o n t r a c t : N/A Lab Code: N/A Case No. : N/A SAS No. : N/A SDG No.:.
Water (g/mL) mL
Matrix: ( s o i l / w a t e r ) _ Sample wt/vol: 5.0 Level: (low/med) Low % Moisture: not dec. N/A Extraction: (SepF/Cont/Sonc) GPC Cleanup: (Y/N) No pH:
N/A
dec. N/A
Lab Sample ID: SLD Batch No:
OR-94-916 127
N/A
Date Received: 3/28/94 Date Extracted: N/A Date Analyzed: 4/05/94 D i l u t i o n Factor: 10 CONCENTRATION UNITS:
(Continued on page 2.)
ANALYTICAL REPORT SLD Accession No. OR-94-0916 Continuation, Page 2 of 4
(ug/L or ug/Kg) : uq/L
This sample was analyzed for the following compounds using EPA Methods 601 & 602
CAS NO. COMPOUND CONC. 0 POL 67-64-1 Acetone U 50.0 71-43-2 Benzene U 10.0 108-86-1 Bromobenzene U 10 .0 74-97-5 B romo c hioromethane U 10.0 75-27-4 Bromodichloromethane U 10.0 75-25-2 Bromoform U 10 . 0 78-93-3 2-Butanone (MEK) U 50.0 104-51-8 n-Butylbenzene U 10.0 135-98-8 sec-Butylbenzene U 10.0 98-06-6 tert-Butylbenzene U 10 . 0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 50 . 0 56-23-5 Carbon t e t r a c h l o r i d e U 10 .0 108-90-7 Chlorobenzene U 10.0 67-66-3 Chloroform U 10.0 95-49-8 2-Chlorotoluene U 10.0 106-43-4 4-Chlorotoluene U 10.0 96-12-8 1.2-Dibromo-3-chloropropane U 10 . 0 124-48-1 Dibromochloromethane U 10 . 0 106-93-4 1,2-Dibromoethane U 10 .0 74-95-3 Dibromomethane u 10.0 95-50-1 1,2-Dichlorobenzene u 10.0 541-73-1 1,3-Dichlorobenzene u 10.0 106-46-7 1,4-Dichlorobenzene u 10.0 75-71-8 Dichlorodifluoromethane u 10.0 75-34-3 1.1-Dichloroethane u 10 . 0 107-06-2 1.2-Dichloroethane u 10 . 0 75-35-4 1.1-Dichloroethene u 10 .0 156-59-4 cis-1,2-Dichloroethene u 10.0 156-60-5 trans-1,2-Dichloroethene u 10.0 78-87-5 1,2-Dichloropropane u 10.0 142-28-9 1,3-Dichloropropane u 10.0 590-20-7 2,2-Dichloropropane u 10 . 0 563-58-6 1,1-Dichloropropene u 10.0 1006-01-5 cis-1,3-Dichloropropene u 10.0 1006-02-6 trans-1,3-Dichloropropene u 10.0 100-41-4 Ethylbenzene u 10.0 87-68-3 Hexachlorobutadiene u 10.0
(Continued on page 3.)
ANALYTICAL REPORT SLD Accession No. OR-94-0916 Continuation, Page 3 of 4
98-82-8 I s opropylbenz ene U 10.0 99-87-6 4-Isopropyltoluene U 10 .0 75-09-2 Methylene c h l o r i d e U 10 . 0 90-12-0 1-Methylnaphthalene U 10.0 91-57-6 2-Methylnaphthalene U 10 . 0 91-20-3 Naphthalene U 10 . 0 103-65-1 n-Propylbenzene U 10 .0 100-42-5 Styrene U 10.0 630-20-6 1,1,1.2-Tetrachloroethane U 10.0 79-34-5 1,1,2,2-Tetrachloroethane U 10.0 127-18-4 Tetrachloroethene U 10.0 109-99-9 Tetrahydrofuran (THF) U 50.0 108-88-3 Toluene U 10.0 87-61-5 1,2,3-Trichlorobenzene U 10.0 120-82-1 1,2,4-Trichlorobenzene U 10.0 71-55-6 1,1,1-Trichloroethane U 10 . 0 79-00-5 1,1,2-Trichloroethane U 10 . 0 79-01-6 Trichloroethene U 10.0 75-69-4 Trichlorofluorornethane U 10 . 0 96-18-4 1,2,3-Trichloropropane U 10.0 95-63-6 1,2,4-Trimethylbenzene U 10.0 108-67-8 1,3,5-Trimethylbenzene U 10.0 75-01-4 V i n y l c h l o r i d e U 10 . 0 95-47-6 o-Xylene u 10 . 0 N/A p- & m-Xylene u 10.0 N/A To t a l Xylenes u 20.0
TENTATIVELY IDENTIFIED COMPOUNDS DATA SHEET
The following compounds were t e n t a t i v e l y i d e n t i f i e d by Mass Spec: CAS NO. I COMPOUND I MATCH I RT I EST. CONC. I 0 124-13-0 octanal 974 19 . 97
* CONC = CONCENTRAION DETERMINED PQL = Practical Quantitation Limit (Approximately 10 times MDL)
* Q = Q u a l i f i e r D e f i n i t i o n s : B - Indicates compound was detected i n the Lab Blank as well
as i n the sample. D - Indicates value taken from a secondary (diluted) sample analysi E - Indicates compound concentration exceeded the range of the
standard curve.
(Continued on page 4.)
ANALYTICAL REPORT SLD Accession No. OR-94-0916 Continuation, Page 4 of 4
J - Indicates an estimated value for t e n t a t i v e l y i d e n t i f i e d compounds, or f o r compounds detected and i d e n t i f i e d but present at a concentration less than the quantitation l i m i t .
N - Indicates that more than one peak was used f o r quantitation. U - Indicates compound was analyzed f o r , but not detected above the
concentration l i s t e d (Quantitation L i m i t ) .
QUALITY CONTROL SUMMARY FOR VOLATILES SCREEN
METHOD BLANK: A laboratory method blank was analyzed along with t h i s sample to assure the absence of i n t e r f e r i n g contaminants from lab reagents, instruments, or the general laboratory environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported detection l i m i t .
COMPOUND DETECTED No Compounds Detected
CONCENTRATION (PPB)
SURROGATE RECOVERIES: SURROGATE
Bromofluorobenzene 2 -Bromo-1-chloropropane
CONCENTRATION 25.0 ppb 25.0 ppb
RECOVERY 97.2
101.0
SPIKE RECOVERY: The % recoveries f o r compounds i n the batch spike were from 80% to 120% with the exception of the compounds l i s t e d below: COMPOUND CONCENTRATION % RECOVERY
No exceptions . ppb
Analyst: Patrick F. Basile Analyst, Organic Chemistry
Reviewed By: Richard F. Meyerhein 05/04/94 Supervisor, Organic Chemistry Section
ORGANIC CHEMISTRY ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E.. ALBUQUERQUE. NM 87106
Organic Chemistry Section • Telephone: (505) 841-2570
rn JjFacHrty
Name:
-^J Sample Location:
2jUser C o d e *
31 Request ID No.:
Request ID No.
