september 20, 2010 asheville, nc 28804 huntersville, nc ... management/dwm/sf... · mills gap...

September 20, 2010

LIMS USE: FR - SUSAN KELLYLIMS OBJECT ID: 9276764

9276764Project:Pace Project No.:

RE:

Ms. Susan KellyMactec Asheville1308 Patton AvenueAsheville, NC 28806

MILLS GAP 6686081744

Dear Ms. Kelly:Enclosed are the analytical results for sample(s) received by the laboratory on September 01, 2010.The results relate only to the samples included in this report. Results reported herein conform to themost current NELAC standards, where applicable, unless otherwise narrated in the body of thereport.

Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory andOrganic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. AllMicrobiological analyses were performed at the laboratory where the samples were received.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Kevin Godwin

[email protected] Manager

Enclosures

REPORT OF LABORATORY ANALYSISThis report shall not be reproduced, except in full,

without the written consent of Pace Analytical Services, Inc..

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Pace Analytical Services, Inc.9800 Kincey Ave. Suite 100

Huntersville, NC 28078

(704)875-9092

Pace Analytical Services, Inc.2225 Riverside Dr.

Asheville, NC 28804

(828)254-7176

CERTIFICATIONS

Pace Project No.:Project:

9276764MILLS GAP 6686081744

Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784

South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031

Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9

North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Virginia Certification #: 00072



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(828)254-7176

SAMPLE SUMMARY


9276764MILLS GAP 6686081744

Lab ID Sample ID Matrix Date Collected Date Received

9276764001 SS-117 Solid 08/30/10 15:45 09/01/10 14:00

9276764002 SS-118 Solid 08/30/10 15:15 09/01/10 14:00

9276764003 SS-119 Solid 08/30/10 17:15 09/01/10 14:00

9276764004 SS-120 Solid 08/30/10 16:45 09/01/10 14:00

9276764005 SS-121 Solid 08/30/10 13:45 09/01/10 14:00



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(828)254-7176

SAMPLE ANALYTE COUNT


9276764MILLS GAP 6686081744

Lab ID Sample ID MethodAnalytesReportedAnalysts

9276764001 SS-117 EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276764002 SS-118 EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276764003 SS-119 EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276764004 SS-120 EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276764005 SS-121 EPA 6010 13JMW

EPA 7471 1JDA

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS



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(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276764MILLS GAP 6686081744

Parameters AnalyzedResultLab Sample ID

Report Limit QualifiersUnitsMethodClient Sample ID

9276764001 SS-117Antimony 2.1 mg/kg 09/15/10 17:341.1EPA 6010Beryllium 1.3 mg/kg 09/15/10 17:340.22EPA 6010Cadmium 2.2 mg/kg 09/15/10 17:340.22EPA 6010Chromium 70.8 mg/kg 09/15/10 17:341.1EPA 6010Copper 34.7 mg/kg 09/15/10 17:341.1EPA 6010Lead 10.1 mg/kg 09/15/10 17:341.1EPA 6010Manganese 332 mg/kg 09/15/10 17:341.1EPA 6010Nickel 17.8 mg/kg 09/15/10 17:341.1EPA 6010Selenium 1.2J mg/kg 09/15/10 17:34 D32.2EPA 6010Silver 0.27J mg/kg 09/15/10 17:34 D31.1EPA 6010Zinc 94.1 mg/kg 09/15/10 17:342.2EPA 6010Mercury 0.0093 mg/kg 09/07/10 17:170.0050EPA 7471Acetone 59.5J ug/kg 09/04/10 15:4795.9EPA 8260cis-1,2-Dichloroethene 1.8J ug/kg 09/04/10 15:474.8EPA 8260Methylene Chloride 3.7J ug/kg 09/04/10 15:4719.2EPA 8260Trichloroethene 85.0 ug/kg 09/04/10 15:474.8EPA 8260Percent Moisture 17.4 % 09/07/10 09:090.10ASTM D2974-87Cyanide 0.44 mg/kg 09/05/10 13:300.19SM 4500-CN-E

9276764002 SS-118Arsenic 5.3 mg/kg 09/15/10 17:375.1EPA 6010Beryllium 1.6 mg/kg 09/15/10 17:371.0EPA 6010Chromium 18.9 mg/kg 09/15/10 17:375.1EPA 6010Copper 12.0 mg/kg 09/15/10 17:375.1EPA 6010Lead 14.1 mg/kg 09/15/10 17:375.1EPA 6010Manganese 328 mg/kg 09/15/10 17:375.1EPA 6010Nickel 9.2 mg/kg 09/15/10 17:375.1EPA 6010Zinc 57.2 mg/kg 09/15/10 17:3710.2EPA 6010Mercury 0.00018J mg/kg 09/07/10 17:190.0048EPA 7471Acetone 14.0J ug/kg 09/04/10 16:05100EPA 8260Trichloroethene 2.8J ug/kg 09/04/10 16:055.0EPA 8260Percent Moisture 18.5 % 09/07/10 09:100.10ASTM D2974-87

9276764003 SS-119Arsenic 6.7 mg/kg 09/15/10 17:505.1EPA 6010Beryllium 2.5 mg/kg 09/15/10 17:501.0EPA 6010Chromium 34.2 mg/kg 09/15/10 17:505.1EPA 6010Copper 22.7 mg/kg 09/15/10 17:505.1EPA 6010Lead 16.0 mg/kg 09/15/10 17:505.1EPA 6010Manganese 775 mg/kg 09/15/10 17:505.1EPA 6010Nickel 30.4 mg/kg 09/15/10 17:505.1EPA 6010Selenium 3.9J mg/kg 09/15/10 17:50 D310.1EPA 6010Zinc 137 mg/kg 09/15/10 17:5010.1EPA 6010Mercury 0.0012J mg/kg 09/07/10 17:220.0046EPA 7471Acetone 45.1J ug/kg 09/04/10 16:29107EPA 8260Methylene Chloride 9.5J ug/kg 09/04/10 16:2921.5EPA 8260Trichloroethene 3.2J ug/kg 09/04/10 16:295.4EPA 8260Percent Moisture 21.5 % 09/07/10 09:110.10ASTM D2974-87



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(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276764MILLS GAP 6686081744



9276764004 SS-120Arsenic 3.4J mg/kg 09/15/10 17:54 D33.9EPA 6010Beryllium 1.6 mg/kg 09/15/10 17:540.78EPA 6010Chromium 25.4 mg/kg 09/15/10 17:543.9EPA 6010Copper 21.1 mg/kg 09/15/10 17:543.9EPA 6010Lead 18.3 mg/kg 09/15/10 17:543.9EPA 6010Manganese 1630 mg/kg 09/15/10 17:543.9EPA 6010Nickel 24.2 mg/kg 09/15/10 17:543.9EPA 6010Zinc 81.9 mg/kg 09/15/10 17:547.8EPA 6010Mercury 0.0060 mg/kg 09/07/10 17:250.0040EPA 7471Acetone 28.2J ug/kg 09/04/10 16:4893.9EPA 8260Trichloroethene 5.3 ug/kg 09/04/10 16:484.7EPA 8260Percent Moisture 13.4 % 09/07/10 09:110.10ASTM D2974-87

9276764005 SS-121Arsenic 4.1J mg/kg 09/15/10 17:57 D35.2EPA 6010Beryllium 2.1 mg/kg 09/15/10 17:571.0EPA 6010Chromium 37.3 mg/kg 09/15/10 17:575.2EPA 6010Copper 31.5 mg/kg 09/15/10 17:575.2EPA 6010Lead 10.4 mg/kg 09/15/10 17:575.2EPA 6010Manganese 714 mg/kg 09/15/10 17:575.2EPA 6010Nickel 14.5 mg/kg 09/15/10 17:575.2EPA 6010Zinc 88.7 mg/kg 09/15/10 17:5710.3EPA 6010Mercury 0.0011J mg/kg 09/07/10 17:270.0049EPA 7471Acetone 10.6J ug/kg 09/04/10 17:0697.9EPA 8260Trichloroethene 8.5 ug/kg 09/04/10 17:064.9EPA 8260Percent Moisture 17.8 % 09/07/10 09:110.10ASTM D2974-87Chromium, Hexavalent 4.9 mg/kg 09/03/10 15:114.3EPA 7196



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(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:

Client: Mactec Asheville

EPA 6010

Date: September 20, 2010

Description: 6010 MET ICP

General Information:5 samples were analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below.

Hold Time:The samples were analyzed within the method required hold times with any exceptions noted below.

Sample Preparation:The samples were prepared in accordance with EPA 3050 with any exceptions noted below.

Initial Calibrations (including MS Tune as applicable):All criteria were within method requirements with any exceptions noted below.

Continuing Calibration:All criteria were within method requirements with any exceptions noted below.

Method Blank:All analytes were below the report limit in the method blank with any exceptions noted below.

Laboratory Control Spike:All laboratory control spike compounds were within QC limits with any exceptions noted below.

Matrix Spikes:All percent recoveries and relative percent differences (RPDs) were within acceptance criteria with any exceptions noted below.

QC Batch: MPRP/7030A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750027

M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• MS (Lab ID: 494449)

• Antimony• Arsenic• Chromium• Manganese• Selenium• Zinc

• MSD (Lab ID: 494450)• Antimony• Arsenic• Manganese• Selenium

R1: RPD value was outside control limits.• MSD (Lab ID: 494450)

• Chromium• Manganese• Zinc



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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


EPA 6010



Duplicate Sample:All duplicate sample results were within method acceptance criteria with any exceptions noted below.

Additional Comments:Analyte Comments:

QC Batch: MPRP/7030D3: Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.

• SS-117 (Lab ID: 9276764001)• Silver• Arsenic• Selenium• Thallium

• SS-118 (Lab ID: 9276764002)• Silver• Cadmium• Antimony• Selenium• Thallium

• SS-119 (Lab ID: 9276764003)• Silver• Cadmium• Antimony• Selenium• Thallium

• SS-120 (Lab ID: 9276764004)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium




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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


EPA 7471


Description: 7471 Mercury









QC Batch: MERP/2996A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750027,9276750028

M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• MSD (Lab ID: 491980)

• Mercury


Additional Comments:



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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


EPA 8270


Description: 8270 MSSV Microwave






Internal Standards:All internal standards were within QC limits with any exceptions noted below.

Surrogates:All surrogates were within QC limits with any exceptions noted below.



QC Batch: OEXT/11146L2: Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated samplesmay be biased low.

• LCS (Lab ID: 496477)• Acetophenone• Benzaldehyde

L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

• LCS (Lab ID: 496477)• 2,3,4,6-Tetrachlorophenol• bis(2-Ethylhexyl)phthalate




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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


EPA 8270



QC Batch: OEXT/11146A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750026


• Benzaldehyde• Caprolactam

M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• MS (Lab ID: 496478)

• CaprolactamR1: RPD value was outside control limits.

• MSD (Lab ID: 496479)• Atrazine• Caprolactam• Di-n-octylphthalate• Hexachlorocyclopentadiene• bis(2-Ethylhexyl)phthalate





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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


EPA 8260


Description: 8260/5035A Volatile Organics














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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


SM 4500-CN-E


Description: 4500CNE Cyanide, Total

General Information:5 samples were analyzed for SM 4500-CN-E. All samples were received in acceptable condition with any exceptions noted below.











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(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276764MILLS GAP 6686081744

Method:


EPA 7196


Description: 7196 Chromium, Hexavalent









QC Batch: WETA/8088A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750013,9276750028


• Chromium, Hexavalent






This data package has been reviewed for quality and completeness and is approved for release.



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(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744

Sample: SS-117 Lab ID: 9276764001 Collected: 08/30/10 15:45 Received: 09/01/10 14:00 Matrix: SolidResults reported on a "dry-weight" basis

Parameters Results Units DF Prepared Analyzed CAS No. QualMDLLimitReport

6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050

Antimony 2.1 mg/kg 2 09/15/10 17:34 7440-36-009/08/10 15:401.1 0.63Arsenic ND mg/kg 2 09/15/10 17:34 7440-38-2 D309/08/10 15:401.1 0.72Beryllium 1.3 mg/kg 2 09/15/10 17:34 7440-41-709/08/10 15:400.22 0.045Cadmium 2.2 mg/kg 2 09/15/10 17:34 7440-43-909/08/10 15:400.22 0.13Chromium 70.8 mg/kg 2 09/15/10 17:34 7440-47-309/08/10 15:401.1 0.067Copper 34.7 mg/kg 2 09/15/10 17:34 7440-50-809/08/10 15:401.1 0.090Lead 10.1 mg/kg 2 09/15/10 17:34 7439-92-109/08/10 15:401.1 1.1Manganese 332 mg/kg 2 09/15/10 17:34 7439-96-509/08/10 15:401.1 0.067Nickel 17.8 mg/kg 2 09/15/10 17:34 7440-02-009/08/10 15:401.1 0.40Selenium 1.2J mg/kg 2 09/15/10 17:34 7782-49-2 D309/08/10 15:402.2 0.85Silver 0.27J mg/kg 2 09/15/10 17:34 7440-22-4 D309/08/10 15:401.1 0.067Thallium ND mg/kg 2 09/15/10 17:34 7440-28-0 D309/08/10 15:402.2 0.58Zinc 94.1 mg/kg 2 09/15/10 17:34 7440-66-609/08/10 15:402.2 0.58

7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471

Mercury 0.0093 mg/kg 1 09/07/10 17:17 7439-97-609/02/10 19:200.0050 0.00010

8270 MSSV Microwave Analytical Method: EPA 8270 Preparation Method: EPA 3546

Acenaphthene ND ug/kg 1 09/18/10 12:49 83-32-909/13/10 12:30399 92.0Acenaphthylene ND ug/kg 1 09/18/10 12:49 208-96-809/13/10 12:30399 94.4Acetophenone ND ug/kg 1 09/18/10 12:49 98-86-209/13/10 12:30399 206Anthracene ND ug/kg 1 09/18/10 12:49 120-12-709/13/10 12:30399 89.6Atrazine ND ug/kg 1 09/18/10 12:49 1912-24-909/13/10 12:30799 157Benzaldehyde ND ug/kg 1 09/18/10 12:49 100-52-709/13/10 12:30799 399Benzo(a)anthracene ND ug/kg 1 09/18/10 12:49 56-55-309/13/10 12:30399 73.8Benzo(a)pyrene ND ug/kg 1 09/18/10 12:49 50-32-809/13/10 12:30399 76.2Benzo(b)fluoranthene ND ug/kg 1 09/18/10 12:49 205-99-209/13/10 12:30399 69.0Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 12:49 191-24-209/13/10 12:30399 102Benzo(k)fluoranthene ND ug/kg 1 09/18/10 12:49 207-08-909/13/10 12:30399 78.7Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 12:49 92-52-409/13/10 12:30399 1264-Bromophenylphenyl ether ND ug/kg 1 09/18/10 12:49 101-55-309/13/10 12:30399 72.6Butylbenzylphthalate ND ug/kg 1 09/18/10 12:49 85-68-709/13/10 12:30399 84.7Caprolactam ND ug/kg 1 09/18/10 12:49 105-60-209/13/10 12:30399 69.0Carbazole ND ug/kg 1 09/18/10 12:49 86-74-809/13/10 12:30399 76.24-Chloro-3-methylphenol ND ug/kg 1 09/18/10 12:49 59-50-709/13/10 12:30799 82.34-Chloroaniline ND ug/kg 1 09/18/10 12:49 106-47-809/13/10 12:302000 111bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 12:49 111-91-109/13/10 12:30399 93.2bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 12:49 111-44-409/13/10 12:30399 102bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 12:49 108-60-109/13/10 12:30399 1062-Chloronaphthalene ND ug/kg 1 09/18/10 12:49 91-58-709/13/10 12:30399 78.72-Chlorophenol ND ug/kg 1 09/18/10 12:49 95-57-809/13/10 12:30399 1094-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 12:49 7005-72-309/13/10 12:30399 82.3Chrysene ND ug/kg 1 09/18/10 12:49 218-01-909/13/10 12:30399 53.2Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 12:49 53-70-309/13/10 12:30399 84.7Dibenzofuran ND ug/kg 1 09/18/10 12:49 132-64-909/13/10 12:30399 65.3



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 12:49 91-94-109/13/10 12:302000 87.12,4-Dichlorophenol ND ug/kg 1 09/18/10 12:49 120-83-209/13/10 12:30399 87.1Diethylphthalate ND ug/kg 1 09/18/10 12:49 84-66-209/13/10 12:30399 61.72,4-Dimethylphenol ND ug/kg 1 09/18/10 12:49 105-67-909/13/10 12:30399 157Dimethylphthalate ND ug/kg 1 09/18/10 12:49 131-11-309/13/10 12:30399 81.1Di-n-butylphthalate ND ug/kg 1 09/18/10 12:49 84-74-209/13/10 12:30399 65.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 12:49 534-52-109/13/10 12:30799 79.92,4-Dinitrophenol ND ug/kg 1 09/18/10 12:49 51-28-509/13/10 12:302000 65.32,4-Dinitrotoluene ND ug/kg 1 09/18/10 12:49 121-14-209/13/10 12:30399 75.02,6-Dinitrotoluene ND ug/kg 1 09/18/10 12:49 606-20-209/13/10 12:30399 83.5Di-n-octylphthalate ND ug/kg 1 09/18/10 12:49 117-84-009/13/10 12:30399 83.5bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 12:49 117-81-709/13/10 12:30399 109Fluoranthene ND ug/kg 1 09/18/10 12:49 206-44-009/13/10 12:30399 58.1Fluorene ND ug/kg 1 09/18/10 12:49 86-73-709/13/10 12:30399 82.3Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 12:49 87-68-309/13/10 12:30399 69.0Hexachlorobenzene ND ug/kg 1 09/18/10 12:49 118-74-109/13/10 12:30399 50.8Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 12:49 77-47-409/13/10 12:30399 73.8Hexachloroethane ND ug/kg 1 09/18/10 12:49 67-72-109/13/10 12:30399 105Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 12:49 193-39-509/13/10 12:30399 82.3Isophorone ND ug/kg 1 09/18/10 12:49 78-59-109/13/10 12:30399 89.62-Methylnaphthalene ND ug/kg 1 09/18/10 12:49 91-57-609/13/10 12:30399 85.92-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 12:49 95-48-709/13/10 12:30399 1213&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 12:4909/13/10 12:30399 157Naphthalene ND ug/kg 1 09/18/10 12:49 91-20-309/13/10 12:30399 98.02-Nitroaniline ND ug/kg 1 09/18/10 12:49 88-74-409/13/10 12:302000 1233-Nitroaniline ND ug/kg 1 09/18/10 12:49 99-09-209/13/10 12:302000 1094-Nitroaniline ND ug/kg 1 09/18/10 12:49 100-01-609/13/10 12:30799 113Nitrobenzene ND ug/kg 1 09/18/10 12:49 98-95-309/13/10 12:30399 1092-Nitrophenol ND ug/kg 1 09/18/10 12:49 88-75-509/13/10 12:30399 96.84-Nitrophenol ND ug/kg 1 09/18/10 12:49 100-02-709/13/10 12:302000 71.4N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 12:49 621-64-709/13/10 12:30399 76.2N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 12:49 86-30-609/13/10 12:30399 119Pentachlorophenol ND ug/kg 1 09/18/10 12:49 87-86-509/13/10 12:302000 72.6Phenanthrene ND ug/kg 1 09/18/10 12:49 85-01-809/13/10 12:30399 66.6Phenol ND ug/kg 1 09/18/10 12:49 108-95-209/13/10 12:30399 120Pyrene ND ug/kg 1 09/18/10 12:49 129-00-009/13/10 12:30399 67.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 12:49 95-94-309/13/10 12:30399 1452,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 12:49 58-90-209/13/10 12:30399 1572,4,5-Trichlorophenol ND ug/kg 1 09/18/10 12:49 95-95-409/13/10 12:30399 1232,4,6-Trichlorophenol ND ug/kg 1 09/18/10 12:49 88-06-209/13/10 12:30399 88.32-Fluorobiphenyl (S) 42 % 1 09/18/10 12:49 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 44 % 1 09/18/10 12:49 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 33 % 1 09/18/10 12:49 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 34 % 1 09/18/10 12:49 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 45 % 1 09/18/10 12:49 118-79-609/13/10 12:3027-110



