sfpp norwalk 1q15 npdes 05152015norwalkrab.com/wp-content/files/environmental reports...

SFPP, L.P. Operating Partnership

1100 Town and Country Road, Orange, CA 92868 714-560-4400 714-560-4601 Fax

ENERGY PARTNERS, L.P.

May 14, 2015

California Regional Water Quality Control Board

Los Angeles Region

320 W. 4th Street, Suite 200

Los Angeles, California 90013

Re: Effluent Monitoring Report January through March 2015

SFPP, L.P. Norwalk Pump Station

15306 Norwalk Boulevard, Norwalk, California

(NPDES No. CA0063509, CI No. 7497)

Attention: Information Technology Unit

In reference to the subject National Pollutant Discharge Elimination System (NPDES) permit,

please find enclosed the First Quarter 2015 Effluent Monitoring Report for the subject discharge.

I certify under penalty of law that this document and all attachments were prepared under my

direction or supervision in accordance with a system designed to assure that qualified personnel

properly gather and evaluate the information submitted. Based on my inquiry of the person or

persons who manage the system or those persons directly responsible for gathering the

information, the information submitted is, to the best of my knowledge and belief, true, accurate,

and complete. I am aware that there are significant penalties for submitting false information,

including the possibility of fine and imprisonment for knowing violations.

Executed on the _ 14 __ day of _ May __ 2015.

at __1:12 p.m.__________________________

______________________ (signature)

Stephen T. Defibaugh__ (printed name)

Remediation Project Manager___ (title)

EN0501151007SCO

CH2M HILL Engineers, Inc. CH2M Santa Ana 6 Hutton Centre Drive Suite 700 Santa Ana, CA 92707 O +1 714 429 2000 F +1 714 429 2050 www.ch2m.com

May 15, 2015 495811.A1.04 Mr. Stephen Defibaugh Kinder Morgan Energy Partners, L.P. 1100 Town and Country Road Orange, California 92868 Subject: Effluent Monitoring Report, January 1 to March 31, 2015 (First Quarter 2015)

SFPP Norwalk Pump Station, 15306 Norwalk Boulevard, Norwalk, California (NPDES No. CA0063509, CI No. 7497)

Dear Mr. Defibaugh:

This report has been prepared by CH2M HILL Engineers, Inc. (CH2M HILL), on behalf of SFPP, L.P. (SFPP), an operating partnership of Kinder Morgan Energy Partners, L.P. (KMEP), to summarize National Pollutant Discharge Elimination System (NPDES) monitoring related to the discharge of treated groundwater from SFPP’s product recovery and groundwater extraction (GWE) system. This system is installed at the SFPP Norwalk Pump Station located within the Defense Fuel Support Point Norwalk, at 15306 Norwalk Boulevard, Norwalk, California (the site).

SFPP performed certain operations, maintenance, and monitoring tasks on the product recovery and GWE systems. SFPP retained CH2M HILL to prepare this report based on the NPDES monitoring performed by SFPP. This report describes NPDES monitoring activities during the period of January 1 to March 31, 2015.

Remediation System SFPP currently operates remediation systems consisting of soil vapor extraction (SVE), total fluids extraction (TFE) of free product, GWE for hydraulic control, and treatment of extracted soil vapors and groundwater to address two specific areas at and near the site: the south‐central area and the southeastern area. Operation of the West Side Barrier (WSB) GWE system (WSB system) for remediation of the western offsite area was discontinued in August 2008 based on the reduced lateral extent and low concentrations of volatile organic compounds (VOCs) west of the site.

SVE is performed using a blower to remove soil vapors at a rate of up to 3,000 standard cubic feet per minute (scfm) from up to 33 SVE wells. The extracted vapors are conveyed to a knock‐out tank that separates entrained moisture from the soil vapors. Accumulated moisture in the knock‐out tank is treated by the main groundwater treatment system (GWTS) described below. The soil vapors are then treated in a thermal oxidizer where volatile organic compounds (VOCs) are converted to carbon dioxide and water prior to being discharged to the atmosphere. Operation of the GWTS and SVE is conducted in accordance with Permits to Construct (Application Nos. 569588 and 567723, respectively; ID 110835) issued by the South Coast Air Quality Management District (SCAQMD).

The main GWTS handles free product and groundwater from up to 20 extraction wells located in the south‐central area and up to 5 extraction wells located in the southeastern area of the site. During the first quarter 2015, the GWTS extracted from 14 wells equipped with pneumatically operated top‐loading total fluids pumps, including 11 wells in the south‐central area (GMW‐9, GMW‐24, GMW‐O‐11, GMW‐O‐20, GMW‐O‐21, GMW‐O‐23, MW‐SF‐2, MW‐SF‐11, MW‐SF‐12, MW‐SF‐14, and MW‐SF‐16) and 3 wells in the southeastern area (GMW‐36, GMW‐O‐15, and GMW‐O‐18). Free product and groundwater recovered by

MR. STEPHEN DEFIBAUGH PAGE 2 MAY 15, 2014

EN0501151007SCO

pneumatically operated top‐loading total fluids pumps are piped to an oil‐water separator (OWS). Free product, if any, from the OWS is collected in a storage tank and recycled at an offsite location. Water from the OWS is treated using liquid‐phase granular activated carbon (LGAC). Treated water is routed through an onsite 3,000‐gallon equalization tank. Two fluidized bed bioreactors (FBBRs) installed downstream of the equalization tank treat fuel oxygenates such as tertiary butyl alcohol (TBA) and methyl tertiary butyl ether (MTBE) that are not treated in the LGAC. The treated groundwater then passes through polishing LGAC units prior to discharge in accordance with the NPDES permit (No. CA0063509, CI No. 7497).

Summary of Quarterly Operations Approximately 936,119 gallons of groundwater were extracted from the south‐central and southeastern areas during the first quarter 2015. No groundwater was extracted from the WSB area during this period. Table 1 summarizes the average daily flow rate during the reporting period. The GWTS operated throughout the quarter, with the following exceptions:

The GWTS was turned off on February 3, 2015, to clean out the OWS, OWS transfer tank, sump, and equalization tank. The system was restarted on the same day.

The GWTS was off on arrival on March 3, 2015, due to a high product tank alarm. The system was restarted on the same day.

The GWTS was off between March 14 and March 19, 2015, due to a broken OWS transfer pump. The pump was replaced and the system was restarted on March 19, 2015.

The GWTS was off between March 20 and March 23, 2015, due to a faulty level switch on the OWS transfer tank. Repair of the level switch was made and the system was restarted on March 23, 2015.

The GWTS was off between March 24 and March 25, 2015, due to a high level tank alarm. The system was restarted on March 25, 2015.

The GWTS was off on March 26, 2015, for troubleshooting of the level switch in the OWS transfer tank. The system was restarted later that same day.

The GWTS was off on March 30 and March 31, 2015, due to a high product tank alarm. A mixture of water and product from the OWS drained to the product tank and vapor‐phase granular activated carbon (VGAC) drums due to a loose fitting. The product tank was emptied and the VGAC drums were replaced, and the system was restarted on March 31, 2015.

Routine Effluent Monitoring Effluent water samples were collected pursuant to the Waste Discharge Requirements (WDRs) under Order No. R4‐2011‐0095. Samples were collected at the Order‐designated monitoring point EFF‐001 (Remediation System Effluent). Samples were transported to Advanced Technology Laboratories (ATL) in Las Vegas, Nevada, for analysis. ATL is certified by the National Environmental Laboratory Accreditation Program and the California Department of Public Health Environmental Laboratory Accreditation Program. The samples were analyzed in accordance with current U.S. Environmental Protection Agency (EPA) guidelines or as specified in the WDRs for the site. Analytical results for the monthly and quarterly effluent monitoring are summarized in Tables 2 and 3. Laboratory analytical reports and chain‐of‐custody documents are included in Appendix A.

Summary of Compliance Results As shown in Tables 1 and 2, the results of the monthly and quarterly effluent monitoring indicate that all discharge limitations were met during the reporting period.

MR. STEPHEN DEFIBAUGH PAGE 3 MAY 15, 2014

EN0501151007SCO

Waste Hauling Approximately 1,700 gallons of non‐Resource Conservation and Recovery Act (RCRA) hazardous waste liquids (oily water) were removed from the site on February 3, 2015, by Patriot Environmental Services (508 East E Street, Wilmington, California 90744). The waste was transported to Demenno/Kerdoon at 2000 North Alameda Street, Compton, California 90222.

Approximately 2,200 gallons of non‐RCRA hazardous waste liquids (oily water) were removed from the site on March 18, 2015, by Patriot Environmental Services. The waste was transported to Demenno/Kerdoon.

Approximately 400 pounds of non‐RCRA hazardous waste solids (filters) were removed from the site on March 23, 2015, by Environmental Logistics, Inc. (140 West Monte Avenue, Bloomington, California 92316). The waste was transported to Filter Recycling Services, Inc., at 180 West Monte Avenue, Bloomington, California 92316.

Approximately 2,000 pounds of nonhazardous spent carbon were removed from the site on March 24, 2015, by Prominent Systems, Inc. (13095 East Temple Avenue, City of Industry, California, 91746). The waste was transported to California Carbon Company at 2825 East Grant Street, Wilmington, California 90744.

Copies of the waste manifests are included in Appendix B.

Should you require any further information, please contact me at (714) 435‐6194.

Sincerely,

CH2M HILL Engineers, Inc.

Vidal Cortes Project Engineer

Attachments: Table 1 – Effluent Flow Rate Measurements, First Quarter 2015 Table 2 – NPDES Effluent Monitoring, Monthly and Quarterly Events, First Quarter 2015 Table 3 – NPDES Effluent Monitoring, Other Priority Pollutants, First Quarter 2015 Appendix A – Laboratory Analytical Reports and Chain‐of‐Custody Documents Appendix B – Waste Manifests

EN0501151007SCO

Tables

01/01/15 10,91301/02/15 10,82101/03/15 10,68701/04/15 10,74201/05/15 10,68001/06/15 10,81101/07/15 11,04501/08/15 11,60801/09/15 11,61801/10/15 11,47601/11/15 11,65801/12/15 11,87101/13/15 11,55401/14/15 11,42201/15/15 11,59601/16/15 10,36801/17/15 7,83701/18/15 7,92701/19/15 7,78101/20/15 7,65401/21/15 7,52801/22/15 7,58401/23/15 7,53901/24/15 7,54101/25/15 6,64901/26/15 6,67101/27/15 6,62401/28/15 10,34501/29/15 13,32301/30/15 14,40201/31/15 14,51002/01/15 14,20702/02/15 14,06602/03/15 13,88802/04/15 11,28802/05/15 13,95202/06/15 13,89802/07/15 14,04902/08/15 14,40502/09/15 14,44302/10/15 14,36902/11/15 13,97602/12/15 14,10202/13/15 13,68102/14/15 12,67902/15/15 12,36302/16/15 12,45402/17/15 12,38802/18/15 12,25402/19/15 12,24902/20/15 12,21802/21/15 12,33002/22/15 12,04502/23/15 12,29602/24/15 11,97002/25/15 12,50602/26/15 13,32602/27/15 13,75302/28/15 14,863

Date

Average Flow Rate (gpd)

(Maximum Daily Discharge Limit = 150,000 gpd1)

TABLE 1

SFPP Norwalk Pump Station, Norwalk, CaliforniaEffluent Flow Rate Measurements, First Quarter 2015

EN0501151007SCO Page 1 of 2

Date

Average Flow Rate (gpd)

(Maximum Daily Discharge Limit = 150,000 gpd1)

TABLE 1

SFPP Norwalk Pump Station, Norwalk, CaliforniaEffluent Flow Rate Measurements, First Quarter 2015

03/01/15 16,69203/02/15 16,64103/03/15 16,32703/04/15 9,04503/05/15 13,22703/06/15 13,19603/07/15 10,92603/08/15 13,96603/09/15 13,50303/10/15 13,89903/11/15 13,43003/12/15 11,27103/13/15 11,38403/14/15 11,74403/15/15 5,73903/16/15 003/17/15 303/18/15 1003/19/15 003/20/15 103/21/15 5303/22/15 1003/23/15 1403/24/15 3,92503/25/15 6,86703/26/15 5,17203/27/15 9,59803/28/15 10,57003/29/15 10,07503/30/15 8,76903/31/15 7,259

Notes1. California Regional Water Quality Control Board Waste Discharge Requirements (WDRs).gpd = gallons per day


