surface area & pore size analyzer product overview · 2014. 9. 24. · surface area & pore...

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Surface Area & Pore Size Analyzer 2013 Quantachrome Corporaon 13003 Rev. A -1013 Quantachrome’s QUADRASORB evo TM Surface Area and Pore Size Analyzer, is a four sample station, bench-top, fully automated, vacuum- volumetric gas sorption system. The QUADRASORB evo TM is a high-throughput, cost- effective system featuring four separate and independent measurement ports allowing for simultaneous analysis of four samples. New & Improved Features: Quantachrome Instruments 1900 Corporate Drive, Boynton Beach, FL 33426 Tel: 800.989.2476 | local: 561.731.4999 email: qc.sales @quantachrome.com Our policy of continuous development may cause the information and specifications contained herein to change without notice or liability Pharma Carbon Energy Ceramics Catalysts QUADRASORB e v o BET QuickMode - For industrial high throughput settings- Time savings up to 50%: By passes most initialization, extended evacuation, and transducer zeroing sequences. Samples can run synchronously . Capable of running four (4) samples in as little as 25 minutes. Dedicated P o transducer and manifold provides uninter- rupted dosing of samples during measurements: P o can be continually measured. No need to stop measurement to update P o. No slow down in analysis to measure P o. Flexible P o Modes: P o can be estimated from ambient atmospheric pressure. P o can be entered as fixed value. P o can be analytically measured. New Dose Wizard™ Flexibility: Can use a previously measured sample as a dosing template for reduced analysis time. Can be used with or without QuickMode™ Proven Features: » Each analysis port can be independently programmed with different analyses and measurement conditions. New samples can be started on each port as prior measurements are completed with little delay to other samples already in progress. » Choose from two measurement techniques: Patented NOVA ® helium-free method and classical helium void-volume method. » Multiple gas dosing methods to optimize analysis time and resolution: Standard -intelligently adjusts dose size in re- sponse to sample demand. Vector Dosing- user selectable dose volumes from 0.25 to 10cc per point Delta (volume) Max - adds data points in regions of large uptake so critical pore filling is never missed. Dose Wizard - can be used with or without Quick- Mode TM enabled. This allows the instrument to dose more aggressively, saving significant analysis time.

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Page 1: Surface Area & Pore Size Analyzer PRODUCT OVERVIEW · 2014. 9. 24. · Surface Area & Pore Size Analyzer 2013 Quantachrome Corporation 13003 Rev. A -1013 Quantachrome’s QUADRASORB

Surface Area & Pore Size Analyzer

2013 Quantachrome Corporation 13003 Rev. A -1013

Quantachrome’s QUADRASORB evoTM Surface Area and Pore Size Analyzer, is a four sample station, bench-top, fully automated, vacuum- volumetric gas sorption system. The QUADRASORB evoTM is a high-throughput, cost- effective system featuring four separate and independent measurement ports allowing for simultaneous analysis of four samples.

New & Improved Features:

PR

OD

UC

T O

VE

RV

IEW

Quantachrome Instruments1900 Corporate Drive, Boynton Beach, FL 33426 Tel: 800.989.2476 | local: 561.731.4999 email: qc.sales @quantachrome.com

Our policy of continuous development may cause the information and specifications contained herein to change without notice or liability

Phar

ma

Carb

onEn

ergy

Cera

mic

sCa

taly

sts

QUADRASORB evo™

BET QuickMode™- For industrial high throughput settings- Time savings up to 50%:

• By passes most initialization, extended evacuation, and transducer zeroing sequences.

• Samples can run synchronously .

Capable of running four (4) samples in as little as 25 minutes.

Dedicated Po transducer and manifold provides uninter-rupted dosing of samples during measurements:

• Po can be continually measured.

• No need to stop measurement to update Po.

• No slow down in analysis to measure Po.

Flexible Po Modes:

• Po can be estimated from ambient atmospheric pressure.

• Po can be entered as fixed value.

• Po can be analytically measured.