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Nitrobenzene-d5 (S) 36 % 1 09/18/10 12:49 4165-60-009/13/10 12:3023-110

8260/5035A Volatile Organics Analytical Method: EPA 8260

Acetone 59.5J ug/kg 1 09/04/10 15:47 67-64-195.9 9.6Benzene ND ug/kg 1 09/04/10 15:47 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/04/10 15:47 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/04/10 15:47 75-27-44.8 1.8Bromoform ND ug/kg 1 09/04/10 15:47 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/04/10 15:47 74-83-99.6 2.42-Butanone (MEK) ND ug/kg 1 09/04/10 15:47 78-93-395.9 2.8Carbon disulfide ND ug/kg 1 09/04/10 15:47 75-15-09.6 2.9Carbon tetrachloride ND ug/kg 1 09/04/10 15:47 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/04/10 15:47 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/04/10 15:47 75-00-39.6 2.3Chloroform ND ug/kg 1 09/04/10 15:47 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/04/10 15:47 74-87-39.6 2.3Cyclohexane ND ug/kg 1 09/04/10 15:47 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/04/10 15:47 96-12-84.8 3.5Dibromochloromethane ND ug/kg 1 09/04/10 15:47 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/04/10 15:47 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/04/10 15:47 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/04/10 15:47 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/04/10 15:47 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/04/10 15:47 75-71-89.6 3.51,1-Dichloroethane ND ug/kg 1 09/04/10 15:47 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/04/10 15:47 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/04/10 15:47 75-35-44.8 1.7cis-1,2-Dichloroethene 1.8J ug/kg 1 09/04/10 15:47 156-59-24.8 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/04/10 15:47 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/04/10 15:47 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/04/10 15:47 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/04/10 15:47 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/04/10 15:47 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/04/10 15:47 591-78-647.9 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/04/10 15:47 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/04/10 15:47 79-20-99.6 1.3Methylcyclohexane ND ug/kg 1 09/04/10 15:47 108-87-29.6 1.4Methylene Chloride 3.7J ug/kg 1 09/04/10 15:47 75-09-219.2 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/04/10 15:47 108-10-147.9 3.5Methyl-tert-butyl ether ND ug/kg 1 09/04/10 15:47 1634-04-44.8 1.4Styrene ND ug/kg 1 09/04/10 15:47 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/04/10 15:47 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/04/10 15:47 127-18-44.8 1.6Toluene ND ug/kg 1 09/04/10 15:47 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/04/10 15:47 87-61-64.8 2.1



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/04/10 15:47 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/04/10 15:47 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/04/10 15:47 79-00-54.8 2.0Trichloroethene 85.0 ug/kg 1 09/04/10 15:47 79-01-64.8 2.0Trichlorofluoromethane ND ug/kg 1 09/04/10 15:47 75-69-44.8 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/04/10 15:47 76-13-14.8 1.8Vinyl chloride ND ug/kg 1 09/04/10 15:47 75-01-49.6 1.7Xylene (Total) ND ug/kg 1 09/04/10 15:47 1330-20-79.6 3.5m&p-Xylene ND ug/kg 1 09/04/10 15:47 179601-23-19.6 3.5o-Xylene ND ug/kg 1 09/04/10 15:47 95-47-64.8 1.8Dibromofluoromethane (S) 99 % 1 09/04/10 15:47 1868-53-770-130Toluene-d8 (S) 96 % 1 09/04/10 15:47 2037-26-570-1304-Bromofluorobenzene (S) 104 % 1 09/04/10 15:47 460-00-470-1301,2-Dichloroethane-d4 (S) 94 % 1 09/04/10 15:47 17060-07-070-132

Percent Moisture Analytical Method: ASTM D2974-87

Percent Moisture 17.4 % 1 09/07/10 09:090.10 0.10

4500CNE Cyanide, Total Analytical Method: SM 4500-CN-E

Cyanide 0.44 mg/kg 1 09/05/10 13:30 57-12-50.19 0.19

7196 Chromium, Hexavalent Analytical Method: EPA 7196 Preparation Method: EPA 7196

Chromium, Hexavalent ND mg/kg 1 09/03/10 11:47 18540-29-909/03/10 10:005.0 5.0



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 17:37 7440-36-0 D309/08/10 15:405.1 2.9Arsenic 5.3 mg/kg 10 09/15/10 17:37 7440-38-209/08/10 15:405.1 3.3Beryllium 1.6 mg/kg 10 09/15/10 17:37 7440-41-709/08/10 15:401.0 0.20Cadmium ND mg/kg 10 09/15/10 17:37 7440-43-9 D309/08/10 15:401.0 0.61Chromium 18.9 mg/kg 10 09/15/10 17:37 7440-47-309/08/10 15:405.1 0.31Copper 12.0 mg/kg 10 09/15/10 17:37 7440-50-809/08/10 15:405.1 0.41Lead 14.1 mg/kg 10 09/15/10 17:37 7439-92-109/08/10 15:405.1 4.9Manganese 328 mg/kg 10 09/15/10 17:37 7439-96-509/08/10 15:405.1 0.31Nickel 9.2 mg/kg 10 09/15/10 17:37 7440-02-009/08/10 15:405.1 1.8Selenium ND mg/kg 10 09/15/10 17:37 7782-49-2 D309/08/10 15:4010.2 3.9Silver ND mg/kg 10 09/15/10 17:37 7440-22-4 D309/08/10 15:405.1 0.31Thallium ND mg/kg 10 09/15/10 17:37 7440-28-0 D309/08/10 15:4010.2 2.7Zinc 57.2 mg/kg 10 09/15/10 17:37 7440-66-609/08/10 15:4010.2 2.7


Mercury 0.00018J mg/kg 1 09/07/10 17:19 7439-97-609/02/10 19:200.0048 0.000097





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744







Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Nitrobenzene-d5 (S) 31 % 1 09/17/10 15:31 4165-60-009/13/10 12:3023-110


Acetone 14.0J ug/kg 1 09/04/10 16:05 67-64-1100 10.0Benzene ND ug/kg 1 09/04/10 16:05 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/04/10 16:05 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/04/10 16:05 75-27-45.0 1.9Bromoform ND ug/kg 1 09/04/10 16:05 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/04/10 16:05 74-83-910.0 2.52-Butanone (MEK) ND ug/kg 1 09/04/10 16:05 78-93-3100 2.9Carbon disulfide ND ug/kg 1 09/04/10 16:05 75-15-010.0 3.0Carbon tetrachloride ND ug/kg 1 09/04/10 16:05 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/04/10 16:05 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/04/10 16:05 75-00-310.0 2.4Chloroform ND ug/kg 1 09/04/10 16:05 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/04/10 16:05 74-87-310.0 2.4Cyclohexane ND ug/kg 1 09/04/10 16:05 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/04/10 16:05 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/04/10 16:05 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/04/10 16:05 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/04/10 16:05 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/04/10 16:05 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/04/10 16:05 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/04/10 16:05 75-71-810.0 3.61,1-Dichloroethane ND ug/kg 1 09/04/10 16:05 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/04/10 16:05 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/04/10 16:05 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/04/10 16:05 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/04/10 16:05 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/04/10 16:05 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/04/10 16:05 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/04/10 16:05 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/04/10 16:05 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/04/10 16:05 591-78-650.2 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/04/10 16:05 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/04/10 16:05 79-20-910.0 1.4Methylcyclohexane ND ug/kg 1 09/04/10 16:05 108-87-210.0 1.5Methylene Chloride ND ug/kg 1 09/04/10 16:05 75-09-220.1 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/04/10 16:05 108-10-150.2 3.7Methyl-tert-butyl ether ND ug/kg 1 09/04/10 16:05 1634-04-45.0 1.5Styrene ND ug/kg 1 09/04/10 16:05 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/04/10 16:05 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/04/10 16:05 127-18-45.0 1.7Toluene ND ug/kg 1 09/04/10 16:05 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/04/10 16:05 87-61-65.0 2.2



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/04/10 16:05 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/04/10 16:05 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/04/10 16:05 79-00-55.0 2.1Trichloroethene 2.8J ug/kg 1 09/04/10 16:05 79-01-65.0 2.1Trichlorofluoromethane ND ug/kg 1 09/04/10 16:05 75-69-45.0 2.21,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/04/10 16:05 76-13-15.0 1.9Vinyl chloride ND ug/kg 1 09/04/10 16:05 75-01-410.0 1.8Xylene (Total) ND ug/kg 1 09/04/10 16:05 1330-20-710.0 3.6m&p-Xylene ND ug/kg 1 09/04/10 16:05 179601-23-110.0 3.6o-Xylene ND ug/kg 1 09/04/10 16:05 95-47-65.0 1.9Dibromofluoromethane (S) 99 % 1 09/04/10 16:05 1868-53-770-130Toluene-d8 (S) 97 % 1 09/04/10 16:05 2037-26-570-1304-Bromofluorobenzene (S) 101 % 1 09/04/10 16:05 460-00-470-1301,2-Dichloroethane-d4 (S) 95 % 1 09/04/10 16:05 17060-07-070-132




Cyanide ND mg/kg 1 09/05/10 13:31 57-12-50.26 0.26





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 17:50 7440-36-0 D309/08/10 15:405.1 2.8Arsenic 6.7 mg/kg 10 09/15/10 17:50 7440-38-209/08/10 15:405.1 3.2Beryllium 2.5 mg/kg 10 09/15/10 17:50 7440-41-709/08/10 15:401.0 0.20Cadmium ND mg/kg 10 09/15/10 17:50 7440-43-9 D309/08/10 15:401.0 0.61Chromium 34.2 mg/kg 10 09/15/10 17:50 7440-47-309/08/10 15:405.1 0.30Copper 22.7 mg/kg 10 09/15/10 17:50 7440-50-809/08/10 15:405.1 0.40Lead 16.0 mg/kg 10 09/15/10 17:50 7439-92-109/08/10 15:405.1 4.9Manganese 775 mg/kg 10 09/15/10 17:50 7439-96-509/08/10 15:405.1 0.30Nickel 30.4 mg/kg 10 09/15/10 17:50 7440-02-009/08/10 15:405.1 1.8Selenium 3.9J mg/kg 10 09/15/10 17:50 7782-49-2 D309/08/10 15:4010.1 3.8Silver ND mg/kg 10 09/15/10 17:50 7440-22-4 D309/08/10 15:405.1 0.30Thallium ND mg/kg 10 09/15/10 17:50 7440-28-0 D309/08/10 15:4010.1 2.6Zinc 137 mg/kg 10 09/15/10 17:50 7440-66-609/08/10 15:4010.1 2.6


Mercury 0.0012J mg/kg 1 09/07/10 17:22 7439-97-609/02/10 19:200.0046 0.000091





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/17/10 16:08 91-94-109/13/10 12:302100 91.82,4-Dichlorophenol ND ug/kg 1 09/17/10 16:08 120-83-209/13/10 12:30421 91.8Diethylphthalate ND ug/kg 1 09/17/10 16:08 84-66-209/13/10 12:30421 65.02,4-Dimethylphenol ND ug/kg 1 09/17/10 16:08 105-67-909/13/10 12:30421 166Dimethylphthalate ND ug/kg 1 09/17/10 16:08 131-11-309/13/10 12:30421 85.4Di-n-butylphthalate ND ug/kg 1 09/17/10 16:08 84-74-209/13/10 12:30421 68.84,6-Dinitro-2-methylphenol ND ug/kg 1 09/17/10 16:08 534-52-109/13/10 12:30841 84.12,4-Dinitrophenol ND ug/kg 1 09/17/10 16:08 51-28-509/13/10 12:302100 68.82,4-Dinitrotoluene ND ug/kg 1 09/17/10 16:08 121-14-209/13/10 12:30421 79.02,6-Dinitrotoluene ND ug/kg 1 09/17/10 16:08 606-20-209/13/10 12:30421 87.9Di-n-octylphthalate ND ug/kg 1 09/17/10 16:08 117-84-009/13/10 12:30421 87.9bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/17/10 16:08 117-81-709/13/10 12:30421 115Fluoranthene ND ug/kg 1 09/17/10 16:08 206-44-009/13/10 12:30421 61.2Fluorene ND ug/kg 1 09/17/10 16:08 86-73-709/13/10 12:30421 86.7Hexachloro-1,3-butadiene ND ug/kg 1 09/17/10 16:08 87-68-309/13/10 12:30421 72.6Hexachlorobenzene ND ug/kg 1 09/17/10 16:08 118-74-109/13/10 12:30421 53.5Hexachlorocyclopentadiene ND ug/kg 1 09/17/10 16:08 77-47-409/13/10 12:30421 77.7Hexachloroethane ND ug/kg 1 09/17/10 16:08 67-72-109/13/10 12:30421 111Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/17/10 16:08 193-39-509/13/10 12:30421 86.7Isophorone ND ug/kg 1 09/17/10 16:08 78-59-109/13/10 12:30421 94.32-Methylnaphthalene ND ug/kg 1 09/17/10 16:08 91-57-609/13/10 12:30421 90.52-Methylphenol(o-Cresol) ND ug/kg 1 09/17/10 16:08 95-48-709/13/10 12:30421 1273&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/17/10 16:0809/13/10 12:30421 166Naphthalene ND ug/kg 1 09/17/10 16:08 91-20-309/13/10 12:30421 1032-Nitroaniline ND ug/kg 1 09/17/10 16:08 88-74-409/13/10 12:302100 1303-Nitroaniline ND ug/kg 1 09/17/10 16:08 99-09-209/13/10 12:302100 1154-Nitroaniline ND ug/kg 1 09/17/10 16:08 100-01-609/13/10 12:30841 119Nitrobenzene ND ug/kg 1 09/17/10 16:08 98-95-309/13/10 12:30421 1152-Nitrophenol ND ug/kg 1 09/17/10 16:08 88-75-509/13/10 12:30421 1024-Nitrophenol ND ug/kg 1 09/17/10 16:08 100-02-709/13/10 12:302100 75.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/17/10 16:08 621-64-709/13/10 12:30421 80.3N-Nitrosodiphenylamine ND ug/kg 1 09/17/10 16:08 86-30-609/13/10 12:30421 125Pentachlorophenol ND ug/kg 1 09/17/10 16:08 87-86-509/13/10 12:302100 76.5Phenanthrene ND ug/kg 1 09/17/10 16:08 85-01-809/13/10 12:30421 70.1Phenol ND ug/kg 1 09/17/10 16:08 108-95-209/13/10 12:30421 126Pyrene ND ug/kg 1 09/17/10 16:08 129-00-009/13/10 12:30421 71.41,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/17/10 16:08 95-94-309/13/10 12:30421 1532,3,4,6-Tetrachlorophenol ND ug/kg 1 09/17/10 16:08 58-90-209/13/10 12:30421 1662,4,5-Trichlorophenol ND ug/kg 1 09/17/10 16:08 95-95-409/13/10 12:30421 1302,4,6-Trichlorophenol ND ug/kg 1 09/17/10 16:08 88-06-209/13/10 12:30421 93.02-Fluorobiphenyl (S) 54 % 1 09/17/10 16:08 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 53 % 1 09/17/10 16:08 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 41 % 1 09/17/10 16:08 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 41 % 1 09/17/10 16:08 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 60 % 1 09/17/10 16:08 118-79-609/13/10 12:3027-110



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Nitrobenzene-d5 (S) 48 % 1 09/17/10 16:08 4165-60-009/13/10 12:3023-110


Acetone 45.1J ug/kg 1 09/04/10 16:29 67-64-1107 10.7Benzene ND ug/kg 1 09/04/10 16:29 71-43-25.4 1.7Bromochloromethane ND ug/kg 1 09/04/10 16:29 74-97-55.4 1.8Bromodichloromethane ND ug/kg 1 09/04/10 16:29 75-27-45.4 2.0Bromoform ND ug/kg 1 09/04/10 16:29 75-25-25.4 2.5Bromomethane ND ug/kg 1 09/04/10 16:29 74-83-910.7 2.72-Butanone (MEK) ND ug/kg 1 09/04/10 16:29 78-93-3107 3.1Carbon disulfide ND ug/kg 1 09/04/10 16:29 75-15-010.7 3.2Carbon tetrachloride ND ug/kg 1 09/04/10 16:29 56-23-55.4 2.8Chlorobenzene ND ug/kg 1 09/04/10 16:29 108-90-75.4 2.0Chloroethane ND ug/kg 1 09/04/10 16:29 75-00-310.7 2.6Chloroform ND ug/kg 1 09/04/10 16:29 67-66-35.4 1.7Chloromethane ND ug/kg 1 09/04/10 16:29 74-87-310.7 2.6Cyclohexane ND ug/kg 1 09/04/10 16:29 110-82-75.4 1.71,2-Dibromo-3-chloropropane ND ug/kg 1 09/04/10 16:29 96-12-85.4 3.9Dibromochloromethane ND ug/kg 1 09/04/10 16:29 124-48-15.4 1.91,2-Dibromoethane (EDB) ND ug/kg 1 09/04/10 16:29 106-93-45.4 1.91,2-Dichlorobenzene ND ug/kg 1 09/04/10 16:29 95-50-15.4 2.01,3-Dichlorobenzene ND ug/kg 1 09/04/10 16:29 541-73-15.4 2.11,4-Dichlorobenzene ND ug/kg 1 09/04/10 16:29 106-46-75.4 1.8Dichlorodifluoromethane ND ug/kg 1 09/04/10 16:29 75-71-810.7 3.91,1-Dichloroethane ND ug/kg 1 09/04/10 16:29 75-34-35.4 1.61,2-Dichloroethane ND ug/kg 1 09/04/10 16:29 107-06-25.4 2.41,1-Dichloroethene ND ug/kg 1 09/04/10 16:29 75-35-45.4 1.9cis-1,2-Dichloroethene ND ug/kg 1 09/04/10 16:29 156-59-25.4 1.5trans-1,2-Dichloroethene ND ug/kg 1 09/04/10 16:29 156-60-55.4 2.01,2-Dichloropropane ND ug/kg 1 09/04/10 16:29 78-87-55.4 1.8cis-1,3-Dichloropropene ND ug/kg 1 09/04/10 16:29 10061-01-55.4 1.9trans-1,3-Dichloropropene ND ug/kg 1 09/04/10 16:29 10061-02-65.4 1.6Ethylbenzene ND ug/kg 1 09/04/10 16:29 100-41-45.4 1.92-Hexanone ND ug/kg 1 09/04/10 16:29 591-78-653.7 4.2Isopropylbenzene (Cumene) ND ug/kg 1 09/04/10 16:29 98-82-85.4 2.0Methyl acetate ND ug/kg 1 09/04/10 16:29 79-20-910.7 1.5Methylcyclohexane ND ug/kg 1 09/04/10 16:29 108-87-210.7 1.6Methylene Chloride 9.5J ug/kg 1 09/04/10 16:29 75-09-221.5 3.24-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/04/10 16:29 108-10-153.7 4.0Methyl-tert-butyl ether ND ug/kg 1 09/04/10 16:29 1634-04-45.4 1.6Styrene ND ug/kg 1 09/04/10 16:29 100-42-55.4 1.91,1,2,2-Tetrachloroethane ND ug/kg 1 09/04/10 16:29 79-34-55.4 2.0Tetrachloroethene ND ug/kg 1 09/04/10 16:29 127-18-45.4 1.8Toluene ND ug/kg 1 09/04/10 16:29 108-88-35.4 1.91,2,3-Trichlorobenzene ND ug/kg 1 09/04/10 16:29 87-61-65.4 2.4