MonthlyAverage

DailyMaximum

Temperature Monthly -- °F -- -- NE -- 80 84.1 -- 71.4 -- 86Oil and Grease Monthly EPA 1664A mg/L 0.88 4.4 NE <0.82 -- <0.86 -- <0.88 10 15TPH as gas (C4-C12) Monthly EPA 8015B µg/L 16 50 NE <16 -- <16 -- <16 -- --TPH as Diesel (C13-C22) Monthly EPA 8015B µg/L 15 25 NE <15 -- <15 -- <15 -- --TPH as Oil (C23+) Monthly EPA 8015B µg/L 14 25 NE <14 -- <14 -- <14 -- --Total TPH Monthly EPA 8015B µg/L 22 51 NE <22 -- <22 -- <22 NE 100Settleable Solids Monthly SM 2540F mL/L/hr 0.1 0.1 NE <0.1 -- <0.1 -- <0.1 0.1 0.3Total Suspended Solids Monthly SM 2540D mg/L 10 10 NE <10 -- <10 -- <10 50 75Phenolics Monthly EPA 420.1 µg/L 150 300 50 <150 -- <150 -- <150 300 NEBenzene Monthly EPA 8260B µg/L 0.048 1 2.0 <0.048 -- <0.048 -- <0.048 1 NE1,1-Dichloroethane Monthly EPA 8260B µg/L 0.054 0.5 1.0 <0.054 -- <0.054 -- <0.054 5 NE1,2-Dichloroethane Monthly EPA 8260B µg/L 0.04 0.5 2.0 <0.044 -- <0.044 -- <0.044 0.5 NEEthylbenzene Monthly EPA 8260B µg/L 0.036 1 2.0 <0.036 -- <0.036 -- <0.036 10 NEToluene Monthly EPA 8260B µg/L 0.025 2 2.0 <0.025 -- <0.025 -- <0.025 10 NEMethyl tertiary-butyl ether Monthly EPA 8260B µg/L 0.098 1 NE <0.098 -- <0.098 -- <0.098 NE 5.0Tertiary butyl alcohol Monthly EPA 8260B µg/L 0.4 5 NE <0.4 -- <0.4 -- <0.4 NE 12Total Xylenes Monthly EPA 8260B µg/L 1.5 2 NE <1.5 -- <1.5 -- <1.5 10 NECopper (total recoverable) (dry weather) Monthly EPA 200.8 µg/L 0.04 0.5 0.5 <0.04 -- <0.04 -- <0.04 16 33Copper (total recoverable) (wet weather) Monthly EPA 200.8 µg/L 0.04 0.5 0.5 <0.04 -- <0.04 -- <0.04 13 27Lead (total recoverable) (dry weather) Monthly EPA 200.8 µg/L 0.011 0.5 0.5 <0.011 -- <0.011 -- <0.011 8.2 15Lead (total recoverable) (wet weather) Monthly EPA 200.8 µg/L 0.011 0.5 0.5 <0.011 -- <0.011 -- <0.011 34 106Mercury (total recoverable) Monthly EPA 245.1 µg/L 0.018 0.05 0.2 <0.018 -- <0.018 -- <0.018 0.051 0.14Selenium (total recoverable) Monthly EPA 200.8 µg/L 0.069 0.5 2.0 <0.069 -- <0.069 -- <0.069 3.4 9.2Thallium (total recoverable) Monthly EPA 200.8 µg/L 0.008 0.5 1.0 <0.008 -- 0.086 J -- 0.067 J 6.3 13

Zinc (total recoverable) (wet weather) 4 Monthly EPA 200.8 µg/L 0.23 10 1.0 0.5 J -- 1.2 J -- 1.1 J 79 158Chromium VI Monthly EPA 7199 µg/L 0.016 0.2 0.5 0.35 -- -- 0.56 1.1 8.1 16pH Quarterly -- s.u. -- -- NE -- 7.2 -- -- -- -- 6.5/8.5Ammonia Nitrogen (as N) Quarterly SM 4500 NH3C mg/L 0.05 0.1 NE <0.05 -- -- -- -- NE NEDi-isopropyl Ether Quarterly EPA 8260B µg/L 0.034 1 NE <0.034 -- -- -- -- NE NEMethylene Blue Active Substances Quarterly SM 5540C mg/L 0.05 0.05 NE <0.05 -- -- -- -- NE NETert-amyl-methyl Ether Quarterly EPA 8260B µg/L 0.054 1 NE <0.054 -- -- -- -- NE NETurbidity Quarterly SM 2130B NTU 0.1 0.1 NE <0.1 -- -- -- -- 50 75Methyl ethyl ketone Quarterly EPA 8260B µg/L 0.7 10 NE <0.7 -- -- -- -- 50 NE

Notes1. ML is the concentration at which the entire analytical system must give a recognizable signal and acceptable calibration point. It is also the concentration in a samplethat is equivalent to the concentration of the lowest calibration standard analyzed by a specific analytical procedure, assuming that all the method specified sampleweights, volumes, and processing steps have been followed.2. California Regional Water Quality Control Board Waste Discharge Requirements (WDRs).3. The highest MDL and RL during this reporting period is shown.4. There are no dry weather limitations for zinc.

-- = not measured or not analyzed.

AbbreviationsBOD = biological oxygen demand (5 days at 20 degrees Celsius)° F = degrees FahrenheitDNQ = detected, but not quantified. Result is greater than or equal to the laboratory MDL but less than the ML (or RL if no ML is listed).J = detected at a concentration below the RL and above the MDL. Reported value is estimated.mg/L = milligrams per literµg/L = micrograms per liters.u. = standard unitsNTU = nephelometric turbidity unitsmL/L/hr = milliliters per liter per hour< = not detected above the MDLMDL = laboratory minimum detection limitRL = laboratory reporting limitML = minimum level. See note 1.NE = not established

2/13/2015 3/3/2015

TABLE 2

NPDES Effluent Monitoring, Monthly and Quarterly Events, First Quarter 2015SFPP Norwalk Pump Station, Norwalk, California

AnalyteSamplingFrequency

Analytical Method Units MDL3 RL3 ML1

Discharge Limits2

1/15/2015 1/27/2015 2/10/2015


Analyte Analytical Method Units MDL RL 1/15/2015 ML1

1,1,1-Trichloroethane EPA 8260B µg/L 0.072 1.0 <0.072 21,1,2,2-Tetrachloroethane EPA 8260B µg/L 0.10 1.0 <0.1 11,1,2-Trichloroethane EPA 8260B µg/L 0.042 1.0 <0.042 21,1-Dichloroethene EPA 8260B µg/L 0.16 1.0 <0.16 21,2,4-Trichlorobenzene EPA 8260B µg/L 0.1 1.0 <0.1 51,2-Dichlorobenzene EPA 8260B µg/L 0.048 1.0 <0.048 21,2-Dichloropropane EPA 8260B µg/L 0.094 1.0 <0.094 11,3-Dichlorobenzene EPA 8260B µg/L 0.061 1.0 <0.061 11,4-Dichlorobenzene EPA 8260B µg/L 0.078 1.0 <0.078 1Bromodichloromethane EPA 8260B µg/L 0.048 1.0 <0.048 2Bromoform EPA 8260B µg/L 0.061 1.0 <0.061 2Bromomethane EPA 8260B µg/L 0.073 1.0 <0.073 2cis-1,3-Dichloropropene EPA 8260B µg/L 0.043 1.0 <0.043 2Carbon Tetrachloride EPA 8260B µg/L 0.057 0.5 <0.057 2Chlorobenzene EPA 8260B µg/L 0.028 1.0 <0.028 2Chloroethane EPA 8260B µg/L 0.099 1.0 <0.099 2Chloroform EPA 8260B µg/L 0.048 1.0 <0.048 2Chloromethane EPA 8260B µg/L 0.043 1.0 0.16 J 2Dibromochloromethane EPA 8260B µg/L 0.057 1.0 <0.057 2Hexachlorobutadiene EPA 8260B µg/L 0.07 1.0 <0.07 1Methylene Chloride EPA 8260B µg/L 0.28 2.0 <0.28 2Naphthalene EPA 8260B µg/L 0.06 1.0 <0.062 1trans-1,2-Dichloroethene EPA 8260B µg/L 0.07 1.0 <0.074 1trans-1,3-Dichloropropene EPA 8260B µg/L 0.05 1.0 <0.051 2Tetrachloroethene EPA 8260B µg/L 0.12 1.0 <0.12 2Trichloroethene EPA 8260B µg/L 0.074 1.0 <0.074 2Vinyl Chloride EPA 8260B µg/L 0.044 0.5 <0.044 2

Note

AbbreviationsJ = detected at a concentration below the RL and above the MDL. Reported value is estimated.µg/L = micrograms per liter< = not detected above the MDLMDL = laboratory minimum detection limitML = minimum level. See note 1.RL = laboratory reporting limit

TABLE 3

NPDES Effluent Monitoring, Other Priority Pollutants, First Quarter 2015

SFPP Norwalk Pump Station, Norwalk, California

1. ML is the concentration at which the entire analytical system must give a recognizable signal and acceptable calibration point. It is also the concentration in a sample that is equivalent to the concentration of the lowest calibration standard analyzed by a specific analytical procedure, assuming that all the method specified sample weights, volumes, and processing steps have been followed.


EN0501151007SCO

Appendix A Laboratory Analytical Reports and

Chain-of-Custody Documents

NEVADA 3151 W. Post Rd., Las Vegas, NV 89118

P: 702.307.2659 F: 702.307.2691

“Serving Clients with Passion and Professionalism”

CALIFORNIA 11060 Artesia Blvd., Ste C, Cerritos, CA 90703

P: 562.219.7435 F: 562.219.7436

January 26, 2015

CH2MHill

Dan Jablonski

Attention: Dan Jablonski

RE: SFPP - Norwalk Site

Workorder No.: N014406FAX:

TEL:

1000 Wilshire Blvd.

Los Angeles, CA 90017

CA-ELAP No.: 2676

NV Cert. No.: NV-00922

Thank you for the opportunity to service the needs of your company.

Please feel free to call me at (702) 307-2659 if I can be of further assistance to your company.

Sincerely,

Glen Gesmundo

QA Manager

Enclosed are the results for sample(s) received on January 16, 2015 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications.

The cover letter is an integral part of this analytical report. This Laboratory Report cannot be reproduced in part or in its entirety without written permission from the client and Advanced Technology Laboratories - Las Vegas.

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26-Jan-15Date:ASSET Laboratories

Project: SFPP - Norwalk Site

CLIENT: CH2MHill

Lab Order: N014406CASE NARRATIVE

SAMPLE RECEIVING/GENERAL COMMENTS:

Samples were received intact with proper chain of custody documentation.

Cooler temperature and sample preservation were verified upon receipt of samples if applicable.

Information on sample receipt conditions including discrepancies can be found in attached Sample Receipt Checklist Form.

Samples were analyzed within method holding time.

Results were J-Flag. "J" is used to flag those results that are between the PQL (Practical Quantitation Limit) and the calculated MDL (Method Detection Limit). Results that are "J" Flagged are estimated values since it becomes difficult to accurately quantitate the analyte near the MDL.

Subcontracted Test:

Ammonia, MBAS and Phenols were subcontracted to AETL - Burbank, CA .

Analytical Comments for EPA 8260B:

Laboratory Control Sample (LCS) recovery biased high for 2-Butanone. Sample result was non-detect (ND) for this analyte therefore reanalysis of the sample was not necessary.