New Dose Wizard™ Flexibility:

• Can use a previously measured sample as a dosing template for reduced analysis time.

• Can be used with or without QuickMode™

Proven Features:» Each analysis port can be independently programmed with different analyses and measurement conditions. New samples can be started on each port as prior measurements are completed with little delay to other samples already in progress.

» Choose from two measurement techniques:

• Patented NOVA® helium-free method and classical helium void-volume method.

» Multiple gas dosing methods to optimize analysis time and resolution:

• Standard™ -intelligently adjusts dose size in re-sponse to sample demand.

• Vector Dosing- user selectable dose volumes from 0.25 to 10cc per point

• Delta (volume) Max™ - adds data points in regions of large uptake so critical pore filling is never missed.

• Dose Wizard™ - can be used with or without Quick-ModeTM enabled. This allows the instrument to dose more aggressively, saving significant analysis time.

Page 2: Surface Area & Pore Size Analyzer PRODUCT OVERVIEW · 2014. 9. 24. · Surface Area & Pore Size Analyzer 2013 Quantachrome Corporation 13003 Rev. A -1013 Quantachrome’s QUADRASORB

Analysis Features / SpecificationsPR

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Our policy of continuous development may cause the information and specifications contained herein to change without notice or liability

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Carb

onEn

ergy

Cera

mic

sCa

taly

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QUADRASORB evo™

2013 Quantachrome Corporation 13003 Rev. A -1013

Quantachrome Instruments1900 Corporate Drive, Boynton Beach, FL 33426 Tel: 800.989.2476 | local: 561.731.4999 email: qc.sales @quantachrome.com

Your local Representative:

Pressure Transducers:Six* 1000 torr transducers (one on each sample station, plus dosing manifold and Po manifold)plus one# 1 torr transducer (dosing manifold)

Transducer Accuracy: 1000 torr: 0.11% full scale1 torr: 0.15% reading

Pressure Resolution:0.016 torr (1000 torr range). 0.000016 torr (1 torr range).

Measurement Modes:• Patented NOVA® method for helium free analysis.• Classical helium void volume measurement.• QuickMode™ for high BET surface area

throughput

Sensitivity: < 1 x 10-7 moles adsorbed/ desorbed gas.

Ultimate Vacuum:<1x10-2 torr achieved by dedicated two (2) stage rotary, direct drive pump.

1x10-9 torr achieved by turbo-molecular vacuum pump in QUADRASORB evoTM - Kr/MP.

Adsorbate: Nitrogen and any other non-corrosive gas with appropriate coolant.

Surface Area Range: 0.01m2/g to no known upper limit (nitrogen). 0.0005 m2/g to no known upper limit (krypton) Kr/MP model only.

Minimum Pore Volume: (liquid): 2x10-6 cc/g (STP): 0.0001cc/g

Pore Size Range: 3.5 to >4000Å / 0.35 to >400nm.

Number of independent Dewar (coolant) baths:Four‡

Coolant Level:Automatically maintained at a level around the sample cell to minimize cold zone volume.

Maximum Analysis Time>30 hours on uninterrupted/unattended operation with LN2 in standard dewar.

Dewars (coolant baths):Number: Four‡ (one per sample station)Nominal Capacity: 1000ml (each)

Independent analysis stations, each consisting of: sample cell, Po cell, pressure transducer, dewar bath and auto-matic dewar lift drive, coolant level sensor. Dedicated Po manifold and Po transducer for continual Po updates.

* Full Quadrasorb evo™ model. 2- and 3-station versions have 4 and 5 respectively.# Kr/MP version only. ‡ Full Quadrasorb evo™ model. 2- and 3-station versions have 2 and 3 respectively.

Physical Specifications:Dimensions: Height 29.0" (73.6 cm) x Width 25.25" (63.7 cm) x Depth 21.0" (53.3 cm)

Weight: 57.5 kg (127 lbs.)*

Electrical: 100-240 volts, 56/60 hertz

Ambient: 10-38°C operating range, 90% maximum relative humidity

* Four (4) station standard model not Kr/MP model.