111 ii un tn 014378-C
SLD No.
Date Received _U Priority
Code# unty:
MM 0916 C
(**'-<wT.
lJ fil M •M.U-3,5 J I L ' 1 I I L ' ' ' ' ' I I L ' i ' i '
ipJCollected
Hntt IM>t«|t-On: 1 < / / Q 3 / X T At:l / t^OlOlhrs
Oata: (YY/MM/OO) " "
iJJCodes: Tim*- 2 4 * e"901
3.-00flrti . I50QWH. T2I Latitude (DOMMSS)
I A 'l I I Longitude (DDDMMSS;
I » 1 '» I I I 11
J . I . I I L _ L Submitter W S S #
J I L
13J Report To: Roger Anders.on
Organization 141 Phone #:
(505) 827-5812 New Mexico Oil Conservation Division
Diy, SUM Zip P. n. Bnv ?naa Santa Fe, New Mexico 87504-2088
• ^ D a t a : P H : *7»"7 . Conductivity. ~73£> umhoa® Tamparatura: e« i_ c> 11 al Raid NotM/
2 Digit IO
ipllng Information:
Sampla Purpoaar^ Compoaita &T££n •-Complianoa Q- Row Proportional ^
Chadt Equal Aliquot Monitoring >g. Sampla Split w/Parmittaa SpaciaJ >Q. Chain of Cuttody
| 1 8 | Plaid No»a/
, Chlorina C. Aasidual: mg/l, Flow:
171 Sample Source •-Stream •-Lake •-Drain •-Pool •-WWTP
Sf-Well; Depth: ^D-Spring
•-Distribution •-Point-of-Entry •-Other. _____
19J Sample Type: M-•-Wastewater, J \ 2 -This form accompanies a -Intfa aamplq consisting of. ____- septum vial(s) (volume » VO r+\ )
- glass jugs (volume • )
20|Prea ervatlon: '"""• Q-NP No Praaarvttion; Sampla atorad at room tamparatura
]lg~P-loa Sampla atorad in an ica bath (Not Froxan) L^P-TS Samp- Praaarvad with Sodium Thtoautfata to ramova chlorina ratidual fT-P-HCl Sampla Praaarvad with Hydrochloric Add (2 dropa/40 ml) fi-Ofter Tr OT I I
-Water, -Other.
• -Soi •-Food,
(volume J _U Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s)
required. Whenever possible, list specific compounds suspected or required.
t l • • • • • • • •
Volatile Screens: (753) Aliphatic Headspace (1-5 Carbons)
i (754) Aromatic & Halogenated Purgeables (EPA 601 & 602) ' (765) Mass Spectrometer Purgeables (EPA 624) (766) SDWA Total Trihalomethanes (EPA 501.1) (774) SDWA VOCs f [8 Regulated +] (EPA 502.2) (775) SDWA VOCs II [EDB & DBCP] (EPA 504)
Other Specific Compounds or C l a s s y
(
Semiv.latile Screens; • - (763) Acid Extractables ~| - (751) Aliphatic Hydrocarbons •-(755) Base/Neutral Extractables (EPA 625) • • (756) Base/Neutral/Acid Extractables (EPA 8270)
8- (758) Herbicides. CNorophenoxy Acid • (759) Herbicides, Triazines
• - (760) Organochlorine Pesticides
S- (761) Organophosphate Pesticides - (767) Polychlorinated Biphenyls (PCB's)
•-(764) Polynuclear Aromatic Hydrocarbons • - (762) SOWA Pesticides & Herbicides
Remarks:
SLD 8912-OR Form Naw i2/8» This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY! I
STATE OF NEW MEXICO DEPARTMENT OF HEALTH
SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE
Albuquerque, NM 87196-4700 [505]-841-2500 WATER CHEMISTRY SECTION [505]-841-2555
June 2, 1994
Request ID No. 028741
\ ANALYTICAL REPORT • \ SLD Accession No. WC-94-1190 \
Distribution QUser 70320 (JJ Submitter 260 (x) SLD Files
To: R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Water Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700
Re: A water,Nonpres/No sample submitted to this laboratory on March 28, 1994
DEMOGRAPHIC DATA COLLECTION LOCATION
On: 25-Mar-94 By: Ols .. . MW-3X C At: 12:00 hrs. In/Near: Sunland Park
ANALYTICAL RESULTS Analvsis Value D. Lmt. Units
calcium 139.00 mG/L magnesium 67.30 mG/L potassium 11.00 mG/L sodium 1430.00 mG/L bicarbonate 692.00 mG/L carbonate 0.00 mG/L chloride 1659.00 mG/L fl u o r i d e 1.30 mG/L sulfate 745.00 mG/L Ion Balance 102.00 % t o t a l diss resid 4424.00 mG/L
Reviewed By: C. Rachael Howell 05/18/94 Analyst, Water Chemistry Section
WATER CHEMISTRY ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD, ALBUQUERQUE, NM 87106 Water Chemistry Section - Telephone: (505) 841 -2555
SLD No.
Date Received:
2 User Code*: I 7 I ° >3 I 2 l° I
Request ID No.:
P _ » F o r m O StiexrHa—
41 Priority Code#: ,3
[If "I-or T . call EIO-SLC Coordinator'
5 Facility Name:
__J3ounty: , 8 IState
j M j ! --i Sample
Location: •M.l/.-l3,J, J I l _J I I—L J I L ipJCollected
Firtt On:
TUala l t .
q y / O l l * T At-.l / l ^ l Q\Q I Oate: (YY/MM/OO) Tima: * 4 h ' e , ° "
3.-00 O— • 1500 riri.
hrs. (YY/MM/OO)
Latitude (DDMMSS)
'l I 1 11(Codes:
J . l . l I I I I I ' l Submitter WSS #
13 Report To:
Nam*
Roger AAderson
I •! I. I I Organization
14) Phone #: 1—' (505) C27-5C12
Add~a :aw Mexico Oil Conservation Division
P. 0. 2088 City, SUM Zip
Santa Fe, New Mexico 87504-2088
J I Longitude (DOOMMSSJ
I I *l I I
2 Digit ID (Hr
i c | ^Sampling Information:
Sampla Purpoaa: "fj j . Compoaita E^ I • - Complianoa n - Flow Proportioned' n-Chaek ff- Equal Aliquot 63: Monitoring £T. Sampla Split w/Permittea • - S p a d a l • • Chain ot Custody
16| Field <-) —) < ~ l n / /,"<=> . . Chlorina — D a t a : P H : / • / .Conductivity: / J f , umhoa@6wV7 FT Tamparatura: C, Rasidual: mg/l, Flow: 17 Sample Source:
"~H C t r a a m Nr~I^AA/«_ll• n a n M i *
18 Plaid Notaa/ — 'Samnla * : /
, i-o ir earn Pypweii. UBLTUI. •-Lake -LPSprlng •-Drsn •-Distribution G-F •-Point-of-Entry n-W. sTP n-Other
, i-o ir earn Pypweii. UBLTUI. •-Lake -LPSprlng •-Drsn •-Distribution G-F •-Point-of-Entry n-W. sTP n-Other
, i-o ir earn Pypweii. UBLTUI. •-Lake -LPSprlng •-Drsn •-Distribution G-F •-Point-of-Entry n-W. sTP n-Other
19 Sample Type: JSrWater, • -Soil, • -Food, n -Wastewater. (~l -Other This form accompanies a single sampla consisting or.
