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Simec AG

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Test report Numb€r C 34812

Obiect ot

Customer:

Batch:

Sublect:

Method(s):

Nandrolone decanoate

Lightbest International Limited Sampl6s: 1

Rec6lpt: 05.08.2015

Assay, ldentification

HPLC

SEmple/Analysls: Method StaluslFäsult Speclflcatlon

Nandrolone decanoate:

ldentificationContent

HPLCHPLC

NN

comPlies'too.7 ./"

comPlies> 98.5 %

yesyes

G = GMP A = accreditated V= generally validat€d P = validat€d on producl N = not validaled

Slgnatur€s: ."^rr.rrU"r...Arf+ I h,u,t-Staff:

20.08.2015page I of '1

Theenclosed resu\s r€,er exclusrcly to the obi€.t ot examinarion descnb€o abow.Tho measunng a6u'acy ßava äbre on requ€si Only händwnrten signatures a€ vatidWithout sritl€n p€mission, t is nor allow€d to pubtish singte parts oi this repon.

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Simec AG Page I of I

Report steroid analysis

HPLC| Nr.5Analysendatum: 19.08.2015 10:39:51 Druckdatum: 20.08.2015 08130:33

Vial: 9 Iniektvolumen: 20

Probenidentifikation: STDNandrolonedecanonateOperator: adminChrom.-Beding. ACN / Wasser, gradientTemperatur: 40'cS.äule Nr, 88, 250 x 4,6, C18Detektion: uV 2,+0nm

0 510 15 20 25 30 35 40 45 50

Channel A

)

I

I

.99,:'

UV ResultsI{ame Time Area Amount Area Percent

Nandrolone decanoate25,140 122545236,593 129156842

0,0000,000

0,94099,060

Totäls130382694 0,000 100.000

Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiveßeSteroideuB,0B,15U9.0B.2015 10-38-37-STD Nandrolone decanonate-Rep1.datI4ethode: c:\Ezchrom Elite\Enterprise\Projects\simec\lvlethod\steroide\Steroide A.met

Simec AG


HPLC:Analysendatum:Vial:Probenidentifikation:Operator:Chrom.-Beding,Temperatur:SäuleDeteKion:

Page I of 1

Nr.519.08.2015 l1:33:239STD Nandrolone decanonateadminACN / Wasser, gradient40 0c

Nr, 88, 250 x 4,6, C18uV 240nm

Druckdatum:Injektvolumen:

20.08.2015 08:31:3220

I

i

- 2Aa

I

6

25

Amount Area PercentTime

Channel A

UV ResultsName

Nändrolone decanoate2s,14736,597

1231937129928198

0,0000,000

0,93999,061

131160135 0,000 100,000

Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroide\18,08,15U9.08.2015 11-32-04-SID Nandrolone decanonate-Rep2.datl4ethode: Cr\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A met

Simec AG Pase l or tReport steroid analysis

HPLC: Nr.5Analysendatum: 19,08,2015 12126t46 Druckdatum: 20.08.2015 08:31:42Vial: 9 Injekwollmen: 20Probenidentifikation: STDNandrolonedecanonateOperatori adminChrom.-Bedin9. ACN / Wasser, gradientTemperatur: 40'C&iule Nr. 88, 250 x 4,6, C18Detektion: UV 240nm

l

9

":i

UV ResultsName

-9

Ii

:*o

I

| +oo

0510r520253035404550

Channel A

Time Area Amount Area Percent

Nändrolone decanoate25.133 122239336,590 129313789

0,0000,000

0,93699,0&

130s36182 0.000 100,000

Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideu8,o8,15U9.08.2015 12-25-31 STD Nandrolone decanonate-Rep3.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met

Simec AG


HPLC:Analysendatum:Vial:Probenidentifikation :

Operator:chrom.-Beding.Temperatur:SäuleDetektion:

Nr.519.08.2015 13:20:09ISTD Nandrolone decanonateadminACN / Wasser, gradient40 .cNr. 88, 250 x 4,6, C18uV 240nm

Druckdatum:Injekwolumen:

20.08.2015 08:31:5120

Page 1 of 1

i 600

iaoo

i

200

r0I

600 -

2oo -

l-9

25

Channel A

UV ResultsName Amount Area PencentTime

Nandrolone decanoate25,14336,547

1218188129000992

0,0000,000

0,93599,05s

I Otats130219180 0,000 100,000

Daten File: C:\Ezchrom Elite\Enterprise\Poects\Simec\Data\2015\August 2015\Diverse

Steroide\18,08,15U9,08.2015 13-18-55-STD Nandrolone decanonate-Rep4 datMethode: C:\EZChrom Elite\Enterprise\Proiects\Simec\Method\steroide\Steroide A.met

Simec AG

Repolt steroid analysis

HPLC:

Analysendatum:Nr.519.08.2015 14:13:32 Druckdatum:

Injektvolumen:20.08.2015 08i32:0420

Page 1 of 1

Vial: 9Probenidentifikation; sTDNandrolonedecanonate

adminACN / Wasser, gradient40 0c

Nr. 88, 250 x 4,6, C18UV 240nm

Operator:Chrom.-Beding.Temperatur:SäuleDetektion:

.

| 2aa

I

6

Time Amount Area Percent

Channel A

UV ResultsName


D42445131235658

0,0000,000

0,93899,062

132478503 0,000 100,000

Daten File: C:\Ezchrom Elite\Enterprise\Projects\simec\Data\2015\August 2015\DiverseSteroideu8,o8,15U9.0B.2015 14-12-20 STD Nandrolone decanonate-Reps.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\steroide A,met

Simec AG


HPLC:Analysendatum:Vial:Probenidentifikation:Operator:Chrom.-Beding,TemperaturlSäuleDetektion:

Nr.519.08.2015 15:06:569STD Nandrolone decanonateadminACN / Wasser, gradient,t0 "cNr. 88, 250 x 4,6, C18uV 240nm

Druckdatum:Injektvolumen r

20.08.2015 08:36:2220

Page I of 1

i

i

I

:oo:

:

fo

Channel A

UV ResultsName

25

Time Amount Arca Percent


1242161130640455

0,0000,000

0,94299,058

Totals131882616 0,000 100.000

Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideU8,08,15U9,08,2015 15-05-42_STD Nandrolone decänonate-Rep6.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\l4ethod\Steroide\Steroide A.met

Simec AG


Page 1 of I

HPLC:AnalysendatumiViäl:Probenidentifikation: Blank

Nr.519.08.2015 16:00:311

20.08.2015 08:36:3220


Operator:Chrom.-Beding,Temperatur:SäuleDetektion:

adminACN / Wasser, gradient40 "cNr. 88, 250 x 4,6, C18tJV 2.l0nm

'l

-2.

Channel A

UV ResultsI{ame

25

Time Areä Amount Area PercentNandrolone decanoate 0,000 BDL

Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\Diverse

SteroideU8,08, 15\19.08.201s 15-59-11-Blank.datMethode: C:\Ezchrom Elite\Enterprise\Projects\Simec\l\4ethod\Steroide\Steroide A.met

HPLCIAnalysendatum:Vial:Probenidentifikation: C34a12A

Simec AG

Report st€roid analysis

Operator:Chrom.-Beding.TemperaturiSäuleDetektion:

Nr.519.08.2015 16r54:0010


Nr. 88, 250 x 4,6, C18uV 240nm

20,08.2015 08:36r4320

Page 1 of 1


O_l

II

II

I

i

.

:0

3

6

Channel A

uV ResultsName Time Ämount Ar€a PercentNandrolone decanoate 36,630 151370427 0,000 100,000

Totals1s1370427 0.000 100.000

Daten File: C:\EZChrom Elite\Enterprise\Proiecls\Simec\Data\2015\August 2015\DiverseSteroide\18,08,15\19.08.2015 16-52-44_C34812 A-Rep1.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met

HPLC:

Analysendatum:Vial:Probenidentifikation: C34812A

Simec AG


Operatorichrom.-B€ding.Temperatur:SäuleDetektion:

Nr,519,08,2015 17 i47 t2710

20.08.2015 08r36:5220

Page I of 1

Druckdatum:Injektvolumen i


Nr. 88, 250 x 4,6, C18UV 240nm

l

I

zoa )

