sitewide environmental monitoring semiannual progress ... · the cms report concluded that...

Pinellas County Florida Site Environmental Restoration Project Sitewide Environmental Monitoring Semiannual Progress Report for the Young - Rainey STAR Center December 2012 Through May 2013 June 2013

LMSPINN01796

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page i

Contents Abbreviations iii 10 Introduction 1

11 Building 100 Area 2 12 Northeast Site 5 13 WWNA 7 14 Site Update 9 15 Waste Minimization 9

20 Water-Level Elevations 9 21 Groundwater Flow 9

30 Groundwater Sampling 10 31 Work Performed 10 32 Quality AssuranceQuality Control 11

40 Plume Stability Monitoring 12 50 Upcoming Tasks 13 60 References 13

Figures Figure 1 Young - Rainey STAR Center Location 16 Figure 2 Location of STAR Center Solid-Waste Management Units (SWMUs) 17 Figure 3 Building 100 Area Shallow Surficial Aquifer Flow March 2013 18 Figure 4 Building 100 Area Deep Surficial Aquifer Flow March 2013 19 Figure 5 Building 100 Area TCOPCs Concentrations March 2013 20 Figure 6 Building 100 Area South TCOPCs Concentrations March 2013 21 Figure 7 Building 100 Area TCE Concentrations March 2013 22 Figure 8 Building 100 Area cDCE Concentrations March 2013 23 Figure 9 Building 100 Area South cDCE Concentrations March 2013 24 Figure 10 Building 100 Area VC Concentrations March 2013 25 Figure 11 Building 100 Area South VC Concentrations March 2013 26 Figure 12 Building 100 Area 14-dioxane Concentrations March 2013 27 Figure 13 Building 100 Area South 14-dioxane Concentrations March 2013 28 Figure 14 Building 100 Area Plume Stability Monitoring Cross-Sections 29 Figure 15 Cross-Section E1-E2 30 Figure 16 Cross-Section E3-E4 31 Figure 17 Cross-Section E5-E6 32 Figure 18 Cross-Section S1-E2 33 Figure 19 Cross-Section S2-S3 34 Figure 20 Cross-Section S4-S5 35

Tables Table 1 Groundwater-Level Data at the STAR Center March 2013 36 Table 2 Surface Water Elevations March 2013 41

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page ii

Table 3 Field Measurements of Samples Collected at the STAR Center March 2013 42 Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 45 Table 5 COPC Concentrations at the Building 100 Area 46 Table 6 Sum of COPCs for Each Plume Stability Monitoring Cross-Section 49 Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-section 50

Plates Plate 1 Sitewide Shallow Surficial Aquifer Contours Pinellas Florida March 2013 Plate 2 Sitewide Deep Surficial Aquifer Contours Pinellas Florida March 2013

Appendix Appendix A Laboratory Reports March 2013 Semiannual Monitoring

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page iii

Abbreviations cDCE cis-12-dichloroethene

CMIP Corrective Measures Implementation Plan

CMS Corrective Measures Study

CMT continuous multichannel tubing

COPC contaminant of potential concern

CTL cleanup target level

11-DCE 11-dichloroethene

DOE US Department of Energy

EPA US Environmental Protection Agency

FAC Florida Administrative Code

FDEP Florida Department of Environmental Protection

ft feet (foot)

HSWA Hazardous and Solid Waste Amendments

IC Institutional Control

IWNF industrial wastewater neutralization facility

LDA large-diameter auger

LM Office of Legacy Management

MCL maximum contaminant level

μgL micrograms per liter

NAPL nonaqueous phase liquid

POTW Publicly Owned Treatment Works

QAQC quality assurancequality control

RBCA Risk-Based Corrective Action

RCRA Resource Conservation and Recovery Act

RFA RCRA Facility Assessment

RPD relative percent difference

SEEPro Site Environmental Evaluation for Projects

STAR Center Young - Rainey Science Technology and Research Center

SWMU solid-waste management unit

TCE trichloroethene

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page iv

TCOPCs total contaminants of potential concern

tDCE trans-12-dichloroethene

VC vinyl chloride

WWNA Wastewater Neutralization AreaBuilding 200 Area

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796

10 Introduction The Young - Rainey Science Technology and Research Center (STAR Center) at the Pinellas County Florida Site is a former US Department of Energy (DOE) facility constructed in the mid-1950s The 99-acre STAR Center is located in Largo Florida and lies in the northeast quarter of Section 13 Township 30 South Range 15 East (Figure 1) While it was owned by DOE the facility primarily manufactured neutron generators for nuclear weapons Other products manufactured at the STAR Center have included radioisotope-powered thermoelectric generators thermal batteries specialty capacitors crystal resonators neutron detectors lightning-arrestor connectors and vacuum-switch tubes In 1987 the US Environmental Protection Agency (EPA) performed a Resource Conservation and Recovery Act (RCRA) Facility Assessment (RFA) (EPA 1988) at the site to gather information on potential releases of hazardous materials In February of 1990 EPA issued a Hazardous and Solid Waste Amendments (HSWA) permit to DOE enabling DOE to investigate and perform remediation activities in those areas designated as solid-waste management units (SWMUs) contaminated by hazardous materials resulting from DOE operations On March 17 1995 DOE sold the facility to the Pinellas County Industrial Council The sales contract included clauses to ensure continued compliance with federal state and local regulations while DOE remediates the site On July 1 1999 the Pinellas County Industrial Council was disestablished and ownership of the STAR Center changed to the Pinellas County Industrial Development Authority In November 2000 the State of Florida received HSWA authorization from EPA The Florida Department of Environmental Protection (FDEP) issued a new HSWA permit to DOE in January 2002 The permit was reissued on August 21 2007 and was modified under the provisions of Section 403722 Florida Statutes and Chapters 62-4 62-160 62-730 62-777 and 62-780 Florida Administrative Code (FAC) to incorporate the Global Risk-Based Corrective Action (RBCA) regulations The permit was revised and reissued again on January 9 2012 The administration of DOE activities at the facility is the responsibility of the DOE Office of Legacy Management (LM) in Grand Junction Colorado SM Stoller Corporation a prime contractor to LM provides technical support to DOE for remediation and closure of all active SWMUs onsite The EPA RFA Report and the HSWA permit identified 15 sites at the former DOE facility that might have environmental contamination as a result of past activities Upon completion of the RCRA Facility Investigation (DOE 1991a) 11 of the 15 SWMUs were recommended by DOE and approved by EPA Region 4 and FDEP for no further action (DOE 1994) A twelfth site the Former Pistol Range Site was remediated in 1993 it was recommended by DOE and approved by EPA Region 4 and FDEP for no further action Two additional SWMUs the West Fenceline Site and the Wastewater Neutralization Area Building 200 Area (WWNA) were identified after the HSWA permit was issued bringing the total to 17 SWMUs that have been identified and investigated at the STAR Center The remediation of the West Fenceline Site was completed in 1997 and DOE recommendedand EPA Region 4 and FDEP approvedno further action for a total of 13 SWMUs remediated A Corrective Measures Study (CMS)Corrective Measures Implementation Plan (CMIP) was

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page 2

prepared and submitted in 1997 to EPA Region 4 and FDEP to address the contamination at the WWNA Therefore four active SWMUs currently exist at the STAR Center These four SWMUs are the Old Drum Storage Site (PIN06) the Industrial Drain LeaksBuilding 100 Area (PIN12) the Northeast Site (PIN15) and the WWNA (PIN18) Two SWMUs PIN06 and PIN12 are collectively known as the Building 100 Area Figure 2 depicts the location of the four SWMUs DOE plans to proceed with closure of the WWNA under RBCA Risk Management Option II and to apply the default poor quality arsenic cleanup target level (CTL) of 100 micrograms per liter (μgL) to onsite groundwater Closure monitoring was completed in October 2006 A No Further Action with Controls proposal for the site was approved by FDEP in May 2007 Acceptance of this closure proposal by FDEP indicates that both soil and groundwater cleanup are complete Closure of the site can be finalized once Institutional Controls (ICs) are implemented DOE is working with the landowner (Pinellas County Industrial Development Authority) to establish ICs at the STAR Center Once ICs are in place there will be no potential for current or future exposure to contaminated groundwater ICs will need to be established and approved by FDEP before a formal No Further Action determination can be made Currently DOE is working with the STAR Center to develop a covenant that incorporates the ICs that will then become part of DOErsquos Long-Term Surveillance and Maintenance Plan at this site Additional background information relative to each SWMU is briefly described below This document serves as the semiannual progress report for each of these four SWMUs The results of recent monitoring activities and a summary of ongoing and projected work are provided in this report 11 Building 100 Area The Building 100 Area is made up of two SWMUs the Industrial Drain LeaksBuilding 100 (PIN12) and the Old Drum Storage Site (PIN06) The Old Drum Storage Site lies beneath and adjacent to the northwest corner of the main building that covers approximately 11 acres located near the southeast corner of the STAR Center (Figure 2) Building 100 is the most notable feature of the STAR Center having housed the majority of the laboratory and production facilities during DOE ownership of the facility One source of contamination at the Building 100 Area is leaks from a liquid waste drain system composed of individual drainage systems previously used for health physics chemical sanitary and storm-water systems The drain systems were flushed grouted and abandoned by 1997 and some of the chemical drain systems were replaced by an aboveground system (DOE 1997a) The Old Drum Storage Site is the former location of a concrete storage pad This area was equipped with a drain and containment system and was once used to store hazardous waste The waste stored at this location included methylene chloride ignitable liquids arsenic and calcium chromate solids Empty drums containing residual waste solvents also were stored in this area A RCRA Facility Investigation was conducted in 1991 at the Pinellas Plant to fulfill the requirements of the HSWA permit and a RCRA Facility Investigation report was produced in 1991 A subsequent report addendum was completed in March 1992 Based on the findings in


these two documents in accordance with the HWSA permit EPA notified DOE of the requirement for a CMS for the Old Drum Storage Site and the Industrial Drain Leaks Building 100 SWMUs The CMS report for the Industrial Drain LeaksBuilding 100 and the Old Drum Storage Site proposed remediation of these two SWMUs together (collectively referred to as the Building 100 Area) The report was submitted to EPA and was subsequently approved on June 9 1994 FDEP approved the CMS report on January 18 1995 The CMS report concluded that pump-and-treat with the existing air-stripping system was the preferred corrective measure for the Building 100 Area This conclusion was based on shallow monitoring-well data that suggested contamination was confined to shallow groundwater at the northwest corner of the building However that characterization was later found to be incomplete Two recovery wells were installed at the northwest corner of the building in 1995 The Building 100 Area Corrective Measures Implementation Plan (DOE 1996a) describes the installation of the wells and the operations and monitoring plan These recovery wells PIN12-RW01 and -RW02 extracted groundwater and pumped the water through secondary containment piping to the Northeast Site treatment system for pretreatment air stripping and discharge to the STAR Center industrial wastewater neutralization facility (IWNF) prior to transfer to the Publicly Owned Treatment Works (POTW) The Northeast Site treatment system was decommissioned in April 2004 so a smaller air-stripper treatment system was installed at the Northeast Site to treat the groundwater recovered via the two Building 100 Area recovery wells Subsequent to recovery well installation additional investigations were conducted by installing monitoring wells at multiple depths both outside the building and through the floor of the building In 1996 these investigations were summarized in the Building 100 Area Data Report (DOE 1996b) and the Building 100 Area Subsurface Investigations Phases I II and III (DOE 1996c) Results of these investigations indicated that (1) significant contaminant concentrations were present at intermediate and deep depths under the building and (2) low levels of contamination were present at the south and east sides of the building The Building 100 Area Data Report recommended that DOE continue operating the two recovery wells that were installed in accordance with the CMSCMIP conduct additional characterization under the building and east of the building conduct additional contaminant transport modeling and evaluate the potential for occurrence of dense nonaqueous phase liquids (NAPLs) These recommendations were addressed in the Building 100 Area Corrective Measures Implementation Plan Addendum (DOE 1998) A pilot test study was conducted in 2003ndash2004 to determine the effectiveness of enhanced biodegradation for this site (DOE 2005) The pilot test results were positive but the test did not result in significant elimination of vinyl chloride (VC) in low-concentration areas Therefore enhanced biodegradation technologies were not considered for use at the Building 100 Area at that time The Building 100 Area Corrective Measures Study Report Addendum (DOE 2006) was finalized in July 2006 The document concluded that DOErsquos original remediation objective of meeting maximum contaminant levels (MCLs) throughout the contaminant plume does not appear to be


reasonable given current knowledge of the site At that time it appeared that containment of the contaminant plume had been achieved and it was determined that human health and the environment were protected The document proposed that ICs be placed on the site property to prevent inappropriate groundwater use and that MCLs for site-related contaminants of potential concern (COPCs) be applied as groundwater cleanup goals outside the IC boundary Because the two existing groundwater recovery wells did not contribute significantly to either contaminant plume containment or mass removal DOE also proposed shutting down these wells and the associated treatment system Operation of these recovery wells and the treatment system was terminated on August 21 2006 with the approval of FDEP An interim remedial action using a single recovery well to collect hydraulic information began in July 2009 and ended in May 2011 Located in the south plume near the southern STAR Center property boundary recovery well PIN12-RW03 had a radius of influence that likely captured the entire south plume as it exited the property Operation of this recovery well ceased in May 2011 to allow treatment of the groundwater produced during the Countyrsquos road work (discussed below) Pinellas County Utilities started a major water line replacement effort along Belcher Road in October 2010 and Pinellas County Public Works started a significant road construction project along Belcher and Bryan Dairy Roads in October 2011 In July 2011 DOE began treating groundwater produced by dewatering conducted during these projects Treatment ended in January 2012 The extracted groundwater was transported to an onsite air stripper for treatment and the treated water was discharged to the STAR Centerrsquos IWNF and subsequently discharged to the POTW Prior to the start of the water line and road projects DOE installed new monitoring wells at the property boundary along the two roads in October 2007 and in January and February 2008 to further define the contaminant plume This investigation confirmed that the plume was offsite south of Bryan Dairy Road on the county right-of-way DOE performed the required notification to FDEP regarding the offsite plume Additional plume delineation was conducted on the property at 8040 Bryan Dairy Road by the installation of three continuous multichannel tubing (CMT) wells in September 2009 (PIN12-0567 -0568 and -0569) Contaminant concentrations exceeded CTLs in well PIN12-0569 DOE reported this discovery to FDEP and to the property owner in October 2009 in accordance with FDEP notification requirements Two additional CMT wells were installed on this property in March 2010 (PIN12-0570 and -0571) To further investigate the extent of the offsite contamination to the south of the STAR Center plume delineation work was conducted at 10980 Belcher Road on August 16ndash30 2010 using direct-push technology to collect groundwater samples from temporary locations This property is located across Bryan Dairy Road immediately south of the Building 100 Area at the STAR Center The results of this investigation indicated that the contaminant plume enters the 10980 Belcher Road property on the western side and extends southeastward (in the direction of groundwater flow) to the southern property boundary DOE reported this discovery to FDEP and to the property owner in October 2010 in accordance with FDEP notification requirements The


results of this investigation are reported in the Building 100 Area Off-Site Plume Delineation South of Bryan Dairy Road Data Report for Rally Stores Property (DOE 2010a) The results from that investigation suggested that the contaminant plume extended south onto property at 10950 Belcher Road Plume delineation was conducted at this property on December 6ndash16 2010 and April 4ndash6 2011 Additional delineation was conducted in the median of Belcher Road just east of this property on January 24ndash28 2011 The results of these investigations demonstrated that the contaminant plume extends in a southeasterly direction from the northern property boundary to the eastern property boundary but not to the median of Belcher Road The results of these investigations are reported in the South Belcher Road Data Report (Daniel 2011a) and the Better Business Forms Data Report (Daniel 2011b) Delineation of the eastern plume at the Building 100 Area was conducted in May June August and September 2011 This work identified a contaminant plume extending from under the eastern edge of Building 100 past the eastern STAR Center property boundary under Belcher Road and onto 11111 Belcher Road DOE made the required notification to FDEP regarding the offsite plume 14-dioxane was measured at elevated concentrations during this work and as a result was added as a COPC for the Building 100 Area in a letter from DOE to FDEP dated October 13 2011 (DOE 2011) Additional delineation at 11111 Belcher Road in March and April 2012 defined the extent of the eastern contaminant plume which appears to attenuate quickly after entering the property The Building 100 Area Site Assessment Report (DOE 2012a) summarizes the results of the plume delineation work conducted at the Building 100 Area and the adjacent private properties from 2007 to 2012 The action proposed in this document is to conduct plume stability monitoring of both the onsite and offsite plumes The Plume Stability Monitoring Plan for the Building 100 Area is included in the Site Monitoring Plan which is an Appendix to the Long-Term Surveillance and Maintenance Plan for the Pinellas Site (DOE 2012b) Plume stability monitoring began with the March 2013 sampling event 12 Northeast Site The Northeast Site is located in the northeast corner of the STAR Center (Figure 2) In the late 1960s before construction of the East Pond in 1968 drums of waste and construction debris were disposed of in the swampy area of the Northeast Site In 1986 an expansion of the East Pond was initiated to create additional storm-water retention capacity but excavation activities ceased when contamination was detected directly west of the pond EPA identified the Northeast Site as a SWMU (EPA 1992) An Interim CMS (DOE 1991b) was developed and submitted to EPA and approval of this document was received in October 1991 An interim groundwater recovery system for the Northeast Site was installed and operation commenced in January 1992 The groundwater treatment system as initially installed consisted of four recovery wells equipped with pneumatic pumps a holding tank centrifugal transfer pumps and approximately 2500 feet (ft) of transfer and secondary containment piping During 1993 DOE proposed a reconfigured system for the site consisting of four shallow and three deep recovery wells After EPA approved the upgrade the system was reconfigured and became operational on March 1 1994


Between August and October 1995 a portion of the Northeast Site was excavated to remove debris drums of waste and other materials that could inhibit future corrective measures Location of the areas of excavation was based primarily on the results of a geophysical survey and knowledge of existing utility locations Detailed descriptions of the debris removal activities were submitted to EPA and FDEP as part of the Northeast Site Interim Measures Quarterly Progress Report (DOE 1996d) In 1996 DOE submitted the Northeast Site Corrective Measures Implementation Plan (DOE 1996e) to EPA Region 4 and FDEP This plan was approved by both regulatory agencies in 1997 As part of the Northeast Site CMS and CMIP a pump-and-treat system in conjunction with a subsurface hydrogeologic barrier wall to prevent migration of the contaminant plume was identified as the best available technology The pump-and-treat system included a pretreatment system for iron removal an air stripper unit and a tank for holding treated groundwater before discharge to the STAR Center IWNF prior to transfer to the POTW The treatment system was constructed in early 1997 and became operational by July 1997 processing groundwater from seven Northeast Site recovery wells and two Building 100 Area recovery wells Subsequently several additional recovery wells were installed at the Northeast Site and some of the old recovery wells were abandoned During 1997 anaerobic bioremediation and rotary steam-stripping pilot tests were conducted in the northern and southern portions of the Northeast Site respectively These tests were designed by the Innovative Treatment Remediation Demonstration group of regulatory and industry members to provide remedial options at the STAR Center At the conclusion of the field tests in July 1997 pump-and-treat technology resumed at the Northeast Site NAPLs were identified in a few monitoring and recovery wells in 1998 An Interim Measures Work Plan for Remediation of Non-Aqueous Phase Liquids at the Northeast Site (DOE 2001) was submitted to FDEP in late November 2001 The purpose of this document was to present the plan to remediate NAPLs at two areas (NAPL Areas A and B) of the Northeast Site using a thermal remediation method FDEP approved this document on January 10 2002 Construction of the NAPL Area A treatment system began in late May 2002 and system startup occurred on September 26 2002 NAPL treatment was completed on February 28 2003 The Northeast Site Area A NAPL Remediation Final Report (DOE 2003) describes the thermal remediation of Area A Construction of the NAPL Area B treatment system began in July 2004 and was completed in early August 2005 and operations began on August 16 2005 NAPL treatment was completed on August 29 2006 The Final Report Northeast Site Area B NAPL Remediation Project at the Young - Rainey STAR Center Largo Pinellas County Florida (DOE 2007) describes Area B remediation Monitoring wells were installed at the former NAPL areas to monitor the remaining dissolved-phase plumes Groundwater samples from a few of the wells continued to show high concentrations of contaminants Soil samples were collected from 12 soil borings in August 2007 to evaluate the potential for a contaminant source remaining in the subsurface at these locations Results indicated high contaminant concentrations in soil at most of these borings so a second phase of sampling was conducted in March and April 2008 during which samples were collected


from 45 soil borings Ten additional borings were sampled in May and 11 more were sampled in June These 78 soil borings defined two areas containing a source of contamination To address this contamination source DOE prepared an interim remedial action plan for soil excavation using the large-diameter auger (LDA) method in accordance with the RBCA regulations and submitted the document to FDEP in August 2008 This plan was approved on August 22 2008 An engineering design was developed and a source removal subcontract was awarded in 2008 Source removal in the form of LDA excavation began on January 14 2009 and was completed on May 22 2009 Two hundred forty-three large-diameter and 352 small-diameter borings were completed Approximately 8387 cubic yards of soil were excavated including 4667 cubic yards removed as clean overburden and 3720 cubic yards of contaminated soils that were removed characterized for waste disposal and disposed of as nonhazardous waste at a RCRA Subtitle D landfill Additional information regarding the Northeast Site LDA work is available in the Data Report for Overburden Soil at the Northeast Site and the 45 Acre Site (DOE 2009a) and the Interim Remedial Action for Source Removal at the Northeast Site Final Report (DOE 2009b) As a follow-up to the LDA work emulsified soybean oil and the Dehalococcoides ethenogenes microorganism were injected into the subsurface at 75 points at the site in January and February 2010 The Injection of Emulsified Soybean Oil at the Northeast Site and 45 Acre Site (DOE 2010b) was prepared to describe the work required for this task This project has resulted in a significant decrease in contaminant mass and concentration around the former contaminant source areas and in the downgradient contaminant plume With the completion of the LDA project to remove contaminant source material and the follow-up enhanced bioremediation project DOE is proceeding to close the Northeast Site under the FDEPrsquos RBCA rules (Chapter 62-780680 FAC) The Closure Monitoring Plan for the Northeast Site and 45 Acre Site (DOE 2009c) describes the closure monitoring that is necessary under RBCA according to the requirements for Post Active Remediation Monitoring (Chapter 62-780750 FAC) Closure monitoring was implemented starting with the September 2009 sampling event and was completed in September 2012 COPCs concentrations decreased significantly over this time period DOE submitted the Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site (DOE 2013) to FDEP in May 2013 That document proposes a risk-based closure for the Northeast Site under the Statersquos RBCA regulations 13 WWNA The WWNA (PIN18) includes the IWNF the area south of the IWNF (including the parking lot) and Building 200 (Figure 2) In April 1993 the WWNA and the Building 200 Area were identified as potential SWMUs and an RFA was conducted (EPA 1994) The RFA recommended that the WWNA and Building 200 be considered one SWMU and this SWMU is now referred to as the WWNA RFA field activities began in September 1994 and included soil characterization monitoring well installation and groundwater sampling Arsenic was identified as the major COPC Trichloroethene (TCE) and VC were detected at low concentrations in groundwater and were subsequently dismissed as COPCs once their concentrations decreased below cleanup levels


A CMSCMIP (DOE 1997b) was completed for this SWMU in 1997 The recommended remediation alternative for the WWNA was groundwater recovery with the Building 100 Area wells and an additional recovery well located in the WWNA The CMIP recommended (1) that the recovery well in the WWNA withdraw surficial aquifer groundwater directly from the arsenic plume thereby reducing contaminant mass and preventing contaminant migration and (2) that the recovered water be discharged directly to the STAR Centerrsquos wastewater neutralization facility Because FDEP expressed concerns about elevated concentrations of arsenic in the soil DOE conducted extensive sampling and analysis of soil in January and February 1999 in an effort to locate the source of arsenic contamination Elevated levels of arsenic were identified at several locations and at various depths within the SWMU A treatability study was conducted to determine the leachability of arsenic from the soil into the groundwater The study concluded that arsenic leachability from the soil was very limited as demonstrated by a measured average soilwater distribution coefficient of 63 liters per kilogram DOE then conducted a statistical evaluation of arsenic soil data that resulted in the proposal to excavate two areas where the highest concentrations of arsenic were identified Follow-up monitoring of strategically located wells would then determine whether arsenic concentrations in the groundwater decrease with time This proposal was approved by FDEP in September 1999 An excavation plan was developed to address logistics sampling and analytical concerns and waste management issues regarding the generation of contaminated media This document and the statistical evaluation are included in the WWNA CMIP Addendum (DOE 2000) Excavation of the two areas was completed in early October 1999 Subsequently the existing recovery well was abandoned and two recovery wells were installed to continue plume control in the area In addition a third recovery well was created by converting the monitoring well with the highest arsenic concentration (PIN18-0501) to a recovery well On December 20 2005 DOE received concurrence from FDEP to shut down the groundwater recovery system and begin monitoring to determine a closure approach through FDEPrsquos RBCA regulations promulgated by the Florida Legislature in 2003 The 1-year RBCA closure monitoring program specified by FDEP began in October 2005 and was completed in October 2006 A No Further Action with Controls proposal was submitted to FDEP on March 14 2007 FDEP approved the document on May 24 2007 and requested that DOE submit an updated Statement of Basis for the WWNA Submittal of the Statement of Basis is awaiting finalization of ICs at the STAR Center The goal of the 1999 soil excavation was to remove the areas containing the highest arsenic concentrations such that the remaining soils met the industrial CTL of 12 milligrams per kilogram Soils containing arsenic concentrations above the residential CTL of 21 milligrams per kilogram were left in place because the current site use is solely industrial After the No Further Action with Controls proposal was submitted in 2007 FDEP expressed concern about arsenic exceeding the residential standard in shallow soils (less than 2 ft deep) In response DOE determined that a potential course of action was to identify the area where the residential arsenic


standard is exceeded and apply an IC that would prohibit future residential development in this area Negotiations to apply the IC are ongoing 14 Site Update

FDEP verbally approved cessation of closure monitoring at the Northeast Site during a teleconference with DOE on January 17 2013

The Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site (DOE 2013) was submitted to FDEP in May 2013

Twenty-seven new monitoring wells (ie nine well triples) were installed at the Building 100 Area in February 2013 to facilitate plume stability monitoring

Twenty monitoring wells at the Building 100 Area and three monitoring wells at the WWNA were abandoned on April 22 and 23 2013

The sitewide semiannual sampling was conducted March 4ndash14 2013 and included collection of water samples from 100 monitoring wells Water level measurements were obtained from all accessible monitoring wells recovery wells and ponds on March 5

The results of semiannual monitoring were reported (this document) 15 Waste Minimization The following materials were recycled at the Pinellas site from December 2012 through May 2013

31 pounds of paper

23 pounds of cardboard

7 pounds of plastic

43 pounds of magazines

1 pound of aluminum

16 pounds of batteries

20 Water-Level Elevations Depth-to-water measurements were taken at all accessible monitoring wells piezometers and ponds (including two offsite ponds) at the STAR Center on March 5 2013 The water levels were measured with an electronic water level indicator or directly from a staff gauge Groundwater elevations are listed in Table 1 21 Groundwater Flow Groundwater and surface water elevations were used to construct sitewide groundwater contour maps of the shallow and deep surficial aquifers (Plates 1 and 2 respectively) Individual contour maps were also constructed for the shallow and deep surficial aquifers at the Building 100 Area (Figures 3 and 4)


For the past several years shallow groundwater beneath Building 100 has been observed to flow to the southeast under a very slight gradient and this flow pattern was observed again in March 2013 (Figure 3) A similar flow pattern was observed in the deep surficial aquifer (Figure 4) The hydraulic gradient in the Building 100 Area in March 2013 was about 0002 ftft onsite and about 0005 offsite Based on calculations using Darcyrsquos Law along with approximations of 1 ftday for hydraulic conductivity and 03 for effective porosity groundwater velocity in this area is estimated to be about 24 to 61 ftyear An aquifer test conducted in July 2009 in the area around recovery well RW03 indicated that the hydraulic conductivity of the surficial aquifer around well RW03 might be higher than that observed in other parts of the STAR Center Analysis of the aquifer test yielded an estimated hydraulic conductivity of 67 to 74 ftday which is higher than previous tests conducted in other areas of the STAR Center where estimated hydraulic conductivities were closer to 1 ftday Surface water elevations were recorded in March 2013 from the East South Southwest and West Ponds Pond 5 and the pond just east of Belcher Road (Table 2) All the ponds are hydraulically connected to the shallow surficial aquifer system (Plate 1)

30 Groundwater Sampling 31 Work Performed During the annual sampling event at the STAR Center in March 2013 groundwater samples were collected from 100 monitoring wells at the Building 100 Area Volatile organic compounds were analyzed in these samples using EPA SW-846 method 8260B and 14-dioxane was analyzed in the same samples using EPA method 8260B SIM Laboratory reports are provided in Appendix A The analytical results are discussed in Section 4 Figures 5ndash13 are plume maps for the Building 100 Area for March 2013 Figures 5 and 6 show the total COPCs (TCOPCs) concentrations TCOPCs is the sum of the individual COPC concentrations for each well The Building 100 Area COPCs are TCE cis-12-dichloroethene (cDCE) trans-12-dichloroethene (tDCE) 11-dichloroethene (11-DCE) VC and 14-dioxane Figures 7ndash13 show the plumes for the individual COPCs a plume map for tDCE is not shown because this COPC exceeded the CTL only in well 12-S35B All samples were collected in accordance with the Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites (LMSPROS04351) using FDEP procedures All samples were submitted to TestAmerica Laboratories Inc in Denver Colorado for analysis TestAmerica Denver is accredited by the Florida Department of Health in accordance with the National Environmental Laboratory Accreditation Conference (certification number E87667) All monitoring wells were micropurged using a dedicated bladder pump or a peristaltic pump Sampling was performed when the field measurements stabilized in accordance with FDEP procedures Table 3 lists field measurements of temperature specific conductance turbidity pH oxidation-reduction potential and dissolved oxygen recorded at the time the samples were


collected Measurements were made using a calibrated multiparameter meter with a flow cell and turbidity was measured using a nephelometer 32 Quality AssuranceQuality Control The results from the analytical laboratory TestAmerica Denver were checked for quality assurancequality control (QAQC) through duplicate samples and trip blanks The duplicate sample results were compared and the relative percent differences (RPDs) between the results were calculated (Table 4) trans-12-Dichloroethene in well PIN12-0580-2 VC in well PIN12-0582-2 and 11-dichloroethene in well PIN12-0587-2 all had RPD values that exceeded the EPA-recommended laboratory duplicate criterion of less than 20 RPD for results that are greater than 25 times the method detection limit These results were ldquoJrdquo qualified as estimated values due to the poor RPD value Table 4 also lists analytes in the duplicate samples from wells 12-0581-2 and 12-0582-2 that did not have an RPD calculated because the results were less than 25 times the method detection limit Some of these results show significant disagreement (eg 14-dioxane in well 12-0582-2) The poor precision of these results may be due to the fact that the laboratory diluted the original samples but not the duplicate samples These two wells were installed in February 2013 and sampled for the first time in March 2013 so historical data were not available to compare to the current results A detailed review of the chromatograms and mass spectra in the lab reports for original and duplicate samples collected from these wells confirmed the presence of the detected analytes in the duplicate samples This confirmation in combination with the results from temporary sampling points nearby in 2011 (see Section 11) strongly suggested that the results for the duplicate samples were the most representative for these wells Therefore the results from the original samples were excluded and the results from the duplicate samples are reported in this document This issue will be revisited after the second sampling event at these wells in September 2013 As specified in the Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites duplicate samples should be collected at a frequency of one duplicate for every 20 or fewer samples For the STAR Center and the 45 Acre Site 119 samples and 6 duplicates were collected for volatiles analysis and 100 samples and 5 duplicates were collected for 14-dioxane analysis The duplicate requirements for this sampling event were met Six trip blanks and two equipment blanks also were collected during this event A data validation software module for identifying and tracking anomalous groundwater data within the Site Environmental Evaluation for Projects (SEEPro) database was used to generate a report of analytical results that fall outside of historical minimum or maximum values No anomalous results were identified


40 Plume Stability Monitoring The Plume Stability Monitoring Plan for the Building 100 Area is included in an appendix to the Long-Term Surveillance and Maintenance Plan for the Pinellas Site (DOE 2012b) This plan defines the strategy to determine the stability of the onsite and offsite plumes The plume stability monitoring approach involves establishment of plume cross-sections using certain sets of wells and the determination of an area under the curve for each cross-section The cross-section lines are shown on Figure 14 The lateral cross-sections allow evaluation of the entire width of each plume as it emerges from under the building and at the site boundary if the plume is expanding laterally (concentrations increasing at the sides of the plume) this will be seen as an increase in the area under the curve The longitudinal cross-section in each plume will use wells in the centerline of the plume (the highest concentration area) to determine if the plume is expanding at its leading edge and if concentrations are decreasing stable or increasing in the plume centerline Each ldquodata pointrdquo in the cross-sections is the location of a well triple (ie wells with three different screened intervals) or a well pair The value plotted at each data point is the sum of COPC concentrations in all sampled intervals in the well pair or triple at that location For example in cross-section E1-E2 the northern data point will be the sum of TCE cDCE tDCE 11-DCE VC and 14-dioxane concentrations measured in wells 12-0555A 12-0555B and 12-0555C

For each sampling event a ldquocurverdquo will be plotted for each cross-section and then the area under the curve will be calculated The area under the curve values will be tracked from event to event and a trend line will be fit to the data The plume will be designated as unstable if an increasing trend is observed

In addition to the plume stability monitoring scheme presented above several wells that are not part of a cross-section will also be sampled to determine whether the plume is advancing at any of its boundaries (Figure 14) At each of these well locations the COPC concentrations from all screened intervals will be summed and the sum will be plotted For example for the well triple 0570 located on the Harrod property the COPC concentrations in all three screened intervals (0570-1 -2 and -3) will be summed and plotted A trend line will be fit to the plotted data and as with the area under the curve values the plume will be designated as unstable if an increasing trend is observed The March 2013 sampling event was the first plume stability monitoring event The COPCs concentrations from each well are listed in Table 5 The sum of COPCs at each ldquodata pointrdquo in each cross-section is listed in Table 6 Figures 15ndash20 show the curve plots for each cross-section The area under the curve for each cross-section is listed in Table 7 The area under the curve value is calculated using a spreadsheet it is not the sum of the COPCs in each cross-section Because the March 2013 sampling event was the first plume stability monitoring event the area under the curve values are not plotted because there is only one data point for each cross-section The area under the curve values will be plotted after the second plume stability monitoring event in September 2013


50 Upcoming Tasks The following major tasks are planned for the next semiannual period (June through November 2013)

Plume stability monitoring at the Building 100 Area will continue with the semiannual sampling event in September 2013

60 References Daniel 2011a Joe Daniel Site Manager Pinellas Environmental Restoration Project SM Stoller Corporation letter (about the South Belcher Road Data Report) to Scott Surovchak Pinellas Site Manager Office of Legacy Management US Department of Energy April 4 Daniel 2011b Joe Daniel Site Manager Pinellas Environmental Restoration Project SM Stoller Corporation letter (about the Better Business Forms Data Report) to Scott Surovchak Pinellas Site Manager Office of Legacy Management US Department of Energy May 13 DOE (US Department of Energy) 1991a Environmental Restoration Program RCRA Facility Investigation Report Pinellas Plant (Draft) Albuquerque Operations Office Albuquerque New Mexico September DOE (US Department of Energy) 1991b Interim Corrective Measures Study Northeast Site Pinellas Plant Largo Florida May DOE (US Department of Energy) 1994 Statement of Basis for Twelve Solid Waste Management Units Recommended for No Further Action Pinellas Plant Largo Florida January DOE (US Department of Energy) 1996a Building 100 Area Corrective Measures Implementation Plan (Draft) Environmental Restoration Program Pinellas Plant Largo Florida January DOE (US Department of Energy) 1996b Building 100 Area Data Report October 1993 to July 1996 Office of Legacy Management Grand Junction Colorado November DOE (US Department of Energy) 1996c Building 100 Area Subsurface Investigations Phases I II and III Volumes 1 and 2 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 1996d Northeast Site Interim Measures Quarterly Progress Report October through December 1995 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 1996e Northeast Site Corrective Measures Implementation Plan Office of Legacy Management Grand Junction Colorado March


DOE (US Department of Energy) 1997a Pinellas Plant Environmental Baseline Report prepared by Lockheed Martin Specialty Components Inc for DOE Pinellas Area Office June DOE (US Department of Energy) 1997b Corrective Measures Study ReportCorrective Measures Implementation Plan WWNABuilding 200 Office of Legacy Management Grand Junction Colorado June DOE (US Department of Energy) 1998 Building 100 Area Corrective Measures Implementation Plan Addendum Pinellas STAR Center Largo Florida February DOE (US Department of Energy) 2000 WWNABuilding 200 Corrective Measures Implementation Plan Addendum Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 2001 Interim Measures Work Plan for Remediation of Non-Aqueous Phase Liquids at the Northeast Site MAC-PIN 13105-1 prepared for DOE Grand Junction Office Grand Junction Colorado November DOE (US Department of Energy) 2003 Northeast Site Area A NAPL Remediation Final Report GJOminus2003minus482minusTAC prepared by US Department of Energy Grand Junction Colorado September DOE (US Department of Energy) 2005 Building 100 Area Enhanced Bioremediation Pilot Test Final Report DOE-LMGJ791-2005 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 2006 Building 100 Area Corrective Measures Study Report Addendum DOE-LMGJ1241-2006 Office of Legacy Management Grand Junction Colorado July DOE (US Department of Energy) 2007 Final Report Northeast Site Area B NAPL Remediation Project at the Young - Rainey STAR Center Largo Pinellas County Florida DOE-LM1457-2007 Office of Legacy Management Grand Junction Colorado April DOE (US Department of Energy) 2009a Data Report for Overburden Soil at the Northeast Site and the 45 Acre Site LMSPINN01395 Office of Legacy Management Grand Junction Colorado July DOE (US Department of Energy) 2009b Interim Remedial Action for Source Removal at the Northeast Site Final Report LMSPINN01357 Office of Legacy Management Grand Junction Colorado September DOE (US Department of Energy) 2009c Closure Monitoring Plan for the Northeast Site and 45 Acre Site LMSPINN01401 Office of Legacy Management Grand Junction Colorado August


DOE (US Department of Energy) 2010a Building 100 Area Off-Site Plume Delineation South of Bryan Dairy Road Data Report for Rally Stores Property LMSPINN01535 Office of Legacy Management Grand Junction Colorado October DOE (US Department of Energy) 2010b Injection of Emulsified Soybean Oil at the Northeast Site and 45 Acre Site LMSPINN01494 Office of Legacy Management Grand Junction Colorado April DOE (US Department of Energy) 2011 Scott Surovchak Pinellas Site Manager letter (about Groundwater Samples at the Young-Rainey STAR Center) to John Armstrong Remedial Project Manager FDEP October 13 DOE (US Department of Energy) 2012a Building 100 Area Site Assessment Report LMSPINN01747 Office of Legacy Management Grand Junction Colorado August DOE (US Department of Energy) 2012b Long-Term Surveillance and Maintenance Plan for the Pinellas Site LMSPINN01058-100 Office of Legacy Management Grand Junction Colorado November DOE (US Department of Energy) 2013 Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site LMSPINN01778 Office of Legacy Management Grand Junction Colorado May EPA (US Environmental Protection Agency) 1988 RCRA Facility Assessment Department of EnergymdashFl6 890 090 008 June EPA (US Environmental Protection Agency) 1992 Letter to DOE Gerald W Johnson Approval of Pinellas Site Remedial Facility Investigation Report April EPA (US Environmental Protection Agency) 1994 RCRA Facility Assessment Report WWNABuilding 200 Area March Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites LMSPROS04351 continually updated prepared by SM Stoller Corporation for the US Department of Energy Office of Legacy Management Grand Junction Colorado


Figure 1 Young - Rainey STAR Center Location

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Pinellas S

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emiannual P

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June 2013

Doc N

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Figure 2 Location of STAR Center Solid-Waste Management Units (SWMUs)

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itewide S

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Figure 3 Building 100 Area Shallow Surficial Aquifer Flow March 2013

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itewide S

emiannual P


ecember 2012mdash

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Figure 4 Building 100 Area Deep Surficial Aquifer Flow March 2013

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emiannual P


ecember 2012mdash

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Figure 5 Building 100 Area TCOPCs Concentrations March 2013

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itewide S

emiannual P


ecember 2012mdash

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Page 21

Figure 6 Building 100 Area South TCOPCs Concentrations March 2013

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itewide S

emiannual P


ecember 2012mdash

May 2013

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Figure 7 Building 100 Area TCE Concentrations March 2013

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Figure 8 Building 100 Area cDCE Concentrations March 2013

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Figure 9 Building 100 Area South cDCE Concentrations March 2013

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Figure 10 Building 100 Area VC Concentrations March 2013

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May 2013

June 2013

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Figure 11 Building 100 Area South VC Concentrations March 2013

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itewide S

emiannual P


ecember 2012mdash

May 2013

June 2013

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Figure 12 Building 100 Area 14-dioxane Concentrations March 2013

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June 2013

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Figure 13 Building 100 Area South 14-dioxane Concentrations March 2013


Figure 14 Building 100 Area Plume Stability Monitoring Cross-Sections

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Figure 15 Cross-Section E1-E2

0

50

100

150

200

250

300

350

400

450

0555 0554 0580 S71 S70 S69

E1 ‐ E2March 2013

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0

100

200

300

400

500

600

541542549 0581 0582 539540 S73 0583

E3 ‐ E4March 2013

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May 2013

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0

100

200

300

400

500

600

S67 0580 0582 0576 0578

E5 ‐ E6March 2013

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itewide S

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ecember 2012mdash

May 2013

June 2013

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Figure 18 Cross-Section S1-E2

0

500

1000

1500

2000

2500

3000

3500

4000

4500

5000

0561 0584 0585 524525 S68 S69

S1 ‐ E2March 2013

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itewide S

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ecember 2012mdash

May 2013

June 2013

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Figure 19 Cross-Section S2-S3

0

100

200

300

400

500

600

700

800

900

0586 0587 0588

S2 ‐ S3March 2013

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June 2013

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0

1000

2000

3000

4000

5000

6000

0585 0587 0569 0572 0574 0575

S4 ‐ S5March 2013


Table 1 Groundwater-Level Data at the STAR Center March 2013

Location Measurement Water Depth

(ft bls)

Groundwater Elevation (ft amsl) Date Time

PIN02 Sitewide Piezometers

PZ03 352013 1023 421 1549

PZ04 352013 1029 283 1537

PZ05 352013 1018 356 1454

PZ08 352013 1012 439 1401

PZ09 352013 1344 412 1388

PZ10 352013 1003 454 1434

PZ11 352013 0945 483 1405

Building 100 Area

PIN12

0509 352013 1142 361 1443

0515 352013 0631 428 1362

0516 352013 0609 448 1352

0517 352013 0641 406 1384

0518 352013 0645 397 1397

0520 352013 1132 366 1435

0521 352013 1128 370 1435

0524 352013 0711 366 1375

0525 352013 0657 371 1371

0527 352013 1035 1272 535

0528 352013 1348 1213 547

0539 352013 1413 336 1324

0540 352013 1421 292 1318

0541 352013 0841 484 1282

0542 352013 1424 451 1319

0549 352013 0847 451 1315

0550-1 352013 1436 272 1198

0550-2 352013 1436 262 1208

0550-3 352013 1437 257 1213

0551-1 352013 1425 329 1211

0551-2 352013 1425 293 1247

0551-3 352013 1425 318 1222

0553A 352013 0800 450 1361

0553B 352013 0824 466 1345

0553C 352013 0828 464 1347

0554A 352013 0752 463 1361

0554B 352013 0750 463 1361

0554C 352013 0743 465 1359

0555A 352013 0754 412 1377

0555B 352013 0758 421 1368

0555C 352013 0759 420 1369

0559-1 352013 0926 535 1255

0559-2 352013 1132 507 1283

0559-3 352013 1133 689 1101

Table 1 (continued) Groundwater-Level Data at the STAR Center March 2013



(ft bls)


0560-1 352013 0640 394 1378

0560-2 352013 0639 385 1387

0560-3 352013 0640 370 1402

0561-1 352013 0647 431 1391

0561-2 352013 0656 436 1386

0561-3 352013 0656 434 1388

0562-1 352013 1135 489 1337

0562-2 352013 1140 487 1339

0562-3 352013 1141 484 1342

0563-1 352013 1141 349 1378

0563-2 352013 1342 346 1381

0563-3 352013 1343 341 1386

0564-1 352013 1453 296 1254

0564-2 352013 1454 307 1243

0564-3 352013 1455 313 1237

0565-1 352013 1506 412 1158

0565-2 352013 1507 416 1154

0565-3 352013 1508 413 1157

0566-1 352013 1530 426 1134

0566-2 352013 1530 421 1139

0566-3 352013 1531 423 1137

0567-1 352013 1410 413 1413

0567-2 352013 1411 433 1393

0567-3 352013 1412 457 1369

0568-1 352013 1418 436 1390

0568-2 352013 1419 461 1365

0568-3 352013 1420 459 1367

0569-1 352013 1430 463 1348

0569-2 352013 1431 488 1323

0569-3 352013 1432 488 1323

0571-1 352013 1445 529 1291

0571-2 352013 1446 540 1280

0571-3 352013 1447 534 1286

0572-1 352013 1515 330 1230

0572-2 352013 1516 330 1230

0573-1 352013 1537 328 1172

0573-2 352013 1537 328 1172

0573-3 352013 1537 330 1170

0574-1 352013 1518 541 1089

0574-2 352013 1519 533 1097

0574-3 352013 1520 537 1093

0575-1 352013 1509 491 1039

0575-2 352013 1511 487 1043

0576-1 352013 1411 465 1285

0576-2 352013 1412 453 1297




(ft bls)


0576-3 352013 1412 452 1298

0577-1 352013 1202 464 1326

0577-2 352013 1203 464 1326

0577-3 352013 1204 464 1326

0578-1 352013 1355 425 1355

0578-2 352013 1356 429 1351

0578-3 352013 1357 431 1349

0579-1 352013 1451 421 1319

0579-2 352013 1451 424 1316

0579-3 352013 1452 425 1315

0580-1 352013 0940 486 1364

0580-2 352013 0941 491 1359

0580-3 352013 0942 490 1360

0581-1 352013 1055 412 1324

0581-2 352013 1056 413 1323

0581-3 352013 1057 415 1321

0582-1 352013 1100 353 1320

0582-2 352013 1101 353 1320

0582-3 352013 1102 355 1318

0583-1 352013 1111 342 1309

0583-2 352013 1112 335 1316

0583-3 352013 1113 337 1314

0584-1 352013 0857 379 1381

0584-2 352013 0858 383 1377

0584-3 352013 0859 387 1373

0585-1 352013 0903 368 1381

0585-2 352013 0904 373 1376

0585-3 352013 0905 377 1372

0586-1 352013 1350 387 1353

0586-2 352013 1351 382 1358

0586-3 352013 1352 383 1357

0587-1 352013 1354 402 1348

0587-2 352013 1355 398 1352

0587-3 352013 1356 399 1351

0588-1 352013 1357 396 1344

0588-2 352013 1358 394 1346

0588-3 352013 1359 396 1344

PZ01 352013 1427 415 1335

PZ02 352013 1443 520 1370

PZ03 352013 1437 354 1336

S29C 352013 0911 420 1431

S30B 352013 0918 415 1436

S31B 352013 0853 429 1422

S32B 352013 0900 418 1433

S33C 352013 0937 410 1441




(ft bls)


S35B 352013 0951 439 1412

S36B 352013 0847 461 1390

S37B 352013 0931 408 1443

S67B 352013 1036 439 1408

S67C 352013 1037 448 1399

S67D 352013 1038 448 1400

S68B 352013 1408 404 1386

S68C 352013 1412 428 1362

S68D 352013 1412 424 1366

S69B 352013 0713 260 1340

S69C 352013 0722 262 1338

S69D 352013 0724 277 1323

S70B 352013 0732 311 1359

S70C 352013 0730 305 1365

S70D 352013 0726 323 1347

S71B 352013 0734 448 1392

S71C 352013 0737 480 1360

S71D 352013 0739 475 1365

S72B 352013 0833 495 1325

S72C 352013 0838 492 1328

S72D 352013 0840 491 1329

S73B 352013 0849 386 1314

S73C 352013 0911 386 1314

S73D 352013 0910 386 1314

PIN21

0502 352013 0912 250 1270

0503 352013 0925 263 1257

0503 352013 1357 346 1174

0504 352013 1400 390 1370

0512 352013 1405 388 1342

PIN15 Northeast Site

0506 352013 1108 327 1373

0507 352013 1104 322 1378

0513 352013 1058 1210 550

0520 352013 1100 339 1371

0530 352013 1053 371 1369

0534 352013 1104 222 1488

0535 352013 1057 379 1381

0537 352013 1109 428 1432

0568 352013 1044 448 1402

0569 352013 1040 427 1411

0573 352013 1125 442 1396

0574 352013 1128 428 1414

0594 352013 1112 465 1385

0595 352013 1135 449 1411




(ft bls)


M16D 352013 1125 382 1438

M16S 352013 1123 381 1439

M24D 352013 1135 390 1390

M33D 352013 1134 325 1435

PIN18 WWNA

0503 352013 1137 346 1422

0507 352013 1343 370 1403

0523 352013 1116 522 1418

0524 352013 1119 477 1423

0525 352013 1118 457 1433

0526 352013 1017 466 1394

Abbreviations amsl = above mean sea level bls = below land surface


Table 2 Surface Water Elevations March 2013

Location Measurement Surface Water

Elevation (ft amsl) Date Time

PIN01 Pond 5

P501 352013 1013 1360

P502 352013 1009 1389

PIN02 West Pond

W005 352013 1004 1409

PIN12 Belcher Road Pond

BR01 352013 1447 1295

PIN15 East Pond

E001 352013 1045 1377

PIN23 Southwest Pond

SW01 352013 1351 1359

PIN37 South Pond

S001 352013 1355 1361

S002 352013 1401 14661

Notes 1questionable value not used for water elevation contours Abbreviations amsl = above mean sea level


Table 3 Field Measurements of Samples Collected at the STAR Center March 2013

Location Screen Depth (ft bls)

Temperature (degC)

Specific Conductance (micromhoscm)a

Turbidity (NTU)

pH

Oxidation Reduction Potential

(mV)

Dissolved Oxygen (mgL)

PIN12

0524 27ndash37 246 1426 4 661 -14 08

0525 12ndash22 241 742 29 679 -63 05

0539 95ndash195 241 1612 14 651 -46 06

0540 20ndash30 243 1457 13 653 -35 06

0541 10ndash20 277 784 16 660 -63 06

0542 20ndash30 281 796 7 661 -53 06

0549 30ndash40 273 1404 15 663 -52 07

0551-1 9ndash18 228 1004 3 665 39 15

0551-2 20ndash29 232 1055 13 665 44 11

0554A 3ndash13 216 650 9 648 40 08

0554B 13ndash23 227 682 11 665 -34 05

0554C 23ndash33 244 880 14 672 -63 06

0555A 25ndash125 233 379 - 660 -26 12

0555B 13ndash23 225 376 26 702 -30 10

0555C 23ndash33 210 534 16 679 -33 13

0561-1 9ndash18 223 511 13 682 9 05

0561-2 20ndash29 229 603 2 677 -12 05

0561-3 31ndash40 210 1055 1 658 -20 04

0565-1 9ndash18 219 1345 1 672 -36 11

0565-2 20ndash29 204 1250 1 668 -30 18

0565-3 31ndash40 222 1502 2 664 -31 14

0568-1 9ndash18 246 1819 4 670 -4 17

0568-2 20ndash29 252 1402 10 672 -27 16

0568-3 31ndash40 254 1798 10 673 -22 17

0569-1 9ndash18 205 1847 4 679 -14 14

0569-2 20ndash29 209 1248 7 674 -30 13

0569-3 31ndash40 214 1292 3 673 -31 14

0570-1 9ndash18 241 2048 4 676 -43 15

0570-2 20ndash29 267 1665 8 677 -20 -

0570-3 31ndash40 220 1363 9 676 37 11

0572-1 9ndash18 267 1638 6 671 -39 20

0572-2 20ndash29 267 1017 5 674 -23 16

0573-1 9ndash18 210 1594 7 666 -47 16

0573-2 20ndash29 231 1172 4 668 -45 17

0573-3 31ndash40 229 1514 1 661 -22 14

0574-1 9ndash18 202 1258 9 675 -24 18

0574-2 20ndash29 225 1274 5 673 -18 16

0574-3 31ndash40 237 1492 5 672 -19 18

0575-1 9ndash18 228 1323 5 674 -38 17

0575-2 20ndash29 218 1459 9 667 -35 14

0576-1 4ndash13 191 1112 2 663 59 15

0576-2 15ndash24 200 1099 6 664 26 12

0576-3 26ndash35 226 1719 9 672 48 12

Table 3 (continued) Field Measurements of Samples Collected at the STAR Center March 2013



Temperature (degC)


Turbidity (NTU)

pH


(mV)


0577-1 4ndash13 206 2069 6 642 40 18

0577-2 15ndash24 204 1458 3 648 41 19

0577-3 26ndash35 200 1245 3 668 30 -

0578-1 4ndash13 179 726 6 637 128 12

0578-2 15ndash24 193 901 3 647 73 13

0578-3 26ndash35 193 1077 4 647 38 13

0579-1 4ndash13 193 1324 5 614 36 15

0579-2 15ndash24 210 1084 6 653 26 16

0579-3 26ndash35 207 1439 31 669 4 16

0580-1 9ndash18 162 653 29 702 -66 12

0580-2 20ndash29 189 1260 13 710 -75 12

0580-3 31ndash40 218 1538 11 702 -108 13

0581-1 9ndash18 225 1350 11 688 -129 08

0581-2 20ndash29 237 1100 17 702 -136 08

0581-3 31ndash40 258 1484 11 671 -74 07

0582-1 9ndash18 263 2261 12 674 -113 06

0582-2 20ndash29 264 1234 9 676 -97 06

0582-3 31ndash40 267 1527 24 663 -55 07

0583-1 9ndash18 240 1224 47 689 -132 04

0583-2 20ndash29 234 1739 5 659 -83 07

0583-3 31ndash40 247 1779 13 668 -74 06

0584-1 9ndash18 178 696 12 711 -61 15

0584-2 20ndash29 192 1057 12 778 -143 12

0584-3 31ndash40 205 1617 14 689 -79 16

0585-1 9ndash18 236 778 11 705 -107 13

0585-2 20ndash29 249 1196 11 698 -116 12

0585-3 31ndash40 253 1621 9 678 -105 06

0586-1 8ndash17 210 604 16 714 -103 04

0586-2 19ndash28 233 717 8 715 -151 04

0586-3 30ndash39 243 1579 10 692 -113 06

0587-1 9ndash18 251 686 30 718 -140 04

0587-2 20ndash29 255 886 5 677 -80 06

0587-3 31ndash40 250 1363 15 679 -106 07

0588-1 9ndash18 179 926 15 713 -139 04

0588-2 20ndash29 172 1072 2 677 -85 05

0588-3 31ndash40 175 1511 8 685 -76 04

S30B 5ndash15 223 1030 19 692 -26 13

S33C 11ndash21 210 638 21 682 17 12

S35B 5ndash15 228 1766 5 654 47 14

S67B 10ndash1983 206 1067 8 676 -1 14

S67C 20ndash2983 210 891 18 679 -27 14

S67D 30ndash3983 211 842 10 678 -22 12

S68B 10ndash20 195 819 14 676 -75 06

S68C 18ndash28 200 955 4 666 2 06




Temperature (degC)