I • 1 liter cubitainers (1 quart) • 4 liter cubitainers (1 gallon)
20| Preservation: — n-Wrtf Watar Not Praaarvad; Rltarad
§ fWNN Watar Not Praaarvad; Not RKarad • • WPF Wktar Praaarvad with Sulfuric Add (H2S04); Filtarad •-WPN Watar Praaarvad wtth Sulfuric Add; NotFlltarad •-WNL Watar Not Praaarvad in Flald;Plaaaa Add H2S04 at Ub 50-ICE Watar toad
211 Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required. Group Analysts; Q (859) SWQB SS Anion - Cation Group + • • (854) SDWA Group II (Nitrate as N) Q- (868) SWQB NPS Anion, Cation, Physical + TSS • - (861) SDWA Group III (Fluoride) Q- (869) SWQB Nutrient Analysis Group + • - (860) SDWA Comptete Secondary r E £ (867) Major Anions & Cations
Cations; • • Calcium (as Ca) • - Magnesium (as Mg) " • - Potassium (as K) [ • - Sodium (as Na) [ • - Total Hardness (as CaC03)~ Anions; • - Alkalinity (as CaC03) • - Bicarbonate (as HC03) • - Carbonate (as G03) •-Chloride (as a ) •-Fluoride (as F) •-Sulfate (as S04) ~
^ lon Charge Balance
Remarks:
Physical Parameteri; •-Color • - C O n d U C t a n C e (Mtaomho.«JSQ '
•-Odor • - p H • • Surfactants • • Total Dissolved Solids •-Turbidity Other • -• -• -• -
Surface and Waste Water: • - Biological Oxygen Demand • - Total Suspended Solids Q- Chemical Oxygen Demand • - Total Organic Carbon •-Cyanide Nutrients: • • Nitrate + Nitrite (as N) • - Ammonia (as N) •-Total Kjeldahl (as N) • - Nitrite (as N) • - Orthophosphate (as P) •-Total Phosphorus (as P)
S L D 8 9 1 2 - W C Form Naw 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI
"STATE OF NEW MEXICO DEPARTMENT OF HEALTH
SCIENTIFIC LABORATORY DIVISION , ^ P.O. Box 4700 700 Camino de Salud, NE
Albuquerque, NM 87196-4700 [505]-841-2500 p ,j f j r;g ORGANIC CHEMISTRY SECTION [505]-841-2570
May 23, 1994 mmmmmmmmmmmmmmmmmmmmmmmmummmmmmumummmmmm Distribution
• ANALYTICAL REPORT • ^7 TZa • • ( i j Submitter 260
ro No.St 014375 S S L D Accession No. OR-94-0917 : « SLD Fues
To: Roger Anderson From: Organic Chemistry Section NM Oil Consv. Div. Scientific Laboratory Div. State Land Office Bldg. 700 Camino de Salud, N.E. P.O. Box 2088 P.O. Box 4700 Santa Fe, NM 87504-2088 Albuquerque, NM 87196-4700
Re: A water,Purgeable sample submitted to this laboratory on March 28, 1994
DEMOGRAPHIC DATA COLLECTION LOCATION
On:25-Mar-94 By: Ols . . . MW-6X-At: 11:30 hrs. In/Near: Sunland Park
ANALYTICAL RESULTS: Aromatic & Halogenated Purgeable rEPA-601/21 Screen {754} Parameter Value Note POL Units
Tetrahydrofuran 11.00 T 50 . 00 ppb Benzene 101.00 10. 00 ppb Toluene 2 .60 T 10. 00 ppb Ethylbenzene 46.00 10 . 00 ppb p- & m-Xylene 13 .00 10 . 00 ppb o-Xylene 8.90 T 10 . 00 ppb Isopropylbenzene 21.00 10 . 00 ppb
See Laboratory Remarks f o r A d d i t i o n a l I n f o r m a t i o n Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit; P = Compound Present, but not quantified; T = Trace (< Detection Limit); U = Compound Identity Not Confirmed. Evidentiary Seals: Not Sealed^); Intact: No |~ | , Yes|~| & Broken By: Date:
Laboratory Remarks: Foamy sample; unable to achieve a lower detection l i m i t .
Reported compound i d e n t i t i e s were confirmed by GC/MS.
Compound Note Value PQL n-Propylbenzene 52 10 1,2,4-Trimethylbenzene 270 10 Naphthlene 13 10 Methylene c h l o r i d e 29 10
VOLATILE ORGANICS ANALYSIS DATA SHEET
(Continued on page 2.)
ANALYTICAL REPORT SLD Accession No. OR-94-0917 Continuation, Page 2 of 4
Lab Name: NM SCIENTIFIC LABORATORY DIVISION Contract:_N/A Lab Code: N/A Case No. : N/A SAS No. : N/A SDG No.: N/A Matrix: (soil/water) Water Lab Sample ID: OR-94-917 Sample wt/vol: 5.0 (g/mL) mL SLD Batch No: 127 Level: (low/med) Low Date Received: 3/28/94 % Moisture: not dec. N/A dec. N/A Date Extracted: N/A Extraction: (SepF/Cont/Sonc) N/A Date Analyzed: 4/05/94 GPC Cleanup: (Y/N) No pH: D i l u t i o n Factor: 10
CONCENTRATION UNITS: (ug/L or ug/Kg) : ug/L
This sample was analyzed f o r the following compounds using EPA Methods 601 & 602
CAS NO. COMPOUND CONC. 0 POL 67-64-1 Acetone U 50 .0 71-43-2 Benzene 101 10 . 0 108-86-1 Bromobenzene U 10 . 0 74-97-5 Bromochloromethane U 10 . 0 75-27-4 Bromodichloromethane U 10.0 75-25-2 Bromoform U 10.0 78-93-3 2-Butanone (MEK) U 50 .0 104-51-8 n-Butylbenzene U 10 .0 135-98-8 sec-Butylbenzene U 10.0 98-06-6 tert-Butylbenzene U 10 .0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 50 . 0 56-23-5 Carbon t e t r a c h l o r i d e U 10 . 0 108-90-7 Chlorobenzene U 10 .0 67-66-3 Chloroform U 10 .0 95-49-8 2-Chlorotoluene U 10 . 0 106-43-4 4-Chlorotoluene U 10.0 96-12-8 1,2-Dibromo-3-chloropropane U 10.0 124-48-1 Dibromochloromethane U 10.0 106-93-4 1,2-Dibromoethane U 10.0 74-95-3 Dibromomethane u 10.0 95-50-1 1,2-Dichlorobenzene u 10 .0 541-73-1 1,3-Dichlorobenzene u 10 .0 106-46-7 1,4-Dichlorobenzene u 10.0 75-71-8 Dichlorodifluoromethane u 10.0 75-34-3 1.1-Dichloroethane u 10 .0 107-06-2 1,2-Dichloroethane u 10 .0 75-35-4 1.1-Dichloroethene u 10.0 156-59-4 cis-1,2-Dichloroethene u 10.0
(Continued on page 3.)