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:32 57-12-50.20 0.20





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Antimony ND mg/kg 10 09/15/10 17:54 7440-36-0 D309/08/10 15:403.9 2.2Arsenic 3.4J mg/kg 10 09/15/10 17:54 7440-38-2 D309/08/10 15:403.9 2.5Beryllium 1.6 mg/kg 10 09/15/10 17:54 7440-41-709/08/10 15:400.78 0.16Cadmium ND mg/kg 10 09/15/10 17:54 7440-43-9 D309/08/10 15:400.78 0.47Chromium 25.4 mg/kg 10 09/15/10 17:54 7440-47-309/08/10 15:403.9 0.23Copper 21.1 mg/kg 10 09/15/10 17:54 7440-50-809/08/10 15:403.9 0.31Lead 18.3 mg/kg 10 09/15/10 17:54 7439-92-109/08/10 15:403.9 3.7Manganese 1630 mg/kg 10 09/15/10 17:54 7439-96-509/08/10 15:403.9 0.23Nickel 24.2 mg/kg 10 09/15/10 17:54 7440-02-009/08/10 15:403.9 1.4Selenium ND mg/kg 10 09/15/10 17:54 7782-49-2 D309/08/10 15:407.8 3.0Silver ND mg/kg 10 09/15/10 17:54 7440-22-4 D309/08/10 15:403.9 0.23Thallium ND mg/kg 10 09/15/10 17:54 7440-28-0 D309/08/10 15:407.8 2.0Zinc 81.9 mg/kg 10 09/15/10 17:54 7440-66-609/08/10 15:407.8 2.0


Mercury 0.0060 mg/kg 1 09/07/10 17:25 7439-97-609/02/10 19:200.0040 0.000081


Acenaphthene ND ug/kg 1 09/17/10 16:45 83-32-909/13/10 12:30381 87.7Acenaphthylene ND ug/kg 1 09/17/10 16:45 208-96-809/13/10 12:30381 90.1Acetophenone ND ug/kg 1 09/17/10 16:45 98-86-209/13/10 12:30381 196Anthracene ND ug/kg 1 09/17/10 16:45 120-12-709/13/10 12:30381 85.4Atrazine ND ug/kg 1 09/17/10 16:45 1912-24-909/13/10 12:30762 150Benzaldehyde ND ug/kg 1 09/17/10 16:45 100-52-709/13/10 12:30762 381Benzo(a)anthracene ND ug/kg 1 09/17/10 16:45 56-55-309/13/10 12:30381 70.4Benzo(a)pyrene ND ug/kg 1 09/17/10 16:45 50-32-809/13/10 12:30381 72.7Benzo(b)fluoranthene ND ug/kg 1 09/17/10 16:45 205-99-209/13/10 12:30381 65.8Benzo(g,h,i)perylene ND ug/kg 1 09/17/10 16:45 191-24-209/13/10 12:30381 97.0Benzo(k)fluoranthene ND ug/kg 1 09/17/10 16:45 207-08-909/13/10 12:30381 75.0Biphenyl (Diphenyl) ND ug/kg 1 09/17/10 16:45 92-52-409/13/10 12:30381 1204-Bromophenylphenyl ether ND ug/kg 1 09/17/10 16:45 101-55-309/13/10 12:30381 69.3Butylbenzylphthalate ND ug/kg 1 09/17/10 16:45 85-68-709/13/10 12:30381 80.8Caprolactam ND ug/kg 1 09/17/10 16:45 105-60-209/13/10 12:30381 65.8Carbazole ND ug/kg 1 09/17/10 16:45 86-74-809/13/10 12:30381 72.74-Chloro-3-methylphenol ND ug/kg 1 09/17/10 16:45 59-50-709/13/10 12:30762 78.54-Chloroaniline ND ug/kg 1 09/17/10 16:45 106-47-809/13/10 12:301910 106bis(2-Chloroethoxy)methane ND ug/kg 1 09/17/10 16:45 111-91-109/13/10 12:30381 88.9bis(2-Chloroethyl) ether ND ug/kg 1 09/17/10 16:45 111-44-409/13/10 12:30381 97.0bis(2-Chloroisopropyl) ether ND ug/kg 1 09/17/10 16:45 108-60-109/13/10 12:30381 1022-Chloronaphthalene ND ug/kg 1 09/17/10 16:45 91-58-709/13/10 12:30381 75.02-Chlorophenol ND ug/kg 1 09/17/10 16:45 95-57-809/13/10 12:30381 1044-Chlorophenylphenyl ether ND ug/kg 1 09/17/10 16:45 7005-72-309/13/10 12:30381 78.5Chrysene ND ug/kg 1 09/17/10 16:45 218-01-909/13/10 12:30381 50.8Dibenz(a,h)anthracene ND ug/kg 1 09/17/10 16:45 53-70-309/13/10 12:30381 80.8Dibenzofuran ND ug/kg 1 09/17/10 16:45 132-64-909/13/10 12:30381 62.3



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744







Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Nitrobenzene-d5 (S) 38 % 1 09/17/10 16:45 4165-60-009/13/10 12:3023-110


Acetone 28.2J ug/kg 1 09/04/10 16:48 67-64-193.9 9.4Benzene ND ug/kg 1 09/04/10 16:48 71-43-24.7 1.5Bromochloromethane ND ug/kg 1 09/04/10 16:48 74-97-54.7 1.6Bromodichloromethane ND ug/kg 1 09/04/10 16:48 75-27-44.7 1.8Bromoform ND ug/kg 1 09/04/10 16:48 75-25-24.7 2.2Bromomethane ND ug/kg 1 09/04/10 16:48 74-83-99.4 2.32-Butanone (MEK) ND ug/kg 1 09/04/10 16:48 78-93-393.9 2.7Carbon disulfide ND ug/kg 1 09/04/10 16:48 75-15-09.4 2.8Carbon tetrachloride ND ug/kg 1 09/04/10 16:48 56-23-54.7 2.4Chlorobenzene ND ug/kg 1 09/04/10 16:48 108-90-74.7 1.8Chloroethane ND ug/kg 1 09/04/10 16:48 75-00-39.4 2.3Chloroform ND ug/kg 1 09/04/10 16:48 67-66-34.7 1.5Chloromethane ND ug/kg 1 09/04/10 16:48 74-87-39.4 2.3Cyclohexane ND ug/kg 1 09/04/10 16:48 110-82-74.7 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/04/10 16:48 96-12-84.7 3.4Dibromochloromethane ND ug/kg 1 09/04/10 16:48 124-48-14.7 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/04/10 16:48 106-93-44.7 1.71,2-Dichlorobenzene ND ug/kg 1 09/04/10 16:48 95-50-14.7 1.81,3-Dichlorobenzene ND ug/kg 1 09/04/10 16:48 541-73-14.7 1.91,4-Dichlorobenzene ND ug/kg 1 09/04/10 16:48 106-46-74.7 1.6Dichlorodifluoromethane ND ug/kg 1 09/04/10 16:48 75-71-89.4 3.41,1-Dichloroethane ND ug/kg 1 09/04/10 16:48 75-34-34.7 1.41,2-Dichloroethane ND ug/kg 1 09/04/10 16:48 107-06-24.7 2.11,1-Dichloroethene ND ug/kg 1 09/04/10 16:48 75-35-44.7 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/04/10 16:48 156-59-24.7 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/04/10 16:48 156-60-54.7 1.81,2-Dichloropropane ND ug/kg 1 09/04/10 16:48 78-87-54.7 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/04/10 16:48 10061-01-54.7 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/04/10 16:48 10061-02-64.7 1.4Ethylbenzene ND ug/kg 1 09/04/10 16:48 100-41-44.7 1.72-Hexanone ND ug/kg 1 09/04/10 16:48 591-78-646.9 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/04/10 16:48 98-82-84.7 1.8Methyl acetate ND ug/kg 1 09/04/10 16:48 79-20-99.4 1.3Methylcyclohexane ND ug/kg 1 09/04/10 16:48 108-87-29.4 1.4Methylene Chloride ND ug/kg 1 09/04/10 16:48 75-09-218.8 2.84-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/04/10 16:48 108-10-146.9 3.5Methyl-tert-butyl ether ND ug/kg 1 09/04/10 16:48 1634-04-44.7 1.4Styrene ND ug/kg 1 09/04/10 16:48 100-42-54.7 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/04/10 16:48 79-34-54.7 1.8Tetrachloroethene ND ug/kg 1 09/04/10 16:48 127-18-44.7 1.6Toluene ND ug/kg 1 09/04/10 16:48 108-88-34.7 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/04/10 16:48 87-61-64.7 2.1



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:34 57-12-50.35 0.35





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744






Mercury 0.0011J mg/kg 1 09/07/10 17:27 7439-97-609/02/10 19:200.0049 0.000099





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744







Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744




Nitrobenzene-d5 (S) 41 % 1 09/18/10 13:25 4165-60-009/13/10 12:3023-110





Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276764MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/05/10 13:36 57-12-50.17 0.17


Chromium, Hexavalent 4.9 mg/kg 1 09/03/10 15:11 18540-29-909/03/10 14:004.3 4.3



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

QUALITY CONTROL DATA


9276764MILLS GAP 6686081744

QC Batch:QC Batch Method:

Analysis Method:Analysis Description:

MPRP/7030EPA 3050

EPA 60106010 MET

Associated Lab Samples: 9276764001, 9276764002, 9276764003, 9276764004, 9276764005

Parameter UnitsBlankResult

ReportingLimit Qualifiers

METHOD BLANK: 494447


Matrix: Solid

Analyzed

Antimony mg/kg ND 0.50 09/15/10 07:52Arsenic mg/kg ND 0.50 09/15/10 07:52Beryllium mg/kg ND 0.10 09/15/10 07:52Cadmium mg/kg ND 0.10 09/15/10 07:52Chromium mg/kg ND 0.50 09/15/10 07:52Copper mg/kg ND 0.50 09/15/10 07:52Lead mg/kg ND 0.50 09/15/10 07:52Manganese mg/kg 0.33J 0.50 09/15/10 07:52Nickel mg/kg ND 0.50 09/15/10 07:52Selenium mg/kg ND 1.0 09/15/10 07:52Silver mg/kg ND 0.50 09/15/10 07:52Thallium mg/kg ND 1.0 09/15/10 07:52Zinc mg/kg 0.31J 1.0 09/15/10 07:52

Parameter UnitsLCS

Result% RecLimits Qualifiers% RecConc.

494448LABORATORY CONTROL SAMPLE:LCSSpike

Antimony mg/kg 49.850 100 80-120Arsenic mg/kg 50.250 100 80-120Beryllium mg/kg 50.850 102 80-120Cadmium mg/kg 50.650 101 80-120Chromium mg/kg 50.450 101 80-120Copper mg/kg 51.950 104 80-120Lead mg/kg 50.850 102 80-120Manganese mg/kg 51.050 102 80-120Nickel mg/kg 50.450 101 80-120Selenium mg/kg 49.650 99 80-120Silver mg/kg 22.925 92 80-120Thallium mg/kg 48.950 98 80-120Zinc mg/kg 50.650 101 80-120

Parameter UnitsMS

Result% RecLimits Qual% RecConc.

494449MATRIX SPIKE & MATRIX SPIKE DUPLICATE:

MSSpikeResult

9276750027

494450

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Antimony mg/kg M045.7 45 75-12548 16 2050.8ND 21.5 25.1Arsenic mg/kg M045.7 62 75-12559 5 2050.8ND 31.0 32.6Beryllium mg/kg 45.7 90 75-12588 8 2050.81.5 42.4 45.9Cadmium mg/kg 45.7 83 75-12582 9 2050.8ND 38.0 41.7Chromium mg/kg M0,R145.7 137 75-12585 27 2050.819.1 82.0 62.4



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750027

494450

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Copper mg/kg 45.7 87 75-12580 2 2050.816.0 55.6 56.9Lead mg/kg 45.7 104 75-12582 11 2050.89.4 57.1 51.3Manganese mg/kg M0,R145.7 669 75-125-46 40 2050.8692 998 669Nickel mg/kg 45.7 110 75-12581 15 2050.816.8 67.2 57.9Selenium mg/kg M045.7 63 75-12556 0 2050.8ND 30.8 30.8Silver mg/kg 22.8 79 75-12577 8 2025.3ND 18.0 19.6Thallium mg/kg 45.7 76 75-12577 12 2050.8ND 34.5 38.9Zinc mg/kg M0,R145.7 149 75-12581 26 2050.848.9 117 89.9



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



MERP/2996EPA 7471

EPA 74717471 Mercury






Matrix: Solid

Analyzed

Mercury mg/kg ND 0.0050 09/07/10 16:28

Parameter UnitsLCS



Mercury mg/kg 0.072.067 108 80-120

Parameter UnitsMS



MSSpikeResult

9276750027

491980

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg D6,M1.056 85 75-125190 80 20.0590.00043J

0.048 0.11

Parameter UnitsMS



MSSpikeResult

9276750028

491982

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .069 107 75-12588 17 20.071ND 0.073 0.062



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



OEXT/11146EPA 3546

EPA 82708270 Solid MSSV Microwave






Matrix: Solid

Analyzed

1,2,4,5-Tetrachlorobenzene ug/kg ND 330 09/17/10 05:392,3,4,6-Tetrachlorophenol ug/kg ND 330 09/17/10 05:392,4,5-Trichlorophenol ug/kg ND 330 09/17/10 05:392,4,6-Trichlorophenol ug/kg ND 330 09/17/10 05:392,4-Dichlorophenol ug/kg ND 330 09/17/10 05:392,4-Dimethylphenol ug/kg ND 330 09/17/10 05:392,4-Dinitrophenol ug/kg ND 1650 09/17/10 05:392,4-Dinitrotoluene ug/kg ND 330 09/17/10 05:392,6-Dinitrotoluene ug/kg ND 330 09/17/10 05:392-Chloronaphthalene ug/kg ND 330 09/17/10 05:392-Chlorophenol ug/kg ND 330 09/17/10 05:392-Methylnaphthalene ug/kg ND 330 09/17/10 05:392-Methylphenol(o-Cresol) ug/kg ND 330 09/17/10 05:392-Nitroaniline ug/kg ND 1650 09/17/10 05:392-Nitrophenol ug/kg ND 330 09/17/10 05:393&4-Methylphenol(m&p Cresol) ug/kg ND 330 09/17/10 05:393,3'-Dichlorobenzidine ug/kg ND 1650 09/17/10 05:393-Nitroaniline ug/kg ND 1650 09/17/10 05:394,6-Dinitro-2-methylphenol ug/kg ND 660 09/17/10 05:394-Bromophenylphenyl ether ug/kg ND 330 09/17/10 05:394-Chloro-3-methylphenol ug/kg ND 660 09/17/10 05:394-Chloroaniline ug/kg ND 1650 09/17/10 05:394-Chlorophenylphenyl ether ug/kg ND 330 09/17/10 05:394-Nitroaniline ug/kg ND 660 09/17/10 05:394-Nitrophenol ug/kg ND 1650 09/17/10 05:39Acenaphthene ug/kg ND 330 09/17/10 05:39Acenaphthylene ug/kg ND 330 09/17/10 05:39Acetophenone ug/kg ND 330 09/17/10 05:39Anthracene ug/kg ND 330 09/17/10 05:39Atrazine ug/kg ND 660 09/17/10 05:39Benzaldehyde ug/kg ND 660 09/17/10 05:39Benzo(a)anthracene ug/kg ND 330 09/17/10 05:39Benzo(a)pyrene ug/kg ND 330 09/17/10 05:39Benzo(b)fluoranthene ug/kg ND 330 09/17/10 05:39Benzo(g,h,i)perylene ug/kg ND 330 09/17/10 05:39Benzo(k)fluoranthene ug/kg ND 330 09/17/10 05:39Biphenyl (Diphenyl) ug/kg ND 330 09/17/10 05:39bis(2-Chloroethoxy)methane ug/kg ND 330 09/17/10 05:39bis(2-Chloroethyl) ether ug/kg ND 330 09/17/10 05:39bis(2-Chloroisopropyl) ether ug/kg ND 330 09/17/10 05:39bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/17/10 05:39Butylbenzylphthalate ug/kg ND 330 09/17/10 05:39Caprolactam ug/kg ND 330 09/17/10 05:39



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744





Matrix: Solid

Analyzed

Carbazole ug/kg ND 330 09/17/10 05:39Chrysene ug/kg ND 330 09/17/10 05:39Di-n-butylphthalate ug/kg ND 330 09/17/10 05:39Di-n-octylphthalate ug/kg ND 330 09/17/10 05:39Dibenz(a,h)anthracene ug/kg ND 330 09/17/10 05:39Dibenzofuran ug/kg ND 330 09/17/10 05:39Diethylphthalate ug/kg ND 330 09/17/10 05:39Dimethylphthalate ug/kg ND 330 09/17/10 05:39Fluoranthene ug/kg ND 330 09/17/10 05:39Fluorene ug/kg ND 330 09/17/10 05:39Hexachloro-1,3-butadiene ug/kg ND 330 09/17/10 05:39Hexachlorobenzene ug/kg ND 330 09/17/10 05:39Hexachlorocyclopentadiene ug/kg ND 330 09/17/10 05:39Hexachloroethane ug/kg ND 330 09/17/10 05:39Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/17/10 05:39Isophorone ug/kg ND 330 09/17/10 05:39N-Nitroso-di-n-propylamine ug/kg ND 330 09/17/10 05:39N-Nitrosodiphenylamine ug/kg ND 330 09/17/10 05:39Naphthalene ug/kg ND 330 09/17/10 05:39Nitrobenzene ug/kg ND 330 09/17/10 05:39Pentachlorophenol ug/kg ND 1650 09/17/10 05:39Phenanthrene ug/kg ND 330 09/17/10 05:39Phenol ug/kg ND 330 09/17/10 05:39Pyrene ug/kg ND 330 09/17/10 05:392,4,6-Tribromophenol (S) % 98 27-110 09/17/10 05:392-Fluorobiphenyl (S) % 73 30-110 09/17/10 05:392-Fluorophenol (S) % 61 13-110 09/17/10 05:39Nitrobenzene-d5 (S) % 65 23-110 09/17/10 05:39Phenol-d6 (S) % 59 22-110 09/17/10 05:39Terphenyl-d14 (S) % 82 28-110 09/17/10 05:39

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/kg 9612,3,4,6-Tetrachlorophenol ug/kg 2480 L31670 149 39-1122,4,5-Trichlorophenol ug/kg 11001670 66 48-1092,4,6-Trichlorophenol ug/kg 11501670 69 45-1112,4-Dichlorophenol ug/kg 9091670 55 51-1162,4-Dimethylphenol ug/kg 8691670 52 42-1032,4-Dinitrophenol ug/kg 52408330 63 28-1032,4-Dinitrotoluene ug/kg 10601670 63 46-1142,6-Dinitrotoluene ug/kg 10301670 62 48-1122-Chloronaphthalene ug/kg 11801670 71 44-1052-Chlorophenol ug/kg 8521670 51 36-110