Turbidity (NTU)

pH


(mV)


S68D 30ndash40 204 1369 3 661 -22 06

S69B 10ndash20 242 687 30 684 -78 07

S69C 20ndash30 260 689 11 687 -12 08

S69D 30ndash40 250 1633 6 665 -25 08

S70B 10ndash20 242 931 220 678 -50 05

S70C 20ndash30 250 1420 143 658 -73 07

S70D 30ndash40 256 1553 22 655 -57 08

S71B 10ndash20 247 781 29 671 -73 05

S71C 20ndash30 262 1271 311 659 -51 06

S71D 30ndash40 267 1555 10 660 -56 07

S73B 10ndash20 274 1178 27 652 -314 00

S73C 20ndash30 279 1737 17 651 -134 10

S73D 30ndash40 267 1854 33 621 -66 12

Notes a Temperature corrected to 25 degC Abbreviations ndash = not measured bls = below land surface micromhoscm = micromhos per centimeter mgL = milligrams per liter mV = millivolts NTU = nephelometric turbidity units


Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 (Reported in microgL)

Sample ID Duplicate ID Analyte Result MDL Duplicate

Result Duplicate

MDL RPD

PIN12-0580-2 PIN12-2450

11-Dichloroethane 67 022 62 022 8

14-Dioxane 160 44 190 44 17

cis-12-Dichloroethene 18 015 16 015 12

trans-12-Dichloroethene 50 015 40 015 22

Vinyl chloride 150 040 150 040 0

PIN12-0581-2 PIN12-2451

11-Dichloroethanea 94J 22 12 022

11-Dichloroethenea 23U 23 047J 023

cis-12-Dichloroethenea 29J 15 36 015

Methylene chloridea 37J 32 032U 032

Vinyl chloridea 10U 10 73 010

PIN12-0582-2 PIN12-2452


11-Dichloroethenea 063J 046 072J 023

14-Dioxanea 044U 044 170 88

Acetonea 73J 38 19U 19


Naphthalenea 044U 044 023J 022



PIN12-0583-2 PIN12-2453 trans-12-Dichloroethene 22 015 26 015 17


PIN12-0587-2 PIN12-2454

11-Dichloroethene 79 023 11 023 33




Notes a An RPD was not calculated for these analytes because the result is less than 25 times the MDL Abbreviations J = Estimated value MDL = method detection limit RPD = relative percent difference U = not detected


Table 5 COPC Concentrations at the Building 100 Area (microgL)a

Well TCE cis-12-DCE trans-12-

DCE 11-DCE

Vinyl chloride

14 Dioxane TCOPCs

CTLsb 30 700 1000 70 10 32

E1 to E2 Cross Section

0555A lt016 lt015 lt015 lt023 lt01 lt022 ND

0555B lt016 lt015 lt015 lt023 lt01 lt022 ND

0555C lt016 11 043J lt023 lt01 lt022 153



0554C lt016 16 55 1 88 76 1865

0580-1 lt016 054J lt015 lt023 42 4 874

0580-2 lt016 18 5J lt023 150J 160 333

0580-3 lt016 12 088J lt023 23 28 6388

S71B lt016 lt015 lt015 lt023 lt01 lt022 ND

S71C lt016 18 10 029J 44 34 10629

S71D lt016 29 17 06J 60 lt044 1066

S70B lt016 15 047J lt023 75 lt022 2297

S70C lt016 19 72 047J 22 15 6367

S70D lt016 23 92 068J 19 12 6388


S69C lt016 lt015 lt015 lt023 lt01 lt088 ND

S69D lt016 03J lt015 lt023 lt01 lt088 03


0541 lt016 02J lt015 lt023 lt01 lt022 02

0542 lt064 lt06 lt06 lt092 lt04 lt044 ND

0549 lt016 017J lt015 lt023 lt01 lt044 017

0581-1 lt016 026J lt015 lt023 05J lt044 076

0581-2 lt016 36 lt015 047J 73 lt044 1137c

0581-3 lt032 lt03 lt03 lt046 lt02 lt044 ND

0582-1 lt016 lt015 lt015 lt023 12 lt044 12

0582-2 lt016 13 25 072J 130J 170J 31622c

0582-3 lt016 02J lt015 lt023 12 lt044 14

0539 lt016 16 13 lt023 53 38 939

0540 lt016 12 68 lt023 230 170J 4188

S73B lt016 14 05J lt023 11 lt044 129

S73C lt016 18 17 047J 230 130 39547

S73D lt016 021J lt015 lt023 047J lt088 068

0583-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0583-2 lt016 025J 22 lt023 16 lt44 1845

0583-3 lt016 lt015 lt015 lt023 lt01 lt088 ND


S67B lt016 13 33 lt023 250 91 3573

S67C lt016 48 97 064J 65 lt088 12334

S67D lt016 62 19 lt023 11 lt022 191

0580-1 lt016 054J lt015 lt023 42 4 874

0580-2 lt016 18 5J lt023 150J 160 333

0580-3 lt016 12 088J lt023 23 28 6388

Table 5 (continued) COPC Concentrations at the Building 100 Area (microgL)a



DCE 11-DCE

Vinyl chloride

14 Dioxane TCOPCs

CTLsb 30 700 1000 70 10 32

0582-1 lt016 lt015 lt015 lt023 12 lt044 12

0582-2 lt016 13 25 072J 130J 170J 31622c

0582-3 lt016 02J lt015 lt023 12 lt044 14

0576-1 lt016 74 017J 2 15 36 6057

0576-2 lt016 89 021J 24 17 27J 5551

0576-3 lt016 046J lt015 lt023 12 lt088 166

0578-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0578-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0578-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

S1 to E2 Cross Section

0561-1 lt016 lt015 lt015 lt023 lt01 lt022 ND

0561-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0561-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

0584-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0584-2 lt016 035J lt015 lt023 lt01 lt044 035

0584-3 lt032 lt03 lt03 lt046 1J lt044 1

0585-1 53 59 041J 27 98 lt044 7721

0585-2 420 3500 17 160 420 lt88 4517

0585-3 071J 140 11 4 200 lt044 34581

0524 lt032 570 71 16 600 lt088 11931

0525 lt016 13 lt015 lt023 lt01 lt044 13


S68C lt064 53 lt06 lt092 lt04 45 98

S68D lt064 41 lt06 lt092 16 33 603



S69D lt016 03J lt015 lt023 lt01 lt088 03

S2 to S3 Cross Section

0586-1 lt016 036J lt015 lt023 lt01 lt044 036

0586-2 lt016 3 lt015 lt023 29 lt044 59

0586-3 lt016 053J lt015 lt023 15 lt044 203

0587-1 lt016 50 03J 13 13 lt044 646

0587-2 lt016 190 14 79J 71 lt044 2703

0587-3 lt016 280 22 16 130 lt044 4282

0588-1 lt064 lt06 lt06 lt092 lt04 lt044 ND

0588-2 lt016 12 lt015 lt023 16 66 346

0588-3 lt016 087J lt015 lt023 14 lt044 227


0585-1 53 59 041J 27 98 lt044 7721

0585-2 420 3500 17 160 420 lt88 4517

0585-3 071J 140 11 4 200 lt044 34581

0587-1 lt016 50 03J 13 13 lt044 646

0587-2 lt016 190 14 79J 71 lt044 2703

0587-3 lt016 280 22 16 130 lt044 4282

0569-1 lt016 lt015 lt015 lt023 lt01 lt044 ND




DCE 11-DCE

Vinyl chloride

14 Dioxane TCOPCs

CTLsb 30 700 1000 70 10 32

0569-2 lt064 22J lt06 lt092 lt04 16J 38

0569-3 lt064 54 lt06 25J 37 13J 948

0572-1 lt064 lt06 lt06 lt092 lt04 lt044 ND

0572-2 lt08 200 17J 10 42 lt044 2537

0574-1 lt064 73 lt06 lt092 12 lt044 193

0574-2 lt016 17 028J lt023 18 lt044 3528

0574-3 lt016 059J lt015 lt023 1 lt044 159

0575-1 lt064 lt06 lt06 lt092 lt04 19 19

0575-2 lt064 lt06 lt06 lt092 lt04 lt022 ND

Other Wells

0551-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0551-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0565-1 lt064 lt06 lt06 lt092 lt04 lt022 ND

0565-2 lt064 lt06 lt06 lt092 lt04 lt022 ND

0565-3 lt064 lt06 lt06 lt092 lt04 lt022 ND

0568-1 lt064 lt06 lt06 lt092 lt04 lt044 ND

0568-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0568-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

0570-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0570-2 lt016 lt015 lt015 lt023 055J lt044 055

0570-3 lt016 lt015 lt015 lt023 34 lt044 34

0573-1 lt064 lt06 lt06 lt092 lt04 lt022 ND

0573-2 lt064 lt06 lt06 lt092 lt04 lt022 ND

0573-3 lt064 lt06 lt06 lt092 lt04 lt022 ND

0577-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0577-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0577-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

0579-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0579-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0579-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

S30B 23 43 45 054J 10 lt044 8104d

S33C 180 920 48 33 150 lt044 1331d

S35B 5500 40000 5100 940 12000 lt044 63540d

Notes a lt values are method detection limits b The offsite CTL is a factor of 10 lower than the listed onsite (poor water quality) CTL c As explained in Section 32 this table lists the results for duplicate samples for wells 12-0581-2 and 12-0582-2 d Wells S30B S33C and S35B were sampled to track potential source depletion under the northwest corner of the

building These wells are not part of the plume stability monitoring program Abbreviations J = Estimated value ND = Not detected


Table 6 Sum of COPCs for Each Plume Stability Monitoring Cross-Section

Cross Section Sum of COPCs (microgL) E1 to E2 Cross Section

0555 153

0554 1865

0580 40562

S71 21289

S70 15052

S69 03


054105420549 037

0581 1213

0582 31882

05390540 5127

S73 40905

0583 1845


S67 49974

0580 40562

0582 31882

0576 11774

0578 0


0561 0

0584 135

0585 494002

05240525 11944

S68 701

S69 03


0586 829

0587 7631

0588 3687


0585 494002

0587 7631

0569 986

0572 2537

0574 5617

0575 19


Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-Section

Cross Section Area Under the Curve

March 2013 (dimensionless)

E1-E2 956

E3-E4 1262

E5-E6 1092

S1-E2 6206

S2-S3 786

S4-S5 3643

WestPond

East Pond

Pond 5

Southwest PondSouth Pond South Pond

Pond North of the45 Acre Site

Belcher Road Pond

12-0571-11291

12-S30B1436

12-S31B1422

12-S32B1433

12-S35B1412

12-S36B139

12-S37B1443

20-M0031488

12-S70B1359

12-S72B1325

12-S73B1314

12-S67B1408

12-S71B1392

12-S69B134

20-M40S1504

18-05251433

20-M0241445

23-SW011359

12-05091443

21-0502127

21-0504137

37-S0011361

15-05071378

15-05201371

15-05301369

15-05681402

15-05731396

01-P501136

02-W0051409

02-PZ051454

20-BP011426

02-PZ091388

02-PZ031549

02-PZ081401

01-P5021389

15-05951411

12-0567-11413

12-0568-1139

12-0569-11348

12-0564-11254

12-0565-11158

12-0566-11134

12-0573-11172

12-0575-11039

02-PZ101434

12-0576-11285

12-0577-11326

12-0579-11319

12-0572-1123

12-0587-11348

12-0588-11344

12-0582-1132

12-0581-11324

12-0580-11364

12-0585-11381

12-0584-11381

12-0554A1361

12-0563-11378

12-0560-11378

12-0559-11255

12-0561-11391 12-0539

1324

12-05411282

20-M0671461

20-M0691485

12-0553A1361

12-S68B1386

20-M0351465

15-M16S1439

12-0578-11355

12-0551-11211

12-0586-11353

12-0583-11309

12-0562-11337

12-0550-11198

20-M06515

12-0555A1377

21-05121342

02-PZ041537

12-0574-11089

15-E0011377

12-BR011295

11

15

15

15

14

14

14

12

12

12

12

15

15

15 15

15

13

13

13

13

13

13

14 14

14

14

14

1414

1414

14

14

14

14

15

15

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-11291

12-S30B1436

12-S31B1422

12-S32B1433

12-S35B1412

12-S36B139

12-S37B1443

20-M0031488

12-S70B1359

12-S72B1325

12-S73B1314

12-S67B1408

12-S71B1392

12-S69B134

20-M40S1504

18-05251433

20-M0241445

23-SW011359

12-05091443

21-0502127

21-0504137

37-S0011361

15-05071378

15-05201371

15-05301369

15-05681402

15-05731396

01-P501136

02-W0051409

02-PZ051454

20-BP011426

02-PZ091388

02-PZ031549

02-PZ081401

01-P5021389

15-05951411

12-0567-11413

12-0568-1139

12-0569-11348

12-0564-11254

12-0565-11158

12-0566-11134

12-0573-11172

12-0575-11039

02-PZ101434

12-0576-11285

12-0577-11326

12-0579-11319

12-0572-1123

12-0587-11348

12-0588-11344

12-0582-1132

12-0581-11324

12-0580-11364

12-0585-11381

12-0584-11381

12-0554A1361

12-0563-11378

12-0560-11378

12-0559-11255

12-0561-11391 12-0539

1324

12-05411282

20-M0671461

20-M0691485

12-0553A1361

12-S68B1386

20-M0351465

15-M16S1439

12-0578-11355

12-0551-11211

12-0586-11353

12-0583-11309

12-0562-11337

12-0550-11198

20-M06515

12-0555A1377

21-05121342

02-PZ041537

12-0574-11089

15-E0011377

12-BR011295

11

15

15

15

14

14

14

12

12

12

12

15

15

15 15

15

13

13

13

13

13

13

14 14

14

14

14

1414

1414

14

14

14

14

15

15

DATE PREPARED FILENAME

GRAND JUNCTION COLORADO

US DEPARTMENT OF ENERGY

Plate 1 Sitewide Shallow Surficial Aquifer Contours

Pinellas Florida March 2013

N0179900-01MPIN041001014000N01799N0179900-01mxd smithw 06252013 83621 AM

June 25 2013

0 150 300 Feet

Under DOE ContractNo DE-AC01-07LM00060

Prepared bySM Stoller Corporation

12-S35B1412

Well Number and Groundwater Elevation in Feet (amsl)

Monitoring Well

Extraction Well

Surface Sample

Piezometer

Water Level Not Used in Contouring

Water Elevation Contour in Feet (amsl)Contour Interval = 10 Foot

Inferred Water Elevation Contour in Feet (amsl)

Inferred Groundwater Flow Direction

Slurrywall

Fence

Road

Railroad

Tank

Building

Pond

14

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-31286

12-05201435

12-05211435

12-05181397

15-05341488

20-M0011456

20-M0051484

20-M0531446

12-S68D1366

12-S73D1314

12-S69D1323

12-S71D1365

12-S72D1329

18-05071403

20-05021437

20-M0361494

20-M38D1384

20-M40D1489

20-M0231436

18-05231418

20-M41D1463

12-S70D1347

20-M18D1463

20-M22D1483

12-05241375

12-05161352

15-M24D139

15-M33D1435

15-05351381

12-0550-31213

20-M0551417

20-M0591476

15-05691411

20-M0581475

12-05491315

12-0567-31369

12-0569-31323

12-0564-31237

12-0566-31137

12-0572-2123

12-0573-3117

02-PZ111405

12-0576-31298

12-0577-31326

12-PZ011335

12-PZ02137

12-PZ031336

12-0579-31315

12-0586-31357 12-0587-3

1351

12-0588-31344

12-0583-31314

12-0582-31318

12-0581-31321

12-0580-3136

12-0584-31373

12-0554C1359

12-0559-31101 12-0561-3

1388

12-0551-31222

15-05941385

20-M0151434

20-M0661589

20-M0681482

12-0553C1347

12-0555C1369

20-M0561428

12-S67D14

12-0574-31093

12-0565-31157

12-0575-21043

12-0560-31402

12-0585-31372

12-0562-31342 12-0563-3

1386

20-M0571461

12-0568-31367

12-0578-31349

14

11

11

15

15

15

12

12

12

14

14

14

1414

14

13

13

13

13

13

1414

14 14

14

14

14

14

15

15

14

14

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-31286

12-05201435

12-05211435

12-05181397

15-05341488

20-M0011456

20-M0051484

20-M0531446

12-S68D1366

12-S73D1314

12-S69D1323

12-S71D1365

12-S72D1329

18-05071403

20-05021437

20-M0361494

20-M38D1384

20-M40D1489

20-M0231436

18-05231418

20-M41D1463

12-S70D1347

20-M18D1463

20-M22D1483

12-05241375

12-05161352

15-M24D139

15-M33D1435

15-05351381

12-0550-31213

20-M0551417

20-M0591476

15-05691411

20-M0581475

12-05491315

12-0567-31369

12-0569-31323

12-0564-31237

12-0566-31137

12-0572-2123

12-0573-3117

02-PZ111405

12-0576-31298

12-0577-31326

12-PZ011335

12-PZ02137

12-PZ031336

12-0579-31315

12-0586-31357 12-0587-3

1351

12-0588-31344

12-0583-31314

12-0582-31318

12-0581-31321

12-0580-3136

12-0584-31373

12-0554C1359

12-0559-31101 12-0561-3

1388

12-0551-31222

15-05941385

20-M0151434

20-M0661589

20-M0681482

12-0553C1347

12-0555C1369

20-M0561428

12-S67D14

12-0574-31093

12-0565-31157

12-0575-21043

12-0560-31402

12-0585-31372

12-0562-31342 12-0563-3

1386

20-M0571461

12-0568-31367

12-0578-31349

14

11

11

15

15

15

12

12

12

14

14

14

1414

14

13

13

13

13

13

1414

14 14

14

14

14

14

15

15

14

14




Plate 2 Sitewide Deep Surficial Aquifer Contours



June 25 2013

0 150 300 Feet



18-05071403


Monitoring Well

Extraction Well

Surface Sample

Piezometer





Slurrywall

Fence

Road

Railroad

Tank

Building

Pond

14

Appendix A

Laboratory Reports

March 2013 Semiannual Monitoring

ANALYTICAL REPORT

Job Number 280-39772-1

SDG Number 13025120

Job Description PINELLAS MONITORING

ForSM Stoller Corporation

2597 Legacy WayGrand Junction CO 81503

Attention Mr Steve Donivan

_____________________________________________

Approved for releaseKae E YoderProject Manager II3222013 256 PM

Kae E YoderProject Manager II

kaeyodertestamericainccom03222013

The test results in this report relate only to the samples in this report and meet all requirements of NELAC with anyexceptions noted Pursuant to NELAP this report shall not be reproduced except in full without the written approval ofthe laboratory All questions regarding this report should be directed to the TestAmerica Denver Project Manager

The Lab Certification ID is E87667

Reporting limits are adjusted for sample size used dilutions and moisture content if applicable

TestAmerica Laboratories Inc

TestAmerica Denver 4955 Yarrow Street Arvada CO 80002

Tel (303) 736-0100 Fax (303) 431-7171 wwwtestamericainccom

Page 1 of 962

Pages have been deleted from this laboratory report file to reduce file size The deleted pages contain raw data and instrument calibrations If the full laboratory report is needed contact ScottSurovchaklmdoegov

Table of ContentsCover Title Page 1

Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 9

Method Analyst Summary 10

Sample Datasheets 11

Surrogate Summary 71

QC Data Summary 75

QC Association Summary 101

Lab Chronicle 103

Manual Integration Summary 110

Organic Sample Data 132

GCMS VOA 132

Method 8260B 132Method 8260B QC Summary 133Method 8260B Sample Data 157Standards Data 306

Method 8260B ICAL Data 306Method 8260B CCAL Data 429

Raw QC Data 493Method 8260B Tune Data 493Method 8260B Blank Data 514Method 8260B LCSLCSD Data 535

Page 2 of 962

Table of ContentsMethod 8260B MSMSD Data 553

Method 8260B Run Logs 595

Method 8260B SIM 685Method 8260B SIM QC Summary 686Method 8260B SIM Sample Data 713Standards Data 778

Method 8260B SIM ICAL Data 778Method 8260B SIM CCAL Data 836

Raw QC Data 854Method 8260B SIM Tune Data 854Method 8260B SIM Blank Data 869Method 8260B SIM LCSLCSD Data 881Method 8260B SIM MSMSD Data 909

Method 8260B SIM Run Logs 930

Shipping and Receiving Documents 957

Client Chain of Custody 958

Sample Receipt Checklist 960

Page 3 of 962

CASE NARRATIVE

Client SM Stoller Corporation

Project PINELLAS MONITORING - 13025120

Report Number 280-39772-1

With exceptions noted as flags or footnotes standard analytical protocols were followed in the analysis of the samples and no problems

were encountered or anomalies observed All laboratory quality control samples analyzed in conjunction with the samples in this project

were within established control limits with any exceptions noted Calculations are performed before rounding to avoid round-off errors in

calculated results

This report includes reporting limits (RLs) less than TestAmerica Denvers practical quantitation limits These reporting limits are being

used specifically at the clients request to meet the needs of this project Please note that data are not normally reported to these levels

without qualification since they are inherently less reliable and potentially less defensible than required by the current NELAC standards

Results between the method detection limit (MDL) and reporting limit (RL) are flagged with a J qualifier to indicate an estimated value

These results are statistically less reliable than results greater than or equal to the RL and should be considered a qualitative value

All holding times were met and proper preservation noted for the methods performed on these samples unless otherwise detailed in the

individual sections below

RECEIPT

The samples were received on 392013 930 AM the samples arrived in good condition properly preserved and where required on ice

The temperatures of the 2 coolers at receipt time were 26ordm C and 31ordm C

GCMS VOLATILES - SW846 8260B

Due to the nature of the sample matrix (foamy) a reduced aliquot size had to be used for the analysis of several samples The reporting

limits have been elevated accordingly

Due to high constituent concentration reduced aliquot sizes had to be used for the analysis of Vinyl chloride in samples PIN12-0580-2

(LDU 874) PIN12-2450 (LDU 956) PIN12-S67B (LDU 904) and PIN12-S67C (LDU 905) The reporting limits have been elevated

accordingly

Surrogates 12-Dichloroethane-d4 and Dibromofluoromethane were recovered outside the control limits biased low in the 5 mL initial

volume analysis of sample PIN12-0580-2 (LDU 874) The sample was reanalyzed with similar results indicating matrix interference as

the cause for the surrogate recovery outliers

No other anomalies were encountered

GCMS VOLATILES - SW846 8260B SIM - 14-Dioxane

Due to the nature of the sample matrix (foamy) a reduced aliquot size had to be used for the analysis of sample PIN12-S67C (LDU 905)

The reporting limit haS been elevated accordingly

In some cases due to high constituent concentration samples had to be analyzed using reduced aliquot sizes The reporting limits have

been elevated accordingly

Internal standard 14-Dichlorobenzene-d4 failed to meet acceptance criteria for sample PIN12-S67C (LDU 905) As this internal standard

is not associated with the analyte of interest (14-Dioxane) data are reported as is

The MSD aliquot of the MSMSD associated with batch 280-164929 exhibited the percent recovery outside the control limits The LCS

and LCSD were within control limits

MSMSD data is not available for batch 280-164670 due to a QC failure associated with the parent sample requiring reanalysis Method

precision and accuracy have been verified by the acceptable LCSLCSD analysis data


Page 4 of 962

DATA REPORTING QUALIFIERS

Client SM Stoller Corporation Job Number 280-39772-1

Lab Section Qualifier Description

Sdg Number 13025120

GCMS VOA

Indicates the analyte was analyzed for but not detectedU

MS or MSD exceeds the control limitsF

Result is less than the RL but greater than or equal to the MDL and the

concentration is an approximate value

J

Surrogate is outside control limitsX

TestAmerica Denver Page 5 of 962

SAMPLE SUMMARY


Sdg Number 13025120

Client Sample IDLab Sample ID Client Matrix Sampled Received

DateTime DateTime

280-39772-1 PIN12-0555A Water 03072013 1605 03092013 0930

280-39772-1MS PIN12-0555A Water 03072013 1605 03092013 0930

280-39772-1MSD PIN12-0555A Water 03072013 1605 03092013 0930

280-39772-2 PIN12-0555B Water 03072013 1640 03092013 0930

280-39772-2MS PIN12-0555B Water 03072013 1640 03092013 0930

280-39772-2MSD PIN12-0555B Water 03072013 1640 03092013 0930

280-39772-3 PIN12-0555C Water 03072013 1740 03092013 0930

280-39772-4 PIN12-0565-1 Water 03062013 0936 03092013 0930

280-39772-5 PIN12-0565-2 Water 03062013 1015 03092013 0930

280-39772-6 PIN12-0565-3 Water 03062013 1110 03092013 0930

280-39772-7 PIN12-0573-1 Water 03062013 1335 03092013 0930

280-39772-8 PIN12-0573-2 Water 03062013 1405 03092013 0930

280-39772-9 PIN12-0573-3 Water 03062013 1440 03092013 0930

280-39772-10 PIN12-0575-1 Water 03062013 1540 03092013 0930

280-39772-11 PIN12-0575-2 Water 03062013 1620 03092013 0930

280-39772-12 PIN12-0580-1 Water 03072013 0935 03092013 0930

280-39772-13 PIN12-0580-2 Water 03072013 1030 03092013 0930

280-39772-14 PIN12-0580-3 Water 03072013 1110 03092013 0930

280-39772-15 PIN12-2450 Water 03072013 1200 03092013 0930

280-39772-16 PIN12-S67B Water 03072013 1315 03092013 0930

280-39772-17 PIN12-S67C Water 03072013 1225 03092013 0930

280-39772-18 PIN12-S67D Water 03072013 1355 03092013 0930

280-39772-19 PIN99-2198 Water 03062013 1200 03092013 0930


EXECUTIVE SUMMARY - Detections


Analyte Result

Reporting

Limit Units Method

Lab Sample ID Client Sample ID

Sdg Number 13025120

Qualifier

280-39772-3 PIN12-0555C

10 ugL 8260B11cis-12-Dichloroethene

10 ugL 8260B043 Jtrans-12-Dichloroethene

280-39772-6 PIN12-0565-3

40 ugL 8260B10 JAcetone

280-39772-8 PIN12-0573-2


280-39772-10 PIN12-0575-1


10 ugL 8260B SIM1914-Dioxane

280-39772-12 PIN12-0580-1

10 ugL 8260B054 Jcis-12-Dichloroethene

10 ugL 8260B42Vinyl chloride


280-39772-13 PIN12-0580-2

10 ugL 8260B6711-Dichloroethane


10 ugL 8260B50trans-12-Dichloroethene



280-39772-14 PIN12-0580-3






280-39772-15 PIN12-2450









Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39772-16 PIN12-S67B






280-39772-17 PIN12-S67C




10 ugL 8260B064 J11-Dichloroethene


280-39772-18 PIN12-S67D

10 ugL 8260B086 J11-Dichloroethane





METHOD SUMMARY


Sdg Number 13025120

Preparation MethodMethodLab LocationDescription

Matrix Water

Volatile Organic Compounds (GCMS) TAL DEN SW846 8260B

Purge and Trap TAL DEN SW846 5030B

Volatile Organic Compounds (GCMS-SIM) TAL DEN SW846 8260B SIM


Lab References

TAL DEN = TestAmerica Denver

Method References

SW846 = Test Methods For Evaluating Solid Waste PhysicalChemical Methods Third Edition November 1986 And Its Updates


METHOD ANALYST SUMMARY


Method Analyst Analyst ID

Sdg Number 13025120

Berger Brent BBSW846 8260B

Dobransky Michael E MDSW846 8260B

Moan Matthew R MRMSW846 8260B

Tinkham Sarah A SATSW846 8260B SIM

TestAmerica Denver

Page 10 of 962

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555A

Client Matrix

280-39772-1

Water

Date Sampled 03072013 1605

Date Received 03092013 0930

8260B Volatile Organic Compounds (GCMS)

Dilution

03142013 2211

03142013 2211

10

8260B

Final WeightVolume

Initial WeightVolume

Lab File ID

Instrument ID

RR1862D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method

Analyte Result (ugL) Qualifier MDL RL

19 U 1019Acetone

016 U 10016Benzene

017 U 10017Bromobenzene

010 U 10010Bromochloromethane

017 U 10017Bromodichloromethane

019 U 10019Bromoform

021 U 10021Bromomethane

20 U 50202-Butanone (MEK)

032 U 10032n-Butylbenzene

017 U 10017sec-Butylbenzene

016 U 10016tert-Butylbenzene

045 U 10045Carbon disulfide

019 U 10019Carbon tetrachloride

017 U 10017Chlorobenzene

017 U 10017Dibromochloromethane

041 U 10041Chloroethane

016 U 10016Chloroform

030 U 10030Chloromethane

017 U 100172-Chlorotoluene


047 U 1004712-Dibromo-3-Chloropropane

017 U 10017Dibromomethane

015 U 1001512-Dichlorobenzene



031 U 10031Dichlorodifluoromethane

022 U 1002211-Dichloroethane


015 U 10015cis-12-Dichloroethene

015 U 10015trans-12-Dichloroethene

023 U 1002311-Dichloroethene

018 U 1001812-Dichloropropane



016 U 10016cis-13-Dichloropropene

019 U 10019trans-13-Dichloropropene

019 U 1001911-Dichloropropene

016 U 10016Ethylbenzene

036 U 10036Hexachlorobutadiene

17 U 50172-Hexanone

019 U 10019Isopropylbenzene

020 U 100204-Isopropyltoluene

032 U 10032Methylene Chloride

098 U 500984-Methyl-2-pentanone

022 U 10022Naphthalene

016 U 10016n-Propylbenzene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555A

Client Matrix

280-39772-1

Water




Dilution

03142013 2211

03142013 2211

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1862D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene

021 U 100211112-Tetrachloroethane


020 U 10020Tetrachloroethene

017 U 10017Toluene

021 U 10021123-Trichlorobenzene


016 U 10016111-Trichloroethane


016 U 10016Trichloroethene

029 U 10029Trichlorofluoromethane

033 U 10033123-Trichloropropane

015 U 10015124-Trimethylbenzene


010 U 10010Vinyl chloride

019 U 10019Xylenes Total

018 U 1001812-Dibromoethane

Surrogate Rec Acceptance LimitsQualifier

75 70 - 12712-Dichloroethane-d4 (Surr)

96 80 - 125Toluene-d8 (Surr)

90 78 - 1204-Bromofluorobenzene (Surr)

85 77 - 120Dibromofluoromethane (Surr)


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555B

Client Matrix

280-39772-2

Water




Dilution

03142013 2234

03142013 2234

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1863D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555B

Client Matrix

280-39772-2

Water




Dilution

03142013 2234

03142013 2234

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1863D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555C

Client Matrix

280-39772-3

Water




Dilution

03152013 0116

03152013 0116

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1870D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene



























11 10015cis-12-Dichloroethene

043 J 10015trans-12-Dichloroethene










17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555C

Client Matrix

280-39772-3

Water




Dilution

03152013 0116

03152013 0116

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1870D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-1

Client Matrix

280-39772-4

Water




Dilution

03152013 1426

03152013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6154D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-1

Client Matrix

280-39772-4

Water




Dilution

03152013 1426

03152013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6154D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-2

Client Matrix

280-39772-5

Water




Dilution

03152013 1445

03152013 1445

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6155D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-2

Client Matrix

280-39772-5

Water




Dilution

03152013 1445

03152013 1445

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6155D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-3

Client Matrix

280-39772-6

Water




Dilution

03152013 1504

03152013 1504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6156D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


10 J 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-3

Client Matrix

280-39772-6

Water




Dilution

03152013 1504

03152013 1504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6156D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-1

Client Matrix

280-39772-7

Water




Dilution

03152013 1232

03152013 1232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6148D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-1

Client Matrix

280-39772-7

Water




Dilution

03152013 1232

03152013 1232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6148D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-2

Client Matrix

280-39772-8

Water




Dilution

03152013 1251

03152013 1251

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6149D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


18 J 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-2

Client Matrix

280-39772-8

Water




Dilution

03152013 1251

03152013 1251

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6149D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-3

Client Matrix

280-39772-9

Water




Dilution

03152013 1310

03152013 1310

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6150D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-3

Client Matrix

280-39772-9

Water




Dilution

03152013 1310

03152013 1310

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6150D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-1

Client Matrix

280-39772-10

Water




Dilution

03152013 1329

03152013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6151D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


83 J 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-1

Client Matrix

280-39772-10

Water




Dilution

03152013 1329

03152013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6151D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-2

Client Matrix

280-39772-11

Water




Dilution

03152013 1348

03152013 1348

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6152D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-2

Client Matrix

280-39772-11

Water




Dilution

03152013 1348

03152013 1348

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6152D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-1

Client Matrix

280-39772-12

Water




Dilution

03152013 0139

03152013 0139

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1871D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene



























054 J 10015cis-12-Dichloroethene











17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-1

Client Matrix

280-39772-12

Water




Dilution

03152013 0139

03152013 0139

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1871D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene










42 10010Vinyl chloride









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03152013 0202

03152013 0202

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1872D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene

























67 1002211-Dichloroethane



50 10015trans-12-Dichloroethene










17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03152013 0202

03152013 0202

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1872D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03152013 2140

03152013 2140

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1919D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method




67 70 - 127X12-Dichloroethane-d4 (Surr)



76 77 - 120XDibromofluoromethane (Surr)


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-3

Client Matrix

280-39772-14

Water




Dilution

03152013 0225

03152013 0225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1873D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-3

Client Matrix

280-39772-14

Water




Dilution

03152013 0225

03152013 0225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1873D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 0248

03152013 0248

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1874D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 0248

03152013 0248

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1874D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 2203

03152013 2203

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1920D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03152013 0311

03152013 0311

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1875D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03152013 0311

03152013 0311

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1875D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03152013 2226

03152013 2226

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1921D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03152013 0333

03152013 0333

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1876D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene





























064 J 1002311-Dichloroethene









17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03152013 0333

03152013 0333

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1876D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03162013 0524

03162013 0524

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1939D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67D

Client Matrix

280-39772-18

Water




Dilution

03152013 0356

03152013 0356

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1877D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene

























086 J 1002211-Dichloroethane













17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67D

Client Matrix

280-39772-18

Water




Dilution

03152013 0356

03152013 0356

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1877D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2198

Client Matrix

280-39772-19

Water




Dilution

03152013 1407

03152013 1407

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6153D

20 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2198

Client Matrix

280-39772-19

Water




Dilution

03152013 1407

03152013 1407

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6153D

20 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555A

Client Matrix

280-39772-1

Water



8260B SIM Volatile Organic Compounds (GCMS-SIM)

Dilution

03122013 2146

03122013 2146

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3715D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555B

Client Matrix

280-39772-2

Water




Dilution

03122013 2204

03122013 2204

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3716D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555C

Client Matrix

280-39772-3

Water




Dilution

03122013 2256

03122013 2256

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3719D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-1

Client Matrix

280-39772-4

Water




Dilution

03122013 2314

03122013 2314

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3720D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-2

Client Matrix

280-39772-5

Water




Dilution

03122013 2331

03122013 2331

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3721D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-3

Client Matrix

280-39772-6

Water




Dilution

03122013 2349

03122013 2349

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3722D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-1

Client Matrix

280-39772-7

Water




Dilution

03132013 0006

03132013 0006

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3723D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-2

Client Matrix

280-39772-8

Water




Dilution

03132013 0024

03132013 0024

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3724D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-3

Client Matrix

280-39772-9

Water




Dilution

03132013 0041

03132013 0041

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3725D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-1

Client Matrix

280-39772-10

Water




Dilution

03132013 0059

03132013 0059

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3726D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


19 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-2

Client Matrix

280-39772-11

Water




Dilution

03132013 0116

03132013 0116

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3727D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-1

Client Matrix

280-39772-12

Water




Dilution

03132013 0134

03132013 0134

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3728D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


40 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03132013 2100

03132013 2100

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3741D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


160 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-3

Client Matrix

280-39772-14

Water




Dilution

03152013 0323

03152013 0323

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3795D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


28 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 0341

03152013 0341

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3796D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


190 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03132013 2153

03132013 2153

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3744D

2 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


91 102214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03162013 0420

03162013 0420

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3844D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67D

Client Matrix

280-39772-18

Water




Dilution

03142013 0434

03142013 0434

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3767D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Quality Control Results


Sdg Number 13025120


Surrogate Recovery Report


Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39772-1 PIN12-0555A 85 75 96 90

280-39772-2 PIN12-0555B 89 84 92 89

280-39772-3 PIN12-0555C 106 101 105 103

280-39772-4 PIN12-0565-1 94 87 94 88

280-39772-5 PIN12-0565-2 90 87 91 90

280-39772-6 PIN12-0565-3 94 87 94 90

280-39772-7 PIN12-0573-1 90 85 93 90

280-39772-8 PIN12-0573-2 91 85 95 91

280-39772-9 PIN12-0573-3 92 87 93 89

280-39772-10 PIN12-0575-1 92 87 95 88

280-39772-11 PIN12-0575-2 92 88 94 90

280-39772-12 PIN12-0580-1 92 89 88 84

280-39772-13 PIN12-0580-2 94 94 89 88

280-39772-13 DL PIN12-0580-2 DL 76X 67X 88 85

280-39772-14 PIN12-0580-3 100 97 99 97

280-39772-15 PIN12-2450 96 98 94 91

280-39772-15 DL PIN12-2450 DL 83 72 96 89

280-39772-16 PIN12-S67B 89 86 88 84

280-39772-16 DL PIN12-S67B DL 80 70 91 83

280-39772-17 PIN12-S67C 100 97 100 98

280-39772-17 DL PIN12-S67C DL 95 80 100 90

280-39772-18 PIN12-S67D 93 87 92 89

280-39772-19 PIN99-2198 94 85 95 86

MB 280-1649205 93 89 94 90

MB 280-1649347 86 83 95 88

MB 280-1651125 82 73 92 84

LCS 280-1649204 93 92 92 92

LCS 280-1649346 88 83 95 88

LCS 280-1651124 84 82 94 86

Surrogate Acceptance Limits

DBFM = Dibromofluoromethane (Surr) 77-120

DCA = 12-Dichloroethane-d4 (Surr) 70-127

TOL = Toluene-d8 (Surr) 80-125

BFB = 4-Bromofluorobenzene (Surr) 78-120

TestAmerica Denver

Page 71 of 962



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39772-1 MS PIN12-0555A MS 89 84 92 88

280-39751-I-1 MS 91 87 99 86

280-39756-O-16 MS 89 83 90 87

280-39772-1 MSD PIN12-0555A MSD 89 85 90 88

280-39751-I-1 MSD 93 87 98 86

280-39756-O-16 MSD 91 89 91 89






TestAmerica Denver

Page 72 of 962



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39772-1 PIN12-0555A 99

280-39772-2 PIN12-0555B 96

280-39772-3 PIN12-0555C 94

280-39772-4 PIN12-0565-1 96

280-39772-5 PIN12-0565-2 97

280-39772-6 PIN12-0565-3 102

280-39772-7 PIN12-0573-1 100

280-39772-8 PIN12-0573-2 103

280-39772-9 PIN12-0573-3 101

280-39772-10 PIN12-0575-1 103

280-39772-11 PIN12-0575-2 102

280-39772-12 PIN12-0580-1 102

280-39772-13 PIN12-0580-2 108

280-39772-14 PIN12-0580-3 103

280-39772-15 PIN12-2450 108

280-39772-16 PIN12-S67B 99

280-39772-17 PIN12-S67C 120

280-39772-18 PIN12-S67D 114

MB 280-1644325 95

MB 280-1646705 105

MB 280-16492917 99

MB 280-1651115 99

LCS 280-1644323 92

LCS 280-1646703 106

LCS 280-16492915 102

LCS 280-1651113 103

LCSD 280-1644324 94

LCSD 280-1646704 103

LCSD 280-16492916 97



TestAmerica Denver

Page 73 of 962



Sdg Number 13025120




Client Matrix Water


DCA

Rec

LCSD 280-1651114 105

280-39772-2 MS PIN12-0555B MS 96

280-39873-C-4 MS 97

280-39873-A-2 MS 98

280-39772-2 MSD PIN12-0555B MSD 98

280-39873-C-4 MSD 100

280-39873-A-2 MSD 102



TestAmerica Denver

Page 74 of 962


Job Number 280-39772-1Client SM Stoller Corporation

Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID

Method Blank - Batch 280-164920

Instrument ID

Lab File ID


Final WeightVolume

RR1859D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1649205

Analysis Date 03142013 2102

Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164920

Prep Date

Leach Date

03142013 2102

NA

Analyte RLMDLQualResult

19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1859D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1649205


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164920

Prep Date

Leach Date

03142013 2102

NA



017 U 10017Styrene




017 U 10017Toluene













Surrogate Rec Acceptance Limits

12-Dichloroethane-d4 (Surr) 89 70 - 127

Toluene-d8 (Surr) 94 80 - 125

4-Bromofluorobenzene (Surr) 90 78 - 120

Dibromofluoromethane (Surr) 93 77 - 120




Sdg Number 13025120

Water

10

Lab Control Sample - Batch 280-164920

Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR1858D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1649204


Analysis Batch

Prep Batch

Leach Batch

280-164920

NA

NA

Prep Date

Leach Date

03142013 2039

NA

Analyte QualLimit RecResultSpike Amount

500 450 90 74 - 135Benzene

500 518 104 73 - 135Bromodichloromethane

500 543 109 67 - 135Carbon tetrachloride

500 435 87 76 - 135Chlorobenzene

500 509 102 76 - 120Chloroform

500 457 91 74 - 13513-Dichlorobenzene

500 456 91 75 - 13511-Dichloroethane

500 461 92 75 - 135trans-12-Dichloroethene

500 515 103 71 - 13611-Dichloroethene

500 458 92 71 - 12012-Dichloropropane

500 457 91 72 - 120Ethylbenzene

500 429 86 54 - 141Methylene Chloride

500 450 90 70 - 135Tetrachloroethene

500 459 92 73 - 120Toluene

500 542 108 70 - 135111-Trichloroethane

500 476 95 73 - 135Trichloroethene









Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR1864D

20 mL

20 mL

RR1865D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39772-1

280-39772-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike

Matrix Spike Duplicate Recovery Report - Batch 280-164920

03142013 2258

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164920

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2321

03142013 2321

NA

Analysis Batch

Prep Batch

Leach Batch

280-164920

NA

NA

03142013 2258

Analyte RPD LimitRPDLimit

Rec

MS MSD MS Qual MSD Qual

96 87 74 - 135 10 20Benzene

101 95 73 - 135 6 20Bromodichloromethane

120 104 67 - 135 14 21Carbon tetrachloride

95 85 76 - 135 11 20Chlorobenzene

107 97 76 - 120 10 20Chloroform

102 91 74 - 135 11 2013-Dichlorobenzene

95 86 75 - 135 10 2111-Dichloroethane

101 92 75 - 135 9 24trans-12-Dichloroethene

111 99 71 - 136 11 2011-Dichloroethene

90 81 71 - 120 11 2012-Dichloropropane

103 92 72 - 120 11 26Ethylbenzene

76 70 54 - 141 8 20Methylene Chloride

103 93 70 - 135 10 20Tetrachloroethene

100 91 73 - 120 10 20Toluene

120 106 70 - 135 12 20111-Trichloroethane

106 96 73 - 135 10 20Trichloroethene

Surrogate Acceptance LimitsMS Rec MSD Rec

12-Dichloroethane-d4 (Surr) 84 85 70 - 127

Toluene-d8 (Surr) 92 90 80 - 125

4-Bromofluorobenzene (Surr) 88 88 78 - 120

Dibromofluoromethane (Surr) 89 89 77 - 120




Sdg Number 13025120

Water

03142013 2258 03142013 2321

Dilution Dilution10 10

Client Matrix Client Matrix Water

Method 8260B

Preparation 5030B

Units ugL280-39772-1 280-39772-1MS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03142013 2258

NA

Analysis Date

Prep Date

Leach Date

03142013 2321

NA

Amount

Sample

Analyte ResultQual Amount ResultQual ResultQual

MS MSDMS Spike MSD Spike

016 U 500 500 479 433Benzene

017 U 500 500 506 476Bromodichloromethane

019 U 500 500 598 518Carbon tetrachloride

017 U 500 500 476 425Chlorobenzene

016 U 500 500 533 484Chloroform

013 U 500 500 509 45613-Dichlorobenzene

022 U 500 500 475 43011-Dichloroethane

015 U 500 500 504 460trans-12-Dichloroethene

023 U 500 500 556 49511-Dichloroethene

018 U 500 500 450 40412-Dichloropropane

016 U 500 500 513 461Ethylbenzene

032 U 500 500 379 350Methylene Chloride

020 U 500 500 514 466Tetrachloroethene

017 U 500 500 502 454Toluene

016 U 500 500 599 531111-Trichloroethane

016 U 500 500 528 478Trichloroethene




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

g2_6134D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_G2MB 280-1649347


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164934

Prep Date

Leach Date

03152013 0716

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

g2_6134D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_G2MB 280-1649347


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164934

Prep Date

Leach Date

03152013 0716

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

g2_6133D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_G2LCS 280-1649346


Analysis Batch

Prep Batch

Leach Batch

280-164934

NA

NA

Prep Date

Leach Date

03152013 0650

NA


500 406 81 74 - 135Benzene




500 396 79 76 - 120Chloroform


500 408 82 75 - 13511-Dichloroethane


500 447 89 71 - 13611-Dichloroethene


500 425 85 72 - 120Ethylbenzene



500 423 85 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

g2_6139D

20 mL

20 mL

g2_6140D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_G2

VMS_G2

280-39751-I-1 MS

280-39751-I-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0940

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164934

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0959

03152013 0959

NA

Analysis Batch

Prep Batch

Leach Batch

280-164934

NA

NA

03152013 0940


Rec


86 84 74 - 135 2 20Benzene



89 85 76 - 135 5 20Chlorobenzene

86 84 76 - 120 3 20Chloroform


90 87 75 - 135 3 2111-Dichloroethane


97 95 71 - 136 2 2011-Dichloroethene


90 89 72 - 120 1 26Ethylbenzene



87 86 73 - 120 2 20Toluene





Toluene-d8 (Surr) 99 98 80 - 125






Sdg Number 13025120

Water

03152013 0940 03152013 0959



Method 8260B

Preparation 5030B

Units ugL280-39751-I-1 MS 280-39751-I-1 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0940

NA

Analysis Date

Prep Date

Leach Date

03152013 0959

NA

Amount

Sample



016 U 500 500 432 422Benzene




016 U 500 500 428 418Chloroform






016 U 500 500 448 443Ethylbenzene



017 U 500 500 437 429Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1914D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1651125


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165112

Prep Date

Leach Date

03152013 1939

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1914D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1651125


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165112

Prep Date

Leach Date

03152013 1939

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR1913D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1651124


Analysis Batch

Prep Batch

Leach Batch

280-165112

NA

NA

Prep Date

Leach Date

03152013 1916

NA


500 525 105 74 - 135Benzene




500 481 96 76 - 120Chloroform


500 477 95 75 - 13511-Dichloroethane


500 569 114 71 - 13611-Dichloroethene


500 523 105 72 - 120Ethylbenzene



500 513 103 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR1916D

20 mL

20 mL

RR1917D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39756-O-16 MS

280-39756-O-16 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 2030

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165112

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2053

03152013 2053

NA

Analysis Batch

Prep Batch

Leach Batch

280-165112

NA

NA

03152013 2030


Rec


99 92 74 - 135 7 20Benzene




96 92 76 - 120 4 20Chloroform


92 84 75 - 135 9 2111-Dichloroethane


110 99 71 - 136 11 2011-Dichloroethene


95 89 72 - 120 6 26Ethylbenzene



98 94 73 - 120 4 20Toluene





Toluene-d8 (Surr) 90 91 80 - 125






Sdg Number 13025120

Water

03152013 2030 03152013 2053



Method 8260B

Preparation 5030B

Units ugL280-39756-O-16 MS 280-39756-O-16 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 2030

NA

Analysis Date

Prep Date

Leach Date

03152013 2053

NA

Amount

Sample



016 U 500 500 493 460Benzene




016 U 500 500 482 462Chloroform






016 U 500 500 474 446Ethylbenzene



017 U 500 500 492 472Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3709D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1644325


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164432

Prep Date

Leach Date

03122013 1959

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample

Lab Control Sample Duplicate Recovery Report - Batch 280-164432

10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3707D

20 mL

20 mL

E3708D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1644323

LCSD 280-1644324

Analysis Date

Prep Date

Leach Date

03122013 1924

03122013 1924

NA

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

Analysis Date

Prep Date

Leach Date

03122013 1942

03122013 1942

NA

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

Analyte LCSD QualLCS QualRPD LimitRPDLimitLCSDLCS

Rec

8985 25 - 141 4 2014-Dioxane

Surrogate LCS Rec LCSD Rec Acceptance Limits





Sdg Number 13025120

Water

03122013 1924


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control

Laboratory Duplicate Data Report - Batch 280-164432

Method 8260B SIM

Preparation 5030B

Units ugLLCS 280-1644323 LCSD 280-1644324LCS Lab Sample ID

Analysis Date

Prep Date

Leach Date

03122013 1924

Analysis Date

Prep Date

Leach Date

03122013 1942

03122013 1942

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443426500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3717D

20 mL

20 mL

E3718D

20 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39772-2

280-39772-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03122013 2221

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

Analysis Date

Prep Date

Leach Date

03122013 2239

03122013 2239

NA

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

03122013 2221


Rec


94 97 25 - 141 3 2014-Dioxane






Sdg Number 13025120

Water

03122013 2221 03122013 2239



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03122013 2221

NA

Analysis Date

Prep Date

Leach Date

03122013 2239

NA

Amount

Sample



022 U 500 500 470 48314-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3740D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1646705


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164670

Prep Date

Leach Date

03132013 2042

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3738D

20 mL

20 mL

E3739D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1646703

LCSD 280-1646704

Analysis Date

Prep Date

Leach Date

03132013 2007

03132013 2007

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA


Rec

7883 25 - 141 7 2014-Dioxane






Sdg Number 13025120

Water

03132013 2007


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03132013 2007

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

390417500 50014-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3783D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16492917


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164929

Prep Date

Leach Date

03142013 2354

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3781D

20 mL

20 mL

E3782D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16492915

LCSD 280-16492916

Analysis Date

Prep Date

Leach Date

03142013 2319

03142013 2319

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA


Rec

8980 25 - 141 10 2014-Dioxane






Sdg Number 13025120

Water

03142013 2319


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03142013 2319

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443400500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3787D

1 mL

20 mL

E3788D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-C-4 MS

280-39873-C-4 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0104

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

03152013 0121

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

03152013 0104


Rec


125 154 25 - 141 10 20 F14-Dioxane






Sdg Number 13025120

Water

03152013 0104 03152013 0121



Method 8260B SIM

Preparation 5030B

Units ugL280-39873-C-4 MS 280-39873-C-4 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0104

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

NA

Amount

Sample



170 100 100 292 322 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3822D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1651115


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165111

Prep Date

Leach Date

03152013 1916

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3820D

20 mL

20 mL

E3821D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1651113

LCSD 280-1651114

Analysis Date

Prep Date

Leach Date

03152013 1841

03152013 1841

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA


Rec

8278 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1841


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03152013 1841

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

409391500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3824D

10 mL

20 mL

E3825D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-A-2 MS

280-39873-A-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 1951

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

03152013 2009

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

03152013 1951


Rec


89 94 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1951 03152013 2009



Method 8260B SIM

Preparation 5030B

Units ugL280-39873-A-2 MS 280-39873-A-2 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 1951

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

NA

Amount

Sample



044 U 100 100 895 94414-Dioxane




QC Association Summary

Lab Sample ID Client Sample ID Client Matrix Method Prep Batch

Sdg Number 13025120

Report

Basis

GCMS VOA

Analysis Batch280-164432

Lab Control Sample Water 8260B SIMLCS 280-1644323 T

Lab Control Sample Duplicate Water 8260B SIMLCSD 280-1644324 T

Method Blank Water 8260B SIMMB 280-1644325 T

WaterPIN12-0555A 8260B SIM280-39772-1 T

WaterPIN12-0555B 8260B SIM280-39772-2 T

Matrix Spike Water 8260B SIM280-39772-2MS T

Matrix Spike Duplicate Water 8260B SIM280-39772-2MSD T

WaterPIN12-0555C 8260B SIM280-39772-3 T

WaterPIN12-0565-1 8260B SIM280-39772-4 T

WaterPIN12-0565-2 8260B SIM280-39772-5 T

WaterPIN12-0565-3 8260B SIM280-39772-6 T

WaterPIN12-0573-1 8260B SIM280-39772-7 T

WaterPIN12-0573-2 8260B SIM280-39772-8 T

WaterPIN12-0573-3 8260B SIM280-39772-9 T

WaterPIN12-0575-1 8260B SIM280-39772-10 T

WaterPIN12-0575-2 8260B SIM280-39772-11 T

WaterPIN12-0580-1 8260B SIM280-39772-12 T





WaterPIN12-0580-2 8260B SIM280-39772-13 T

WaterPIN12-S67B 8260B SIM280-39772-16 T

WaterPIN12-S67D 8260B SIM280-39772-18 T


Lab Control Sample Water 8260BLCS 280-1649204 T

Method Blank Water 8260BMB 280-1649205 T

WaterPIN12-0555A 8260B280-39772-1 T

Matrix Spike Water 8260B280-39772-1MS T

Matrix Spike Duplicate Water 8260B280-39772-1MSD T

WaterPIN12-0555B 8260B280-39772-2 T

WaterPIN12-0555C 8260B280-39772-3 T

WaterPIN12-0580-1 8260B280-39772-12 T

WaterPIN12-0580-2 8260B280-39772-13 T

WaterPIN12-0580-3 8260B280-39772-14 T

WaterPIN12-2450 8260B280-39772-15 T

WaterPIN12-S67B 8260B280-39772-16 T

WaterPIN12-S67C 8260B280-39772-17 T

WaterPIN12-S67D 8260B280-39772-18 T

TestAmerica Denver

Page 101 of 962





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0580-3 8260B SIM280-39772-14 T

WaterPIN12-2450 8260B SIM280-39772-15 T

Matrix Spike Water 8260B SIM280-39873-C-4 MS T

Matrix Spike Duplicate Water 8260B SIM280-39873-C-4 MSD T




Matrix Spike Water 8260B280-39751-I-1 MS T

Matrix Spike Duplicate Water 8260B280-39751-I-1 MSD T

WaterPIN12-0565-1 8260B280-39772-4 T

WaterPIN12-0565-2 8260B280-39772-5 T

WaterPIN12-0565-3 8260B280-39772-6 T

WaterPIN12-0573-1 8260B280-39772-7 T

WaterPIN12-0573-2 8260B280-39772-8 T

WaterPIN12-0573-3 8260B280-39772-9 T

WaterPIN12-0575-1 8260B280-39772-10 T

WaterPIN12-0575-2 8260B280-39772-11 T

WaterPIN99-2198 8260B280-39772-19 T





WaterPIN12-S67C 8260B SIM280-39772-17 T

Matrix Spike Water 8260B SIM280-39873-A-2 MS T

Matrix Spike Duplicate Water 8260B SIM280-39873-A-2 MSD T




Matrix Spike Water 8260B280-39756-O-16 MS T

Matrix Spike Duplicate Water 8260B280-39756-O-16 MSD T

WaterPIN12-0580-2 8260B280-39772-13DL T

WaterPIN12-2450 8260B280-39772-15DL T

WaterPIN12-S67B 8260B280-39772-16DL T

WaterPIN12-S67C 8260B280-39772-17DL T

Report Basis

T = Total

TestAmerica Denver

Page 102 of 962

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 1510



Data Summaries 4

Report Narrative 4

Data Qualifiers 6

Sample Summary 7

Executive Summary 8

Method Summary 12




QC Data Summary 103


Lab Chronicle 140



GCMS VOA 196




Page 2 of 1510










Page 3 of 1510

CASE NARRATIVE







calculated results








RECEIPT

The samples were received on 3132013 900 AM the samples arrived in good condition properly preserved and where required on

ice The temperature of the cooler at receipt was 17ordm C


In some cases due to high concentrations of target analytes andor the nature of the sample matrix (foamy) reduced aliquot sizes had to

be used for the analysis of samples The reporting limits have been elevated accordingly To provide the lowest possible detection limits

multiple runs are reported where available

Sample PIN12-0539 (LDU 854) was received at the laboratory with insufficient preservation measuring a pH of 7 If samples are not

preserved to a pH of 20 and analyses are performed outside a 7 day holding time experimental evidence suggests that some aromatic

compounds in wastewater samples notably benzene toluene and ethylbenzene are susceptible to biological degradation The sample

was analyzed within the normal 14 day holding time but outside a 7 day holding time