ANALYTICAL REPORT SLD Accession No. OR-94-0917 Continuation, Page 3 of 4
156-60-5 t r a n s - 1 , 2 - D i c h l o r o e t h e n e U 10.0 78-87-5 1,2-Dichloropropane U 10.0 142-28-9 1,3-Dichloropropane U 10 .0 590-20-7 2,2-Dichloropropane U 10 .0 563-58-6 1,1-Dichloropropene U 10.0 1006-01-5 c i s - 1 , 3 - D i c h l o r o p r o p e n e U 10.0 1006-02-6 t r a n s - 1 , 3 - D i c h l o r o p r o p e n e U 10.0 100-41-4 Ethylbenzene 46 10.0 87-68-3 He x a c h l o r o b u t a d i e n e U 10.0 98-82-8 Is o p r o p y l b e n z e n e 21 10.0 99-87-6 4 - I s o p r o p y l t o l u e n e U 10 .0 75-09-2 Methylene c h l o r i d e 29 10 .0 90-12-0 1-Methylnaphthalene U 10.0 91-57-6 2-Methylnaphthalene U 10.0 91-20-3 Naphthalene 13 10.0 103-65-1 n-Propylbenzene 52 10 .0 100-42-5 Styre n e U 10 . 0 630-20-6 1,1.1,2-Tetrachloroethane U 10.0 79-34-5 1,1,2,2-Tetrachloroethane U 10 .0 127-18-4 T e t r a c h l o r o e t h e n e U 10 .0 109-99-9 T e t r a h y d r o f u r a n (THF) 11 J 50.0 108-88-3 Toluene 2.6 J 10.0 87-61-5 1,2,3-Trichlorobenzene U 10.0 120-82-1 1.2.4-Trichlorobenzene U 10.0 71-55-6 1 . 1 . 1 - T r i c h l o r o e t h a n e U 10.0 79-00-5 1 , 1 , 2 - T r i c h l o r o e t h a n e U 10.0 79-01-6 T r i c h l o r o e t h e n e U 10.0 75-69-4 T r i c h l o r o f l u o r o r n e t h a n e U 10 . 0 96-18-4 1 , 2 , 3 - T r i c h l o r o p r o p a n e U 10.0 95-63-6 1.2.4-Trimethylbenzene 270 10.0 108-67-8 1,3,5-Trimethylbenzene U 10.0 75-01-4 V i n y l c h l o r i d e U 10.0 95-47-6 o-Xylene 8.9 J 10.0 N/A p- Sc. m-Xylene 13 10.0 N/A T o t a l Xylenes 21.9 20 . 0
TENTATIVELY IDENTIFIED COMPOUNDS DATA SHEET
The f o l l o w i n g compounds were t e n t a t i v e l y i d e n t i f i e d by Mass Spec: CAS NO. COMPOUND MATCH RT EST. CONC. 0
637-50-3 1-propenylbenzene 953 20 . 65 200
(Continued on page 4.)
ANALYTICAL REPORT SLD Accession No. OR-94-0917 Continuation, Page 4 of 4
933-98-2 1 - e t h y l - 2 , 3 - d i m e t h y l benzene 974 21.35 100
7525-62-4 1-ethenyl-3 - e t h y l -benzene 900 21.60 100
874-41-9 1 - e t h y l - 2 , 4 - d i m e t h y l benzene 834 21.17 100
611-14-3 1 - e t h y l - 2 - m e t h y l -benzene 973 19 .29 90
488-23-3 1 , 2 , 3 , 4 - t e t r a m e t h y l -benzene 968 22 .12 90
824-63-5 2 , 3- d i h y d r o - 2 - m e t h y l -l h - i n d e n e 970 22 .62 50
* CONC = CONCENTRAION DETERMINED PQL = P r a c t i c a l Q u a n t i t a t i o n L i m i t (Approximately 10 times MDL)
* Q = Q u a l i f i e r D e f i n i t i o n s : B - I n d i c a t e s compound was detected i n the Lab Blank as w e l l
as i n the sample. D - I n d i c a t e s value taken from a secondary ( d i l u t e d ) sample a n a l y s i s . E - I n d i c a t e s compound concentration exceeded the range of the
standard curve. J - I n d i c a t e s an estimated value f o r t e n t a t i v e l y i d e n t i f i e d compounds,
or f o r compounds detected and i d e n t i f i e d but present a t a conce n t r a t i o n less than the q u a n t i t a t i o n l i m i t .
N - I n d i c a t e s t h a t more than one peak was used f o r q u a n t i t a t i o n . U - I n d i c a t e s compound was analyzed f o r , but not detected above the
conc e n t r a t i o n l i s t e d ( Q u a n t i t a t i o n L i m i t ) .
QUALITY CONTROL SUMMARY FOR VOLATILES SCREEN
METHOD BLANK: A l a b o r a t o r y method blank was analyzed along w i t h t h i s sample t o assure the absence of i n t e r f e r i n g contaminants from l a b reagents, instruments, or the general l a b o r a t o r y environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported d e t e c t i o n l i m i t .
COMPOUND DETECTED CONCENTRATION (PPB) No Compounds Detected
SURROGATE RECOVERIES: SURROGATE CONCENTRATION % RECOVERY
(Continued on page 5.)
ANALYTICAL REPORT SLD Accession No. OR-94-0917 Continuation, Page 5 of 4
Bromofluorobenzene 25.0 ppb 90.0 2-Bromo-l-chloropropane 25.0 ppb 92.0
SPIKE RECOVERY: The % recoveries f o r compounds i n the batch spike were from 80% to 120% with the exception of the compounds l i s t e d below: COMPOUND CONCENTRATION % RECOVERY
No exceptions . ppb
Reviewed By: _ RicharcTF. Meyerhein 05/04/94 Supervisor, Organic Chemistry Section
ORGANIC CHEMISTRY ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E., ALBUQUERQUE, NM 87106
Organic Chemistry Section - Telephone: (505) 841 -2570 JJUser
Code#: I 7 I tt i 3 j 2 i 0 |
^Name? S f i M c J
31 Request ID No.:
Request 11111 UU Ui ID No. 014375-C
SLD No.