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 8291670 50 39-1122-Methylphenol(o-Cresol) ug/kg 9031670 54 39-1012-Nitroaniline ug/kg 18203330 55 44-1112-Nitrophenol ug/kg 7581670 45 41-1003&4-Methylphenol(m&p Cresol) ug/kg 9391670 56 43-1033,3'-Dichlorobenzidine ug/kg 25003330 75 10-1503-Nitroaniline ug/kg 17703330 53 35-1104,6-Dinitro-2-methylphenol ug/kg 23103330 69 38-1184-Bromophenylphenyl ether ug/kg 12501670 75 47-1154-Chloro-3-methylphenol ug/kg 18603330 56 43-1274-Chloroaniline ug/kg 1620J3330 49 34-1094-Chlorophenylphenyl ether ug/kg 11901670 72 44-1154-Nitroaniline ug/kg 18703330 56 37-1114-Nitrophenol ug/kg 60608330 73 21-152Acenaphthene ug/kg 10501670 63 38-117Acenaphthylene ug/kg 10201670 61 46-107Acetophenone ug/kg 917 L23330 28 39-112Anthracene ug/kg 10101670 61 50-110Atrazine ug/kg 15301670 92 39-112Benzaldehyde ug/kg 628J L21670 38 39-112Benzo(a)anthracene ug/kg 13201670 79 47-116Benzo(a)pyrene ug/kg 10501670 63 47-106Benzo(b)fluoranthene ug/kg 12401670 74 47-109Benzo(g,h,i)perylene ug/kg 11401670 68 39-115Benzo(k)fluoranthene ug/kg 11301670 68 45-117Biphenyl (Diphenyl) ug/kg 9961670 60 39-112bis(2-Chloroethoxy)methane ug/kg 9491670 57 39-110bis(2-Chloroethyl) ether ug/kg 8141670 49 19-119bis(2-Chloroisopropyl) ether ug/kg 6471670 39 21-110bis(2-Ethylhexyl)phthalate ug/kg 3320 L31670 199 35-116Butylbenzylphthalate ug/kg 9641670 58 38-110Caprolactam ug/kg 8351670 50 39-112Carbazole ug/kg 9831670 59 39-112Chrysene ug/kg 10701670 64 49-110Di-n-butylphthalate ug/kg 9961670 60 43-109Di-n-octylphthalate ug/kg 9441670 57 37-109Dibenz(a,h)anthracene ug/kg 12701670 76 43-116Dibenzofuran ug/kg 10801670 65 45-106Diethylphthalate ug/kg 10601670 63 41-114Dimethylphthalate ug/kg 10301670 62 43-110Fluoranthene ug/kg 10501670 63 50-114Fluorene ug/kg 11601670 70 46-114Hexachloro-1,3-butadiene ug/kg 8841670 53 28-111Hexachlorobenzene ug/kg 12401670 74 46-120Hexachlorocyclopentadiene ug/kg 10001670 60 18-119Hexachloroethane ug/kg 9651670 58 33-110Indeno(1,2,3-cd)pyrene ug/kg 11901670 71 42-115Isophorone ug/kg 7681670 46 44-109



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsLCS



N-Nitroso-di-n-propylamine ug/kg 8931670 54 43-104N-Nitrosodiphenylamine ug/kg 10901670 66 48-113Naphthalene ug/kg 7591670 46 41-110Nitrobenzene ug/kg 7121670 43 38-110Pentachlorophenol ug/kg 27103330 81 32-128Phenanthrene ug/kg 10801670 65 50-110Phenol ug/kg 8691670 52 28-106Pyrene ug/kg 9711670 58 45-1142,4,6-Tribromophenol (S) % 78 27-1102-Fluorobiphenyl (S) % 62 30-1102-Fluorophenol (S) % 46 13-110Nitrobenzene-d5 (S) % 41 23-110Phenol-d6 (S) % 48 22-110Terphenyl-d14 (S) % 63 28-110

Parameter UnitsMS



MSSpikeResult

9276750026

496479

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 16 30967 8262,3,4,6-Tetrachlorophenol ug/kg 28 302230 16802,4,5-Trichlorophenol ug/kg 18 301090 9092,4,6-Trichlorophenol ug/kg 17 301130 9542,4-Dichlorophenol ug/kg 15 30937 8072,4-Dimethylphenol ug/kg 9 30772 7092,4-Dinitrophenol ug/kg 17 304370 36902,4-Dinitrotoluene ug/kg 6 301030 9712,6-Dinitrotoluene ug/kg 5 301010 9602-Chloronaphthalene ug/kg 6 301210 11502-Chlorophenol ug/kg 16 30958 8192-Methylnaphthalene ug/kg 5 30876 8312-Methylphenol(o-Cresol) ug/kg 13 30917 8072-Nitroaniline ug/kg 3 301790 18402-Nitrophenol ug/kg 9 30837 7623&4-Methylphenol(m&pCresol)

ug/kg 25 30964 747

3,3'-Dichlorobenzidine ug/kg 301840 1430J3-Nitroaniline ug/kg 301530J 1730J4,6-Dinitro-2-methylphenol ug/kg 19 302020 16704-Bromophenylphenyl ether ug/kg 23 301180 9414-Chloro-3-methylphenol ug/kg 8 301820 16804-Chloroaniline ug/kg 301470J 1490J4-Chlorophenylphenyl ether ug/kg 16 301180 10004-Nitroaniline ug/kg 6 301720 18204-Nitrophenol ug/kg 11 305600 5030Acenaphthene ug/kg 2 301060 1040Acenaphthylene ug/kg 0 301020 1020



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750026

496479

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg 14 301010 878Anthracene ug/kg 2 30955 939Atrazine ug/kg R155 301180 2090Benzaldehyde ug/kg M030584J 693JBenzo(a)anthracene ug/kg 26 301190 915Benzo(a)pyrene ug/kg 9 30973 892Benzo(b)fluoranthene ug/kg 30 301230 912Benzo(g,h,i)perylene ug/kg 8 301100 1010Benzo(k)fluoranthene ug/kg 2 30969 988Biphenyl (Diphenyl) ug/kg 1 301030 1010bis(2-Chloroethoxy)methane ug/kg 10 301020 919bis(2-Chloroethyl) ether ug/kg 4 30904 870bis(2-Chloroisopropyl) ether ug/kg 5 30712 751bis(2-Ethylhexyl)phthalate ug/kg R140 302940 1960Butylbenzylphthalate ug/kg 15 30867 749Caprolactam ug/kg M0,

M1,R135 30729 1040

Carbazole ug/kg 7 30919 981Chrysene ug/kg 6 30999 939Di-n-butylphthalate ug/kg 14 30908 789Di-n-octylphthalate ug/kg R135 30880 616Dibenz(a,h)anthracene ug/kg 18 301200 1000Dibenzofuran ug/kg 3 301080 1050Diethylphthalate ug/kg 10 301020 926Dimethylphthalate ug/kg 4 301010 972Fluoranthene ug/kg 2 30956 938Fluorene ug/kg 12 301130 995Hexachloro-1,3-butadiene ug/kg 8 301000 922Hexachlorobenzene ug/kg 18 301180 989Hexachlorocyclopentadiene ug/kg R143 301210 776Hexachloroethane ug/kg 8 301060 976Indeno(1,2,3-cd)pyrene ug/kg 16 301130 969Isophorone ug/kg 0 30802 805N-Nitroso-di-n-propylamine ug/kg 15 30946 816N-Nitrosodiphenylamine ug/kg 12 301020 906Naphthalene ug/kg 1 30866 871Nitrobenzene ug/kg 2 30812 825Pentachlorophenol ug/kg 302420 1520JPhenanthrene ug/kg 6 301020 960Phenol ug/kg 12 30931 825Pyrene ug/kg 2 30927 9442,4,6-Tribromophenol (S) % 69 27-110572-Fluorobiphenyl (S) % 62 30-110612-Fluorophenol (S) % 50 13-11049Nitrobenzene-d5 (S) % 44 23-11047Phenol-d6 (S) % 49 22-11047Terphenyl-d14 (S) % 56 28-11054



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



MSV/12131EPA 8260

EPA 82608260 MSV 5035A Volatile Organics






Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/04/10 13:191,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/04/10 13:191,1,2-Trichloroethane ug/kg ND 5.0 09/04/10 13:191,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/04/10 13:191,1-Dichloroethane ug/kg ND 5.0 09/04/10 13:191,1-Dichloroethene ug/kg ND 5.0 09/04/10 13:191,2,3-Trichlorobenzene ug/kg ND 5.0 09/04/10 13:191,2,4-Trichlorobenzene ug/kg ND 5.0 09/04/10 13:191,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/04/10 13:191,2-Dibromoethane (EDB) ug/kg ND 5.0 09/04/10 13:191,2-Dichlorobenzene ug/kg ND 5.0 09/04/10 13:191,2-Dichloroethane ug/kg ND 5.0 09/04/10 13:191,2-Dichloropropane ug/kg ND 5.0 09/04/10 13:191,3-Dichlorobenzene ug/kg ND 5.0 09/04/10 13:191,4-Dichlorobenzene ug/kg ND 5.0 09/04/10 13:192-Butanone (MEK) ug/kg ND 100 09/04/10 13:192-Hexanone ug/kg ND 50.0 09/04/10 13:194-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/04/10 13:19Acetone ug/kg ND 100 09/04/10 13:19Benzene ug/kg ND 5.0 09/04/10 13:19Bromochloromethane ug/kg ND 5.0 09/04/10 13:19Bromodichloromethane ug/kg ND 5.0 09/04/10 13:19Bromoform ug/kg ND 5.0 09/04/10 13:19Bromomethane ug/kg ND 10.0 09/04/10 13:19Carbon disulfide ug/kg ND 10.0 09/04/10 13:19Carbon tetrachloride ug/kg ND 5.0 09/04/10 13:19Chlorobenzene ug/kg ND 5.0 09/04/10 13:19Chloroethane ug/kg ND 10.0 09/04/10 13:19Chloroform ug/kg ND 5.0 09/04/10 13:19Chloromethane ug/kg ND 10.0 09/04/10 13:19cis-1,2-Dichloroethene ug/kg ND 5.0 09/04/10 13:19cis-1,3-Dichloropropene ug/kg ND 5.0 09/04/10 13:19Cyclohexane ug/kg ND 5.0 09/04/10 13:19Dibromochloromethane ug/kg ND 5.0 09/04/10 13:19Dichlorodifluoromethane ug/kg ND 10.0 09/04/10 13:19Ethylbenzene ug/kg ND 5.0 09/04/10 13:19Isopropylbenzene (Cumene) ug/kg ND 5.0 09/04/10 13:19m&p-Xylene ug/kg ND 10.0 09/04/10 13:19Methyl acetate ug/kg ND 10.0 09/04/10 13:19Methyl-tert-butyl ether ug/kg ND 5.0 09/04/10 13:19Methylcyclohexane ug/kg ND 10.0 09/04/10 13:19Methylene Chloride ug/kg ND 20.0 09/04/10 13:19o-Xylene ug/kg ND 5.0 09/04/10 13:19



Date: 09/20/2010 01:52 PM of 54



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(828)254-7176



9276764MILLS GAP 6686081744





Matrix: Solid

Analyzed

Styrene ug/kg ND 5.0 09/04/10 13:19Tetrachloroethene ug/kg ND 5.0 09/04/10 13:19Toluene ug/kg ND 5.0 09/04/10 13:19trans-1,2-Dichloroethene ug/kg ND 5.0 09/04/10 13:19trans-1,3-Dichloropropene ug/kg ND 5.0 09/04/10 13:19Trichloroethene ug/kg ND 5.0 09/04/10 13:19Trichlorofluoromethane ug/kg ND 5.0 09/04/10 13:19Vinyl chloride ug/kg ND 10.0 09/04/10 13:19Xylene (Total) ug/kg ND 10.0 09/04/10 13:191,2-Dichloroethane-d4 (S) % 91 70-132 09/04/10 13:194-Bromofluorobenzene (S) % 100 70-130 09/04/10 13:19Dibromofluoromethane (S) % 99 70-130 09/04/10 13:19Toluene-d8 (S) % 99 70-130 09/04/10 13:19

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 49.050 98 70-1411,1,2,2-Tetrachloroethane ug/kg 59.350 119 70-1301,1,2-Trichloroethane ug/kg 56.250 112 70-1321,1,2-Trichlorotrifluoroethane ug/kg 52.350 105 70-1301,1-Dichloroethane ug/kg 51.350 103 70-1431,1-Dichloroethene ug/kg 52.550 105 70-1371,2,3-Trichlorobenzene ug/kg 54.250 108 69-1531,2,4-Trichlorobenzene ug/kg 56.750 113 55-1711,2-Dibromo-3-chloropropane ug/kg 52.850 106 68-1411,2-Dibromoethane (EDB) ug/kg 57.650 115 70-1301,2-Dichlorobenzene ug/kg 53.950 108 70-1401,2-Dichloroethane ug/kg 49.250 98 70-1371,2-Dichloropropane ug/kg 47.950 96 70-1331,3-Dichlorobenzene ug/kg 53.950 108 70-1441,4-Dichlorobenzene ug/kg 50.950 102 70-1422-Butanone (MEK) ug/kg 99.3J100 99 70-1492-Hexanone ug/kg 119100 119 70-1494-Methyl-2-pentanone (MIBK) ug/kg 99.5100 100 70-153Acetone ug/kg 108100 108 70-157Benzene ug/kg 50.950 102 70-130Bromochloromethane ug/kg 60.550 121 70-149Bromodichloromethane ug/kg 50.250 100 70-130Bromoform ug/kg 53.450 107 70-131Bromomethane ug/kg 47.150 94 64-136Carbon disulfide ug/kg 52.150 104 70-130Carbon tetrachloride ug/kg 56.150 112 70-154Chlorobenzene ug/kg 57.750 115 70-135Chloroethane ug/kg 50.850 102 68-151



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsLCS



Chloroform ug/kg 50.850 102 70-130Chloromethane ug/kg 45.050 90 70-132cis-1,2-Dichloroethene ug/kg 49.550 99 70-140cis-1,3-Dichloropropene ug/kg 49.350 99 70-137Cyclohexane ug/kg 49.350 99 70-130Dibromochloromethane ug/kg 51.450 103 70-130Dichlorodifluoromethane ug/kg 47.750 95 36-148Ethylbenzene ug/kg 57.150 114 70-137Isopropylbenzene (Cumene) ug/kg 59.150 118 70-141m&p-Xylene ug/kg 115100 115 70-140Methyl acetate ug/kg 55.250 110 70-130Methyl-tert-butyl ether ug/kg 50.950 102 45-150Methylcyclohexane ug/kg 54.050 108 70-130Methylene Chloride ug/kg 34.950 70 70-133o-Xylene ug/kg 57.550 115 70-141Styrene ug/kg 59.450 119 70-138Tetrachloroethene ug/kg 59.450 119 70-140Toluene ug/kg 53.350 107 70-130trans-1,2-Dichloroethene ug/kg 49.650 99 70-136trans-1,3-Dichloropropene ug/kg 48.950 98 70-138Trichloroethene ug/kg 54.850 110 70-132Trichlorofluoromethane ug/kg 53.650 107 69-134Vinyl chloride ug/kg 50.050 100 55-140Xylene (Total) ug/kg 173150 115 70-1411,2-Dichloroethane-d4 (S) % 91 70-1324-Bromofluorobenzene (S) % 107 70-130Dibromofluoromethane (S) % 96 70-130Toluene-d8 (S) % 98 70-130

Parameter UnitsMS


493670MATRIX SPIKE SAMPLE:MSSpike

Result9276939001

1,1-Dichloroethene ug/kg 43.646.4 94 49-180NDBenzene ug/kg 40.346.4 87 50-166NDChlorobenzene ug/kg 38.146.4 82 43-169NDToluene ug/kg 40.446.4 87 52-163NDTrichloroethene ug/kg 41.246.4 89 49-167ND1,2-Dichloroethane-d4 (S) % 109 70-1324-Bromofluorobenzene (S) % 99 70-130Dibromofluoromethane (S) % 102 70-130Toluene-d8 (S) % 99 70-130



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsMS



Result9276964002


Parameter UnitsDup

ResultMaxRPD QualifiersRPDResult

9276964001493669SAMPLE DUPLICATE:

1,1,1-Trichloroethane ug/kg ND 30ND1,1,2,2-Tetrachloroethane ug/kg ND 30ND1,1,2-Trichloroethane ug/kg ND 30ND1,1,2-Trichlorotrifluoroethane ug/kg ND 30ND1,1-Dichloroethane ug/kg ND 30ND1,1-Dichloroethene ug/kg ND 30ND1,2,3-Trichlorobenzene ug/kg ND 30ND1,2,4-Trichlorobenzene ug/kg ND 30ND1,2-Dibromo-3-chloropropane ug/kg ND 30ND1,2-Dibromoethane (EDB) ug/kg ND 30ND1,2-Dichlorobenzene ug/kg ND 30ND1,2-Dichloroethane ug/kg ND 30ND1,2-Dichloropropane ug/kg ND 30ND1,3-Dichlorobenzene ug/kg ND 30ND1,4-Dichlorobenzene ug/kg ND 30ND2-Butanone (MEK) ug/kg ND 30ND2-Hexanone ug/kg ND 30ND4-Methyl-2-pentanone (MIBK) ug/kg ND 30NDAcetone ug/kg 34.6J 30NDBenzene ug/kg ND 30NDBromochloromethane ug/kg ND 30NDBromodichloromethane ug/kg ND 30NDBromoform ug/kg ND 30NDBromomethane ug/kg ND 30NDCarbon disulfide ug/kg ND 30NDCarbon tetrachloride ug/kg ND 30NDChlorobenzene ug/kg ND 30NDChloroethane ug/kg ND 30NDChloroform ug/kg ND 30NDChloromethane ug/kg ND 30NDcis-1,2-Dichloroethene ug/kg 2.8J 30NDcis-1,3-Dichloropropene ug/kg ND 30NDCyclohexane ug/kg ND 30NDDibromochloromethane ug/kg ND 30ND



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsDup



Dichlorodifluoromethane ug/kg ND 30NDEthylbenzene ug/kg ND 30NDIsopropylbenzene (Cumene) ug/kg ND 30NDm&p-Xylene ug/kg ND 30NDMethyl acetate ug/kg ND 30NDMethyl-tert-butyl ether ug/kg ND 30NDMethylcyclohexane ug/kg ND 30NDMethylene Chloride ug/kg ND 30NDo-Xylene ug/kg ND 30NDStyrene ug/kg ND 30NDTetrachloroethene ug/kg ND 30NDToluene ug/kg ND 30NDtrans-1,2-Dichloroethene ug/kg ND 30NDtrans-1,3-Dichloropropene ug/kg ND 30NDTrichloroethene ug/kg 130 30NDTrichlorofluoromethane ug/kg ND 30NDVinyl chloride ug/kg ND 30NDXylene (Total) ug/kg ND 30ND1,2-Dichloroethane-d4 (S) % 105 19974-Bromofluorobenzene (S) % 96 4103Dibromofluoromethane (S) % 99 9101Toluene-d8 (S) % 98 1297

Parameter UnitsDup



1,1,1-Trichloroethane ug/kg ND 30ND1,1,2,2-Tetrachloroethane ug/kg ND 30ND1,1,2-Trichloroethane ug/kg ND 30ND1,1,2-Trichlorotrifluoroethane ug/kg ND 30ND1,1-Dichloroethane ug/kg ND 30ND1,1-Dichloroethene ug/kg ND 30ND1,2,3-Trichlorobenzene ug/kg ND 30ND1,2,4-Trichlorobenzene ug/kg ND 30ND1,2-Dibromo-3-chloropropane ug/kg ND 30ND1,2-Dibromoethane (EDB) ug/kg ND 30ND1,2-Dichlorobenzene ug/kg ND 30ND1,2-Dichloroethane ug/kg ND 30ND1,2-Dichloropropane ug/kg ND 30ND1,3-Dichlorobenzene ug/kg ND 30ND1,4-Dichlorobenzene ug/kg ND 30ND2-Butanone (MEK) ug/kg ND 30ND2-Hexanone ug/kg ND 30ND4-Methyl-2-pentanone (MIBK) ug/kg ND 30NDAcetone ug/kg ND 3059.5JBenzene ug/kg ND 30NDBromochloromethane ug/kg ND 30ND