The MSD aliquot of the MSMSD performed on sample PIN12-0524 (LDU 852) in batch 280-165236 exhibited spike compound recoveries

outside the control limits biased high The LCS was within control limits

The accuracy and precision of the MSMSD associated with batch 280-165434 could not be reliably evaluated for some compounds as

the concentrations present in the parent sample are 4 times greater than the matrix spike concentrations In addition MS andor MSD

concentrations are present above the instrument calibration range for some compounds The LCS and LCSD were within control limits

The MSMSD associated with batch 280-165627 exhibited percent recoveries outside the control limits biased high for

11-Dichloroethane The LCS was within control limits



In some cases due to the nature of the sample matrix (foamy) andor due to high constituent concentration samples had to be analyzed

using reduced aliquot sizes The reporting limits have been elevated accordingly

Surrogate 12-Dichloroethane-d4 was recovered outside the control limits biased high in samples PIN12-0581-1 (LDU-876)

PIN12-0581-2 (LDU 877) and PIN12-0582-1 (LDU 879) As no detectable concentrations are present in the sampleS data are reported

as is

In some cases the internal standard response for 14-Dichlorobenzene-d4 was outside acceptance criteria for samples in batch

280-165111 As this internal standard is not associated with the analyte of interest (14-Dioxane) data are reported as is



The MSD aliquot of the MSMSD performed on sample PIN12-0540 (LDU 855) in batch 280-164929 exhibited the percent recovery

outside the control limits biased high The LCS and LCSD were within control limits

Page 4 of 1510

The RPD limit was exceeded in the MSMSD associated with batch 280-165812 Method precision and accuracy have been verified by

the acceptable LCSLCSD analysis data

The MSMSD associated with batch 280-166279 exhibited percent recoveries outside the control limits biased high It can be noted that

the MS and MSD concentrations were present above the instrument calibration range The LCS and LCSD were within control limits


Page 5 of 1510




Sdg Number 13025120

GCMS VOA



MS MSD The analyte present in the original sample is 4 times greater

than the matrix spike concentration therefore control limits are not

applicable

4

Result exceeded calibration rangeE



J

RPD of the MS and MSD exceeds the control limitsF



SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39873-1 PIN12-0524 Water 03092013 0748 03132013 0900

280-39873-1MS PIN12-0524 Water 03092013 0748 03132013 0900

280-39873-1MSD PIN12-0524 Water 03092013 0748 03132013 0900

280-39873-2 PIN12-0525 Water 03092013 0826 03132013 0900

280-39873-2MS PIN12-0525 Water 03092013 0826 03132013 0900

280-39873-2MSD PIN12-0525 Water 03092013 0826 03132013 0900

280-39873-3 PIN12-0539 Water 03082013 1635 03132013 0900

280-39873-4 PIN12-0540 Water 03082013 1548 03132013 0900

280-39873-5 PIN12-0541 Water 03082013 1241 03132013 0900

280-39873-6 PIN12-0542 Water 03082013 1310 03132013 0900

280-39873-7 PIN12-0549 Water 03082013 1413 03132013 0900

280-39873-8 PIN12-0554A Water 03082013 0919 03132013 0900

280-39873-9 PIN12-0554B Water 03082013 1005 03132013 0900

280-39873-10 PIN12-0554C Water 03082013 1110 03132013 0900

280-39873-11 PIN12-0581-1 Water 03112013 0851 03132013 0900

280-39873-12 PIN12-0581-2 Water 03112013 0923 03132013 0900

280-39873-13 PIN12-0581-3 Water 03112013 1025 03132013 0900

280-39873-14 PIN12-0582-1 Water 03112013 1147 03132013 0900

280-39873-15 PIN12-0582-2 Water 03112013 1218 03132013 0900

280-39873-16 PIN12-0582-3 Water 03112013 1253 03132013 0900

280-39873-17 PIN12-0585-3 Water 03092013 1133 03132013 0900

280-39873-18 PIN12-2451 Water 03112013 1200 03132013 0900

280-39873-19 PIN12-2452 Water 03112013 1210 03132013 0900

280-39873-20 PIN12-S71B Water 03092013 0908 03132013 0900

280-39873-21 PIN12-S71C Water 03092013 0936 03132013 0900

280-39873-22 PIN12-S71D Water 03092013 1026 03132013 0900

280-39873-23 PIN12-S73B Water 03112013 1430 03132013 0900

280-39873-24 PIN12-S73C Water 03112013 1603 03132013 0900

280-39873-25 PIN12-S73D Water 03112013 1648 03132013 0900

280-39873-26 PIN99-2448 Water 03082013 0900 03132013 0900




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-1 PIN12-0524

20 ugL 8260B19 JBenzene



20 ugL 8260B1611-Dichloroethene


280-39873-2 PIN12-0525


280-39873-3 PIN12-0539







280-39873-4 PIN12-0540







280-39873-5 PIN12-0541

10 ugL 8260B10Acetone


280-39873-6 PIN12-0542

40 ugL 8260B44Methylene Chloride

280-39873-7 PIN12-0549







Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-8 PIN12-0554A


280-39873-10 PIN12-0554C








280-39873-11 PIN12-0581-1




10 ugL 8260B050 JVinyl chloride

280-39873-12 PIN12-0581-2



10 ugL 8260B37 JMethylene Chloride

280-39873-13 PIN12-0581-3


280-39873-14 PIN12-0582-1




280-39873-15 PIN12-0582-2










Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-16 PIN12-0582-3



280-39873-17 PIN12-0585-3

10 ugL 8260B41Carbon disulfide




50 ugL 8260B39 J2-Hexanone

10 ugL 8260B071 JTrichloroethene


280-39873-18 PIN12-2451





280-39873-19 PIN12-2452





10 ugL 8260B023 JNaphthalene



280-39873-21 PIN12-S71C










Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-22 PIN12-S71D






280-39873-23 PIN12-S73B





280-39873-24 PIN12-S73C







280-39873-25 PIN12-S73D




METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120


Meier Greg P GPMSW846 8260B

Wickham Tom TWSW846 8260B


TestAmerica Denver

Page 13 of 1510

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03182013 1142

03182013 1142

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5339D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


38 U 2038Acetone

19 J 20032Benzene




























16 2004611-Dichloroethene









34 U 10342-Hexanone







034 U 20034Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03182013 1142

03182013 1142

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5339D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method





034 U 20034Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03182013 1202

03182013 1202

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5340D

1 mL

20 mLRun Type DL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0525

Client Matrix

280-39873-2

Water




Dilution

03182013 1304

03182013 1304

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5343D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0525

Client Matrix

280-39873-2

Water




Dilution

03182013 1304

03182013 1304

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5343D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03182013 1324

03182013 1324

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5344D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


47 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03182013 1324

03182013 1324

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5344D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03192013 1338

03192013 1338

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2023D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03182013 1345

03182013 1345

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5345D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


57 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03182013 1345

03182013 1345

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5345D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03192013 1203

03192013 1203

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2019D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0541

Client Matrix

280-39873-5

Water




Dilution

03182013 1426

03182013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5347D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


10 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0541

Client Matrix

280-39873-5

Water




Dilution

03182013 1426

03182013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5347D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0542

Client Matrix

280-39873-6

Water




Dilution

03192013 1536

03192013 1536

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2028D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone



44 4013Methylene Chloride





Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0542

Client Matrix

280-39873-6

Water




Dilution

03192013 1536

03192013 1536

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2028D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0549

Client Matrix

280-39873-7

Water




Dilution

03182013 1507

03182013 1507

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5349D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


14 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0549

Client Matrix

280-39873-7

Water




Dilution

03182013 1507

03182013 1507

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5349D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554A

Client Matrix

280-39873-8

Water




Dilution

03182013 1527

03182013 1527

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5350D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


98 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554A

Client Matrix

280-39873-8

Water




Dilution

03182013 1527

03182013 1527

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5350D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554B

Client Matrix

280-39873-9

Water




Dilution

03192013 1600

03192013 1600

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2029D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554B

Client Matrix

280-39873-9

Water




Dilution

03192013 1600

03192013 1600

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2029D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03182013 1607

03182013 1607

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5352D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


67 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03182013 1607

03182013 1607

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5352D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method





017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03182013 1627

03182013 1627

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5353D

10 mL

20 mLRun Type DL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-1

Client Matrix

280-39873-11

Water




Dilution

03182013 1648

03182013 1648

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5354D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


87 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-1

Client Matrix

280-39873-11

Water




Dilution

03182013 1648

03182013 1648

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5354D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene










050 J 10010Vinyl chloride









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-2

Client Matrix

280-39873-12

Water




Dilution

03192013 1250

03192013 1250

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2021D

2 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 10019Acetone

16 U 1016Benzene




19 U 1019Bromoform











16 U 1016Chloroform























17 U 50172-Hexanone



37 J 1032Methylene Chloride





Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-2

Client Matrix

280-39873-12

Water




Dilution

03192013 1250

03192013 1250

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2021D

2 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


17 U 1017Styrene




17 U 1017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-3

Client Matrix

280-39873-13

Water




Dilution

03182013 1728

03182013 1728

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5356D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


93 J 2038Acetone

032 U 20032Benzene






































34 U 10342-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-3

Client Matrix

280-39873-13

Water




Dilution

03182013 1728

03182013 1728

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5356D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


034 U 20034Styrene




034 U 20034Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-1

Client Matrix

280-39873-14

Water




Dilution

03182013 1748

03182013 1748

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5357D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


73 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-1

Client Matrix

280-39873-14

Water




Dilution

03182013 1748

03182013 1748

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5357D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03182013 1808

03182013 1808

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5358D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


73 J 2038Acetone

032 U 20032Benzene






































34 U 10342-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03182013 1808

03182013 1808

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5358D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


034 U 20034Styrene




034 U 20034Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03192013 1314

03192013 1314

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2022D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-3

Client Matrix

280-39873-16

Water




Dilution

03192013 1042

03192013 1042

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0948D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-3

Client Matrix

280-39873-16

Water




Dilution

03192013 1042

03192013 1042

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0948D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03192013 1127

03192013 1127

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0950D

4 mL

20 mLRun Type DL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03202013 0810

03202013 0810

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2931D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene










41 10045Carbon disulfide



























39 J 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03202013 0810

03202013 0810

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2931D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method





017 U 10017Toluene





071 J 10016Trichloroethene













Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2451

Client Matrix

280-39873-18

Water




Dilution

03192013 1448

03192013 1448

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0959D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2451

Client Matrix

280-39873-18

Water




Dilution

03192013 1448

03192013 1448

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0959D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03192013 1510

03192013 1510

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0960D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone





023 J 10022Naphthalene



Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03192013 1510

03192013 1510

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0960D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03202013 0833

03202013 0833

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2932D

5 mL

20 mLRun Type DL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71B

Client Matrix

280-39873-20

Water




Dilution

03192013 1554

03192013 1554

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0962D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71B

Client Matrix

280-39873-20

Water




Dilution

03192013 1554

03192013 1554

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0962D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71C

Client Matrix

280-39873-21

Water




Dilution

03192013 1617

03192013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0963D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71C

Client Matrix

280-39873-21

Water




Dilution

03192013 1617

03192013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0963D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71D

Client Matrix

280-39873-22

Water




Dilution

03202013 0857

03202013 0857

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2933D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71D

Client Matrix

280-39873-22

Water




Dilution

03202013 0857

03202013 0857

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2933D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73B

Client Matrix

280-39873-23

Water




Dilution

03192013 1701

03192013 1701

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0965D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73B

Client Matrix

280-39873-23

Water




Dilution

03192013 1701

03192013 1701

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0965D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03202013 0919

03202013 0919

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2934D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03202013 0919

03202013 0919

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2934D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03202013 0942

03202013 0942

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2935D

4 mL

20 mLRun Type DL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73D

Client Matrix

280-39873-25

Water




Dilution

03192013 1745

03192013 1745

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0967D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73D

Client Matrix

280-39873-25

Water




Dilution

03192013 1745

03192013 1745

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0967D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2448

Client Matrix

280-39873-26

Water




Dilution

03192013 1149

03192013 1149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0951D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2448

Client Matrix

280-39873-26

Water




Dilution

03192013 1149

03192013 1149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0951D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03222013 2012

03222013 2012

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4018D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0525

Client Matrix

280-39873-2

Water




Dilution

03152013 1934

03152013 1934

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3823D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03152013 0029

03152013 0029

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3785D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


38 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03152013 0046

03152013 0046

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3786D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


170 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0541

Client Matrix

280-39873-5

Water




Dilution

03142013 0030

03142013 0030

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3753D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0542

Client Matrix

280-39873-6

Water




Dilution

03152013 0139

03152013 0139

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3789D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0549

Client Matrix

280-39873-7

Water




Dilution

03152013 0156

03152013 0156

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3790D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554A

Client Matrix

280-39873-8

Water




Dilution

03142013 0122

03142013 0122

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3756D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554B

Client Matrix

280-39873-9

Water




Dilution

03152013 0214

03152013 0214

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3791D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03152013 0231

03152013 0231

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3792D

4 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


76 501114-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-1

Client Matrix

280-39873-11

Water




Dilution

03152013 2028

03152013 2028

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3826D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-2

Client Matrix

280-39873-12

Water




Dilution

03152013 2323

03152013 2323

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3827D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-3

Client Matrix

280-39873-13

Water




Dilution

03202013 2244

03202013 2244

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3932D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-1

Client Matrix

280-39873-14

Water




Dilution

03152013 2358

03152013 2358

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3829D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03202013 2302

03202013 2302

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3933D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-3

Client Matrix

280-39873-16

Water




Dilution

03162013 0033

03162013 0033

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3831D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03152013 0249

03152013 0249

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3793D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2451

Client Matrix

280-39873-18

Water




Dilution

03162013 0051

03162013 0051

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3832D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03222013 2029

03222013 2029

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4019D

05 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


170 408814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71B

Client Matrix

280-39873-20

Water




Dilution

03142013 0232

03142013 0232

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3760D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71C

Client Matrix

280-39873-21

Water




Dilution

03152013 0306

03152013 0306

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3794D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


34 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71D

Client Matrix

280-39873-22

Water




Dilution

03162013 0126

03162013 0126

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3834D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73B

Client Matrix

280-39873-23

Water




Dilution

03162013 0143

03162013 0143

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3835D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03222013 2046

03222013 2046

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4020D

2 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


130 102214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73D

Client Matrix

280-39873-25

Water




Dilution

03222013 2104

03222013 2104

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4021D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39873-1 PIN12-0524 105 109 97 101

280-39873-1 DL PIN12-0524 DL 114 121 101 101

280-39873-2 PIN12-0525 112 126 98 109

280-39873-3 PIN12-0539 103 113 90 95

280-39873-3 DL PIN12-0539 DL 82 74 90 87

280-39873-4 PIN12-0540 105 113 91 94

280-39873-4 DL PIN12-0540 DL 85 75 95 93

280-39873-5 PIN12-0541 103 117 87 94

280-39873-6 PIN12-0542 84 75 94 87

280-39873-7 PIN12-0549 109 124 95 96

280-39873-8 PIN12-0554A 115 127 92 99

280-39873-9 PIN12-0554B 85 76 90 88

280-39873-10 PIN12-0554C 111 123 95 95

280-39873-10 DL PIN12-0554C DL 108 120 92 93

280-39873-11 PIN12-0581-1 95 110 82 82

280-39873-12 PIN12-0581-2 82 75 92 85

280-39873-13 PIN12-0581-3 112 125 94 97

280-39873-14 PIN12-0582-1 107 121 89 89

280-39873-15 PIN12-0582-2 110 119 92 90

280-39873-15 DL PIN12-0582-2 DL 87 77 95 89

280-39873-16 PIN12-0582-3 111 127 101 102

280-39873-17 DL PIN12-0585-3 DL 107 117 95 97

280-39873-17 PIN12-0585-3 99 101 119 96

280-39873-18 PIN12-2451 110 127 106 101

280-39873-19 PIN12-2452 106 123 94 96

280-39873-19 DL PIN12-2452 DL 101 101 98 98

280-39873-20 PIN12-S71B 105 120 94 99

280-39873-21 PIN12-S71C 109 126 99 99

280-39873-22 PIN12-S71D 116 119 92 92






TestAmerica Denver

Page 99 of 1510



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39873-23 PIN12-S73B 108 121 95 98

280-39873-24 PIN12-S73C 97 99 91 92

280-39873-24 DL PIN12-S73C DL 95 94 92 92

280-39873-25 PIN12-S73D 108 122 98 95

280-39873-26 PIN99-2448 112 125 102 102

MB 280-16523632 105 113 93 97

MB 280-1654345 108 117 98 100

MB 280-1654515 82 70 98 90

MB 280-1656275 100 100 100 98

LCS 280-16523631 106 112 92 89

LCS 280-1654344 106 121 107 97

LCS 280-1654514 85 74 98 94

LCS 280-1656274 97 96 103 93

280-39873-1 MS PIN12-0524 MS 105 114 93 95

280-39974-C-1 MS 108 122 113 106

280-39875-B-1 MS 84 74 96 90

280-40045-A-1 MS 97 96 96 92

280-39873-1 MSD PIN12-0524 MSD 110 117 97 97

280-39974-C-1 MSD 104 120 100 93

280-39875-B-1 MSD 86 77 96 90

280-40045-A-1 MSD 100 100 98 92






TestAmerica Denver

Page 100 of 1510



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39873-1 PIN12-0524 93

280-39873-2 PIN12-0525 99

280-39873-3 PIN12-0539 98

280-39873-4 PIN12-0540 100

280-39873-5 PIN12-0541 108

280-39873-6 PIN12-0542 103

280-39873-7 PIN12-0549 108

280-39873-8 PIN12-0554A 114

280-39873-9 PIN12-0554B 102

280-39873-10 PIN12-0554C 100

280-39873-11 PIN12-0581-1 132X

280-39873-12 PIN12-0581-2 134X

280-39873-13 PIN12-0581-3 99

280-39873-14 PIN12-0582-1 130X

280-39873-15 PIN12-0582-2 112

280-39873-16 PIN12-0582-3 112

280-39873-17 PIN12-0585-3 108

280-39873-18 PIN12-2451 121

280-39873-19 PIN12-2452 94

280-39873-20 PIN12-S71B 109

280-39873-21 PIN12-S71C 107

280-39873-22 PIN12-S71D 113

280-39873-23 PIN12-S73B 110

280-39873-24 PIN12-S73C 96

280-39873-25 PIN12-S73D 97

MB 280-1646705 105

MB 280-16492917 99

MB 280-1651115 99

MB 280-16581217 96



TestAmerica Denver

Page 101 of 1510



Sdg Number 13025120




Client Matrix Water


DCA

Rec

MB 280-1662795 93

LCS 280-1646703 106

LCS 280-16492915 102

LCS 280-1651113 103

LCS 280-16581215 100

LCS 280-1662793 97

LCSD 280-1646704 103

LCSD 280-16492916 97

LCSD 280-1651114 105

LCSD 280-16581216 96

LCSD 280-1662794 97

280-39873-2 MS PIN12-0525 MS 98

280-39873-4 MS PIN12-0540 MS 97

280-39875-D-2 MS 98

280-39986-B-5 MS 105

280-39873-2 MSD PIN12-0525 MSD 102

280-39873-4 MSD PIN12-0540 MSD 100

280-39875-D-2 MSD 101

280-39986-B-5 MSD 107



TestAmerica Denver

Page 102 of 1510



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5338D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-16523632


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165236

Prep Date

Leach Date

03182013 1050

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5338D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-16523632


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165236

Prep Date

Leach Date

03182013 1050

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

C5337D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CLCS 280-16523631


Analysis Batch

Prep Batch

Leach Batch

280-165236

NA

NA

Prep Date

Leach Date

03182013 1030

NA


500 521 104 74 - 135Benzene




500 599 120 76 - 120Chloroform


500 535 107 75 - 13511-Dichloroethane


500 591 118 71 - 13611-Dichloroethene


500 473 95 72 - 120Ethylbenzene



500 544 109 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5341D

10 mL

20 mL

C5342D

10 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-39873-1

280-39873-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03182013 1222

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165236

NA

NA

Analysis Date

Prep Date

Leach Date

03182013 1243

03182013 1243

NA

Analysis Batch

Prep Batch

Leach Batch

280-165236

NA

NA

03182013 1222


Rec


104 106 74 - 135 2 20Benzene


134 136 67 - 135 1 21 FCarbon tetrachloride


116 121 76 - 120 4 20 FChloroform


110 115 75 - 135 5 2111-Dichloroethane


109 112 71 - 136 1 2011-Dichloroethene


95 97 72 - 120 2 26Ethylbenzene



112 113 73 - 120 1 20Toluene

132 136 70 - 135 3 20 F111-Trichloroethane




Toluene-d8 (Surr) 93 97 80 - 125






Sdg Number 13025120

Water

03182013 1222 03182013 1243



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03182013 1222

NA

Analysis Date

Prep Date

Leach Date

03182013 1243

NA

Amount

Sample



19 J 100 100 123 125Benzene


038 U 100 100 134 136 FCarbon tetrachloride


032 U 100 100 116 121 FChloroform



71 100 100 179 185trans-12-Dichloroethene

16 100 100 274 27611-Dichloroethene


032 U 100 100 951 973Ethylbenzene



034 U 100 100 112 113Toluene

032 U 100 100 132 136 F111-Trichloroethane





Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

H0939D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_HMB 280-1654345


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165434

Prep Date

Leach Date

03192013 0722

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

H0939D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_HMB 280-1654345


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165434

Prep Date

Leach Date

03192013 0722

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

H0938D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_HLCS 280-1654344


Analysis Batch

Prep Batch

Leach Batch

280-165434

NA

NA

Prep Date

Leach Date

03192013 0700

NA


500 500 100 74 - 135Benzene



500 515 103 76 - 135Chlorobenzene

500 540 108 76 - 120Chloroform


500 527 105 75 - 13511-Dichloroethane


500 559 112 71 - 13611-Dichloroethene


500 522 104 72 - 120Ethylbenzene



500 512 102 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

H0941D

20 mL

20 mL

H0942D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_H

VMS_H

280-39974-C-1 MS

280-39974-C-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 0807

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165434

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 0829

03192013 0829

NA

Analysis Batch

Prep Batch

Leach Batch

280-165434

NA

NA

03192013 0807


Rec


99 96 74 - 135 3 20Benzene


133 77 67 - 135 10 21 4 4Carbon tetrachloride

100 97 76 - 135 4 20Chlorobenzene

124 91 76 - 120 6 20 4 4Chloroform


102 100 75 - 135 2 2111-Dichloroethane


109 104 71 - 136 4 2011-Dichloroethene


103 97 72 - 120 5 26Ethylbenzene


247 81 70 - 135 14 20 E 4 4Tetrachloroethene

103 100 73 - 120 3 20Toluene


187 -984 73 - 135 10 20 E 4 E 4Trichloroethene



Toluene-d8 (Surr) 113 100 80 - 125






Sdg Number 13025120

Water

03192013 0807 03192013 0829



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 0807

NA

Analysis Date

Prep Date

Leach Date

03192013 0829

NA

Amount

Sample



028 J 500 500 524 508Benzene


23 500 500 299 2724 4Carbon tetrachloride


24 500 500 299 2824 4Chloroform


036 J 500 500 548 53611-Dichloroethane


088 J 500 500 631 60611-Dichloroethene


016 U 500 500 513 486Ethylbenzene

099 J 500 500 570 555Methylene Chloride

53 500 500 655 572E 4 4Tetrachloroethene

017 U 500 500 515 500Toluene

075 J 500 500 663 629111-Trichloroethane

590 500 500 598 540E 4 E 4Trichloroethene




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2010D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1654514


Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Prep Date

Leach Date

03192013 0805

NA


500 491 98 74 - 135Benzene




500 454 91 76 - 120Chloroform


500 453 91 75 - 13511-Dichloroethane


500 545 109 71 - 13611-Dichloroethene


500 499 100 72 - 120Ethylbenzene



500 483 97 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2016D

5 mL

20 mL

RR2017D

5 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39875-B-1 MS

280-39875-B-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 1052

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

03192013 1116

NA

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

03192013 1052


Rec


91 89 74 - 135 2 20Benzene




87 84 76 - 120 5 20Chloroform


84 82 75 - 135 4 2111-Dichloroethane


101 96 71 - 136 4 2011-Dichloroethene


94 89 72 - 120 5 26Ethylbenzene



90 90 73 - 120 0 20Toluene





Toluene-d8 (Surr) 96 96 80 - 125






Sdg Number 13025120

Water

03192013 1052 03192013 1116



Method 8260B

Preparation 5030B

Units ugL280-39875-B-1 MS 280-39875-B-1 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 1052

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

NA

Amount

Sample



064 U 200 200 182 177Benzene




064 U 200 200 175 167Chloroform






064 U 200 200 187 179Ethylbenzene

41 200 200 233 235Methylene Chloride


068 U 200 200 180 179Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

Z2929D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_ZMB 280-1656275


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165627

Prep Date

Leach Date

03202013 0724

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

Z2929D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_ZMB 280-1656275


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165627

Prep Date

Leach Date

03202013 0724

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

Z2928D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_ZLCS 280-1656274


Analysis Batch

Prep Batch

Leach Batch

280-165627

NA

NA

Prep Date

Leach Date

03202013 0701

NA


500 465 93 74 - 135Benzene




500 478 96 76 - 120Chloroform


500 481 96 75 - 13511-Dichloroethane


500 557 111 71 - 13611-Dichloroethene


500 469 94 72 - 120Ethylbenzene



500 423 85 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Z2939D

20 mL

20 mL

Z2940D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_Z

VMS_Z

280-40045-A-1 MS

280-40045-A-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03202013 1115

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165627

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 1138

03202013 1138

NA

Analysis Batch

Prep Batch

Leach Batch

280-165627

NA

NA

03202013 1115


Rec


96 95 74 - 135 1 20Benzene




99 99 76 - 120 0 20Chloroform


101 100 75 - 135 1 2111-Dichloroethane


148 147 71 - 136 1 20 F F11-Dichloroethene


97 96 72 - 120 2 26Ethylbenzene



97 96 73 - 120 1 20Toluene





Toluene-d8 (Surr) 96 98 80 - 125






Sdg Number 13025120

Water

03202013 1115 03202013 1138



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03202013 1115

NA

Analysis Date

Prep Date

Leach Date

03202013 1138

NA

Amount

Sample



016 U 500 500 480 476Benzene




016 U 500 500 495 493Chloroform




023 U 500 500 742 737F F11-Dichloroethene


016 U 500 500 487 479Ethylbenzene



017 U 500 500 485 479Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3740D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1646705


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164670

Prep Date

Leach Date

03132013 2042

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3738D

20 mL

20 mL

E3739D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1646703

LCSD 280-1646704

Analysis Date

Prep Date

Leach Date

03132013 2007

03132013 2007

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA


Rec

7883 25 - 141 7 2014-Dioxane






Sdg Number 13025120

Water

03132013 2007


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03132013 2007

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

390417500 50014-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3783D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16492917


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164929

Prep Date

Leach Date

03142013 2354

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3781D

20 mL

20 mL

E3782D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16492915

LCSD 280-16492916

Analysis Date

Prep Date

Leach Date

03142013 2319

03142013 2319

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA


Rec

8980 25 - 141 10 2014-Dioxane






Sdg Number 13025120

Water

03142013 2319


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03142013 2319

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443400500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3787D

1 mL

20 mL

E3788D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-4

280-39873-4

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0104

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

03152013 0121

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

03152013 0104


Rec


125 154 25 - 141 10 20 F14-Dioxane






Sdg Number 13025120

Water

03152013 0104 03152013 0121



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0104

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

NA

Amount

Sample



170 100 100 292 322 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3822D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1651115


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165111

Prep Date

Leach Date

03152013 1916

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3820D

20 mL

20 mL

E3821D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1651113

LCSD 280-1651114

Analysis Date

Prep Date

Leach Date

03152013 1841

03152013 1841

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA


Rec

8278 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1841


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03152013 1841

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

409391500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3824D

10 mL

20 mL

E3825D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-2

280-39873-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 1951

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

03152013 2009

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

03152013 1951


Rec


89 94 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1951 03152013 2009



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 1951

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

NA

Amount

Sample



044 U 100 100 895 94414-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3931D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16581217


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165812

Prep Date

Leach Date

03202013 2222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3929D

20 mL

20 mL

E3930D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16581215

LCSD 280-16581216

Analysis Date

Prep Date

Leach Date

03202013 2147

03202013 2147

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA


Rec

107106 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03202013 2147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03202013 2147

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

535532500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3940D

10 mL

20 mL

E3941D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39875-D-2 MS

280-39875-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0105

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

03212013 0122

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

03212013 0105


Rec


82 26 25 - 141 103 20 F14-Dioxane






Sdg Number 13025120

Water

03212013 0105 03212013 0122



Method 8260B SIM

Preparation 5030B

Units ugL280-39875-D-2 MS 280-39875-D-2 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0105

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

NA

Amount

Sample



044 U 100 100 816 262 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4017D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1662795


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166279

Prep Date

Leach Date

03222013 1946

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4015D

20 mL

20 mL

E4016D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1662793

LCSD 280-1662794

Analysis Date

Prep Date

Leach Date

03222013 1911

03222013 1911

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA


Rec

103103 25 - 141 0 2014-Dioxane






Sdg Number 13025120

Water

03222013 1911


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03222013 1911

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

514516500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4027D

10 mL

20 mL

E4028D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39986-B-5 MS

280-39986-B-5 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 2249

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

03222013 2306

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

03222013 2249


Rec


146 225 25 - 141 17 20 E F E F14-Dioxane






Sdg Number 13025120

Water

03222013 2249 03222013 2306



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 2249

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

NA

Amount

Sample



27 100 100 419 499E F E F14-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0541 8260B SIM280-39873-5 T

WaterPIN12-0554A 8260B SIM280-39873-8 T






WaterPIN12-0539 8260B SIM280-39873-3 T

WaterPIN12-0540 8260B SIM280-39873-4 T



WaterPIN12-0542 8260B SIM280-39873-6 T

WaterPIN12-0549 8260B SIM280-39873-7 T

WaterPIN12-0554B 8260B SIM280-39873-9 T

WaterPIN12-0554C 8260B SIM280-39873-10 T

WaterPIN12-0585-3 8260B SIM280-39873-17 T






WaterPIN12-0525 8260B SIM280-39873-2 T



WaterPIN12-0581-1 8260B SIM280-39873-11 T

WaterPIN12-0581-2 8260B SIM280-39873-12 T

WaterPIN12-0582-1 8260B SIM280-39873-14 T

WaterPIN12-0582-3 8260B SIM280-39873-16 T

WaterPIN12-2451 8260B SIM280-39873-18 T



TestAmerica Denver

Page 137 of 1510





Sdg Number 13025120

Report

Basis

GCMS VOA




WaterPIN12-0524 8260B280-39873-1 T

WaterPIN12-0524 8260B280-39873-1DL T



WaterPIN12-0525 8260B280-39873-2 T

WaterPIN12-0539 8260B280-39873-3 T

WaterPIN12-0540 8260B280-39873-4 T

WaterPIN12-0541 8260B280-39873-5 T

WaterPIN12-0549 8260B280-39873-7 T

WaterPIN12-0554A 8260B280-39873-8 T

WaterPIN12-0554C 8260B280-39873-10 T

WaterPIN12-0554C 8260B280-39873-10DL T

WaterPIN12-0581-1 8260B280-39873-11 T

WaterPIN12-0581-3 8260B280-39873-13 T

WaterPIN12-0582-1 8260B280-39873-14 T

WaterPIN12-0582-2 8260B280-39873-15 T




WaterPIN12-0582-3 8260B280-39873-16 T

WaterPIN12-0585-3 8260B280-39873-17DL T

WaterPIN12-2451 8260B280-39873-18 T

WaterPIN12-2452 8260B280-39873-19 T

WaterPIN12-S71B 8260B280-39873-20 T

WaterPIN12-S71C 8260B280-39873-21 T

WaterPIN12-S73B 8260B280-39873-23 T

WaterPIN12-S73D 8260B280-39873-25 T

WaterPIN99-2448 8260B280-39873-26 T

Matrix Spike Water 8260B280-39974-C-1 MS T

Matrix Spike Duplicate Water 8260B280-39974-C-1 MSD T




WaterPIN12-0539 8260B280-39873-3DL T

WaterPIN12-0540 8260B280-39873-4DL T

WaterPIN12-0542 8260B280-39873-6 T

WaterPIN12-0554B 8260B280-39873-9 T

WaterPIN12-0581-2 8260B280-39873-12 T

WaterPIN12-0582-2 8260B280-39873-15DL T

Matrix Spike Water 8260B280-39875-B-1 MS T

Matrix Spike Duplicate Water 8260B280-39875-B-1 MSD T

TestAmerica Denver

Page 138 of 1510





Sdg Number 13025120

Report

Basis

GCMS VOA




WaterPIN12-0585-3 8260B280-39873-17 T

WaterPIN12-2452 8260B280-39873-19DL T

WaterPIN12-S71D 8260B280-39873-22 T

WaterPIN12-S73C 8260B280-39873-24 T

WaterPIN12-S73C 8260B280-39873-24DL T

Matrix Spike Water 8260B280-40045-A-1 MS T

Matrix Spike Duplicate Water 8260B280-40045-A-1 MSD T





WaterPIN12-0581-3 8260B SIM280-39873-13 T

WaterPIN12-0582-2 8260B SIM280-39873-15 T

Matrix Spike Water 8260B SIM280-39875-D-2 MS T

Matrix Spike Duplicate Water 8260B SIM280-39875-D-2 MSD T





WaterPIN12-0524 8260B SIM280-39873-1 T

WaterPIN12-2452 8260B SIM280-39873-19 T



Matrix Spike Water 8260B SIM280-39986-B-5 MS T

Matrix Spike Duplicate Water 8260B SIM280-39986-B-5 MSD T

Report Basis

T = Total

TestAmerica Denver

Page 139 of 1510

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 1167



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 10




QC Data Summary 85


Lab Chronicle 115



GCMS VOA 150




Page 2 of 1167










Page 3 of 1167

CASE NARRATIVE







calculated results








RECEIPT


ice The temperatures of the 2 coolers at receipt time were -03ordm C and 17ordm C


In some cases due to high concentrations of target analytes andor the nature of the sample matrix (foamy) samples had to be analyzed

using reduced aliquot sizes The reporting limits have been elevated accordingly To provide the lowest possible detection limits


Acetone a common laboratory contaminant was detected in the method blank associated with batch 280-165844 at a level that was

above the method detection limit but below the reporting limit The value should be considered an estimate and has been flagged ldquoJrdquo If

the associated samples reported a result above the MDL andor RL the result has been ldquoBrdquo flagged



Due to the nature of the sample matrix (foamy) the samples presented in this report had to be analyzed using reduced aliquot sizes The

reporting limits have been elevated accordingly

Due to the presence of interfering non-target analytes as well as the nature of the sample matrix (foamy) sample PIN12-0585-2 (LDU

886) had to be analyzed using a reduced aliquot size The reporting limit has been elevated accordingly

The internal standard response for 14-Dichlorobenzene-d4 was outside acceptance criteria for samples in batch 280-165111 As this

internal standard is not associated with the analyte of interest (14-Dioxane) data are reported as is

The MSD aliquot of the MSMSD associated with batch 280-164929 exhibited the percent recovery outside the control limits biased high

The LCS and LCSD were within control limits

The RPD limit was exceeded in the MSMSD performed on sample PIN12-0568-2 (LDU 868) in batch 280-165812 Method precision and

accuracy have been verified by the acceptable LCSLCSD analysis data


Page 4 of 1167




Sdg Number 13025120

GCMS VOA

Compound was found in the blank and sampleB





J



SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39875-1 PIN12-0568-1 Water 03112013 1456 03132013 0900

280-39875-1MS PIN12-0568-1 Water 03112013 1456 03132013 0900

280-39875-1MSD PIN12-0568-1 Water 03112013 1456 03132013 0900

280-39875-2 PIN12-0568-2 Water 03112013 1530 03132013 0900

280-39875-2MS PIN12-0568-2 Water 03112013 1530 03132013 0900

280-39875-2MSD PIN12-0568-2 Water 03112013 1530 03132013 0900

280-39875-3 PIN12-0569-1 Water 03082013 1305 03132013 0900

280-39875-4 PIN12-0569-2 Water 03082013 1355 03132013 0900

280-39875-5 PIN12-0569-3 Water 03082013 1445 03132013 0900

280-39875-6 PIN12-0570-1 Water 03082013 1535 03132013 0900

280-39875-7 PIN12-0572-1 Water 03112013 1313 03132013 0900

280-39875-8 PIN12-0572-2 Water 03112013 1350 03132013 0900

280-39875-9 PIN12-0574-1 Water 03112013 0908 03132013 0900

280-39875-10 PIN12-0574-2 Water 03112013 0958 03132013 0900

280-39875-11 PIN12-0574-3 Water 03112013 1050 03132013 0900

280-39875-12 PIN12-0584-1 Water 03092013 0820 03132013 0900

280-39875-13 PIN12-0584-2 Water 03092013 0850 03132013 0900

280-39875-14 PIN12-0584-3 Water 03092013 0955 03132013 0900

280-39875-15 PIN12-0585-1 Water 03092013 1055 03132013 0900

280-39875-16 PIN12-0585-2 Water 03092013 1135 03132013 0900

280-39875-17 PIN12-S30B Water 03082013 0930 03132013 0900

280-39875-18 PIN12-S33C Water 03082013 1036 03132013 0900

280-39875-19 PIN12-S35B Water 03082013 1130 03132013 0900

280-39875-20 PIN99-2199 Water 03082013 1200 03132013 0900

280-39875-21 PIN12-0568-3 Water 03112013 1605 03132013 0900

280-39875-22 PIN12-0570-2 Water 03112013 1652 03132013 0900




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39875-1 PIN12-0568-1


280-39875-4 PIN12-0569-2


20 ugL 8260B SIM16 J14-Dioxane

280-39875-5 PIN12-0569-3





280-39875-8 PIN12-0572-2





280-39875-9 PIN12-0574-1



280-39875-10 PIN12-0574-2





280-39875-11 PIN12-0574-3



280-39875-12 PIN12-0584-1


50 ugL 8260B152-Butanone (MEK)


50 ugL 8260B13 J4-Methyl-2-pentanone

10 ugL 8260B17Naphthalene




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39875-13 PIN12-0584-2


10 ugL 8260B055 JCarbon disulfide



50 ugL 8260B122-Hexanone


10 ugL 8260B020 JToluene

280-39875-14 PIN12-0584-3

20 ugL 8260B15 J BAcetone


280-39875-15 PIN12-0585-1






10 ugL 8260B53Trichloroethene


280-39875-16 PIN12-0585-2






280-39875-17 PIN12-S30B












Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39875-18 PIN12-S33C







280-39875-19 PIN12-S35B






280-39875-20 PIN99-2199



280-39875-21 PIN12-0568-3


280-39875-22 PIN12-0570-2




METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120



Ilczyszyn Dennis P DPISW846 8260B


TestAmerica Denver

Page 11 of 1167

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-1

Client Matrix

280-39875-1

Water




Dilution

03192013 1029

03192013 1029

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2015D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-1

Client Matrix

280-39875-1

Water




Dilution

03192013 1029

03192013 1029

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2015D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-2

Client Matrix

280-39875-2

Water




Dilution

03192013 1243

03192013 1243

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3121D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-2

Client Matrix

280-39875-2

Water




Dilution

03192013 1243

03192013 1243

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3121D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-1

Client Matrix

280-39875-3

Water




Dilution

03192013 1647

03192013 1647

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2031D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-1

Client Matrix

280-39875-3

Water




Dilution

03192013 1647

03192013 1647

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2031D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-2

Client Matrix

280-39875-4

Water




Dilution

03192013 1711

03192013 1711

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2032D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-2

Client Matrix

280-39875-4

Water




Dilution

03192013 1711

03192013 1711

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2032D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-3

Client Matrix

280-39875-5

Water




Dilution

03192013 0942

03192013 0942

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2013D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-3

Client Matrix

280-39875-5

Water




Dilution

03192013 0942

03192013 0942

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2013D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-1

Client Matrix

280-39875-6

Water




Dilution

03192013 1734

03192013 1734

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2033D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-1

Client Matrix

280-39875-6

Water




Dilution

03192013 1734

03192013 1734

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2033D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-1

Client Matrix

280-39875-7

Water




Dilution

03192013 1757

03192013 1757

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2034D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-1

Client Matrix

280-39875-7

Water




Dilution

03192013 1757

03192013 1757

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2034D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-2

Client Matrix

280-39875-8

Water




Dilution

03192013 1005

03192013 1005

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2014D

4 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


95 U 5095Acetone

080 U 50080Benzene






































85 U 25852-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-2

Client Matrix

280-39875-8

Water




Dilution

03192013 1005

03192013 1005

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2014D

4 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


085 U 50085Styrene




085 U 50085Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-1

Client Matrix

280-39875-9

Water




Dilution

03192013 1821

03192013 1821

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2035D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-1

Client Matrix

280-39875-9

Water




Dilution

03192013 1821

03192013 1821

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2035D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-2

Client Matrix

280-39875-10

Water




Dilution

03192013 1305

03192013 1305

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3122D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-2

Client Matrix

280-39875-10

Water




Dilution

03192013 1305

03192013 1305

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3122D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-3

Client Matrix

280-39875-11

Water




Dilution

03192013 1328

03192013 1328

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3123D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-3

Client Matrix

280-39875-11

Water




Dilution

03192013 1328

03192013 1328

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3123D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-1

Client Matrix

280-39875-12

Water




Dilution

03192013 1350

03192013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3124D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


200 1019Acetone

016 U 10016Benzene






15 50202-Butanone (MEK)
































32 J 50172-Hexanone




13 J 500984-Methyl-2-pentanone

17 10022Naphthalene



Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-1

Client Matrix

280-39875-12

Water




Dilution

03192013 1350

03192013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3124D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-2

Client Matrix

280-39875-13

Water




Dilution

03192013 1413

03192013 1413

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3125D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 U 1019Acetone

017 J 10016Benzene










055 J 10045Carbon disulfide




























12 50172-Hexanone





22 10022Naphthalene



Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-2

Client Matrix

280-39875-13

Water




Dilution

03192013 1413

03192013 1413

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3125D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




020 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-3

Client Matrix

280-39875-14

Water




Dilution

03202013 2309

03202013 2309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6668D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


15 J B 2038Acetone

032 U 20032Benzene






































34 U 10342-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-3

Client Matrix

280-39875-14

Water




Dilution

03202013 2309

03202013 2309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6668D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


034 U 20034Styrene




034 U 20034Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03212013 0017

03212013 0017

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6671D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


84 J B 1019Acetone

016 U 10016Benzene





































30 J 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03212013 0017

03212013 0017

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6671D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





017 U 10017Toluene





53 10016Trichloroethene














Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03212013 0037

03212013 0037

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6672D

10 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03212013 0058

03212013 0058

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6673D

2 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


19 U 10019Acetone

16 U 1016Benzene




19 U 1019Bromoform











16 U 1016Chloroform






















17 U 50172-Hexanone







17 U 1017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03212013 0058

03212013 0058

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6673D

2 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





17 U 1017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03212013 0119

03212013 0119

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6674D

02 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S30B

Client Matrix

280-39875-17

Water




Dilution

03212013 0140

03212013 0140

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6675D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


93 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S30B

Client Matrix

280-39875-17

Water




Dilution

03212013 0140

03212013 0140

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6675D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




029 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03212013 0221

03212013 0221

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6677D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


98 J B 2038Acetone

032 U 20032Benzene





































34 U 10342-Hexanone







034 U 20034Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03212013 0221

03212013 0221

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6677D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





034 U 20034Toluene

















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03212013 0241

03212013 0241

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6678D

1 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method











Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03212013 0302

03212013 0302

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6679D

02 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


190 U 1000190Acetone

16 U 10016Benzene




19 U 10019Bromoform

































170 U 5001702-Hexanone







17 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03212013 0302

03212013 0302

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6679D

02 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





17 U 10017Toluene

















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03212013 0322

03212013 0322

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6680D

002 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method











Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2199

Client Matrix

280-39875-20

Water




Dilution

03212013 0343

03212013 0343

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6681D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


51 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2199

Client Matrix

280-39875-20

Water




Dilution

03212013 0343

03212013 0343

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6681D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-3

Client Matrix

280-39875-21

Water




Dilution

03212013 0403

03212013 0403

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6682D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


70 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-3

Client Matrix

280-39875-21

Water




Dilution

03212013 0403

03212013 0403

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6682D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-2

Client Matrix

280-39875-22

Water




Dilution

03212013 0424

03212013 0424

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6683D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


58 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-2

Client Matrix

280-39875-22

Water




Dilution

03212013 0424

03212013 0424

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6683D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-1

Client Matrix

280-39875-1

Water




Dilution

03212013 0030

03212013 0030

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3938D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-2

Client Matrix

280-39875-2

Water




Dilution

03212013 0048

03212013 0048

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3939D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-1

Client Matrix

280-39875-3

Water




Dilution

03152013 0416

03152013 0416

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3798D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-2

Client Matrix

280-39875-4

Water




Dilution

03152013 0433

03152013 0433

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3799D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


16 J 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-3

Client Matrix

280-39875-5

Water




Dilution

03152013 0451

03152013 0451

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3800D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method






Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-1

Client Matrix

280-39875-6

Water




Dilution

03152013 0508

03152013 0508

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3801D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-1

Client Matrix

280-39875-7

Water




Dilution

03212013 0140

03212013 0140

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3942D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-2

Client Matrix

280-39875-8

Water




Dilution

03212013 0157

03212013 0157

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3943D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-1

Client Matrix

280-39875-9

Water




Dilution

03212013 0215

03212013 0215

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3944D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-2

Client Matrix

280-39875-10

Water




Dilution

03212013 0232

03212013 0232

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3945D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-3

Client Matrix

280-39875-11

Water




Dilution

03212013 0250

03212013 0250

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3946D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-1

Client Matrix

280-39875-12

Water




Dilution

03152013 0526

03152013 0526

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3802D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-2

Client Matrix

280-39875-13

Water




Dilution

03152013 0543

03152013 0543

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3803D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-3

Client Matrix

280-39875-14

Water




Dilution

03162013 0403

03162013 0403

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3843D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03162013 0236

03162013 0236

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3838D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03222013 0303

03222013 0303

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3979D

05 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


88 U 408814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S30B

Client Matrix

280-39875-17

Water




Dilution

03162013 0311

03162013 0311

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3840D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03162013 0328

03162013 0328

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3841D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03162013 0346

03162013 0346

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3842D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-3

Client Matrix

280-39875-21

Water




Dilution

03212013 0307

03212013 0307

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3947D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-2

Client Matrix

280-39875-22

Water




Dilution

03212013 0324

03212013 0324

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3948D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39875-1 PIN12-0568-1 81 71 93 89

280-39875-2 PIN12-0568-2 95 93 93 87

280-39875-3 PIN12-0569-1 85 75 91 86

280-39875-4 PIN12-0569-2 83 74 92 86

280-39875-5 PIN12-0569-3 85 74 96 95

280-39875-6 PIN12-0570-1 84 75 90 85

280-39875-7 PIN12-0572-1 82 74 92 87

280-39875-8 PIN12-0572-2 86 75 99 90

280-39875-9 PIN12-0574-1 85 76 95 89

280-39875-10 PIN12-0574-2 102 102 101 100

280-39875-11 PIN12-0574-3 99 102 92 89

280-39875-12 PIN12-0584-1 104 107 100 95

280-39875-13 PIN12-0584-2 98 108 89 87

280-39875-14 PIN12-0584-3 113 109 102 108

280-39875-15 PIN12-0585-1 111 111 98 107

280-39875-15 DL PIN12-0585-1 DL 113 114 100 114

280-39875-16 PIN12-0585-2 110 111 98 107

280-39875-16 DL PIN12-0585-2 DL 111 111 102 108

280-39875-17 PIN12-S30B 113 116 97 104

280-39875-18 PIN12-S33C 114 116 100 112

280-39875-18 DL PIN12-S33C DL 109 110 97 106

280-39875-19 PIN12-S35B 113 112 101 110

280-39875-19 DL PIN12-S35B DL 112 115 101 113

280-39875-20 PIN99-2199 113 113 98 112

280-39875-21 PIN12-0568-3 118 118 101 113

280-39875-22 PIN12-0570-2 116 119 100 111

MB 280-1654515 82 70 98 90

MB 280-1654645 95 91 98 92

MB 280-1658448 109 108 100 110






TestAmerica Denver

Page 81 of 1167



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

LCS 280-1654514 85 74 98 94

LCS 280-1654644 93 90 94 92

LCS 280-1658446 109 107 100 99

280-39875-1 MS PIN12-0568-1 MS 84 74 96 90

280-39875-14 MS PIN12-0584-3 MS 109 115 98 99

280-39826-B-10 MS 98 93 100 97

280-39875-1 MSD PIN12-0568-1 MSD 86 77 96 90

280-39875-14 MSD PIN12-0584-3 MSD 110 111 97 100

280-39826-B-10 MSD 93 90 92 89






TestAmerica Denver

Page 82 of 1167



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39875-1 PIN12-0568-1 99

280-39875-2 PIN12-0568-2 102

280-39875-3 PIN12-0569-1 103

280-39875-4 PIN12-0569-2 105

280-39875-5 PIN12-0569-3 103

280-39875-6 PIN12-0570-1 104

280-39875-7 PIN12-0572-1 101

280-39875-8 PIN12-0572-2 102

280-39875-9 PIN12-0574-1 114

280-39875-10 PIN12-0574-2 100

280-39875-11 PIN12-0574-3 98

280-39875-12 PIN12-0584-1 103

280-39875-13 PIN12-0584-2 122

280-39875-14 PIN12-0584-3 120

280-39875-15 PIN12-0585-1 118

280-39875-16 PIN12-0585-2 95

280-39875-17 PIN12-S30B 107

280-39875-18 PIN12-S33C 112

280-39875-19 PIN12-S35B 111

280-39875-21 PIN12-0568-3 97

280-39875-22 PIN12-0570-2 101

MB 280-16492917 99

MB 280-1651115 99

MB 280-16581217 96

MB 280-1660505 100

LCS 280-16492915 102

LCS 280-1651113 103

LCS 280-16581215 100

LCS 280-1660503 98



TestAmerica Denver

Page 83 of 1167



Sdg Number 13025120




Client Matrix Water


DCA

Rec

LCSD 280-16492916 97

LCSD 280-1651114 105

LCSD 280-16581216 96

LCSD 280-1660504 95

280-39875-2 MS PIN12-0568-2 MS 98

280-39873-C-4 MS 97

280-39873-A-2 MS 98

280-39997-D-2 MS 102

280-39875-2 MSD PIN12-0568-2 MSD 101

280-39873-C-4 MSD 100

280-39873-A-2 MSD 102

280-39997-D-2 MSD 101



TestAmerica Denver

Page 84 of 1167



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2010D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1654514


Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Prep Date

Leach Date

03192013 0805

NA


500 491 98 74 - 135Benzene




500 454 91 76 - 120Chloroform


500 453 91 75 - 13511-Dichloroethane


500 545 109 71 - 13611-Dichloroethene


500 499 100 72 - 120Ethylbenzene



500 483 97 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2016D

5 mL

20 mL

RR2017D

5 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39875-1

280-39875-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 1052

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

03192013 1116

NA

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

03192013 1052


Rec


91 89 74 - 135 2 20Benzene




87 84 76 - 120 5 20Chloroform


84 82 75 - 135 4 2111-Dichloroethane


101 96 71 - 136 4 2011-Dichloroethene


94 89 72 - 120 5 26Ethylbenzene



90 90 73 - 120 0 20Toluene





Toluene-d8 (Surr) 96 96 80 - 125






Sdg Number 13025120

Water

03192013 1052 03192013 1116



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 1052

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

NA

Amount

Sample



064 U 200 200 182 177Benzene




064 U 200 200 175 167Chloroform






064 U 200 200 187 179Ethylbenzene



068 U 200 200 180 179Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

G3113D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_GMB 280-1654645


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165464

Prep Date

Leach Date

03192013 0926

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

G3113D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_GMB 280-1654645


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165464

Prep Date

Leach Date

03192013 0926

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

G3112D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_GLCS 280-1654644


Analysis Batch

Prep Batch

Leach Batch

280-165464

NA

NA

Prep Date

Leach Date

03192013 0903

NA


500 474 95 74 - 135Benzene




500 451 90 76 - 120Chloroform


500 471 94 75 - 13511-Dichloroethane


500 547 109 71 - 13611-Dichloroethene


500 485 97 72 - 120Ethylbenzene



500 481 96 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

G3116D

01 mL

20 mL

G3117D

01 mL

20 mL

Method 8260B

Preparation 5030B

VMS_G

VMS_G

280-39826-B-10 MS

280-39826-B-10 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 1034

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165464

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 1056

03192013 1056

NA

Analysis Batch

Prep Batch

Leach Batch

280-165464

NA

NA

03192013 1034


Rec


97 97 74 - 135 1 20Benzene




93 92 76 - 120 1 20Chloroform


99 97 75 - 135 2 2111-Dichloroethane


108 109 71 - 136 1 2011-Dichloroethene


100 92 72 - 120 8 26Ethylbenzene



99 99 73 - 120 0 20Toluene





Toluene-d8 (Surr) 100 92 80 - 125






Sdg Number 13025120

Water

03192013 1034 03192013 1056



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 1034

NA

Analysis Date

Prep Date

Leach Date

03192013 1056

NA

Amount

Sample



39 J 1000 1000 1010 1010Benzene




38 J 1000 1000 967 961Chloroform






32 U 1000 1000 1000 925Ethylbenzene



34 U 1000 1000 993 994Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

P6667D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_PMB 280-1658448


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165844

Prep Date

Leach Date

03202013 2242

NA


293 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

P6667D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_PMB 280-1658448


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165844

Prep Date

Leach Date

03202013 2242

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

P6666D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_PLCS 280-1658446


Analysis Batch

Prep Batch

Leach Batch

280-165844

NA

NA

Prep Date

Leach Date

03202013 2222

NA


500 439 88 74 - 135Benzene




500 468 94 76 - 120Chloroform


500 444 89 75 - 13511-Dichloroethane


500 493 99 71 - 13611-Dichloroethene


500 449 90 72 - 120Ethylbenzene



500 451 90 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

P6669D

10 mL

20 mL

P6670D

10 mL

20 mL

Method 8260B

Preparation 5030B

VMS_P

VMS_P

280-39875-14

280-39875-14

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03202013 2335

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165844

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2356

03202013 2356

NA

Analysis Batch

Prep Batch

Leach Batch

280-165844

NA

NA

03202013 2335


Rec


93 90 74 - 135 3 20Benzene




98 97 76 - 120 2 20Chloroform


95 93 75 - 135 2 2111-Dichloroethane


109 106 71 - 136 3 2011-Dichloroethene


92 91 72 - 120 2 26Ethylbenzene



93 91 73 - 120 2 20Toluene





Toluene-d8 (Surr) 98 97 80 - 125






Sdg Number 13025120

Water

03202013 2335 03202013 2356



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03202013 2335

NA

Analysis Date

Prep Date

Leach Date

03202013 2356

NA

Amount

Sample



032 U 100 100 929 905Benzene




032 U 100 100 982 967Chloroform






032 U 100 100 925 911Ethylbenzene



034 U 100 100 929 912Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3783D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16492917