Date Received Jj Priority 7"
Code #: \£j
0R94 0917 C
caaeO-SLD
-^J Sample Location: ( -AS I I I I L J I I L J I I I I L J I
lOjCollected By:
Brat ILIitUt On: 9±M21I2^Z At: 1 j) l\J\Q\hrs
Dm: (YY/MM/OO) ~ jjJCodes:
Submitter
Tima- 2* <*• oae* 3.-00 cm • '300 ~v
JJ] Latitude (D0MM,ss)
. 1 uL 'i ' 1 ' 1
Longitude (DOOMMSS)
I > I 'I I 1
1 I I L 13j RePOrt Ntrcm
To: Roger Anders.on
'wssV 1_J L Organization
141 Phone #: ^ (505) 827-5812
Addrea New Mexico Oil Conservation Division
City, SUM Zip p. o_ Bnv ?nafl Santa Fe, New Mexico 87504-2088
2 Digit ID l» itt eta)
j 5 j .Sampling Information:
Sampla Purpoaa: •fcompo«it« £"« • • Complianoa n- Row Proportionad
• Sim!
lOOtlt*
Monitoring t?£ Special /XJ.
pit Split w/Parmittaa Chain of Custody
• ^ D a t a : P H : ( > J $ • Conductivity. umho>®^6.(o Tamparatura:
17J Sample Source •-Stream •-Lake •-Drain •-Pod •-WWTP
101 Flald Nota*/ 1 — 1 Sampta »
Chlorina C, flaaidual: mg/l, Row:
19J Sample Type: ^-Water. • -Wastewater, Q -Other.
^-Well; Depth: . TJ-Spring ••Distribution •-Point-of-Entry •-Other
201 Preservation: Q N P MB Pnaaarvatton; Sampta atorad at room tamparatura
££P4oa Sampla aion»d In an lea bath (Not Bonn)
SP-TS Sampla Praaarvad with Sodium TMoautfata to ramova chlorina rasidual P+O Sampla Praaarvad with Hydrochloric Acid (2 dropt/40 ml)
&09m fyU?
• - S o i D-Food.
This form accompanies a single sample consisting of : septumvial(s) (volume - yo mj ) glass jugs (volume -
(volume ) 2iJ Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s)
required. Whenever possible, list specific compounds suspected or required.
Volatile Screens:
(753) Aliphatic Headspace (1 -5 Carbons) (754) Aromatic & Halogenated Purgeables (EPA 601 & 602) (765) Mass Spectrometer Purgeables (EPA 624) (766) SDWA Totai Trihalomethanes (EPA 501.1) (774) SDWA VOC's f (8 Regulated +] (EPA 502.2) (775) SDWA VOCs li {EDB & DBCP) (EPA 504)
Other Specific Compounds or Classes; ( ) .
Semivolatile Screens; • - (763) Acid Extractables • - (751) Aliphatic Hydrocarbons • • (755) Base/Neutral Extractables (EPA 625) • - (756) Base/Neutral/Acid Extractables (EPA 8270)
8 - (758) Herbicides. Chlorophenoxy Acid - (759) Herbicides, Triazines
• - (760) Organochlorine Pesticides
8- (761) Organophosphate Pesticides - (767) Polychlorinated Biphenyls (PCB's)
• - (764) Polynuclear Aromatic Hydrocarbons • - (762) SDWA Pesticides & Herbicides
Remarks:
SLD 8912~OR Form Naw 12/S» This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY!
i£TATE OF NEW MEXICO DEPARTMENT OF HEALTH SCIENTIFIC LABORATORY DIVISION
P.O. Box 4700 700 Camino de Salud, NE Albuquerque, NM 87196-4700 [505]-841-2500
WATER CHEMISTRY SECTION [505]-841-2555
May 26, 1994
Request ID No. 014376
ANALYTICAL REPORT ior No. WC-94-1189 g SLD Acc;
Distribution QUser 70320 (2£ Submitter 260 (x) SLD Files
To:
Re:
R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Water Chemistry Section Scientific Laboratory Div. 700 Camino de Salud, N.E. P.O. Box 4700 Albuquerque, NM 87196-4700
A water,Nonpres/No sample submitted to this laboratory on March 28, 1994
DEMOGWK1C DATA COLLECTION LOCATION
On: 25-Mar-94 At: 11:30 hrs.
By: Ols . . . In/Near: Sunland Park
MW-6X
ANALYTICAL RESULTS Analvsis
calcium magnesium potassium sodium bicarbonate carbonate chloride f l u o r i d e sulfate Ion Balance t o t a l diss resid
Vy-Ioe 147.00 108 .00
16 .00 1575.00 1772.00
0 .00 1796.00
1.00 107.00 104.00
S200 .00
D. Lmt. Units mG/L mG/L mG/L mG/L mG/L mG/L mG/L mG/L mG/L
% mG/L
Reviewed By: C. Rachael Howell 05/18/94 Analyst, Water Chemistry Section
W A J E R C H E M I S T R Y ANALYT ICAL R E Q U E S T FORM
j SCIENTIRC LABORATORY DIVISION 700 CAMINO DE SALUD, ALBUQUERQUE. NM 87106 Water Chemistry Section - Telephone: (505) 841 -2555
SLD No.
Date Received
2jUser C o d e * : ' 7 ' ° *2 I2 l° I
31 Request ID No.:
P t a o f e n n O SdoawHam
_U Priority Code#: 3,
[ T V o r V . call EIO-SU Coortinalo»|
U Facility Name:
Sample Location: I I I I L J I
lOj Collected By:
First On:
IM«l«|t. 9( / /C3/ + r At:l/ | / | 3 | Q l h r s , 0>i«: (YY/MM/OO) ~ Tim*' 24 m. ciocn
3.00 twn - IS0OW1. 111Codes:
•I J , I l3jReport
To:
Submitter I I 1 l - l I I I L
WSS»
Roger AAderson "?4[ Phone #:
1— 1 (505) C27-5C12
' I I Organization
New Mexico Oil Conservation Division P. 0. 2088
City, Slaw Zip Santa Fe, New Mexico 87504-2088
16|P'eld-Data:
TJ] Latitude IODMMSS)
Longitude (OOOMMSS)
• I I 'l I I I H
2 Digit IO (Si
Sampling Information:
Sampl* Purpo**: ' Q ? Composit* P^ESS, • - Complianc* n- Flow Proportioned'"* n- Cnadc Q- Equal Aliquot
JSg Monitoring Jg\. Sampla Split w/Permittee ^••Spaciai • • Chain ot Custody
pH: b r f f i . Conductivity: j ? f ) Q umhoa@(^.^ Tamparatura:
171 Sample Source: 18| Plaid Not**/ Sampla »
, Chlorina C, Residual: mg/l, Row:
•-Stream U-Lake •-Drain •-Pool --WWTP
J9] Sample Type: J3-Water~ • -Wastewater, • -Other.
frf-Well; Depth: /LT-Spring •-Distribution •-Point-of-Entry •-Other
Q-Soit, • -Food , 201 Preservation: 1 " W N F Watar Not Pr***rv*d; Rltarad
Watar Not Praaarvad; Not Firtarad Watar Praaarvad with Sulfuric Acid (H2S04); Filtarad Watar Praaarvad wtth Sulfuric Add; Not Firtarad Watar Not Praaarvad in Raid; Ptaaaa Add H2S04 at Ub Watar lead
This form accompanies a ainoja sampla consisting of: j -1 liter cubitainers (1 quart)
- 4 liter cubitainers (1 gallon)
FWNN ••WPP •-WPN •-WNL
Othar.
