status of ld interlab · rpe- pm group m eti ng, 1 ja 05 thank you for your attention! for further...

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R P E - P M P G r o u p m e e t i n g , 1 1 J a n 0 5 GRPE WG PMP informal meeting Status of LD Interlab P. Dilara, J. Andersson Working paper No. GRPE-PMP-14-3 (14th PMP meeting, Geneva 11th January 2005)

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Page 1: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

GRPE WG PMP informal meeting

Status of LD Interlab

P. Dilara, J. Andersson

Working paper No. GRPE-PMP-14-3

(14th PMP meeting,

Geneva 11th January 2005)

Page 2: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Inter-laboratory Correlation ExerciseSummary

– Light Duty prioritised– Commenced late summer 2004– Kick-off meeting at JRC, Ispra on 2-3 Sept. 04– 9 labs participating (11 repetitions)– Project managed by DG JRC (Ispra, Italy)– Golden Engineer funded by DfT (UK)– Foreseen end by Autumn 2005

Page 3: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Kick-off meetingJRC, Ispra, 2-3 September ‘04

• First letter and questionnaire in mid July• 22 experts mainly from labs, and instrument manufacturers• Presentation of labs• Presentation of possible instrumentation• Meeting with Japanese delegation a few days before

• Resulted in participation of 9 labs to final testing programme and strong involvement of instrumentation companies

Page 4: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Inter-laboratory Correlation Exercise

• Aims– Evaluate repeatability– Determine reproducibility of candidate measurement

systems– Evaluate robustness of draft test protocols for mass

and number

Page 5: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

• Repeated measurements at several laboratories (with JRC bookends)

• Travelling ‘Golden Engineer’ + two of JRC staff to ensure best and reproducible testing practice

• Very low PM ‘Golden Vehicle’ at all labs Repeatability• Optionally test other Euro IV vehicles (with/without DPFs)• Test ‘Golden Measurement System’ for particle numbers

Set-up

Page 6: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Outcomes• Evaluation of modified PM method• Regular and strict calibration protocols for particle

number measurements• Validation exercises for key measurement system

components– Volatile Particle Remover– Particle Number Counter– Diluters

Page 7: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

• Repeated measurements at several laboratories (with JRC bookends)

• Travelling ‘Golden Engineer’ + two of JRC staff to ensure best and reproducible testing practice

• Very low PM ‘Golden Vehicle’ at all labs Repeatability• Optionally test other Euro IV vehicles (with/without DPFs)• Test ‘Golden Measurement System’ for particle numbers

Set-up

Page 8: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Timetable (PART A)

April- Transfer to Japan INTERIM REPORT

Calibration of Golden Measurement SystemAEA Technology, UK

Late March 05JRC, Ispra, Italy

6

Early March 05Lab of Applied Thermodynamics (LAT)Greece

5

Late February 05RWTÜV Essen, Germany4

Mid January 05Ricardo Consulting EngineersUK

3

Calibration of Golden Measurement SystemAEA Technology, UK

29 November-3 Dec 04AVL MTCSweden

2

9 to 17 NovemberJRC, Ispra, Italy

1

PMP testing week:Address:No

Page 9: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Timetable (PART B)

Sept-Oct 05FINAL REPORT

August-Sept 05JRC, Ispra, Italy

11

Calibration of Golden Measurement SystemAEA Technology, UK

Late July 05UTACFrance

10

July 05Shell Global SolutionsUK

9

June 05 –Transfer to Europe

Early June 05National Motor Vehicle Emission Research Laboratory, Korea

8

Early May 05NTSEL, Japan7

Page 10: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

• Repeated measurements at several laboratories (with JRC bookends)

• Travelling ‘Golden Engineer’ + two of JRC staff to observe experiments

• Very low PM ‘Golden Vehicle’ at all labs Repeatability• Optionally test other Euro IV vehicles (with/without DPFs)• Test ‘Golden Measurement System’ for particle numbers

Set-up

Page 11: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

On site:• Preliminary visit by Golden Engineer (1 day) to

– guide on interpretation of docs– review and advise on set-up of instruments– selection of alternative vehicles and systems