Page 2 of 25

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CLIENT: CH2MHill

Lab Order: N014406Work Order Sample Summary

Lab Sample ID Client Sample ID Collection DateMatrix Date Received

Contract No:

Date Reported

N014406-001A EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001B EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001C EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001D EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001E EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001F EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001G EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001H EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001I EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001J EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001K EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

N014406-001L EFF-01-15 1/15/2015 12:35:00 PM 1/16/2015 1/26/2015Wastewater

Page 1 of 1

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P: 562.219.7435 F: 562.219.7436


Client Sample ID: EFF-01-15

Collection Date: 1/15/2015 12:35:00 PM

Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014406

Lab ID: N014406-001

ASSET Laboratories Print Date: 26-Jan-15

Analyses Result Qual Units Date AnalyzedDFPQLMDL

ANALYTICAL RESULTS

TOTAL NON-FILTERABLE RESIDUESM2540D

Analyst: RBRunID: WETCHEM_150119E 48460QC Batch: PrepDate: 1/19/2015

Suspended Solids (Residue, Non-Filterable)

10 mg/L 1ND 10 1/19/2015 09:00 AM

SETTLEABLE MATTERSM2540F

Analyst: QBMRunID: WETCHEM_150118A 48531QC Batch: PrepDate: 1/18/2015

Settleable Matter 0.10 ml/L 1ND 0.10 1/18/2015

TURBIDITYSM 2130B

Analyst: RBRunID: WETCHEM_150117C R97645QC Batch: PrepDate:

Turbidity 0.10 NTU 1ND 0.10 1/17/2015

HEXANE EXTRACTABLE MATERIAL (HEM)EPA 1664 _HEM

Analyst: adminRunID: WETCHEM_150122A 48505QC Batch: PrepDate: 1/22/2015

Oil & Grease 4.1 mg/L 1ND 0.82 1/22/2015 10:00 AM

VOLATILE ORGANIC COMPOUNDS BY GC/MSEPA 8260B

Analyst: QBMRunID: MS5_150118A P15VW013QC Batch: PrepDate:

1,1,1-Trichloroethane 1.0 ug/L 1ND 0.072 1/18/2015 05:00 PM

1,1,2,2-Tetrachloroethane 1.0 ug/L 1ND 0.10 1/18/2015 05:00 PM

1,1,2-Trichloroethane 1.0 ug/L 1ND 0.042 1/18/2015 05:00 PM

1,1-Dichloroethane 0.50 ug/L 1ND 0.054 1/18/2015 05:00 PM

1,1-Dichloroethene 1.0 ug/L 1ND 0.16 1/18/2015 05:00 PM

1,2,4-Trichlorobenzene 1.0 ug/L 1ND 0.10 1/18/2015 05:00 PM

1,2-Dichlorobenzene 1.0 ug/L 1ND 0.048 1/18/2015 05:00 PM


1,2-Dichloropropane 1.0 ug/L 1ND 0.094 1/18/2015 05:00 PM



2-Butanone 10 ug/L 1ND 0.70 1/18/2015 05:00 PM

Benzene 1.0 ug/L 1ND 0.048 1/18/2015 05:00 PM

Bromodichloromethane 1.0 ug/L 1ND 0.048 1/18/2015 05:00 PM

Bromoform 1.0 ug/L 1ND 0.061 1/18/2015 05:00 PM

Bromomethane 1.0 ug/L 1ND 0.073 1/18/2015 05:00 PM

Qualifiers: B Analyte detected in the associated Method Blank E Value above quantitation range

H Holding times for preparation or analysis exceeded J Analyte detected below quantitation limits

ND Not Detected at the Reporting Limit S Spike/Surrogate outside of limits due to matrix interference

Results are wet unless otherwise specified DO Surrogate Diluted Out

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Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014406

Lab ID: N014406-001



ANALYTICAL RESULTS



Carbon tetrachloride 0.50 ug/L 1ND 0.057 1/18/2015 05:00 PM

Chlorobenzene 1.0 ug/L 1ND 0.028 1/18/2015 05:00 PM

Chloroethane 1.0 ug/L 1ND 0.099 1/18/2015 05:00 PM

Chloroform 1.0 ug/L 1ND 0.048 1/18/2015 05:00 PM

Chloromethane J1.0 ug/L 10.16 0.043 1/18/2015 05:00 PM

cis-1,3-Dichloropropene 1.0 ug/L 1ND 0.043 1/18/2015 05:00 PM

Di-isopropyl ether 1.0 ug/L 1ND 0.034 1/18/2015 05:00 PM

Dibromochloromethane 1.0 ug/L 1ND 0.057 1/18/2015 05:00 PM

Ethylbenzene 1.0 ug/L 1ND 0.036 1/18/2015 05:00 PM

Hexachlorobutadiene 1.0 ug/L 1ND 0.070 1/18/2015 05:00 PM

m,p-Xylene 1.0 ug/L 1ND 0.14 1/18/2015 05:00 PM

Methylene chloride 2.0 ug/L 1ND 0.28 1/18/2015 05:00 PM

MTBE 1.0 ug/L 1ND 0.098 1/18/2015 05:00 PM

Naphthalene 1.0 ug/L 1ND 0.062 1/18/2015 05:00 PM

o-Xylene 1.0 ug/L 1ND 0.042 1/18/2015 05:00 PM

Tert-amyl methyl ether 1.0 ug/L 1ND 0.054 1/18/2015 05:00 PM

Tert-Butanol 5.0 ug/L 1ND 0.40 1/18/2015 05:00 PM

Tetrachloroethene 1.0 ug/L 1ND 0.12 1/18/2015 05:00 PM

Toluene 2.0 ug/L 1ND 0.025 1/18/2015 05:00 PM

trans-1,2-Dichloroethene 1.0 ug/L 1ND 0.074 1/18/2015 05:00 PM

trans-1,3-Dichloropropene 1.0 ug/L 1ND 0.051 1/18/2015 05:00 PM

Trichloroethene 1.0 ug/L 1ND 0.074 1/18/2015 05:00 PM

Vinyl chloride 0.50 ug/L 1ND 0.044 1/18/2015 05:00 PM

Xylenes, Total 2.0 ug/L 1ND 1.5 1/18/2015 05:00 PM

Surr: 1,2-Dichloroethane-d4 72-119 %REC 192.5 0 1/18/2015 05:00 PM

Surr: 4-Bromofluorobenzene 76-119 %REC 191.8 0 1/18/2015 05:00 PM

Surr: Dibromofluoromethane 85-115 %REC 197.0 0 1/18/2015 05:00 PM

Surr: Toluene-d8 81-120 %REC 1100 0 1/18/2015 05:00 PM

TPH EXTRACTABLE BY GC/FIDEPA 8015B

Analyst: MDM

EPA 3510C

RunID: GC3_150119A 48456QC Batch: PrepDate: 1/19/2015

TPH-Diesel (C13-C22) 25 ug/L 1ND 15 1/19/2015 04:06 PM

TPH-Oil (C23-C36) 25 ug/L 1ND 14 1/19/2015 04:06 PM

Surr: Octacosane 26-152 %REC 180.3 0 1/19/2015 04:06 PM

Surr: p-Terphenyl 57-132 %REC 177.9 0 1/19/2015 04:06 PM





05 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436




Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014406

Lab ID: N014406-001



ANALYTICAL RESULTS

GASOLINE RANGE ORGANICS BY GC/FIDEPA 8015B

Analyst: QBMRunID: GC4_150119A E15VW005QC Batch: PrepDate:

TPH-Gasoline (C4-C12) 50 ug/L 1ND 16 1/19/2015 11:10 AM

Surr: Chlorobenzene - d5 74-138 %REC 1108 0 1/19/2015 11:10 AM

HEXAVALENT CHROMIUM BY ICEPA 7199

Analyst: RBRunID: IC6_150116A R97567QC Batch: PrepDate:

Hexavalent Chromium 0.20 µg/L 10.35 0.016 1/16/2015 11:57 AM

MERCURY BY COLD VAPOR TECHNIQUEEPA 245.1

Analyst: CEIRunID: AA1_150120A 48471QC Batch: PrepDate: 1/20/2015

Mercury 0.050 µg/L 1ND 0.018 1/20/2015 04:27 PM

TOTAL METALS BY COLLISION/REACTION CELL ICPMSEPA 200.8

Analyst: CEIRunID: ICP7_150119C 48466QC Batch: PrepDate: 1/19/2015

Selenium 0.50 µg/L 1ND 0.069 1/20/2015 06:21 AM

TOTAL METALS BY ICPMSEPA 200.8

Analyst: CEIRunID: ICP7_150119C 48466QC Batch: PrepDate: 1/19/2015

Copper 0.50 µg/L 1ND 0.040 1/20/2015 06:21 AM

Lead 0.50 µg/L 1ND 0.011 1/20/2015 06:21 AM

Thallium 0.50 µg/L 1ND 0.0080 1/20/2015 06:21 AM

Zinc J10 µg/L 10.50 0.23 1/20/2015 06:21 AM

TOTAL TPHEPA 8015B

Analyst: MDM

EPA 3510C


Total TPH 50 ug/L 1ND 22 1/19/2015 04:06 PM





06 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill

Work Order: N014406ANALYTICAL QC SUMMARY REPORT

TestCode: 160.2_2540D_W

Sample ID: MB-48460

Batch ID: 48460 TestNo: SM2540D Analysis Date: 1/19/2015

Prep Date: 1/19/2015

Analyte Result SPK value SPK Ref Val %REC RPD Ref Val %RPDLowLimit HighLimit RPDLimit Qual

Units: mg/L

PQL

Client ID: PBW

RunNo: 97654

SeqNo: 1915166

MBLKSampType: TestCode: 160.2_2540D

Suspended Solids (Residue, Non-Filter 10ND

Sample ID: LCS-48460




Units: mg/L

PQL

Client ID: LCSW

RunNo: 97654

SeqNo: 1915167

LCSSampType: TestCode: 160.2_2540D

Suspended Solids (Residue, Non-Filter 1000 92.3 80 12010 0923.000

Sample ID: N014406-001DDUP




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 97654

SeqNo: 1915172

DUPSampType: TestCode: 160.2_2540D

Suspended Solids (Residue, Non-Filter 510 0 0ND

Qualifiers:

B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or analysis exceeded

J Analyte detected below quantitation limits ND Not Detected at the Reporting Limit R RPD outside accepted recovery limits

S Spike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values

07 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 160.5_2540F_W

Sample ID: MB-48531

Batch ID: 48531 TestNo: SM2540F Analysis Date: 1/18/2015



Units: ml/L

PQL

Client ID: PBW

RunNo: 97712

SeqNo: 1918519

MBLKSampType: TestCode: 160.5_2540F_

Settleable Matter 0.10ND

Qualifiers:




08 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 1664_HEM_W

Sample ID: MB-R97671

Batch ID: 48505 TestNo: EPA 1664 _H Analysis Date: 1/22/2015



Units: mg/L

PQL

Client ID: PBW

RunNo: 97671

SeqNo: 1916699

MBLKSampType: TestCode: 1664_HEM_W

Oil & Grease 4.0ND

Sample ID: LCS-R97671




Units: mg/L

PQL

Client ID: LCSW

RunNo: 97671

SeqNo: 1916700

LCSSampType: TestCode: 1664_HEM_W

Oil & Grease 40.00 104 78 1144.0 041.500

Sample ID: N014406-001G-MS




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 97671

SeqNo: 1916702

MSSampType: TestCode: 1664_HEM_W

Oil & Grease 40.82 79.0 78 1144.1 032.245

Sample ID: N014406-001G-MSD




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 97671

SeqNo: 1916703

MSDSampType: TestCode: 1664_HEM_W

Oil & Grease 40.82 78.2 78 114 184.1 0 32.24 0.95431.939

Qualifiers:




09 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 200.8_W_DRC

Sample ID: MB-48466

Batch ID: 48466 TestNo: EPA 200.8 Analysis Date: 1/20/2015



Units: µg/L

PQL

Client ID: PBW

RunNo: 97627

SeqNo: 1913661

MBLKSampType: TestCode: 200.8_W_DR

Selenium 0.50ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 97627

SeqNo: 1913662

LCSSampType: TestCode: 200.8_W_DR

Selenium 10.00 96.8 85 1150.50 09.678

Sample ID: N014406-001E-MS




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97627

SeqNo: 1913666

MSSampType: TestCode: 200.8_W_DR

Selenium 10.00 87.9 75 1250.50 08.793

Sample ID: N014406-001E-MSD




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97627

SeqNo: 1913667

MSDSampType: TestCode: 200.8_W_DR

Selenium 10.00 91.3 75 125 200.50 0 8.793 3.729.127

Qualifiers:




10 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 200.8_W_SFPP

Sample ID: MB-48466




Units: µg/L

PQL

Client ID: PBW

RunNo: 97627

SeqNo: 1913821

MBLKSampType: TestCode: 200.8_W_SFP

Copper 0.50ND

Lead J0.500.083

Thallium 0.50ND

Zinc 10ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 97627

SeqNo: 1913822

LCSSampType: TestCode: 200.8_W_SFP

Copper 10.00 109 85 1150.50 010.947

Lead 10.00 108 85 1150.50 010.834

Thallium 10.00 110 85 1150.50 010.982

Zinc 100.0 100 85 11510 0100.447





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97627

SeqNo: 1913826

MSSampType: TestCode: 200.8_W_SFP

Copper 10.00 75.7 75 1250.50 07.570

Lead 10.00 104 75 1250.50 010.357

Thallium 10.00 106 75 1250.50 010.610

Zinc 100.0 83.1 75 12510 0.496683.632





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97627

SeqNo: 1913827

MSDSampType: TestCode: 200.8_W_SFP

Copper 10.00 77.4 75 125 200.50 0 7.570 2.287.745

Lead 10.00 103 75 125 200.50 0 10.36 0.71410.283

Qualifiers:




11 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill







Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97627

SeqNo: 1913827


Thallium 10.00 106 75 125 200.50 0 10.61 0.48010.559

Zinc 100.0 84.3 75 125 2010 0.4966 83.63 1.4184.821

Qualifiers:




12 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 2130_W

Sample ID: N014406-001DDUP

Batch ID: R97645 TestNo: SM 2130B Analysis Date: 1/17/2015

Prep Date:


Units: NTU

PQL

Client ID: ZZZZZZ

RunNo: 97645

SeqNo: 1914973

DUPSampType: TestCode: 2130_W

Turbidity 300.10 0 0ND

Qualifiers:




13 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 245.1_W_LL

Sample ID: MB-48471




Units: µg/L

PQL

Client ID: PBW

RunNo: 97624

SeqNo: 1913217

MBLKSampType: TestCode: 245.1_W_LL

Mercury 0.050ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 97624

SeqNo: 1913220

LCSSampType: TestCode: 245.1_W_LL

Mercury 2.500 102 85 1150.050 02.551





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97624

SeqNo: 1913221

MSSampType: TestCode: 245.1_W_LL

Mercury 2.500 104 75 1250.050 02.597





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97624

SeqNo: 1913222

MSDSampType: TestCode: 245.1_W_LL

Mercury 2.500 105 75 125 200.050 0 2.597 1.012.623

Qualifiers:




14 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 7199_WPGE


Batch ID: R97567 TestNo: EPA 7199 Analysis Date: 1/16/2015

Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 97567

SeqNo: 1910495

MBLKSampType: TestCode: 7199_WPGE

Hexavalent Chromium 0.20ND



Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 97567

SeqNo: 1910496

LCSSampType: TestCode: 7199_WPGE

Hexavalent Chromium 5.000 100 90 1100.20 05.023

Sample ID: N014403-001A-DUP


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97567

SeqNo: 1910498

DUPSampType: TestCode: 7199_WPGE

Hexavalent Chromium 200.20 1.763 0.4871.772

Sample ID: N014403-001A-MSD


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97567

SeqNo: 1910499

MSDSampType: TestCode: 7199_WPGE

Hexavalent Chromium 1.000 108 85 115 200.20 1.763 2.815 0.8382.838

Sample ID: N014403-001A-MS


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97567

SeqNo: 1910504

MSSampType: TestCode: 7199_WPGE

Hexavalent Chromium 1.000 105 85 1150.20 1.7632.815

Qualifiers:




15 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 7199_WPGE

Sample ID: N014406-001F-REP


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97567

SeqNo: 1910508



Qualifiers:




16 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 8015_W_FP_SFPP

Sample ID: MB-48456

Batch ID: 48456 TestNo: EPA 8015B Analysis Date: 1/19/2015



Units: ug/L

PQL

Client ID: PBW

RunNo: 97608

SeqNo: 1912272

MBLKSampType: TestCode: 8015_W_FP_

EPA 3510C

TPH-Diesel (C13-C22) 25ND

TPH-Oil (C23-C36) 25ND

Surr: Octacosane 80.00 98.1 26 15278.519

Surr: p-Terphenyl 80.00 94.8 57 13275.866

Qualifiers:




17 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 8015_W_SFPPTOT

Sample ID: MB-48456




Units: ug/L

PQL

Client ID: PBW

RunNo: 97608

SeqNo: 1912710

MBLKSampType: TestCode: 8015_W_SFP

EPA 3510C

Total TPH 500

Qualifiers:




18 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 8015GAS_WSFPP

Sample ID: E150119LCS

Batch ID: E15VW005 TestNo: EPA 8015B Analysis Date: 1/19/2015

Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 97613

SeqNo: 1912724

LCSSampType: TestCode: 8015GAS_WS

TPH-Gasoline (C4-C12) 1000 88.0 67 13650 0880.000

Surr: Chlorobenzene - d5 50000 102 74 13850933.000

Sample ID: E150119MB1


Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97613

SeqNo: 1912725

MBLKSampType: TestCode: 8015GAS_WS

TPH-Gasoline (C4-C12) 50ND


Sample ID: N014406-001JMS


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97613

SeqNo: 1912727

MSSampType: TestCode: 8015GAS_WS

TPH-Gasoline (C4-C12) 1000 91.7 67 13650 0917.000


Sample ID: N014406-001JMSD


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97613

SeqNo: 1912728

MSDSampType: TestCode: 8015GAS_WS

TPH-Gasoline (C4-C12) 1000 93.3 67 136 3050 0 917.0 1.73933.000

Surr: Chlorobenzene - d5 50000 110 74 138 0055081.000

Qualifiers:




19 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 8260_WP_SFPP

Sample ID: P150118LCS

Batch ID: P15VW013 TestNo: EPA 8260B Analysis Date: 1/18/2015

Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 97604

SeqNo: 1911833

LCSSampType: TestCode: 8260_WP_SF

1,1,1-Trichloroethane 20.00 90.8 67 1321.0 018.150

1,1,2,2-Tetrachloroethane 20.00 97.3 63 1281.0 019.450

1,1,2-Trichloroethane 20.00 100 75 1251.0 020.090

1,1-Dichloroethane 20.00 85.7 69 1330.50 017.130

1,1-Dichloroethene 20.00 88.6 68 1301.0 017.720

1,2,4-Trichlorobenzene 20.00 92.2 66 1341.0 018.440

1,2-Dichlorobenzene 20.00 107 71 1221.0 021.380

1,2-Dichloroethane 20.00 92.6 69 1320.50 018.510

1,2-Dichloropropane 20.00 88.0 75 1251.0 017.610

1,3-Dichlorobenzene 20.00 98.8 75 1241.0 019.760


2-Butanone 200.0 150 49 136 S10 0300.810

Benzene 20.00 96.8 81 1221.0 019.350

Bromodichloromethane 20.00 108 76 1211.0 021.670

Bromoform 20.00 115 69 1281.0 022.940

Bromomethane 20.00 72.7 53 1411.0 014.540

Carbon tetrachloride 20.00 126 66 1380.50 025.280

Chlorobenzene 20.00 96.4 81 1221.0 019.280

Chloroethane 20.00 89.2 58 1331.0 017.830

Chloroform 20.00 89.9 69 1281.0 017.980

Chloromethane 20.00 62.0 56 1311.0 012.390

cis-1,3-Dichloropropene 20.00 98.7 69 1311.0 019.740

Di-isopropyl ether 20.00 78.8 70 1301.0 015.770

Dibromochloromethane 20.00 117 66 1331.0 023.420

Ethylbenzene 20.00 94.3 73 1271.0 018.850

Hexachlorobutadiene 20.00 104 67 1311.0 020.820

m,p-Xylene 40.00 95.8 76 1281.0 038.300

Methylene chloride 20.00 85.0 63 1372.0 017.010

MTBE 20.00 87.3 65 1231.0 017.460

Naphthalene 20.00 102 54 1381.0 020.350

Qualifiers:




20 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 97604

SeqNo: 1911833


o-Xylene 20.00 95.6 80 1211.0 019.110

Tert-amyl methyl ether 20.00 94.4 70 1301.0 018.890

Tert-Butanol 100.0 86.8 70 1305.0 086.780

Tetrachloroethene 20.00 94.2 66 1281.0 018.840

Toluene 20.00 99.5 77 1222.0 019.900

trans-1,2-Dichloroethene 20.00 91.1 63 1371.0 018.210

trans-1,3-Dichloropropene 20.00 102 59 1351.0 020.440

Trichloroethene 20.00 100 70 1271.0 020.070

Vinyl chloride 20.00 84.1 50 1340.50 016.820

Xylenes, Total 60.00 95.7 75 1252.0 057.410

Surr: 1,2-Dichloroethane-d4 25.00 90.2 72 11922.560

Surr: 4-Bromofluorobenzene 25.00 101 76 11925.200

Surr: Dibromofluoromethane 25.00 95.0 85 11523.760

Surr: Toluene-d8 25.00 100 81 12025.120

Sample ID: N014413-001AMS


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97604

SeqNo: 1911834

MSSampType: TestCode: 8260_WP_SF

1,1,1-Trichloroethane 20.00 93.8 67 1321.0 018.770

1,1,2,2-Tetrachloroethane 20.00 104 63 1281.0 020.880

1,1,2-Trichloroethane 20.00 109 75 1251.0 021.730

1,1-Dichloroethane 20.00 87.9 69 1330.50 017.580

1,1-Dichloroethene 20.00 90.6 68 1301.0 018.120

1,2,4-Trichlorobenzene 20.00 93.6 66 1341.0 018.710


1,2-Dichloroethane 20.00 97.6 69 1320.50 019.520

1,2-Dichloropropane 20.00 92.5 75 1251.0 018.490



Qualifiers:




21 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97604

SeqNo: 1911834


2-Butanone 200.0 85.8 49 13610 0171.500

Benzene 20.00 99.1 81 1221.0 019.820

Bromodichloromethane 20.00 111 76 1211.0 022.200

Bromoform 20.00 123 69 1281.0 024.520

Bromomethane 20.00 76.5 53 1411.0 015.290

Carbon tetrachloride 20.00 119 66 1380.50 023.790

Chlorobenzene 20.00 103 81 1221.0 020.670

Chloroethane 20.00 92.2 58 1331.0 018.430

Chloroform 20.00 93.2 69 1281.0 018.630

Chloromethane 20.00 65.3 56 1311.0 013.050

cis-1,3-Dichloropropene 20.00 100 69 1311.0 020.010

Di-isopropyl ether 20.00 83.4 70 1301.0 016.670

Dibromochloromethane 20.00 124 66 1331.0 024.830

Ethylbenzene 20.00 98.2 73 1271.0 019.640

Hexachlorobutadiene 20.00 105 67 1311.0 021.030

m,p-Xylene 40.00 99.7 76 1281.0 039.860

Methylene chloride 20.00 87.2 63 1372.0 017.440

MTBE 20.00 92.5 65 1231.0 018.500

Naphthalene 20.00 106 54 1381.0 021.100

o-Xylene 20.00 101 80 1211.0 020.180

Tert-amyl methyl ether 20.00 97.9 70 1301.0 019.570

Tert-Butanol 100.0 88.7 70 1305.0 088.740

Tetrachloroethene 20.00 97.9 66 1281.0 019.580

Toluene 20.00 102 77 1222.0 020.480

trans-1,2-Dichloroethene 20.00 92.2 63 1371.0 018.450

trans-1,3-Dichloropropene 20.00 104 59 1351.0 020.820

Trichloroethene 20.00 104 70 1271.0 020.720

Vinyl chloride 20.00 85.2 50 1340.50 017.050

Xylenes, Total 60.00 100 75 1252.0 060.040


Qualifiers:




22 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97604

SeqNo: 1911834




Surr: Toluene-d8 25.00 100 81 12025.060

Sample ID: N014413-001AMSD


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97604

SeqNo: 1911835

MSDSampType: TestCode: 8260_WP_SF

1,1,1-Trichloroethane 20.00 92.8 67 132 201.0 0 18.77 1.1318.560

1,1,2,2-Tetrachloroethane 20.00 103 63 128 201.0 0 20.88 0.96220.680

1,1,2-Trichloroethane 20.00 105 75 125 201.0 0 21.73 3.2721.030

1,1-Dichloroethane 20.00 85.0 69 133 200.50 0 17.58 3.4116.990

1,1-Dichloroethene 20.00 87.3 68 130 201.0 0 18.12 3.7117.460

1,2,4-Trichlorobenzene 20.00 87.4 66 134 201.0 0 18.71 6.8517.470

1,2-Dichlorobenzene 20.00 107 71 122 201.0 0 22.33 4.6321.320

1,2-Dichloroethane 20.00 95.9 69 132 200.50 0 19.52 1.7619.180

1,2-Dichloropropane 20.00 92.5 75 125 201.0 0 18.49 018.490

1,3-Dichlorobenzene 20.00 98.4 75 124 201.0 0 20.45 3.8919.670

1,4-Dichlorobenzene 20.00 102 74 123 201.0 0 20.87 2.3320.390

2-Butanone 200.0 84.9 49 136 2010 0 171.5 1.04169.730

Benzene 20.00 99.4 81 122 201.0 0 19.82 0.35319.890

Bromodichloromethane 20.00 109 76 121 201.0 0 22.20 2.0921.740

Bromoform 20.00 120 69 128 201.0 0 24.52 2.3523.950

Bromomethane 20.00 73.9 53 141 201.0 0 15.29 3.3914.780

Carbon tetrachloride 20.00 124 66 138 200.50 0 23.79 4.2824.830

Chlorobenzene 20.00 97.9 81 122 201.0 0 20.67 5.4719.570

Chloroethane 20.00 87.4 58 133 201.0 0 18.43 5.3517.470

Chloroform 20.00 89.8 69 128 201.0 0 18.63 3.6117.970

Chloromethane 20.00 60.6 56 131 201.0 0 13.05 7.3112.130

cis-1,3-Dichloropropene 20.00 99.2 69 131 201.0 0 20.01 0.80319.850

Qualifiers:




23 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: N014413-001AMSD


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97604

SeqNo: 1911835


Di-isopropyl ether 20.00 79.8 70 130 201.0 0 16.67 4.3515.960

Dibromochloromethane 20.00 120 66 133 201.0 0 24.83 3.7823.910

Ethylbenzene 20.00 95.0 73 127 201.0 0 19.64 3.3718.990

Hexachlorobutadiene 20.00 94.5 67 131 201.0 0 21.03 10.718.900

m,p-Xylene 40.00 94.0 76 128 201.0 0 39.86 5.8437.600

Methylene chloride 20.00 86.4 63 137 202.0 0 17.44 0.92217.280

MTBE 20.00 89.3 65 123 201.0 0 18.50 3.5217.860

Naphthalene 20.00 99.2 54 138 201.0 0 21.10 6.1619.840

o-Xylene 20.00 96.2 80 121 201.0 0 20.18 4.7219.250

Tert-amyl methyl ether 20.00 95.5 70 130 201.0 0 19.57 2.4319.100

Tert-Butanol 100.0 101 70 130 205.0 0 88.74 12.7100.790

Tetrachloroethene 20.00 92.1 66 128 201.0 0 19.58 6.1118.420

Toluene 20.00 100 77 122 202.0 0 20.48 2.3220.010

trans-1,2-Dichloroethene 20.00 90.8 63 137 201.0 0 18.45 1.6418.150

trans-1,3-Dichloropropene 20.00 105 59 135 201.0 0 20.82 0.47920.920

Trichloroethene 20.00 103 70 127 201.0 0 20.72 0.92120.530

Vinyl chloride 20.00 83.2 50 134 200.50 0 17.05 2.4316.640

Xylenes, Total 60.00 94.8 75 125 202.0 0 60.04 5.4656.850

Surr: 1,2-Dichloroethane-d4 25.00 89.4 72 119 022.350

Surr: 4-Bromofluorobenzene 25.00 100 76 119 025.030

Surr: Dibromofluoromethane 25.00 94.6 85 115 023.640

Surr: Toluene-d8 25.00 101 81 120 025.250

Sample ID: P150118MB3


Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97604

SeqNo: 1911836

MBLKSampType: TestCode: 8260_WP_SF

1,1,1-Trichloroethane 1.0ND

1,1,2,2-Tetrachloroethane 1.0ND

1,1,2-Trichloroethane 1.0ND

Qualifiers:




24 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97604

SeqNo: 1911836


1,1-Dichloroethane 0.50ND

1,1-Dichloroethene 1.0ND

1,2,4-Trichlorobenzene 1.0ND

1,2-Dichlorobenzene 1.0ND


1,2-Dichloropropane 1.0ND



2-Butanone 10ND

Benzene 1.0ND

Bromodichloromethane 1.0ND

Bromoform 1.0ND

Bromomethane 1.0ND

Carbon tetrachloride 0.50ND

Chlorobenzene 1.0ND

Chloroethane 1.0ND

Chloroform 1.0ND

Chloromethane J1.00.190

cis-1,3-Dichloropropene 1.0ND

Di-isopropyl ether 1.0ND

Dibromochloromethane 1.0ND

Ethylbenzene 1.0ND

Hexachlorobutadiene 1.0ND

m,p-Xylene 1.0ND

Methylene chloride 2.0ND

MTBE 1.0ND

Naphthalene 1.0ND

o-Xylene 1.0ND

Tert-amyl methyl ether 1.0ND

Tert-Butanol 5.0ND

Qualifiers:




25 of 26


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97604

SeqNo: 1911836


Tetrachloroethene 1.0ND

Toluene 2.0ND

trans-1,2-Dichloroethene 1.0ND

trans-1,3-Dichloropropene 1.0ND

Trichloroethene 1.0ND

Vinyl chloride 0.50ND

Xylenes, Total 2.0ND


Surr: 4-Bromofluorobenzene 25.00 94.2 76 11923.560


Surr: Toluene-d8 25.00 99.9 81 12024.980

Qualifiers:




26 of 26

ASSET LaboratoriesPlease review the checklist below. Any NO signifies non-compliance. Any non-compliance will be noted and must be understood as having an impact on the quality of the data. All tests will be performed as requested regardless of any compliance issues.

If you have any questions or further instruction, please contact our Project Coordinator at (702) 307-2659.

Carrier name: Golden State Overnight

Cooler Received/Opened On: 1/16/2014

Rep sample Temp (Deg C): 4.6 IR Gun ID: 1

Temp Blank: Yes No

Last 4 digits of Tracking No.: 1091

Cooling process: Ice Ice Pack Dry Ice Other None

Packing Material Used: Bubble Wrap

Workorder: N014406

Sample Receipt Checklist

4. Chain of custody present? Yes No

6. Chain of custody signed when relinquished and received? Yes No

7. Chain of custody agrees with sample labels? Yes No

8. Samples in proper container/bottle? Yes No

9. Sample containers intact? Yes No

10. Sufficient sample volume for indicated test? Yes No

11. All samples received within holding time? Yes No

Yes No NA13. Water - VOA vials have zero headspace?

14. Water - pH acceptable upon receipt? Yes No NAExample: pH > 12 for (CN,S); pH<2 for Metals

1. Shipping container/cooler in good condition? Yes No Not Present

2. Custody seals intact, signed, dated on shippping container/cooler? Yes No Not Present

3. Custody seals intact on sample bottles? Yes No Not Present

5. Sampler's name present in COC? Yes No

12. Temperature of rep sample or Temp Blank within acceptable limit? Yes No NA

Yes No NA15. Did the bottle labels indicate correct preservatives used?

16. Were there Non-Conformance issues at login? Yes No NAWas Client notified? Yes No NA

Comments

Checklist Completed B JPG Reviewed By:

CHAIN-OF-CUSTODY RECORD Page 1 of 1

Sample ID Matrix Date Collected Bottle TypeRequested Tests

EPA 420.1 SM 5540 C SM4500-NH3C

Subcontractor:

AETL2834 North Naomi StreetBurbank, CA 91504

TEL: (818) 845-8200FAX: (818) 845-8840Acct #: 19-Jan-15

QC Level: RTNE

Field Sampler: James Dye

ASSET Laboratories3151-3153 W Post Rd., Las Vegas, NV 89118

TEL: 7023072659 FAX: 7023072691www.atl-labs.com

N014406-001A Wastewater 1/15/2015 12:35:00 PM 16OZP 1 / EFF-01-15N014406-001C Wastewater 1/15/2015 12:35:00 PM 32OZP 1 / EFF-01-15N014406-001I Wastewater 1/15/2015 12:35:00 PM 32OZA 1 / EFF-01-15

Relinquished by:

Relinquished by:

Received by:

Received by:

Date/TimeDate/Time

General Comments: Please email sample receipt acknowledgement to the PM.

Please use PO#: N14406A For questions, call Marlon at (702)-307-2659. Please e-mail results to [email protected] by: 5day TAT

Please analyze for Ammonia, Phenols and Surfactants.

http://www.atl-labs.com

mailto:[email protected]

Sample ID Client Sample ID Date Collected

Date Received:

Date Due Matrix Test No

WORK ORDER Summary 19-Jan-15

WorkOrder: N014406

Comments: Report to D. Jablonski/CH2M HILL, cc:KMEP. Direct Bill KMEP/SFPP-Steve Defibaugh-ref.AFE# 81195. "J" Flags required / Use lowest possible detection l

Client ID: CH2HI03

Project: SFPP - Norwalk Site QC Level: RTNE

Hld MS Sub

1/16/2015

Test Name

ASSET Laboratories

Storage

N014406-001A EFF-01-15 1/15/2015 12:35:00 PM 1/23/2015 Wastewater SM4500-NH3C AMMONIA-N SUB

N014406-001B 1/20/2015 EPA 8260B VOLATILE ORGANIC COMPOUNDS BY GC/MS

WV

N014406-001C 1/23/2015 SM 5540 C SURFACTANTS SUB

N014406-001D 1/23/2015 SM2540D TOTAL NON-FILTERABLE RESIDUE WW

1/23/2015 Total Suspended Solids Prep WW

1/23/2015 SM 2130B TURBIDITY WW

N014406-001E 1/23/2015 AQPREP TOTAL METALS: ICP, FLAA WW

1/23/2015 EPA 200.8 TOTAL METALS BY COLLISION/REACTION CELL ICPMS

WW

1/23/2015 EPA 200.8 TOTAL METALS BY ICPMS WW

1/23/2015 EPA 245.1 MERCURY BY COLD VAPOR TECHNIQUE

WW

1/23/2015 MERCURY PREP WW

N014406-001F 1/23/2015 EPA 7199 Hexavalent Chromium by IC WW

N014406-001G 1/23/2015 Oil and Grease Sample Prep WW

1/23/2015 EPA 1664 _HEM Hexane Extractable Material (HEM) WW

N014406-001H 1/23/2015 SM2540F SETTLEABLE MATTER WW

N014406-001I 1/23/2015 EPA 420.1 PHENOLICS SUB

N014406-001J 1/23/2015 EPA 8015B GASOLINE RANGE ORGANICS BY GC/FID

WV

N014406-001K 1/23/2015 EPA 3510C SEPARATORY FUNNEL EXTRACTION: EXTRACTABLE FUELS

WW

1/23/2015 EPA 8015B TPH EXTRACTABLE BY GC/FID WW

1/23/2015 EPA 8015B Total TPH WW

1 of 2Page


Date Received:


WORK ORDER Summary 19-Jan-15

WorkOrder: N014406

Comments: Report to D. Jablonski/CH2M HILL, cc:KMEP. Direct Bill KMEP/SFPP-Steve Defibaugh-ref.AFE# 81195. "J" Flags required / Use lowest possible detection l

Client ID: CH2HI03


Hld MS Sub

1/16/2015

Test Name

ASSET Laboratories

Storage

N014406-001L EFF-01-15 1/15/2015 12:35:00 PM 1/23/2015 Wastewater EPA 8260B VOLATILE ORGANIC COMPOUNDS BY GC/MS

WV

N014406-002A FOLDER 1/20/2015 Folder Folder LAB

2 of 2Page

Job Number Order Date Client 75676 01/16/2015 ASSET

Number of Pages 4 Date Received 01/16/2015 Date Reported 01/20/2015

ASSET Laboratories3151-3153 W Post RoadLas Vegas, NV 89118-

Project ID:Project Name:

N014406N14406A

Ordered By

Attention: Marlon CartinTelephone: (702)307-2659

Enclosed please find results of analyses of 1 waste watersample which was analyzed as specified on the attached chainof custody. If there are any questions, please do not hesitateto call.

2834 & 2908 North Naomi Street Burbank, CA 91504 • DOHS NO: 1541, LACSD NO: 10181Tel: (888) 288-AETL • (818) 845-8200 • Fax: (818) 845-8840 • www.aetlab.com

American Environmental Testing Laboratory Inc.

Cyrus Razmara, Ph.D.Laboratory Director

Approved By:Checked By:


Project ID: N014406

Date Received 01/16/2015

Date Reported 01/20/2015

ASSET Laboratories

3151-3153 W Post Road

Las Vegas, NV 89118-

Ordered By


Page: 1 A

AETL received 1 samples with the following specification on 01/16/2015.

CERTIFICATE OF ANALYSISCASE NARRATIVE



Lab ID Sample ID Sample Date Matrix Quantity Of Containers75676.01 EFF-01-15 01/15/2015 Aqueous 2

Method ^ Submethod Priority TAT UnitsReq Date

420.1 2 Normal mg/L01/23/2015SM-4500-NH3-C 2 Normal mg/L01/23/2015SM-5540C 2 Normal mg/L01/23/2015

The samples were analyzed as specified on the enclosed chain of custody.No analytical non-conformances were encountered.

Cyrus Razmara, Ph.D.

Laboratory Director


QC Batch No: 011915-1

75676 01/16/2015 ASSET

AETL Job Number Submitted Client



N014406N14406A

2Page:

Ordered By

Attn: Marlon Cartin

ANALYTICAL RESULTS

Telephone: (702)307-2659

Method: 420.1, Phenolics, Total Recoverable, Spectrophotometric, Manual



Date Sampled 01/15/2015

Dilution Factor 1 1Units mg/L mg/LMatrix Aqueous AqueousDate Analyzed 01/19/2015 01/19/2015

Date Prepared 01/19/2015 01/19/2015

EFF-01-15Client Sample I.D.