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164929

Prep Date

Leach Date

03142013 2354

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3781D

20 mL

20 mL

E3782D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16492915

LCSD 280-16492916

Analysis Date

Prep Date

Leach Date

03142013 2319

03142013 2319

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA


Rec

8980 25 - 141 10 2014-Dioxane






Sdg Number 13025120

Water

03142013 2319


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03142013 2319

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443400500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3787D

1 mL

20 mL

E3788D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-C-4 MS

280-39873-C-4 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0104

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

03152013 0121

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

03152013 0104


Rec


125 154 25 - 141 10 20 F14-Dioxane






Sdg Number 13025120

Water

03152013 0104 03152013 0121



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0104

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

NA

Amount

Sample



170 100 100 292 322 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3822D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1651115


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165111

Prep Date

Leach Date

03152013 1916

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3820D

20 mL

20 mL

E3821D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1651113

LCSD 280-1651114

Analysis Date

Prep Date

Leach Date

03152013 1841

03152013 1841

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA


Rec

8278 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1841


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03152013 1841

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

409391500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3824D

10 mL

20 mL

E3825D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-A-2 MS

280-39873-A-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 1951

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

03152013 2009

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

03152013 1951


Rec


89 94 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1951 03152013 2009



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 1951

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

NA

Amount

Sample



044 U 100 100 895 94414-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3931D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16581217


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165812

Prep Date

Leach Date

03202013 2222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3929D

20 mL

20 mL

E3930D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16581215

LCSD 280-16581216

Analysis Date

Prep Date

Leach Date

03202013 2147

03202013 2147

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA


Rec

107106 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03202013 2147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03202013 2147

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

535532500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3940D

10 mL

20 mL

E3941D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39875-2

280-39875-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0105

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

03212013 0122

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

03212013 0105


Rec


82 26 25 - 141 103 20 F14-Dioxane






Sdg Number 13025120

Water

03212013 0105 03212013 0122



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0105

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

NA

Amount

Sample



044 U 100 100 816 262 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3958D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1660505


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166050

Prep Date

Leach Date

03212013 2034

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3956D

20 mL

20 mL

E3957D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1660503

LCSD 280-1660504

Analysis Date

Prep Date

Leach Date

03212013 1959

03212013 1959

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA


Rec

9596 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03212013 1959


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03212013 1959

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

474479500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3981D

1 mL

20 mL

E3982D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39997-D-2 MS

280-39997-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 0338

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

03222013 0355

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

03222013 0338


Rec


113 107 25 - 141 6 2014-Dioxane






Sdg Number 13025120

Water

03222013 0338 03222013 0355



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 0338

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

NA

Amount

Sample



44 U 100 100 113 10714-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA







WaterPIN12-0569-1 8260B SIM280-39875-3 T

WaterPIN12-0569-2 8260B SIM280-39875-4 T

WaterPIN12-0569-3 8260B SIM280-39875-5 T

WaterPIN12-0570-1 8260B SIM280-39875-6 T

WaterPIN12-0584-1 8260B SIM280-39875-12 T

WaterPIN12-0584-2 8260B SIM280-39875-13 T







WaterPIN12-0584-3 8260B SIM280-39875-14 T

WaterPIN12-0585-1 8260B SIM280-39875-15 T







WaterPIN12-0568-1 8260B280-39875-1 T



WaterPIN12-0569-1 8260B280-39875-3 T

WaterPIN12-0569-2 8260B280-39875-4 T

WaterPIN12-0569-3 8260B280-39875-5 T

WaterPIN12-0570-1 8260B280-39875-6 T

WaterPIN12-0572-1 8260B280-39875-7 T

WaterPIN12-0572-2 8260B280-39875-8 T

WaterPIN12-0574-1 8260B280-39875-9 T

TestAmerica Denver

Page 112 of 1167





Sdg Number 13025120

Report

Basis

GCMS VOA






WaterPIN12-0568-2 8260B280-39875-2 T

WaterPIN12-0574-2 8260B280-39875-10 T

WaterPIN12-0574-3 8260B280-39875-11 T

WaterPIN12-0584-1 8260B280-39875-12 T

WaterPIN12-0584-2 8260B280-39875-13 T





WaterPIN12-0568-1 8260B SIM280-39875-1 T

WaterPIN12-0568-2 8260B SIM280-39875-2 T



WaterPIN12-0572-1 8260B SIM280-39875-7 T

WaterPIN12-0572-2 8260B SIM280-39875-8 T

WaterPIN12-0574-1 8260B SIM280-39875-9 T

WaterPIN12-0574-2 8260B SIM280-39875-10 T

WaterPIN12-0574-3 8260B SIM280-39875-11 T

WaterPIN12-0568-3 8260B SIM280-39875-21 T

WaterPIN12-0570-2 8260B SIM280-39875-22 T




WaterPIN12-0584-3 8260B280-39875-14 T



WaterPIN12-0585-1 8260B280-39875-15 T

WaterPIN12-0585-1 8260B280-39875-15DL T

WaterPIN12-0585-2 8260B280-39875-16 T

WaterPIN12-0585-2 8260B280-39875-16DL T

WaterPIN12-S30B 8260B280-39875-17 T

WaterPIN12-S33C 8260B280-39875-18 T

WaterPIN12-S33C 8260B280-39875-18DL T

WaterPIN12-S35B 8260B280-39875-19 T

WaterPIN12-S35B 8260B280-39875-19DL T

WaterPIN99-2199 8260B280-39875-20 T

WaterPIN12-0568-3 8260B280-39875-21 T

WaterPIN12-0570-2 8260B280-39875-22 T

TestAmerica Denver

Page 113 of 1167





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0585-2 8260B SIM280-39875-16 T



Report Basis

T = Total

TestAmerica Denver

Page 114 of 1167

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________

Approved for releaseKae E YoderProject Manager II3292013 906 AM









Page 1 of 764



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 9




QC Data Summary 67


Lab Chronicle 88



GCMS VOA 115




Page 2 of 764










Page 3 of 764

CASE NARRATIVE







calculated results








RECEIPT


ice The temperatures of the 2 coolers at receipt time were 19ordm C and 21ordm C

The chains-of-custody were not relinquished by TestAmericarsquos Tampa laboratory the forwarding laboratory The client was notified on

3182013


No anomalies were encountered


In some cases due to the nature of the sample matrix (foamy) samples had to be analyzed using reduced aliquot sizes The reporting


Due to high constituent concentration samples PIN12-0576-1 (LDU 920) and PIN12-0576-2 (LDU 921) had to be analyzed using reduced

aliquot sizes The reporting limits have been elevated accordingly

The MSMSD performed on sample PIN12-0576-2 (LDU 921) in batch 280-166279 exhibited percent recoveries outside the control limits

biased high It can be noted that the MS and MSD concentrations were present above the instrument calibration range The LCS and

LCSD were within control limits

The RPD limit was exceeded for 14-Dioxane in the MSMSD associated with batch 280-165812 The LCS and LCSD were within control

limits


Page 4 of 764




Sdg Number 13025120

GCMS VOA






J



SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39986-1 PIN12-0551-1 Water 03132013 1614 03152013 0930

280-39986-2 PIN12-0551-2 Water 03132013 1648 03152013 0930

280-39986-3 PIN12-0570-3 Water 03132013 1430 03152013 0930

280-39986-4 PIN12-0576-1 Water 03132013 1025 03152013 0930

280-39986-4MS PIN12-0576-1 Water 03132013 1025 03152013 0930

280-39986-4MSD PIN12-0576-1 Water 03132013 1025 03152013 0930

280-39986-5 PIN12-0576-2 Water 03132013 1057 03152013 0930

280-39986-5MS PIN12-0576-2 Water 03132013 1057 03152013 0930

280-39986-5MSD PIN12-0576-2 Water 03132013 1057 03152013 0930

280-39986-6 PIN12-0576-3 Water 03132013 1528 03152013 0930

280-39986-7 PIN12-0577-1 Water 03122013 1614 03152013 0930

280-39986-8 PIN12-0577-2 Water 03122013 1642 03152013 0930

280-39986-9 PIN12-0577-3 Water 03122013 1715 03152013 0930

280-39986-10 PIN12-0578-1 Water 03132013 0820 03152013 0930

280-39986-11 PIN12-0578-2 Water 03132013 0850 03152013 0930

280-39986-12 PIN12-0578-3 Water 03132013 0920 03152013 0930

280-39986-13 PIN12-0579-1 Water 03122013 1435 03152013 0930

280-39986-14 PIN12-0579-2 Water 03122013 1459 03152013 0930

280-39986-15 PIN12-0579-3 Water 03122013 1528 03152013 0930

280-39986-16 PIN99-2200 Water 03122013 1200 03152013 0930

280-39986-17 PIN12-2464 Water 03122013 0905 03152013 0930

280-39986-18 PIN12-2465 Water 03122013 0910 03152013 0930




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39986-1 PIN12-0551-1


280-39986-2 PIN12-0551-2


280-39986-3 PIN12-0570-3



280-39986-4 PIN12-0576-1









280-39986-5 PIN12-0576-2








280-39986-6 PIN12-0576-3




10 ugL 8260B80Toluene


280-39986-7 PIN12-0577-1





Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39986-8 PIN12-0577-2


280-39986-9 PIN12-0577-3



280-39986-10 PIN12-0578-1


280-39986-11 PIN12-0578-2


280-39986-12 PIN12-0578-3


280-39986-13 PIN12-0579-1


280-39986-14 PIN12-0579-2


280-39986-15 PIN12-0579-3



280-39986-16 PIN99-2200


280-39986-17 PIN12-2464



10 ugL 8260B037 JXylenes Total

280-39986-18 PIN12-2465



METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120

Tinkham Sarah A SATSW846 8260B



TestAmerica Denver

Page 10 of 764

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-1

Client Matrix

280-39986-1

Water




Dilution

03212013 1204

03212013 1204

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1999D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


16 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-1

Client Matrix

280-39986-1

Water




Dilution

03212013 1204

03212013 1204

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1999D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-2

Client Matrix

280-39986-2

Water




Dilution

03212013 1225

03212013 1225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2000D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


11 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-2

Client Matrix

280-39986-2

Water




Dilution

03212013 1225

03212013 1225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2000D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-3

Client Matrix

280-39986-3

Water




Dilution

03212013 1246

03212013 1246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2001D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


39 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-3

Client Matrix

280-39986-3

Water




Dilution

03212013 1246

03212013 1246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2001D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-1

Client Matrix

280-39986-4

Water




Dilution

03212013 1100

03212013 1100

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1996D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


25 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-1

Client Matrix

280-39986-4

Water




Dilution

03212013 1100

03212013 1100

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1996D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




026 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-2

Client Matrix

280-39986-5

Water




Dilution

03212013 1307

03212013 1307

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2002D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


23 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-2

Client Matrix

280-39986-5

Water




Dilution

03212013 1307

03212013 1307

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2002D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-3

Client Matrix

280-39986-6

Water




Dilution

03212013 1329

03212013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2003D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


95 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-3

Client Matrix

280-39986-6

Water




Dilution

03212013 1329

03212013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2003D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




80 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-1

Client Matrix

280-39986-7

Water




Dilution

03212013 1350

03212013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2004D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


63 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-1

Client Matrix

280-39986-7

Water




Dilution

03212013 1350

03212013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2004D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-2

Client Matrix

280-39986-8

Water




Dilution

03212013 1411

03212013 1411

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2005D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


25 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-2

Client Matrix

280-39986-8

Water




Dilution

03212013 1411

03212013 1411

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2005D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-3

Client Matrix

280-39986-9

Water




Dilution

03212013 1432

03212013 1432

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2006D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


50 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-3

Client Matrix

280-39986-9

Water




Dilution

03212013 1432

03212013 1432

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2006D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




029 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-1

Client Matrix

280-39986-10

Water




Dilution

03212013 1453

03212013 1453

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2007D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


29 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-1

Client Matrix

280-39986-10

Water




Dilution

03212013 1453

03212013 1453

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2007D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-2

Client Matrix

280-39986-11

Water




Dilution

03212013 1514

03212013 1514

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2008D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


14 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-2

Client Matrix

280-39986-11

Water




Dilution

03212013 1514

03212013 1514

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2008D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-3

Client Matrix

280-39986-12

Water




Dilution

03212013 1535

03212013 1535

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2009D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


11 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-3

Client Matrix

280-39986-12

Water




Dilution

03212013 1535

03212013 1535

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2009D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-1

Client Matrix

280-39986-13

Water




Dilution

03212013 1556

03212013 1556

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2010D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


13 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-1

Client Matrix

280-39986-13

Water




Dilution

03212013 1556

03212013 1556

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2010D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-2

Client Matrix

280-39986-14

Water




Dilution

03212013 1617

03212013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2011D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


15 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-2

Client Matrix

280-39986-14

Water




Dilution

03212013 1617

03212013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2011D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-3

Client Matrix

280-39986-15

Water




Dilution

03212013 1638

03212013 1638

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2012D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


24 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-3

Client Matrix

280-39986-15

Water




Dilution

03212013 1638

03212013 1638

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2012D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




49 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2200

Client Matrix

280-39986-16

Water




Dilution

03252013 2334

03252013 2334

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5545D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


96 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2200

Client Matrix

280-39986-16

Water




Dilution

03252013 2334

03252013 2334

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5545D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2464

Client Matrix

280-39986-17

Water




Dilution

03252013 2354

03252013 2354

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5546D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


52 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2464

Client Matrix

280-39986-17

Water




Dilution

03252013 2354

03252013 2354

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5546D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


017 U 10017Styrene




019 J 10017Toluene











037 J 10019Xylenes Total








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2465

Client Matrix

280-39986-18

Water




Dilution

03262013 0014

03262013 0014

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5547D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


20 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2465

Client Matrix

280-39986-18

Water




Dilution

03262013 0014

03262013 0014

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5547D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-1

Client Matrix

280-39986-1

Water




Dilution

03222013 2121

03222013 2121

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4022D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-2

Client Matrix

280-39986-2

Water




Dilution

03222013 2139

03222013 2139

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4023D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-3

Client Matrix

280-39986-3

Water




Dilution

03222013 2156

03222013 2156

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4024D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-1

Client Matrix

280-39986-4

Water




Dilution

03222013 2214

03222013 2214

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4025D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


36 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-2

Client Matrix

280-39986-5

Water




Dilution

03222013 2231

03222013 2231

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4026D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


27 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-3

Client Matrix

280-39986-6

Water




Dilution

03222013 2324

03222013 2324

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4029D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-1

Client Matrix

280-39986-7

Water




Dilution

03212013 0342

03212013 0342

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3949D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-2

Client Matrix

280-39986-8

Water




Dilution

03212013 0359

03212013 0359

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3950D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-3

Client Matrix

280-39986-9

Water




Dilution

03212013 0417

03212013 0417

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3951D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-1

Client Matrix

280-39986-10

Water




Dilution

03222013 0043

03222013 0043

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3971D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-2

Client Matrix

280-39986-11

Water




Dilution

03222013 0101

03222013 0101

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3972D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-3

Client Matrix

280-39986-12

Water




Dilution

03222013 0118

03222013 0118

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3973D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-1

Client Matrix

280-39986-13

Water




Dilution

03222013 0136

03222013 0136

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3974D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-2

Client Matrix

280-39986-14

Water




Dilution

03222013 0153

03222013 0153

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3975D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-3

Client Matrix

280-39986-15

Water




Dilution

03222013 0211

03222013 0211

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3976D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2464

Client Matrix

280-39986-17

Water




Dilution

03222013 0228

03222013 0228

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3977D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2465

Client Matrix

280-39986-18

Water




Dilution

03222013 0246

03222013 0246

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3978D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39986-1 PIN12-0551-1 94 96 104 101

280-39986-2 PIN12-0551-2 98 99 104 99

280-39986-3 PIN12-0570-3 100 101 104 100

280-39986-4 PIN12-0576-1 92 93 101 94

280-39986-5 PIN12-0576-2 101 100 103 99

280-39986-6 PIN12-0576-3 93 97 97 91

280-39986-7 PIN12-0577-1 102 104 104 97

280-39986-8 PIN12-0577-2 98 102 102 98

280-39986-9 PIN12-0577-3 102 105 103 101

280-39986-10 PIN12-0578-1 102 102 103 98

280-39986-11 PIN12-0578-2 99 102 100 97

280-39986-12 PIN12-0578-3 98 101 98 94

280-39986-13 PIN12-0579-1 101 103 95 96

280-39986-14 PIN12-0579-2 103 104 95 94

280-39986-15 PIN12-0579-3 99 102 91 93

280-39986-16 PIN99-2200 94 79 100 99

280-39986-17 PIN12-2464 92 78 82 93

280-39986-18 PIN12-2465 103 91 95 98

MB 280-1658586 95 95 102 96

MB 280-1665545 91 77 91 86

LCS 280-1658585 96 93 97 95

LCS 280-1665544 97 84 98 96

280-39986-4 MS PIN12-0576-1 MS 96 98 99 99

280-40133-C-1 MS 102 86 96 98

280-39986-4 MSD PIN12-0576-1 MSD 98 100 102 100

280-40133-C-1 MSD 92 79 94 93






TestAmerica Denver

Page 64 of 764



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39986-1 PIN12-0551-1 100

280-39986-2 PIN12-0551-2 112

280-39986-3 PIN12-0570-3 122

280-39986-4 PIN12-0576-1 118

280-39986-5 PIN12-0576-2 110

280-39986-6 PIN12-0576-3 103

280-39986-7 PIN12-0577-1 99

280-39986-8 PIN12-0577-2 98

280-39986-9 PIN12-0577-3 99

280-39986-10 PIN12-0578-1 102

280-39986-11 PIN12-0578-2 103

280-39986-12 PIN12-0578-3 100

280-39986-13 PIN12-0579-1 99

280-39986-14 PIN12-0579-2 99

280-39986-15 PIN12-0579-3 99

280-39986-17 PIN12-2464 98

280-39986-18 PIN12-2465 98

MB 280-16581217 96

MB 280-1660505 100

MB 280-1662795 93

LCS 280-16581215 100

LCS 280-1660503 98

LCS 280-1662793 97

LCSD 280-16581216 96

LCSD 280-1660504 95

LCSD 280-1662794 97

280-39986-5 MS PIN12-0576-2 MS 105

280-39875-D-2 MS 98

280-39997-D-2 MS 102



TestAmerica Denver

Page 65 of 764



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39986-5 MSD PIN12-0576-2 MSD 107

280-39875-D-2 MSD 101

280-39997-D-2 MSD 101



TestAmerica Denver

Page 66 of 764



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

MS1992D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_MS1MB 280-1658586


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165858

Prep Date

Leach Date

03212013 0924

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

MS1992D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_MS1MB 280-1658586


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165858

Prep Date

Leach Date

03212013 0924

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

MS1991D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_MS1LCS 280-1658585


Analysis Batch

Prep Batch

Leach Batch

280-165858

NA

NA

Prep Date

Leach Date

03212013 0903

NA


500 441 88 74 - 135Benzene




500 446 89 76 - 120Chloroform


500 445 89 75 - 13511-Dichloroethane


500 490 98 71 - 13611-Dichloroethene


500 455 91 72 - 120Ethylbenzene



500 446 89 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

MS1997D

20 mL

20 mL

MS1998D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_MS1

VMS_MS1

280-39986-4

280-39986-4

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 1121

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165858

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 1142

03212013 1142

NA

Analysis Batch

Prep Batch

Leach Batch

280-165858

NA

NA

03212013 1121


Rec


96 93 74 - 135 3 20Benzene




94 93 76 - 120 1 20Chloroform


103 94 75 - 135 2 2111-Dichloroethane


105 102 71 - 136 2 2011-Dichloroethene


97 96 72 - 120 1 26Ethylbenzene



93 92 73 - 120 1 20Toluene





Toluene-d8 (Surr) 99 102 80 - 125






Sdg Number 13025120

Water

03212013 1121 03212013 1142



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 1121

NA

Analysis Date

Prep Date

Leach Date

03212013 1142

NA

Amount

Sample



016 U 500 500 481 466Benzene




016 U 500 500 472 466Chloroform


15 500 500 203 19911-Dichloroethane

017 J 500 500 484 484trans-12-Dichloroethene



016 U 500 500 483 481Ethylbenzene



026 J 500 500 490 485Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5544D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1665545


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166554

Prep Date

Leach Date

03252013 2314

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5544D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1665545


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166554

Prep Date

Leach Date

03252013 2314

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

C5543D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CLCS 280-1665544


Analysis Batch

Prep Batch

Leach Batch

280-166554

NA

NA

Prep Date

Leach Date

03252013 2254

NA


500 525 105 74 - 135Benzene



500 510 102 76 - 135Chlorobenzene

500 499 100 76 - 120Chloroform


500 484 97 75 - 13511-Dichloroethane


500 626 125 71 - 13611-Dichloroethene


500 515 103 72 - 120Ethylbenzene



500 576 115 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5549D

20 mL

20 mL

C5550D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-40133-C-1 MS

280-40133-C-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03262013 0054

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166554

NA

NA

Analysis Date

Prep Date

Leach Date

03262013 0114

03262013 0114

NA

Analysis Batch

Prep Batch

Leach Batch

280-166554

NA

NA

03262013 0054


Rec


108 104 74 - 135 3 20Benzene



104 105 76 - 135 2 20Chlorobenzene

105 101 76 - 120 4 20Chloroform


102 96 75 - 135 5 2111-Dichloroethane


130 123 71 - 136 6 2011-Dichloroethene


103 103 72 - 120 0 26Ethylbenzene



117 115 73 - 120 2 20Toluene





Toluene-d8 (Surr) 96 94 80 - 125






Sdg Number 13025120

Water

03262013 0054 03262013 0114



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03262013 0054

NA

Analysis Date

Prep Date

Leach Date

03262013 0114

NA

Amount

Sample



016 U 500 500 538 521Benzene




016 U 500 500 525 507Chloroform






016 U 500 500 516 517Ethylbenzene


037 J 500 500 580 605Tetrachloroethene

017 U 500 500 586 575Toluene


16 500 500 672 669Trichloroethene




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3931D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16581217


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165812

Prep Date

Leach Date

03202013 2222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3929D

20 mL

20 mL

E3930D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16581215

LCSD 280-16581216

Analysis Date

Prep Date

Leach Date

03202013 2147

03202013 2147

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA


Rec

107106 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03202013 2147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03202013 2147

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

535532500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3940D

10 mL

20 mL

E3941D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39875-D-2 MS

280-39875-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0105

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

03212013 0122

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

03212013 0105


Rec


82 26 25 - 141 103 20 F14-Dioxane






Sdg Number 13025120

Water

03212013 0105 03212013 0122



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0105

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

NA

Amount

Sample



044 U 100 100 816 262 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3958D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1660505


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166050

Prep Date

Leach Date

03212013 2034

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3956D

20 mL

20 mL

E3957D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1660503

LCSD 280-1660504

Analysis Date

Prep Date

Leach Date

03212013 1959

03212013 1959

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA


Rec

9596 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03212013 1959


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03212013 1959

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

474479500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3981D

1 mL

20 mL

E3982D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39997-D-2 MS

280-39997-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 0338

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

03222013 0355

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

03222013 0338


Rec


113 107 25 - 141 6 2014-Dioxane






Sdg Number 13025120

Water

03222013 0338 03222013 0355



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 0338

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

NA

Amount

Sample



44 U 100 100 113 10714-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4017D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1662795


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166279

Prep Date

Leach Date

03222013 1946

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4015D

20 mL

20 mL

E4016D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1662793

LCSD 280-1662794

Analysis Date

Prep Date

Leach Date

03222013 1911

03222013 1911

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA


Rec

103103 25 - 141 0 2014-Dioxane






Sdg Number 13025120

Water

03222013 1911


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03222013 1911

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

514516500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4027D

10 mL

20 mL

E4028D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39986-5

280-39986-5

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 2249

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

03222013 2306

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

03222013 2249


Rec


146 225 25 - 141 17 20 E F E F14-Dioxane






Sdg Number 13025120

Water

03222013 2249 03222013 2306



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 2249

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

NA

Amount

Sample



27 100 100 419 499E F E F14-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA







WaterPIN12-0577-1 8260B SIM280-39986-7 T

WaterPIN12-0577-2 8260B SIM280-39986-8 T

WaterPIN12-0577-3 8260B SIM280-39986-9 T




WaterPIN12-0551-1 8260B280-39986-1 T

WaterPIN12-0551-2 8260B280-39986-2 T

WaterPIN12-0570-3 8260B280-39986-3 T

WaterPIN12-0576-1 8260B280-39986-4 T



WaterPIN12-0576-2 8260B280-39986-5 T

WaterPIN12-0576-3 8260B280-39986-6 T

WaterPIN12-0577-1 8260B280-39986-7 T

WaterPIN12-0577-2 8260B280-39986-8 T

WaterPIN12-0577-3 8260B280-39986-9 T

WaterPIN12-0578-1 8260B280-39986-10 T

WaterPIN12-0578-2 8260B280-39986-11 T

WaterPIN12-0578-3 8260B280-39986-12 T

WaterPIN12-0579-1 8260B280-39986-13 T

WaterPIN12-0579-2 8260B280-39986-14 T

WaterPIN12-0579-3 8260B280-39986-15 T





WaterPIN12-0578-1 8260B SIM280-39986-10 T

WaterPIN12-0578-2 8260B SIM280-39986-11 T

WaterPIN12-0578-3 8260B SIM280-39986-12 T

WaterPIN12-0579-1 8260B SIM280-39986-13 T

WaterPIN12-0579-2 8260B SIM280-39986-14 T

WaterPIN12-0579-3 8260B SIM280-39986-15 T

WaterPIN12-2464 8260B SIM280-39986-17 T

WaterPIN12-2465 8260B SIM280-39986-18 T



TestAmerica Denver

Page 86 of 764





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0551-1 8260B SIM280-39986-1 T

WaterPIN12-0551-2 8260B SIM280-39986-2 T

WaterPIN12-0570-3 8260B SIM280-39986-3 T

WaterPIN12-0576-1 8260B SIM280-39986-4 T

WaterPIN12-0576-2 8260B SIM280-39986-5 T



WaterPIN12-0576-3 8260B SIM280-39986-6 T




WaterPIN99-2200 8260B280-39986-16 T

WaterPIN12-2464 8260B280-39986-17 T

WaterPIN12-2465 8260B280-39986-18 T



Report Basis

T = Total

TestAmerica Denver

Page 87 of 764

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 1003



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 10




QC Data Summary 90


Lab Chronicle 119



GCMS VOA 148




Page 2 of 1003










Page 3 of 1003

CASE NARRATIVE







calculated results








RECEIPT




3182013


Due to high constituent concentration a reduced aliquot size had to be used for the analysis of cis-12-Dichloroethene and Vinyl chloride

in samples PIN12-0587-2 (LDU 902) PIN12-0587-3 (LDU 888) and PIN12-2454 (LDU 960) The reporting limits have been elevated

accordingly

Due to the nature of the sample matrix (foamy) samples PIN12-0588-1 (LDU 889) PIN12-S68C (LDU 933) and PIN12-S68D (DU 934)

had to be analyzed using reduced aliquot sizes The reporting limits have been elevated accordingly

The MS aliquot of the MSMSD performed on sample PIN12-0583-1 (LDU 881) in batch 280-165603 exhibited spike compound recoveries









Page 4 of 1003




Sdg Number 13025120

GCMS VOA






J


SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39997-1 PIN12-0583-1 Water 03122013 1400 03152013 0930

280-39997-1MS PIN12-0583-1 Water 03122013 1400 03152013 0930

280-39997-1MSD PIN12-0583-1 Water 03122013 1400 03152013 0930

280-39997-2 PIN12-0583-2 Water 03122013 1434 03152013 0930

280-39997-2MS PIN12-0583-2 Water 03122013 1434 03152013 0930

280-39997-2MSD PIN12-0583-2 Water 03122013 1434 03152013 0930

280-39997-3 PIN12-0583-3 Water 03122013 1512 03152013 0930

280-39997-4 PIN12-0586-1 Water 03132013 1054 03152013 0930

280-39997-5 PIN12-0586-2 Water 03132013 1125 03152013 0930

280-39997-6 PIN12-0586-3 Water 03132013 1342 03152013 0930

280-39997-7 PIN12-0587-1 Water 03132013 1440 03152013 0930

280-39997-8 PIN12-0587-2 Water 03132013 1508 03152013 0930

280-39997-9 PIN12-0587-3 Water 03132013 1644 03152013 0930

280-39997-10 PIN12-0588-1 Water 03142013 0900 03152013 0930

280-39997-11 PIN12-0588-2 Water 03142013 0933 03152013 0930

280-39997-12 PIN12-0588-3 Water 03142013 1007 03152013 0930

280-39997-13 PIN12-2453 Water 03122013 1200 03152013 0930

280-39997-14 PIN12-2454 Water 03132013 1446 03152013 0930

280-39997-15 PIN12-S68B Water 03132013 0856 03152013 0930

280-39997-16 PIN12-S68C Water 03132013 0931 03152013 0930

280-39997-17 PIN12-S68D Water 03132013 1004 03152013 0930

280-39997-18 PIN12-S69B Water 03122013 0906 03152013 0930

280-39997-19 PIN12-S69C Water 03122013 0933 03152013 0930

280-39997-20 PIN12-S69D Water 03122013 1013 03152013 0930

280-39997-21 PIN12-S70B Water 03122013 1110 03152013 0930

280-39997-22 PIN12-S70C Water 03122013 1157 03152013 0930

280-39997-23 PIN12-S70D Water 03122013 1303 03152013 0930

280-39997-24 PIN99-2449 Water 03122013 0845 03152013 0930




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39997-1 PIN12-0583-1




280-39997-2 PIN12-0583-2







280-39997-4 PIN12-0586-1



280-39997-5 PIN12-0586-2





280-39997-6 PIN12-0586-3






280-39997-7 PIN12-0587-1









Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39997-8 PIN12-0587-2







280-39997-9 PIN12-0587-3







280-39997-11 PIN12-0588-2






280-39997-12 PIN12-0588-3




280-39997-13 PIN12-2453





280-39997-14 PIN12-2454










Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39997-16 PIN12-S68C




280-39997-17 PIN12-S68D





280-39997-20 PIN12-S69D


280-39997-21 PIN12-S70B




280-39997-22 PIN12-S70C







280-39997-23 PIN12-S70D








METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120



TestAmerica Denver

Page 11 of 1003

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-1

Client Matrix

280-39997-1

Water




Dilution

03202013 0112

03202013 0112

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5428D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


77 J 1019Acetone

016 U 10016Benzene






































21 J 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-1

Client Matrix

280-39997-1

Water




Dilution

03202013 0112

03202013 0112

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5428D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




026 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-2

Client Matrix

280-39997-2

Water




Dilution

03202013 0212

03202013 0212

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5431D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


55 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-2

Client Matrix

280-39997-2

Water




Dilution

03202013 0212

03202013 0212

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5431D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




026 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-3

Client Matrix

280-39997-3

Water




Dilution

03202013 0246

03202013 0246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2054D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-3

Client Matrix

280-39997-3

Water




Dilution

03202013 0246

03202013 0246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2054D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-1

Client Matrix

280-39997-4

Water




Dilution

03202013 0232

03202013 0232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5432D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


39 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-1

Client Matrix

280-39997-4

Water




Dilution

03202013 0232

03202013 0232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5432D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-2

Client Matrix

280-39997-5

Water




Dilution

03202013 0252

03202013 0252

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5433D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


63 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-2

Client Matrix

280-39997-5

Water




Dilution

03202013 0252

03202013 0252

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5433D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-3

Client Matrix

280-39997-6

Water




Dilution

03202013 0312

03202013 0312

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5434D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


87 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-3

Client Matrix

280-39997-6

Water




Dilution

03202013 0312

03202013 0312

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5434D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-1

Client Matrix

280-39997-7

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5435D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


53 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-1

Client Matrix

280-39997-7

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5435D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03202013 0352

03202013 0352

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5436D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


82 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03202013 0352

03202013 0352

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5436D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method





027 J 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03212013 0400

03212013 0400

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2116D

4 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03202013 0412

03202013 0412

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5437D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


63 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03202013 0412

03202013 0412

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5437D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method





017 J 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03212013 0423

03212013 0423

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2117D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-1

Client Matrix

280-39997-10

Water




Dilution

03212013 0446

03212013 0446

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2118D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-1

Client Matrix

280-39997-10

Water




Dilution

03212013 0446

03212013 0446

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2118D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-2

Client Matrix

280-39997-11

Water




Dilution

03202013 0452

03202013 0452

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5439D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


44 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-2

Client Matrix

280-39997-11

Water




Dilution

03202013 0452

03202013 0452

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5439D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-3

Client Matrix

280-39997-12

Water




Dilution

03202013 0512

03202013 0512

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5440D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-3

Client Matrix

280-39997-12

Water




Dilution

03202013 0512

03202013 0512

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5440D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2453

Client Matrix

280-39997-13

Water




Dilution

03202013 0309

03202013 0309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2055D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2453

Client Matrix

280-39997-13

Water




Dilution

03202013 0309

03202013 0309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2055D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03202013 0532

03202013 0532

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5441D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


66 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03202013 0532

03202013 0532

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5441D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method





022 J 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03212013 0510

03212013 0510

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2119D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68B

Client Matrix

280-39997-15

Water




Dilution

03202013 0614

03202013 0614

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2063D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68B

Client Matrix

280-39997-15

Water




Dilution

03202013 0614

03202013 0614

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2063D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68C

Client Matrix

280-39997-16

Water




Dilution

03202013 0637

03202013 0637

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2064D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68C

Client Matrix

280-39997-16

Water




Dilution

03202013 0637

03202013 0637

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2064D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68D

Client Matrix

280-39997-17

Water




Dilution

03202013 0700

03202013 0700

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2065D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68D

Client Matrix

280-39997-17

Water




Dilution

03202013 0700

03202013 0700

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2065D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69B

Client Matrix

280-39997-18

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2056D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69B

Client Matrix

280-39997-18

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2056D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69C

Client Matrix

280-39997-19

Water




Dilution

03202013 0355

03202013 0355

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2057D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69C

Client Matrix

280-39997-19

Water




Dilution

03202013 0355

03202013 0355

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2057D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69D

Client Matrix

280-39997-20

Water




Dilution

03202013 0418

03202013 0418

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2058D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69D

Client Matrix

280-39997-20

Water




Dilution

03202013 0418

03202013 0418

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2058D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70B

Client Matrix

280-39997-21

Water




Dilution

03202013 0441

03202013 0441

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2059D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70B

Client Matrix

280-39997-21

Water




Dilution

03202013 0441

03202013 0441

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2059D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70C

Client Matrix

280-39997-22

Water




Dilution

03202013 0504

03202013 0504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2060D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70C

Client Matrix

280-39997-22

Water




Dilution

03202013 0504

03202013 0504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2060D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70D

Client Matrix

280-39997-23

Water




Dilution

03202013 0528

03202013 0528

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2061D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70D

Client Matrix

280-39997-23

Water




Dilution

03202013 0528

03202013 0528

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2061D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2449

Client Matrix

280-39997-24

Water




Dilution

03202013 0551

03202013 0551

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2062D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2449

Client Matrix

280-39997-24

Water




Dilution

03202013 0551

03202013 0551

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2062D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-1

Client Matrix

280-39997-1

Water




Dilution

03212013 2114

03212013 2114

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3959D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-2

Client Matrix

280-39997-2

Water




Dilution

03222013 0320

03222013 0320

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3980D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


44 U 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-3

Client Matrix

280-39997-3

Water




Dilution

03222013 0413

03222013 0413

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3983D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-1

Client Matrix

280-39997-4

Water




Dilution

03222013 2341

03222013 2341

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4030D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-2

Client Matrix

280-39997-5

Water




Dilution

03222013 2359

03222013 2359

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4031D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-3

Client Matrix

280-39997-6

Water




Dilution

03232013 0016

03232013 0016

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4032D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-1

Client Matrix

280-39997-7

Water




Dilution

03232013 0034

03232013 0034

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4033D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03232013 0051

03232013 0051

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4034D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03232013 0108

03232013 0108

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4035D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-1

Client Matrix

280-39997-10

Water




Dilution

03262013 0701

03262013 0701

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4109D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166553

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-2

Client Matrix

280-39997-11

Water




Dilution

03262013 0718

03262013 0718

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4110D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166553

NA

Analysis Method

Prep Method


66 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-3

Client Matrix

280-39997-12

Water




Dilution

03262013 0736

03262013 0736

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4111D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166553

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2453

Client Matrix

280-39997-13

Water




Dilution

03212013 2241

03212013 2241

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3964D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03232013 0126

03232013 0126

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4036D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68B

Client Matrix

280-39997-15

Water




Dilution

03232013 0143

03232013 0143

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4037D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68C

Client Matrix

280-39997-16

Water




Dilution

03232013 0201

03232013 0201

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4038D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


45 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68D

Client Matrix

280-39997-17

Water




Dilution

03232013 0218

03232013 0218

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4039D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


33 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69B

Client Matrix

280-39997-18

Water




Dilution

03222013 0430

03222013 0430

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3984D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69C

Client Matrix

280-39997-19

Water




Dilution

03222013 0447

03222013 0447

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3985D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69D

Client Matrix

280-39997-20

Water




Dilution

03222013 0505

03222013 0505

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3986D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70B

Client Matrix

280-39997-21

Water




Dilution

03212013 2351

03212013 2351

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3968D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70C

Client Matrix

280-39997-22

Water




Dilution

03222013 0008

03222013 0008

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3969D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


15 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70D

Client Matrix

280-39997-23

Water




Dilution

03222013 0026

03222013 0026

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3970D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


12 2004414-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39997-1 PIN12-0583-1 116 117 101 107

280-39997-2 PIN12-0583-2 103 103 88 92

280-39997-3 PIN12-0583-3 92 86 96 94

280-39997-4 PIN12-0586-1 118 117 90 104

280-39997-5 PIN12-0586-2 119 122 98 108

280-39997-6 PIN12-0586-3 102 100 86 93

280-39997-7 PIN12-0587-1 107 107 84 97

280-39997-8 PIN12-0587-2 106 107 87 95

280-39997-8 DL PIN12-0587-2 DL 88 84 93 92

280-39997-9 PIN12-0587-3 110 109 88 96

280-39997-9 DL PIN12-0587-3 DL 84 79 87 89

280-39997-10 PIN12-0588-1 92 87 93 97

280-39997-11 PIN12-0588-2 114 112 94 103

280-39997-12 PIN12-0588-3 118 116 96 102

280-39997-13 PIN12-2453 94 90 97 95

280-39997-14 PIN12-2454 107 108 81 91

280-39997-14 DL PIN12-2454 DL 92 88 96 98

280-39997-15 PIN12-S68B 90 82 97 94

280-39997-16 PIN12-S68C 86 80 91 90

280-39997-17 PIN12-S68D 91 84 92 91

280-39997-18 PIN12-S69B 92 86 92 91

280-39997-19 PIN12-S69C 86 78 91 94

280-39997-20 PIN12-S69D 86 78 90 90

280-39997-21 PIN12-S70B 86 77 92 91

280-39997-22 PIN12-S70C 99 94 104 104

280-39997-23 PIN12-S70D 92 87 96 94

280-39997-24 PIN99-2449 85 80 91 92

MB 280-1656035 106 104 91 101

MB 280-1656105 88 81 97 92






TestAmerica Denver

Page 86 of 1003



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

MB 280-1658425 91 90 93 95

LCS 280-1656034 106 102 95 94

LCS 280-1656104 88 83 93 91

LCS 280-1658424 82 81 87 88

280-39997-1 MS PIN12-0583-1 MS 103 107 82 81

280-39993-D-1 MS 105 100 96 92

280-39865-B-1 MS 87 81 99 96

280-39966-B-1 MS 91 89 96 98

280-39997-1 MSD PIN12-0583-1 MSD 117 123 95 95

280-39993-D-1 MSD 109 103 97 93

280-39865-B-1 MSD 83 77 90 90

280-39966-B-1 MSD 92 92 93 97






TestAmerica Denver

Page 87 of 1003



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39997-1 PIN12-0583-1 117

280-39997-2 PIN12-0583-2 98

280-39997-3 PIN12-0583-3 109

280-39997-4 PIN12-0586-1 101

280-39997-5 PIN12-0586-2 102

280-39997-6 PIN12-0586-3 102

280-39997-7 PIN12-0587-1 100

280-39997-8 PIN12-0587-2 103

280-39997-9 PIN12-0587-3 120

280-39997-10 PIN12-0588-1 99

280-39997-11 PIN12-0588-2 103

280-39997-12 PIN12-0588-3 108

280-39997-13 PIN12-2453 119

280-39997-14 PIN12-2454 105

280-39997-15 PIN12-S68B 102

280-39997-16 PIN12-S68C 107

280-39997-17 PIN12-S68D 100

280-39997-18 PIN12-S69B 96

280-39997-19 PIN12-S69C 95

280-39997-20 PIN12-S69D 97

280-39997-21 PIN12-S70B 102

280-39997-22 PIN12-S70C 103

280-39997-23 PIN12-S70D 103

MB 280-1660505 100

MB 280-1662795 93

MB 280-16655317 101

LCS 280-1660503 98

LCS 280-1662793 97

LCS 280-16655315 108



TestAmerica Denver

Page 88 of 1003



Sdg Number 13025120




Client Matrix Water


DCA

Rec

LCSD 280-1660504 95

LCSD 280-1662794 97

LCSD 280-16655316 102

280-39997-2 MS PIN12-0583-2 MS 102

280-39986-B-5 MS 105

280-40230-D-1 MS 95

280-39997-2 MSD PIN12-0583-2 MSD 101

280-39986-B-5 MSD 107

280-40230-D-1 MSD 101



TestAmerica Denver

Page 89 of 1003



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5415D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1656035


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165603

Prep Date

Leach Date

03192013 2050

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5415D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1656035


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165603

Prep Date

Leach Date

03192013 2050

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

C5414D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CLCS 280-1656034


Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

Prep Date

Leach Date

03192013 2030

NA


500 502 100 74 - 135Benzene




500 544 109 76 - 120Chloroform


500 505 101 75 - 13511-Dichloroethane


500 584 117 71 - 13611-Dichloroethene


500 470 94 72 - 120Ethylbenzene



500 529 106 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5418D

20 mL

20 mL

C5419D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-39993-D-1 MS

280-39993-D-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 2152

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 2212

03192013 2212

NA

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

03192013 2152


Rec


105 103 74 - 135 2 20Benzene




116 114 76 - 120 2 20Chloroform


107 108 75 - 135 1 2111-Dichloroethane


118 119 71 - 136 1 2011-Dichloroethene


99 97 72 - 120 1 26Ethylbenzene



112 109 73 - 120 3 20Toluene





Toluene-d8 (Surr) 96 97 80 - 125






Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5429D

20 mL

20 mL

C5430D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-39997-1

280-39997-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03202013 0132

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 0152

03202013 0152

NA

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

03202013 0132


Rec


106 100 74 - 135 6 20Benzene




126 117 76 - 120 8 20 FChloroform


114 107 75 - 135 7 2111-Dichloroethane


124 112 71 - 136 10 2011-Dichloroethene


93 88 72 - 120 6 26Ethylbenzene



108 106 73 - 120 2 20Toluene





Toluene-d8 (Surr) 82 95 80 - 125






Sdg Number 13025120

Water

03192013 2152 03192013 2212



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 2152

NA

Analysis Date

Prep Date

Leach Date

03192013 2212

NA

Amount

Sample



016 U 500 500 524 515Benzene




016 U 500 500 578 568Chloroform






016 U 500 500 493 486Ethylbenzene



025 J 500 500 585 569Toluene






Sdg Number 13025120

Water

03202013 0132 03202013 0152



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03202013 0132

NA

Analysis Date

Prep Date

Leach Date

03202013 0152

NA

Amount

Sample



016 U 500 500 531 500Benzene


019 U 500 500 709 659FCarbon tetrachloride


016 U 500 500 631 585FChloroform






016 U 500 500 467 440Ethylbenzene



026 J 500 500 569 556Toluene

016 U 500 500 711 657F111-Trichloroethane





Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2041D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1656105


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165610

Prep Date

Leach Date

03192013 2135

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2041D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1656105


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165610

Prep Date

Leach Date

03192013 2135

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2040D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1656104


Analysis Batch

Prep Batch

Leach Batch

280-165610

NA

NA

Prep Date

Leach Date

03192013 2112

NA


500 466 93 74 - 135Benzene




500 459 92 76 - 120Chloroform


500 455 91 75 - 13511-Dichloroethane


500 516 103 71 - 13611-Dichloroethene


500 452 90 72 - 120Ethylbenzene



500 473 95 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2045D

20 mL

20 mL

RR2046D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39865-B-1 MS

280-39865-B-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 2318

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165610

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 2341

03192013 2341

NA

Analysis Batch

Prep Batch

Leach Batch

280-165610

NA

NA

03192013 2318


Rec


87 82 74 - 135 6 20Benzene




89 84 76 - 120 6 20Chloroform


86 78 75 - 135 10 2111-Dichloroethane


97 91 71 - 136 6 2011-Dichloroethene


92 87 72 - 120 6 26Ethylbenzene



90 84 73 - 120 7 20Toluene





Toluene-d8 (Surr) 99 90 80 - 125






Sdg Number 13025120

Water

03192013 2318 03192013 2341



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 2318

NA

Analysis Date

Prep Date

Leach Date

03192013 2341

NA

Amount

Sample



016 U 500 500 434 408Benzene




016 U 500 500 447 421Chloroform






016 U 500 500 462 436Ethylbenzene



017 U 500 500 451 420Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2107D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1658425


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165842

Prep Date

Leach Date

03212013 0020

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2107D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1658425


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165842

Prep Date

Leach Date

03212013 0020

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2106D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1658424


Analysis Batch

Prep Batch

Leach Batch

280-165842

NA

NA

Prep Date

Leach Date

03202013 2356

NA


500 388 78 74 - 135Benzene




500 403 81 76 - 120Chloroform


500 392 78 75 - 13511-Dichloroethane


500 441 88 71 - 13611-Dichloroethene


500 413 83 72 - 120Ethylbenzene



500 410 82 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2109D

20 mL

20 mL

RR2110D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39966-B-1 MS

280-39966-B-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0118

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165842

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0141

03212013 0141

NA

Analysis Batch

Prep Batch

Leach Batch

280-165842

NA

NA

03212013 0118


Rec


88 85 74 - 135 3 20Benzene




89 89 76 - 120 0 20Chloroform


90 87 75 - 135 3 2111-Dichloroethane


102 95 71 - 136 7 2011-Dichloroethene


92 87 72 - 120 5 26Ethylbenzene



91 89 73 - 120 2 20Toluene





Toluene-d8 (Surr) 96 93 80 - 125






Sdg Number 13025120

Water

03212013 0118 03212013 0141



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0118

NA

Analysis Date

Prep Date

Leach Date

03212013 0141

NA

Amount

Sample



016 U 500 500 440 427Benzene




016 U 500 500 444 445Chloroform






016 U 500 500 459 436Ethylbenzene



017 U 500 500 455 447Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3958D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1660505


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166050

Prep Date

Leach Date

03212013 2034

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3956D

20 mL

20 mL

E3957D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1660503

LCSD 280-1660504

Analysis Date

Prep Date

Leach Date

03212013 1959

03212013 1959

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA


Rec

9596 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03212013 1959


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03212013 1959

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

474479500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3981D

1 mL

20 mL

E3982D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39997-2

280-39997-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 0338

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

03222013 0355

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

03222013 0338


Rec


113 107 25 - 141 6 2014-Dioxane






Sdg Number 13025120

Water

03222013 0338 03222013 0355



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 0338

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

NA

Amount

Sample



44 U 100 100 113 10714-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4017D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1662795


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166279

Prep Date

Leach Date

03222013 1946

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4015D

20 mL

20 mL

E4016D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1662793

LCSD 280-1662794

Analysis Date

Prep Date

Leach Date

03222013 1911

03222013 1911

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA


Rec

103103 25 - 141 0 2014-Dioxane






Sdg Number 13025120

Water

03222013 1911


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03222013 1911

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

514516500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4027D

10 mL

20 mL

E4028D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39986-B-5 MS

280-39986-B-5 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 2249

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

03222013 2306

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

03222013 2249


Rec


146 225 25 - 141 17 20 E F E F14-Dioxane






Sdg Number 13025120

Water

03222013 2249 03222013 2306



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 2249

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

NA

Amount

Sample



27 100 100 419 499E F E F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4093D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16655317


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166553

Prep Date

Leach Date

03262013 0222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4091D

20 mL

20 mL

E4092D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16655315

LCSD 280-16655316

Analysis Date

Prep Date

Leach Date

03262013 0147

03262013 0147

NA

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA

Analysis Date

Prep Date

Leach Date

03262013 0204

03262013 0204

NA

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA


Rec

103107 25 - 141 4 2014-Dioxane






Sdg Number 13025120

Water

03262013 0147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03262013 0147

Analysis Date

Prep Date

Leach Date

03262013 0204

03262013 0204

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

516537500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4101D

10 mL

20 mL

E4102D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-40230-D-1 MS

280-40230-D-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03262013 0442

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA

Analysis Date

Prep Date

Leach Date

03262013 0459

03262013 0459

NA

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA

03262013 0442


Rec


104 120 25 - 141 7 2014-Dioxane






Sdg Number 13025120

Water

03262013 0442 03262013 0459



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03262013 0442

NA

Analysis Date

Prep Date

Leach Date

03262013 0459

NA

Amount

Sample



12 100 100 222 23814-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA




Matrix Spike Water 8260B280-39993-D-1 MS T

Matrix Spike Duplicate Water 8260B280-39993-D-1 MSD T

WaterPIN12-0583-1 8260B280-39997-1 T



WaterPIN12-0583-2 8260B280-39997-2 T

WaterPIN12-0586-1 8260B280-39997-4 T

WaterPIN12-0586-2 8260B280-39997-5 T

WaterPIN12-0586-3 8260B280-39997-6 T

WaterPIN12-0587-1 8260B280-39997-7 T

WaterPIN12-0587-2 8260B280-39997-8 T

WaterPIN12-0587-3 8260B280-39997-9 T

WaterPIN12-0588-2 8260B280-39997-11 T

WaterPIN12-0588-3 8260B280-39997-12 T

WaterPIN12-2454 8260B280-39997-14 T






WaterPIN12-0583-3 8260B280-39997-3 T

WaterPIN12-2453 8260B280-39997-13 T

WaterPIN12-S68B 8260B280-39997-15 T

WaterPIN12-S68C 8260B280-39997-16 T

WaterPIN12-S68D 8260B280-39997-17 T

WaterPIN12-S69B 8260B280-39997-18 T

WaterPIN12-S69C 8260B280-39997-19 T

WaterPIN12-S69D 8260B280-39997-20 T

WaterPIN12-S70B 8260B280-39997-21 T

WaterPIN12-S70C 8260B280-39997-22 T

WaterPIN12-S70D 8260B280-39997-23 T

WaterPIN99-2449 8260B280-39997-24 T






WaterPIN12-0587-2 8260B280-39997-8DL T

WaterPIN12-0587-3 8260B280-39997-9DL T

WaterPIN12-0588-1 8260B280-39997-10 T

WaterPIN12-2454 8260B280-39997-14DL T

TestAmerica Denver

Page 116 of 1003





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0583-1 8260B SIM280-39997-1 T

WaterPIN12-0583-2 8260B SIM280-39997-2 T



WaterPIN12-0583-3 8260B SIM280-39997-3 T

WaterPIN12-2453 8260B SIM280-39997-13 T













WaterPIN12-0586-1 8260B SIM280-39997-4 T

WaterPIN12-0586-2 8260B SIM280-39997-5 T

WaterPIN12-0586-3 8260B SIM280-39997-6 T

WaterPIN12-0587-1 8260B SIM280-39997-7 T

WaterPIN12-0587-2 8260B SIM280-39997-8 T

WaterPIN12-0587-3 8260B SIM280-39997-9 T

WaterPIN12-2454 8260B SIM280-39997-14 T








WaterPIN12-0588-1 8260B SIM280-39997-10 T

WaterPIN12-0588-2 8260B SIM280-39997-11 T

WaterPIN12-0588-3 8260B SIM280-39997-12 T



TestAmerica Denver

Page 117 of 1003





Sdg Number 13025120

Report

Basis

Report Basis

T = Total

TestAmerica Denver

Page 118 of 1003

ANALYTICAL REPORT


SDG Number 13045231





_____________________________________________










Page 1 of 304



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 8




QC Data Summary 24


Lab Chronicle 33



GCMS VOA 42




Page 2 of 304










Page 3 of 304

CASE NARRATIVE







calculated results








RECEIPT


The temperature of the cooler at receipt was 02ordm C


The MSMSD performed on sample PIN12-0561-1 (LFZ 335) exhibited RPD data outside the control limits for 12-Dichloropropane and

Methylene Chloride The acceptable LCS analysis data indicated that the analytical system was operating within control therefore

corrective action is deemed unnecessary



Due to the sample matrix being excessively foamy reduced aliquot sizes had to be used for the analysis of samples PIN12-0561-2 (LFZ

336) and PIN12-0561-3 (LFZ 337) The reporting limits have been elevated accordingly


Page 4 of 304




Sdg Number 13045231

GCMS VOA




SAMPLE SUMMARY


Sdg Number 13045231


DateTime DateTime

280-40744-1 PIN12-0561-1 Water 04042013 1020 04052013 1428

280-40744-1MS PIN12-0561-1 Water 04042013 1020 04052013 1428

280-40744-1MSD PIN12-0561-1 Water 04042013 1020 04052013 1428

280-40744-2 PIN12-0561-2 Water 04042013 1103 04052013 1428

280-40744-3 PIN12-0561-3 Water 04042013 1329 04052013 1428

280-40744-4 PIN12-2474 Water 04042013 0800 04052013 1428




Analyte Result

Reporting

Limit Units Method


Sdg Number 13045231

Qualifier

No Detections


METHOD SUMMARY


Sdg Number 13045231


Matrix Water





Lab References


Method References






Sdg Number 13045231



TestAmerica Denver

Page 9 of 304

Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-1

Client Matrix

280-40744-1

Water




Dilution

04062013 0537

04062013 0537

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2748D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-1

Client Matrix

280-40744-1

Water




Dilution

04062013 0537

04062013 0537

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2748D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-2

Client Matrix

280-40744-2

Water




Dilution

04062013 0102

04062013 0102

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2736D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-2

Client Matrix

280-40744-2

Water




Dilution

04062013 0102

04062013 0102

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2736D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-3

Client Matrix

280-40744-3

Water




Dilution

04062013 0125

04062013 0125

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2737D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-3

Client Matrix

280-40744-3

Water




Dilution

04062013 0125

04062013 0125

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2737D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-2474

Client Matrix

280-40744-4

Water




Dilution

04062013 0149

04062013 0149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2738D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-2474

Client Matrix

280-40744-4

Water




Dilution

04062013 0149

04062013 0149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2738D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-1

Client Matrix

280-40744-1

Water




Dilution

04052013 2302

04052013 2302

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4268D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-2