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744

Parameter UnitsDup



Bromodichloromethane ug/kg ND 30NDBromoform ug/kg ND 30NDBromomethane ug/kg ND 30NDCarbon disulfide ug/kg ND 30NDCarbon tetrachloride ug/kg ND 30NDChlorobenzene ug/kg ND 30NDChloroethane ug/kg ND 30NDChloroform ug/kg ND 30NDChloromethane ug/kg ND 30NDcis-1,2-Dichloroethene ug/kg ND 301.8Jcis-1,3-Dichloropropene ug/kg ND 30NDCyclohexane ug/kg ND 30NDDibromochloromethane ug/kg ND 30NDDichlorodifluoromethane ug/kg ND 30NDEthylbenzene ug/kg ND 30NDIsopropylbenzene (Cumene) ug/kg ND 30NDm&p-Xylene ug/kg ND 30NDMethyl acetate ug/kg ND 30NDMethyl-tert-butyl ether ug/kg ND 30NDMethylcyclohexane ug/kg ND 30NDMethylene Chloride ug/kg ND 303.7Jo-Xylene ug/kg ND 30NDStyrene ug/kg ND 30NDTetrachloroethene ug/kg ND 30NDToluene ug/kg ND 30NDtrans-1,2-Dichloroethene ug/kg ND 30NDtrans-1,3-Dichloropropene ug/kg ND 30NDTrichloroethene ug/kg ND 3085.0Trichlorofluoromethane ug/kg ND 30NDVinyl chloride ug/kg ND 30NDXylene (Total) ug/kg ND 30ND1,2-Dichloroethane-d4 (S) % 111 9944-Bromofluorobenzene (S) % 97 14104Dibromofluoromethane (S) % 103 499Toluene-d8 (S) % 99 496



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



PMST/3398ASTM D2974-87

ASTM D2974-87Dry Weight/Percent Moisture


Parameter UnitsDup



Percent Moisture % 16.1 10 2514.6

Parameter UnitsDup






Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



WETA/8109SM 4500-CN-E

SM 4500-CN-E4500CNE Cyanide, Total






Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/05/10 13:23

Parameter UnitsLCS



Cyanide mg/kg 3.23 106 80-120

Parameter UnitsMS



Result9276750006

Cyanide mg/kg 3.02.9 102 75-125ND

Parameter UnitsDup



Cyanide mg/kg ND 20ND



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



WETA/8088EPA 7196

EPA 71967196 Chromium, Hexavalent

Associated Lab Samples: 9276764001





Matrix: Solid

Analyzed

Chromium, Hexavalent mg/kg ND 5.0 09/03/10 11:37

Parameter UnitsLCS



Chromium, Hexavalent mg/kg 52.250 104 90-110

Parameter UnitsMS



Result9276750013

Chromium, Hexavalent mg/kg 27.1 M139.8 64 75-125ND

Parameter UnitsMS



Result9276750028

Chromium, Hexavalent mg/kg 49.349.7 98 75-125ND

Parameter UnitsDup



Chromium, Hexavalent mg/kg ND 20ND

Parameter UnitsDup






Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276764MILLS GAP 6686081744



WETA/8098EPA 7196


Associated Lab Samples: 9276764002, 9276764003, 9276764004, 9276764005





Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



Result9276833001

Chromium, Hexavalent mg/kg ND M147.7 0 75-125ND

Parameter UnitsMS



Result9276872013


Parameter UnitsDup




Parameter UnitsDup






Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

QUALIFIERS


9276764MILLS GAP 6686081744

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.U - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.

ANALYTE QUALIFIERS

Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.

L2

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1RPD value was outside control limits.R1



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

QUALITY CONTROL DATA CROSS REFERENCE TABLE


9276764MILLS GAP 6686081744

Lab ID Sample ID QC Batch Method QC Batch Analytical MethodAnalyticalBatch

9276764001 MPRP/7030 ICP/6479SS-117 EPA 3050 EPA 60109276764002 MPRP/7030 ICP/6479SS-118 EPA 3050 EPA 60109276764003 MPRP/7030 ICP/6479SS-119 EPA 3050 EPA 60109276764004 MPRP/7030 ICP/6479SS-120 EPA 3050 EPA 60109276764005 MPRP/7030 ICP/6479SS-121 EPA 3050 EPA 6010

9276764001 MERP/2996 MERC/2955SS-117 EPA 7471 EPA 74719276764002 MERP/2996 MERC/2955SS-118 EPA 7471 EPA 74719276764003 MERP/2996 MERC/2955SS-119 EPA 7471 EPA 74719276764004 MERP/2996 MERC/2955SS-120 EPA 7471 EPA 74719276764005 MERP/2996 MERC/2955SS-121 EPA 7471 EPA 7471

9276764001 OEXT/11146 MSSV/4003SS-117 EPA 3546 EPA 82709276764002 OEXT/11146 MSSV/4003SS-118 EPA 3546 EPA 82709276764003 OEXT/11146 MSSV/4003SS-119 EPA 3546 EPA 82709276764004 OEXT/11146 MSSV/4003SS-120 EPA 3546 EPA 82709276764005 OEXT/11146 MSSV/4003SS-121 EPA 3546 EPA 8270

9276764001 MSV/12131SS-117 EPA 82609276764002 MSV/12131SS-118 EPA 82609276764003 MSV/12131SS-119 EPA 82609276764004 MSV/12131SS-120 EPA 82609276764005 MSV/12131SS-121 EPA 8260

9276764001 PMST/3398SS-117 ASTM D2974-879276764002 PMST/3398SS-118 ASTM D2974-879276764003 PMST/3398SS-119 ASTM D2974-879276764004 PMST/3398SS-120 ASTM D2974-879276764005 PMST/3398SS-121 ASTM D2974-87

9276764001 WETA/8109SS-117 SM 4500-CN-E9276764002 WETA/8109SS-118 SM 4500-CN-E9276764003 WETA/8109SS-119 SM 4500-CN-E9276764004 WETA/8109SS-120 SM 4500-CN-E9276764005 WETA/8109SS-121 SM 4500-CN-E

9276764001 WETA/8088 WETA/8102SS-117 EPA 7196 EPA 7196

9276764002 WETA/8098 WETA/8104SS-118 EPA 7196 EPA 71969276764003 WETA/8098 WETA/8104SS-119 EPA 7196 EPA 71969276764004 WETA/8098 WETA/8104SS-120 EPA 7196 EPA 71969276764005 WETA/8098 WETA/8104SS-121 EPA 7196 EPA 7196



Date: 09/20/2010 01:52 PM of 54



(704)875-9092


Asheville, NC 28804

(828)254-7176

September 27, 2010

LIMS USE: FR - SUSAN KELLYLIMS OBJECT ID: 9276872

9276872Project:Pace Project No.:

RE:

Ms. Susan KellyMactec Asheville1308 Patton AvenueAsheville, NC 28806

MILLS GAP 6686081744

Dear Ms. Kelly:Enclosed are the analytical results for sample(s) received by the laboratory between September 02,2010 and September 03, 2010. The results relate only to the samples included in this report.Results reported herein conform to the most current NELAC standards, where applicable, unlessotherwise narrated in the body of the report.

Inorganic Wet Chemistry and Metals analyses were performed at our Pace Asheville laboratory andOrganic testing was performed at our Pace Huntersville laboratory unless otherwise footnoted. AllMicrobiological analyses were performed at the laboratory where the samples were received.

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Kevin Godwin

[email protected] Manager

Enclosures



Page 1 of 383



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(828)254-7176

CERTIFICATIONS


9276872MILLS GAP 6686081744

Charlotte Certification IDs9800 Kincey Ave. Ste 100, Huntersville, NC 28078Louisiana/LELAP Certification #: 04034New Jersey Certification #: NC012North Carolina Drinking Water Certification #: 37706North Carolina Field Services Certification #: 5342North Carolina Wastewater Certification #: 12Pennsylvania Certification #: 68-00784

South Carolina Certification #: 99006001South Carolina Drinking Water Cert. #: 99006003Virginia Certification #: 00213Connecticut Certification #: PH-0104Florida/NELAP Certification #: E87627Kentucky UST Certification #: 84Louisiana DHH Drinking Water # LA 100031

Asheville Certification IDs2225 Riverside Dr., Asheville, NC 28804Connecticut Certification #: PH-0106Florida/NELAP Certification #: E87648Massachusetts Certification #: M-NC030New Jersey Certification #: NC011North Carolina Bioassay Certification #: 9

North Carolina Drinking Water Certification #: 37712North Carolina Wastewater Certification #: 40Pennsylvania Certification #: 68-03578South Carolina Bioassay Certification #: 99030002South Carolina Certification #: 99030001Virginia Certification #: 00072



Page 2 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

SAMPLE SUMMARY


9276872MILLS GAP 6686081744


9276872001 SS-110A Solid 09/01/10 16:10 09/02/10 16:22

9276872002 SS-110B Solid 09/01/10 16:15 09/02/10 16:22

9276872003 SS-110C Solid 09/01/10 16:20 09/02/10 16:22

9276872004 SS-110D Solid 09/01/10 16:25 09/02/10 16:22

9276872005 SS-110E Solid 09/01/10 16:30 09/02/10 16:22

9276872006 SS-111A Solid 09/01/10 17:30 09/02/10 16:22

9276872007 SS-111B Solid 09/01/10 17:35 09/02/10 16:22

9276872008 SS-111B Solid 09/01/10 17:35 09/02/10 16:22

9276872009 SS-111C Solid 09/01/10 17:45 09/02/10 16:22

9276872010 SS-111C Solid 09/01/10 17:45 09/02/10 16:22

9276872011 SS-111E Solid 09/01/10 18:00 09/02/10 16:22

9276872012 SS-111E Solid 09/01/10 18:00 09/02/10 16:22

9276872013 SS-111D Solid 09/01/10 17:50 09/02/10 16:22

9276872014 SS-111D Solid 09/01/10 17:50 09/02/10 16:22

9276872015 SS-106A Solid 09/01/10 14:05 09/02/10 16:22

9276872016 SS-106B Solid 09/01/10 14:15 09/02/10 16:22

9276872017 SS-106C Solid 09/01/10 14:25 09/02/10 16:22

9276872018 SS-106D Solid 09/01/10 14:35 09/02/10 16:22

9276872019 SS-106E Solid 09/01/10 14:45 09/02/10 16:22

9276872020 SS-105A Solid 09/01/10 15:35 09/02/10 16:22

9276872021 SS-105B Solid 09/01/10 15:45 09/02/10 16:22

9276872022 SS-105C Solid 09/01/10 15:55 09/02/10 16:22

9276872023 SS-105D Solid 09/01/10 16:00 09/02/10 16:22

9276872024 SS-105E Solid 09/01/10 16:05 09/02/10 16:22

9276872025 SS-107A Solid 09/02/10 08:20 09/02/10 16:22

9276872026 SS-107A Solid 09/02/10 08:20 09/02/10 16:22

9276872027 SS-107B Solid 09/02/10 08:30 09/02/10 16:22

9276872028 SS-107B Solid 09/02/10 08:30 09/02/10 16:22

9276872029 SS-107C Solid 09/02/10 08:40 09/02/10 16:22

9276872030 SS-107C Solid 09/02/10 08:40 09/02/10 16:22

9276872031 SS-107D Solid 09/02/10 08:50 09/02/10 16:22

9276872032 SS-107D Solid 09/02/10 08:50 09/02/10 16:22

9276872033 SS-107E Solid 09/02/10 09:00 09/02/10 16:22

9276872034 SS-107E Solid 09/02/10 09:00 09/02/10 16:22

9276872035 SS-112A Solid 09/02/10 09:30 09/02/10 16:22

9276872036 SS-112B Solid 09/02/10 09:40 09/02/10 16:22

9276872037 SS-112C Solid 09/02/10 09:45 09/02/10 16:22



Page 3 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

SAMPLE SUMMARY


9276872MILLS GAP 6686081744


9276872038 SS-112D Solid 09/02/10 09:55 09/02/10 16:22

9276872039 SS-112E Solid 09/02/10 10:00 09/02/10 16:22

9276872040 SS-108A Solid 09/02/10 10:35 09/02/10 16:22

9276872041 SS-108A Solid 09/02/10 10:35 09/02/10 16:22

9276872042 SS-108B Solid 09/02/10 10:45 09/02/10 16:22

9276872043 SS-108B Solid 09/02/10 10:45 09/02/10 16:22

9276872044 SS-108C Solid 09/02/10 10:50 09/02/10 16:22

9276872045 SS-108C Solid 09/02/10 10:50 09/02/10 16:22

9276872046 SS-108D Solid 09/02/10 10:55 09/02/10 16:22

9276872047 SS-108D Solid 09/02/10 10:55 09/02/10 16:22

9276872048 SS-108E Solid 09/02/10 11:00 09/02/10 16:22

9276872049 SS-108E Solid 09/02/10 11:00 09/02/10 16:22

9276872050 SS-114A Solid 09/02/10 12:00 09/02/10 16:22

9276872051 SS-114B Solid 09/02/10 13:45 09/02/10 16:22

9276872052 SS-131 Solid 09/02/10 14:35 09/02/10 16:22

9276872053 SS-132 Solid 09/02/10 14:45 09/02/10 16:22

9276872054 FD-16 Solid 09/01/10 00:00 09/02/10 16:22

9276872055 FD-17 Solid 09/01/10 00:00 09/02/10 16:22

9276872056 FD-18 Solid 09/01/10 00:00 09/02/10 16:22

9276872057 FD-19 Solid 09/01/10 00:00 09/02/10 16:22

9276872058 FD-21 Solid 09/01/10 00:00 09/02/10 16:22

9276872059 FD-22 Solid 09/01/10 00:00 09/02/10 16:22

9276872060 FD-24 Solid 09/01/10 00:00 09/02/10 16:22

9276872061 FD-25 Solid 09/01/10 00:00 09/02/10 16:22

9276872062 FD-26 Solid 09/01/10 00:00 09/02/10 16:22

9276872063 FD-27 Solid 09/01/10 00:00 09/02/10 16:22

9276872064 FD-28 Solid 09/01/10 00:00 09/02/10 16:22

9276872065 FD-29 Solid 09/01/10 00:00 09/02/10 16:22

9276872066 FD-30 Solid 09/01/10 00:00 09/02/10 16:22

9276872067 FD-31 Solid 09/01/10 00:00 09/02/10 16:22

9276872068 FD-32 Solid 09/01/10 00:00 09/02/10 16:22

9276872069 FD-33 Solid 09/01/10 00:00 09/02/10 16:22

9276872070 TB-06 Solid 09/01/10 00:00 09/02/10 16:22

9276872071 SS-110A Solid 09/01/10 16:10 09/03/10 08:00

9276872072 SS-110B Solid 09/01/10 16:15 09/03/10 08:00

9276872073 SS-110C Solid 09/01/10 16:20 09/03/10 08:00

9276872074 SS-110D Solid 09/01/10 16:25 09/03/10 08:00



Page 4 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

SAMPLE SUMMARY


9276872MILLS GAP 6686081744


9276872075 SS-110E Solid 09/01/10 16:30 09/03/10 08:00

9276872076 SS-111A Solid 09/01/10 17:30 09/03/10 08:00

9276872077 SS-111B Solid 09/01/10 17:35 09/03/10 08:00

9276872078 SS-111C Solid 09/01/10 17:45 09/03/10 08:00

9276872079 SS-111E Solid 09/01/10 18:00 09/03/10 08:00

9276872080 SS-111D Solid 09/01/10 17:50 09/03/10 08:00

9276872081 SS-106A Solid 09/01/10 14:05 09/03/10 08:00

9276872082 SS-106B Solid 09/01/10 14:15 09/03/10 08:00

9276872083 SS-106C Solid 09/01/10 14:25 09/03/10 08:00

9276872084 SS-106D Solid 09/01/10 14:35 09/03/10 08:00

9276872085 SS-106E Solid 09/01/10 14:45 09/03/10 08:00

9276872086 SS-105A Solid 09/01/10 15:35 09/03/10 08:00

9276872087 SS-105B Solid 09/01/10 15:45 09/03/10 08:00

9276872088 SS-105C Solid 09/01/10 15:55 09/03/10 08:00

9276872089 SS-105D Solid 09/01/10 16:00 09/03/10 08:00

9276872090 SS-105E Solid 09/01/10 16:05 09/03/10 08:00

9276872091 FD-20 Solid 09/01/10 00:00 09/03/10 08:00

9276872092 FD-23 Solid 09/01/10 00:00 09/03/10 08:00

9276872093 EB-02 Water 09/01/10 17:15 09/03/10 08:00

9276872094 TB-04 Solid 09/01/10 00:00 09/03/10 08:00

9276872095 TB-05 Water 09/01/10 00:00 09/03/10 08:00



Page 5 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872001 SS-110A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872002 SS-110B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872003 SS-110C EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872004 SS-110D EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872005 SS-110E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1KDF

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872006 SS-111A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872007 SS-111B EPA 8270 73BPJ



Page 6 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


ASTM D2974-87 1TNM

9276872008 SS-111B EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872009 SS-111C EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

9276872010 SS-111C EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872011 SS-111E ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872012 SS-111E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

EPA 7196 1EWS

9276872013 SS-111D ASTM D2974-87 1TNM

EPA 7196 1EWS

9276872014 SS-111D EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872015 SS-106A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872016 SS-106B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM



Page 7 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872017 SS-106C EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872018 SS-106D EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872019 SS-106E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872020 SS-105A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872021 SS-105B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872022 SS-105C EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA



Page 8 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


EPA 7196 1EWS

9276872023 SS-105D EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872024 SS-105E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872025 SS-107A EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

9276872026 SS-107A EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872027 SS-107B ASTM D2974-87 1TNM

EPA 7196 1EWS

9276872028 SS-107B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872029 SS-107C EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872030 SS-107C EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS



Page 9 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872031 SS-107D ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872032 SS-107D EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

EPA 7196 1EWS

9276872033 SS-107E EPA 8270 73BPJ

ASTM D2974-87 1TNM

9276872034 SS-107E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872035 SS-112A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872036 SS-112B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872037 SS-112C EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS



Page 10 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872038 SS-112D EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872039 SS-112E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1EWS

9276872040 SS-108A EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872041 SS-108A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1DMN

9276872042 SS-108B ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872043 SS-108B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872044 SS-108C ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872045 SS-108C EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73BPJ

EPA 8260 56DLK

ASTM D2974-87 1TNM



Page 11 of 383



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(828)254-7176



9276872MILLS GAP 6686081744


SM 4500-CN-E 1JDA

9276872046 SS-108D EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

9276872047 SS-108D EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1DMN

9276872048 SS-108E EPA 8270 73BPJ

ASTM D2974-87 1TNM

9276872049 SS-108E EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1DMN

9276872050 SS-114A EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1DMN

9276872051 SS-114B EPA 6010 13JMW

EPA 7471 1SAJ

EPA 8270 73RRH

EPA 8260 56DLK

ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

EPA 7196 1DMN

9276872052 SS-131 EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872053 SS-132 EPA 6010 13JMW

EPA 7471 1SAJ



Page 12 of 383



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9276872MILLS GAP 6686081744


ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872054 FD-16 EPA 8270 73RRH

ASTM D2974-87 1TNM

9276872055 FD-17 EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

9276872056 FD-18 ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872057 FD-19 ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872058 FD-21 EPA 8270 73RRH

ASTM D2974-87 1TNM

9276872059 FD-22 EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

9276872060 FD-24 ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872061 FD-25 ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872062 FD-26 EPA 8270 73BPJ

ASTM D2974-87 1TNM

9276872063 FD-27 EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872064 FD-28 EPA 6010 13JMW

EPA 7471 1SAJ

ASTM D2974-87 1TNM

9276872065 FD-29 ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872066 FD-30 ASTM D2974-87 1TNM

SM 4500-CN-E 1JDA

9276872067 FD-31 EPA 8270 73RRH

ASTM D2974-87 1TNM

9276872068 FD-32 ASTM D2974-87 1TNM

EPA 7196 1DMN

9276872069 FD-33 EPA 6010 13JMW

EPA 7471 1SAJ



Page 13 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


ASTM D2974-87 1TNM

9276872070 TB-06 EPA 8260 56DLK

9276872071 SS-110A EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872072 SS-110B EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872073 SS-110C EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872074 SS-110D EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872075 SS-110E EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872076 SS-111A EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872077 SS-111B EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872078 SS-111C EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872079 SS-111E EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872080 SS-111D EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872081 SS-106A EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872082 SS-106B EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872083 SS-106C EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872084 SS-106D EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872085 SS-106E EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872086 SS-105A EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872087 SS-105B EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872088 SS-105C EPA 8260 56DLK