I

-9

25

llme Area A.nount al€a Percent

| 300

l

| 600

It

i aoo

t

I

| 2oo

I

i

fo

o

channel A

uV ResultsNameNandrolone decanoate 36,600 1s2231615 0,000 100,000

Totals152231615 0,000 100,000

Daten File: C:\EZChrom Elite\Enterprise\Proiects\Simec\Data\2015\August 2015\Diverse

SteroideU8,08,1sU9.08.2015 17-46-12-C34812 A-Rep2.datMethode: C:\EZChrom Elite\Enterprise\Projects\Simec\lvlethod\Steroide\Steroide A.met

Simec AG

Repod steroid analysis

Päge I of 1

HPLC:

Analysendatum:Vial:

Nr.519.08.2015 18:40:5610


20.08.2015 08:37:0320

Probenidentifikation: c348124Operator:chrom.-Bedin9.Temperatur:SäuleDetektion:


Nr. 88, 250 x 4,6, c18UV 2,t0nm

:! 600

t2aa

I

3

-sö

15 20

Channel A

UV ResultsName Area Amount Area Percent

Nändrolone decanoate 36,573 151769419 0,000 100,000

Totals151769419 0,000 100.000

Daten File: Cr\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\Djverse

Steroideu8,o8,15U9.0B.2015 18-39-40 C34812 A-Rep3.datl.lethode: Cr\EZChrom Elite\Enterprise\Projects\S'mec\Method\Steroide\Steroide A.met

Simec AG

Report steroid anälysis

HPLCI

Analysendatum:Viäl:

OperatoriChrom.-Beding.Temperatur:SäuleDetektion:

Page I of 1

Nr.519.08.2015 19r34:2211

adminACN / Wasser, gradient40 .cNr. 88, 250 x 4,6, C18UV 240nm

Druckdatum:Injektvolumen :

20,08.2015 08:37:1420

Probenidentifikation: C348128

.600

l.lame

i9

1200I

.

,o

-9I

:

Channel A

UV ResultsName Time Area Amount area PercentNandrolone decanoate 36,U3 123116414 0,000 100,000

123716418 0.000 100,000

Daten File: C:\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideu8,08,15U9.08.201s 19-33-0s-C34812 B-Rep1.datl4ethode: C:\EZCh rom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met

Simec AG


Page I of 1

HPLC:

Analysendatum:Vial:

Operator:Chrom.-B€ding.Temperatur:SäuleDetektion:

*ls.

Nr,519.08.2015 20127'.4911

Druckdatum:Injektvolumeni

20.08.2015 08:37r2620

Pmbenidentifikation: C348128adminACN / Wasser, gradient40 0c

Nr. 88, 250 x 4,6, C18UV 240nm

3

Channel A

UV ResultsName

t5 25

Time Amount Area PercentNandrolone decanoate 36,590 124222209 0,000 100,000

Totals124222209 0.000 100,000

Daten File: Cr\EZChrom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideU8,0B, 15U9.08.2015 20-26-30_C34812 B-Rep2.datf4ethode: Cr\EZChrom Elite\Enterprise\Projects\Simec\l4ethod\Steroide\Steroide A,met

Simec AG Pase 1 or 1

Repolt steroid analysis

HPLC: Nr.5Analysendatum: 19.08.2015 21r21i14 Druckdatum: 20.08.2015 08:37:38Vial: 11 Injektvolumen: 20Probenidentifikation: C34a12BOperator: adminChrom.-B€ding. ACN / Wasser, gradientTemperatur: 40 oC

säiule Nr, 88, 250 x 4,6, C18Detektion: UV 2.l0nm

0-

0 510 15 20 25 30 35 1A 45 50

Channel A

UV ResultsName

r 600

i

j2aa -,

:

Time Area Amount Area PercentNandrolone decanoate 36,650 123643516 0,000 100,000

Totals1236r''3516 0,000 100,000

Daten File: Ci \Ezch rom Elite\Enterprise\Projects\Simec\Data\2015\August 2015\DiverseSteroideu8,08,15U9.08.20l5 21-20-00_C34812 B-Rep3.datl4ethode: C:\EZChrom Elite\Enterprise\Projects\Simec\Method\Steroide\Steroide A.met

simec cl l' - int.basicstero.ws decanoate purity 08... · g = gmp a = accreditated v=...

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