Client Matrix

280-40744-2

Water




Dilution

04052013 2354

04052013 2354

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4271D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-3

Client Matrix

280-40744-3

Water




Dilution

04062013 0011

04062013 0011

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4272D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-2474

Client Matrix

280-40744-4

Water




Dilution

04062013 0029

04062013 0029

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4273D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane






Sdg Number 13045231




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-40744-1 PIN12-0561-1 99 90 98 93

280-40744-2 PIN12-0561-2 96 90 96 89

280-40744-3 PIN12-0561-3 107 102 101 97

280-40744-4 PIN12-2474 102 94 103 98

MB 280-1682887 106 103 102 95

LCS 280-1682886 107 105 99 96

280-40744-1 MS PIN12-0561-1 MS 101 94 96 91

280-40744-1 MSD PIN12-0561-1 MSD 106 99 102 98






TestAmerica Denver

Page 22 of 304



Sdg Number 13045231




Client Matrix Water


DCA

Rec

280-40744-1 PIN12-0561-1 113

280-40744-2 PIN12-0561-2 113

280-40744-3 PIN12-0561-3 107

280-40744-4 PIN12-2474 108

MB 280-1682865 115

LCS 280-1682863 114

LCSD 280-1682864 113

280-40744-1 MS PIN12-0561-1 MS 110

280-40744-1 MSD PIN12-0561-1 MSD 114



TestAmerica Denver

Page 23 of 304



Sdg Number 13045231

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2731D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1682887


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-168288

Prep Date

Leach Date

04052013 2307

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13045231

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2731D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1682887


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-168288

Prep Date

Leach Date

04052013 2307

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13045231

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2730D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1682886


Analysis Batch

Prep Batch

Leach Batch

280-168288

NA

NA

Prep Date

Leach Date

04052013 2244

NA


500 507 101 74 - 135Benzene




500 538 108 76 - 120Chloroform


500 517 103 75 - 13511-Dichloroethane


500 595 119 71 - 13611-Dichloroethene


500 540 108 72 - 120Ethylbenzene



500 535 107 73 - 120Toluene











Sdg Number 13045231

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2734D

20 mL

20 mL

RR2735D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-40744-1

280-40744-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


04062013 0016

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-168288

NA

NA

Analysis Date

Prep Date

Leach Date

04062013 0039

04062013 0039

NA

Analysis Batch

Prep Batch

Leach Batch

280-168288

NA

NA

04062013 0016


Rec


98 113 74 - 135 14 20Benzene



92 107 76 - 135 15 20Chlorobenzene

100 116 76 - 120 15 20Chloroform


101 116 75 - 135 14 2111-Dichloroethane


113 121 71 - 136 7 2011-Dichloroethene

95 119 71 - 120 22 20 F12-Dichloropropane

102 117 72 - 120 14 26Ethylbenzene

71 92 54 - 141 26 20 FMethylene Chloride


99 116 73 - 120 16 20Toluene





Toluene-d8 (Surr) 96 102 80 - 125






Sdg Number 13045231

Water

04062013 0016 04062013 0039



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

04062013 0016

NA

Analysis Date

Prep Date

Leach Date

04062013 0039

NA

Amount

Sample



016 U 500 500 491 564Benzene




016 U 500 500 498 580Chloroform





018 U 500 500 477 597 F12-Dichloropropane

016 U 500 500 510 585Ethylbenzene

032 U 500 500 355 461 FMethylene Chloride


017 U 500 500 497 582Toluene






Sdg Number 13045231

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4263D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1682865


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-168286

Prep Date

Leach Date

04052013 2134

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4261D

20 mL

20 mL

E4262D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1682863

LCSD 280-1682864

Analysis Date

Prep Date

Leach Date

04052013 2059

04052013 2059

NA

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA

Analysis Date

Prep Date

Leach Date

04052013 2117

04052013 2117

NA

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA


Rec

9093 25 - 141 4 2014-Dioxane






Sdg Number 13045231

Water

04052013 2059


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

04052013 2059

Analysis Date

Prep Date

Leach Date

04052013 2117

04052013 2117

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

448466500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4269D

20 mL

20 mL

E4270D

20 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-40744-1

280-40744-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


04052013 2319

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA

Analysis Date

Prep Date

Leach Date

04052013 2337

04052013 2337

NA

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA

04052013 2319


Rec


79 85 25 - 141 8 2014-Dioxane






Sdg Number 13045231

Water

04052013 2319 04052013 2337



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

04052013 2319

NA

Analysis Date

Prep Date

Leach Date

04052013 2337

NA

Amount

Sample



022 U 500 500 394 42514-Dioxane






Sdg Number 13045231

Report

Basis

GCMS VOA





WaterPIN12-0561-1 8260B SIM280-40744-1 T



WaterPIN12-0561-2 8260B SIM280-40744-2 T

WaterPIN12-0561-3 8260B SIM280-40744-3 T

WaterPIN12-2474 8260B SIM280-40744-4 T




WaterPIN12-0561-1 8260B280-40744-1 T



WaterPIN12-0561-2 8260B280-40744-2 T

WaterPIN12-0561-3 8260B280-40744-3 T

WaterPIN12-2474 8260B280-40744-4 T

Report Basis

T = Total

TestAmerica Denver

Page 32 of 304

Sitewide Environmental Monitoring Semiannual Progress Report for the Young - Rainey STAR Center December 2012 Through May 2013

Contents

Abbreviations

10 Introduction

11 Building 100 Area

12 Northeast Site

13 WWNA

14 Site Update

15 Waste Minimization

20 Water-Level Elevations

21 Groundwater Flow

30 Groundwater Sampling

31 Work Performed

32 Quality AssuranceQuality Control

40 Plume Stability Monitoring

50 Upcoming Tasks

60 References

Figures





















Tables




Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 (Reported in μgL)

Table 5 COPC Concentrations at the Building 100 Area (μgL)


Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-section

Plates

Plate 1 Sitewide Shallow Surficial Aquifer Contours Pinellas Florida March 2013

Plate 2 Sitewide Deep Surficial Aquifer Contours Pinellas Florida March 2013

Appendix

Appendix A Laboratory Reports March 2013 Semiannual Monitoring







US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page i

Contents Abbreviations iii 10 Introduction 1

11 Building 100 Area 2 12 Northeast Site 5 13 WWNA 7 14 Site Update 9 15 Waste Minimization 9

20 Water-Level Elevations 9 21 Groundwater Flow 9

30 Groundwater Sampling 10 31 Work Performed 10 32 Quality AssuranceQuality Control 11

40 Plume Stability Monitoring 12 50 Upcoming Tasks 13 60 References 13

Figures Figure 1 Young - Rainey STAR Center Location 16 Figure 2 Location of STAR Center Solid-Waste Management Units (SWMUs) 17 Figure 3 Building 100 Area Shallow Surficial Aquifer Flow March 2013 18 Figure 4 Building 100 Area Deep Surficial Aquifer Flow March 2013 19 Figure 5 Building 100 Area TCOPCs Concentrations March 2013 20 Figure 6 Building 100 Area South TCOPCs Concentrations March 2013 21 Figure 7 Building 100 Area TCE Concentrations March 2013 22 Figure 8 Building 100 Area cDCE Concentrations March 2013 23 Figure 9 Building 100 Area South cDCE Concentrations March 2013 24 Figure 10 Building 100 Area VC Concentrations March 2013 25 Figure 11 Building 100 Area South VC Concentrations March 2013 26 Figure 12 Building 100 Area 14-dioxane Concentrations March 2013 27 Figure 13 Building 100 Area South 14-dioxane Concentrations March 2013 28 Figure 14 Building 100 Area Plume Stability Monitoring Cross-Sections 29 Figure 15 Cross-Section E1-E2 30 Figure 16 Cross-Section E3-E4 31 Figure 17 Cross-Section E5-E6 32 Figure 18 Cross-Section S1-E2 33 Figure 19 Cross-Section S2-S3 34 Figure 20 Cross-Section S4-S5 35

Tables Table 1 Groundwater-Level Data at the STAR Center March 2013 36 Table 2 Surface Water Elevations March 2013 41

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page ii

Table 3 Field Measurements of Samples Collected at the STAR Center March 2013 42 Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 45 Table 5 COPC Concentrations at the Building 100 Area 46 Table 6 Sum of COPCs for Each Plume Stability Monitoring Cross-Section 49 Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-section 50

Plates Plate 1 Sitewide Shallow Surficial Aquifer Contours Pinellas Florida March 2013 Plate 2 Sitewide Deep Surficial Aquifer Contours Pinellas Florida March 2013

Appendix Appendix A Laboratory Reports March 2013 Semiannual Monitoring

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page iii

Abbreviations cDCE cis-12-dichloroethene

CMIP Corrective Measures Implementation Plan

CMS Corrective Measures Study

CMT continuous multichannel tubing

COPC contaminant of potential concern

CTL cleanup target level

11-DCE 11-dichloroethene

DOE US Department of Energy

EPA US Environmental Protection Agency

FAC Florida Administrative Code

FDEP Florida Department of Environmental Protection

ft feet (foot)

HSWA Hazardous and Solid Waste Amendments

IC Institutional Control

IWNF industrial wastewater neutralization facility

LDA large-diameter auger

LM Office of Legacy Management

MCL maximum contaminant level

μgL micrograms per liter

NAPL nonaqueous phase liquid

POTW Publicly Owned Treatment Works

QAQC quality assurancequality control

RBCA Risk-Based Corrective Action

RCRA Resource Conservation and Recovery Act

RFA RCRA Facility Assessment

RPD relative percent difference

SEEPro Site Environmental Evaluation for Projects

STAR Center Young - Rainey Science Technology and Research Center

SWMU solid-waste management unit

TCE trichloroethene

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796 Page iv

TCOPCs total contaminants of potential concern

tDCE trans-12-dichloroethene

VC vinyl chloride

WWNA Wastewater Neutralization AreaBuilding 200 Area


10 Introduction The Young - Rainey Science Technology and Research Center (STAR Center) at the Pinellas County Florida Site is a former US Department of Energy (DOE) facility constructed in the mid-1950s The 99-acre STAR Center is located in Largo Florida and lies in the northeast quarter of Section 13 Township 30 South Range 15 East (Figure 1) While it was owned by DOE the facility primarily manufactured neutron generators for nuclear weapons Other products manufactured at the STAR Center have included radioisotope-powered thermoelectric generators thermal batteries specialty capacitors crystal resonators neutron detectors lightning-arrestor connectors and vacuum-switch tubes In 1987 the US Environmental Protection Agency (EPA) performed a Resource Conservation and Recovery Act (RCRA) Facility Assessment (RFA) (EPA 1988) at the site to gather information on potential releases of hazardous materials In February of 1990 EPA issued a Hazardous and Solid Waste Amendments (HSWA) permit to DOE enabling DOE to investigate and perform remediation activities in those areas designated as solid-waste management units (SWMUs) contaminated by hazardous materials resulting from DOE operations On March 17 1995 DOE sold the facility to the Pinellas County Industrial Council The sales contract included clauses to ensure continued compliance with federal state and local regulations while DOE remediates the site On July 1 1999 the Pinellas County Industrial Council was disestablished and ownership of the STAR Center changed to the Pinellas County Industrial Development Authority In November 2000 the State of Florida received HSWA authorization from EPA The Florida Department of Environmental Protection (FDEP) issued a new HSWA permit to DOE in January 2002 The permit was reissued on August 21 2007 and was modified under the provisions of Section 403722 Florida Statutes and Chapters 62-4 62-160 62-730 62-777 and 62-780 Florida Administrative Code (FAC) to incorporate the Global Risk-Based Corrective Action (RBCA) regulations The permit was revised and reissued again on January 9 2012 The administration of DOE activities at the facility is the responsibility of the DOE Office of Legacy Management (LM) in Grand Junction Colorado SM Stoller Corporation a prime contractor to LM provides technical support to DOE for remediation and closure of all active SWMUs onsite The EPA RFA Report and the HSWA permit identified 15 sites at the former DOE facility that might have environmental contamination as a result of past activities Upon completion of the RCRA Facility Investigation (DOE 1991a) 11 of the 15 SWMUs were recommended by DOE and approved by EPA Region 4 and FDEP for no further action (DOE 1994) A twelfth site the Former Pistol Range Site was remediated in 1993 it was recommended by DOE and approved by EPA Region 4 and FDEP for no further action Two additional SWMUs the West Fenceline Site and the Wastewater Neutralization Area Building 200 Area (WWNA) were identified after the HSWA permit was issued bringing the total to 17 SWMUs that have been identified and investigated at the STAR Center The remediation of the West Fenceline Site was completed in 1997 and DOE recommendedand EPA Region 4 and FDEP approvedno further action for a total of 13 SWMUs remediated A Corrective Measures Study (CMS)Corrective Measures Implementation Plan (CMIP) was

US Department of Energy Pinellas Sitewide Semiannual Progress Report for December 2012mdashMay 2013 June 2013 Doc No N01796

prepared and submitted in 1997 to EPA Region 4 and FDEP to address the contamination at the WWNA Therefore four active SWMUs currently exist at the STAR Center These four SWMUs are the Old Drum Storage Site (PIN06) the Industrial Drain LeaksBuilding 100 Area (PIN12) the Northeast Site (PIN15) and the WWNA (PIN18) Two SWMUs PIN06 and PIN12 are collectively known as the Building 100 Area Figure 2 depicts the location of the four SWMUs DOE plans to proceed with closure of the WWNA under RBCA Risk Management Option II and to apply the default poor quality arsenic cleanup target level (CTL) of 100 micrograms per liter (μgL) to onsite groundwater Closure monitoring was completed in October 2006 A No Further Action with Controls proposal for the site was approved by FDEP in May 2007 Acceptance of this closure proposal by FDEP indicates that both soil and groundwater cleanup are complete Closure of the site can be finalized once Institutional Controls (ICs) are implemented DOE is working with the landowner (Pinellas County Industrial Development Authority) to establish ICs at the STAR Center Once ICs are in place there will be no potential for current or future exposure to contaminated groundwater ICs will need to be established and approved by FDEP before a formal No Further Action determination can be made Currently DOE is working with the STAR Center to develop a covenant that incorporates the ICs that will then become part of DOErsquos Long-Term Surveillance and Maintenance Plan at this site Additional background information relative to each SWMU is briefly described below This document serves as the semiannual progress report for each of these four SWMUs The results of recent monitoring activities and a summary of ongoing and projected work are provided in this report 11 Building 100 Area The Building 100 Area is made up of two SWMUs the Industrial Drain LeaksBuilding 100 (PIN12) and the Old Drum Storage Site (PIN06) The Old Drum Storage Site lies beneath and adjacent to the northwest corner of the main building that covers approximately 11 acres located near the southeast corner of the STAR Center (Figure 2) Building 100 is the most notable feature of the STAR Center having housed the majority of the laboratory and production facilities during DOE ownership of the facility One source of contamination at the Building 100 Area is leaks from a liquid waste drain system composed of individual drainage systems previously used for health physics chemical sanitary and storm-water systems The drain systems were flushed grouted and abandoned by 1997 and some of the chemical drain systems were replaced by an aboveground system (DOE 1997a) The Old Drum Storage Site is the former location of a concrete storage pad This area was equipped with a drain and containment system and was once used to store hazardous waste The waste stored at this location included methylene chloride ignitable liquids arsenic and calcium chromate solids Empty drums containing residual waste solvents also were stored in this area A RCRA Facility Investigation was conducted in 1991 at the Pinellas Plant to fulfill the requirements of the HSWA permit and a RCRA Facility Investigation report was produced in 1991 A subsequent report addendum was completed in March 1992 Based on the findings in


these two documents in accordance with the HWSA permit EPA notified DOE of the requirement for a CMS for the Old Drum Storage Site and the Industrial Drain Leaks Building 100 SWMUs The CMS report for the Industrial Drain LeaksBuilding 100 and the Old Drum Storage Site proposed remediation of these two SWMUs together (collectively referred to as the Building 100 Area) The report was submitted to EPA and was subsequently approved on June 9 1994 FDEP approved the CMS report on January 18 1995 The CMS report concluded that pump-and-treat with the existing air-stripping system was the preferred corrective measure for the Building 100 Area This conclusion was based on shallow monitoring-well data that suggested contamination was confined to shallow groundwater at the northwest corner of the building However that characterization was later found to be incomplete Two recovery wells were installed at the northwest corner of the building in 1995 The Building 100 Area Corrective Measures Implementation Plan (DOE 1996a) describes the installation of the wells and the operations and monitoring plan These recovery wells PIN12-RW01 and -RW02 extracted groundwater and pumped the water through secondary containment piping to the Northeast Site treatment system for pretreatment air stripping and discharge to the STAR Center industrial wastewater neutralization facility (IWNF) prior to transfer to the Publicly Owned Treatment Works (POTW) The Northeast Site treatment system was decommissioned in April 2004 so a smaller air-stripper treatment system was installed at the Northeast Site to treat the groundwater recovered via the two Building 100 Area recovery wells Subsequent to recovery well installation additional investigations were conducted by installing monitoring wells at multiple depths both outside the building and through the floor of the building In 1996 these investigations were summarized in the Building 100 Area Data Report (DOE 1996b) and the Building 100 Area Subsurface Investigations Phases I II and III (DOE 1996c) Results of these investigations indicated that (1) significant contaminant concentrations were present at intermediate and deep depths under the building and (2) low levels of contamination were present at the south and east sides of the building The Building 100 Area Data Report recommended that DOE continue operating the two recovery wells that were installed in accordance with the CMSCMIP conduct additional characterization under the building and east of the building conduct additional contaminant transport modeling and evaluate the potential for occurrence of dense nonaqueous phase liquids (NAPLs) These recommendations were addressed in the Building 100 Area Corrective Measures Implementation Plan Addendum (DOE 1998) A pilot test study was conducted in 2003ndash2004 to determine the effectiveness of enhanced biodegradation for this site (DOE 2005) The pilot test results were positive but the test did not result in significant elimination of vinyl chloride (VC) in low-concentration areas Therefore enhanced biodegradation technologies were not considered for use at the Building 100 Area at that time The Building 100 Area Corrective Measures Study Report Addendum (DOE 2006) was finalized in July 2006 The document concluded that DOErsquos original remediation objective of meeting maximum contaminant levels (MCLs) throughout the contaminant plume does not appear to be


reasonable given current knowledge of the site At that time it appeared that containment of the contaminant plume had been achieved and it was determined that human health and the environment were protected The document proposed that ICs be placed on the site property to prevent inappropriate groundwater use and that MCLs for site-related contaminants of potential concern (COPCs) be applied as groundwater cleanup goals outside the IC boundary Because the two existing groundwater recovery wells did not contribute significantly to either contaminant plume containment or mass removal DOE also proposed shutting down these wells and the associated treatment system Operation of these recovery wells and the treatment system was terminated on August 21 2006 with the approval of FDEP An interim remedial action using a single recovery well to collect hydraulic information began in July 2009 and ended in May 2011 Located in the south plume near the southern STAR Center property boundary recovery well PIN12-RW03 had a radius of influence that likely captured the entire south plume as it exited the property Operation of this recovery well ceased in May 2011 to allow treatment of the groundwater produced during the Countyrsquos road work (discussed below) Pinellas County Utilities started a major water line replacement effort along Belcher Road in October 2010 and Pinellas County Public Works started a significant road construction project along Belcher and Bryan Dairy Roads in October 2011 In July 2011 DOE began treating groundwater produced by dewatering conducted during these projects Treatment ended in January 2012 The extracted groundwater was transported to an onsite air stripper for treatment and the treated water was discharged to the STAR Centerrsquos IWNF and subsequently discharged to the POTW Prior to the start of the water line and road projects DOE installed new monitoring wells at the property boundary along the two roads in October 2007 and in January and February 2008 to further define the contaminant plume This investigation confirmed that the plume was offsite south of Bryan Dairy Road on the county right-of-way DOE performed the required notification to FDEP regarding the offsite plume Additional plume delineation was conducted on the property at 8040 Bryan Dairy Road by the installation of three continuous multichannel tubing (CMT) wells in September 2009 (PIN12-0567 -0568 and -0569) Contaminant concentrations exceeded CTLs in well PIN12-0569 DOE reported this discovery to FDEP and to the property owner in October 2009 in accordance with FDEP notification requirements Two additional CMT wells were installed on this property in March 2010 (PIN12-0570 and -0571) To further investigate the extent of the offsite contamination to the south of the STAR Center plume delineation work was conducted at 10980 Belcher Road on August 16ndash30 2010 using direct-push technology to collect groundwater samples from temporary locations This property is located across Bryan Dairy Road immediately south of the Building 100 Area at the STAR Center The results of this investigation indicated that the contaminant plume enters the 10980 Belcher Road property on the western side and extends southeastward (in the direction of groundwater flow) to the southern property boundary DOE reported this discovery to FDEP and to the property owner in October 2010 in accordance with FDEP notification requirements The


results of this investigation are reported in the Building 100 Area Off-Site Plume Delineation South of Bryan Dairy Road Data Report for Rally Stores Property (DOE 2010a) The results from that investigation suggested that the contaminant plume extended south onto property at 10950 Belcher Road Plume delineation was conducted at this property on December 6ndash16 2010 and April 4ndash6 2011 Additional delineation was conducted in the median of Belcher Road just east of this property on January 24ndash28 2011 The results of these investigations demonstrated that the contaminant plume extends in a southeasterly direction from the northern property boundary to the eastern property boundary but not to the median of Belcher Road The results of these investigations are reported in the South Belcher Road Data Report (Daniel 2011a) and the Better Business Forms Data Report (Daniel 2011b) Delineation of the eastern plume at the Building 100 Area was conducted in May June August and September 2011 This work identified a contaminant plume extending from under the eastern edge of Building 100 past the eastern STAR Center property boundary under Belcher Road and onto 11111 Belcher Road DOE made the required notification to FDEP regarding the offsite plume 14-dioxane was measured at elevated concentrations during this work and as a result was added as a COPC for the Building 100 Area in a letter from DOE to FDEP dated October 13 2011 (DOE 2011) Additional delineation at 11111 Belcher Road in March and April 2012 defined the extent of the eastern contaminant plume which appears to attenuate quickly after entering the property The Building 100 Area Site Assessment Report (DOE 2012a) summarizes the results of the plume delineation work conducted at the Building 100 Area and the adjacent private properties from 2007 to 2012 The action proposed in this document is to conduct plume stability monitoring of both the onsite and offsite plumes The Plume Stability Monitoring Plan for the Building 100 Area is included in the Site Monitoring Plan which is an Appendix to the Long-Term Surveillance and Maintenance Plan for the Pinellas Site (DOE 2012b) Plume stability monitoring began with the March 2013 sampling event 12 Northeast Site The Northeast Site is located in the northeast corner of the STAR Center (Figure 2) In the late 1960s before construction of the East Pond in 1968 drums of waste and construction debris were disposed of in the swampy area of the Northeast Site In 1986 an expansion of the East Pond was initiated to create additional storm-water retention capacity but excavation activities ceased when contamination was detected directly west of the pond EPA identified the Northeast Site as a SWMU (EPA 1992) An Interim CMS (DOE 1991b) was developed and submitted to EPA and approval of this document was received in October 1991 An interim groundwater recovery system for the Northeast Site was installed and operation commenced in January 1992 The groundwater treatment system as initially installed consisted of four recovery wells equipped with pneumatic pumps a holding tank centrifugal transfer pumps and approximately 2500 feet (ft) of transfer and secondary containment piping During 1993 DOE proposed a reconfigured system for the site consisting of four shallow and three deep recovery wells After EPA approved the upgrade the system was reconfigured and became operational on March 1 1994


Between August and October 1995 a portion of the Northeast Site was excavated to remove debris drums of waste and other materials that could inhibit future corrective measures Location of the areas of excavation was based primarily on the results of a geophysical survey and knowledge of existing utility locations Detailed descriptions of the debris removal activities were submitted to EPA and FDEP as part of the Northeast Site Interim Measures Quarterly Progress Report (DOE 1996d) In 1996 DOE submitted the Northeast Site Corrective Measures Implementation Plan (DOE 1996e) to EPA Region 4 and FDEP This plan was approved by both regulatory agencies in 1997 As part of the Northeast Site CMS and CMIP a pump-and-treat system in conjunction with a subsurface hydrogeologic barrier wall to prevent migration of the contaminant plume was identified as the best available technology The pump-and-treat system included a pretreatment system for iron removal an air stripper unit and a tank for holding treated groundwater before discharge to the STAR Center IWNF prior to transfer to the POTW The treatment system was constructed in early 1997 and became operational by July 1997 processing groundwater from seven Northeast Site recovery wells and two Building 100 Area recovery wells Subsequently several additional recovery wells were installed at the Northeast Site and some of the old recovery wells were abandoned During 1997 anaerobic bioremediation and rotary steam-stripping pilot tests were conducted in the northern and southern portions of the Northeast Site respectively These tests were designed by the Innovative Treatment Remediation Demonstration group of regulatory and industry members to provide remedial options at the STAR Center At the conclusion of the field tests in July 1997 pump-and-treat technology resumed at the Northeast Site NAPLs were identified in a few monitoring and recovery wells in 1998 An Interim Measures Work Plan for Remediation of Non-Aqueous Phase Liquids at the Northeast Site (DOE 2001) was submitted to FDEP in late November 2001 The purpose of this document was to present the plan to remediate NAPLs at two areas (NAPL Areas A and B) of the Northeast Site using a thermal remediation method FDEP approved this document on January 10 2002 Construction of the NAPL Area A treatment system began in late May 2002 and system startup occurred on September 26 2002 NAPL treatment was completed on February 28 2003 The Northeast Site Area A NAPL Remediation Final Report (DOE 2003) describes the thermal remediation of Area A Construction of the NAPL Area B treatment system began in July 2004 and was completed in early August 2005 and operations began on August 16 2005 NAPL treatment was completed on August 29 2006 The Final Report Northeast Site Area B NAPL Remediation Project at the Young - Rainey STAR Center Largo Pinellas County Florida (DOE 2007) describes Area B remediation Monitoring wells were installed at the former NAPL areas to monitor the remaining dissolved-phase plumes Groundwater samples from a few of the wells continued to show high concentrations of contaminants Soil samples were collected from 12 soil borings in August 2007 to evaluate the potential for a contaminant source remaining in the subsurface at these locations Results indicated high contaminant concentrations in soil at most of these borings so a second phase of sampling was conducted in March and April 2008 during which samples were collected


from 45 soil borings Ten additional borings were sampled in May and 11 more were sampled in June These 78 soil borings defined two areas containing a source of contamination To address this contamination source DOE prepared an interim remedial action plan for soil excavation using the large-diameter auger (LDA) method in accordance with the RBCA regulations and submitted the document to FDEP in August 2008 This plan was approved on August 22 2008 An engineering design was developed and a source removal subcontract was awarded in 2008 Source removal in the form of LDA excavation began on January 14 2009 and was completed on May 22 2009 Two hundred forty-three large-diameter and 352 small-diameter borings were completed Approximately 8387 cubic yards of soil were excavated including 4667 cubic yards removed as clean overburden and 3720 cubic yards of contaminated soils that were removed characterized for waste disposal and disposed of as nonhazardous waste at a RCRA Subtitle D landfill Additional information regarding the Northeast Site LDA work is available in the Data Report for Overburden Soil at the Northeast Site and the 45 Acre Site (DOE 2009a) and the Interim Remedial Action for Source Removal at the Northeast Site Final Report (DOE 2009b) As a follow-up to the LDA work emulsified soybean oil and the Dehalococcoides ethenogenes microorganism were injected into the subsurface at 75 points at the site in January and February 2010 The Injection of Emulsified Soybean Oil at the Northeast Site and 45 Acre Site (DOE 2010b) was prepared to describe the work required for this task This project has resulted in a significant decrease in contaminant mass and concentration around the former contaminant source areas and in the downgradient contaminant plume With the completion of the LDA project to remove contaminant source material and the follow-up enhanced bioremediation project DOE is proceeding to close the Northeast Site under the FDEPrsquos RBCA rules (Chapter 62-780680 FAC) The Closure Monitoring Plan for the Northeast Site and 45 Acre Site (DOE 2009c) describes the closure monitoring that is necessary under RBCA according to the requirements for Post Active Remediation Monitoring (Chapter 62-780750 FAC) Closure monitoring was implemented starting with the September 2009 sampling event and was completed in September 2012 COPCs concentrations decreased significantly over this time period DOE submitted the Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site (DOE 2013) to FDEP in May 2013 That document proposes a risk-based closure for the Northeast Site under the Statersquos RBCA regulations 13 WWNA The WWNA (PIN18) includes the IWNF the area south of the IWNF (including the parking lot) and Building 200 (Figure 2) In April 1993 the WWNA and the Building 200 Area were identified as potential SWMUs and an RFA was conducted (EPA 1994) The RFA recommended that the WWNA and Building 200 be considered one SWMU and this SWMU is now referred to as the WWNA RFA field activities began in September 1994 and included soil characterization monitoring well installation and groundwater sampling Arsenic was identified as the major COPC Trichloroethene (TCE) and VC were detected at low concentrations in groundwater and were subsequently dismissed as COPCs once their concentrations decreased below cleanup levels


A CMSCMIP (DOE 1997b) was completed for this SWMU in 1997 The recommended remediation alternative for the WWNA was groundwater recovery with the Building 100 Area wells and an additional recovery well located in the WWNA The CMIP recommended (1) that the recovery well in the WWNA withdraw surficial aquifer groundwater directly from the arsenic plume thereby reducing contaminant mass and preventing contaminant migration and (2) that the recovered water be discharged directly to the STAR Centerrsquos wastewater neutralization facility Because FDEP expressed concerns about elevated concentrations of arsenic in the soil DOE conducted extensive sampling and analysis of soil in January and February 1999 in an effort to locate the source of arsenic contamination Elevated levels of arsenic were identified at several locations and at various depths within the SWMU A treatability study was conducted to determine the leachability of arsenic from the soil into the groundwater The study concluded that arsenic leachability from the soil was very limited as demonstrated by a measured average soilwater distribution coefficient of 63 liters per kilogram DOE then conducted a statistical evaluation of arsenic soil data that resulted in the proposal to excavate two areas where the highest concentrations of arsenic were identified Follow-up monitoring of strategically located wells would then determine whether arsenic concentrations in the groundwater decrease with time This proposal was approved by FDEP in September 1999 An excavation plan was developed to address logistics sampling and analytical concerns and waste management issues regarding the generation of contaminated media This document and the statistical evaluation are included in the WWNA CMIP Addendum (DOE 2000) Excavation of the two areas was completed in early October 1999 Subsequently the existing recovery well was abandoned and two recovery wells were installed to continue plume control in the area In addition a third recovery well was created by converting the monitoring well with the highest arsenic concentration (PIN18-0501) to a recovery well On December 20 2005 DOE received concurrence from FDEP to shut down the groundwater recovery system and begin monitoring to determine a closure approach through FDEPrsquos RBCA regulations promulgated by the Florida Legislature in 2003 The 1-year RBCA closure monitoring program specified by FDEP began in October 2005 and was completed in October 2006 A No Further Action with Controls proposal was submitted to FDEP on March 14 2007 FDEP approved the document on May 24 2007 and requested that DOE submit an updated Statement of Basis for the WWNA Submittal of the Statement of Basis is awaiting finalization of ICs at the STAR Center The goal of the 1999 soil excavation was to remove the areas containing the highest arsenic concentrations such that the remaining soils met the industrial CTL of 12 milligrams per kilogram Soils containing arsenic concentrations above the residential CTL of 21 milligrams per kilogram were left in place because the current site use is solely industrial After the No Further Action with Controls proposal was submitted in 2007 FDEP expressed concern about arsenic exceeding the residential standard in shallow soils (less than 2 ft deep) In response DOE determined that a potential course of action was to identify the area where the residential arsenic


standard is exceeded and apply an IC that would prohibit future residential development in this area Negotiations to apply the IC are ongoing 14 Site Update

FDEP verbally approved cessation of closure monitoring at the Northeast Site during a teleconference with DOE on January 17 2013

The Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site (DOE 2013) was submitted to FDEP in May 2013

Twenty-seven new monitoring wells (ie nine well triples) were installed at the Building 100 Area in February 2013 to facilitate plume stability monitoring

Twenty monitoring wells at the Building 100 Area and three monitoring wells at the WWNA were abandoned on April 22 and 23 2013

The sitewide semiannual sampling was conducted March 4ndash14 2013 and included collection of water samples from 100 monitoring wells Water level measurements were obtained from all accessible monitoring wells recovery wells and ponds on March 5

The results of semiannual monitoring were reported (this document) 15 Waste Minimization The following materials were recycled at the Pinellas site from December 2012 through May 2013

31 pounds of paper

23 pounds of cardboard

7 pounds of plastic

43 pounds of magazines

1 pound of aluminum

16 pounds of batteries

20 Water-Level Elevations Depth-to-water measurements were taken at all accessible monitoring wells piezometers and ponds (including two offsite ponds) at the STAR Center on March 5 2013 The water levels were measured with an electronic water level indicator or directly from a staff gauge Groundwater elevations are listed in Table 1 21 Groundwater Flow Groundwater and surface water elevations were used to construct sitewide groundwater contour maps of the shallow and deep surficial aquifers (Plates 1 and 2 respectively) Individual contour maps were also constructed for the shallow and deep surficial aquifers at the Building 100 Area (Figures 3 and 4)


For the past several years shallow groundwater beneath Building 100 has been observed to flow to the southeast under a very slight gradient and this flow pattern was observed again in March 2013 (Figure 3) A similar flow pattern was observed in the deep surficial aquifer (Figure 4) The hydraulic gradient in the Building 100 Area in March 2013 was about 0002 ftft onsite and about 0005 offsite Based on calculations using Darcyrsquos Law along with approximations of 1 ftday for hydraulic conductivity and 03 for effective porosity groundwater velocity in this area is estimated to be about 24 to 61 ftyear An aquifer test conducted in July 2009 in the area around recovery well RW03 indicated that the hydraulic conductivity of the surficial aquifer around well RW03 might be higher than that observed in other parts of the STAR Center Analysis of the aquifer test yielded an estimated hydraulic conductivity of 67 to 74 ftday which is higher than previous tests conducted in other areas of the STAR Center where estimated hydraulic conductivities were closer to 1 ftday Surface water elevations were recorded in March 2013 from the East South Southwest and West Ponds Pond 5 and the pond just east of Belcher Road (Table 2) All the ponds are hydraulically connected to the shallow surficial aquifer system (Plate 1)

30 Groundwater Sampling 31 Work Performed During the annual sampling event at the STAR Center in March 2013 groundwater samples were collected from 100 monitoring wells at the Building 100 Area Volatile organic compounds were analyzed in these samples using EPA SW-846 method 8260B and 14-dioxane was analyzed in the same samples using EPA method 8260B SIM Laboratory reports are provided in Appendix A The analytical results are discussed in Section 4 Figures 5ndash13 are plume maps for the Building 100 Area for March 2013 Figures 5 and 6 show the total COPCs (TCOPCs) concentrations TCOPCs is the sum of the individual COPC concentrations for each well The Building 100 Area COPCs are TCE cis-12-dichloroethene (cDCE) trans-12-dichloroethene (tDCE) 11-dichloroethene (11-DCE) VC and 14-dioxane Figures 7ndash13 show the plumes for the individual COPCs a plume map for tDCE is not shown because this COPC exceeded the CTL only in well 12-S35B All samples were collected in accordance with the Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites (LMSPROS04351) using FDEP procedures All samples were submitted to TestAmerica Laboratories Inc in Denver Colorado for analysis TestAmerica Denver is accredited by the Florida Department of Health in accordance with the National Environmental Laboratory Accreditation Conference (certification number E87667) All monitoring wells were micropurged using a dedicated bladder pump or a peristaltic pump Sampling was performed when the field measurements stabilized in accordance with FDEP procedures Table 3 lists field measurements of temperature specific conductance turbidity pH oxidation-reduction potential and dissolved oxygen recorded at the time the samples were


collected Measurements were made using a calibrated multiparameter meter with a flow cell and turbidity was measured using a nephelometer 32 Quality AssuranceQuality Control The results from the analytical laboratory TestAmerica Denver were checked for quality assurancequality control (QAQC) through duplicate samples and trip blanks The duplicate sample results were compared and the relative percent differences (RPDs) between the results were calculated (Table 4) trans-12-Dichloroethene in well PIN12-0580-2 VC in well PIN12-0582-2 and 11-dichloroethene in well PIN12-0587-2 all had RPD values that exceeded the EPA-recommended laboratory duplicate criterion of less than 20 RPD for results that are greater than 25 times the method detection limit These results were ldquoJrdquo qualified as estimated values due to the poor RPD value Table 4 also lists analytes in the duplicate samples from wells 12-0581-2 and 12-0582-2 that did not have an RPD calculated because the results were less than 25 times the method detection limit Some of these results show significant disagreement (eg 14-dioxane in well 12-0582-2) The poor precision of these results may be due to the fact that the laboratory diluted the original samples but not the duplicate samples These two wells were installed in February 2013 and sampled for the first time in March 2013 so historical data were not available to compare to the current results A detailed review of the chromatograms and mass spectra in the lab reports for original and duplicate samples collected from these wells confirmed the presence of the detected analytes in the duplicate samples This confirmation in combination with the results from temporary sampling points nearby in 2011 (see Section 11) strongly suggested that the results for the duplicate samples were the most representative for these wells Therefore the results from the original samples were excluded and the results from the duplicate samples are reported in this document This issue will be revisited after the second sampling event at these wells in September 2013 As specified in the Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites duplicate samples should be collected at a frequency of one duplicate for every 20 or fewer samples For the STAR Center and the 45 Acre Site 119 samples and 6 duplicates were collected for volatiles analysis and 100 samples and 5 duplicates were collected for 14-dioxane analysis The duplicate requirements for this sampling event were met Six trip blanks and two equipment blanks also were collected during this event A data validation software module for identifying and tracking anomalous groundwater data within the Site Environmental Evaluation for Projects (SEEPro) database was used to generate a report of analytical results that fall outside of historical minimum or maximum values No anomalous results were identified


40 Plume Stability Monitoring The Plume Stability Monitoring Plan for the Building 100 Area is included in an appendix to the Long-Term Surveillance and Maintenance Plan for the Pinellas Site (DOE 2012b) This plan defines the strategy to determine the stability of the onsite and offsite plumes The plume stability monitoring approach involves establishment of plume cross-sections using certain sets of wells and the determination of an area under the curve for each cross-section The cross-section lines are shown on Figure 14 The lateral cross-sections allow evaluation of the entire width of each plume as it emerges from under the building and at the site boundary if the plume is expanding laterally (concentrations increasing at the sides of the plume) this will be seen as an increase in the area under the curve The longitudinal cross-section in each plume will use wells in the centerline of the plume (the highest concentration area) to determine if the plume is expanding at its leading edge and if concentrations are decreasing stable or increasing in the plume centerline Each ldquodata pointrdquo in the cross-sections is the location of a well triple (ie wells with three different screened intervals) or a well pair The value plotted at each data point is the sum of COPC concentrations in all sampled intervals in the well pair or triple at that location For example in cross-section E1-E2 the northern data point will be the sum of TCE cDCE tDCE 11-DCE VC and 14-dioxane concentrations measured in wells 12-0555A 12-0555B and 12-0555C

For each sampling event a ldquocurverdquo will be plotted for each cross-section and then the area under the curve will be calculated The area under the curve values will be tracked from event to event and a trend line will be fit to the data The plume will be designated as unstable if an increasing trend is observed

In addition to the plume stability monitoring scheme presented above several wells that are not part of a cross-section will also be sampled to determine whether the plume is advancing at any of its boundaries (Figure 14) At each of these well locations the COPC concentrations from all screened intervals will be summed and the sum will be plotted For example for the well triple 0570 located on the Harrod property the COPC concentrations in all three screened intervals (0570-1 -2 and -3) will be summed and plotted A trend line will be fit to the plotted data and as with the area under the curve values the plume will be designated as unstable if an increasing trend is observed The March 2013 sampling event was the first plume stability monitoring event The COPCs concentrations from each well are listed in Table 5 The sum of COPCs at each ldquodata pointrdquo in each cross-section is listed in Table 6 Figures 15ndash20 show the curve plots for each cross-section The area under the curve for each cross-section is listed in Table 7 The area under the curve value is calculated using a spreadsheet it is not the sum of the COPCs in each cross-section Because the March 2013 sampling event was the first plume stability monitoring event the area under the curve values are not plotted because there is only one data point for each cross-section The area under the curve values will be plotted after the second plume stability monitoring event in September 2013


50 Upcoming Tasks The following major tasks are planned for the next semiannual period (June through November 2013)

Plume stability monitoring at the Building 100 Area will continue with the semiannual sampling event in September 2013

60 References Daniel 2011a Joe Daniel Site Manager Pinellas Environmental Restoration Project SM Stoller Corporation letter (about the South Belcher Road Data Report) to Scott Surovchak Pinellas Site Manager Office of Legacy Management US Department of Energy April 4 Daniel 2011b Joe Daniel Site Manager Pinellas Environmental Restoration Project SM Stoller Corporation letter (about the Better Business Forms Data Report) to Scott Surovchak Pinellas Site Manager Office of Legacy Management US Department of Energy May 13 DOE (US Department of Energy) 1991a Environmental Restoration Program RCRA Facility Investigation Report Pinellas Plant (Draft) Albuquerque Operations Office Albuquerque New Mexico September DOE (US Department of Energy) 1991b Interim Corrective Measures Study Northeast Site Pinellas Plant Largo Florida May DOE (US Department of Energy) 1994 Statement of Basis for Twelve Solid Waste Management Units Recommended for No Further Action Pinellas Plant Largo Florida January DOE (US Department of Energy) 1996a Building 100 Area Corrective Measures Implementation Plan (Draft) Environmental Restoration Program Pinellas Plant Largo Florida January DOE (US Department of Energy) 1996b Building 100 Area Data Report October 1993 to July 1996 Office of Legacy Management Grand Junction Colorado November DOE (US Department of Energy) 1996c Building 100 Area Subsurface Investigations Phases I II and III Volumes 1 and 2 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 1996d Northeast Site Interim Measures Quarterly Progress Report October through December 1995 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 1996e Northeast Site Corrective Measures Implementation Plan Office of Legacy Management Grand Junction Colorado March


DOE (US Department of Energy) 1997a Pinellas Plant Environmental Baseline Report prepared by Lockheed Martin Specialty Components Inc for DOE Pinellas Area Office June DOE (US Department of Energy) 1997b Corrective Measures Study ReportCorrective Measures Implementation Plan WWNABuilding 200 Office of Legacy Management Grand Junction Colorado June DOE (US Department of Energy) 1998 Building 100 Area Corrective Measures Implementation Plan Addendum Pinellas STAR Center Largo Florida February DOE (US Department of Energy) 2000 WWNABuilding 200 Corrective Measures Implementation Plan Addendum Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 2001 Interim Measures Work Plan for Remediation of Non-Aqueous Phase Liquids at the Northeast Site MAC-PIN 13105-1 prepared for DOE Grand Junction Office Grand Junction Colorado November DOE (US Department of Energy) 2003 Northeast Site Area A NAPL Remediation Final Report GJOminus2003minus482minusTAC prepared by US Department of Energy Grand Junction Colorado September DOE (US Department of Energy) 2005 Building 100 Area Enhanced Bioremediation Pilot Test Final Report DOE-LMGJ791-2005 Office of Legacy Management Grand Junction Colorado January DOE (US Department of Energy) 2006 Building 100 Area Corrective Measures Study Report Addendum DOE-LMGJ1241-2006 Office of Legacy Management Grand Junction Colorado July DOE (US Department of Energy) 2007 Final Report Northeast Site Area B NAPL Remediation Project at the Young - Rainey STAR Center Largo Pinellas County Florida DOE-LM1457-2007 Office of Legacy Management Grand Junction Colorado April DOE (US Department of Energy) 2009a Data Report for Overburden Soil at the Northeast Site and the 45 Acre Site LMSPINN01395 Office of Legacy Management Grand Junction Colorado July DOE (US Department of Energy) 2009b Interim Remedial Action for Source Removal at the Northeast Site Final Report LMSPINN01357 Office of Legacy Management Grand Junction Colorado September DOE (US Department of Energy) 2009c Closure Monitoring Plan for the Northeast Site and 45 Acre Site LMSPINN01401 Office of Legacy Management Grand Junction Colorado August


DOE (US Department of Energy) 2010a Building 100 Area Off-Site Plume Delineation South of Bryan Dairy Road Data Report for Rally Stores Property LMSPINN01535 Office of Legacy Management Grand Junction Colorado October DOE (US Department of Energy) 2010b Injection of Emulsified Soybean Oil at the Northeast Site and 45 Acre Site LMSPINN01494 Office of Legacy Management Grand Junction Colorado April DOE (US Department of Energy) 2011 Scott Surovchak Pinellas Site Manager letter (about Groundwater Samples at the Young-Rainey STAR Center) to John Armstrong Remedial Project Manager FDEP October 13 DOE (US Department of Energy) 2012a Building 100 Area Site Assessment Report LMSPINN01747 Office of Legacy Management Grand Junction Colorado August DOE (US Department of Energy) 2012b Long-Term Surveillance and Maintenance Plan for the Pinellas Site LMSPINN01058-100 Office of Legacy Management Grand Junction Colorado November DOE (US Department of Energy) 2013 Site Rehabilitation Completion Report with No Further Action Proposal for the Northeast Site LMSPINN01778 Office of Legacy Management Grand Junction Colorado May EPA (US Environmental Protection Agency) 1988 RCRA Facility Assessment Department of EnergymdashFl6 890 090 008 June EPA (US Environmental Protection Agency) 1992 Letter to DOE Gerald W Johnson Approval of Pinellas Site Remedial Facility Investigation Report April EPA (US Environmental Protection Agency) 1994 RCRA Facility Assessment Report WWNABuilding 200 Area March Sampling and Analysis Plan for US Department of Energy Office of Legacy Management Sites LMSPROS04351 continually updated prepared by SM Stoller Corporation for the US Department of Energy Office of Legacy Management Grand Junction Colorado



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0555 0554 0580 S71 S70 S69

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541542549 0581 0582 539540 S73 0583

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0561 0584 0585 524525 S68 S69

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0586 0587 0588

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0

1000

2000

3000

4000

5000

6000

0585 0587 0569 0572 0574 0575

S4 ‐ S5March 2013




(ft bls)


PIN02 Sitewide Piezometers

PZ03 352013 1023 421 1549

PZ04 352013 1029 283 1537

PZ05 352013 1018 356 1454

PZ08 352013 1012 439 1401

PZ09 352013 1344 412 1388

PZ10 352013 1003 454 1434

PZ11 352013 0945 483 1405

Building 100 Area

PIN12

0509 352013 1142 361 1443

0515 352013 0631 428 1362

0516 352013 0609 448 1352

0517 352013 0641 406 1384

0518 352013 0645 397 1397

0520 352013 1132 366 1435

0521 352013 1128 370 1435

0524 352013 0711 366 1375

0525 352013 0657 371 1371

0527 352013 1035 1272 535

0528 352013 1348 1213 547

0539 352013 1413 336 1324

0540 352013 1421 292 1318

0541 352013 0841 484 1282

0542 352013 1424 451 1319

0549 352013 0847 451 1315

0550-1 352013 1436 272 1198

0550-2 352013 1436 262 1208

0550-3 352013 1437 257 1213

0551-1 352013 1425 329 1211

0551-2 352013 1425 293 1247

0551-3 352013 1425 318 1222

0553A 352013 0800 450 1361

0553B 352013 0824 466 1345

0553C 352013 0828 464 1347

0554A 352013 0752 463 1361

0554B 352013 0750 463 1361

0554C 352013 0743 465 1359

0555A 352013 0754 412 1377

0555B 352013 0758 421 1368

0555C 352013 0759 420 1369

0559-1 352013 0926 535 1255

0559-2 352013 1132 507 1283

0559-3 352013 1133 689 1101




(ft bls)


0560-1 352013 0640 394 1378

0560-2 352013 0639 385 1387

0560-3 352013 0640 370 1402

0561-1 352013 0647 431 1391

0561-2 352013 0656 436 1386

0561-3 352013 0656 434 1388

0562-1 352013 1135 489 1337

0562-2 352013 1140 487 1339

0562-3 352013 1141 484 1342

0563-1 352013 1141 349 1378

0563-2 352013 1342 346 1381

0563-3 352013 1343 341 1386

0564-1 352013 1453 296 1254

0564-2 352013 1454 307 1243

0564-3 352013 1455 313 1237

0565-1 352013 1506 412 1158

0565-2 352013 1507 416 1154

0565-3 352013 1508 413 1157

0566-1 352013 1530 426 1134

0566-2 352013 1530 421 1139

0566-3 352013 1531 423 1137

0567-1 352013 1410 413 1413

0567-2 352013 1411 433 1393

0567-3 352013 1412 457 1369

0568-1 352013 1418 436 1390

0568-2 352013 1419 461 1365

0568-3 352013 1420 459 1367

0569-1 352013 1430 463 1348

0569-2 352013 1431 488 1323

0569-3 352013 1432 488 1323

0571-1 352013 1445 529 1291

0571-2 352013 1446 540 1280

0571-3 352013 1447 534 1286

0572-1 352013 1515 330 1230

0572-2 352013 1516 330 1230

0573-1 352013 1537 328 1172

0573-2 352013 1537 328 1172

0573-3 352013 1537 330 1170

0574-1 352013 1518 541 1089

0574-2 352013 1519 533 1097

0574-3 352013 1520 537 1093

0575-1 352013 1509 491 1039

0575-2 352013 1511 487 1043

0576-1 352013 1411 465 1285

0576-2 352013 1412 453 1297




(ft bls)


0576-3 352013 1412 452 1298

0577-1 352013 1202 464 1326

0577-2 352013 1203 464 1326

0577-3 352013 1204 464 1326

0578-1 352013 1355 425 1355

0578-2 352013 1356 429 1351

0578-3 352013 1357 431 1349

0579-1 352013 1451 421 1319

0579-2 352013 1451 424 1316

0579-3 352013 1452 425 1315

0580-1 352013 0940 486 1364

0580-2 352013 0941 491 1359

0580-3 352013 0942 490 1360

0581-1 352013 1055 412 1324

0581-2 352013 1056 413 1323

0581-3 352013 1057 415 1321

0582-1 352013 1100 353 1320

0582-2 352013 1101 353 1320

0582-3 352013 1102 355 1318

0583-1 352013 1111 342 1309

0583-2 352013 1112 335 1316

0583-3 352013 1113 337 1314

0584-1 352013 0857 379 1381

0584-2 352013 0858 383 1377

0584-3 352013 0859 387 1373

0585-1 352013 0903 368 1381

0585-2 352013 0904 373 1376

0585-3 352013 0905 377 1372

0586-1 352013 1350 387 1353

0586-2 352013 1351 382 1358

0586-3 352013 1352 383 1357

0587-1 352013 1354 402 1348

0587-2 352013 1355 398 1352

0587-3 352013 1356 399 1351

0588-1 352013 1357 396 1344

0588-2 352013 1358 394 1346

0588-3 352013 1359 396 1344

PZ01 352013 1427 415 1335

PZ02 352013 1443 520 1370

PZ03 352013 1437 354 1336

S29C 352013 0911 420 1431

S30B 352013 0918 415 1436

S31B 352013 0853 429 1422

S32B 352013 0900 418 1433

S33C 352013 0937 410 1441




(ft bls)


S35B 352013 0951 439 1412

S36B 352013 0847 461 1390

S37B 352013 0931 408 1443

S67B 352013 1036 439 1408

S67C 352013 1037 448 1399

S67D 352013 1038 448 1400

S68B 352013 1408 404 1386

S68C 352013 1412 428 1362

S68D 352013 1412 424 1366

S69B 352013 0713 260 1340

S69C 352013 0722 262 1338

S69D 352013 0724 277 1323

S70B 352013 0732 311 1359

S70C 352013 0730 305 1365

S70D 352013 0726 323 1347

S71B 352013 0734 448 1392

S71C 352013 0737 480 1360

S71D 352013 0739 475 1365

S72B 352013 0833 495 1325

S72C 352013 0838 492 1328

S72D 352013 0840 491 1329

S73B 352013 0849 386 1314

S73C 352013 0911 386 1314

S73D 352013 0910 386 1314

PIN21

0502 352013 0912 250 1270

0503 352013 0925 263 1257

0503 352013 1357 346 1174

0504 352013 1400 390 1370

0512 352013 1405 388 1342

PIN15 Northeast Site

0506 352013 1108 327 1373

0507 352013 1104 322 1378

0513 352013 1058 1210 550

0520 352013 1100 339 1371

0530 352013 1053 371 1369

0534 352013 1104 222 1488

0535 352013 1057 379 1381

0537 352013 1109 428 1432

0568 352013 1044 448 1402

0569 352013 1040 427 1411

0573 352013 1125 442 1396

0574 352013 1128 428 1414

0594 352013 1112 465 1385

0595 352013 1135 449 1411




(ft bls)


M16D 352013 1125 382 1438

M16S 352013 1123 381 1439

M24D 352013 1135 390 1390

M33D 352013 1134 325 1435

PIN18 WWNA

0503 352013 1137 346 1422

0507 352013 1343 370 1403

0523 352013 1116 522 1418

0524 352013 1119 477 1423

0525 352013 1118 457 1433

0526 352013 1017 466 1394

Abbreviations amsl = above mean sea level bls = below land surface



Location Measurement Surface Water

Elevation (ft amsl) Date Time

PIN01 Pond 5

P501 352013 1013 1360

P502 352013 1009 1389

PIN02 West Pond

W005 352013 1004 1409

PIN12 Belcher Road Pond

BR01 352013 1447 1295

PIN15 East Pond

E001 352013 1045 1377

PIN23 Southwest Pond

SW01 352013 1351 1359

PIN37 South Pond

S001 352013 1355 1361

S002 352013 1401 14661

Notes 1questionable value not used for water elevation contours Abbreviations amsl = above mean sea level




Temperature (degC)


Turbidity (NTU)

pH


(mV)


PIN12

0524 27ndash37 246 1426 4 661 -14 08

0525 12ndash22 241 742 29 679 -63 05

0539 95ndash195 241 1612 14 651 -46 06

0540 20ndash30 243 1457 13 653 -35 06

0541 10ndash20 277 784 16 660 -63 06

0542 20ndash30 281 796 7 661 -53 06

0549 30ndash40 273 1404 15 663 -52 07

0551-1 9ndash18 228 1004 3 665 39 15

0551-2 20ndash29 232 1055 13 665 44 11

0554A 3ndash13 216 650 9 648 40 08

0554B 13ndash23 227 682 11 665 -34 05

0554C 23ndash33 244 880 14 672 -63 06

0555A 25ndash125 233 379 - 660 -26 12

0555B 13ndash23 225 376 26 702 -30 10

0555C 23ndash33 210 534 16 679 -33 13

0561-1 9ndash18 223 511 13 682 9 05

0561-2 20ndash29 229 603 2 677 -12 05

0561-3 31ndash40 210 1055 1 658 -20 04

0565-1 9ndash18 219 1345 1 672 -36 11

0565-2 20ndash29 204 1250 1 668 -30 18

0565-3 31ndash40 222 1502 2 664 -31 14

0568-1 9ndash18 246 1819 4 670 -4 17

0568-2 20ndash29 252 1402 10 672 -27 16

0568-3 31ndash40 254 1798 10 673 -22 17

0569-1 9ndash18 205 1847 4 679 -14 14

0569-2 20ndash29 209 1248 7 674 -30 13

0569-3 31ndash40 214 1292 3 673 -31 14

0570-1 9ndash18 241 2048 4 676 -43 15

0570-2 20ndash29 267 1665 8 677 -20 -

0570-3 31ndash40 220 1363 9 676 37 11

0572-1 9ndash18 267 1638 6 671 -39 20

0572-2 20ndash29 267 1017 5 674 -23 16

0573-1 9ndash18 210 1594 7 666 -47 16

0573-2 20ndash29 231 1172 4 668 -45 17

0573-3 31ndash40 229 1514 1 661 -22 14

0574-1 9ndash18 202 1258 9 675 -24 18

0574-2 20ndash29 225 1274 5 673 -18 16

0574-3 31ndash40 237 1492 5 672 -19 18

0575-1 9ndash18 228 1323 5 674 -38 17

0575-2 20ndash29 218 1459 9 667 -35 14

0576-1 4ndash13 191 1112 2 663 59 15

0576-2 15ndash24 200 1099 6 664 26 12

0576-3 26ndash35 226 1719 9 672 48 12




Temperature (degC)