Page 14 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


ASTM D2974-87 1TNM

9276872089 SS-105D EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872090 SS-105E EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872091 FD-20 EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872092 FD-23 EPA 8260 56DLK

ASTM D2974-87 1TNM

9276872093 EB-02 EPA 6010 13JMW

EPA 7470 1SAJ

EPA 8270 73RRH

EPA 8260 56MCK

SM 4500-CN-E 1JDA

9276872094 TB-04 EPA 8260 56DLK

9276872095 TB-05 EPA 8260 56MCK



Page 15 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872001 SS-110ABeryllium 0.81 mg/kg 09/22/10 18:360.59EPA 6010Chromium 23.0 mg/kg 09/22/10 18:362.9EPA 6010Copper 4.2 mg/kg 09/22/10 18:362.9EPA 6010Lead 8.0 mg/kg 09/22/10 18:362.9EPA 6010Manganese 228 mg/kg 09/22/10 18:362.9EPA 6010Nickel 10.6 mg/kg 09/22/10 18:362.9EPA 6010Zinc 49.1 mg/kg 09/22/10 18:365.9EPA 6010Mercury 0.041 mg/kg 09/10/10 12:31 M10.0052EPA 7471Percent Moisture 19.4 % 09/07/10 09:120.10ASTM D2974-87

9276872002 SS-110BBeryllium 1.3 mg/kg 09/22/10 18:391.1EPA 6010Chromium 18.4 mg/kg 09/22/10 18:395.4EPA 6010Copper 0.51J mg/kg 09/22/10 18:39 D35.4EPA 6010Manganese 221 mg/kg 09/22/10 18:395.4EPA 6010Nickel 14.6 mg/kg 09/22/10 18:395.4EPA 6010Zinc 84.1 mg/kg 09/22/10 18:3910.8EPA 6010Mercury 0.0031J mg/kg 09/10/10 12:390.0045EPA 7471Percent Moisture 16.1 % 09/07/10 09:130.10ASTM D2974-87

9276872003 SS-110CBeryllium 1.6 mg/kg 09/22/10 18:431.1EPA 6010Chromium 23.1 mg/kg 09/22/10 18:435.3EPA 6010Copper 10.9 mg/kg 09/22/10 18:435.3EPA 6010Lead 6.3 mg/kg 09/22/10 18:435.3EPA 6010Manganese 599 mg/kg 09/22/10 18:435.3EPA 6010Nickel 13.8 mg/kg 09/22/10 18:435.3EPA 6010Zinc 90.0 mg/kg 09/22/10 18:4310.7EPA 6010Mercury 0.00047J mg/kg 09/10/10 12:420.0042EPA 7471Percent Moisture 16.3 % 09/07/10 09:130.10ASTM D2974-87

9276872004 SS-110DBeryllium 1.5 mg/kg 09/22/10 18:461.4EPA 6010Chromium 24.7 mg/kg 09/22/10 18:466.9EPA 6010Copper 5.8J mg/kg 09/22/10 18:46 D36.9EPA 6010Manganese 380 mg/kg 09/22/10 18:466.9EPA 6010Nickel 11.1 mg/kg 09/22/10 18:466.9EPA 6010Zinc 67.5 mg/kg 09/22/10 18:4613.9EPA 6010Mercury 0.00037J mg/kg 09/10/10 12:450.0044EPA 7471Percent Moisture 12.2 % 09/07/10 09:140.10ASTM D2974-87

9276872005 SS-110EBeryllium 1.4 mg/kg 09/22/10 18:501.1EPA 6010Chromium 22.6 mg/kg 09/22/10 18:505.3EPA 6010Copper 0.68J mg/kg 09/22/10 18:50 D35.3EPA 6010Manganese 304 mg/kg 09/22/10 18:505.3EPA 6010Nickel 11.3 mg/kg 09/22/10 18:505.3EPA 6010Zinc 53.7 mg/kg 09/22/10 18:5010.6EPA 6010Mercury 0.0021J mg/kg 09/13/10 13:22 B0.0037EPA 7471



Page 16 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872005 SS-110EPercent Moisture 10.9 % 09/07/10 09:140.10ASTM D2974-87

9276872006 SS-111ABeryllium 0.58 mg/kg 09/22/10 18:530.21EPA 6010Cadmium 0.26 mg/kg 09/22/10 18:530.21EPA 6010Chromium 19.9 mg/kg 09/22/10 18:531.1EPA 6010Copper 5.3 mg/kg 09/22/10 18:531.1EPA 6010Lead 11.8 mg/kg 09/22/10 18:531.1EPA 6010Manganese 134 mg/kg 09/22/10 18:531.1EPA 6010Nickel 6.1 mg/kg 09/22/10 18:531.1EPA 6010Zinc 25.1 mg/kg 09/22/10 18:532.1EPA 6010Mercury 0.069 mg/kg 09/13/10 14:04 B0.0030EPA 7471Percent Moisture 23.4 % 09/09/10 08:310.10ASTM D2974-87

9276872007 SS-111BPercent Moisture 13.1 % 09/09/10 08:320.10ASTM D2974-87

9276872008 SS-111BArsenic 1.5J mg/kg 09/22/10 18:57 D32.3EPA 6010Beryllium 0.89 mg/kg 09/22/10 18:570.46EPA 6010Chromium 15.3 mg/kg 09/22/10 18:572.3EPA 6010Copper 2.5 mg/kg 09/22/10 18:572.3EPA 6010Lead 9.1 mg/kg 09/22/10 18:572.3EPA 6010Manganese 586 mg/kg 09/22/10 18:572.3EPA 6010Nickel 11.7 mg/kg 09/22/10 18:572.3EPA 6010Zinc 77.0 mg/kg 09/22/10 18:574.6EPA 6010Mercury 0.0031J mg/kg 09/15/10 11:590.0052EPA 7471Percent Moisture 12.1 % 09/09/10 08:320.10ASTM D2974-87

9276872009 SS-111CArsenic 1.8J mg/kg 09/22/10 19:10 D32.2EPA 6010Beryllium 0.86 mg/kg 09/22/10 19:100.44EPA 6010Chromium 16.8 mg/kg 09/22/10 19:102.2EPA 6010Copper 2.5 mg/kg 09/22/10 19:102.2EPA 6010Lead 6.4 mg/kg 09/22/10 19:102.2EPA 6010Manganese 269 mg/kg 09/22/10 19:102.2EPA 6010Nickel 12.2 mg/kg 09/22/10 19:102.2EPA 6010Zinc 78.9 mg/kg 09/22/10 19:104.4EPA 6010Mercury 0.0011J mg/kg 09/15/10 12:010.0046EPA 7471Percent Moisture 10.3 % 09/09/10 08:330.10ASTM D2974-87

9276872010 SS-111CPercent Moisture 10.4 % 09/09/10 08:330.10ASTM D2974-87


9276872012 SS-111EArsenic 4.0 mg/kg 09/22/10 19:204.0EPA 6010Beryllium 1.2 mg/kg 09/22/10 19:200.81EPA 6010



Page 17 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872012 SS-111EChromium 16.4 mg/kg 09/22/10 19:204.0EPA 6010Copper 13.5 mg/kg 09/22/10 19:204.0EPA 6010Manganese 304 mg/kg 09/22/10 19:204.0EPA 6010Nickel 12.3 mg/kg 09/22/10 19:204.0EPA 6010Thallium 2.4J mg/kg 09/22/10 19:20 D38.1EPA 6010Zinc 88.8 mg/kg 09/22/10 19:208.1EPA 6010Mercury 0.00066J mg/kg 09/15/10 12:090.0041EPA 7471Percent Moisture 11.6 % 09/09/10 08:340.10ASTM D2974-87

9276872013 SS-111DPercent Moisture 11.1 % 09/09/10 08:340.10ASTM D2974-87

9276872014 SS-111DArsenic 4.4J mg/kg 09/22/10 19:23 D35.2EPA 6010Beryllium 1.2 mg/kg 09/22/10 19:231.0EPA 6010Chromium 13.6 mg/kg 09/22/10 19:235.2EPA 6010Copper 5.9 mg/kg 09/22/10 19:235.2EPA 6010Lead 7.3 mg/kg 09/22/10 19:235.2EPA 6010Manganese 552 mg/kg 09/22/10 19:235.2EPA 6010Nickel 8.5 mg/kg 09/22/10 19:235.2EPA 6010Zinc 56.7 mg/kg 09/22/10 19:2310.3EPA 6010Percent Moisture 11.7 % 09/09/10 08:350.10ASTM D2974-87

9276872015 SS-106AArsenic 1.4J mg/kg 09/22/10 19:27 D31.9EPA 6010Beryllium 0.95 mg/kg 09/22/10 19:270.38EPA 6010Chromium 16.7 mg/kg 09/22/10 19:271.9EPA 6010Copper 12.4 mg/kg 09/22/10 19:271.9EPA 6010Lead 7.8 mg/kg 09/22/10 19:271.9EPA 6010Manganese 306 mg/kg 09/22/10 19:271.9EPA 6010Nickel 9.1 mg/kg 09/22/10 19:271.9EPA 6010Silver 0.14J mg/kg 09/22/10 19:27 D31.9EPA 6010Zinc 47.8 mg/kg 09/22/10 19:273.8EPA 6010Mercury 0.022 mg/kg 09/15/10 12:180.0046EPA 7471Percent Moisture 9.3 % 09/09/10 08:350.10ASTM D2974-87

9276872016 SS-106BBeryllium 1.4 mg/kg 09/22/10 19:300.76EPA 6010Chromium 20.2 mg/kg 09/22/10 19:303.8EPA 6010Copper 8.5 mg/kg 09/22/10 19:303.8EPA 6010Lead 5.3 mg/kg 09/22/10 19:303.8EPA 6010Manganese 546 mg/kg 09/22/10 19:303.8EPA 6010Nickel 10.9 mg/kg 09/22/10 19:303.8EPA 6010Thallium 2.4J mg/kg 09/22/10 19:30 D37.6EPA 6010Zinc 85.8 mg/kg 09/22/10 19:307.6EPA 6010Mercury 0.0074 mg/kg 09/15/10 12:260.0054EPA 7471Percent Moisture 7.3 % 09/09/10 08:360.10ASTM D2974-87



Page 18 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872017 SS-106CBeryllium 1.4 mg/kg 09/22/10 19:340.90EPA 6010Chromium 16.3 mg/kg 09/22/10 19:344.5EPA 6010Copper 3.5J mg/kg 09/22/10 19:34 D34.5EPA 6010Lead 5.2 mg/kg 09/22/10 19:344.5EPA 6010Manganese 354 mg/kg 09/22/10 19:344.5EPA 6010Nickel 9.8 mg/kg 09/22/10 19:344.5EPA 6010Zinc 75.4 mg/kg 09/22/10 19:349.0EPA 6010Mercury 0.00073J mg/kg 09/15/10 12:280.0046EPA 7471Percent Moisture 9.3 % 09/09/10 08:360.10ASTM D2974-87

9276872018 SS-106DBeryllium 1.2 mg/kg 09/22/10 19:370.82EPA 6010Chromium 17.3 mg/kg 09/22/10 19:374.1EPA 6010Copper 10.7 mg/kg 09/22/10 19:374.1EPA 6010Lead 5.1 mg/kg 09/22/10 19:374.1EPA 6010Manganese 813 mg/kg 09/22/10 19:374.1EPA 6010Nickel 9.1 mg/kg 09/22/10 19:374.1EPA 6010Zinc 46.0 mg/kg 09/22/10 19:378.2EPA 6010Percent Moisture 12.0 % 09/09/10 08:360.10ASTM D2974-87

9276872019 SS-106EBeryllium 1.5 mg/kg 09/22/10 19:400.98EPA 6010Chromium 14.3 mg/kg 09/22/10 19:404.9EPA 6010Copper 4.2J mg/kg 09/22/10 19:40 D34.9EPA 6010Manganese 426 mg/kg 09/22/10 19:404.9EPA 6010Nickel 9.5 mg/kg 09/22/10 19:404.9EPA 6010Zinc 66.4 mg/kg 09/22/10 19:409.8EPA 6010Mercury 0.00014J mg/kg 09/15/10 12:340.0037EPA 7471Percent Moisture 11.9 % 09/09/10 08:360.10ASTM D2974-87

9276872020 SS-105AArsenic 1.9J mg/kg 09/22/10 19:54 D32.2EPA 6010Beryllium 0.86 mg/kg 09/22/10 19:540.43EPA 6010Cadmium 0.43 mg/kg 09/22/10 19:540.43EPA 6010Chromium 14.7 mg/kg 09/22/10 19:542.2EPA 6010Copper 9.4 mg/kg 09/22/10 19:542.2EPA 6010Lead 10.9 mg/kg 09/22/10 19:542.2EPA 6010Manganese 370 mg/kg 09/22/10 19:542.2EPA 6010Nickel 8.6 mg/kg 09/22/10 19:542.2EPA 6010Zinc 47.4 mg/kg 09/22/10 19:544.3EPA 6010Mercury 0.024 mg/kg 09/15/10 12:360.0043EPA 7471Percent Moisture 12.9 % 09/09/10 08:370.10ASTM D2974-87

9276872021 SS-105BBeryllium 1.1 mg/kg 09/22/10 19:570.40EPA 6010Chromium 14.8 mg/kg 09/22/10 19:572.0EPA 6010Copper 3.3 mg/kg 09/22/10 19:572.0EPA 6010Lead 3.3 mg/kg 09/22/10 19:572.0EPA 6010Manganese 266 mg/kg 09/22/10 19:572.0EPA 6010



Page 19 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872021 SS-105BNickel 12.1 mg/kg 09/22/10 19:572.0EPA 6010Zinc 52.7 mg/kg 09/22/10 19:574.0EPA 6010Mercury 0.010 mg/kg 09/15/10 12:390.0041EPA 7471Percent Moisture 9.3 % 09/09/10 08:370.10ASTM D2974-87

9276872022 SS-105CArsenic 6.1 mg/kg 09/22/10 20:005.5EPA 6010Beryllium 2.5 mg/kg 09/22/10 20:001.1EPA 6010Chromium 30.1 mg/kg 09/22/10 20:005.5EPA 6010Copper 8.9 mg/kg 09/22/10 20:005.5EPA 6010Lead 15.9 mg/kg 09/22/10 20:005.5EPA 6010Manganese 3130 mg/kg 09/22/10 20:005.5EPA 6010Nickel 24.6 mg/kg 09/22/10 20:005.5EPA 6010Zinc 128 mg/kg 09/22/10 20:0011.0EPA 6010Mercury 0.0016J mg/kg 09/15/10 12:420.0046EPA 7471Percent Moisture 15.8 % 09/09/10 08:370.10ASTM D2974-87

9276872023 SS-105DBeryllium 1.4 mg/kg 09/22/10 20:040.88EPA 6010Chromium 12.8 mg/kg 09/22/10 20:044.4EPA 6010Copper 7.1 mg/kg 09/22/10 20:044.4EPA 6010Manganese 2030 mg/kg 09/22/10 20:044.4EPA 6010Nickel 8.7 mg/kg 09/22/10 20:044.4EPA 6010Thallium 2.4J mg/kg 09/22/10 20:04 D38.8EPA 6010Zinc 45.5 mg/kg 09/22/10 20:048.8EPA 6010Percent Moisture 13.4 % 09/09/10 18:250.10ASTM D2974-87

9276872024 SS-105EBeryllium 1.5J mg/kg 09/23/10 12:18 D31.8EPA 6010Chromium 14.3 mg/kg 09/23/10 12:188.8EPA 6010Manganese 194 mg/kg 09/23/10 12:188.8EPA 6010Nickel 6.8J mg/kg 09/23/10 12:18 D38.8EPA 6010Zinc 45.9 mg/kg 09/23/10 12:1817.6EPA 6010Percent Moisture 14.1 % 09/09/10 18:250.10ASTM D2974-87

9276872025 SS-107ABeryllium 0.91 mg/kg 09/22/10 16:500.43EPA 6010Chromium 18.1 mg/kg 09/22/10 16:502.2EPA 6010Copper 10.5 mg/kg 09/22/10 16:502.2EPA 6010Lead 10.9 mg/kg 09/22/10 16:502.2EPA 6010Manganese 290 mg/kg 09/22/10 16:502.2EPA 6010Nickel 8.7 mg/kg 09/22/10 16:502.2EPA 6010Silver 1.3J mg/kg 09/22/10 16:50 D32.2EPA 6010Zinc 40.8 mg/kg 09/22/10 16:504.3EPA 6010Mercury 0.019 mg/kg 09/15/10 12:50 M10.0054EPA 7471Percent Moisture 13.4 % 09/09/10 09:050.10ASTM D2974-87

9276872026 SS-107AAcetone 90.7J ug/kg 09/09/10 04:5497.9EPA 8260



Page 20 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872026 SS-107A2-Butanone (MEK) 2.9J ug/kg 09/09/10 04:5497.9EPA 8260Trichloroethene 28.0 ug/kg 09/09/10 04:544.9EPA 8260Percent Moisture 5.4 % 09/09/10 09:050.10ASTM D2974-87


9276872028 SS-107BArsenic 1.4J mg/kg 09/22/10 17:06 D32.2EPA 6010Beryllium 1.2 mg/kg 09/22/10 17:060.44EPA 6010Chromium 13.3 mg/kg 09/22/10 17:062.2EPA 6010Copper 2.7 mg/kg 09/22/10 17:062.2EPA 6010Lead 11.3 mg/kg 09/22/10 17:062.2EPA 6010Manganese 2510 mg/kg 09/22/10 17:062.2EPA 6010Nickel 10.4 mg/kg 09/22/10 17:062.2EPA 6010Thallium 2.1J mg/kg 09/22/10 17:06 D34.4EPA 6010Zinc 59.2 mg/kg 09/22/10 17:064.4EPA 6010Mercury 0.010 mg/kg 09/15/10 13:030.0042EPA 7471Percent Moisture 2.5 % 09/09/10 09:060.10ASTM D2974-87


9276872030 SS-107CArsenic 3.7J mg/kg 09/22/10 17:18 D34.3EPA 6010Beryllium 1.3 mg/kg 09/22/10 17:180.86EPA 6010Chromium 21.0 mg/kg 09/22/10 17:184.3EPA 6010Copper 8.5 mg/kg 09/22/10 17:184.3EPA 6010Lead 5.4 mg/kg 09/22/10 17:184.3EPA 6010Manganese 284 mg/kg 09/22/10 17:184.3EPA 6010Nickel 20.6 mg/kg 09/22/10 17:184.3EPA 6010Zinc 81.7 mg/kg 09/22/10 17:188.6EPA 6010Mercury 0.00018J mg/kg 09/15/10 13:050.0057EPA 7471Percent Moisture 12.8 % 09/09/10 09:060.10ASTM D2974-87


9276872032 SS-107DBeryllium 1.8 mg/kg 09/22/10 17:211.1EPA 6010Chromium 19.5 mg/kg 09/22/10 17:215.4EPA 6010Copper 7.3 mg/kg 09/22/10 17:215.4EPA 6010Manganese 257 mg/kg 09/22/10 17:215.4EPA 6010Nickel 11.8 mg/kg 09/22/10 17:215.4EPA 6010Zinc 77.1 mg/kg 09/22/10 17:2110.9EPA 6010Acetone 18.1J ug/kg 09/09/10 05:50102EPA 8260Percent Moisture 16.6 % 09/09/10 09:060.10ASTM D2974-87