• Visit during start of testing by Golden Engineer, Programme Manager and JRC Technician (1.5 days)– Inspect the installation of the golden and other systems– Confirm the results of linearity checks– Witness preliminary and start of testing – Optimise sampling parameters

• For non-EU labs, only JRC Programme Manager visit

Page 12: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

• Repeated measurements at several laboratories (with JRC bookends)

• Travelling ‘Golden Engineer’ + two of JRC staff to ensure best and reproducible testing practice

• Very low PM ‘Golden Vehicle’ at all labs Repeatability• Optionally test other Euro IV vehicles (with/without DPFs)• Test ‘Golden Measurement System’ for particle numbers

Set-up

Page 13: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Golden Vehicle• Peugeot 407 Saloon 2.0 HDi 136 SE 4Dr, Tyres 215/55R17• New vehicle sponsored by the AECC• Registered in the UK (right-hand drive)• Has been run in on the road

• Particulate emissions according to the PMP protocol significantly less than 0.0025 g/km

• Particle numbers measured by the PMP Particle Number protocol were less than 1011 per km for the NEDC cycle.

Page 14: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

A really “golden” vehicle!

Page 15: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Other vehicles?• EURO 4 conventional Diesel w/o DPF Best current

technology/ baseline• EURO 4 Gasoline PFI Lowest Achievable

Particle Count• Modern technology DISI Emission levels in

perspective to trap Diesel

• Yet to be defined

Page 16: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Other “Golden” items• Standard low-S fuel and synthetic lube oil kindly offered

by CONCAWE• Filters offered by JRC (Pallflex TX40)• Two URG PM 10 cyclones (2.5µm at 90 l/min)

• Each EU lab will pay for transportation of golden vehicle and equipment to the next lab

• Transportation of golden vehicle to Japan-Korea to be arranged separately

Page 17: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

• Repeated measurement set at several laboratories (with JRC bookend for the two parts)

• Travelling ‘Golden Engineer’ + two of JRC staff to ensure best and reproducible testing practice

• Very low PM ‘Golden Vehicle’ at all labs Repeatability• Optionally test other Euro IV vehicles (with/without DPFs)• Test ‘Golden Measurement System’ for particles

Set-up

Page 18: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Particulates Mass Sampling

Page 19: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Golden PM Measurement System

C HEPACVS Tunnel

To mass flow controller and

pump

PCF: provides sharp cut-point at 2.5µm

Carbon and HEPA filters provide particle free and low HC

background air

PND1

heats and dilutes

Particle number concentration

ET: Heatedevaporation tube

Dilution air in

Humidity and T controlled

To CFV

Size selective

inlet:D50 ~20nm

PSP and PTT comprise the sample probe

PND2

cools and dilutes

VPR

PSP

PTT

PNC

Model 3010D CPCOffered by TSI

Modified NANOMET-C Offered by MATTER ENG.

Lab Number System

Page 20: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Golden Particle Number System

Page 21: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Alternative options• Other instruments to check:

– dilution variables (modified Dekati as option)– alternative CPCs (GRIMM modified CPC 5.403 as parallel

equipment for all labs)– Other components?

• Alternative systems tested at participating labs• Yet to be defined

Page 22: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Calibration of Measurement Systems• Calibration of golden measurement system for:

– Penetration of solid particles– Calibration of CPC– Gas Calibration– VPR Efficiency

• Funded by the DfT• Performed at AEA Technology

Page 23: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Next Steps

– Finalise details of testing in non-EU countries (Japan, Korea)

– Finalise list of vehicles and alternative systems to be tested

– Prepare reports to PMP WG

– Heavy Duty Inter-lab exercise

Page 24: Status of LD Interlab · RPE- PM Group m eti ng, 1 Ja 05 Thank you for your attention! For further details or questions, please contact The PMP Interlab Manager: Penny Dilara JRC,

RPE- PMP Group meeting, 11 Jan 05

Thank you for your attention!

For further details or questions, please contactThe PMP Interlab Manager:

Penny DilaraJRC, TP 441,

Ispra, (VA) 21020, ItalyTel:+39-0332-789207

Fax: +39-0332-786328E-mail: [email protected]