Analytes MDL Results ResultsPQL

Preparation Method 420.1 420.1

Our Lab I.D. 75676.01Method Blank

0.30Phenolic compounds as phenol 0.15 ND ND

AnalytesSample MSMS MS MS DUP MS DUP MS DUP RPD MS/MSD MS RPD

Result RecovConcen % REC Concen Recov % REC % % Limit % Limit

QUALITY CONTROL REPORT

QC Batch No: 011915-1; Dup or Spiked Sample: 75676.01; LCS: Clean Water; QC Prepared: 01/19/2015; QC Analyzed: 01/19/2015; Units: mg/L

Phenol 80-120 <15 0.00 0.200 0.180 90.0 0.200 0.187 93.6 3.9

AnalytesLCS LCSLCS LCS DUP LCS DUP LCS DUP LCS RPD LCS/LCSD LCS RPD

Concen % RECRecov Concen Recov % REC % REC % Limit % Limit


Phenol <20 0.200 0.174 86.8 0.200 0.178 89.0 2.5 80-120


75676 01/16/2015 ASSET




N014406N14406A

3Page:

Ordered By

Attn: Marlon Cartin

ANALYTICAL RESULTS

Telephone: (702)307-2659

Method: SM-4500-NH3-C, Ammonia by Nesslerization Method





Date Prepared 01/19/2015 01/19/2015



Preparation Method SM4500NH3C SM4500NH3C


0.10Ammonia as Nitrogen 0.05 ND ND





Ammonia as Nitrogen 80-120 <15 0.00 0.500 0.491 98.2 0.500 0.488 97.6 <1




Ammonia as Nitrogen <15 0.500 0.488 97.6 0.500 0.483 96.6 1.0 80-120


75676 01/16/2015 ASSET




N014406N14406A

4Page:

Ordered By

Attn: Marlon Cartin

ANALYTICAL RESULTS

Telephone: (702)307-2659

Method: SM-5540C, Methylene Blue Active Substances (MBAS)





Date Prepared 01/16/2015 01/16/2015



Preparation Method SM5540C SM5540C


0.05Surfactants (MBAS) 0.05 ND ND





Surfactants (MBAS) 80-120 <15 0.00 0.500 0.510 102 0.500 0.495 99.0 3.0




Surfactants (MBAS) <15 0.500 0.485 97.0 0.500 0.492 98.4 1.4 80-120


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436

February 18, 2015

CH2MHill

Dan Jablonski




TEL:

1000 Wilshire Blvd.


CA-ELAP No.: 2676




Sincerely,

Glen Gesmundo

QA Manager

Enclosed are the results for sample(s) received on February 12, 2015 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications.


01 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436

18-Feb-15Date:ASSET Laboratories


CLIENT: CH2MHill








Subcontracted Test:

Phenol was subcontracted to AETL - Burbank, CA .

Analytical Comments for EPA 200.8:

Matrix Spike (MS) and Matrix Spike Duplicate (MSD) are outside recovery criteria for Copper on QC samples N014636-001B-MS and N014636-001B-MSD possibly due to matrix interference. The associated Laboratory Control Sample (LCS) recovery was acceptable.

Page 2 of 17

02 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill



Contract No:

Date Reported










Page 1 of 1

03 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436




Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014651

Lab ID: N014651-001

ASSET Laboratories Print Date: 18-Feb-15


ANALYTICAL RESULTS


Analyst: LRRunID: WETCHEM_150212B 49686QC Batch: PrepDate: 2/12/2015


10 mg/L 1ND 10 2/12/2015 12:30 PM


Analyst: QBMRunID: WETCHEM_150212C 49688QC Batch: PrepDate: 2/12/2015



Analyst: LRRunID: WETCHEM_150213A 49696QC Batch: PrepDate: 2/13/2015

Oil & Grease 4.3 mg/L 1ND 0.86 2/13/2015 01:00 PM



1,1-Dichloroethane 0.50 ug/L 1ND 0.054 2/12/2015 11:51 AM

1,2-Dichloroethane 0.50 ug/L 1ND 0.044 2/12/2015 11:51 AM

Benzene 1.0 ug/L 1ND 0.048 2/12/2015 11:51 AM

Ethylbenzene 1.0 ug/L 1ND 0.036 2/12/2015 11:51 AM

m,p-Xylene 1.0 ug/L 1ND 0.14 2/12/2015 11:51 AM

MTBE 1.0 ug/L 1ND 0.098 2/12/2015 11:51 AM

o-Xylene 1.0 ug/L 1ND 0.042 2/12/2015 11:51 AM

Tert-Butanol 5.0 ug/L 1ND 0.40 2/12/2015 11:51 AM

Toluene 2.0 ug/L 1ND 0.025 2/12/2015 11:51 AM

Xylenes, Total 2.0 ug/L 1ND 1.5 2/12/2015 11:51 AM

Surr: 1,2-Dichloroethane-d4 72-119 %REC 1108 0 2/12/2015 11:51 AM

Surr: 4-Bromofluorobenzene 76-119 %REC 199.6 0 2/12/2015 11:51 AM

Surr: Dibromofluoromethane 85-115 %REC 1109 0 2/12/2015 11:51 AM

Surr: Toluene-d8 81-120 %REC 1102 0 2/12/2015 11:51 AM


Analyst: MDM

EPA 3510C









04 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436




Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014651

Lab ID: N014651-001



ANALYTICAL RESULTS


Analyst: MDM

EPA 3510C





TPH-Gasoline (C4-C12) 50 ug/L 1ND 16 2/12/2015 11:27 AM

Surr: Chlorobenzene - d5 74-138 %REC 1113 0 2/12/2015 11:27 AM


Analyst: CEIRunID: AA1_150213B 49691QC Batch: PrepDate: 2/13/2015

Mercury 0.050 µg/L 1ND 0.018 2/13/2015 03:48 PM


Analyst: CEIRunID: ICP7_150212A 49683QC Batch: PrepDate: 2/12/2015

Selenium 0.50 µg/L 1ND 0.069 2/12/2015 04:05 PM


Analyst: CEIRunID: ICP7_150212A R97994QC Batch: PrepDate:

Copper 0.50 µg/L 1ND 0.040 2/12/2015 04:05 PM

Lead 0.50 µg/L 1ND 0.011 2/12/2015 04:05 PM

Thallium J0.50 µg/L 10.086 0.0080 2/12/2015 04:05 PM

Zinc J10 µg/L 11.2 0.23 2/12/2015 04:05 PM

TOTAL TPHEPA 8015B

Analyst: MDM

EPA 3510C


Total TPH 50 ug/L 1ND 22 2/13/2015





05 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill



Sample ID: MB-49686




Units: mg/L

PQL

Client ID: PBW

RunNo: 97997

SeqNo: 1932985







Units: mg/L

PQL

Client ID: LCSW

RunNo: 97997

SeqNo: 1932986



Sample ID: N014651-001E DUP




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 97997

SeqNo: 1932988



Qualifiers:




06 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49688




Units: ml/L

PQL

Client ID: PBW

RunNo: 98066

SeqNo: 1936570



Qualifiers:




07 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49696




Units: mg/L

PQL

Client ID: PBW

RunNo: 97998

SeqNo: 1932996


Oil & Grease 4.0ND





Units: mg/L

PQL

Client ID: LCSW

RunNo: 97998

SeqNo: 1932997


Oil & Grease 40.00 78.5 78 1144.0 031.400

Sample ID: N014651-001A MS




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 97998

SeqNo: 1932999


Oil & Grease 41.67 97.5 78 1144.2 040.625

Sample ID: N014651-001A MSD




Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 97998

SeqNo: 1933000


Oil & Grease 41.67 96.2 78 114 184.2 0 40.62 1.2940.104

Qualifiers:




08 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49683




Units: µg/L

PQL

Client ID: PBW

RunNo: 97994

SeqNo: 1932739


Selenium 0.50ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 97994

SeqNo: 1932740


Selenium 10.00 93.2 85 1150.50 09.323

Sample ID: N014636-001B-MS




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97994

SeqNo: 1932744


Selenium 10.00 85.0 75 1250.50 2.83411.332

Sample ID: N014636-001B-MSD




Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97994

SeqNo: 1932745


Selenium 10.00 84.8 75 125 200.50 2.834 11.33 0.18911.310

Qualifiers:




09 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49683

Batch ID: R97994 TestNo: EPA 200.8 Analysis Date: 2/12/2015

Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 97994

SeqNo: 1932852


Copper 0.50ND

Lead 0.50ND

Thallium 0.50ND

Zinc 10ND



Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 97994

SeqNo: 1932853


Copper 10.00 95.7 85 1150.50 09.570

Lead 10.00 109 85 1150.50 010.944

Thallium 10.00 110 85 1150.50 010.984

Zinc 100.0 95.3 85 11510 095.276

Sample ID: N014636-001B-MS


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97994

SeqNo: 1932857


Copper 10.00 34.5 75 125 S0.50 03.448

Lead 10.00 108 75 1250.50 010.767

Thallium 10.00 112 75 1250.50 0.0646711.253

Zinc 100.0 76.8 75 12510 076.772



Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97994

SeqNo: 1932858


Copper 10.00 34.5 75 125 20 S0.50 0 3.448 0.05813.450

Lead 10.00 108 75 125 200.50 0 10.77 0.41710.812

Qualifiers:




10 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 97994

SeqNo: 1932858


Thallium 10.00 112 75 125 200.50 0.06467 11.25 0.13411.269

Zinc 100.0 77.9 75 125 2010 0 76.77 1.4477.886

Qualifiers:




11 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49691




Units: µg/L

PQL

Client ID: PBW

RunNo: 98017

SeqNo: 1933557


Mercury 0.050ND





Units: µg/L

PQL

Client ID: LCSW

RunNo: 98017

SeqNo: 1933559


Mercury 2.500 100 85 1150.050 02.511





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 98017

SeqNo: 1933560


Mercury 2.500 115 75 1250.050 02.881





Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 98017

SeqNo: 1933561


Mercury 2.500 116 75 125 200.050 0 2.881 0.7502.903

Qualifiers:




12 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49689




Units: ug/L

PQL

Client ID: PBW

RunNo: 98012

SeqNo: 1933429


EPA 3510C



Surr: Octacosane 80.00 101 26 15280.804

Surr: p-Terphenyl 80.00 98.5 57 13278.773

Qualifiers:




13 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49689


Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 98012

SeqNo: 1936579


EPA 3510C

Total TPH 50ND

Qualifiers:




14 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 97983

SeqNo: 1931602


TPH-Gasoline (C4-C12) 1000 96.0 67 13650 0960.000




Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97983

SeqNo: 1931603




Sample ID: N014651-001BMS


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97983

SeqNo: 1931605


TPH-Gasoline (C4-C12) 1000 90.9 67 13650 0909.000


Sample ID: N014651-001BMSD


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97983

SeqNo: 1931606


TPH-Gasoline (C4-C12) 1000 90.5 67 136 3050 0 909.0 0.441905.000


Qualifiers:




15 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 97979

SeqNo: 1931315


1,1-Dichloroethane 20.00 102 69 1330.50 020.380

1,2-Dichloroethane 20.00 102 69 1320.50 020.410

Benzene 20.00 101 81 1221.0 020.270

Ethylbenzene 20.00 101 73 1271.0 020.220

m,p-Xylene 40.00 104 76 1281.0 041.780

MTBE 20.00 102 65 1231.0 020.310

o-Xylene 20.00 104 80 1211.0 020.900

Tert-Butanol 100.0 119 70 1305.0 0119.450

Toluene 20.00 104 77 1222.0 020.740

Xylenes, Total 60.00 104 75 1252.0 062.680

Surr: 1,2-Dichloroethane-d4 25.00 105 72 11926.230


Surr: Dibromofluoromethane 25.00 103 85 11525.660

Surr: Toluene-d8 25.00 103 81 12025.740



Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97979

SeqNo: 1931317




Benzene 1.0ND

Ethylbenzene 1.0ND

m,p-Xylene 1.0ND

MTBE 1.0ND

o-Xylene 1.0ND

Tert-Butanol 5.0ND

Toluene 2.0ND



Qualifiers:




16 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 97979

SeqNo: 1931317


Surr: 4-Bromofluorobenzene 25.00 99.0 76 11924.760


Surr: Toluene-d8 25.00 102 81 12025.500

Sample ID: N014651-001CMS


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97979

SeqNo: 1931319


1,1-Dichloroethane 20.00 105 69 1330.50 020.980

1,2-Dichloroethane 20.00 101 69 1320.50 020.240

Benzene 20.00 101 81 1221.0 020.240

Ethylbenzene 20.00 97.9 73 1271.0 019.580

m,p-Xylene 40.00 101 76 1281.0 040.300

MTBE 20.00 97.5 65 1231.0 019.500

o-Xylene 20.00 100 80 1211.0 020.080

Tert-Butanol 100.0 109 70 1305.0 0109.160

Toluene 20.00 100 77 1222.0 020.060

Xylenes, Total 60.00 101 75 1252.0 060.380




Surr: Toluene-d8 25.00 103 81 12025.800

Sample ID: N014651-001CMSD


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97979

SeqNo: 1931320


1,1-Dichloroethane 20.00 108 69 133 200.50 0 20.98 3.0521.630

1,2-Dichloroethane 20.00 102 69 132 200.50 0 20.24 0.83620.410

Benzene 20.00 104 81 122 201.0 0 20.24 2.3020.710

Qualifiers:




17 of 18


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 97979

SeqNo: 1931320


Ethylbenzene 20.00 101 73 127 201.0 0 19.58 2.6720.110

m,p-Xylene 40.00 103 76 128 201.0 0 40.30 1.9941.110

MTBE 20.00 103 65 123 201.0 0 19.50 5.1920.540

o-Xylene 20.00 104 80 121 201.0 0 20.08 3.7120.840

Tert-Butanol 100.0 117 70 130 205.0 0 109.2 7.13117.230

Toluene 20.00 103 77 122 202.0 0 20.06 2.4120.550

Xylenes, Total 60.00 103 75 125 202.0 0 60.38 2.5761.950

Surr: 1,2-Dichloroethane-d4 25.00 106 72 119 026.460


Surr: Dibromofluoromethane 25.00 105 85 115 026.310

Surr: Toluene-d8 25.00 102 81 120 025.610

Qualifiers:




18 of 18





Rep sample Temp (Deg C): -0.8 IR Gun ID: 2

Temp Blank: Yes No




Workorder: N014651










14. Water - pH acceptable upon receipt? Yes No NA

Example: pH > 12 for (CN,S); pH<2 for Metals







16. Were there Non-Conformance issues at login? Yes No NA

W as Client notified? Yes No NA

Comments:

Checklist Completed By: HG Reviewed By:


Sample ID Matr ix Date Collected Bottle TypeRequested Tests

EPA 420.1

Subcontractor:


TEL: (818) 845-8200FAX: (818) 845-8840Acct #: 16-Feb-15

QC Level: RTNE




N014651-001F W astewater 2/10/2015 2:30:00 PM 32OZA 1 / EFF-02-10

Relinquished by:

Relinquished by:

Received by:

Received by:

Date/TimeDate/Time


Please use PO#:N14651A For questions, call Marlon at (702)-307-2659. Please e-mail results to [email protected] by:Normal TAT

Please analyze for Phenolics.



1

[email protected]

From: Marlon B. Cartin [[email protected]]Sent: Friday, February 13, 2015 5:39 PMTo: [email protected]: 'Sample Control'; ''Glen Gesmundo''Subject: Cr+6

Hi Vidal, We already got the 7199 sample from Norwalk site and we will receive it here at the lab tomorrow morning. This will be the replacement sample for the one that expires because we failed to pick-up the samples on Tuesday (2/10). We will run this ASAP and report at the same time with the samples from Tuesday. Thanks, Marlon Cartin Project Manager California: 11060 Artesia Blvd., Ste. C, Cerritos, CA 90703 I P: 562.219.7435 I F: 562.219.7436

Nevada: 3151 W. Post Road, Las Vegas, NV 89118 I P: 702.307.2659 Ext. 410 I F: 702.307.2691 I M: 702.882.3289 www.assetlaboratories.com

ASSET LABORATORIES - Serving Clients with Passion and Professionalism This message is intended for the use of the individual or entity to which it is addressed. This may contain information that is privileged, confidential, and exempt from disclosure under applicable law. If the reader of this message is not the intended recipient, or the employee or agent responsible for delivering the message to the intended recipient, you are hereby notified that any dissemination, distribution or copying of this communication is strictly prohibited. If you have received this communication in error, please notify us immediately by telephone and delete the original message. Thank you.




http://www.assetlaboratories.com


Date Received:


WORK ORDER Summary 13-Feb-15

WorkOrder: N014651

Comments: Report to D. Jablonski/CH2M HILL, cc:KMEP

Client ID: CH2HI03


Hld MS Sub

2/12/2015

Test Name

ASSET Laboratories

Storage

N014651-001A EFF-02-10 2/10/2015 2:30:00 PM 2/19/2015 Wastewater Oil and Grease Sample Prep WW


N014651-001B 2/19/2015 EPA 8015B GASOLINE RANGE ORGANICS BY GC/FID

WW

N014651-001C 2/16/2015 EPA 8260B VOLATILE ORGANIC COMPOUNDS BY GC/MS

WW

N014651-001D 2/19/2015 SM2540F SETTLEABLE MATTER WW

N014651-001E 2/19/2015 SM2540D TOTAL NON-FILTERABLE RESIDUE WW


N014651-001F 2/19/2015 EPA 420.1 PHENOLICS SUB

N014651-001G 2/16/2015 AQPREP TOTAL METALS: ICP, FLAA WW

2/16/2015 EPA 200.8 TOTAL METALS BY COLLISION/REACTION CELL ICPMS

WW


2/16/2015 EPA 245.1 MERCURY BY COLD VAPOR TECHNIQUE

WW


N014651-001H 2/19/2015 EPA 3510C SEPARATORY FUNNEL EXTRACTION: EXTRACTABLE FUELS

WW


N014651-001I 2/19/2015 EPA 7199 Hexavalent Chromium by IC WW


1 of 1Page





N014651PO# 14651A

Ordered By



Site: SFPP-Norwalk Site






Project ID: N014651



ASSET Laboratories



Ordered By


Page: 1 A





Lab ID Sample ID Sample Date Matrix Quantity Of Containers75960.01 N014651-001F 02/10/2015 Aqueous 1


420.1 2 Normal mg/L02/19/2015



Laboratory Director



75960 02/12/2015 ASSET


SFPP-Norwalk SiteASSET Laboratories3151-3153 W Post RoadLas Vegas, NV 89118-


N014651PO# 14651A

2Page:

Ordered By

Attn: Marlon Cartin

SiteANALYTICAL RESULTS

Telephone: (702)307-2659






Date Prepared 02/12/2015 02/12/2015

N014651-001F

Client Sample I.D.









Phenol 80-120 <15 0.00 0.500 0.405 81.0 0.500 0.418 83.6 3.2




Phenol <20 0.500 0.452 90.4 0.500 0.443 88.6 2.0 80-120


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436

February 18, 2015

CH2MHill

Dan Jablonski


RE: SFPP-Norwalk Site


TEL:

1000 Wilshire Blvd.


CA-ELAP No.: 2676




Sincerely,

Glen Gesmundo

QA Manager

Enclosed are the results for sample(s) received on February 14, 2015 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications.


01 of 05


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


Project: SFPP-Norwalk Site

CLIENT: CH2MHill



Sample was received intact with proper chain of custody documentation.



Sample was analyzed within method holding time.


Page 2 of 4

02 of 05


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill



Contract No:

Date Reported

N014679-001A EFF-02-13 2/13/2015 11:25:00 AM 2/14/2015 2/18/2015Wastewater

Page 1 of 1

03 of 05


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



Collection Date: 2/13/2015 11:25:00 AM

Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014679

Lab ID: N014679-001



ANALYTICAL RESULTS








04 of 05


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill


TestCode: 7199_WPGE



Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 98024

SeqNo: 1933802





Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 98024

SeqNo: 1933803


Hexavalent Chromium 5.000 101 90 1100.20 05.055



Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 98024

SeqNo: 1933806


Hexavalent Chromium 25.00 102 85 1151.0 37.5463.109



Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 98024

SeqNo: 1933807


Hexavalent Chromium 25.00 103 85 115 201.0 37.54 63.11 0.10163.172

Qualifiers:




05 of 05






Temp Blank: Yes No




Workorder: N014679




















Comments:

Checklist Completed By: MBC Reviewed By:


Date Received:

Date Due Matr ix Test No

WORK ORDER Summary 16-Feb-15

WorkOrder: N014679


Client ID: CH2HI03Project: SFPP-Norwalk Site QC Level: RTNE

Hld MS Sub

2/14/2015

Test Name

ASSET Laboratories

Storage

N014679-001A EFF-02-13 2/13/2015 11:25:00 AM 2/23/2015 Wastewater EPA 7199 Hexavalent Chromium by IC WW


1 of 1Page


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436

March 11, 2015

CH2MHill

Dan Jablonski




TEL:

1000 Wilshire Blvd.


CA-ELAP No.: 2676




Sincerely,

Glen Gesmundo

QA Manager

Enclosed are the results for sample(s) received on March 04, 2015 by ASSET Laboratories . The sample(s) are tested for the parameters as indicated in the enclosed chain of custody in accordance with the applicable laboratory certifications.


01 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436

11-Mar-15Date:ASSET Laboratories


CLIENT: CH2MHill








Subcontracted Test:

Phenol was subcontracted to AETL - Burbank, CA .

Analytical Comments for EPA 8015B DRO:

RPD for Matrix Spike (MS)/Matrix Spike Duplicate (MSD) is outside criteria on QC samples N014853-001H-MS and N014853-001H-MSD possibly due to matrix interference; however, the analytical batch was validated by the Laboratory Control Sample (LCS).

Page 2 of 18

02 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill



Contract No:

Date Reported










Page 1 of 1

03 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436




Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014853

Lab ID: N014853-001

ASSET Laboratories Print Date: 11-Mar-15


ANALYTICAL RESULTS


Analyst: LRRunID: WETCHEM_150304D 49830QC Batch: PrepDate: 3/4/2015


10 mg/L 1ND 10 3/4/2015 08:31 AM


Analyst: QBMRunID: WETCHEM_150304K 49893QC Batch: PrepDate: 3/4/2015



Analyst: LRRunID: WETCHEM_150309A 49869QC Batch: PrepDate: 3/9/2015

Oil & Grease 4.4 mg/L 1ND 0.88 3/9/2015 09:30 AM





Benzene 1.0 ug/L 1ND 0.048 3/5/2015 12:25 PM

Ethylbenzene 1.0 ug/L 1ND 0.036 3/5/2015 12:25 PM

m,p-Xylene 1.0 ug/L 1ND 0.14 3/5/2015 12:25 PM

MTBE 1.0 ug/L 1ND 0.098 3/5/2015 12:25 PM

o-Xylene 1.0 ug/L 1ND 0.042 3/5/2015 12:25 PM

Tert-Butanol 5.0 ug/L 1ND 0.40 3/5/2015 12:25 PM

Toluene 2.0 ug/L 1ND 0.025 3/5/2015 12:25 PM

Xylenes, Total 2.0 ug/L 1ND 1.5 3/5/2015 12:25 PM

Surr: 1,2-Dichloroethane-d4 72-119 %REC 191.0 0 3/5/2015 12:25 PM

Surr: 4-Bromofluorobenzene 76-119 %REC 198.7 0 3/5/2015 12:25 PM

Surr: Dibromofluoromethane 85-115 %REC 194.4 0 3/5/2015 12:25 PM

Surr: Toluene-d8 81-120 %REC 199.0 0 3/5/2015 12:25 PM


Analyst: MDM

EPA 3510C









04 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436




Matrix: WASTEWATER

CLIENT: CH2MHill

Lab Order: N014853

Lab ID: N014853-001

ASSET Laboratories Print Date: 11-Mar-15


ANALYTICAL RESULTS


Analyst: MDM

EPA 3510C





TPH-Gasoline (C4-C12) 50 ug/L 1ND 16 3/4/2015 12:10 PM

Surr: Chlorobenzene - d5 74-138 %REC 1115 0 3/4/2015 12:10 PM





Analyst: CEIRunID: AA1_150305B 49848QC Batch: PrepDate: 3/5/2015

Mercury 0.050 µg/L 1ND 0.018 3/5/2015 05:49 PM



Selenium 0.50 µg/L 1ND 0.069 3/4/2015 01:41 PM



Copper 0.50 µg/L 1ND 0.040 3/4/2015 01:41 PM

Lead 0.50 µg/L 1ND 0.011 3/4/2015 01:41 PM

Thallium J0.50 µg/L 10.067 0.0080 3/4/2015 01:41 PM

Zinc J10 µg/L 11.1 0.23 3/4/2015 01:41 PM

TOTAL TPHEPA 8015B

Analyst: MDM

EPA 3510C


Total TPH 51 ug/L 1ND 22 3/9/2015 08:50 PM





05 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436



CLIENT: CH2MHill



Sample ID: MB-49830


Prep Date: 3/4/2015


Units: mg/L

PQL

Client ID: PBW

RunNo: 99288

SeqNo: 1946086





Prep Date: 3/4/2015


Units: mg/L

PQL

Client ID: LCSW

RunNo: 99288

SeqNo: 1946087



Sample ID: N014853-001E DUP


Prep Date: 3/4/2015


Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 99288

SeqNo: 1946090



Qualifiers:




06 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49893


Prep Date: 3/4/2015


Units: ml/L

PQL

Client ID: PBW

RunNo: 99383

SeqNo: 1950107



Qualifiers:




07 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49869


Prep Date: 3/9/2015


Units: mg/L

PQL

Client ID: PBW

RunNo: 99345

SeqNo: 1948006


Oil & Grease 4.0ND



Prep Date: 3/9/2015


Units: mg/L

PQL

Client ID: LCSW

RunNo: 99345

SeqNo: 1948007


Oil & Grease 40.00 86.5 78 1144.0 034.600

Sample ID: N014853-001A MS


Prep Date: 3/9/2015


Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 99345

SeqNo: 1948009


Oil & Grease 40.00 110 78 1144.4 044.111

Sample ID: N014853-001A MSD


Prep Date: 3/9/2015


Units: mg/L

PQL

Client ID: ZZZZZZ

RunNo: 99345

SeqNo: 1948010


Oil & Grease 40.00 93.9 78 114 184.4 0 44.11 16.137.555

Qualifiers:




08 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49832


Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: PBW

RunNo: 99293

SeqNo: 1946244


Selenium 0.50ND



Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: LCSW

RunNo: 99293

SeqNo: 1946245


Selenium 10.00 88.9 85 1150.50 08.886



Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99293

SeqNo: 1946249


Selenium 10.00 86.9 75 1250.50 08.689



Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99293

SeqNo: 1946250


Selenium 10.00 84.3 75 125 200.50 0 8.689 3.088.426

Qualifiers:




09 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49832


Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: PBW

RunNo: 99293

SeqNo: 1946213


Copper J0.500.050

Lead 0.50ND

Thallium J0.500.016

Zinc 10ND



Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: LCSW

RunNo: 99293

SeqNo: 1946214


Copper 10.00 91.8 85 1150.50 09.176

Lead 10.00 96.4 85 1150.50 09.638

Thallium 10.00 91.5 85 1150.50 09.145

Zinc 100.0 90.0 85 11510 089.987



Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99293

SeqNo: 1946218


Copper 10.00 78.0 75 1250.50 07.802

Lead 10.00 104 75 1250.50 010.446

Thallium 10.00 106 75 1250.50 0.0666010.619

Zinc 100.0 81.5 75 12510 1.08682.561



Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99293

SeqNo: 1946219


Copper 10.00 78.2 75 125 200.50 0 7.802 0.1857.816

Lead 10.00 104 75 125 200.50 0 10.45 0.58010.386

Qualifiers:




10 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date: 3/4/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99293

SeqNo: 1946219


Thallium 10.00 105 75 125 200.50 0.06660 10.62 0.25710.592

Zinc 100.0 81.1 75 125 2010 1.086 82.56 0.49982.149

Qualifiers:




11 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49848


Prep Date: 3/5/2015


Units: µg/L

PQL

Client ID: PBW

RunNo: 99316

SeqNo: 1946881


Mercury 0.050ND



Prep Date: 3/5/2015


Units: µg/L

PQL

Client ID: LCSW

RunNo: 99316

SeqNo: 1946882


Mercury 2.500 104 85 1150.050 02.596



Prep Date: 3/5/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99316

SeqNo: 1946884


Mercury 2.500 101 75 1250.050 02.524



Prep Date: 3/5/2015


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99316

SeqNo: 1946885


Mercury 2.500 101 75 125 200.050 0 2.524 0.1222.527

Qualifiers:




12 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill


TestCode: 7199_WPGE



Prep Date:


Units: µg/L

PQL

Client ID: PBW

RunNo: 99304

SeqNo: 1946695





Prep Date:


Units: µg/L

PQL

Client ID: LCSW

RunNo: 99304

SeqNo: 1946696


Hexavalent Chromium 5.000 97.2 90 1100.20 04.859

Sample ID: N014853-001I-DUP


Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99304

SeqNo: 1946698





Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99304

SeqNo: 1946706


Hexavalent Chromium 200.0 104 85 11540 783.7990.720



Prep Date:


Units: µg/L

PQL

Client ID: ZZZZZZ

RunNo: 99304

SeqNo: 1946707


Hexavalent Chromium 200.0 97.9 85 115 2040 783.7 990.7 1.15979.380

Qualifiers:




13 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49866


Prep Date: 3/9/2015


Units: ug/L

PQL

Client ID: PBW

RunNo: 99352

SeqNo: 1948456


EPA 3510C



Surr: Octacosane 80.00 94.8 26 15275.802

Surr: p-Terphenyl 80.00 86.2 57 13268.926

Qualifiers:




14 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill



Sample ID: MB-49866


Prep Date: 3/9/2015


Units: ug/L

PQL

Client ID: PBW

RunNo: 99352

SeqNo: 1948459


EPA 3510C

Total TPH 500

Qualifiers:




15 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 99297

SeqNo: 1946313


TPH-Gasoline (C4-C12) 1000 101 67 13650 01006.000




Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 99297

SeqNo: 1946314




Sample ID: N014853-001BMS


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 99297

SeqNo: 1946318


TPH-Gasoline (C4-C12) 1000 104 67 13650 01038.000


Sample ID: N014853-001BMSD


Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 99297

SeqNo: 1946319


TPH-Gasoline (C4-C12) 1000 105 67 136 3050 0 1038 0.7681046.000


Qualifiers:




16 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: LCSW

RunNo: 99311

SeqNo: 1946802


1,1-Dichloroethane 20.00 89.2 69 1330.50 017.840

1,2-Dichloroethane 20.00 91.6 69 1320.50 018.310

Benzene 20.00 97.8 81 1221.0 019.560

Ethylbenzene 20.00 98.6 73 1271.0 019.720

m,p-Xylene 40.00 104 76 1281.0 041.500

MTBE 20.00 90.9 65 1231.0 018.180

o-Xylene 20.00 106 80 1211.0 021.290

Tert-Butanol 100.0 79.0 70 1305.0 079.020

Toluene 20.00 101 77 1222.0 020.160

Xylenes, Total 60.00 105 75 1252.0 062.790




Surr: Toluene-d8 25.00 99.7 81 12024.930



Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 99311

SeqNo: 1946803


1,1-Dichloroethane 20.00 88.7 69 1330.50 017.740

1,2-Dichloroethane 20.00 92.9 69 1320.50 018.580

Benzene 20.00 97.2 81 1221.0 019.440

Ethylbenzene 20.00 97.4 73 1271.0 019.480

m,p-Xylene 40.00 102 76 1281.0 040.790

MTBE 20.00 86.4 65 1231.0 017.280

o-Xylene 20.00 104 80 1211.0 020.740

Tert-Butanol 100.0 71.0 70 1305.0 070.950

Toluene 20.00 101 77 1222.0 020.220

Xylenes, Total 60.00 103 75 1252.0 061.530


Qualifiers:




17 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 99311

SeqNo: 1946803




Surr: Toluene-d8 25.00 101 81 12025.170



Prep Date:


Units: ug/L

PQL

Client ID: ZZZZZZ

RunNo: 99311

SeqNo: 1946804


1,1-Dichloroethane 20.00 88.6 69 133 200.50 0 17.74 0.16917.710

1,2-Dichloroethane 20.00 94.4 69 132 200.50 0 18.58 1.6018.880

Benzene 20.00 98.8 81 122 201.0 0 19.44 1.6819.770

Ethylbenzene 20.00 101 73 127 201.0 0 19.48 3.2820.130

m,p-Xylene 40.00 105 76 128 201.0 0 40.79 2.5441.840

MTBE 20.00 91.7 65 123 201.0 0 17.28 5.9518.340

o-Xylene 20.00 109 80 121 201.0 0 20.74 4.6221.720

Tert-Butanol 100.0 84.3 70 130 205.0 0 70.95 17.284.280

Toluene 20.00 102 77 122 202.0 0 20.22 0.98420.420

Xylenes, Total 60.00 106 75 125 202.0 0 61.53 3.2563.560

Surr: 1,2-Dichloroethane-d4 25.00 87.9 72 119 021.970


Surr: Dibromofluoromethane 25.00 93.6 85 115 023.400

Surr: Toluene-d8 25.00 102 81 120 025.570



Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 99311

SeqNo: 1946805




Benzene 1.0ND

Qualifiers:




18 of 19


P: 702.307.2659 F: 702.307.2691



P: 562.219.7435 F: 562.219.7436


CLIENT: CH2MHill





Prep Date:


Units: ug/L

PQL

Client ID: PBW

RunNo: 99311

SeqNo: 1946805


Ethylbenzene 1.0ND

m,p-Xylene 1.0ND

MTBE 1.0ND

o-Xylene 1.0ND

Tert-Butanol 5.0ND

Toluene 2.0ND





Surr: Toluene-d8 25.00 101 81 12025.160

Qualifiers:




19 of 19






Temp Blank: Yes No




Workorder: N014853




















Comments:

Checklist Completed By: HG Reviewed By:


Sample ID Matr ix Date Collected Bottle TypeRequested Tests

EPA 420.1

Subcontractor:


TEL: (818) 845-8200FAX: (818) 845-8840Acct #: 06-Mar-15

QC Level: RTNE




N014853-001F W astewater 3/3/2015 2:15:00 PM 32OZA 1 / EFF-03-03

Relinquished by:

Relinquished by:

Received by:

Received by:

Date/TimeDate/Time


Please use PO#:N14853A For questions, call Marlon at (702)-307-2659. Please e-mail results to [email protected] by:Normal TAT

Please analyze for Phenolics.




Date Received:


WORK ORDER Summary 04-Mar-15

WorkOrder: N014853


Client ID: CH2HI03


Hld MS Sub

3/4/2015

Test Name

ASSET Laboratories

Storage

N014853-001A EFF-03-03 3/3/2015 2:15:00 PM 3/11/2015 Wastewater Oil and Grease Sample Prep WW


N014853-001B 3/11/2015 EPA 8015B GASOLINE RANGE ORGANICS BY

GC/FID

WW

N014853-001C 3/5/2015 EPA 8260B VOLATILE ORGANIC COMPOUNDS BY

GC/MS

VW

N014853-001D 3/11/2015 SM2540F SETTLEABLE MATTER WW

3/11/2015 Setteable Matter WW

N014853-001E 3/11/2015 SM2540D TOTAL NON-FILTERABLE RESIDUE WW


N014853-001F 3/11/2015 EPA 420.1 PHENOLICS SUB

N014853-001G 3/5/2015 AQPREP TOTAL METALS: ICP, FLAA WW

3/5/2015 EPA 200.8 TOTAL METALS BY

COLLISION/REACTION CELL ICPMS

WW


3/5/2015 EPA 245.1 MERCURY BY COLD VAPOR

TECHNIQUE

WW


N014853-001H 3/11/2015 EPA 3510C SEPARATORY FUNNEL EXTRACTION:

EXTRACTABLE FUELS

WW


3/11/2015 EPA 8015B Total TPH WW

N014853-001I 3/11/2015 EPA 7199 Hexavalent Chromium by IC WW


1 of 1Page




Project Name: SFPP-Norwalk Site

Ordered By








Project ID: None



ASSET Laboratories



Ordered By


Page: 1 A





Lab ID Sample ID Sample Date Matrix Quantity Of Containers76173.01 EFF-03-03 Effluent 03/03/2015 Aqueous 1


420.1 2 Normal mg/L03/11/2015



Laboratory Director



76173 03/04/2015 ASSET



Project Name: SFPP-Norwalk Site

2Page:

Ordered By

Attn: Marlon Cartin

ANALYTICAL RESULTS

Telephone: (702)307-2659






Date Prepared 03/04/2015 03/04/2015

EFF-03-03Effluent

Client Sample I.D.









Phenol 80-120 <15 0.00 0.500 0.432 86.4 0.500 0.445 89.0 3.0




Phenol <20 0.500 0.444 88.8 0.500 0.432 86.4 2.7 80-120

EN0501151007SCO

Appendix B Waste Manifests