2JJ Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required. Group ArtalYitsi Q . (559) SWQB SS Anion - Cation Group +
• - (854) SDWA Group 11 (Nitrate as N) Q (868) SWQB NPS Anion. Cation, Physical + TSS • - (861) SDWA Group III (Fluoride) Q- (869) SWQB Nutrient Analysis Group + • - (860) SDWA Complete Secondary J&£ (867) Major Anions & Cations
Cations: • - Calcium (as Ca) • - Magnesium (as Mg) n - Potassium (as K) •-Sodium (as Na) • • Total Hardness (as CaC03)[ Anions; •-Alkalinity (as CaC03) • - Bicarbonate (as HC03) • - Carbonate (as C03) • - Chloride (as Cf) •-Fluoride (as F) •-Sulfate (as S04)
X
Physical Parameters: • -Color • * Conductance (M«O«T*O«®29C> • -Odor • - P H • • Surfactants O - Total Dissolved Solids •-Turbidity Other • -• -• -• -
Surface end Waste Water: • - Biological Oxygen Demand ••Total Suspended Solids • - Chemical Oxygen Demand • - Total Organic Carbon •-Cyanide Nutrients; • - Nitrate + Nitrite (as N) • - Ammonia (as N) •-Total KJeldahl (as N) Q-Nitrite (as N) • - Orthophosphate (as P) • - Total Phosphorus (as P)
lon Charge Balance
Remarks:
SLD8912-WC FormNawt2/ao This Form W3I NOT Be Returned With Your Results. Please RETAIN A COPY!
STATE OF NEW MEXICO DEPARTMENT OF HEALTH
* SCIENTIFIC LABORATORY DIVISION P.O. Box 4700 700 Camino de Salud, NE
Albuquerque, NM 87196-4700 [505]-841-2500 AIR & HEAVY METALS SECTION [505]-841-2553
May 11, 1994
Request ID No. 014377
ANALYTICAL REPORT g SLD Accession No. IC-94-0047 g
Distribution (JUser 70320
Submitter 260 (x> SLD Files
To: R. Anderson NM Oil Consv. Div. State Land Office Bldg. P.O. Box 2088 Santa Fe, NM 87504-2088
From: Air & Heavy Metals Section Scientific Laboratory Div. 700 Camino de Salud, NE Albuquerque, NM 87106
A water,Nonpres/No sample submitted to this laboratory on March 28,1994
User: NM Energy & Min - Oil Conserv. , NM
DEMOGRAPHIC DATA COLLECTION LOCATION
On.-25-Mar-94 By: Ols . . . M W - ^ < At: 11:30 hrs. In/Near: Sunland Park
ANALYTICAL RESULTS in mG/L Analvsis Value Analysis Value Analvsis Value
Aluminum 4 .40 Copper < 0 .10 S i l v e r < 0 .10 B a r i u m 1.40 I r o n 12 .00 S t r o n t i u m 4 .90 B e r y l l i u m < 0 .10 Lead < 0 .10 T i n < 0 .10 Boron 1.20 Magnesium 100.00 Vanadium < 0 .10 Cadmium < 0 .10 Manganese 1.30 Z i n c < 0 .10 C a l c i u m 270 .00 Molybdenum < 0 .10 M e r c u r y < 0 .0005 Chromium < 0 .10 N i c k e l < 0 .10 S e l e n i u m < 0 .0050 C o b a l t < 0 .05 S i l i c o n 0.20
Laboratory Remarks: ICP by method 270.2 on 4/29/94 by RAH. Mercury by method 245.1 on 4/13/94 by SD. Selenium by method 270.2 on 4/8/94 by RAH.
Reviewed By: Jim F. Ashbyy// 05/11/94 Supervisor, Air tk Heavy Metals Section
AIR & HEAVY METALS ANALYTICAL REQUEST FORM SCIENTIFIC LABORATORY DIVISION
700 CAMINO DE SALUD N.E., ALBUQUERQUE. NM 87106 Air & Heavy Metals Section - Telephone: (505) 841-2553
SLD No.
Date Received:
JJUser Code #:
U Facility Name:
I 7 I 0 I 3 I 2 I 0 I 31 Request
ID No.: Plot* FormO
6J County:
i f Priority -> U O d S # • I s j I Coordin*o«|
(Ifl" 0»T , C*II EID-SLD
[TJCTty 8 JStatei
3J Location: I I I
jtpjCollected i A j .
Rrat /lJ\<S>H On: At:| / \ / \ 3 IO I hrs
|Lla|alt Ofc»: (YY/MM/DO) Time; *«J»: <??£!_ 100cm • '800hn.
11 [Codes:'
•4 I, I I L ubmitter
I I - I I I I—L WSS»
13
nization Report To: Roger Anderson
14) Phone #: U J (505) 827-5812
New Mexico Oil Conservation Division
City, SUM Zip P . n. BOV ?na«
Santa Fe, New Maxico 87504-2088
12 Latitude (DDMMSS) e '
, • ul 1 1 1 1 1
Longitude (DODMMSS)
I t 1 I I . I N
2 Digit IO
iH4 PajfioO^
1 c j dimpling Information:
Sampla Purpoaa:' [^Composite pompo*. • - Complianoa n - Plow Proportioned H- Check n - Equal Aliquot
Jj2*"Monitoring ^fif- Sampla Split w/Permittee 1j>Specia] Q . Chain of Custody
16) Field Data: P H : C - • Conductivity: Q umhos ® L\ * £ " Tamparatura:
e . m n i . c« . . r«» . 1181 Raid Notsa/ l8|PiaidNotaa/ — Sample »:
Chlorine C, Residual: mg/l, Row:
17| Sample Source: ~-Stream •-Lake •-Drain •-Pool r-i-WWTP
^-Well; Depth: . U-Spring •-Distribution • -Point-of-Entry •-Other:
20| Preservation: 1 — • • W N F Watar Not Praaarvad; Rltarad
Watar Not Praaarvad; Not Rltarad Watar Praaarvad with Nitric Acid (HN03); Rltarad Watar Praaarvad wftf) Nitric Add; Not Rltarad Watar Not Praaarvad in Raid; Please Add HN03 at Lab Watar load
tsj Sample Type: ^-Water, • -Wastewater, • -Other,
•-Sofl. •-Food,
This form accompanies a aingia sample consisting of: \ -1 liter cubitainers (1 quart)
- 4 liter cubitainers (1 gallon)
-Q-WNN -g-wpf
JWPN WML ICE
Lj-Othar. 21 j Analyses Requested: Please check the appropriate box(es) below to indicate the type of analyses required.