Turbidity (NTU)

pH


(mV)


0577-1 4ndash13 206 2069 6 642 40 18

0577-2 15ndash24 204 1458 3 648 41 19

0577-3 26ndash35 200 1245 3 668 30 -

0578-1 4ndash13 179 726 6 637 128 12

0578-2 15ndash24 193 901 3 647 73 13

0578-3 26ndash35 193 1077 4 647 38 13

0579-1 4ndash13 193 1324 5 614 36 15

0579-2 15ndash24 210 1084 6 653 26 16

0579-3 26ndash35 207 1439 31 669 4 16

0580-1 9ndash18 162 653 29 702 -66 12

0580-2 20ndash29 189 1260 13 710 -75 12

0580-3 31ndash40 218 1538 11 702 -108 13

0581-1 9ndash18 225 1350 11 688 -129 08

0581-2 20ndash29 237 1100 17 702 -136 08

0581-3 31ndash40 258 1484 11 671 -74 07

0582-1 9ndash18 263 2261 12 674 -113 06

0582-2 20ndash29 264 1234 9 676 -97 06

0582-3 31ndash40 267 1527 24 663 -55 07

0583-1 9ndash18 240 1224 47 689 -132 04

0583-2 20ndash29 234 1739 5 659 -83 07

0583-3 31ndash40 247 1779 13 668 -74 06

0584-1 9ndash18 178 696 12 711 -61 15

0584-2 20ndash29 192 1057 12 778 -143 12

0584-3 31ndash40 205 1617 14 689 -79 16

0585-1 9ndash18 236 778 11 705 -107 13

0585-2 20ndash29 249 1196 11 698 -116 12

0585-3 31ndash40 253 1621 9 678 -105 06

0586-1 8ndash17 210 604 16 714 -103 04

0586-2 19ndash28 233 717 8 715 -151 04

0586-3 30ndash39 243 1579 10 692 -113 06

0587-1 9ndash18 251 686 30 718 -140 04

0587-2 20ndash29 255 886 5 677 -80 06

0587-3 31ndash40 250 1363 15 679 -106 07

0588-1 9ndash18 179 926 15 713 -139 04

0588-2 20ndash29 172 1072 2 677 -85 05

0588-3 31ndash40 175 1511 8 685 -76 04

S30B 5ndash15 223 1030 19 692 -26 13

S33C 11ndash21 210 638 21 682 17 12

S35B 5ndash15 228 1766 5 654 47 14

S67B 10ndash1983 206 1067 8 676 -1 14

S67C 20ndash2983 210 891 18 679 -27 14

S67D 30ndash3983 211 842 10 678 -22 12

S68B 10ndash20 195 819 14 676 -75 06

S68C 18ndash28 200 955 4 666 2 06




Temperature (degC)


Turbidity (NTU)

pH


(mV)


S68D 30ndash40 204 1369 3 661 -22 06

S69B 10ndash20 242 687 30 684 -78 07

S69C 20ndash30 260 689 11 687 -12 08

S69D 30ndash40 250 1633 6 665 -25 08

S70B 10ndash20 242 931 220 678 -50 05

S70C 20ndash30 250 1420 143 658 -73 07

S70D 30ndash40 256 1553 22 655 -57 08

S71B 10ndash20 247 781 29 671 -73 05

S71C 20ndash30 262 1271 311 659 -51 06

S71D 30ndash40 267 1555 10 660 -56 07

S73B 10ndash20 274 1178 27 652 -314 00

S73C 20ndash30 279 1737 17 651 -134 10

S73D 30ndash40 267 1854 33 621 -66 12

Notes a Temperature corrected to 25 degC Abbreviations ndash = not measured bls = below land surface micromhoscm = micromhos per centimeter mgL = milligrams per liter mV = millivolts NTU = nephelometric turbidity units


Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 (Reported in microgL)

Sample ID Duplicate ID Analyte Result MDL Duplicate

Result Duplicate

MDL RPD

PIN12-0580-2 PIN12-2450


14-Dioxane 160 44 190 44 17




PIN12-0581-2 PIN12-2451

11-Dichloroethanea 94J 22 12 022

11-Dichloroethenea 23U 23 047J 023

cis-12-Dichloroethenea 29J 15 36 015

Methylene chloridea 37J 32 032U 032

Vinyl chloridea 10U 10 73 010

PIN12-0582-2 PIN12-2452


11-Dichloroethenea 063J 046 072J 023

14-Dioxanea 044U 044 170 88

Acetonea 73J 38 19U 19


Naphthalenea 044U 044 023J 022



PIN12-0583-2 PIN12-2453 trans-12-Dichloroethene 22 015 26 015 17


PIN12-0587-2 PIN12-2454

11-Dichloroethene 79 023 11 023 33




Notes a An RPD was not calculated for these analytes because the result is less than 25 times the MDL Abbreviations J = Estimated value MDL = method detection limit RPD = relative percent difference U = not detected


Table 5 COPC Concentrations at the Building 100 Area (microgL)a


DCE 11-DCE

Vinyl chloride

14 Dioxane TCOPCs

CTLsb 30 700 1000 70 10 32




0555C lt016 11 043J lt023 lt01 lt022 153



0554C lt016 16 55 1 88 76 1865

0580-1 lt016 054J lt015 lt023 42 4 874

0580-2 lt016 18 5J lt023 150J 160 333

0580-3 lt016 12 088J lt023 23 28 6388


S71C lt016 18 10 029J 44 34 10629

S71D lt016 29 17 06J 60 lt044 1066

S70B lt016 15 047J lt023 75 lt022 2297

S70C lt016 19 72 047J 22 15 6367

S70D lt016 23 92 068J 19 12 6388



S69D lt016 03J lt015 lt023 lt01 lt088 03


0541 lt016 02J lt015 lt023 lt01 lt022 02

0542 lt064 lt06 lt06 lt092 lt04 lt044 ND

0549 lt016 017J lt015 lt023 lt01 lt044 017

0581-1 lt016 026J lt015 lt023 05J lt044 076

0581-2 lt016 36 lt015 047J 73 lt044 1137c

0581-3 lt032 lt03 lt03 lt046 lt02 lt044 ND

0582-1 lt016 lt015 lt015 lt023 12 lt044 12

0582-2 lt016 13 25 072J 130J 170J 31622c

0582-3 lt016 02J lt015 lt023 12 lt044 14

0539 lt016 16 13 lt023 53 38 939

0540 lt016 12 68 lt023 230 170J 4188

S73B lt016 14 05J lt023 11 lt044 129

S73C lt016 18 17 047J 230 130 39547

S73D lt016 021J lt015 lt023 047J lt088 068

0583-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0583-2 lt016 025J 22 lt023 16 lt44 1845

0583-3 lt016 lt015 lt015 lt023 lt01 lt088 ND


S67B lt016 13 33 lt023 250 91 3573

S67C lt016 48 97 064J 65 lt088 12334

S67D lt016 62 19 lt023 11 lt022 191

0580-1 lt016 054J lt015 lt023 42 4 874

0580-2 lt016 18 5J lt023 150J 160 333

0580-3 lt016 12 088J lt023 23 28 6388




DCE 11-DCE

Vinyl chloride

14 Dioxane TCOPCs

CTLsb 30 700 1000 70 10 32

0582-1 lt016 lt015 lt015 lt023 12 lt044 12

0582-2 lt016 13 25 072J 130J 170J 31622c

0582-3 lt016 02J lt015 lt023 12 lt044 14

0576-1 lt016 74 017J 2 15 36 6057

0576-2 lt016 89 021J 24 17 27J 5551

0576-3 lt016 046J lt015 lt023 12 lt088 166

0578-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0578-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0578-3 lt016 lt015 lt015 lt023 lt01 lt044 ND


0561-1 lt016 lt015 lt015 lt023 lt01 lt022 ND

0561-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0561-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

0584-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0584-2 lt016 035J lt015 lt023 lt01 lt044 035

0584-3 lt032 lt03 lt03 lt046 1J lt044 1

0585-1 53 59 041J 27 98 lt044 7721

0585-2 420 3500 17 160 420 lt88 4517

0585-3 071J 140 11 4 200 lt044 34581

0524 lt032 570 71 16 600 lt088 11931

0525 lt016 13 lt015 lt023 lt01 lt044 13


S68C lt064 53 lt06 lt092 lt04 45 98

S68D lt064 41 lt06 lt092 16 33 603



S69D lt016 03J lt015 lt023 lt01 lt088 03


0586-1 lt016 036J lt015 lt023 lt01 lt044 036

0586-2 lt016 3 lt015 lt023 29 lt044 59

0586-3 lt016 053J lt015 lt023 15 lt044 203

0587-1 lt016 50 03J 13 13 lt044 646

0587-2 lt016 190 14 79J 71 lt044 2703

0587-3 lt016 280 22 16 130 lt044 4282

0588-1 lt064 lt06 lt06 lt092 lt04 lt044 ND

0588-2 lt016 12 lt015 lt023 16 66 346

0588-3 lt016 087J lt015 lt023 14 lt044 227


0585-1 53 59 041J 27 98 lt044 7721

0585-2 420 3500 17 160 420 lt88 4517

0585-3 071J 140 11 4 200 lt044 34581

0587-1 lt016 50 03J 13 13 lt044 646

0587-2 lt016 190 14 79J 71 lt044 2703

0587-3 lt016 280 22 16 130 lt044 4282

0569-1 lt016 lt015 lt015 lt023 lt01 lt044 ND




DCE 11-DCE

Vinyl chloride

14 Dioxane TCOPCs

CTLsb 30 700 1000 70 10 32

0569-2 lt064 22J lt06 lt092 lt04 16J 38

0569-3 lt064 54 lt06 25J 37 13J 948

0572-1 lt064 lt06 lt06 lt092 lt04 lt044 ND

0572-2 lt08 200 17J 10 42 lt044 2537

0574-1 lt064 73 lt06 lt092 12 lt044 193

0574-2 lt016 17 028J lt023 18 lt044 3528

0574-3 lt016 059J lt015 lt023 1 lt044 159

0575-1 lt064 lt06 lt06 lt092 lt04 19 19

0575-2 lt064 lt06 lt06 lt092 lt04 lt022 ND

Other Wells

0551-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0551-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0565-1 lt064 lt06 lt06 lt092 lt04 lt022 ND

0565-2 lt064 lt06 lt06 lt092 lt04 lt022 ND

0565-3 lt064 lt06 lt06 lt092 lt04 lt022 ND

0568-1 lt064 lt06 lt06 lt092 lt04 lt044 ND

0568-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0568-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

0570-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0570-2 lt016 lt015 lt015 lt023 055J lt044 055

0570-3 lt016 lt015 lt015 lt023 34 lt044 34

0573-1 lt064 lt06 lt06 lt092 lt04 lt022 ND

0573-2 lt064 lt06 lt06 lt092 lt04 lt022 ND

0573-3 lt064 lt06 lt06 lt092 lt04 lt022 ND

0577-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0577-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0577-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

0579-1 lt016 lt015 lt015 lt023 lt01 lt044 ND

0579-2 lt016 lt015 lt015 lt023 lt01 lt044 ND

0579-3 lt016 lt015 lt015 lt023 lt01 lt044 ND

S30B 23 43 45 054J 10 lt044 8104d

S33C 180 920 48 33 150 lt044 1331d

S35B 5500 40000 5100 940 12000 lt044 63540d

Notes a lt values are method detection limits b The offsite CTL is a factor of 10 lower than the listed onsite (poor water quality) CTL c As explained in Section 32 this table lists the results for duplicate samples for wells 12-0581-2 and 12-0582-2 d Wells S30B S33C and S35B were sampled to track potential source depletion under the northwest corner of the

building These wells are not part of the plume stability monitoring program Abbreviations J = Estimated value ND = Not detected



Cross Section Sum of COPCs (microgL) E1 to E2 Cross Section

0555 153

0554 1865

0580 40562

S71 21289

S70 15052

S69 03


054105420549 037

0581 1213

0582 31882

05390540 5127

S73 40905

0583 1845


S67 49974

0580 40562

0582 31882

0576 11774

0578 0


0561 0

0584 135

0585 494002

05240525 11944

S68 701

S69 03


0586 829

0587 7631

0588 3687


0585 494002

0587 7631

0569 986

0572 2537

0574 5617

0575 19


Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-Section

Cross Section Area Under the Curve

March 2013 (dimensionless)

E1-E2 956

E3-E4 1262

E5-E6 1092

S1-E2 6206

S2-S3 786

S4-S5 3643

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-11291

12-S30B1436

12-S31B1422

12-S32B1433

12-S35B1412

12-S36B139

12-S37B1443

20-M0031488

12-S70B1359

12-S72B1325

12-S73B1314

12-S67B1408

12-S71B1392

12-S69B134

20-M40S1504

18-05251433

20-M0241445

23-SW011359

12-05091443

21-0502127

21-0504137

37-S0011361

15-05071378

15-05201371

15-05301369

15-05681402

15-05731396

01-P501136

02-W0051409

02-PZ051454

20-BP011426

02-PZ091388

02-PZ031549

02-PZ081401

01-P5021389

15-05951411

12-0567-11413

12-0568-1139

12-0569-11348

12-0564-11254

12-0565-11158

12-0566-11134

12-0573-11172

12-0575-11039

02-PZ101434

12-0576-11285

12-0577-11326

12-0579-11319

12-0572-1123

12-0587-11348

12-0588-11344

12-0582-1132

12-0581-11324

12-0580-11364

12-0585-11381

12-0584-11381

12-0554A1361

12-0563-11378

12-0560-11378

12-0559-11255

12-0561-11391 12-0539

1324

12-05411282

20-M0671461

20-M0691485

12-0553A1361

12-S68B1386

20-M0351465

15-M16S1439

12-0578-11355

12-0551-11211

12-0586-11353

12-0583-11309

12-0562-11337

12-0550-11198

20-M06515

12-0555A1377

21-05121342

02-PZ041537

12-0574-11089

15-E0011377

12-BR011295

11

15

15

15

14

14

14

12

12

12

12

15

15

15 15

15

13

13

13

13

13

13

14 14

14

14

14

1414

1414

14

14

14

14

15

15

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-11291

12-S30B1436

12-S31B1422

12-S32B1433

12-S35B1412

12-S36B139

12-S37B1443

20-M0031488

12-S70B1359

12-S72B1325

12-S73B1314

12-S67B1408

12-S71B1392

12-S69B134

20-M40S1504

18-05251433

20-M0241445

23-SW011359

12-05091443

21-0502127

21-0504137

37-S0011361

15-05071378

15-05201371

15-05301369

15-05681402

15-05731396

01-P501136

02-W0051409

02-PZ051454

20-BP011426

02-PZ091388

02-PZ031549

02-PZ081401

01-P5021389

15-05951411

12-0567-11413

12-0568-1139

12-0569-11348

12-0564-11254

12-0565-11158

12-0566-11134

12-0573-11172

12-0575-11039

02-PZ101434

12-0576-11285

12-0577-11326

12-0579-11319

12-0572-1123

12-0587-11348

12-0588-11344

12-0582-1132

12-0581-11324

12-0580-11364

12-0585-11381

12-0584-11381

12-0554A1361

12-0563-11378

12-0560-11378

12-0559-11255

12-0561-11391 12-0539

1324

12-05411282

20-M0671461

20-M0691485

12-0553A1361

12-S68B1386

20-M0351465

15-M16S1439

12-0578-11355

12-0551-11211

12-0586-11353

12-0583-11309

12-0562-11337

12-0550-11198

20-M06515

12-0555A1377

21-05121342

02-PZ041537

12-0574-11089

15-E0011377

12-BR011295

11

15

15

15

14

14

14

12

12

12

12

15

15

15 15

15

13

13

13

13

13

13

14 14

14

14

14

1414

1414

14

14

14

14

15

15




Plate 1 Sitewide Shallow Surficial Aquifer Contours



June 25 2013

0 150 300 Feet



12-S35B1412


Monitoring Well

Extraction Well

Surface Sample

Piezometer





Slurrywall

Fence

Road

Railroad

Tank

Building

Pond

14

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-31286

12-05201435

12-05211435

12-05181397

15-05341488

20-M0011456

20-M0051484

20-M0531446

12-S68D1366

12-S73D1314

12-S69D1323

12-S71D1365

12-S72D1329

18-05071403

20-05021437

20-M0361494

20-M38D1384

20-M40D1489

20-M0231436

18-05231418

20-M41D1463

12-S70D1347

20-M18D1463

20-M22D1483

12-05241375

12-05161352

15-M24D139

15-M33D1435

15-05351381

12-0550-31213

20-M0551417

20-M0591476

15-05691411

20-M0581475

12-05491315

12-0567-31369

12-0569-31323

12-0564-31237

12-0566-31137

12-0572-2123

12-0573-3117

02-PZ111405

12-0576-31298

12-0577-31326

12-PZ011335

12-PZ02137

12-PZ031336

12-0579-31315

12-0586-31357 12-0587-3

1351

12-0588-31344

12-0583-31314

12-0582-31318

12-0581-31321

12-0580-3136

12-0584-31373

12-0554C1359

12-0559-31101 12-0561-3

1388

12-0551-31222

15-05941385

20-M0151434

20-M0661589

20-M0681482

12-0553C1347

12-0555C1369

20-M0561428

12-S67D14

12-0574-31093

12-0565-31157

12-0575-21043

12-0560-31402

12-0585-31372

12-0562-31342 12-0563-3

1386

20-M0571461

12-0568-31367

12-0578-31349

14

11

11

15

15

15

12

12

12

14

14

14

1414

14

13

13

13

13

13

1414

14 14

14

14

14

14

15

15

14

14

WestPond

East Pond

Pond 5



Belcher Road Pond

12-0571-31286

12-05201435

12-05211435

12-05181397

15-05341488

20-M0011456

20-M0051484

20-M0531446

12-S68D1366

12-S73D1314

12-S69D1323

12-S71D1365

12-S72D1329

18-05071403

20-05021437

20-M0361494

20-M38D1384

20-M40D1489

20-M0231436

18-05231418

20-M41D1463

12-S70D1347

20-M18D1463

20-M22D1483

12-05241375

12-05161352

15-M24D139

15-M33D1435

15-05351381

12-0550-31213

20-M0551417

20-M0591476

15-05691411

20-M0581475

12-05491315

12-0567-31369

12-0569-31323

12-0564-31237

12-0566-31137

12-0572-2123

12-0573-3117

02-PZ111405

12-0576-31298

12-0577-31326

12-PZ011335

12-PZ02137

12-PZ031336

12-0579-31315

12-0586-31357 12-0587-3

1351

12-0588-31344

12-0583-31314

12-0582-31318

12-0581-31321

12-0580-3136

12-0584-31373

12-0554C1359

12-0559-31101 12-0561-3

1388

12-0551-31222

15-05941385

20-M0151434

20-M0661589

20-M0681482

12-0553C1347

12-0555C1369

20-M0561428

12-S67D14

12-0574-31093

12-0565-31157

12-0575-21043

12-0560-31402

12-0585-31372

12-0562-31342 12-0563-3

1386

20-M0571461

12-0568-31367

12-0578-31349

14

11

11

15

15

15

12

12

12

14

14

14

1414

14

13

13

13

13

13

1414

14 14

14

14

14

14

15

15

14

14




Plate 2 Sitewide Deep Surficial Aquifer Contours



June 25 2013

0 150 300 Feet



18-05071403


Monitoring Well

Extraction Well

Surface Sample

Piezometer





Slurrywall

Fence

Road

Railroad

Tank

Building

Pond

14

Appendix A

Laboratory Reports

March 2013 Semiannual Monitoring

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 962



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 9




QC Data Summary 75


Lab Chronicle 103



GCMS VOA 132




Page 2 of 962










Page 3 of 962

CASE NARRATIVE







calculated results








RECEIPT


The temperatures of the 2 coolers at receipt time were 26ordm C and 31ordm C


Due to the nature of the sample matrix (foamy) a reduced aliquot size had to be used for the analysis of several samples The reporting


Due to high constituent concentration reduced aliquot sizes had to be used for the analysis of Vinyl chloride in samples PIN12-0580-2

(LDU 874) PIN12-2450 (LDU 956) PIN12-S67B (LDU 904) and PIN12-S67C (LDU 905) The reporting limits have been elevated

accordingly

Surrogates 12-Dichloroethane-d4 and Dibromofluoromethane were recovered outside the control limits biased low in the 5 mL initial

volume analysis of sample PIN12-0580-2 (LDU 874) The sample was reanalyzed with similar results indicating matrix interference as

the cause for the surrogate recovery outliers



Due to the nature of the sample matrix (foamy) a reduced aliquot size had to be used for the analysis of sample PIN12-S67C (LDU 905)

The reporting limit haS been elevated accordingly

In some cases due to high constituent concentration samples had to be analyzed using reduced aliquot sizes The reporting limits have

been elevated accordingly

Internal standard 14-Dichlorobenzene-d4 failed to meet acceptance criteria for sample PIN12-S67C (LDU 905) As this internal standard

is not associated with the analyte of interest (14-Dioxane) data are reported as is

The MSD aliquot of the MSMSD associated with batch 280-164929 exhibited the percent recovery outside the control limits The LCS

and LCSD were within control limits




Page 4 of 962




Sdg Number 13025120

GCMS VOA





J



SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39772-1 PIN12-0555A Water 03072013 1605 03092013 0930

280-39772-1MS PIN12-0555A Water 03072013 1605 03092013 0930

280-39772-1MSD PIN12-0555A Water 03072013 1605 03092013 0930

280-39772-2 PIN12-0555B Water 03072013 1640 03092013 0930

280-39772-2MS PIN12-0555B Water 03072013 1640 03092013 0930

280-39772-2MSD PIN12-0555B Water 03072013 1640 03092013 0930

280-39772-3 PIN12-0555C Water 03072013 1740 03092013 0930

280-39772-4 PIN12-0565-1 Water 03062013 0936 03092013 0930

280-39772-5 PIN12-0565-2 Water 03062013 1015 03092013 0930

280-39772-6 PIN12-0565-3 Water 03062013 1110 03092013 0930

280-39772-7 PIN12-0573-1 Water 03062013 1335 03092013 0930

280-39772-8 PIN12-0573-2 Water 03062013 1405 03092013 0930

280-39772-9 PIN12-0573-3 Water 03062013 1440 03092013 0930

280-39772-10 PIN12-0575-1 Water 03062013 1540 03092013 0930

280-39772-11 PIN12-0575-2 Water 03062013 1620 03092013 0930

280-39772-12 PIN12-0580-1 Water 03072013 0935 03092013 0930

280-39772-13 PIN12-0580-2 Water 03072013 1030 03092013 0930

280-39772-14 PIN12-0580-3 Water 03072013 1110 03092013 0930

280-39772-15 PIN12-2450 Water 03072013 1200 03092013 0930

280-39772-16 PIN12-S67B Water 03072013 1315 03092013 0930

280-39772-17 PIN12-S67C Water 03072013 1225 03092013 0930

280-39772-18 PIN12-S67D Water 03072013 1355 03092013 0930

280-39772-19 PIN99-2198 Water 03062013 1200 03092013 0930




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39772-3 PIN12-0555C



280-39772-6 PIN12-0565-3


280-39772-8 PIN12-0573-2


280-39772-10 PIN12-0575-1



280-39772-12 PIN12-0580-1




280-39772-13 PIN12-0580-2






280-39772-14 PIN12-0580-3






280-39772-15 PIN12-2450









Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39772-16 PIN12-S67B






280-39772-17 PIN12-S67C






280-39772-18 PIN12-S67D






METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120





TestAmerica Denver

Page 10 of 962

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555A

Client Matrix

280-39772-1

Water




Dilution

03142013 2211

03142013 2211

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1862D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555A

Client Matrix

280-39772-1

Water




Dilution

03142013 2211

03142013 2211

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1862D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555B

Client Matrix

280-39772-2

Water




Dilution

03142013 2234

03142013 2234

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1863D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555B

Client Matrix

280-39772-2

Water




Dilution

03142013 2234

03142013 2234

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1863D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555C

Client Matrix

280-39772-3

Water




Dilution

03152013 0116

03152013 0116

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1870D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555C

Client Matrix

280-39772-3

Water




Dilution

03152013 0116

03152013 0116

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1870D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-1

Client Matrix

280-39772-4

Water




Dilution

03152013 1426

03152013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6154D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-1

Client Matrix

280-39772-4

Water




Dilution

03152013 1426

03152013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6154D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-2

Client Matrix

280-39772-5

Water




Dilution

03152013 1445

03152013 1445

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6155D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-2

Client Matrix

280-39772-5

Water




Dilution

03152013 1445

03152013 1445

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6155D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-3

Client Matrix

280-39772-6

Water




Dilution

03152013 1504

03152013 1504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6156D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


10 J 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-3

Client Matrix

280-39772-6

Water




Dilution

03152013 1504

03152013 1504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6156D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-1

Client Matrix

280-39772-7

Water




Dilution

03152013 1232

03152013 1232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6148D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-1

Client Matrix

280-39772-7

Water




Dilution

03152013 1232

03152013 1232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6148D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-2

Client Matrix

280-39772-8

Water




Dilution

03152013 1251

03152013 1251

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6149D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


18 J 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-2

Client Matrix

280-39772-8

Water




Dilution

03152013 1251

03152013 1251

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6149D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-3

Client Matrix

280-39772-9

Water




Dilution

03152013 1310

03152013 1310

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6150D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-3

Client Matrix

280-39772-9

Water




Dilution

03152013 1310

03152013 1310

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6150D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-1

Client Matrix

280-39772-10

Water




Dilution

03152013 1329

03152013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6151D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


83 J 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-1

Client Matrix

280-39772-10

Water




Dilution

03152013 1329

03152013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6151D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-2

Client Matrix

280-39772-11

Water




Dilution

03152013 1348

03152013 1348

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6152D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-2

Client Matrix

280-39772-11

Water




Dilution

03152013 1348

03152013 1348

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6152D

5 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-1

Client Matrix

280-39772-12

Water




Dilution

03152013 0139

03152013 0139

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1871D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-1

Client Matrix

280-39772-12

Water




Dilution

03152013 0139

03152013 0139

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1871D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03152013 0202

03152013 0202

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1872D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03152013 0202

03152013 0202

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1872D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03152013 2140

03152013 2140

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1919D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method







76 77 - 120XDibromofluoromethane (Surr)


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-3

Client Matrix

280-39772-14

Water




Dilution

03152013 0225

03152013 0225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1873D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-3

Client Matrix

280-39772-14

Water




Dilution

03152013 0225

03152013 0225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1873D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 0248

03152013 0248

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1874D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 0248

03152013 0248

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1874D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 2203

03152013 2203

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1920D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03152013 0311

03152013 0311

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1875D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03152013 0311

03152013 0311

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1875D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03152013 2226

03152013 2226

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1921D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03152013 0333

03152013 0333

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1876D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03152013 0333

03152013 0333

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1876D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03162013 0524

03162013 0524

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1939D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165112

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67D

Client Matrix

280-39772-18

Water




Dilution

03152013 0356

03152013 0356

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1877D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67D

Client Matrix

280-39772-18

Water




Dilution

03152013 0356

03152013 0356

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR1877D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164920

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2198

Client Matrix

280-39772-19

Water




Dilution

03152013 1407

03152013 1407

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6153D

20 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2198

Client Matrix

280-39772-19

Water




Dilution

03152013 1407

03152013 1407

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

g2_6153D

20 mL

20 mL

5030B

VMS_G2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164934

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555A

Client Matrix

280-39772-1

Water




Dilution

03122013 2146

03122013 2146

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3715D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555B

Client Matrix

280-39772-2

Water




Dilution

03122013 2204

03122013 2204

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3716D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0555C

Client Matrix

280-39772-3

Water




Dilution

03122013 2256

03122013 2256

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3719D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-1

Client Matrix

280-39772-4

Water




Dilution

03122013 2314

03122013 2314

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3720D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-2

Client Matrix

280-39772-5

Water




Dilution

03122013 2331

03122013 2331

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3721D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0565-3

Client Matrix

280-39772-6

Water




Dilution

03122013 2349

03122013 2349

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3722D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-1

Client Matrix

280-39772-7

Water




Dilution

03132013 0006

03132013 0006

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3723D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-2

Client Matrix

280-39772-8

Water




Dilution

03132013 0024

03132013 0024

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3724D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0573-3

Client Matrix

280-39772-9

Water




Dilution

03132013 0041

03132013 0041

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3725D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-1

Client Matrix

280-39772-10

Water




Dilution

03132013 0059

03132013 0059

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3726D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


19 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0575-2

Client Matrix

280-39772-11

Water




Dilution

03132013 0116

03132013 0116

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3727D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-1

Client Matrix

280-39772-12

Water




Dilution

03132013 0134

03132013 0134

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3728D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164432

NA

Analysis Method

Prep Method


40 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-2

Client Matrix

280-39772-13

Water




Dilution

03132013 2100

03132013 2100

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3741D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


160 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0580-3

Client Matrix

280-39772-14

Water




Dilution

03152013 0323

03152013 0323

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3795D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


28 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2450

Client Matrix

280-39772-15

Water




Dilution

03152013 0341

03152013 0341

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3796D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


190 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67B

Client Matrix

280-39772-16

Water




Dilution

03132013 2153

03132013 2153

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3744D

2 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


91 102214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67C

Client Matrix

280-39772-17

Water




Dilution

03162013 0420

03162013 0420

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3844D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S67D

Client Matrix

280-39772-18

Water




Dilution

03142013 0434

03142013 0434

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3767D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39772-1 PIN12-0555A 85 75 96 90

280-39772-2 PIN12-0555B 89 84 92 89

280-39772-3 PIN12-0555C 106 101 105 103

280-39772-4 PIN12-0565-1 94 87 94 88

280-39772-5 PIN12-0565-2 90 87 91 90

280-39772-6 PIN12-0565-3 94 87 94 90

280-39772-7 PIN12-0573-1 90 85 93 90

280-39772-8 PIN12-0573-2 91 85 95 91

280-39772-9 PIN12-0573-3 92 87 93 89

280-39772-10 PIN12-0575-1 92 87 95 88

280-39772-11 PIN12-0575-2 92 88 94 90

280-39772-12 PIN12-0580-1 92 89 88 84

280-39772-13 PIN12-0580-2 94 94 89 88

280-39772-13 DL PIN12-0580-2 DL 76X 67X 88 85

280-39772-14 PIN12-0580-3 100 97 99 97

280-39772-15 PIN12-2450 96 98 94 91

280-39772-15 DL PIN12-2450 DL 83 72 96 89

280-39772-16 PIN12-S67B 89 86 88 84

280-39772-16 DL PIN12-S67B DL 80 70 91 83

280-39772-17 PIN12-S67C 100 97 100 98

280-39772-17 DL PIN12-S67C DL 95 80 100 90

280-39772-18 PIN12-S67D 93 87 92 89

280-39772-19 PIN99-2198 94 85 95 86

MB 280-1649205 93 89 94 90

MB 280-1649347 86 83 95 88

MB 280-1651125 82 73 92 84

LCS 280-1649204 93 92 92 92

LCS 280-1649346 88 83 95 88

LCS 280-1651124 84 82 94 86






TestAmerica Denver

Page 71 of 962



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39772-1 MS PIN12-0555A MS 89 84 92 88

280-39751-I-1 MS 91 87 99 86

280-39756-O-16 MS 89 83 90 87

280-39772-1 MSD PIN12-0555A MSD 89 85 90 88

280-39751-I-1 MSD 93 87 98 86

280-39756-O-16 MSD 91 89 91 89






TestAmerica Denver

Page 72 of 962



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39772-1 PIN12-0555A 99

280-39772-2 PIN12-0555B 96

280-39772-3 PIN12-0555C 94

280-39772-4 PIN12-0565-1 96

280-39772-5 PIN12-0565-2 97

280-39772-6 PIN12-0565-3 102

280-39772-7 PIN12-0573-1 100

280-39772-8 PIN12-0573-2 103

280-39772-9 PIN12-0573-3 101

280-39772-10 PIN12-0575-1 103

280-39772-11 PIN12-0575-2 102

280-39772-12 PIN12-0580-1 102

280-39772-13 PIN12-0580-2 108

280-39772-14 PIN12-0580-3 103

280-39772-15 PIN12-2450 108

280-39772-16 PIN12-S67B 99

280-39772-17 PIN12-S67C 120

280-39772-18 PIN12-S67D 114

MB 280-1644325 95

MB 280-1646705 105

MB 280-16492917 99

MB 280-1651115 99

LCS 280-1644323 92

LCS 280-1646703 106

LCS 280-16492915 102

LCS 280-1651113 103

LCSD 280-1644324 94

LCSD 280-1646704 103

LCSD 280-16492916 97



TestAmerica Denver

Page 73 of 962



Sdg Number 13025120




Client Matrix Water


DCA

Rec

LCSD 280-1651114 105

280-39772-2 MS PIN12-0555B MS 96

280-39873-C-4 MS 97

280-39873-A-2 MS 98

280-39772-2 MSD PIN12-0555B MSD 98

280-39873-C-4 MSD 100

280-39873-A-2 MSD 102



TestAmerica Denver

Page 74 of 962



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1859D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1649205


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164920

Prep Date

Leach Date

03142013 2102

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1859D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1649205


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164920

Prep Date

Leach Date

03142013 2102

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR1858D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1649204


Analysis Batch

Prep Batch

Leach Batch

280-164920

NA

NA

Prep Date

Leach Date

03142013 2039

NA


500 450 90 74 - 135Benzene




500 509 102 76 - 120Chloroform


500 456 91 75 - 13511-Dichloroethane


500 515 103 71 - 13611-Dichloroethene


500 457 91 72 - 120Ethylbenzene



500 459 92 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR1864D

20 mL

20 mL

RR1865D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39772-1

280-39772-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03142013 2258

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164920

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2321

03142013 2321

NA

Analysis Batch

Prep Batch

Leach Batch

280-164920

NA

NA

03142013 2258


Rec


96 87 74 - 135 10 20Benzene



95 85 76 - 135 11 20Chlorobenzene

107 97 76 - 120 10 20Chloroform


95 86 75 - 135 10 2111-Dichloroethane


111 99 71 - 136 11 2011-Dichloroethene


103 92 72 - 120 11 26Ethylbenzene



100 91 73 - 120 10 20Toluene





Toluene-d8 (Surr) 92 90 80 - 125






Sdg Number 13025120

Water

03142013 2258 03142013 2321



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03142013 2258

NA

Analysis Date

Prep Date

Leach Date

03142013 2321

NA

Amount

Sample



016 U 500 500 479 433Benzene




016 U 500 500 533 484Chloroform






016 U 500 500 513 461Ethylbenzene



017 U 500 500 502 454Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

g2_6134D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_G2MB 280-1649347


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164934

Prep Date

Leach Date

03152013 0716

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

g2_6134D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_G2MB 280-1649347


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164934

Prep Date

Leach Date

03152013 0716

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

g2_6133D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_G2LCS 280-1649346


Analysis Batch

Prep Batch

Leach Batch

280-164934

NA

NA

Prep Date

Leach Date

03152013 0650

NA


500 406 81 74 - 135Benzene




500 396 79 76 - 120Chloroform


500 408 82 75 - 13511-Dichloroethane


500 447 89 71 - 13611-Dichloroethene


500 425 85 72 - 120Ethylbenzene



500 423 85 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

g2_6139D

20 mL

20 mL

g2_6140D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_G2

VMS_G2

280-39751-I-1 MS

280-39751-I-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0940

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164934

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0959

03152013 0959

NA

Analysis Batch

Prep Batch

Leach Batch

280-164934

NA

NA

03152013 0940


Rec


86 84 74 - 135 2 20Benzene




86 84 76 - 120 3 20Chloroform


90 87 75 - 135 3 2111-Dichloroethane


97 95 71 - 136 2 2011-Dichloroethene


90 89 72 - 120 1 26Ethylbenzene



87 86 73 - 120 2 20Toluene





Toluene-d8 (Surr) 99 98 80 - 125






Sdg Number 13025120

Water

03152013 0940 03152013 0959



Method 8260B

Preparation 5030B

Units ugL280-39751-I-1 MS 280-39751-I-1 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0940

NA

Analysis Date

Prep Date

Leach Date

03152013 0959

NA

Amount

Sample



016 U 500 500 432 422Benzene




016 U 500 500 428 418Chloroform






016 U 500 500 448 443Ethylbenzene



017 U 500 500 437 429Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1914D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1651125


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165112

Prep Date

Leach Date

03152013 1939

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR1914D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1651125


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165112

Prep Date

Leach Date

03152013 1939

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR1913D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1651124


Analysis Batch

Prep Batch

Leach Batch

280-165112

NA

NA

Prep Date

Leach Date

03152013 1916

NA


500 525 105 74 - 135Benzene




500 481 96 76 - 120Chloroform


500 477 95 75 - 13511-Dichloroethane


500 569 114 71 - 13611-Dichloroethene


500 523 105 72 - 120Ethylbenzene



500 513 103 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR1916D

20 mL

20 mL

RR1917D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39756-O-16 MS

280-39756-O-16 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 2030

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165112

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2053

03152013 2053

NA

Analysis Batch

Prep Batch

Leach Batch

280-165112

NA

NA

03152013 2030


Rec


99 92 74 - 135 7 20Benzene




96 92 76 - 120 4 20Chloroform


92 84 75 - 135 9 2111-Dichloroethane


110 99 71 - 136 11 2011-Dichloroethene


95 89 72 - 120 6 26Ethylbenzene



98 94 73 - 120 4 20Toluene





Toluene-d8 (Surr) 90 91 80 - 125






Sdg Number 13025120

Water

03152013 2030 03152013 2053



Method 8260B

Preparation 5030B

Units ugL280-39756-O-16 MS 280-39756-O-16 MSDMS Lab Sample ID MSD Lab Sample ID

Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 2030

NA

Analysis Date

Prep Date

Leach Date

03152013 2053

NA

Amount

Sample



016 U 500 500 493 460Benzene




016 U 500 500 482 462Chloroform






016 U 500 500 474 446Ethylbenzene



017 U 500 500 492 472Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3709D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1644325


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164432

Prep Date

Leach Date

03122013 1959

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3707D

20 mL

20 mL

E3708D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1644323

LCSD 280-1644324

Analysis Date

Prep Date

Leach Date

03122013 1924

03122013 1924

NA

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

Analysis Date

Prep Date

Leach Date

03122013 1942

03122013 1942

NA

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA


Rec

8985 25 - 141 4 2014-Dioxane






Sdg Number 13025120

Water

03122013 1924


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03122013 1924

Analysis Date

Prep Date

Leach Date

03122013 1942

03122013 1942

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443426500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3717D

20 mL

20 mL

E3718D

20 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39772-2

280-39772-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03122013 2221

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

Analysis Date

Prep Date

Leach Date

03122013 2239

03122013 2239

NA

Analysis Batch

Prep Batch

Leach Batch

280-164432

NA

NA

03122013 2221


Rec


94 97 25 - 141 3 2014-Dioxane






Sdg Number 13025120

Water

03122013 2221 03122013 2239



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03122013 2221

NA

Analysis Date

Prep Date

Leach Date

03122013 2239

NA

Amount

Sample



022 U 500 500 470 48314-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3740D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1646705


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164670

Prep Date

Leach Date

03132013 2042

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3738D

20 mL

20 mL

E3739D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1646703

LCSD 280-1646704

Analysis Date

Prep Date

Leach Date

03132013 2007

03132013 2007

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA


Rec

7883 25 - 141 7 2014-Dioxane






Sdg Number 13025120

Water

03132013 2007


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03132013 2007

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

390417500 50014-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3783D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16492917


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164929

Prep Date

Leach Date

03142013 2354

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3781D

20 mL

20 mL

E3782D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16492915

LCSD 280-16492916

Analysis Date

Prep Date

Leach Date

03142013 2319

03142013 2319

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA


Rec

8980 25 - 141 10 2014-Dioxane






Sdg Number 13025120

Water

03142013 2319


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03142013 2319

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443400500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3787D

1 mL

20 mL

E3788D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-C-4 MS

280-39873-C-4 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0104

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

03152013 0121

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

03152013 0104


Rec


125 154 25 - 141 10 20 F14-Dioxane






Sdg Number 13025120

Water

03152013 0104 03152013 0121



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0104

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

NA

Amount

Sample



170 100 100 292 322 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3822D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1651115


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165111

Prep Date

Leach Date

03152013 1916

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3820D

20 mL

20 mL

E3821D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1651113

LCSD 280-1651114

Analysis Date

Prep Date

Leach Date

03152013 1841

03152013 1841

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA


Rec

8278 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1841


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03152013 1841

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

409391500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3824D

10 mL

20 mL

E3825D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-A-2 MS

280-39873-A-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 1951

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

03152013 2009

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

03152013 1951


Rec


89 94 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1951 03152013 2009



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 1951

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

NA

Amount

Sample



044 U 100 100 895 94414-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0555A 8260B SIM280-39772-1 T

WaterPIN12-0555B 8260B SIM280-39772-2 T



WaterPIN12-0555C 8260B SIM280-39772-3 T

WaterPIN12-0565-1 8260B SIM280-39772-4 T

WaterPIN12-0565-2 8260B SIM280-39772-5 T

WaterPIN12-0565-3 8260B SIM280-39772-6 T

WaterPIN12-0573-1 8260B SIM280-39772-7 T

WaterPIN12-0573-2 8260B SIM280-39772-8 T

WaterPIN12-0573-3 8260B SIM280-39772-9 T

WaterPIN12-0575-1 8260B SIM280-39772-10 T

WaterPIN12-0575-2 8260B SIM280-39772-11 T

WaterPIN12-0580-1 8260B SIM280-39772-12 T





WaterPIN12-0580-2 8260B SIM280-39772-13 T






WaterPIN12-0555A 8260B280-39772-1 T



WaterPIN12-0555B 8260B280-39772-2 T

WaterPIN12-0555C 8260B280-39772-3 T

WaterPIN12-0580-1 8260B280-39772-12 T

WaterPIN12-0580-2 8260B280-39772-13 T

WaterPIN12-0580-3 8260B280-39772-14 T

WaterPIN12-2450 8260B280-39772-15 T

WaterPIN12-S67B 8260B280-39772-16 T

WaterPIN12-S67C 8260B280-39772-17 T

WaterPIN12-S67D 8260B280-39772-18 T

TestAmerica Denver

Page 101 of 962





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0580-3 8260B SIM280-39772-14 T

WaterPIN12-2450 8260B SIM280-39772-15 T






Matrix Spike Water 8260B280-39751-I-1 MS T

Matrix Spike Duplicate Water 8260B280-39751-I-1 MSD T

WaterPIN12-0565-1 8260B280-39772-4 T

WaterPIN12-0565-2 8260B280-39772-5 T

WaterPIN12-0565-3 8260B280-39772-6 T

WaterPIN12-0573-1 8260B280-39772-7 T

WaterPIN12-0573-2 8260B280-39772-8 T

WaterPIN12-0573-3 8260B280-39772-9 T

WaterPIN12-0575-1 8260B280-39772-10 T

WaterPIN12-0575-2 8260B280-39772-11 T

WaterPIN99-2198 8260B280-39772-19 T











Matrix Spike Water 8260B280-39756-O-16 MS T

Matrix Spike Duplicate Water 8260B280-39756-O-16 MSD T

WaterPIN12-0580-2 8260B280-39772-13DL T

WaterPIN12-2450 8260B280-39772-15DL T

WaterPIN12-S67B 8260B280-39772-16DL T

WaterPIN12-S67C 8260B280-39772-17DL T

Report Basis

T = Total

TestAmerica Denver

Page 102 of 962

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 1510



Data Summaries 4

Report Narrative 4

Data Qualifiers 6

Sample Summary 7

Executive Summary 8

Method Summary 12




QC Data Summary 103


Lab Chronicle 140



GCMS VOA 196




Page 2 of 1510










Page 3 of 1510

CASE NARRATIVE







calculated results








RECEIPT


ice The temperature of the cooler at receipt was 17ordm C


In some cases due to high concentrations of target analytes andor the nature of the sample matrix (foamy) reduced aliquot sizes had to

be used for the analysis of samples The reporting limits have been elevated accordingly To provide the lowest possible detection limits


Sample PIN12-0539 (LDU 854) was received at the laboratory with insufficient preservation measuring a pH of 7 If samples are not

preserved to a pH of 20 and analyses are performed outside a 7 day holding time experimental evidence suggests that some aromatic

compounds in wastewater samples notably benzene toluene and ethylbenzene are susceptible to biological degradation The sample

was analyzed within the normal 14 day holding time but outside a 7 day holding time

The MSD aliquot of the MSMSD performed on sample PIN12-0524 (LDU 852) in batch 280-165236 exhibited spike compound recoveries


The accuracy and precision of the MSMSD associated with batch 280-165434 could not be reliably evaluated for some compounds as

the concentrations present in the parent sample are 4 times greater than the matrix spike concentrations In addition MS andor MSD

concentrations are present above the instrument calibration range for some compounds The LCS and LCSD were within control limits

The MSMSD associated with batch 280-165627 exhibited percent recoveries outside the control limits biased high for

11-Dichloroethane The LCS was within control limits



In some cases due to the nature of the sample matrix (foamy) andor due to high constituent concentration samples had to be analyzed

using reduced aliquot sizes The reporting limits have been elevated accordingly

Surrogate 12-Dichloroethane-d4 was recovered outside the control limits biased high in samples PIN12-0581-1 (LDU-876)

PIN12-0581-2 (LDU 877) and PIN12-0582-1 (LDU 879) As no detectable concentrations are present in the sampleS data are reported

as is

In some cases the internal standard response for 14-Dichlorobenzene-d4 was outside acceptance criteria for samples in batch

280-165111 As this internal standard is not associated with the analyte of interest (14-Dioxane) data are reported as is



The MSD aliquot of the MSMSD performed on sample PIN12-0540 (LDU 855) in batch 280-164929 exhibited the percent recovery

outside the control limits biased high The LCS and LCSD were within control limits

Page 4 of 1510

The RPD limit was exceeded in the MSMSD associated with batch 280-165812 Method precision and accuracy have been verified by

the acceptable LCSLCSD analysis data




Page 5 of 1510




Sdg Number 13025120

GCMS VOA



MS MSD The analyte present in the original sample is 4 times greater

than the matrix spike concentration therefore control limits are not

applicable

4




J




SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39873-1 PIN12-0524 Water 03092013 0748 03132013 0900

280-39873-1MS PIN12-0524 Water 03092013 0748 03132013 0900

280-39873-1MSD PIN12-0524 Water 03092013 0748 03132013 0900

280-39873-2 PIN12-0525 Water 03092013 0826 03132013 0900

280-39873-2MS PIN12-0525 Water 03092013 0826 03132013 0900

280-39873-2MSD PIN12-0525 Water 03092013 0826 03132013 0900

280-39873-3 PIN12-0539 Water 03082013 1635 03132013 0900

280-39873-4 PIN12-0540 Water 03082013 1548 03132013 0900

280-39873-5 PIN12-0541 Water 03082013 1241 03132013 0900

280-39873-6 PIN12-0542 Water 03082013 1310 03132013 0900

280-39873-7 PIN12-0549 Water 03082013 1413 03132013 0900

280-39873-8 PIN12-0554A Water 03082013 0919 03132013 0900

280-39873-9 PIN12-0554B Water 03082013 1005 03132013 0900

280-39873-10 PIN12-0554C Water 03082013 1110 03132013 0900

280-39873-11 PIN12-0581-1 Water 03112013 0851 03132013 0900

280-39873-12 PIN12-0581-2 Water 03112013 0923 03132013 0900

280-39873-13 PIN12-0581-3 Water 03112013 1025 03132013 0900

280-39873-14 PIN12-0582-1 Water 03112013 1147 03132013 0900

280-39873-15 PIN12-0582-2 Water 03112013 1218 03132013 0900

280-39873-16 PIN12-0582-3 Water 03112013 1253 03132013 0900

280-39873-17 PIN12-0585-3 Water 03092013 1133 03132013 0900

280-39873-18 PIN12-2451 Water 03112013 1200 03132013 0900

280-39873-19 PIN12-2452 Water 03112013 1210 03132013 0900

280-39873-20 PIN12-S71B Water 03092013 0908 03132013 0900

280-39873-21 PIN12-S71C Water 03092013 0936 03132013 0900

280-39873-22 PIN12-S71D Water 03092013 1026 03132013 0900

280-39873-23 PIN12-S73B Water 03112013 1430 03132013 0900

280-39873-24 PIN12-S73C Water 03112013 1603 03132013 0900

280-39873-25 PIN12-S73D Water 03112013 1648 03132013 0900

280-39873-26 PIN99-2448 Water 03082013 0900 03132013 0900




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-1 PIN12-0524






280-39873-2 PIN12-0525


280-39873-3 PIN12-0539







280-39873-4 PIN12-0540







280-39873-5 PIN12-0541



280-39873-6 PIN12-0542


280-39873-7 PIN12-0549







Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-8 PIN12-0554A


280-39873-10 PIN12-0554C








280-39873-11 PIN12-0581-1





280-39873-12 PIN12-0581-2




280-39873-13 PIN12-0581-3


280-39873-14 PIN12-0582-1




280-39873-15 PIN12-0582-2










Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-16 PIN12-0582-3



280-39873-17 PIN12-0585-3






10 ugL 8260B071 JTrichloroethene


280-39873-18 PIN12-2451





280-39873-19 PIN12-2452





10 ugL 8260B023 JNaphthalene



280-39873-21 PIN12-S71C










Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39873-22 PIN12-S71D






280-39873-23 PIN12-S73B





280-39873-24 PIN12-S73C







280-39873-25 PIN12-S73D




METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120


Meier Greg P GPMSW846 8260B



TestAmerica Denver

Page 13 of 1510

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03182013 1142

03182013 1142

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5339D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


38 U 2038Acetone

19 J 20032Benzene





































34 U 10342-Hexanone







034 U 20034Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03182013 1142

03182013 1142

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5339D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method





034 U 20034Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03182013 1202

03182013 1202

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5340D

1 mL

20 mLRun Type DL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0525

Client Matrix

280-39873-2

Water




Dilution

03182013 1304

03182013 1304

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5343D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0525

Client Matrix

280-39873-2

Water




Dilution

03182013 1304

03182013 1304

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5343D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03182013 1324

03182013 1324

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5344D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


47 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03182013 1324

03182013 1324

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5344D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03192013 1338

03192013 1338

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2023D

5 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03182013 1345

03182013 1345

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5345D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


57 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03182013 1345

03182013 1345

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5345D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03192013 1203

03192013 1203

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2019D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0541

Client Matrix

280-39873-5

Water




Dilution

03182013 1426

03182013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5347D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


10 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0541

Client Matrix

280-39873-5

Water




Dilution

03182013 1426

03182013 1426

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5347D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0542

Client Matrix

280-39873-6

Water




Dilution

03192013 1536

03192013 1536

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2028D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0542

Client Matrix

280-39873-6

Water




Dilution

03192013 1536

03192013 1536

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2028D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0549

Client Matrix

280-39873-7

Water




Dilution

03182013 1507

03182013 1507

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5349D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


14 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0549

Client Matrix

280-39873-7

Water




Dilution

03182013 1507

03182013 1507

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5349D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554A

Client Matrix

280-39873-8

Water




Dilution

03182013 1527

03182013 1527

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5350D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


98 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554A

Client Matrix

280-39873-8

Water




Dilution

03182013 1527

03182013 1527

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5350D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554B

Client Matrix

280-39873-9

Water




Dilution

03192013 1600

03192013 1600

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2029D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554B

Client Matrix

280-39873-9

Water




Dilution

03192013 1600

03192013 1600

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2029D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03182013 1607

03182013 1607

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5352D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


67 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03182013 1607

03182013 1607

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5352D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method





017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03182013 1627

03182013 1627

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5353D

10 mL

20 mLRun Type DL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-1

Client Matrix

280-39873-11

Water




Dilution

03182013 1648

03182013 1648

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5354D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


87 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-1

Client Matrix

280-39873-11

Water




Dilution

03182013 1648

03182013 1648

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5354D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-2

Client Matrix

280-39873-12

Water




Dilution

03192013 1250

03192013 1250

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2021D

2 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 10019Acetone

16 U 1016Benzene




19 U 1019Bromoform











16 U 1016Chloroform























17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-2

Client Matrix

280-39873-12

Water




Dilution

03192013 1250

03192013 1250

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2021D

2 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


17 U 1017Styrene




17 U 1017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-3

Client Matrix

280-39873-13

Water




Dilution

03182013 1728

03182013 1728

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5356D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


93 J 2038Acetone

032 U 20032Benzene






































34 U 10342-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-3

Client Matrix

280-39873-13

Water




Dilution

03182013 1728

03182013 1728

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5356D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


034 U 20034Styrene




034 U 20034Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-1

Client Matrix

280-39873-14

Water




Dilution

03182013 1748

03182013 1748

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5357D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


73 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-1

Client Matrix

280-39873-14

Water




Dilution

03182013 1748

03182013 1748

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5357D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03182013 1808

03182013 1808

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5358D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


73 J 2038Acetone

032 U 20032Benzene






































34 U 10342-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03182013 1808

03182013 1808

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5358D

10 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165236

NA

Analysis Method

Prep Method


034 U 20034Styrene




034 U 20034Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03192013 1314

03192013 1314

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2022D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-3

Client Matrix

280-39873-16

Water




Dilution

03192013 1042

03192013 1042

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0948D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-3

Client Matrix

280-39873-16

Water




Dilution

03192013 1042

03192013 1042

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0948D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03192013 1127

03192013 1127

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0950D

4 mL

20 mLRun Type DL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03202013 0810

03202013 0810

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2931D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene





































39 J 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03202013 0810

03202013 0810

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2931D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method





017 U 10017Toluene





071 J 10016Trichloroethene













Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2451

Client Matrix

280-39873-18

Water




Dilution

03192013 1448

03192013 1448

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0959D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2451

Client Matrix

280-39873-18

Water




Dilution

03192013 1448

03192013 1448

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0959D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03192013 1510

03192013 1510

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0960D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone





023 J 10022Naphthalene



Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03192013 1510

03192013 1510

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0960D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03202013 0833

03202013 0833

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2932D

5 mL

20 mLRun Type DL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71B

Client Matrix

280-39873-20

Water




Dilution

03192013 1554

03192013 1554

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0962D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71B

Client Matrix

280-39873-20

Water




Dilution

03192013 1554

03192013 1554

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0962D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71C

Client Matrix

280-39873-21

Water




Dilution

03192013 1617

03192013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0963D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71C

Client Matrix

280-39873-21

Water




Dilution

03192013 1617

03192013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0963D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71D

Client Matrix

280-39873-22

Water




Dilution

03202013 0857

03202013 0857

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2933D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71D

Client Matrix

280-39873-22

Water




Dilution

03202013 0857

03202013 0857

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2933D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73B

Client Matrix

280-39873-23

Water




Dilution

03192013 1701

03192013 1701

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0965D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73B

Client Matrix

280-39873-23

Water




Dilution

03192013 1701

03192013 1701

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0965D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03202013 0919