Page 21 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872034 SS-107EBeryllium 1.3 mg/kg 09/22/10 17:250.79EPA 6010Chromium 21.4 mg/kg 09/22/10 17:254.0EPA 6010Copper 1.7J mg/kg 09/22/10 17:25 D34.0EPA 6010Manganese 294 mg/kg 09/22/10 17:254.0EPA 6010Nickel 15.5 mg/kg 09/22/10 17:254.0EPA 6010Zinc 74.5 mg/kg 09/22/10 17:257.9EPA 6010Percent Moisture 11.0 % 09/09/10 09:090.10ASTM D2974-87

9276872035 SS-112AArsenic 1.7J mg/kg 09/22/10 17:28 D31.9EPA 6010Beryllium 0.70 mg/kg 09/22/10 17:280.38EPA 6010Chromium 15.2 mg/kg 09/22/10 17:281.9EPA 6010Copper 3.3 mg/kg 09/22/10 17:281.9EPA 6010Lead 3.7 mg/kg 09/22/10 17:281.9EPA 6010Manganese 150 mg/kg 09/22/10 17:281.9EPA 6010Nickel 14.4 mg/kg 09/22/10 17:281.9EPA 6010Zinc 53.2 mg/kg 09/22/10 17:283.8EPA 6010Mercury 0.0096 mg/kg 09/15/10 13:130.0036EPA 7471Acetone 41.9J ug/kg 09/09/10 17:54108EPA 8260Methylene Chloride 19.7J ug/kg 09/09/10 17:5421.7EPA 8260Percent Moisture 9.3 % 09/09/10 09:100.10ASTM D2974-87

9276872036 SS-112BBeryllium 0.74 mg/kg 09/22/10 17:410.65EPA 6010Chromium 15.7 mg/kg 09/22/10 17:413.2EPA 6010Copper 11.4 mg/kg 09/22/10 17:413.2EPA 6010Lead 6.3 mg/kg 09/22/10 17:413.2EPA 6010Manganese 230 mg/kg 09/22/10 17:413.2EPA 6010Nickel 10.1 mg/kg 09/22/10 17:413.2EPA 6010Thallium 2.0J mg/kg 09/22/10 17:41 D36.5EPA 6010Zinc 73.6 mg/kg 09/22/10 17:416.5EPA 6010Percent Moisture 5.5 % 09/09/10 09:100.10ASTM D2974-87

9276872037 SS-112CArsenic 2.0J mg/kg 09/22/10 17:45 D32.2EPA 6010Beryllium 1.4 mg/kg 09/22/10 17:450.44EPA 6010Chromium 16.1 mg/kg 09/22/10 17:452.2EPA 6010Copper 7.7 mg/kg 09/22/10 17:452.2EPA 6010Lead 5.1 mg/kg 09/22/10 17:452.2EPA 6010Manganese 368 mg/kg 09/22/10 17:452.2EPA 6010Nickel 10.1 mg/kg 09/22/10 17:452.2EPA 6010Zinc 61.5 mg/kg 09/22/10 17:454.4EPA 6010Mercury 0.00063J mg/kg 09/14/10 14:370.0049EPA 7471Acetone 10.4J ug/kg 09/09/10 06:4594.7EPA 8260Percent Moisture 7.6 % 09/09/10 09:100.10ASTM D2974-87

9276872038 SS-112DArsenic 1.5J mg/kg 09/22/10 17:48 D31.8EPA 6010Beryllium 0.88 mg/kg 09/22/10 17:480.36EPA 6010



Page 22 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872038 SS-112DChromium 17.1 mg/kg 09/22/10 17:481.8EPA 6010Copper 20.2 mg/kg 09/22/10 17:481.8EPA 6010Lead 6.2 mg/kg 09/22/10 17:481.8EPA 6010Manganese 240 mg/kg 09/22/10 17:481.8EPA 6010Nickel 10.6 mg/kg 09/22/10 17:481.8EPA 6010Zinc 63.1 mg/kg 09/22/10 17:483.6EPA 6010Dibenz(a,h)anthracene 78.2J ug/kg 09/25/10 04:28350EPA 8270Indeno(1,2,3-cd)pyrene 72.6J ug/kg 09/25/10 04:28350EPA 8270Percent Moisture 5.8 % 09/09/10 09:100.10ASTM D2974-87

9276872039 SS-112EArsenic 1.9J mg/kg 09/22/10 17:52 D32.4EPA 6010Beryllium 0.87 mg/kg 09/22/10 17:520.48EPA 6010Chromium 18.3 mg/kg 09/22/10 17:522.4EPA 6010Copper 11.6 mg/kg 09/22/10 17:522.4EPA 6010Lead 5.5 mg/kg 09/22/10 17:522.4EPA 6010Manganese 209 mg/kg 09/22/10 17:522.4EPA 6010Nickel 9.8 mg/kg 09/22/10 17:522.4EPA 6010Zinc 60.1 mg/kg 09/22/10 17:524.8EPA 6010Percent Moisture 9.4 % 09/09/10 09:110.10ASTM D2974-87

9276872040 SS-108AAcetone 44.0J ug/kg 09/09/10 17:35119EPA 8260Percent Moisture 14.0 % 09/09/10 09:110.10ASTM D2974-87

9276872041 SS-108ABeryllium 0.79 mg/kg 09/22/10 17:550.41EPA 6010Chromium 17.5 mg/kg 09/22/10 17:552.1EPA 6010Copper 11.2 mg/kg 09/22/10 17:552.1EPA 6010Lead 6.7 mg/kg 09/22/10 17:552.1EPA 6010Manganese 116 mg/kg 09/22/10 17:552.1EPA 6010Nickel 8.5 mg/kg 09/22/10 17:552.1EPA 6010Zinc 59.2 mg/kg 09/22/10 17:554.1EPA 6010Mercury 0.051 mg/kg 09/14/10 14:440.0051EPA 7471Percent Moisture 7.9 % 09/09/10 09:120.10ASTM D2974-87


9276872043 SS-108BBeryllium 1.5 mg/kg 09/22/10 17:590.80EPA 6010Chromium 20.2 mg/kg 09/22/10 17:594.0EPA 6010Copper 9.7 mg/kg 09/22/10 17:594.0EPA 6010Lead 9.5 mg/kg 09/22/10 17:594.0EPA 6010Manganese 393 mg/kg 09/22/10 17:594.0EPA 6010Nickel 17.6 mg/kg 09/22/10 17:594.0EPA 6010Zinc 115 mg/kg 09/22/10 17:598.0EPA 6010Mercury 0.0075 mg/kg 09/14/10 14:470.0035EPA 7471Percent Moisture 4.1 % 09/09/10 09:130.10ASTM D2974-87



Page 23 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744




9276872045 SS-108CArsenic 4.6J mg/kg 09/22/10 18:02 D35.1EPA 6010Beryllium 1.8 mg/kg 09/22/10 18:021.0EPA 6010Chromium 27.3 mg/kg 09/22/10 18:025.1EPA 6010Copper 4.3J mg/kg 09/22/10 18:02 D35.1EPA 6010Lead 9.5 mg/kg 09/22/10 18:025.1EPA 6010Manganese 664 mg/kg 09/22/10 18:025.1EPA 6010Nickel 17.5 mg/kg 09/22/10 18:025.1EPA 6010Zinc 93.5 mg/kg 09/22/10 18:0210.2EPA 6010Mercury 0.0046 mg/kg 09/14/10 14:500.0045EPA 7471Percent Moisture 10.6 % 09/09/10 15:560.10ASTM D2974-87

9276872046 SS-108DArsenic 2.9J mg/kg 09/14/10 14:55 D34.0EPA 6010Beryllium 1.8 mg/kg 09/14/10 14:55 D30.79EPA 6010Chromium 23.6 mg/kg 09/14/10 14:55 D34.0EPA 6010Copper 7.0 mg/kg 09/14/10 14:55 D34.0EPA 6010Lead 4.1 mg/kg 09/14/10 14:55 D34.0EPA 6010Manganese 509 mg/kg 09/14/10 14:55 D34.0EPA 6010Nickel 16.0 mg/kg 09/14/10 14:55 D34.0EPA 6010Selenium 3.5J mg/kg 09/14/10 14:55 D37.9EPA 6010Thallium 17.5 mg/kg 09/14/10 14:55 D37.9EPA 6010Zinc 88.0 mg/kg 09/14/10 14:55 D37.9EPA 6010Percent Moisture 13.6 % 09/09/10 15:570.10ASTM D2974-87



9276872049 SS-108EArsenic 4.0J mg/kg 09/22/10 18:05 D34.3EPA 6010Beryllium 1.5 mg/kg 09/22/10 18:050.86EPA 6010Chromium 17.5 mg/kg 09/22/10 18:054.3EPA 6010Copper 2.4J mg/kg 09/22/10 18:05 D34.3EPA 6010Lead 7.4 mg/kg 09/22/10 18:054.3EPA 6010Manganese 502 mg/kg 09/22/10 18:054.3EPA 6010Nickel 15.5 mg/kg 09/22/10 18:054.3EPA 6010Zinc 61.4 mg/kg 09/22/10 18:058.6EPA 6010Percent Moisture 11.6 % 09/09/10 15:580.10ASTM D2974-87

9276872050 SS-114AArsenic 5.3J mg/kg 09/22/10 18:09 D37.0EPA 6010Beryllium 4.0 mg/kg 09/22/10 18:091.4EPA 6010Cadmium 1.4 mg/kg 09/22/10 18:091.4EPA 6010Chromium 34.3 mg/kg 09/22/10 18:097.0EPA 6010Copper 44.1 mg/kg 09/22/10 18:097.0EPA 6010



Page 24 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872050 SS-114ALead 31.5 mg/kg 09/22/10 18:097.0EPA 6010Manganese 739 mg/kg 09/22/10 18:097.0EPA 6010Nickel 82.5 mg/kg 09/22/10 18:097.0EPA 6010Silver 101 mg/kg 09/22/10 18:097.0EPA 6010Zinc 515 mg/kg 09/22/10 18:0914.1EPA 6010Mercury 0.010 mg/kg 09/14/10 15:080.0037EPA 7471Acetone 51.5J ug/kg 09/09/10 08:54101EPA 82602-Butanone (MEK) 6.1J ug/kg 09/09/10 08:54101EPA 8260Methyl acetate 85.7 ug/kg 09/09/10 08:5410.1EPA 8260Trichloroethene 3.5J ug/kg 09/09/10 08:545.0EPA 8260Percent Moisture 8.9 % 09/09/10 15:580.10ASTM D2974-87

9276872051 SS-114BArsenic 2.7 mg/kg 09/22/10 18:122.6EPA 6010Beryllium 3.0 mg/kg 09/22/10 18:120.52EPA 6010Chromium 42.1 mg/kg 09/22/10 18:122.6EPA 6010Copper 25.6 mg/kg 09/22/10 18:122.6EPA 6010Lead 8.8 mg/kg 09/22/10 18:122.6EPA 6010Manganese 446 mg/kg 09/22/10 18:122.6EPA 6010Nickel 25.9 mg/kg 09/22/10 18:122.6EPA 6010Silver 72.1 mg/kg 09/22/10 18:122.6EPA 6010Thallium 1.7J mg/kg 09/22/10 18:12 D35.2EPA 6010Zinc 106 mg/kg 09/22/10 18:125.2EPA 6010Mercury 0.0061 mg/kg 09/14/10 15:110.0051EPA 7471bis(2-Ethylhexyl)phthalate 144J ug/kg 09/25/10 06:53367EPA 8270Fluoranthene 75.9J ug/kg 09/25/10 06:53367EPA 8270Acetone 153 ug/kg 09/10/10 01:20 C9129EPA 82602-Butanone (MEK) 12.7J ug/kg 09/10/10 01:20129EPA 8260Carbon disulfide 5.2J ug/kg 09/10/10 01:2012.9EPA 8260Trichloroethene 28.9 ug/kg 09/10/10 01:206.4EPA 8260Percent Moisture 10.1 % 09/09/10 15:580.10ASTM D2974-87

9276872052 SS-131Arsenic 2.7 mg/kg 09/22/10 18:25 D32.7EPA 6010Beryllium 1.7 mg/kg 09/22/10 18:250.54EPA 6010Chromium 33.1 mg/kg 09/22/10 18:252.7EPA 6010Copper 27.3 mg/kg 09/22/10 18:252.7EPA 6010Lead 12.6 mg/kg 09/22/10 18:252.7EPA 6010Manganese 433 mg/kg 09/22/10 18:252.7EPA 6010Nickel 16.4 mg/kg 09/22/10 18:252.7EPA 6010Silver 0.22J mg/kg 09/22/10 18:25 D32.7EPA 6010Zinc 65.7 mg/kg 09/22/10 18:255.4EPA 6010Mercury 0.070 mg/kg 09/14/10 15:140.0064EPA 7471Percent Moisture 24.5 % 09/09/10 15:580.10ASTM D2974-87

9276872053 SS-132Beryllium 1.2 mg/kg 09/22/10 18:290.24EPA 6010Chromium 24.6 mg/kg 09/22/10 18:291.2EPA 6010Copper 18.9 mg/kg 09/22/10 18:291.2EPA 6010



Page 25 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744



9276872053 SS-132Lead 9.9 mg/kg 09/22/10 18:291.2EPA 6010Manganese 150 mg/kg 09/22/10 18:291.2EPA 6010Nickel 11.9 mg/kg 09/22/10 18:291.2EPA 6010Zinc 45.4 mg/kg 09/22/10 18:292.4EPA 6010Mercury 0.040 mg/kg 09/14/10 15:160.0050EPA 7471Percent Moisture 20.4 % 09/09/10 15:580.10ASTM D2974-87

9276872054 FD-16Percent Moisture 11.1 % 09/09/10 15:590.10ASTM D2974-87

9276872055 FD-17Beryllium 1.3 mg/kg 09/22/10 18:320.59EPA 6010Chromium 18.2 mg/kg 09/22/10 18:323.0EPA 6010Copper 3.7 mg/kg 09/22/10 18:323.0EPA 6010Lead 5.0 mg/kg 09/22/10 18:323.0EPA 6010Manganese 370 mg/kg 09/22/10 18:323.0EPA 6010Nickel 11.8 mg/kg 09/22/10 18:323.0EPA 6010Zinc 72.4 mg/kg 09/22/10 18:325.9EPA 6010Mercury 0.0061 mg/kg 09/14/10 15:190.0042EPA 7471Percent Moisture 6.4 % 09/09/10 15:590.10ASTM D2974-87




9276872059 FD-22Beryllium 1.4J mg/kg 09/14/10 15:40 D31.6EPA 6010Chromium 18.0 mg/kg 09/14/10 15:40 D37.9EPA 6010Copper 1.6J mg/kg 09/14/10 15:40 D37.9EPA 6010Manganese 249 mg/kg 09/14/10 15:40 D37.9EPA 6010Nickel 14.6 mg/kg 09/14/10 15:40 D37.9EPA 6010Zinc 90.1 mg/kg 09/14/10 15:4015.8EPA 6010Mercury 0.0010J mg/kg 09/14/10 15:220.0031EPA 7471Percent Moisture 8.4 % 09/09/10 16:010.10ASTM D2974-87




9276872063 FD-27Acetone 47.6J ug/kg 09/08/10 04:39108EPA 8260



Page 26 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744




9276872064 FD-28Beryllium 1.1 mg/kg 09/14/10 15:47 D30.48EPA 6010Chromium 12.6 mg/kg 09/14/10 15:47 D32.4EPA 6010Copper 13.3 mg/kg 09/14/10 15:47 D32.4EPA 6010Lead 5.0 mg/kg 09/14/10 15:47 D32.4EPA 6010Manganese 681 mg/kg 09/14/10 15:47 D32.4EPA 6010Nickel 8.7 mg/kg 09/14/10 15:47 D32.4EPA 6010Thallium 1.5J mg/kg 09/14/10 15:47 D34.8EPA 6010Zinc 82.5 mg/kg 09/14/10 15:47 D34.8EPA 6010Percent Moisture 5.2 % 09/09/10 16:130.10ASTM D2974-87





9276872069 FD-33Antimony 0.76J mg/kg 09/14/10 15:50 D31.2EPA 6010Arsenic 1.3 mg/kg 09/14/10 15:50 D31.2EPA 6010Beryllium 1.4 mg/kg 09/14/10 15:50 D30.23EPA 6010Cadmium 0.18J mg/kg 09/14/10 15:50 D30.23EPA 6010Chromium 24.3 mg/kg 09/14/10 15:50 D31.2EPA 6010Copper 21.0 mg/kg 09/14/10 15:50 D31.2EPA 6010Lead 9.4 mg/kg 09/14/10 15:50 D31.2EPA 6010Manganese 171 mg/kg 09/14/10 15:50 D31.2EPA 6010Nickel 11.0 mg/kg 09/14/10 15:50 D31.2EPA 6010Zinc 46.5 mg/kg 09/14/10 15:50 D32.3EPA 6010Mercury 0.026 mg/kg 09/16/10 12:22 B0.0056EPA 7471Percent Moisture 19.3 % 09/09/10 16:160.10ASTM D2974-87

9276872071 SS-110AAcetone 12.1J ug/kg 09/08/10 04:57100EPA 8260Methyl acetate 1.7J ug/kg 09/08/10 04:5710.0EPA 8260Percent Moisture 14.6 % 09/10/10 08:440.10ASTM D2974-87


9276872073 SS-110CAcetone 13.4J ug/kg 09/08/10 05:35114EPA 8260Percent Moisture 18.2 % 09/10/10 08:450.10ASTM D2974-87



Page 27 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744




9276872075 SS-110ETrichloroethene 2.6J ug/kg 09/08/10 06:125.1EPA 8260Percent Moisture 12.5 % 09/10/10 08:460.10ASTM D2974-87











9276872086 SS-105AAcetone 71.2J ug/kg 09/08/10 21:3291.3EPA 8260cis-1,2-Dichloroethene 2.1J ug/kg 09/08/10 21:324.6EPA 8260Methyl acetate 2.2J ug/kg 09/08/10 21:329.1EPA 8260Trichloroethene 15.2 ug/kg 09/08/10 21:324.6EPA 8260Percent Moisture 8.1 % 09/10/10 08:490.10ASTM D2974-87



9276872089 SS-105DAcetone 19.3J ug/kg 09/09/10 03:23108EPA 8260



Page 28 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

HITS ONLY


9276872MILLS GAP 6686081744




9276872090 SS-105ETrichloroethene 6.3 ug/kg 09/09/10 03:415.1EPA 8260Percent Moisture 11.6 % 09/10/10 15:260.10ASTM D2974-87

9276872091 FD-20Acetone 81.3J ug/kg 09/09/10 03:5988.6EPA 82602-Butanone (MEK) 5.4J ug/kg 09/09/10 03:5988.6EPA 8260cis-1,2-Dichloroethene 2.4J ug/kg 09/09/10 03:594.4EPA 8260Methyl acetate 3.8J ug/kg 09/09/10 03:598.9EPA 8260Trichloroethene 15.5 ug/kg 09/09/10 03:594.4EPA 8260Percent Moisture 8.2 % 09/10/10 15:260.10ASTM D2974-87

9276872092 FD-23Acetone 29.3J ug/kg 09/09/10 04:18103EPA 8260Percent Moisture 8.3 % 09/10/10 15:260.10ASTM D2974-87

9276872093 EB-02Arsenic 5.4 ug/L 09/10/10 19:515.0EPA 6010Chromium 0.53J ug/L 09/10/10 19:515.0EPA 6010Selenium 11.9 ug/L 09/10/10 19:5110.0EPA 6010Zinc 1.9J ug/L 09/10/10 19:5110.0EPA 6010Mercury 0.11J ug/L 09/16/10 14:17 B0.20EPA 7470Benzo(g,h,i)perylene 4.1J ug/L 09/25/10 02:4010.0EPA 8270Dibenz(a,h)anthracene 3.7J ug/L 09/25/10 02:4010.0EPA 8270Indeno(1,2,3-cd)pyrene 3.5J ug/L 09/25/10 02:4010.0EPA 8270Acetone 6.3J ug/L 09/08/10 01:2925.0EPA 8260