ft (704) ICAP Scan (720) SDWA Group I Only
• - (721) SDWA Group I + other parameter (s) marked below
• - Aluminum • - Arsenic • - Barium • - Cadmium • - Chromium • - Cobalt • - Copper • - Iron
• -Lead Q - Manganese
Mercury • -Molybdenum Q- Nickel M.- Selenium • -Silver • - Uranium
• - Vanadium • -Zinc • -• -• -• -
• •ZZZZZ • -
Remarks:
S L D 8912-HM Form New 12/89 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPYI
, >; r -
CL' in u i JU
STATE OF NEW MEXICO DEPARTMENT OF HEALTH SCIENTIFIC LABORATORY DIVISION
,- n u ' J f*.<0. Box 4700 700 Camino de Salud, NE Albuquerque, NM 87196-4700 [505]-841-2500
f ' f l 8 5 0 ORGANIC CHEMISTRY SECTION [505]-841-2570
May 23, 1994 M^^m^mmamL^umam—mmmm^ Distribution
• ANALYTICAL REPORT • ^^ e r I° 3 2L • • ( i j Submitter 260
ID No. 014372 B S L D Accession No. OR-94-0918 : (x> SLOPES
To: Roger Anderson From: Organic Chemistry Section NM Oil Consv. Div. Scientific Laboratory Div. State Land Office Bldg. 700 Camino de Salud, N.E. P.O. Box 2088 P.O. Box 4700 Santa Fe, NM 87504-2088 Albuquerque, NM 87196-4700
Re: A water,Purgeable sample submitted to this laboratory on March 28, 1994
DEMOGRAPHIC DATA COLLECTION LOCATION
0«.-25-Mar-94 By: Ols . . . MW-9X 5 At: 10:40 hrs. In/Near: Sunland Park
ANALYTICAL RESULTS: Aromatic & Halogenated Purgeable [EPA-601/21 Screen (754) Parameter Value Note POL Units
EPA 601/2 V o l a t i l e s (60) 0.00 N 1.00 ppb See Laboratory Remarks fo r Additional Information
Notations & Comments: PQL = Practical Quantitation Level. A = Approximate Value; N = None Detected above Detection Limit; P = Compound Present, but not quantified; T = Trace (< Detection Limit); U = Compound Identity Not Confirmed. Evidentiary Seals: Not Sealed pj£|; Intact: No |~ | , Yes |~ | & Broken By: Date:
Laboratory Remarks: No target compounds observed, however C8, C9, C10, aldehydes observed on GC/MS, but not quantified.
Reported compound i d e n t i t i e s were confirmed by GC/MS.
VOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name: NM SCIENTIFIC LABORATORY DIVISION Contract: N/A Lab Code: N/A Case No. : N/A SAS No. : N/A SDG No.: N/A Matrix: (soil/water) Water Lab Sample ID: OR-94-918 Sample wt/vol: 5.0 (q/mL) mL SLD Batch No: 127 Level: (low/med)_Low Date Received: 3/28/94
Moisture: not dec. N/A dec. N/A Date Extracted: N/A Extraction: (SepF/Cont/Sonc) N/A Date Analyzed: 4/05/94 GPC Cleanup: (Y/N) No pH: D i l u t i o n Factor: 1
CONCENTRATION UNITS: (ug/L or ug/Kg) : ug/L
(Continued on page 2.)
ANALYTICAL REPORT SLD Accession No. OR-94-0918 Continuation, Page 2 of 4
This sample was analyzed for the following compounds using EPA Methods 601 & 602
CAS NO. COMPOUND CONC. 0 POL 67-64-1 Acetone U 5.0 71-43-2 Benzene U 1.0 108-86-1 Bromobenzene U 1.0 74-97-5 Bromochloromethane U 1.0 75-27-4 Bromodichloromethane U 1.0 75-25-2 Bromoform U 1.0 78-93-3 2-Butanone (MEK) U 5.0 104-51-8 n-Butylbenzene U 1.0 135-98-8 sec-Butylbenz ene U 1.0 98-06-6 tert-Butylbenzene U 1.0 1634-04-4 t e r t - B u t y l methyl ether (MTBE) U 5 . 0 56-23-5 Carbon t e t r a c h l o r i d e U 1. 0 108-90-7 Chlorobenzene U 1.0 67-66-3 Chloroform U 1.0 95-49-8 2-Chlorotoluene U 1.0 106-43-4 4-Chlorotoluene •TJ 1.0 96-12-8 1.2-Dibromo-3-chloropropane U 1. 0 124-48-1 Dibromochloromethane U 1.0 106-93-4 1,2-Dibromoethane U 1.0 74-95-3 Dibromomethane U 1.0 95-50-1 1.2-Dichlorobenzene U 1.0 541-73-1 1.3-Dichlorobenzene U 1.0 106-46-7 1,4-Dichlorobenzene u 1.0 75-71-8 Dichlorodifluoromethane u 1.0 75-34-3 1.1-Dichloroethane u 1. 0 107-06-2 1,2-Dichloroethane u 1. 0 75-35-4 1.1-Dichloroethene u 1.0 156-59-4 cis-1,2-Dichloroethene u 1. 0 156-60-5 trans-1.2-Dichloroethene u 1.0 78-87-5 1, 2-Dichloropropane u 1. 0 142-28-9 1.3-Dichloropropane u 1. 0 590-20-7 2.2-Dichloropropane u 1.0 563-58-6 1.1-Dichloropropene u 1.0 1006-01-5 cis-1,3-Dichloropropene u 1.0 1006-02-6 trans-1,3-Dichloropropene u 1.0 100-41-4 Ethylbenzene u 1.0 87-68-3 Hexachlorobutadiene u 1.0 98-82-8 Isopropylbenzene u 1. 0 99-87-6 4-lsopropyltoluene u 1. 0
(Continued on page 3.)