03202013 0919

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2934D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03202013 0919

03202013 0919

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2934D

20 mL

20 mL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03202013 0942

03202013 0942

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

Z2935D

4 mL

20 mLRun Type DL

5030B

VMS_Z

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165627

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73D

Client Matrix

280-39873-25

Water




Dilution

03192013 1745

03192013 1745

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0967D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73D

Client Matrix

280-39873-25

Water




Dilution

03192013 1745

03192013 1745

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0967D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2448

Client Matrix

280-39873-26

Water




Dilution

03192013 1149

03192013 1149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0951D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2448

Client Matrix

280-39873-26

Water




Dilution

03192013 1149

03192013 1149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

H0951D

20 mL

20 mL

5030B

VMS_H

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165434

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0524

Client Matrix

280-39873-1

Water




Dilution

03222013 2012

03222013 2012

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4018D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0525

Client Matrix

280-39873-2

Water




Dilution

03152013 1934

03152013 1934

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3823D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0539

Client Matrix

280-39873-3

Water




Dilution

03152013 0029

03152013 0029

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3785D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


38 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0540

Client Matrix

280-39873-4

Water




Dilution

03152013 0046

03152013 0046

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3786D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


170 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0541

Client Matrix

280-39873-5

Water




Dilution

03142013 0030

03142013 0030

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3753D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0542

Client Matrix

280-39873-6

Water




Dilution

03152013 0139

03152013 0139

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3789D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0549

Client Matrix

280-39873-7

Water




Dilution

03152013 0156

03152013 0156

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3790D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554A

Client Matrix

280-39873-8

Water




Dilution

03142013 0122

03142013 0122

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3756D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554B

Client Matrix

280-39873-9

Water




Dilution

03152013 0214

03152013 0214

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3791D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0554C

Client Matrix

280-39873-10

Water




Dilution

03152013 0231

03152013 0231

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3792D

4 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


76 501114-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-1

Client Matrix

280-39873-11

Water




Dilution

03152013 2028

03152013 2028

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3826D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-2

Client Matrix

280-39873-12

Water




Dilution

03152013 2323

03152013 2323

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3827D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0581-3

Client Matrix

280-39873-13

Water




Dilution

03202013 2244

03202013 2244

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3932D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-1

Client Matrix

280-39873-14

Water




Dilution

03152013 2358

03152013 2358

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3829D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-2

Client Matrix

280-39873-15

Water




Dilution

03202013 2302

03202013 2302

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3933D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0582-3

Client Matrix

280-39873-16

Water




Dilution

03162013 0033

03162013 0033

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3831D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-3

Client Matrix

280-39873-17

Water




Dilution

03152013 0249

03152013 0249

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3793D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2451

Client Matrix

280-39873-18

Water




Dilution

03162013 0051

03162013 0051

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3832D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2452

Client Matrix

280-39873-19

Water




Dilution

03222013 2029

03222013 2029

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4019D

05 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


170 408814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71B

Client Matrix

280-39873-20

Water




Dilution

03142013 0232

03142013 0232

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3760D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164670

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71C

Client Matrix

280-39873-21

Water




Dilution

03152013 0306

03152013 0306

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3794D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


34 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S71D

Client Matrix

280-39873-22

Water




Dilution

03162013 0126

03162013 0126

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3834D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73B

Client Matrix

280-39873-23

Water




Dilution

03162013 0143

03162013 0143

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3835D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73C

Client Matrix

280-39873-24

Water




Dilution

03222013 2046

03222013 2046

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4020D

2 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


130 102214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S73D

Client Matrix

280-39873-25

Water




Dilution

03222013 2104

03222013 2104

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4021D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39873-1 PIN12-0524 105 109 97 101

280-39873-1 DL PIN12-0524 DL 114 121 101 101

280-39873-2 PIN12-0525 112 126 98 109

280-39873-3 PIN12-0539 103 113 90 95

280-39873-3 DL PIN12-0539 DL 82 74 90 87

280-39873-4 PIN12-0540 105 113 91 94

280-39873-4 DL PIN12-0540 DL 85 75 95 93

280-39873-5 PIN12-0541 103 117 87 94

280-39873-6 PIN12-0542 84 75 94 87

280-39873-7 PIN12-0549 109 124 95 96

280-39873-8 PIN12-0554A 115 127 92 99

280-39873-9 PIN12-0554B 85 76 90 88

280-39873-10 PIN12-0554C 111 123 95 95

280-39873-10 DL PIN12-0554C DL 108 120 92 93

280-39873-11 PIN12-0581-1 95 110 82 82

280-39873-12 PIN12-0581-2 82 75 92 85

280-39873-13 PIN12-0581-3 112 125 94 97

280-39873-14 PIN12-0582-1 107 121 89 89

280-39873-15 PIN12-0582-2 110 119 92 90

280-39873-15 DL PIN12-0582-2 DL 87 77 95 89

280-39873-16 PIN12-0582-3 111 127 101 102

280-39873-17 DL PIN12-0585-3 DL 107 117 95 97

280-39873-17 PIN12-0585-3 99 101 119 96

280-39873-18 PIN12-2451 110 127 106 101

280-39873-19 PIN12-2452 106 123 94 96

280-39873-19 DL PIN12-2452 DL 101 101 98 98

280-39873-20 PIN12-S71B 105 120 94 99

280-39873-21 PIN12-S71C 109 126 99 99

280-39873-22 PIN12-S71D 116 119 92 92






TestAmerica Denver

Page 99 of 1510



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39873-23 PIN12-S73B 108 121 95 98

280-39873-24 PIN12-S73C 97 99 91 92

280-39873-24 DL PIN12-S73C DL 95 94 92 92

280-39873-25 PIN12-S73D 108 122 98 95

280-39873-26 PIN99-2448 112 125 102 102

MB 280-16523632 105 113 93 97

MB 280-1654345 108 117 98 100

MB 280-1654515 82 70 98 90

MB 280-1656275 100 100 100 98

LCS 280-16523631 106 112 92 89

LCS 280-1654344 106 121 107 97

LCS 280-1654514 85 74 98 94

LCS 280-1656274 97 96 103 93

280-39873-1 MS PIN12-0524 MS 105 114 93 95

280-39974-C-1 MS 108 122 113 106

280-39875-B-1 MS 84 74 96 90

280-40045-A-1 MS 97 96 96 92

280-39873-1 MSD PIN12-0524 MSD 110 117 97 97

280-39974-C-1 MSD 104 120 100 93

280-39875-B-1 MSD 86 77 96 90

280-40045-A-1 MSD 100 100 98 92






TestAmerica Denver

Page 100 of 1510



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39873-1 PIN12-0524 93

280-39873-2 PIN12-0525 99

280-39873-3 PIN12-0539 98

280-39873-4 PIN12-0540 100

280-39873-5 PIN12-0541 108

280-39873-6 PIN12-0542 103

280-39873-7 PIN12-0549 108

280-39873-8 PIN12-0554A 114

280-39873-9 PIN12-0554B 102

280-39873-10 PIN12-0554C 100

280-39873-11 PIN12-0581-1 132X

280-39873-12 PIN12-0581-2 134X

280-39873-13 PIN12-0581-3 99

280-39873-14 PIN12-0582-1 130X

280-39873-15 PIN12-0582-2 112

280-39873-16 PIN12-0582-3 112

280-39873-17 PIN12-0585-3 108

280-39873-18 PIN12-2451 121

280-39873-19 PIN12-2452 94

280-39873-20 PIN12-S71B 109

280-39873-21 PIN12-S71C 107

280-39873-22 PIN12-S71D 113

280-39873-23 PIN12-S73B 110

280-39873-24 PIN12-S73C 96

280-39873-25 PIN12-S73D 97

MB 280-1646705 105

MB 280-16492917 99

MB 280-1651115 99

MB 280-16581217 96



TestAmerica Denver

Page 101 of 1510



Sdg Number 13025120




Client Matrix Water


DCA

Rec

MB 280-1662795 93

LCS 280-1646703 106

LCS 280-16492915 102

LCS 280-1651113 103

LCS 280-16581215 100

LCS 280-1662793 97

LCSD 280-1646704 103

LCSD 280-16492916 97

LCSD 280-1651114 105

LCSD 280-16581216 96

LCSD 280-1662794 97

280-39873-2 MS PIN12-0525 MS 98

280-39873-4 MS PIN12-0540 MS 97

280-39875-D-2 MS 98

280-39986-B-5 MS 105

280-39873-2 MSD PIN12-0525 MSD 102

280-39873-4 MSD PIN12-0540 MSD 100

280-39875-D-2 MSD 101

280-39986-B-5 MSD 107



TestAmerica Denver

Page 102 of 1510



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5338D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-16523632


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165236

Prep Date

Leach Date

03182013 1050

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5338D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-16523632


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165236

Prep Date

Leach Date

03182013 1050

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

C5337D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CLCS 280-16523631


Analysis Batch

Prep Batch

Leach Batch

280-165236

NA

NA

Prep Date

Leach Date

03182013 1030

NA


500 521 104 74 - 135Benzene




500 599 120 76 - 120Chloroform


500 535 107 75 - 13511-Dichloroethane


500 591 118 71 - 13611-Dichloroethene


500 473 95 72 - 120Ethylbenzene



500 544 109 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5341D

10 mL

20 mL

C5342D

10 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-39873-1

280-39873-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03182013 1222

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165236

NA

NA

Analysis Date

Prep Date

Leach Date

03182013 1243

03182013 1243

NA

Analysis Batch

Prep Batch

Leach Batch

280-165236

NA

NA

03182013 1222


Rec


104 106 74 - 135 2 20Benzene




116 121 76 - 120 4 20 FChloroform


110 115 75 - 135 5 2111-Dichloroethane


109 112 71 - 136 1 2011-Dichloroethene


95 97 72 - 120 2 26Ethylbenzene



112 113 73 - 120 1 20Toluene





Toluene-d8 (Surr) 93 97 80 - 125






Sdg Number 13025120

Water

03182013 1222 03182013 1243



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03182013 1222

NA

Analysis Date

Prep Date

Leach Date

03182013 1243

NA

Amount

Sample



19 J 100 100 123 125Benzene


038 U 100 100 134 136 FCarbon tetrachloride


032 U 100 100 116 121 FChloroform



71 100 100 179 185trans-12-Dichloroethene



032 U 100 100 951 973Ethylbenzene



034 U 100 100 112 113Toluene

032 U 100 100 132 136 F111-Trichloroethane





Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

H0939D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_HMB 280-1654345


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165434

Prep Date

Leach Date

03192013 0722

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

H0939D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_HMB 280-1654345


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165434

Prep Date

Leach Date

03192013 0722

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

H0938D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_HLCS 280-1654344


Analysis Batch

Prep Batch

Leach Batch

280-165434

NA

NA

Prep Date

Leach Date

03192013 0700

NA


500 500 100 74 - 135Benzene



500 515 103 76 - 135Chlorobenzene

500 540 108 76 - 120Chloroform


500 527 105 75 - 13511-Dichloroethane


500 559 112 71 - 13611-Dichloroethene


500 522 104 72 - 120Ethylbenzene



500 512 102 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

H0941D

20 mL

20 mL

H0942D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_H

VMS_H

280-39974-C-1 MS

280-39974-C-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 0807

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165434

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 0829

03192013 0829

NA

Analysis Batch

Prep Batch

Leach Batch

280-165434

NA

NA

03192013 0807


Rec


99 96 74 - 135 3 20Benzene


133 77 67 - 135 10 21 4 4Carbon tetrachloride

100 97 76 - 135 4 20Chlorobenzene

124 91 76 - 120 6 20 4 4Chloroform


102 100 75 - 135 2 2111-Dichloroethane


109 104 71 - 136 4 2011-Dichloroethene


103 97 72 - 120 5 26Ethylbenzene


247 81 70 - 135 14 20 E 4 4Tetrachloroethene

103 100 73 - 120 3 20Toluene


187 -984 73 - 135 10 20 E 4 E 4Trichloroethene



Toluene-d8 (Surr) 113 100 80 - 125






Sdg Number 13025120

Water

03192013 0807 03192013 0829



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 0807

NA

Analysis Date

Prep Date

Leach Date

03192013 0829

NA

Amount

Sample



028 J 500 500 524 508Benzene


23 500 500 299 2724 4Carbon tetrachloride


24 500 500 299 2824 4Chloroform




088 J 500 500 631 60611-Dichloroethene


016 U 500 500 513 486Ethylbenzene

099 J 500 500 570 555Methylene Chloride

53 500 500 655 572E 4 4Tetrachloroethene

017 U 500 500 515 500Toluene


590 500 500 598 540E 4 E 4Trichloroethene




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2010D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1654514


Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Prep Date

Leach Date

03192013 0805

NA


500 491 98 74 - 135Benzene




500 454 91 76 - 120Chloroform


500 453 91 75 - 13511-Dichloroethane


500 545 109 71 - 13611-Dichloroethene


500 499 100 72 - 120Ethylbenzene



500 483 97 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2016D

5 mL

20 mL

RR2017D

5 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39875-B-1 MS

280-39875-B-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 1052

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

03192013 1116

NA

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

03192013 1052


Rec


91 89 74 - 135 2 20Benzene




87 84 76 - 120 5 20Chloroform


84 82 75 - 135 4 2111-Dichloroethane


101 96 71 - 136 4 2011-Dichloroethene


94 89 72 - 120 5 26Ethylbenzene



90 90 73 - 120 0 20Toluene





Toluene-d8 (Surr) 96 96 80 - 125






Sdg Number 13025120

Water

03192013 1052 03192013 1116



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 1052

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

NA

Amount

Sample



064 U 200 200 182 177Benzene




064 U 200 200 175 167Chloroform






064 U 200 200 187 179Ethylbenzene



068 U 200 200 180 179Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

Z2929D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_ZMB 280-1656275


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165627

Prep Date

Leach Date

03202013 0724

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

Z2929D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_ZMB 280-1656275


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165627

Prep Date

Leach Date

03202013 0724

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

Z2928D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_ZLCS 280-1656274


Analysis Batch

Prep Batch

Leach Batch

280-165627

NA

NA

Prep Date

Leach Date

03202013 0701

NA


500 465 93 74 - 135Benzene




500 478 96 76 - 120Chloroform


500 481 96 75 - 13511-Dichloroethane


500 557 111 71 - 13611-Dichloroethene


500 469 94 72 - 120Ethylbenzene



500 423 85 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Z2939D

20 mL

20 mL

Z2940D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_Z

VMS_Z

280-40045-A-1 MS

280-40045-A-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03202013 1115

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165627

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 1138

03202013 1138

NA

Analysis Batch

Prep Batch

Leach Batch

280-165627

NA

NA

03202013 1115


Rec


96 95 74 - 135 1 20Benzene




99 99 76 - 120 0 20Chloroform


101 100 75 - 135 1 2111-Dichloroethane


148 147 71 - 136 1 20 F F11-Dichloroethene


97 96 72 - 120 2 26Ethylbenzene



97 96 73 - 120 1 20Toluene





Toluene-d8 (Surr) 96 98 80 - 125






Sdg Number 13025120

Water

03202013 1115 03202013 1138



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03202013 1115

NA

Analysis Date

Prep Date

Leach Date

03202013 1138

NA

Amount

Sample



016 U 500 500 480 476Benzene




016 U 500 500 495 493Chloroform




023 U 500 500 742 737F F11-Dichloroethene


016 U 500 500 487 479Ethylbenzene



017 U 500 500 485 479Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3740D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1646705


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164670

Prep Date

Leach Date

03132013 2042

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3738D

20 mL

20 mL

E3739D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1646703

LCSD 280-1646704

Analysis Date

Prep Date

Leach Date

03132013 2007

03132013 2007

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NA

Analysis Batch

Prep Batch

Leach Batch

280-164670

NA

NA


Rec

7883 25 - 141 7 2014-Dioxane






Sdg Number 13025120

Water

03132013 2007


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03132013 2007

Analysis Date

Prep Date

Leach Date

03132013 2025

03132013 2025

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

390417500 50014-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3783D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16492917


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164929

Prep Date

Leach Date

03142013 2354

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3781D

20 mL

20 mL

E3782D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16492915

LCSD 280-16492916

Analysis Date

Prep Date

Leach Date

03142013 2319

03142013 2319

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA


Rec

8980 25 - 141 10 2014-Dioxane






Sdg Number 13025120

Water

03142013 2319


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03142013 2319

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443400500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3787D

1 mL

20 mL

E3788D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-4

280-39873-4

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0104

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

03152013 0121

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

03152013 0104


Rec


125 154 25 - 141 10 20 F14-Dioxane






Sdg Number 13025120

Water

03152013 0104 03152013 0121



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0104

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

NA

Amount

Sample



170 100 100 292 322 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3822D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1651115


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165111

Prep Date

Leach Date

03152013 1916

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3820D

20 mL

20 mL

E3821D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1651113

LCSD 280-1651114

Analysis Date

Prep Date

Leach Date

03152013 1841

03152013 1841

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA


Rec

8278 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1841


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03152013 1841

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

409391500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3824D

10 mL

20 mL

E3825D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-2

280-39873-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 1951

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

03152013 2009

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

03152013 1951


Rec


89 94 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1951 03152013 2009



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 1951

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

NA

Amount

Sample



044 U 100 100 895 94414-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3931D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16581217


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165812

Prep Date

Leach Date

03202013 2222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3929D

20 mL

20 mL

E3930D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16581215

LCSD 280-16581216

Analysis Date

Prep Date

Leach Date

03202013 2147

03202013 2147

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA


Rec

107106 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03202013 2147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03202013 2147

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

535532500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3940D

10 mL

20 mL

E3941D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39875-D-2 MS

280-39875-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0105

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

03212013 0122

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

03212013 0105


Rec


82 26 25 - 141 103 20 F14-Dioxane






Sdg Number 13025120

Water

03212013 0105 03212013 0122



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0105

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

NA

Amount

Sample



044 U 100 100 816 262 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4017D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1662795


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166279

Prep Date

Leach Date

03222013 1946

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4015D

20 mL

20 mL

E4016D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1662793

LCSD 280-1662794

Analysis Date

Prep Date

Leach Date

03222013 1911

03222013 1911

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA


Rec

103103 25 - 141 0 2014-Dioxane






Sdg Number 13025120

Water

03222013 1911


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03222013 1911

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

514516500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4027D

10 mL

20 mL

E4028D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39986-B-5 MS

280-39986-B-5 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 2249

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

03222013 2306

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

03222013 2249


Rec


146 225 25 - 141 17 20 E F E F14-Dioxane






Sdg Number 13025120

Water

03222013 2249 03222013 2306



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 2249

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

NA

Amount

Sample



27 100 100 419 499E F E F14-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0541 8260B SIM280-39873-5 T

WaterPIN12-0554A 8260B SIM280-39873-8 T






WaterPIN12-0539 8260B SIM280-39873-3 T

WaterPIN12-0540 8260B SIM280-39873-4 T



WaterPIN12-0542 8260B SIM280-39873-6 T

WaterPIN12-0549 8260B SIM280-39873-7 T

WaterPIN12-0554B 8260B SIM280-39873-9 T

WaterPIN12-0554C 8260B SIM280-39873-10 T

WaterPIN12-0585-3 8260B SIM280-39873-17 T






WaterPIN12-0525 8260B SIM280-39873-2 T



WaterPIN12-0581-1 8260B SIM280-39873-11 T

WaterPIN12-0581-2 8260B SIM280-39873-12 T

WaterPIN12-0582-1 8260B SIM280-39873-14 T

WaterPIN12-0582-3 8260B SIM280-39873-16 T

WaterPIN12-2451 8260B SIM280-39873-18 T



TestAmerica Denver

Page 137 of 1510





Sdg Number 13025120

Report

Basis

GCMS VOA




WaterPIN12-0524 8260B280-39873-1 T

WaterPIN12-0524 8260B280-39873-1DL T



WaterPIN12-0525 8260B280-39873-2 T

WaterPIN12-0539 8260B280-39873-3 T

WaterPIN12-0540 8260B280-39873-4 T

WaterPIN12-0541 8260B280-39873-5 T

WaterPIN12-0549 8260B280-39873-7 T

WaterPIN12-0554A 8260B280-39873-8 T

WaterPIN12-0554C 8260B280-39873-10 T

WaterPIN12-0554C 8260B280-39873-10DL T

WaterPIN12-0581-1 8260B280-39873-11 T

WaterPIN12-0581-3 8260B280-39873-13 T

WaterPIN12-0582-1 8260B280-39873-14 T

WaterPIN12-0582-2 8260B280-39873-15 T




WaterPIN12-0582-3 8260B280-39873-16 T

WaterPIN12-0585-3 8260B280-39873-17DL T

WaterPIN12-2451 8260B280-39873-18 T

WaterPIN12-2452 8260B280-39873-19 T

WaterPIN12-S71B 8260B280-39873-20 T

WaterPIN12-S71C 8260B280-39873-21 T

WaterPIN12-S73B 8260B280-39873-23 T

WaterPIN12-S73D 8260B280-39873-25 T

WaterPIN99-2448 8260B280-39873-26 T






WaterPIN12-0539 8260B280-39873-3DL T

WaterPIN12-0540 8260B280-39873-4DL T

WaterPIN12-0542 8260B280-39873-6 T

WaterPIN12-0554B 8260B280-39873-9 T

WaterPIN12-0581-2 8260B280-39873-12 T

WaterPIN12-0582-2 8260B280-39873-15DL T



TestAmerica Denver

Page 138 of 1510





Sdg Number 13025120

Report

Basis

GCMS VOA




WaterPIN12-0585-3 8260B280-39873-17 T

WaterPIN12-2452 8260B280-39873-19DL T

WaterPIN12-S71D 8260B280-39873-22 T

WaterPIN12-S73C 8260B280-39873-24 T

WaterPIN12-S73C 8260B280-39873-24DL T

Matrix Spike Water 8260B280-40045-A-1 MS T

Matrix Spike Duplicate Water 8260B280-40045-A-1 MSD T





WaterPIN12-0581-3 8260B SIM280-39873-13 T

WaterPIN12-0582-2 8260B SIM280-39873-15 T







WaterPIN12-0524 8260B SIM280-39873-1 T

WaterPIN12-2452 8260B SIM280-39873-19 T





Report Basis

T = Total

TestAmerica Denver

Page 139 of 1510

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 1167



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 10




QC Data Summary 85


Lab Chronicle 115



GCMS VOA 150




Page 2 of 1167










Page 3 of 1167

CASE NARRATIVE







calculated results








RECEIPT


ice The temperatures of the 2 coolers at receipt time were -03ordm C and 17ordm C


In some cases due to high concentrations of target analytes andor the nature of the sample matrix (foamy) samples had to be analyzed

using reduced aliquot sizes The reporting limits have been elevated accordingly To provide the lowest possible detection limits


Acetone a common laboratory contaminant was detected in the method blank associated with batch 280-165844 at a level that was

above the method detection limit but below the reporting limit The value should be considered an estimate and has been flagged ldquoJrdquo If

the associated samples reported a result above the MDL andor RL the result has been ldquoBrdquo flagged



Due to the nature of the sample matrix (foamy) the samples presented in this report had to be analyzed using reduced aliquot sizes The

reporting limits have been elevated accordingly

Due to the presence of interfering non-target analytes as well as the nature of the sample matrix (foamy) sample PIN12-0585-2 (LDU

886) had to be analyzed using a reduced aliquot size The reporting limit has been elevated accordingly

The internal standard response for 14-Dichlorobenzene-d4 was outside acceptance criteria for samples in batch 280-165111 As this

internal standard is not associated with the analyte of interest (14-Dioxane) data are reported as is

The MSD aliquot of the MSMSD associated with batch 280-164929 exhibited the percent recovery outside the control limits biased high

The LCS and LCSD were within control limits

The RPD limit was exceeded in the MSMSD performed on sample PIN12-0568-2 (LDU 868) in batch 280-165812 Method precision and

accuracy have been verified by the acceptable LCSLCSD analysis data


Page 4 of 1167




Sdg Number 13025120

GCMS VOA

Compound was found in the blank and sampleB





J



SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39875-1 PIN12-0568-1 Water 03112013 1456 03132013 0900

280-39875-1MS PIN12-0568-1 Water 03112013 1456 03132013 0900

280-39875-1MSD PIN12-0568-1 Water 03112013 1456 03132013 0900

280-39875-2 PIN12-0568-2 Water 03112013 1530 03132013 0900

280-39875-2MS PIN12-0568-2 Water 03112013 1530 03132013 0900

280-39875-2MSD PIN12-0568-2 Water 03112013 1530 03132013 0900

280-39875-3 PIN12-0569-1 Water 03082013 1305 03132013 0900

280-39875-4 PIN12-0569-2 Water 03082013 1355 03132013 0900

280-39875-5 PIN12-0569-3 Water 03082013 1445 03132013 0900

280-39875-6 PIN12-0570-1 Water 03082013 1535 03132013 0900

280-39875-7 PIN12-0572-1 Water 03112013 1313 03132013 0900

280-39875-8 PIN12-0572-2 Water 03112013 1350 03132013 0900

280-39875-9 PIN12-0574-1 Water 03112013 0908 03132013 0900

280-39875-10 PIN12-0574-2 Water 03112013 0958 03132013 0900

280-39875-11 PIN12-0574-3 Water 03112013 1050 03132013 0900

280-39875-12 PIN12-0584-1 Water 03092013 0820 03132013 0900

280-39875-13 PIN12-0584-2 Water 03092013 0850 03132013 0900

280-39875-14 PIN12-0584-3 Water 03092013 0955 03132013 0900

280-39875-15 PIN12-0585-1 Water 03092013 1055 03132013 0900

280-39875-16 PIN12-0585-2 Water 03092013 1135 03132013 0900

280-39875-17 PIN12-S30B Water 03082013 0930 03132013 0900

280-39875-18 PIN12-S33C Water 03082013 1036 03132013 0900

280-39875-19 PIN12-S35B Water 03082013 1130 03132013 0900

280-39875-20 PIN99-2199 Water 03082013 1200 03132013 0900

280-39875-21 PIN12-0568-3 Water 03112013 1605 03132013 0900

280-39875-22 PIN12-0570-2 Water 03112013 1652 03132013 0900




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39875-1 PIN12-0568-1


280-39875-4 PIN12-0569-2



280-39875-5 PIN12-0569-3





280-39875-8 PIN12-0572-2





280-39875-9 PIN12-0574-1



280-39875-10 PIN12-0574-2





280-39875-11 PIN12-0574-3



280-39875-12 PIN12-0584-1


50 ugL 8260B152-Butanone (MEK)


50 ugL 8260B13 J4-Methyl-2-pentanone





Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39875-13 PIN12-0584-2


10 ugL 8260B055 JCarbon disulfide



50 ugL 8260B122-Hexanone



280-39875-14 PIN12-0584-3



280-39875-15 PIN12-0585-1








280-39875-16 PIN12-0585-2






280-39875-17 PIN12-S30B












Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39875-18 PIN12-S33C







280-39875-19 PIN12-S35B






280-39875-20 PIN99-2199



280-39875-21 PIN12-0568-3


280-39875-22 PIN12-0570-2




METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120



Ilczyszyn Dennis P DPISW846 8260B


TestAmerica Denver

Page 11 of 1167

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-1

Client Matrix

280-39875-1

Water




Dilution

03192013 1029

03192013 1029

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2015D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-1

Client Matrix

280-39875-1

Water




Dilution

03192013 1029

03192013 1029

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2015D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-2

Client Matrix

280-39875-2

Water




Dilution

03192013 1243

03192013 1243

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3121D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-2

Client Matrix

280-39875-2

Water




Dilution

03192013 1243

03192013 1243

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3121D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-1

Client Matrix

280-39875-3

Water




Dilution

03192013 1647

03192013 1647

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2031D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-1

Client Matrix

280-39875-3

Water




Dilution

03192013 1647

03192013 1647

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2031D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-2

Client Matrix

280-39875-4

Water




Dilution

03192013 1711

03192013 1711

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2032D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-2

Client Matrix

280-39875-4

Water




Dilution

03192013 1711

03192013 1711

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2032D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-3

Client Matrix

280-39875-5

Water




Dilution

03192013 0942

03192013 0942

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2013D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-3

Client Matrix

280-39875-5

Water




Dilution

03192013 0942

03192013 0942

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2013D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-1

Client Matrix

280-39875-6

Water




Dilution

03192013 1734

03192013 1734

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2033D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-1

Client Matrix

280-39875-6

Water




Dilution

03192013 1734

03192013 1734

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2033D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-1

Client Matrix

280-39875-7

Water




Dilution

03192013 1757

03192013 1757

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2034D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-1

Client Matrix

280-39875-7

Water




Dilution

03192013 1757

03192013 1757

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2034D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-2

Client Matrix

280-39875-8

Water




Dilution

03192013 1005

03192013 1005

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2014D

4 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


95 U 5095Acetone

080 U 50080Benzene






































85 U 25852-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-2

Client Matrix

280-39875-8

Water




Dilution

03192013 1005

03192013 1005

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2014D

4 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


085 U 50085Styrene




085 U 50085Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-1

Client Matrix

280-39875-9

Water




Dilution

03192013 1821

03192013 1821

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2035D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-1

Client Matrix

280-39875-9

Water




Dilution

03192013 1821

03192013 1821

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2035D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165451

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-2

Client Matrix

280-39875-10

Water




Dilution

03192013 1305

03192013 1305

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3122D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-2

Client Matrix

280-39875-10

Water




Dilution

03192013 1305

03192013 1305

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3122D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-3

Client Matrix

280-39875-11

Water




Dilution

03192013 1328

03192013 1328

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3123D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-3

Client Matrix

280-39875-11

Water




Dilution

03192013 1328

03192013 1328

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3123D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-1

Client Matrix

280-39875-12

Water




Dilution

03192013 1350

03192013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3124D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


200 1019Acetone

016 U 10016Benzene






15 50202-Butanone (MEK)
































32 J 50172-Hexanone




13 J 500984-Methyl-2-pentanone

17 10022Naphthalene



Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-1

Client Matrix

280-39875-12

Water




Dilution

03192013 1350

03192013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3124D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-2

Client Matrix

280-39875-13

Water




Dilution

03192013 1413

03192013 1413

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3125D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


19 U 1019Acetone

017 J 10016Benzene










055 J 10045Carbon disulfide




























12 50172-Hexanone





22 10022Naphthalene



Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-2

Client Matrix

280-39875-13

Water




Dilution

03192013 1413

03192013 1413

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

G3125D

20 mL

20 mL

5030B

VMS_G

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165464

NA

Analysis Method

Prep Method


017 U 10017Styrene




020 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-3

Client Matrix

280-39875-14

Water




Dilution

03202013 2309

03202013 2309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6668D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


15 J B 2038Acetone

032 U 20032Benzene






































34 U 10342-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-3

Client Matrix

280-39875-14

Water




Dilution

03202013 2309

03202013 2309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6668D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


034 U 20034Styrene




034 U 20034Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03212013 0017

03212013 0017

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6671D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


84 J B 1019Acetone

016 U 10016Benzene





































30 J 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03212013 0017

03212013 0017

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6671D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03212013 0037

03212013 0037

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6672D

10 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03212013 0058

03212013 0058

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6673D

2 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


19 U 10019Acetone

16 U 1016Benzene




19 U 1019Bromoform











16 U 1016Chloroform






















17 U 50172-Hexanone







17 U 1017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03212013 0058

03212013 0058

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6673D

2 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





17 U 1017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03212013 0119

03212013 0119

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6674D

02 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method









Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S30B

Client Matrix

280-39875-17

Water




Dilution

03212013 0140

03212013 0140

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6675D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


93 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S30B

Client Matrix

280-39875-17

Water




Dilution

03212013 0140

03212013 0140

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6675D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




029 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03212013 0221

03212013 0221

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6677D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


98 J B 2038Acetone

032 U 20032Benzene





































34 U 10342-Hexanone







034 U 20034Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03212013 0221

03212013 0221

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6677D

10 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





034 U 20034Toluene

















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03212013 0241

03212013 0241

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6678D

1 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method











Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03212013 0302

03212013 0302

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6679D

02 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


190 U 1000190Acetone

16 U 10016Benzene




19 U 10019Bromoform

































170 U 5001702-Hexanone







17 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03212013 0302

03212013 0302

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6679D

02 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method





17 U 10017Toluene

















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03212013 0322

03212013 0322

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6680D

002 mL

20 mLRun Type DL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method











Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2199

Client Matrix

280-39875-20

Water




Dilution

03212013 0343

03212013 0343

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6681D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


51 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2199

Client Matrix

280-39875-20

Water




Dilution

03212013 0343

03212013 0343

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6681D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-3

Client Matrix

280-39875-21

Water




Dilution

03212013 0403

03212013 0403

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6682D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


70 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-3

Client Matrix

280-39875-21

Water




Dilution

03212013 0403

03212013 0403

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6682D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-2

Client Matrix

280-39875-22

Water




Dilution

03212013 0424

03212013 0424

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6683D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


58 J B 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-2

Client Matrix

280-39875-22

Water




Dilution

03212013 0424

03212013 0424

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

P6683D

20 mL

20 mL

5030B

VMS_P

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165844

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-1

Client Matrix

280-39875-1

Water




Dilution

03212013 0030

03212013 0030

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3938D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-2

Client Matrix

280-39875-2

Water




Dilution

03212013 0048

03212013 0048

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3939D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-1

Client Matrix

280-39875-3

Water




Dilution

03152013 0416

03152013 0416

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3798D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-2

Client Matrix

280-39875-4

Water




Dilution

03152013 0433

03152013 0433

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3799D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method






Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0569-3

Client Matrix

280-39875-5

Water




Dilution

03152013 0451

03152013 0451

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3800D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method






Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-1

Client Matrix

280-39875-6

Water




Dilution

03152013 0508

03152013 0508

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3801D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-1

Client Matrix

280-39875-7

Water




Dilution

03212013 0140

03212013 0140

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3942D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0572-2

Client Matrix

280-39875-8

Water




Dilution

03212013 0157

03212013 0157

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3943D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-1

Client Matrix

280-39875-9

Water




Dilution

03212013 0215

03212013 0215

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3944D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-2

Client Matrix

280-39875-10

Water




Dilution

03212013 0232

03212013 0232

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3945D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0574-3

Client Matrix

280-39875-11

Water




Dilution

03212013 0250

03212013 0250

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3946D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-1

Client Matrix

280-39875-12

Water




Dilution

03152013 0526

03152013 0526

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3802D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-2

Client Matrix

280-39875-13

Water




Dilution

03152013 0543

03152013 0543

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3803D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-164929

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0584-3

Client Matrix

280-39875-14

Water




Dilution

03162013 0403

03162013 0403

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3843D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-1

Client Matrix

280-39875-15

Water




Dilution

03162013 0236

03162013 0236

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3838D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0585-2

Client Matrix

280-39875-16

Water




Dilution

03222013 0303

03222013 0303

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3979D

05 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


88 U 408814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S30B

Client Matrix

280-39875-17

Water




Dilution

03162013 0311

03162013 0311

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3840D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S33C

Client Matrix

280-39875-18

Water




Dilution

03162013 0328

03162013 0328

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3841D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S35B

Client Matrix

280-39875-19

Water




Dilution

03162013 0346

03162013 0346

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3842D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165111

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0568-3

Client Matrix

280-39875-21

Water




Dilution

03212013 0307

03212013 0307

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3947D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-2

Client Matrix

280-39875-22

Water




Dilution

03212013 0324

03212013 0324

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3948D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39875-1 PIN12-0568-1 81 71 93 89

280-39875-2 PIN12-0568-2 95 93 93 87

280-39875-3 PIN12-0569-1 85 75 91 86

280-39875-4 PIN12-0569-2 83 74 92 86

280-39875-5 PIN12-0569-3 85 74 96 95

280-39875-6 PIN12-0570-1 84 75 90 85

280-39875-7 PIN12-0572-1 82 74 92 87

280-39875-8 PIN12-0572-2 86 75 99 90

280-39875-9 PIN12-0574-1 85 76 95 89

280-39875-10 PIN12-0574-2 102 102 101 100

280-39875-11 PIN12-0574-3 99 102 92 89

280-39875-12 PIN12-0584-1 104 107 100 95

280-39875-13 PIN12-0584-2 98 108 89 87

280-39875-14 PIN12-0584-3 113 109 102 108

280-39875-15 PIN12-0585-1 111 111 98 107

280-39875-15 DL PIN12-0585-1 DL 113 114 100 114

280-39875-16 PIN12-0585-2 110 111 98 107

280-39875-16 DL PIN12-0585-2 DL 111 111 102 108

280-39875-17 PIN12-S30B 113 116 97 104

280-39875-18 PIN12-S33C 114 116 100 112

280-39875-18 DL PIN12-S33C DL 109 110 97 106

280-39875-19 PIN12-S35B 113 112 101 110

280-39875-19 DL PIN12-S35B DL 112 115 101 113

280-39875-20 PIN99-2199 113 113 98 112

280-39875-21 PIN12-0568-3 118 118 101 113

280-39875-22 PIN12-0570-2 116 119 100 111

MB 280-1654515 82 70 98 90

MB 280-1654645 95 91 98 92

MB 280-1658448 109 108 100 110






TestAmerica Denver

Page 81 of 1167



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

LCS 280-1654514 85 74 98 94

LCS 280-1654644 93 90 94 92

LCS 280-1658446 109 107 100 99

280-39875-1 MS PIN12-0568-1 MS 84 74 96 90

280-39875-14 MS PIN12-0584-3 MS 109 115 98 99

280-39826-B-10 MS 98 93 100 97

280-39875-1 MSD PIN12-0568-1 MSD 86 77 96 90

280-39875-14 MSD PIN12-0584-3 MSD 110 111 97 100

280-39826-B-10 MSD 93 90 92 89






TestAmerica Denver

Page 82 of 1167



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39875-1 PIN12-0568-1 99

280-39875-2 PIN12-0568-2 102

280-39875-3 PIN12-0569-1 103

280-39875-4 PIN12-0569-2 105

280-39875-5 PIN12-0569-3 103

280-39875-6 PIN12-0570-1 104

280-39875-7 PIN12-0572-1 101

280-39875-8 PIN12-0572-2 102

280-39875-9 PIN12-0574-1 114

280-39875-10 PIN12-0574-2 100

280-39875-11 PIN12-0574-3 98

280-39875-12 PIN12-0584-1 103

280-39875-13 PIN12-0584-2 122

280-39875-14 PIN12-0584-3 120

280-39875-15 PIN12-0585-1 118

280-39875-16 PIN12-0585-2 95

280-39875-17 PIN12-S30B 107

280-39875-18 PIN12-S33C 112

280-39875-19 PIN12-S35B 111

280-39875-21 PIN12-0568-3 97

280-39875-22 PIN12-0570-2 101

MB 280-16492917 99

MB 280-1651115 99

MB 280-16581217 96

MB 280-1660505 100

LCS 280-16492915 102

LCS 280-1651113 103

LCS 280-16581215 100

LCS 280-1660503 98



TestAmerica Denver

Page 83 of 1167



Sdg Number 13025120




Client Matrix Water


DCA

Rec

LCSD 280-16492916 97

LCSD 280-1651114 105

LCSD 280-16581216 96

LCSD 280-1660504 95

280-39875-2 MS PIN12-0568-2 MS 98

280-39873-C-4 MS 97

280-39873-A-2 MS 98

280-39997-D-2 MS 102

280-39875-2 MSD PIN12-0568-2 MSD 101

280-39873-C-4 MSD 100

280-39873-A-2 MSD 102

280-39997-D-2 MSD 101



TestAmerica Denver

Page 84 of 1167



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2011D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1654515


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165451

Prep Date

Leach Date

03192013 0855

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2010D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1654514


Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Prep Date

Leach Date

03192013 0805

NA


500 491 98 74 - 135Benzene




500 454 91 76 - 120Chloroform


500 453 91 75 - 13511-Dichloroethane


500 545 109 71 - 13611-Dichloroethene


500 499 100 72 - 120Ethylbenzene



500 483 97 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2016D

5 mL

20 mL

RR2017D

5 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39875-1

280-39875-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 1052

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

03192013 1116

NA

Analysis Batch

Prep Batch

Leach Batch

280-165451

NA

NA

03192013 1052


Rec


91 89 74 - 135 2 20Benzene




87 84 76 - 120 5 20Chloroform


84 82 75 - 135 4 2111-Dichloroethane


101 96 71 - 136 4 2011-Dichloroethene


94 89 72 - 120 5 26Ethylbenzene



90 90 73 - 120 0 20Toluene





Toluene-d8 (Surr) 96 96 80 - 125






Sdg Number 13025120

Water

03192013 1052 03192013 1116



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 1052

NA

Analysis Date

Prep Date

Leach Date

03192013 1116

NA

Amount

Sample



064 U 200 200 182 177Benzene




064 U 200 200 175 167Chloroform






064 U 200 200 187 179Ethylbenzene



068 U 200 200 180 179Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

G3113D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_GMB 280-1654645


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165464

Prep Date

Leach Date

03192013 0926

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

G3113D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_GMB 280-1654645


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165464

Prep Date

Leach Date

03192013 0926

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

G3112D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_GLCS 280-1654644


Analysis Batch

Prep Batch

Leach Batch

280-165464

NA

NA

Prep Date

Leach Date

03192013 0903

NA


500 474 95 74 - 135Benzene




500 451 90 76 - 120Chloroform


500 471 94 75 - 13511-Dichloroethane


500 547 109 71 - 13611-Dichloroethene


500 485 97 72 - 120Ethylbenzene



500 481 96 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

G3116D

01 mL

20 mL

G3117D

01 mL

20 mL

Method 8260B

Preparation 5030B

VMS_G

VMS_G

280-39826-B-10 MS

280-39826-B-10 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 1034

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165464

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 1056

03192013 1056

NA

Analysis Batch

Prep Batch

Leach Batch

280-165464

NA

NA

03192013 1034


Rec


97 97 74 - 135 1 20Benzene




93 92 76 - 120 1 20Chloroform


99 97 75 - 135 2 2111-Dichloroethane


108 109 71 - 136 1 2011-Dichloroethene


100 92 72 - 120 8 26Ethylbenzene



99 99 73 - 120 0 20Toluene





Toluene-d8 (Surr) 100 92 80 - 125






Sdg Number 13025120

Water

03192013 1034 03192013 1056



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 1034

NA

Analysis Date

Prep Date

Leach Date

03192013 1056

NA

Amount

Sample



39 J 1000 1000 1010 1010Benzene




38 J 1000 1000 967 961Chloroform






32 U 1000 1000 1000 925Ethylbenzene



34 U 1000 1000 993 994Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

P6667D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_PMB 280-1658448


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165844

Prep Date

Leach Date

03202013 2242

NA


293 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

P6667D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_PMB 280-1658448


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165844

Prep Date

Leach Date

03202013 2242

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

P6666D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_PLCS 280-1658446


Analysis Batch

Prep Batch

Leach Batch

280-165844

NA

NA

Prep Date

Leach Date

03202013 2222

NA


500 439 88 74 - 135Benzene




500 468 94 76 - 120Chloroform


500 444 89 75 - 13511-Dichloroethane


500 493 99 71 - 13611-Dichloroethene


500 449 90 72 - 120Ethylbenzene



500 451 90 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

P6669D

10 mL

20 mL

P6670D

10 mL

20 mL

Method 8260B

Preparation 5030B

VMS_P

VMS_P

280-39875-14

280-39875-14

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03202013 2335

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165844

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2356

03202013 2356

NA

Analysis Batch

Prep Batch

Leach Batch

280-165844

NA

NA

03202013 2335


Rec


93 90 74 - 135 3 20Benzene




98 97 76 - 120 2 20Chloroform


95 93 75 - 135 2 2111-Dichloroethane


109 106 71 - 136 3 2011-Dichloroethene


92 91 72 - 120 2 26Ethylbenzene



93 91 73 - 120 2 20Toluene





Toluene-d8 (Surr) 98 97 80 - 125






Sdg Number 13025120

Water

03202013 2335 03202013 2356



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03202013 2335

NA

Analysis Date

Prep Date

Leach Date

03202013 2356

NA

Amount

Sample



032 U 100 100 929 905Benzene




032 U 100 100 982 967Chloroform






032 U 100 100 925 911Ethylbenzene



034 U 100 100 929 912Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3783D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16492917


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-164929

Prep Date

Leach Date

03142013 2354

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3781D

20 mL

20 mL

E3782D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16492915

LCSD 280-16492916

Analysis Date

Prep Date

Leach Date

03142013 2319

03142013 2319

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA


Rec

8980 25 - 141 10 2014-Dioxane






Sdg Number 13025120

Water

03142013 2319


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03142013 2319

Analysis Date

Prep Date

Leach Date

03142013 2336

03142013 2336

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

443400500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3787D

1 mL

20 mL

E3788D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-C-4 MS

280-39873-C-4 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 0104

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

03152013 0121

NA

Analysis Batch

Prep Batch

Leach Batch

280-164929

NA

NA

03152013 0104


Rec


125 154 25 - 141 10 20 F14-Dioxane






Sdg Number 13025120

Water

03152013 0104 03152013 0121



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 0104

NA

Analysis Date

Prep Date

Leach Date

03152013 0121

NA

Amount

Sample



170 100 100 292 322 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3822D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1651115


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165111

Prep Date

Leach Date

03152013 1916

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3820D

20 mL

20 mL

E3821D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1651113

LCSD 280-1651114

Analysis Date

Prep Date

Leach Date

03152013 1841

03152013 1841

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA


Rec

8278 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1841


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03152013 1841

Analysis Date

Prep Date

Leach Date

03152013 1859

03152013 1859

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

409391500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3824D

10 mL

20 mL

E3825D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39873-A-2 MS

280-39873-A-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03152013 1951

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

03152013 2009

NA

Analysis Batch

Prep Batch

Leach Batch

280-165111

NA

NA

03152013 1951


Rec


89 94 25 - 141 5 2014-Dioxane






Sdg Number 13025120

Water

03152013 1951 03152013 2009



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03152013 1951

NA

Analysis Date

Prep Date

Leach Date

03152013 2009

NA

Amount

Sample



044 U 100 100 895 94414-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3931D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16581217


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165812

Prep Date

Leach Date

03202013 2222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3929D

20 mL

20 mL

E3930D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16581215

LCSD 280-16581216

Analysis Date

Prep Date

Leach Date

03202013 2147

03202013 2147

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA


Rec

107106 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03202013 2147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03202013 2147

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

535532500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3940D

10 mL

20 mL

E3941D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39875-2

280-39875-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0105

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

03212013 0122

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

03212013 0105


Rec


82 26 25 - 141 103 20 F14-Dioxane






Sdg Number 13025120

Water

03212013 0105 03212013 0122



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0105

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

NA

Amount

Sample



044 U 100 100 816 262 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3958D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1660505


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166050

Prep Date

Leach Date

03212013 2034

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3956D

20 mL

20 mL

E3957D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1660503

LCSD 280-1660504

Analysis Date

Prep Date

Leach Date

03212013 1959

03212013 1959

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA


Rec

9596 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03212013 1959


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03212013 1959

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

474479500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3981D

1 mL

20 mL

E3982D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39997-D-2 MS

280-39997-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 0338

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

03222013 0355

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

03222013 0338


Rec


113 107 25 - 141 6 2014-Dioxane






Sdg Number 13025120

Water

03222013 0338 03222013 0355



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 0338

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

NA

Amount

Sample



44 U 100 100 113 10714-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA







WaterPIN12-0569-1 8260B SIM280-39875-3 T

WaterPIN12-0569-2 8260B SIM280-39875-4 T

WaterPIN12-0569-3 8260B SIM280-39875-5 T

WaterPIN12-0570-1 8260B SIM280-39875-6 T

WaterPIN12-0584-1 8260B SIM280-39875-12 T

WaterPIN12-0584-2 8260B SIM280-39875-13 T







WaterPIN12-0584-3 8260B SIM280-39875-14 T

WaterPIN12-0585-1 8260B SIM280-39875-15 T







WaterPIN12-0568-1 8260B280-39875-1 T



WaterPIN12-0569-1 8260B280-39875-3 T

WaterPIN12-0569-2 8260B280-39875-4 T

WaterPIN12-0569-3 8260B280-39875-5 T

WaterPIN12-0570-1 8260B280-39875-6 T

WaterPIN12-0572-1 8260B280-39875-7 T

WaterPIN12-0572-2 8260B280-39875-8 T

WaterPIN12-0574-1 8260B280-39875-9 T

TestAmerica Denver

Page 112 of 1167





Sdg Number 13025120

Report

Basis

GCMS VOA






WaterPIN12-0568-2 8260B280-39875-2 T

WaterPIN12-0574-2 8260B280-39875-10 T

WaterPIN12-0574-3 8260B280-39875-11 T

WaterPIN12-0584-1 8260B280-39875-12 T

WaterPIN12-0584-2 8260B280-39875-13 T





WaterPIN12-0568-1 8260B SIM280-39875-1 T

WaterPIN12-0568-2 8260B SIM280-39875-2 T



WaterPIN12-0572-1 8260B SIM280-39875-7 T

WaterPIN12-0572-2 8260B SIM280-39875-8 T

WaterPIN12-0574-1 8260B SIM280-39875-9 T

WaterPIN12-0574-2 8260B SIM280-39875-10 T

WaterPIN12-0574-3 8260B SIM280-39875-11 T

WaterPIN12-0568-3 8260B SIM280-39875-21 T

WaterPIN12-0570-2 8260B SIM280-39875-22 T




WaterPIN12-0584-3 8260B280-39875-14 T



WaterPIN12-0585-1 8260B280-39875-15 T

WaterPIN12-0585-1 8260B280-39875-15DL T

WaterPIN12-0585-2 8260B280-39875-16 T

WaterPIN12-0585-2 8260B280-39875-16DL T

WaterPIN12-S30B 8260B280-39875-17 T

WaterPIN12-S33C 8260B280-39875-18 T

WaterPIN12-S33C 8260B280-39875-18DL T

WaterPIN12-S35B 8260B280-39875-19 T

WaterPIN12-S35B 8260B280-39875-19DL T

WaterPIN99-2199 8260B280-39875-20 T

WaterPIN12-0568-3 8260B280-39875-21 T

WaterPIN12-0570-2 8260B280-39875-22 T

TestAmerica Denver

Page 113 of 1167





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0585-2 8260B SIM280-39875-16 T



Report Basis

T = Total

TestAmerica Denver

Page 114 of 1167

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________

Approved for releaseKae E YoderProject Manager II3292013 906 AM









Page 1 of 764



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 9




QC Data Summary 67


Lab Chronicle 88



GCMS VOA 115




Page 2 of 764










Page 3 of 764

CASE NARRATIVE







calculated results








RECEIPT




3182013


No anomalies were encountered




Due to high constituent concentration samples PIN12-0576-1 (LDU 920) and PIN12-0576-2 (LDU 921) had to be analyzed using reduced

aliquot sizes The reporting limits have been elevated accordingly

The MSMSD performed on sample PIN12-0576-2 (LDU 921) in batch 280-166279 exhibited percent recoveries outside the control limits

biased high It can be noted that the MS and MSD concentrations were present above the instrument calibration range The LCS and

LCSD were within control limits

The RPD limit was exceeded for 14-Dioxane in the MSMSD associated with batch 280-165812 The LCS and LCSD were within control

limits


Page 4 of 764




Sdg Number 13025120

GCMS VOA






J



SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39986-1 PIN12-0551-1 Water 03132013 1614 03152013 0930

280-39986-2 PIN12-0551-2 Water 03132013 1648 03152013 0930

280-39986-3 PIN12-0570-3 Water 03132013 1430 03152013 0930

280-39986-4 PIN12-0576-1 Water 03132013 1025 03152013 0930

280-39986-4MS PIN12-0576-1 Water 03132013 1025 03152013 0930

280-39986-4MSD PIN12-0576-1 Water 03132013 1025 03152013 0930

280-39986-5 PIN12-0576-2 Water 03132013 1057 03152013 0930

280-39986-5MS PIN12-0576-2 Water 03132013 1057 03152013 0930

280-39986-5MSD PIN12-0576-2 Water 03132013 1057 03152013 0930

280-39986-6 PIN12-0576-3 Water 03132013 1528 03152013 0930

280-39986-7 PIN12-0577-1 Water 03122013 1614 03152013 0930

280-39986-8 PIN12-0577-2 Water 03122013 1642 03152013 0930

280-39986-9 PIN12-0577-3 Water 03122013 1715 03152013 0930

280-39986-10 PIN12-0578-1 Water 03132013 0820 03152013 0930

280-39986-11 PIN12-0578-2 Water 03132013 0850 03152013 0930

280-39986-12 PIN12-0578-3 Water 03132013 0920 03152013 0930

280-39986-13 PIN12-0579-1 Water 03122013 1435 03152013 0930

280-39986-14 PIN12-0579-2 Water 03122013 1459 03152013 0930

280-39986-15 PIN12-0579-3 Water 03122013 1528 03152013 0930

280-39986-16 PIN99-2200 Water 03122013 1200 03152013 0930

280-39986-17 PIN12-2464 Water 03122013 0905 03152013 0930

280-39986-18 PIN12-2465 Water 03122013 0910 03152013 0930




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39986-1 PIN12-0551-1


280-39986-2 PIN12-0551-2


280-39986-3 PIN12-0570-3



280-39986-4 PIN12-0576-1









280-39986-5 PIN12-0576-2








280-39986-6 PIN12-0576-3






280-39986-7 PIN12-0577-1





Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39986-8 PIN12-0577-2


280-39986-9 PIN12-0577-3



280-39986-10 PIN12-0578-1


280-39986-11 PIN12-0578-2


280-39986-12 PIN12-0578-3


280-39986-13 PIN12-0579-1


280-39986-14 PIN12-0579-2


280-39986-15 PIN12-0579-3



280-39986-16 PIN99-2200


280-39986-17 PIN12-2464



10 ugL 8260B037 JXylenes Total

280-39986-18 PIN12-2465



METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120




TestAmerica Denver

Page 10 of 764

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-1

Client Matrix

280-39986-1

Water




Dilution

03212013 1204

03212013 1204

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1999D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


16 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-1

Client Matrix

280-39986-1

Water




Dilution

03212013 1204

03212013 1204

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1999D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-2

Client Matrix

280-39986-2

Water




Dilution

03212013 1225

03212013 1225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2000D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


11 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-2

Client Matrix

280-39986-2

Water




Dilution

03212013 1225

03212013 1225

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2000D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-3

Client Matrix

280-39986-3

Water




Dilution

03212013 1246

03212013 1246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2001D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


39 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-3

Client Matrix

280-39986-3

Water




Dilution

03212013 1246

03212013 1246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2001D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-1

Client Matrix

280-39986-4

Water




Dilution

03212013 1100

03212013 1100

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1996D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


25 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-1

Client Matrix

280-39986-4

Water




Dilution

03212013 1100

03212013 1100

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS1996D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




026 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-2

Client Matrix

280-39986-5

Water




Dilution

03212013 1307

03212013 1307

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2002D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


23 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-2

Client Matrix

280-39986-5

Water




Dilution

03212013 1307

03212013 1307

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2002D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-3

Client Matrix

280-39986-6

Water




Dilution

03212013 1329

03212013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2003D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


95 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-3

Client Matrix

280-39986-6

Water




Dilution

03212013 1329

03212013 1329

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2003D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




80 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-1

Client Matrix

280-39986-7

Water




Dilution

03212013 1350

03212013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2004D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


63 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-1

Client Matrix

280-39986-7

Water




Dilution

03212013 1350

03212013 1350

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2004D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-2

Client Matrix

280-39986-8

Water




Dilution

03212013 1411

03212013 1411

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2005D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


25 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-2

Client Matrix

280-39986-8

Water




Dilution

03212013 1411

03212013 1411

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2005D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-3

Client Matrix

280-39986-9

Water




Dilution

03212013 1432

03212013 1432

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2006D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