ANALYTICAL REPORT SLD Accession No. OR-94-0918 Continuation, Page 3 of 4
75-09-2 Methylene c h l o r i d e U 1 .0 90-12-0 1-Methylnaphthalene U 1 .0 91-57-6 2-Methylnaphthalene U 1 .0 91-20-3 Naphthalene U 1 .0 103-65-1 n-Propylbenzene U 1 .0 100-42-5 Styren e U 1 .0 630-20-6 1,1.1, 2 - T e t r a c h l o r o e t h a n e U 1 .0 79-34-5 1,1,2, 2 - T e t r a c h l o r o e t h a n e U 1 .0 127-18-4 T e t r a c h l o r o e t h e n e U 1 .0 109-99-9 T e t r a h y d r o f u r a n (THF) U 5 .0 108-88-3 Toluene U 1 .0 87-61-5 1,2,3-Trichlorobenzene U 1 .0 120-82-1 1,2,4-Trichlorobenzene U 1 .0 71-55-6 1 , 1 , 1 - T r i c h l o r o e t h a n e U 1 .0 79-00-5 1 , 1 , 2 - T r i c h l o r o e t h a n e U 1 .0 79-01-6 T r i c h l o r o e t h e n e U 1 .0 75-69-4 T r i c h l o r o f l u o r o r n e t h a n e U 1 .0 96-18-4 1, 2 , 3 - T r i c h l o r o p r o p a n e U 1 .0 95-63-6 1,2,4-Trimethylbenzene U 1 . 0 108-67-8 1,3,5-Trimethylbenzene U 1 .0 75-01-4 V i n y l c h l o r i d e U 1 . 0 95-47-6 o-Xylene U 1 .0 N/A p- & m-Xylene U 1 .0
TENTATIVELY IDENTIFIED COMPOUNDS DATA SHEET
CAS NO. COMPOUND MATCH RT EST. CONC. 0 124-19-6 nonanal 967 21.97 5 112-31-2 decanal 978 23 .84 2 124-13-0 o c t a n a l 984 20. 2
6032-29-7 2-pentanol 839 7.01 2
* CONC = CONCENTRAION DETERMINED PQL = Practical Quantitation Limit (Approximately 10 times MDL)
* Q = Q u a l i f i e r D e f i n i t i o n s : B - Indicates compound was detected i n the Lab Blank as well
as i n the sample. D - Indicates value taken from a secondary (diluted) sample analysis. E - Indicates compound concentration exceeded the range of the
standard curve. J - Indicates an estimated value f o r t e n t a t i v e l y i d e n t i f i e d compounds,
(Continued on page 4.)
ANALYTICAL REPORT SLD Accession No. OR-94-0918 Continuation, Page 4 of 4
or f o r compounds detected and i d e n t i f i e d but present at a concentration less than the quantitation l i m i t .
N - Indicates that more than one peak was used f o r quantitation. U - Indicates compound was analyzed f o r , but not detected above the
concentration l i s t e d (Quantitation L i m i t ) .
QUALITY CONTROL SUMMARY FOR VOLATILES SCREEN
METHOD BLANK: A laboratory method blank was analyzed along with t h i s sample to assure the absence of i n t e r f e r i n g contaminants from lab reagents, instruments, or the general laboratory environment. Unless l i s t e d below, no contaminants were detected i n t h i s blank above the reported detection l i m i t .
COMPOUND DETECTED CONCENTRATION (PPB) No Compounds Detected
SURROGATE RECOVERIES: SURROGATE CONCENTRATION % RECOVERY
Bromofluorobenzene 25.0 ppb 98.0 2-Bromo-l-chloropropane 25.0 ppb 101.0
SPIKE RECOVERY: The % recoveries f o r compounds i n the batch spike were from 80% to 120% with the exception of the compounds l i s t e d below: COMPOUND CONCENTRATION % RECOVERY
No exceptions . ppb
Analyst:
Analyst, Organic Chemistry Supervisor, Organic Chemistry Section
ORGANIC CHEMISTRY ANALYTICAL REQUEST FORM
SCIENTIFIC LABORATORY DIVISION 700 CAMINO DE SALUD N.E., ALBUQUERQUE, NM 87106
Organic Chemistry Section - Telephone: (505) 841-2570 2lUser
Code*: I 7 i 0. j 3 j 2 | 0 | 31 Request
^"TDNo.
Request ID No.
SLD No.
Date Received:
014372-C Priority Code #:
r**'"<x"r. eauElO-SLO
mo* 8|State
m ^Name? S r i J l L j fief.
Location: ftl.W-.9-s J I L J—J I I I I I I I L JL—J I—l lOjCollected
By: Rftt
Mil JJslltSlL
on On: 9< / /d3 / *S~ At: I ) \ Ol V lO l hrs. Data: (YY/MM/DO) Tima- 34 •"• °oc*
a.-oeem - isoomi. Latitude (OOMMSS)
Longitude (ODOMMSS)
I I I 'I 1 1
iiJCodes:
1 J , I. I I Submitter
13| Report To: Roger Anders.on
wss» J I L I l
Organization 14J Phone #:
(505) 827-5812 New Mexico Oil Conservation Division
City. S U M Zip P. 0. rVTX ?0RR Santa Fe, New Mexioo 87504-2088
^ D a t a : P H : 1 \ 1 , Conductivity: umhoa ® 6^ Tamparatura:
Sample Source: v i miFiaid Nota./
12 2 Digit IO
(RnaMad)
15] \Sampling Information
Sampla P u r p o a a : ^ Compoaita •-Complianoa ~ • Row Proportion*
• Chack . R . Equal Aliquot - Sampla Split w/Parmittaa
[ComooK* •m« Ptnorf)
Monitoring Spatial Chain ot Custoqy
1 8in.ldho»a/ r~-*simo|a»;
Chlorina C, Raaidual: mg/l. Row:
17] Sample Source: •-Stream G-Lake •-Drain •-Pod •-WWTP
]§<Well; Depth: •^Spring
•-Distribution •-Point-of-Entry •-Other
20| Preservation: "" NP No Praaarvatlon; Sampla atorad at room tamparatura
P-tea Sampla atorad In an tea bath (Not Froxan) _ P-TS Sampla Praaarvad with Sodium Thtoaultata to ram ova chlorina raaidual • - P-HQ SampMi Praaarvad with Hydrochloric Acid (2 dropa/40 ml) BTOthar CP I I
191 Sample Type: J^-Water. • - Wastewater, • -Other.
O-Sol, ••Food,
This form accompanies a aingjai sampla consisting of: X • septum vial(s) (volume • HO M I )
- glass jugs (volume - )
T P *
(volume J 2ij Analyses Requested: Please check the appropriate box(es) below to indicate the type of analytical screen(s)
required. Whenever possible, list specific compounds suspected or required.
Volatile Screens:
(753) Aliphatic Headspace (1 -5 Carbons) '(754) Aromatic & Halogenated Purgeables (EPA 601 & 602) • (765) Mass Spectrometer Purgeables (EPA 624) (766) SDWA Total Trihatomethanes (EPA 501.1) (774) SDWA VOCs I [8 Regulated + ] (EPA 502.2) (775) SDWA VOCs II (EDB & DBCP] (EPA 504)
Other Specific Compounds or Classes:
( ) .
I I:
Semivolatile Screens; • - (763) Acid Extractables • - (751) Aliphatic Hydrocarbons • - (755) Base/Neutral Extractables (EPA 625) • - (756) Base/Neutral/Acid Extractables (EPA 8270)
a - (758) Herbicides, Chlorophenoxy Acid - (759) Herbicides, Triazines
• - (760) Organochlorine Pesticides
B - (761) Organophosphate Pesticides • (767) Polychlorinated Biphenyls (PCB's)
• * (764) Polynuclear Aromatic Hydrocarbons • - (762) SDWA Pesticides & Herbicides
Remarks:
SLD8912-OR Form Naw 12/88 This Form Will NOT Be Returned With Your Results. Please RETAIN A COPY)