50 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-3

Client Matrix

280-39986-9

Water




Dilution

03212013 1432

03212013 1432

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2006D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




029 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-1

Client Matrix

280-39986-10

Water




Dilution

03212013 1453

03212013 1453

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2007D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


29 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-1

Client Matrix

280-39986-10

Water




Dilution

03212013 1453

03212013 1453

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2007D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-2

Client Matrix

280-39986-11

Water




Dilution

03212013 1514

03212013 1514

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2008D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


14 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-2

Client Matrix

280-39986-11

Water




Dilution

03212013 1514

03212013 1514

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2008D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-3

Client Matrix

280-39986-12

Water




Dilution

03212013 1535

03212013 1535

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2009D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


11 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-3

Client Matrix

280-39986-12

Water




Dilution

03212013 1535

03212013 1535

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2009D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-1

Client Matrix

280-39986-13

Water




Dilution

03212013 1556

03212013 1556

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2010D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


13 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-1

Client Matrix

280-39986-13

Water




Dilution

03212013 1556

03212013 1556

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2010D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-2

Client Matrix

280-39986-14

Water




Dilution

03212013 1617

03212013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2011D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


15 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-2

Client Matrix

280-39986-14

Water




Dilution

03212013 1617

03212013 1617

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2011D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-3

Client Matrix

280-39986-15

Water




Dilution

03212013 1638

03212013 1638

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2012D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


24 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-3

Client Matrix

280-39986-15

Water




Dilution

03212013 1638

03212013 1638

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

MS2012D

20 mL

20 mL

5030B

VMS_MS1

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165858

NA

Analysis Method

Prep Method


017 U 10017Styrene




49 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2200

Client Matrix

280-39986-16

Water




Dilution

03252013 2334

03252013 2334

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5545D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


96 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2200

Client Matrix

280-39986-16

Water




Dilution

03252013 2334

03252013 2334

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5545D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2464

Client Matrix

280-39986-17

Water




Dilution

03252013 2354

03252013 2354

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5546D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


52 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2464

Client Matrix

280-39986-17

Water




Dilution

03252013 2354

03252013 2354

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5546D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


017 U 10017Styrene




019 J 10017Toluene











037 J 10019Xylenes Total








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2465

Client Matrix

280-39986-18

Water




Dilution

03262013 0014

03262013 0014

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5547D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


20 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2465

Client Matrix

280-39986-18

Water




Dilution

03262013 0014

03262013 0014

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5547D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166554

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-1

Client Matrix

280-39986-1

Water




Dilution

03222013 2121

03222013 2121

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4022D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0551-2

Client Matrix

280-39986-2

Water




Dilution

03222013 2139

03222013 2139

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4023D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0570-3

Client Matrix

280-39986-3

Water




Dilution

03222013 2156

03222013 2156

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4024D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-1

Client Matrix

280-39986-4

Water




Dilution

03222013 2214

03222013 2214

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4025D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


36 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-2

Client Matrix

280-39986-5

Water




Dilution

03222013 2231

03222013 2231

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4026D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


27 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0576-3

Client Matrix

280-39986-6

Water




Dilution

03222013 2324

03222013 2324

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4029D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-1

Client Matrix

280-39986-7

Water




Dilution

03212013 0342

03212013 0342

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3949D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-2

Client Matrix

280-39986-8

Water




Dilution

03212013 0359

03212013 0359

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3950D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0577-3

Client Matrix

280-39986-9

Water




Dilution

03212013 0417

03212013 0417

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3951D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165812

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-1

Client Matrix

280-39986-10

Water




Dilution

03222013 0043

03222013 0043

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3971D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-2

Client Matrix

280-39986-11

Water




Dilution

03222013 0101

03222013 0101

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3972D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0578-3

Client Matrix

280-39986-12

Water




Dilution

03222013 0118

03222013 0118

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3973D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-1

Client Matrix

280-39986-13

Water




Dilution

03222013 0136

03222013 0136

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3974D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-2

Client Matrix

280-39986-14

Water




Dilution

03222013 0153

03222013 0153

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3975D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0579-3

Client Matrix

280-39986-15

Water




Dilution

03222013 0211

03222013 0211

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3976D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2464

Client Matrix

280-39986-17

Water




Dilution

03222013 0228

03222013 0228

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3977D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2465

Client Matrix

280-39986-18

Water




Dilution

03222013 0246

03222013 0246

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3978D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39986-1 PIN12-0551-1 94 96 104 101

280-39986-2 PIN12-0551-2 98 99 104 99

280-39986-3 PIN12-0570-3 100 101 104 100

280-39986-4 PIN12-0576-1 92 93 101 94

280-39986-5 PIN12-0576-2 101 100 103 99

280-39986-6 PIN12-0576-3 93 97 97 91

280-39986-7 PIN12-0577-1 102 104 104 97

280-39986-8 PIN12-0577-2 98 102 102 98

280-39986-9 PIN12-0577-3 102 105 103 101

280-39986-10 PIN12-0578-1 102 102 103 98

280-39986-11 PIN12-0578-2 99 102 100 97

280-39986-12 PIN12-0578-3 98 101 98 94

280-39986-13 PIN12-0579-1 101 103 95 96

280-39986-14 PIN12-0579-2 103 104 95 94

280-39986-15 PIN12-0579-3 99 102 91 93

280-39986-16 PIN99-2200 94 79 100 99

280-39986-17 PIN12-2464 92 78 82 93

280-39986-18 PIN12-2465 103 91 95 98

MB 280-1658586 95 95 102 96

MB 280-1665545 91 77 91 86

LCS 280-1658585 96 93 97 95

LCS 280-1665544 97 84 98 96

280-39986-4 MS PIN12-0576-1 MS 96 98 99 99

280-40133-C-1 MS 102 86 96 98

280-39986-4 MSD PIN12-0576-1 MSD 98 100 102 100

280-40133-C-1 MSD 92 79 94 93






TestAmerica Denver

Page 64 of 764



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39986-1 PIN12-0551-1 100

280-39986-2 PIN12-0551-2 112

280-39986-3 PIN12-0570-3 122

280-39986-4 PIN12-0576-1 118

280-39986-5 PIN12-0576-2 110

280-39986-6 PIN12-0576-3 103

280-39986-7 PIN12-0577-1 99

280-39986-8 PIN12-0577-2 98

280-39986-9 PIN12-0577-3 99

280-39986-10 PIN12-0578-1 102

280-39986-11 PIN12-0578-2 103

280-39986-12 PIN12-0578-3 100

280-39986-13 PIN12-0579-1 99

280-39986-14 PIN12-0579-2 99

280-39986-15 PIN12-0579-3 99

280-39986-17 PIN12-2464 98

280-39986-18 PIN12-2465 98

MB 280-16581217 96

MB 280-1660505 100

MB 280-1662795 93

LCS 280-16581215 100

LCS 280-1660503 98

LCS 280-1662793 97

LCSD 280-16581216 96

LCSD 280-1660504 95

LCSD 280-1662794 97

280-39986-5 MS PIN12-0576-2 MS 105

280-39875-D-2 MS 98

280-39997-D-2 MS 102



TestAmerica Denver

Page 65 of 764



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39986-5 MSD PIN12-0576-2 MSD 107

280-39875-D-2 MSD 101

280-39997-D-2 MSD 101



TestAmerica Denver

Page 66 of 764



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

MS1992D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_MS1MB 280-1658586


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165858

Prep Date

Leach Date

03212013 0924

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

MS1992D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_MS1MB 280-1658586


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165858

Prep Date

Leach Date

03212013 0924

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

MS1991D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_MS1LCS 280-1658585


Analysis Batch

Prep Batch

Leach Batch

280-165858

NA

NA

Prep Date

Leach Date

03212013 0903

NA


500 441 88 74 - 135Benzene




500 446 89 76 - 120Chloroform


500 445 89 75 - 13511-Dichloroethane


500 490 98 71 - 13611-Dichloroethene


500 455 91 72 - 120Ethylbenzene



500 446 89 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

MS1997D

20 mL

20 mL

MS1998D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_MS1

VMS_MS1

280-39986-4

280-39986-4

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 1121

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165858

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 1142

03212013 1142

NA

Analysis Batch

Prep Batch

Leach Batch

280-165858

NA

NA

03212013 1121


Rec


96 93 74 - 135 3 20Benzene




94 93 76 - 120 1 20Chloroform


103 94 75 - 135 2 2111-Dichloroethane


105 102 71 - 136 2 2011-Dichloroethene


97 96 72 - 120 1 26Ethylbenzene



93 92 73 - 120 1 20Toluene





Toluene-d8 (Surr) 99 102 80 - 125






Sdg Number 13025120

Water

03212013 1121 03212013 1142



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 1121

NA

Analysis Date

Prep Date

Leach Date

03212013 1142

NA

Amount

Sample



016 U 500 500 481 466Benzene




016 U 500 500 472 466Chloroform


15 500 500 203 19911-Dichloroethane

017 J 500 500 484 484trans-12-Dichloroethene



016 U 500 500 483 481Ethylbenzene



026 J 500 500 490 485Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5544D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1665545


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166554

Prep Date

Leach Date

03252013 2314

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5544D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1665545


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166554

Prep Date

Leach Date

03252013 2314

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

C5543D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CLCS 280-1665544


Analysis Batch

Prep Batch

Leach Batch

280-166554

NA

NA

Prep Date

Leach Date

03252013 2254

NA


500 525 105 74 - 135Benzene



500 510 102 76 - 135Chlorobenzene

500 499 100 76 - 120Chloroform


500 484 97 75 - 13511-Dichloroethane


500 626 125 71 - 13611-Dichloroethene


500 515 103 72 - 120Ethylbenzene



500 576 115 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5549D

20 mL

20 mL

C5550D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-40133-C-1 MS

280-40133-C-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03262013 0054

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166554

NA

NA

Analysis Date

Prep Date

Leach Date

03262013 0114

03262013 0114

NA

Analysis Batch

Prep Batch

Leach Batch

280-166554

NA

NA

03262013 0054


Rec


108 104 74 - 135 3 20Benzene



104 105 76 - 135 2 20Chlorobenzene

105 101 76 - 120 4 20Chloroform


102 96 75 - 135 5 2111-Dichloroethane


130 123 71 - 136 6 2011-Dichloroethene


103 103 72 - 120 0 26Ethylbenzene



117 115 73 - 120 2 20Toluene





Toluene-d8 (Surr) 96 94 80 - 125






Sdg Number 13025120

Water

03262013 0054 03262013 0114



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03262013 0054

NA

Analysis Date

Prep Date

Leach Date

03262013 0114

NA

Amount

Sample



016 U 500 500 538 521Benzene




016 U 500 500 525 507Chloroform






016 U 500 500 516 517Ethylbenzene



017 U 500 500 586 575Toluene


16 500 500 672 669Trichloroethene




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3931D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16581217


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165812

Prep Date

Leach Date

03202013 2222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3929D

20 mL

20 mL

E3930D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16581215

LCSD 280-16581216

Analysis Date

Prep Date

Leach Date

03202013 2147

03202013 2147

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA


Rec

107106 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03202013 2147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03202013 2147

Analysis Date

Prep Date

Leach Date

03202013 2205

03202013 2205

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

535532500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3940D

10 mL

20 mL

E3941D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39875-D-2 MS

280-39875-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0105

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

03212013 0122

NA

Analysis Batch

Prep Batch

Leach Batch

280-165812

NA

NA

03212013 0105


Rec


82 26 25 - 141 103 20 F14-Dioxane






Sdg Number 13025120

Water

03212013 0105 03212013 0122



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0105

NA

Analysis Date

Prep Date

Leach Date

03212013 0122

NA

Amount

Sample



044 U 100 100 816 262 F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3958D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1660505


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166050

Prep Date

Leach Date

03212013 2034

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3956D

20 mL

20 mL

E3957D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1660503

LCSD 280-1660504

Analysis Date

Prep Date

Leach Date

03212013 1959

03212013 1959

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA


Rec

9596 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03212013 1959


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03212013 1959

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

474479500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3981D

1 mL

20 mL

E3982D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39997-D-2 MS

280-39997-D-2 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 0338

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

03222013 0355

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

03222013 0338


Rec


113 107 25 - 141 6 2014-Dioxane






Sdg Number 13025120

Water

03222013 0338 03222013 0355



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 0338

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

NA

Amount

Sample



44 U 100 100 113 10714-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4017D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1662795


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166279

Prep Date

Leach Date

03222013 1946

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4015D

20 mL

20 mL

E4016D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1662793

LCSD 280-1662794

Analysis Date

Prep Date

Leach Date

03222013 1911

03222013 1911

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA


Rec

103103 25 - 141 0 2014-Dioxane






Sdg Number 13025120

Water

03222013 1911


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03222013 1911

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

514516500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4027D

10 mL

20 mL

E4028D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39986-5

280-39986-5

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 2249

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

03222013 2306

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

03222013 2249


Rec


146 225 25 - 141 17 20 E F E F14-Dioxane






Sdg Number 13025120

Water

03222013 2249 03222013 2306



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 2249

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

NA

Amount

Sample



27 100 100 419 499E F E F14-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA







WaterPIN12-0577-1 8260B SIM280-39986-7 T

WaterPIN12-0577-2 8260B SIM280-39986-8 T

WaterPIN12-0577-3 8260B SIM280-39986-9 T




WaterPIN12-0551-1 8260B280-39986-1 T

WaterPIN12-0551-2 8260B280-39986-2 T

WaterPIN12-0570-3 8260B280-39986-3 T

WaterPIN12-0576-1 8260B280-39986-4 T



WaterPIN12-0576-2 8260B280-39986-5 T

WaterPIN12-0576-3 8260B280-39986-6 T

WaterPIN12-0577-1 8260B280-39986-7 T

WaterPIN12-0577-2 8260B280-39986-8 T

WaterPIN12-0577-3 8260B280-39986-9 T

WaterPIN12-0578-1 8260B280-39986-10 T

WaterPIN12-0578-2 8260B280-39986-11 T

WaterPIN12-0578-3 8260B280-39986-12 T

WaterPIN12-0579-1 8260B280-39986-13 T

WaterPIN12-0579-2 8260B280-39986-14 T

WaterPIN12-0579-3 8260B280-39986-15 T





WaterPIN12-0578-1 8260B SIM280-39986-10 T

WaterPIN12-0578-2 8260B SIM280-39986-11 T

WaterPIN12-0578-3 8260B SIM280-39986-12 T

WaterPIN12-0579-1 8260B SIM280-39986-13 T

WaterPIN12-0579-2 8260B SIM280-39986-14 T

WaterPIN12-0579-3 8260B SIM280-39986-15 T

WaterPIN12-2464 8260B SIM280-39986-17 T

WaterPIN12-2465 8260B SIM280-39986-18 T



TestAmerica Denver

Page 86 of 764





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0551-1 8260B SIM280-39986-1 T

WaterPIN12-0551-2 8260B SIM280-39986-2 T

WaterPIN12-0570-3 8260B SIM280-39986-3 T

WaterPIN12-0576-1 8260B SIM280-39986-4 T

WaterPIN12-0576-2 8260B SIM280-39986-5 T



WaterPIN12-0576-3 8260B SIM280-39986-6 T




WaterPIN99-2200 8260B280-39986-16 T

WaterPIN12-2464 8260B280-39986-17 T

WaterPIN12-2465 8260B280-39986-18 T



Report Basis

T = Total

TestAmerica Denver

Page 87 of 764

ANALYTICAL REPORT


SDG Number 13025120





_____________________________________________










Page 1 of 1003



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 10




QC Data Summary 90


Lab Chronicle 119



GCMS VOA 148




Page 2 of 1003










Page 3 of 1003

CASE NARRATIVE







calculated results








RECEIPT




3182013


Due to high constituent concentration a reduced aliquot size had to be used for the analysis of cis-12-Dichloroethene and Vinyl chloride

in samples PIN12-0587-2 (LDU 902) PIN12-0587-3 (LDU 888) and PIN12-2454 (LDU 960) The reporting limits have been elevated

accordingly

Due to the nature of the sample matrix (foamy) samples PIN12-0588-1 (LDU 889) PIN12-S68C (LDU 933) and PIN12-S68D (DU 934)

had to be analyzed using reduced aliquot sizes The reporting limits have been elevated accordingly

The MS aliquot of the MSMSD performed on sample PIN12-0583-1 (LDU 881) in batch 280-165603 exhibited spike compound recoveries









Page 4 of 1003




Sdg Number 13025120

GCMS VOA






J


SAMPLE SUMMARY


Sdg Number 13025120


DateTime DateTime

280-39997-1 PIN12-0583-1 Water 03122013 1400 03152013 0930

280-39997-1MS PIN12-0583-1 Water 03122013 1400 03152013 0930

280-39997-1MSD PIN12-0583-1 Water 03122013 1400 03152013 0930

280-39997-2 PIN12-0583-2 Water 03122013 1434 03152013 0930

280-39997-2MS PIN12-0583-2 Water 03122013 1434 03152013 0930

280-39997-2MSD PIN12-0583-2 Water 03122013 1434 03152013 0930

280-39997-3 PIN12-0583-3 Water 03122013 1512 03152013 0930

280-39997-4 PIN12-0586-1 Water 03132013 1054 03152013 0930

280-39997-5 PIN12-0586-2 Water 03132013 1125 03152013 0930

280-39997-6 PIN12-0586-3 Water 03132013 1342 03152013 0930

280-39997-7 PIN12-0587-1 Water 03132013 1440 03152013 0930

280-39997-8 PIN12-0587-2 Water 03132013 1508 03152013 0930

280-39997-9 PIN12-0587-3 Water 03132013 1644 03152013 0930

280-39997-10 PIN12-0588-1 Water 03142013 0900 03152013 0930

280-39997-11 PIN12-0588-2 Water 03142013 0933 03152013 0930

280-39997-12 PIN12-0588-3 Water 03142013 1007 03152013 0930

280-39997-13 PIN12-2453 Water 03122013 1200 03152013 0930

280-39997-14 PIN12-2454 Water 03132013 1446 03152013 0930

280-39997-15 PIN12-S68B Water 03132013 0856 03152013 0930

280-39997-16 PIN12-S68C Water 03132013 0931 03152013 0930

280-39997-17 PIN12-S68D Water 03132013 1004 03152013 0930

280-39997-18 PIN12-S69B Water 03122013 0906 03152013 0930

280-39997-19 PIN12-S69C Water 03122013 0933 03152013 0930

280-39997-20 PIN12-S69D Water 03122013 1013 03152013 0930

280-39997-21 PIN12-S70B Water 03122013 1110 03152013 0930

280-39997-22 PIN12-S70C Water 03122013 1157 03152013 0930

280-39997-23 PIN12-S70D Water 03122013 1303 03152013 0930

280-39997-24 PIN99-2449 Water 03122013 0845 03152013 0930




Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39997-1 PIN12-0583-1




280-39997-2 PIN12-0583-2







280-39997-4 PIN12-0586-1



280-39997-5 PIN12-0586-2





280-39997-6 PIN12-0586-3






280-39997-7 PIN12-0587-1









Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39997-8 PIN12-0587-2







280-39997-9 PIN12-0587-3







280-39997-11 PIN12-0588-2






280-39997-12 PIN12-0588-3




280-39997-13 PIN12-2453





280-39997-14 PIN12-2454










Analyte Result

Reporting

Limit Units Method


Sdg Number 13025120

Qualifier

280-39997-16 PIN12-S68C




280-39997-17 PIN12-S68D





280-39997-20 PIN12-S69D


280-39997-21 PIN12-S70B




280-39997-22 PIN12-S70C







280-39997-23 PIN12-S70D








METHOD SUMMARY


Sdg Number 13025120


Matrix Water





Lab References


Method References






Sdg Number 13025120



TestAmerica Denver

Page 11 of 1003

Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-1

Client Matrix

280-39997-1

Water




Dilution

03202013 0112

03202013 0112

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5428D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


77 J 1019Acetone

016 U 10016Benzene






































21 J 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-1

Client Matrix

280-39997-1

Water




Dilution

03202013 0112

03202013 0112

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5428D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




026 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-2

Client Matrix

280-39997-2

Water




Dilution

03202013 0212

03202013 0212

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5431D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


55 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-2

Client Matrix

280-39997-2

Water




Dilution

03202013 0212

03202013 0212

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5431D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




026 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-3

Client Matrix

280-39997-3

Water




Dilution

03202013 0246

03202013 0246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2054D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-3

Client Matrix

280-39997-3

Water




Dilution

03202013 0246

03202013 0246

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2054D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-1

Client Matrix

280-39997-4

Water




Dilution

03202013 0232

03202013 0232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5432D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


39 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-1

Client Matrix

280-39997-4

Water




Dilution

03202013 0232

03202013 0232

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5432D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-2

Client Matrix

280-39997-5

Water




Dilution

03202013 0252

03202013 0252

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5433D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


63 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-2

Client Matrix

280-39997-5

Water




Dilution

03202013 0252

03202013 0252

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5433D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-3

Client Matrix

280-39997-6

Water




Dilution

03202013 0312

03202013 0312

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5434D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


87 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-3

Client Matrix

280-39997-6

Water




Dilution

03202013 0312

03202013 0312

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5434D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-1

Client Matrix

280-39997-7

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5435D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


53 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-1

Client Matrix

280-39997-7

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5435D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03202013 0352

03202013 0352

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5436D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


82 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03202013 0352

03202013 0352

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5436D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method





027 J 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03212013 0400

03212013 0400

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2116D

4 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03202013 0412

03202013 0412

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5437D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


63 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03202013 0412

03202013 0412

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5437D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method





017 J 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03212013 0423

03212013 0423

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2117D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-1

Client Matrix

280-39997-10

Water




Dilution

03212013 0446

03212013 0446

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2118D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-1

Client Matrix

280-39997-10

Water




Dilution

03212013 0446

03212013 0446

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2118D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-2

Client Matrix

280-39997-11

Water




Dilution

03202013 0452

03202013 0452

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5439D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


44 J 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-2

Client Matrix

280-39997-11

Water




Dilution

03202013 0452

03202013 0452

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5439D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-3

Client Matrix

280-39997-12

Water




Dilution

03202013 0512

03202013 0512

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5440D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-3

Client Matrix

280-39997-12

Water




Dilution

03202013 0512

03202013 0512

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5440D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 J 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2453

Client Matrix

280-39997-13

Water




Dilution

03202013 0309

03202013 0309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2055D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2453

Client Matrix

280-39997-13

Water




Dilution

03202013 0309

03202013 0309

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2055D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03202013 0532

03202013 0532

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5441D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method


66 J 1019Acetone

016 U 10016Benzene





































17 U 50172-Hexanone







017 U 10017Styrene


Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03202013 0532

03202013 0532

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

C5441D

20 mL

20 mL

5030B

VMS_C

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165603

NA

Analysis Method

Prep Method





022 J 10017Toluene


















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03212013 0510

03212013 0510

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2119D

2 mL

20 mLRun Type DL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165842

NA

Analysis Method

Prep Method










Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68B

Client Matrix

280-39997-15

Water




Dilution

03202013 0614

03202013 0614

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2063D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68B

Client Matrix

280-39997-15

Water




Dilution

03202013 0614

03202013 0614

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2063D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68C

Client Matrix

280-39997-16

Water




Dilution

03202013 0637

03202013 0637

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2064D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68C

Client Matrix

280-39997-16

Water




Dilution

03202013 0637

03202013 0637

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2064D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68D

Client Matrix

280-39997-17

Water




Dilution

03202013 0700

03202013 0700

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2065D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


76 U 4076Acetone

064 U 40064Benzene






































68 U 20682-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68D

Client Matrix

280-39997-17

Water




Dilution

03202013 0700

03202013 0700

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2065D

5 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


068 U 40068Styrene




068 U 40068Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69B

Client Matrix

280-39997-18

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2056D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69B

Client Matrix

280-39997-18

Water




Dilution

03202013 0332

03202013 0332

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2056D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69C

Client Matrix

280-39997-19

Water




Dilution

03202013 0355

03202013 0355

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2057D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69C

Client Matrix

280-39997-19

Water




Dilution

03202013 0355

03202013 0355

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2057D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69D

Client Matrix

280-39997-20

Water




Dilution

03202013 0418

03202013 0418

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2058D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69D

Client Matrix

280-39997-20

Water




Dilution

03202013 0418

03202013 0418

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2058D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70B

Client Matrix

280-39997-21

Water




Dilution

03202013 0441

03202013 0441

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2059D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70B

Client Matrix

280-39997-21

Water




Dilution

03202013 0441

03202013 0441

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2059D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70C

Client Matrix

280-39997-22

Water




Dilution

03202013 0504

03202013 0504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2060D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70C

Client Matrix

280-39997-22

Water




Dilution

03202013 0504

03202013 0504

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2060D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70D

Client Matrix

280-39997-23

Water




Dilution

03202013 0528

03202013 0528

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2061D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70D

Client Matrix

280-39997-23

Water




Dilution

03202013 0528

03202013 0528

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2061D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2449

Client Matrix

280-39997-24

Water




Dilution

03202013 0551

03202013 0551

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2062D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN99-2449

Client Matrix

280-39997-24

Water




Dilution

03202013 0551

03202013 0551

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2062D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-165610

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-1

Client Matrix

280-39997-1

Water




Dilution

03212013 2114

03212013 2114

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3959D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-2

Client Matrix

280-39997-2

Water




Dilution

03222013 0320

03222013 0320

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3980D

1 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


44 U 204414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0583-3

Client Matrix

280-39997-3

Water




Dilution

03222013 0413

03222013 0413

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3983D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-1

Client Matrix

280-39997-4

Water




Dilution

03222013 2341

03222013 2341

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4030D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-2

Client Matrix

280-39997-5

Water




Dilution

03222013 2359

03222013 2359

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4031D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0586-3

Client Matrix

280-39997-6

Water




Dilution

03232013 0016

03232013 0016

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4032D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-1

Client Matrix

280-39997-7

Water




Dilution

03232013 0034

03232013 0034

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4033D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-2

Client Matrix

280-39997-8

Water




Dilution

03232013 0051

03232013 0051

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4034D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0587-3

Client Matrix

280-39997-9

Water




Dilution

03232013 0108

03232013 0108

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4035D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-1

Client Matrix

280-39997-10

Water




Dilution

03262013 0701

03262013 0701

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4109D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166553

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-2

Client Matrix

280-39997-11

Water




Dilution

03262013 0718

03262013 0718

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4110D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166553

NA

Analysis Method

Prep Method


66 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-0588-3

Client Matrix

280-39997-12

Water




Dilution

03262013 0736

03262013 0736

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4111D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166553

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2453

Client Matrix

280-39997-13

Water




Dilution

03212013 2241

03212013 2241

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3964D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-2454

Client Matrix

280-39997-14

Water




Dilution

03232013 0126

03232013 0126

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4036D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68B

Client Matrix

280-39997-15

Water




Dilution

03232013 0143

03232013 0143

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4037D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68C

Client Matrix

280-39997-16

Water




Dilution

03232013 0201

03232013 0201

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4038D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


45 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S68D

Client Matrix

280-39997-17

Water




Dilution

03232013 0218

03232013 0218

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4039D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166279

NA

Analysis Method

Prep Method


33 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69B

Client Matrix

280-39997-18

Water




Dilution

03222013 0430

03222013 0430

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3984D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69C

Client Matrix

280-39997-19

Water




Dilution

03222013 0447

03222013 0447

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3985D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S69D

Client Matrix

280-39997-20

Water




Dilution

03222013 0505

03222013 0505

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3986D

5 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


088 U 4008814-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70B

Client Matrix

280-39997-21

Water




Dilution

03212013 2351

03212013 2351

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3968D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70C

Client Matrix

280-39997-22

Water




Dilution

03222013 0008

03222013 0008

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3969D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


15 2004414-Dioxane




Analytical Data


Sdg Number 13025120

Client Sample ID

Lab Sample ID

PIN12-S70D

Client Matrix

280-39997-23

Water




Dilution

03222013 0026

03222013 0026

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E3970D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-166050

NA

Analysis Method

Prep Method


12 2004414-Dioxane






Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-39997-1 PIN12-0583-1 116 117 101 107

280-39997-2 PIN12-0583-2 103 103 88 92

280-39997-3 PIN12-0583-3 92 86 96 94

280-39997-4 PIN12-0586-1 118 117 90 104

280-39997-5 PIN12-0586-2 119 122 98 108

280-39997-6 PIN12-0586-3 102 100 86 93

280-39997-7 PIN12-0587-1 107 107 84 97

280-39997-8 PIN12-0587-2 106 107 87 95

280-39997-8 DL PIN12-0587-2 DL 88 84 93 92

280-39997-9 PIN12-0587-3 110 109 88 96

280-39997-9 DL PIN12-0587-3 DL 84 79 87 89

280-39997-10 PIN12-0588-1 92 87 93 97

280-39997-11 PIN12-0588-2 114 112 94 103

280-39997-12 PIN12-0588-3 118 116 96 102

280-39997-13 PIN12-2453 94 90 97 95

280-39997-14 PIN12-2454 107 108 81 91

280-39997-14 DL PIN12-2454 DL 92 88 96 98

280-39997-15 PIN12-S68B 90 82 97 94

280-39997-16 PIN12-S68C 86 80 91 90

280-39997-17 PIN12-S68D 91 84 92 91

280-39997-18 PIN12-S69B 92 86 92 91

280-39997-19 PIN12-S69C 86 78 91 94

280-39997-20 PIN12-S69D 86 78 90 90

280-39997-21 PIN12-S70B 86 77 92 91

280-39997-22 PIN12-S70C 99 94 104 104

280-39997-23 PIN12-S70D 92 87 96 94

280-39997-24 PIN99-2449 85 80 91 92

MB 280-1656035 106 104 91 101

MB 280-1656105 88 81 97 92






TestAmerica Denver

Page 86 of 1003



Sdg Number 13025120




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

MB 280-1658425 91 90 93 95

LCS 280-1656034 106 102 95 94

LCS 280-1656104 88 83 93 91

LCS 280-1658424 82 81 87 88

280-39997-1 MS PIN12-0583-1 MS 103 107 82 81

280-39993-D-1 MS 105 100 96 92

280-39865-B-1 MS 87 81 99 96

280-39966-B-1 MS 91 89 96 98

280-39997-1 MSD PIN12-0583-1 MSD 117 123 95 95

280-39993-D-1 MSD 109 103 97 93

280-39865-B-1 MSD 83 77 90 90

280-39966-B-1 MSD 92 92 93 97






TestAmerica Denver

Page 87 of 1003



Sdg Number 13025120




Client Matrix Water


DCA

Rec

280-39997-1 PIN12-0583-1 117

280-39997-2 PIN12-0583-2 98

280-39997-3 PIN12-0583-3 109

280-39997-4 PIN12-0586-1 101

280-39997-5 PIN12-0586-2 102

280-39997-6 PIN12-0586-3 102

280-39997-7 PIN12-0587-1 100

280-39997-8 PIN12-0587-2 103

280-39997-9 PIN12-0587-3 120

280-39997-10 PIN12-0588-1 99

280-39997-11 PIN12-0588-2 103

280-39997-12 PIN12-0588-3 108

280-39997-13 PIN12-2453 119

280-39997-14 PIN12-2454 105

280-39997-15 PIN12-S68B 102

280-39997-16 PIN12-S68C 107

280-39997-17 PIN12-S68D 100

280-39997-18 PIN12-S69B 96

280-39997-19 PIN12-S69C 95

280-39997-20 PIN12-S69D 97

280-39997-21 PIN12-S70B 102

280-39997-22 PIN12-S70C 103

280-39997-23 PIN12-S70D 103

MB 280-1660505 100

MB 280-1662795 93

MB 280-16655317 101

LCS 280-1660503 98

LCS 280-1662793 97

LCS 280-16655315 108



TestAmerica Denver

Page 88 of 1003



Sdg Number 13025120




Client Matrix Water


DCA

Rec

LCSD 280-1660504 95

LCSD 280-1662794 97

LCSD 280-16655316 102

280-39997-2 MS PIN12-0583-2 MS 102

280-39986-B-5 MS 105

280-40230-D-1 MS 95

280-39997-2 MSD PIN12-0583-2 MSD 101

280-39986-B-5 MSD 107

280-40230-D-1 MSD 101



TestAmerica Denver

Page 89 of 1003



Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5415D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1656035


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165603

Prep Date

Leach Date

03192013 2050

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

C5415D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CMB 280-1656035


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165603

Prep Date

Leach Date

03192013 2050

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

C5414D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_CLCS 280-1656034


Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

Prep Date

Leach Date

03192013 2030

NA


500 502 100 74 - 135Benzene




500 544 109 76 - 120Chloroform


500 505 101 75 - 13511-Dichloroethane


500 584 117 71 - 13611-Dichloroethene


500 470 94 72 - 120Ethylbenzene



500 529 106 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5418D

20 mL

20 mL

C5419D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-39993-D-1 MS

280-39993-D-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 2152

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 2212

03192013 2212

NA

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

03192013 2152


Rec


105 103 74 - 135 2 20Benzene




116 114 76 - 120 2 20Chloroform


107 108 75 - 135 1 2111-Dichloroethane


118 119 71 - 136 1 2011-Dichloroethene


99 97 72 - 120 1 26Ethylbenzene



112 109 73 - 120 3 20Toluene





Toluene-d8 (Surr) 96 97 80 - 125






Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

C5429D

20 mL

20 mL

C5430D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_C

VMS_C

280-39997-1

280-39997-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03202013 0132

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

Analysis Date

Prep Date

Leach Date

03202013 0152

03202013 0152

NA

Analysis Batch

Prep Batch

Leach Batch

280-165603

NA

NA

03202013 0132


Rec


106 100 74 - 135 6 20Benzene




126 117 76 - 120 8 20 FChloroform


114 107 75 - 135 7 2111-Dichloroethane


124 112 71 - 136 10 2011-Dichloroethene


93 88 72 - 120 6 26Ethylbenzene



108 106 73 - 120 2 20Toluene





Toluene-d8 (Surr) 82 95 80 - 125






Sdg Number 13025120

Water

03192013 2152 03192013 2212



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 2152

NA

Analysis Date

Prep Date

Leach Date

03192013 2212

NA

Amount

Sample



016 U 500 500 524 515Benzene




016 U 500 500 578 568Chloroform






016 U 500 500 493 486Ethylbenzene



025 J 500 500 585 569Toluene






Sdg Number 13025120

Water

03202013 0132 03202013 0152



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03202013 0132

NA

Analysis Date

Prep Date

Leach Date

03202013 0152

NA

Amount

Sample



016 U 500 500 531 500Benzene


019 U 500 500 709 659FCarbon tetrachloride


016 U 500 500 631 585FChloroform






016 U 500 500 467 440Ethylbenzene



026 J 500 500 569 556Toluene

016 U 500 500 711 657F111-Trichloroethane





Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2041D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1656105


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165610

Prep Date

Leach Date

03192013 2135

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2041D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1656105


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165610

Prep Date

Leach Date

03192013 2135

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2040D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1656104


Analysis Batch

Prep Batch

Leach Batch

280-165610

NA

NA

Prep Date

Leach Date

03192013 2112

NA


500 466 93 74 - 135Benzene




500 459 92 76 - 120Chloroform


500 455 91 75 - 13511-Dichloroethane


500 516 103 71 - 13611-Dichloroethene


500 452 90 72 - 120Ethylbenzene



500 473 95 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2045D

20 mL

20 mL

RR2046D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39865-B-1 MS

280-39865-B-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03192013 2318

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165610

NA

NA

Analysis Date

Prep Date

Leach Date

03192013 2341

03192013 2341

NA

Analysis Batch

Prep Batch

Leach Batch

280-165610

NA

NA

03192013 2318


Rec


87 82 74 - 135 6 20Benzene




89 84 76 - 120 6 20Chloroform


86 78 75 - 135 10 2111-Dichloroethane


97 91 71 - 136 6 2011-Dichloroethene


92 87 72 - 120 6 26Ethylbenzene



90 84 73 - 120 7 20Toluene





Toluene-d8 (Surr) 99 90 80 - 125






Sdg Number 13025120

Water

03192013 2318 03192013 2341



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03192013 2318

NA

Analysis Date

Prep Date

Leach Date

03192013 2341

NA

Amount

Sample



016 U 500 500 434 408Benzene




016 U 500 500 447 421Chloroform






016 U 500 500 462 436Ethylbenzene



017 U 500 500 451 420Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2107D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1658425


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165842

Prep Date

Leach Date

03212013 0020

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2107D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1658425


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-165842

Prep Date

Leach Date

03212013 0020

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13025120

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2106D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1658424


Analysis Batch

Prep Batch

Leach Batch

280-165842

NA

NA

Prep Date

Leach Date

03202013 2356

NA


500 388 78 74 - 135Benzene




500 403 81 76 - 120Chloroform


500 392 78 75 - 13511-Dichloroethane


500 441 88 71 - 13611-Dichloroethene


500 413 83 72 - 120Ethylbenzene



500 410 82 73 - 120Toluene











Sdg Number 13025120

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2109D

20 mL

20 mL

RR2110D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-39966-B-1 MS

280-39966-B-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03212013 0118

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-165842

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 0141

03212013 0141

NA

Analysis Batch

Prep Batch

Leach Batch

280-165842

NA

NA

03212013 0118


Rec


88 85 74 - 135 3 20Benzene




89 89 76 - 120 0 20Chloroform


90 87 75 - 135 3 2111-Dichloroethane


102 95 71 - 136 7 2011-Dichloroethene


92 87 72 - 120 5 26Ethylbenzene



91 89 73 - 120 2 20Toluene





Toluene-d8 (Surr) 96 93 80 - 125






Sdg Number 13025120

Water

03212013 0118 03212013 0141



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03212013 0118

NA

Analysis Date

Prep Date

Leach Date

03212013 0141

NA

Amount

Sample



016 U 500 500 440 427Benzene




016 U 500 500 444 445Chloroform






016 U 500 500 459 436Ethylbenzene



017 U 500 500 455 447Toluene






Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E3958D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1660505


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166050

Prep Date

Leach Date

03212013 2034

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E3956D

20 mL

20 mL

E3957D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1660503

LCSD 280-1660504

Analysis Date

Prep Date

Leach Date

03212013 1959

03212013 1959

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA


Rec

9596 25 - 141 1 2014-Dioxane






Sdg Number 13025120

Water

03212013 1959


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03212013 1959

Analysis Date

Prep Date

Leach Date

03212013 2017

03212013 2017

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

474479500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E3981D

1 mL

20 mL

E3982D

1 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39997-2

280-39997-2

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 0338

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

03222013 0355

NA

Analysis Batch

Prep Batch

Leach Batch

280-166050

NA

NA

03222013 0338


Rec


113 107 25 - 141 6 2014-Dioxane






Sdg Number 13025120

Water

03222013 0338 03222013 0355



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 0338

NA

Analysis Date

Prep Date

Leach Date

03222013 0355

NA

Amount

Sample



44 U 100 100 113 10714-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4017D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1662795


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166279

Prep Date

Leach Date

03222013 1946

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4015D

20 mL

20 mL

E4016D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1662793

LCSD 280-1662794

Analysis Date

Prep Date

Leach Date

03222013 1911

03222013 1911

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA


Rec

103103 25 - 141 0 2014-Dioxane






Sdg Number 13025120

Water

03222013 1911


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03222013 1911

Analysis Date

Prep Date

Leach Date

03222013 1929

03222013 1929

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

514516500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4027D

10 mL

20 mL

E4028D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-39986-B-5 MS

280-39986-B-5 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03222013 2249

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

03222013 2306

NA

Analysis Batch

Prep Batch

Leach Batch

280-166279

NA

NA

03222013 2249


Rec


146 225 25 - 141 17 20 E F E F14-Dioxane






Sdg Number 13025120

Water

03222013 2249 03222013 2306



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03222013 2249

NA

Analysis Date

Prep Date

Leach Date

03222013 2306

NA

Amount

Sample



27 100 100 419 499E F E F14-Dioxane




Sdg Number 13025120

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4093D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-16655317


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-166553

Prep Date

Leach Date

03262013 0222

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4091D

20 mL

20 mL

E4092D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-16655315

LCSD 280-16655316

Analysis Date

Prep Date

Leach Date

03262013 0147

03262013 0147

NA

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA

Analysis Date

Prep Date

Leach Date

03262013 0204

03262013 0204

NA

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA


Rec

103107 25 - 141 4 2014-Dioxane






Sdg Number 13025120

Water

03262013 0147


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

03262013 0147

Analysis Date

Prep Date

Leach Date

03262013 0204

03262013 0204

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

516537500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4101D

10 mL

20 mL

E4102D

10 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-40230-D-1 MS

280-40230-D-1 MSD

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


03262013 0442

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA

Analysis Date

Prep Date

Leach Date

03262013 0459

03262013 0459

NA

Analysis Batch

Prep Batch

Leach Batch

280-166553

NA

NA

03262013 0442


Rec


104 120 25 - 141 7 2014-Dioxane






Sdg Number 13025120

Water

03262013 0442 03262013 0459



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

03262013 0442

NA

Analysis Date

Prep Date

Leach Date

03262013 0459

NA

Amount

Sample



12 100 100 222 23814-Dioxane






Sdg Number 13025120

Report

Basis

GCMS VOA




Matrix Spike Water 8260B280-39993-D-1 MS T

Matrix Spike Duplicate Water 8260B280-39993-D-1 MSD T

WaterPIN12-0583-1 8260B280-39997-1 T



WaterPIN12-0583-2 8260B280-39997-2 T

WaterPIN12-0586-1 8260B280-39997-4 T

WaterPIN12-0586-2 8260B280-39997-5 T

WaterPIN12-0586-3 8260B280-39997-6 T

WaterPIN12-0587-1 8260B280-39997-7 T

WaterPIN12-0587-2 8260B280-39997-8 T

WaterPIN12-0587-3 8260B280-39997-9 T

WaterPIN12-0588-2 8260B280-39997-11 T

WaterPIN12-0588-3 8260B280-39997-12 T

WaterPIN12-2454 8260B280-39997-14 T






WaterPIN12-0583-3 8260B280-39997-3 T

WaterPIN12-2453 8260B280-39997-13 T

WaterPIN12-S68B 8260B280-39997-15 T

WaterPIN12-S68C 8260B280-39997-16 T

WaterPIN12-S68D 8260B280-39997-17 T

WaterPIN12-S69B 8260B280-39997-18 T

WaterPIN12-S69C 8260B280-39997-19 T

WaterPIN12-S69D 8260B280-39997-20 T

WaterPIN12-S70B 8260B280-39997-21 T

WaterPIN12-S70C 8260B280-39997-22 T

WaterPIN12-S70D 8260B280-39997-23 T

WaterPIN99-2449 8260B280-39997-24 T






WaterPIN12-0587-2 8260B280-39997-8DL T

WaterPIN12-0587-3 8260B280-39997-9DL T

WaterPIN12-0588-1 8260B280-39997-10 T

WaterPIN12-2454 8260B280-39997-14DL T

TestAmerica Denver

Page 116 of 1003





Sdg Number 13025120

Report

Basis

GCMS VOA





WaterPIN12-0583-1 8260B SIM280-39997-1 T

WaterPIN12-0583-2 8260B SIM280-39997-2 T



WaterPIN12-0583-3 8260B SIM280-39997-3 T

WaterPIN12-2453 8260B SIM280-39997-13 T













WaterPIN12-0586-1 8260B SIM280-39997-4 T

WaterPIN12-0586-2 8260B SIM280-39997-5 T

WaterPIN12-0586-3 8260B SIM280-39997-6 T

WaterPIN12-0587-1 8260B SIM280-39997-7 T

WaterPIN12-0587-2 8260B SIM280-39997-8 T

WaterPIN12-0587-3 8260B SIM280-39997-9 T

WaterPIN12-2454 8260B SIM280-39997-14 T








WaterPIN12-0588-1 8260B SIM280-39997-10 T

WaterPIN12-0588-2 8260B SIM280-39997-11 T

WaterPIN12-0588-3 8260B SIM280-39997-12 T



TestAmerica Denver

Page 117 of 1003





Sdg Number 13025120

Report

Basis

Report Basis

T = Total

TestAmerica Denver

Page 118 of 1003

ANALYTICAL REPORT


SDG Number 13045231





_____________________________________________










Page 1 of 304



Data Summaries 4

Report Narrative 4

Data Qualifiers 5

Sample Summary 6

Executive Summary 7

Method Summary 8




QC Data Summary 24


Lab Chronicle 33



GCMS VOA 42




Page 2 of 304










Page 3 of 304

CASE NARRATIVE







calculated results








RECEIPT


The temperature of the cooler at receipt was 02ordm C


The MSMSD performed on sample PIN12-0561-1 (LFZ 335) exhibited RPD data outside the control limits for 12-Dichloropropane and

Methylene Chloride The acceptable LCS analysis data indicated that the analytical system was operating within control therefore

corrective action is deemed unnecessary



Due to the sample matrix being excessively foamy reduced aliquot sizes had to be used for the analysis of samples PIN12-0561-2 (LFZ

336) and PIN12-0561-3 (LFZ 337) The reporting limits have been elevated accordingly


Page 4 of 304




Sdg Number 13045231

GCMS VOA




SAMPLE SUMMARY


Sdg Number 13045231


DateTime DateTime

280-40744-1 PIN12-0561-1 Water 04042013 1020 04052013 1428

280-40744-1MS PIN12-0561-1 Water 04042013 1020 04052013 1428

280-40744-1MSD PIN12-0561-1 Water 04042013 1020 04052013 1428

280-40744-2 PIN12-0561-2 Water 04042013 1103 04052013 1428

280-40744-3 PIN12-0561-3 Water 04042013 1329 04052013 1428

280-40744-4 PIN12-2474 Water 04042013 0800 04052013 1428




Analyte Result

Reporting

Limit Units Method


Sdg Number 13045231

Qualifier

No Detections


METHOD SUMMARY


Sdg Number 13045231


Matrix Water





Lab References


Method References






Sdg Number 13045231



TestAmerica Denver

Page 9 of 304

Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-1

Client Matrix

280-40744-1

Water




Dilution

04062013 0537

04062013 0537

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2748D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-1

Client Matrix

280-40744-1

Water




Dilution

04062013 0537

04062013 0537

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2748D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-2

Client Matrix

280-40744-2

Water




Dilution

04062013 0102

04062013 0102

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2736D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-2

Client Matrix

280-40744-2

Water




Dilution

04062013 0102

04062013 0102

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2736D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-3

Client Matrix

280-40744-3

Water




Dilution

04062013 0125

04062013 0125

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2737D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-3

Client Matrix

280-40744-3

Water




Dilution

04062013 0125

04062013 0125

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2737D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-2474

Client Matrix

280-40744-4

Water




Dilution

04062013 0149

04062013 0149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2738D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone








Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-2474

Client Matrix

280-40744-4

Water




Dilution

04062013 0149

04062013 0149

10

8260B

Final WeightVolume


Lab File ID

Instrument ID

RR2738D

20 mL

20 mL

5030B

VMS_R2

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168288

NA

Analysis Method

Prep Method


017 U 10017Styrene




017 U 10017Toluene



















Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-1

Client Matrix

280-40744-1

Water




Dilution

04052013 2302

04052013 2302

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4268D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane




Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-2

Client Matrix

280-40744-2

Water




Dilution

04052013 2354

04052013 2354

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4271D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-0561-3

Client Matrix

280-40744-3

Water




Dilution

04062013 0011

04062013 0011

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4272D

10 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


044 U 2004414-Dioxane




Analytical Data


Sdg Number 13045231

Client Sample ID

Lab Sample ID

PIN12-2474

Client Matrix

280-40744-4

Water




Dilution

04062013 0029

04062013 0029

10

8260B SIM

Final WeightVolume


Lab File ID

Instrument ID

E4273D

20 mL

20 mL

5030B

VMS_E

Analysis Date

Prep Date

Analysis Batch

Prep Batch

280-168286

NA

Analysis Method

Prep Method


022 U 1002214-Dioxane






Sdg Number 13045231




Client Matrix Water


DBFM DCA TOL BFB

Rec Rec Rec Rec

280-40744-1 PIN12-0561-1 99 90 98 93

280-40744-2 PIN12-0561-2 96 90 96 89

280-40744-3 PIN12-0561-3 107 102 101 97

280-40744-4 PIN12-2474 102 94 103 98

MB 280-1682887 106 103 102 95

LCS 280-1682886 107 105 99 96

280-40744-1 MS PIN12-0561-1 MS 101 94 96 91

280-40744-1 MSD PIN12-0561-1 MSD 106 99 102 98






TestAmerica Denver

Page 22 of 304



Sdg Number 13045231




Client Matrix Water


DCA

Rec

280-40744-1 PIN12-0561-1 113

280-40744-2 PIN12-0561-2 113

280-40744-3 PIN12-0561-3 107

280-40744-4 PIN12-2474 108

MB 280-1682865 115

LCS 280-1682863 114

LCSD 280-1682864 113

280-40744-1 MS PIN12-0561-1 MS 110

280-40744-1 MSD PIN12-0561-1 MSD 114



TestAmerica Denver

Page 23 of 304



Sdg Number 13045231

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2731D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1682887


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-168288

Prep Date

Leach Date

04052013 2307

NA


19 U 1019Acetone

016 U 10016Benzene






































17 U 50172-Hexanone









Sdg Number 13045231

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

RR2731D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2MB 280-1682887


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-168288

Prep Date

Leach Date

04052013 2307

NA



017 U 10017Styrene




017 U 10017Toluene





















Sdg Number 13045231

Water

10


Client Matrix

Lab Sample ID

Dilution

Instrument ID

Lab File ID


Final WeightVolume

RR2730D

20 mL

20 mLUnits ugL

Method 8260B

Preparation 5030B

VMS_R2LCS 280-1682886


Analysis Batch

Prep Batch

Leach Batch

280-168288

NA

NA

Prep Date

Leach Date

04052013 2244

NA


500 507 101 74 - 135Benzene




500 538 108 76 - 120Chloroform


500 517 103 75 - 13511-Dichloroethane


500 595 119 71 - 13611-Dichloroethene


500 540 108 72 - 120Ethylbenzene



500 535 107 73 - 120Toluene











Sdg Number 13045231

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

RR2734D

20 mL

20 mL

RR2735D

20 mL

20 mL

Method 8260B

Preparation 5030B

VMS_R2

VMS_R2

280-40744-1

280-40744-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


04062013 0016

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-168288

NA

NA

Analysis Date

Prep Date

Leach Date

04062013 0039

04062013 0039

NA

Analysis Batch

Prep Batch

Leach Batch

280-168288

NA

NA

04062013 0016


Rec


98 113 74 - 135 14 20Benzene



92 107 76 - 135 15 20Chlorobenzene

100 116 76 - 120 15 20Chloroform


101 116 75 - 135 14 2111-Dichloroethane


113 121 71 - 136 7 2011-Dichloroethene

95 119 71 - 120 22 20 F12-Dichloropropane

102 117 72 - 120 14 26Ethylbenzene

71 92 54 - 141 26 20 FMethylene Chloride


99 116 73 - 120 16 20Toluene





Toluene-d8 (Surr) 96 102 80 - 125






Sdg Number 13045231

Water

04062013 0016 04062013 0039



Method 8260B

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

04062013 0016

NA

Analysis Date

Prep Date

Leach Date

04062013 0039

NA

Amount

Sample



016 U 500 500 491 564Benzene




016 U 500 500 498 580Chloroform





018 U 500 500 477 597 F12-Dichloropropane

016 U 500 500 510 585Ethylbenzene

032 U 500 500 355 461 FMethylene Chloride


017 U 500 500 497 582Toluene






Sdg Number 13045231

WaterClient Matrix

10Dilution

Lab Sample ID


Instrument ID

Lab File ID


Final WeightVolume

E4263D

20 mL

20 mLUnits ugL

Method 8260B SIM

Preparation 5030B

VMS_EMB 280-1682865


Analysis Batch

Prep Batch

Leach Batch

NA

NA

280-168286

Prep Date

Leach Date

04052013 2134

NA


022 U 1002214-Dioxane



Dilution

Dilution

Lab Control Sample


10

10

Water

LCS Lab Sample ID

LCSD Lab Sample ID

Client Matrix

Units

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

Units

Instrument ID

Lab File ID


Final WeightVolume

ugL

E4261D

20 mL

20 mL

E4262D

20 mL

20 mLugL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

LCS 280-1682863

LCSD 280-1682864

Analysis Date

Prep Date

Leach Date

04052013 2059

04052013 2059

NA

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA

Analysis Date

Prep Date

Leach Date

04052013 2117

04052013 2117

NA

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA


Rec

9093 25 - 141 4 2014-Dioxane






Sdg Number 13045231

Water

04052013 2059


Client Matrix

LCSD Lab Sample ID

Client Matrix Water

Laboratory Control


Method 8260B SIM

Preparation 5030B


Analysis Date

Prep Date

Leach Date

04052013 2059

Analysis Date

Prep Date

Leach Date

04052013 2117

04052013 2117

NANA

LCSD

ResultQual

LCS

ResultQual

LCSD Spike

Amount

LCS Spike

AmountAnalyte

448466500 50014-Dioxane

Dilution

Dilution

Water

10

10

Client Matrix

Instrument ID

Lab File ID


Final WeightVolume

Instrument ID

Lab File ID


Final WeightVolume

Client Matrix Water

E4269D

20 mL

20 mL

E4270D

20 mL

20 mL

Method 8260B SIM

Preparation 5030B

VMS_E

VMS_E

280-40744-1

280-40744-1

MS Lab Sample ID

MSD Lab Sample ID

Matrix Spike


04052013 2319

NA

Analysis Date

Prep Date

Leach Date

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA

Analysis Date

Prep Date

Leach Date

04052013 2337

04052013 2337

NA

Analysis Batch

Prep Batch

Leach Batch

280-168286

NA

NA

04052013 2319


Rec


79 85 25 - 141 8 2014-Dioxane






Sdg Number 13045231

Water

04052013 2319 04052013 2337



Method 8260B SIM

Preparation 5030B


Matrix Spike


Analysis Date

Prep Date

Leach Date

04052013 2319

NA

Analysis Date

Prep Date

Leach Date

04052013 2337

NA

Amount

Sample



022 U 500 500 394 42514-Dioxane






Sdg Number 13045231

Report

Basis

GCMS VOA





WaterPIN12-0561-1 8260B SIM280-40744-1 T



WaterPIN12-0561-2 8260B SIM280-40744-2 T

WaterPIN12-0561-3 8260B SIM280-40744-3 T

WaterPIN12-2474 8260B SIM280-40744-4 T




WaterPIN12-0561-1 8260B280-40744-1 T



WaterPIN12-0561-2 8260B280-40744-2 T

WaterPIN12-0561-3 8260B280-40744-3 T

WaterPIN12-2474 8260B280-40744-4 T

Report Basis

T = Total

TestAmerica Denver

Page 32 of 304

Sitewide Environmental Monitoring Semiannual Progress Report for the Young - Rainey STAR Center December 2012 Through May 2013

Contents

Abbreviations

10 Introduction

11 Building 100 Area

12 Northeast Site

13 WWNA

14 Site Update

15 Waste Minimization

20 Water-Level Elevations

21 Groundwater Flow

30 Groundwater Sampling

31 Work Performed

32 Quality AssuranceQuality Control

40 Plume Stability Monitoring

50 Upcoming Tasks

60 References

Figures





















Tables




Table 4 Relative Percent Difference (RPD) for Duplicate Samples March 2013 (Reported in μgL)

Table 5 COPC Concentrations at the Building 100 Area (μgL)


Table 7 Area Under the Curve Values For Each Plume Stability Monitoring Cross-section

Plates

Plate 1 Sitewide Shallow Surficial Aquifer Contours Pinellas Florida March 2013

Plate 2 Sitewide Deep Surficial Aquifer Contours Pinellas Florida March 2013

Appendix

Appendix A Laboratory Reports March 2013 Semiannual Monitoring