9276872095 TB-05Methylene Chloride 1.9J ug/L 09/08/10 01:542.0EPA 8260



Page 29 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010













• Antimony• Arsenic• Manganese• Selenium• Thallium

• MSD (Lab ID: 494456)• Antimony• Arsenic• Selenium


• Antimony• Arsenic• Beryllium• Cadmium• Copper



Page 30 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010




R1: RPD value was outside control limits.• Lead• Selenium• Silver• Thallium



• Antimony• Arsenic• Manganese• Selenium

• MSD (Lab ID: 495086)• Antimony• Arsenic• Chromium• Manganese• Selenium


• Chromium



• Antimony• Arsenic• Manganese• Thallium

• MSD (Lab ID: 495774)• Antimony• Arsenic• Manganese• Selenium• Thallium


• Manganese



Page 31 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010






• SS-105A (Lab ID: 9276872020)• Silver• Arsenic• Antimony• Selenium• Thallium

• SS-105B (Lab ID: 9276872021)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-105C (Lab ID: 9276872022)• Silver• Cadmium• Antimony• Selenium• Thallium

• SS-105D (Lab ID: 9276872023)• Silver• Arsenic• Cadmium• Lead• Antimony• Selenium• Thallium

• SS-105E (Lab ID: 9276872024)• Silver• Arsenic• Beryllium• Cadmium• Copper• Nickel• Lead• Antimony• Selenium



Page 32 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-105E (Lab ID: 9276872024)• Thallium

• SS-106A (Lab ID: 9276872015)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium


• SS-106C (Lab ID: 9276872017)• Silver• Arsenic• Cadmium• Copper• Antimony• Selenium• Thallium

• SS-106D (Lab ID: 9276872018)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-106E (Lab ID: 9276872019)• Silver• Arsenic• Cadmium• Copper• Lead• Antimony• Selenium• Thallium

• SS-110A (Lab ID: 9276872001)• Silver• Arsenic



Page 33 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-110A (Lab ID: 9276872001)• Cadmium• Antimony• Selenium• Thallium

• SS-110B (Lab ID: 9276872002)• Silver• Arsenic• Cadmium• Copper• Lead• Antimony• Selenium• Thallium

• SS-110C (Lab ID: 9276872003)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-110D (Lab ID: 9276872004)• Silver• Arsenic• Cadmium• Copper• Lead• Antimony• Selenium• Thallium

• SS-110E (Lab ID: 9276872005)• Silver• Arsenic• Cadmium• Copper• Antimony• Lead• Selenium• Thallium

• SS-111A (Lab ID: 9276872006)• Silver• Arsenic• Antimony



Page 34 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-111A (Lab ID: 9276872006)• Selenium• Thallium




• SS-111E (Lab ID: 9276872012)• Silver• Cadmium• Lead• Antimony• Selenium• Thallium


• FD-17 (Lab ID: 9276872055)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-107A (Lab ID: 9276872025)• Silver



Page 35 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-107A (Lab ID: 9276872025)• Arsenic• Cadmium• Antimony• Selenium• Thallium



• SS-107D (Lab ID: 9276872032)• Silver• Arsenic• Cadmium• Lead• Antimony• Selenium• Thallium

• SS-107E (Lab ID: 9276872034)• Silver• Arsenic• Cadmium• Copper• Lead• Antimony• Selenium• Thallium

• SS-108A (Lab ID: 9276872041)• Silver• Arsenic• Cadmium• Antimony• Selenium



Page 36 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-108A (Lab ID: 9276872041)• Thallium


• SS-108C (Lab ID: 9276872045)• Silver• Arsenic• Cadmium• Copper• Antimony• Selenium• Thallium

• SS-108E (Lab ID: 9276872049)• Silver• Arsenic• Cadmium• Copper• Antimony• Selenium• Thallium

• SS-112A (Lab ID: 9276872035)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium


• SS-112C (Lab ID: 9276872037)• Silver• Arsenic• Cadmium



Page 37 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-112C (Lab ID: 9276872037)• Antimony• Selenium• Thallium


• SS-112E (Lab ID: 9276872039)• Silver• Arsenic• Cadmium• Antimony• Selenium• Thallium

• SS-114A (Lab ID: 9276872050)• Arsenic• Antimony• Selenium• Thallium

• SS-114B (Lab ID: 9276872051)• Cadmium• Antimony• Selenium• Thallium





Page 38 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• FD-22 (Lab ID: 9276872059)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium

• FD-28 (Lab ID: 9276872064)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• FD-33 (Lab ID: 9276872069)• Silver• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc

• SS-108D (Lab ID: 9276872046)• Silver



Page 39 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010



Analyte Comments:


• SS-108D (Lab ID: 9276872046)• Arsenic• Beryllium• Cadmium• Chromium• Copper• Manganese• Nickel• Lead• Antimony• Selenium• Thallium• Zinc



Page 40 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 6010


Description: 6010 MET ICP, 3030C

General Information:1 sample was analyzed for EPA 6010. All samples were received in acceptable condition with any exceptions noted below.


Sample Preparation:The samples were prepared in accordance with SM 3030C with any exceptions noted below.








• Thallium





Page 41 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 7470













• Mercury• MS (Lab ID: 497301)

• Mercury• MSD (Lab ID: 497300)


• Mercury





Page 42 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 7471














• Mercury




• Mercury





Page 43 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 7471




M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• Mercury

• MSD (Lab ID: 496430)• Mercury

• MSD (Lab ID: 496432)• Mercury




• Mercury





Page 44 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270





H5: Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.• FD-21 (Lab ID: 9276872058)• SS-108A (Lab ID: 9276872041)• SS-114A (Lab ID: 9276872050)• SS-114B (Lab ID: 9276872051)






QC Batch: OEXT/11146S0: Surrogate recovery outside laboratory control limits.

• SS-110C (Lab ID: 9276872003)• 2-Fluorobiphenyl (S)

• SS-110E (Lab ID: 9276872005)• 2-Fluorobiphenyl (S)


• SS-105D (Lab ID: 9276872023)• 2,4,6-Tribromophenol (S)

• SS-106C (Lab ID: 9276872017)• 2-Fluorobiphenyl (S)• Phenol-d6 (S)

• SS-107A (Lab ID: 9276872026)• Phenol-d6 (S)

• SS-112A (Lab ID: 9276872035)• 2-Fluorobiphenyl (S)



Page 45 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270




• Phenol-d6 (S)S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-analysis).

• SS-105D (Lab ID: 9276872023)• Phenol-d6 (S)

• SS-106B (Lab ID: 9276872016)• 2,4,6-Tribromophenol (S)• 2-Fluorobiphenyl (S)• 2-Fluorophenol (S)• Nitrobenzene-d5 (S)• Phenol-d6 (S)• Terphenyl-d14 (S)

• SS-107B (Lab ID: 9276872028)• 2-Fluorobiphenyl (S)• Nitrobenzene-d5 (S)• Phenol-d6 (S)


• MSD (Lab ID: 497435)• Phenol-d6 (S)

• SS-108C (Lab ID: 9276872045)• Phenol-d6 (S)

• SS-111B (Lab ID: 9276872007)• 2-Fluorobiphenyl (S)• Phenol-d6 (S)

• SS-112E (Lab ID: 9276872039)• Phenol-d6 (S)

S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-analysis).

• FD-16 (Lab ID: 9276872054)• 2-Fluorobiphenyl (S)• Nitrobenzene-d5 (S)• Phenol-d6 (S)

• FD-31 (Lab ID: 9276872067)• 2,4,6-Tribromophenol (S)• 2-Fluorobiphenyl (S)• 2-Fluorophenol (S)• Nitrobenzene-d5 (S)• Phenol-d6 (S)

• SS-108B (Lab ID: 9276872043)• 2,4,6-Tribromophenol (S)• 2-Fluorobiphenyl (S)• 2-Fluorophenol (S)



Page 46 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270



QC Batch: OEXT/11170S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-analysis).

• Nitrobenzene-d5 (S)• Phenol-d6 (S)• Terphenyl-d14 (S)

• SS-108D (Lab ID: 9276872047)• 2-Fluorobiphenyl (S)• Nitrobenzene-d5 (S)• Phenol-d6 (S)


• SS-108E (Lab ID: 9276872048)• Phenol-d6 (S)

QC Batch: OEXT/11277S2: Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from sample re-analysis).

• SS-108A (Lab ID: 9276872041)• Phenol-d6 (S)






• LCS (Lab ID: 496477)• 2,3,4,6-Tetrachlorophenol• bis(2-Ethylhexyl)phthalate





Page 47 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270



QC Batch: OEXT/11153L3: Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

• LCS (Lab ID: 496651)• 2,3,4,6-Tetrachlorophenol• Atrazine• bis(2-Ethylhexyl)phthalate






• LCS (Lab ID: 497675)• Acetophenone



QC Batch: OEXT/11234L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.

• LCS (Lab ID: 500222)• 2,3,4,6-Tetrachlorophenol• Acetophenone• Atrazine• bis(2-Ethylhexyl)phthalate


• LCS (Lab ID: 502116)• 2,3,4,6-Tetrachlorophenol• Acetophenone• Atrazine



Page 48 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270






• Benzaldehyde• Caprolactam



• MSD (Lab ID: 496479)• Atrazine• Caprolactam• Di-n-octylphthalate• Hexachlorocyclopentadiene• bis(2-Ethylhexyl)phthalate



• Acetophenone• bis(2-Ethylhexyl)phthalate

• MSD (Lab ID: 496653)• Acetophenone• Atrazine• bis(2-Ethylhexyl)phthalate

QC Batch: OEXT/11177A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276872048,9276981018


• Acetophenone• Atrazine• bis(2-Ethylhexyl)phthalate

• MS (Lab ID: 497678)• Acetophenone• Carbazole

• MSD (Lab ID: 497677)• 2,3,4,6-Tetrachlorophenol• Acetophenone• Atrazine



Page 49 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270



QC Batch: OEXT/11177A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276872048,9276981018

M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• bis(2-Ethylhexyl)phthalate

• MSD (Lab ID: 497679)• Acetophenone• Atrazine• Caprolactam• bis(2-Ethylhexyl)phthalate


• Carbazole• MSD (Lab ID: 497679)


• MSD (Lab ID: 497679)• 2,4-Dinitrophenol• 2-Methylphenol(o-Cresol)• 4,6-Dinitro-2-methylphenol• Benzo(a)pyrene• Carbazole• N-Nitrosodiphenylamine• Phenol• Pyrene



• Acetophenone• Benzaldehyde• Biphenyl (Diphenyl)• Caprolactam• Carbazole• Isophorone

• MSD (Lab ID: 497435)• 2,4,5-Trichlorophenol• 2,4-Dinitrotoluene• 2,6-Dinitrotoluene• 2-Nitroaniline• 2-Nitrophenol• 4-Bromophenylphenyl ether• Acenaphthylene• Acetophenone• Anthracene



Page 50 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270




M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• Benzaldehyde• Benzo(a)pyrene• Benzo(k)fluoranthene• Biphenyl (Diphenyl)• Butylbenzylphthalate• Caprolactam• Carbazole• Chrysene• Di-n-octylphthalate• Dibenzofuran• Diethylphthalate• Fluoranthene• Fluorene• Isophorone• N-Nitroso-di-n-propylamine• Naphthalene• Phenanthrene• Pyrene


• Biphenyl (Diphenyl)• Caprolactam• Carbazole• Isophorone

• MSD (Lab ID: 497435)• 2,4,5-Trichlorophenol• 2,4-Dinitrotoluene• 2,6-Dinitrotoluene• 2-Nitroaniline• 2-Nitrophenol• 4-Bromophenylphenyl ether• Acenaphthylene• Anthracene• Benzo(a)pyrene• Benzo(k)fluoranthene• Biphenyl (Diphenyl)• Butylbenzylphthalate• Caprolactam• Carbazole• Chrysene• Di-n-octylphthalate• Dibenzofuran• Diethylphthalate



Page 51 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270




M1: Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.• Fluoranthene• Fluorene• Isophorone• N-Nitroso-di-n-propylamine• Naphthalene• Phenanthrene• Pyrene


• 1,2,4,5-Tetrachlorobenzene• 2,3,4,6-Tetrachlorophenol• 2,4,5-Trichlorophenol• 2,4,6-Trichlorophenol• 2,4-Dichlorophenol• 2,4-Dinitrotoluene• 2,6-Dinitrotoluene• 2-Chloronaphthalene• 2-Chlorophenol• 2-Methylnaphthalene• 2-Nitrophenol• 4,6-Dinitro-2-methylphenol• 4-Bromophenylphenyl ether• 4-Chloro-3-methylphenol• 4-Chlorophenylphenyl ether• 4-Nitrophenol• Acenaphthene• Acenaphthylene• Acetophenone• Benzo(a)anthracene• Benzo(a)pyrene• Benzo(b)fluoranthene• Benzo(g,h,i)perylene• Benzo(k)fluoranthene• Biphenyl (Diphenyl)• Chrysene• Dibenz(a,h)anthracene• Dibenzofuran• Diethylphthalate• Dimethylphthalate• Fluorene• Hexachloro-1,3-butadiene• Hexachlorobenzene• Hexachlorocyclopentadiene



Page 52 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270




R1: RPD value was outside control limits.• Hexachloroethane• Indeno(1,2,3-cd)pyrene• Isophorone• N-Nitroso-di-n-propylamine• Naphthalene• Pyrene• bis(2-Chloroethoxy)methane• bis(2-Ethylhexyl)phthalate



• 2,3,4,6-Tetrachlorophenol• Acetophenone

• MSD (Lab ID: 502118)• 2,3,4,6-Tetrachlorophenol• Acetophenone



• 2,3,4,6-Tetrachlorophenol• Acetophenone• Benzaldehyde



• 2,3,4,6-Tetrachlorophenol• Acetophenone• Benzaldehyde



• Benzaldehyde• bis(2-Ethylhexyl)phthalate



Page 53 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270





QC Batch: OEXT/11170

• MSD (Lab ID: 497435)• 2,4-Dimethylphenol• Benzaldehyde

• SS-108B (Lab ID: 9276872043)• Phenol


• MS (Lab ID: 497676)• Atrazine

• MSD (Lab ID: 497677)• Atrazine• Atrazine


• MS (Lab ID: 500223)• bis(2-Ethylhexyl)phthalate

• MSD (Lab ID: 500224)• Benzaldehyde



Page 54 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270


Description: 8270 MSSV Semivolatile Organic











• LCS (Lab ID: 494466)• 2,3,4,6-Tetrachlorophenol• Atrazine




• 2,3,4,6-Tetrachlorophenol• 3,3'-Dichlorobenzidine• Benzaldehyde• Caprolactam



Page 55 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8270


Description: 8270 MSSV Semivolatile Organic


M0: Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.• MSD (Lab ID: 494468)

• 2,3,4,6-Tetrachlorophenol• 3,3'-Dichlorobenzidine• 3-Nitroaniline• 4-Nitroaniline• Benzaldehyde• Caprolactam


• 2,3,4,6-Tetrachlorophenol• 3,3'-Dichlorobenzidine• Caprolactam

• MSD (Lab ID: 494468)• 2,3,4,6-Tetrachlorophenol• 3,3'-Dichlorobenzidine• 3-Nitroaniline• 4-Nitroaniline• Benzaldehyde• Caprolactam





Page 56 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8260


Description: 8260 MSV Low Level














Page 57 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8260











QC Batch: MSV/12151L0: Analyte recovery in the laboratory control sample (LCS) was outside QC limits.

• LCS (Lab ID: 493934)• Methyl acetate


• LCS (Lab ID: 493934)• Bromomethane


• LCS (Lab ID: 493939)• Methyl acetate• Methylene Chloride





Page 58 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8260










• LCS (Lab ID: 495146)• Bromodichloromethane• Bromomethane• Chlorobenzene• Dibromochloromethane


QC Batch: MSV/12151A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276750025


• Trichloroethene

QC Batch: MSV/12175A matrix spike and matrix spike duplicate (MS/MSD) were performed on the following sample(s): 9276872040


• 1,1-Dichloroethene• Benzene• Chlorobenzene• Toluene• Trichloroethene





Page 59 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 8260



Analyte Comments:

QC Batch: MSV/12185C9: Common Laboratory Contaminant.

• SS-114B (Lab ID: 9276872051)• Acetone



Page 60 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


SM 4500-CN-E



General Information:40 samples were analyzed for SM 4500-CN-E. All samples were received in acceptable condition with any exceptions noted below.









General Information:1 sample was analyzed for SM 4500-CN-E. All samples were received in acceptable condition with any exceptions noted below.








Page 61 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


SM 4500-CN-E








Page 62 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

PROJECT NARRATIVE


9276872MILLS GAP 6686081744

Method:


EPA 7196


Description: 7196 Chromium, Hexavalent

















This data package has been reviewed for quality and completeness and is approved for release.



Page 63 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: SS-110A Lab ID: 9276872001 Collected: 09/01/10 16:10 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "dry-weight" basis



Antimony ND mg/kg 5 09/22/10 18:36 7440-36-0 D309/08/10 15:402.9 1.6Arsenic ND mg/kg 5 09/22/10 18:36 7440-38-2 D309/08/10 15:402.9 1.9Beryllium 0.81 mg/kg 5 09/22/10 18:36 7440-41-709/08/10 15:400.59 0.12Cadmium ND mg/kg 5 09/22/10 18:36 7440-43-9 D309/08/10 15:400.59 0.35Chromium 23.0 mg/kg 5 09/22/10 18:36 7440-47-309/08/10 15:402.9 0.18Copper 4.2 mg/kg 5 09/22/10 18:36 7440-50-809/08/10 15:402.9 0.23Lead 8.0 mg/kg 5 09/22/10 18:36 7439-92-109/08/10 15:402.9 2.8Manganese 228 mg/kg 5 09/22/10 18:36 7439-96-509/08/10 15:402.9 0.18Nickel 10.6 mg/kg 5 09/22/10 18:36 7440-02-009/08/10 15:402.9 1.1Selenium ND mg/kg 5 09/22/10 18:36 7782-49-2 D309/08/10 15:405.9 2.2Silver ND mg/kg 5 09/22/10 18:36 7440-22-4 D309/08/10 15:402.9 0.18Thallium ND mg/kg 5 09/22/10 18:36 7440-28-0 D309/08/10 15:405.9 1.5Zinc 49.1 mg/kg 5 09/22/10 18:36 7440-66-609/08/10 15:405.9 1.5


Mercury 0.041 mg/kg 1 09/10/10 12:31 7439-97-6 M109/08/10 10:010.0052 0.00010





Date: 09/27/2010 06:48 PM Page 64 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 14:02 91-94-109/13/10 12:302050 89.32,4-Dichlorophenol ND ug/kg 1 09/18/10 14:02 120-83-209/13/10 12:30409 89.3Diethylphthalate ND ug/kg 1 09/18/10 14:02 84-66-209/13/10 12:30409 63.32,4-Dimethylphenol ND ug/kg 1 09/18/10 14:02 105-67-909/13/10 12:30409 161Dimethylphthalate ND ug/kg 1 09/18/10 14:02 131-11-309/13/10 12:30409 83.1Di-n-butylphthalate ND ug/kg 1 09/18/10 14:02 84-74-209/13/10 12:30409 67.04,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 14:02 534-52-109/13/10 12:30819 81.92,4-Dinitrophenol ND ug/kg 1 09/18/10 14:02 51-28-509/13/10 12:302050 67.02,4-Dinitrotoluene ND ug/kg 1 09/18/10 14:02 121-14-209/13/10 12:30409 76.92,6-Dinitrotoluene ND ug/kg 1 09/18/10 14:02 606-20-209/13/10 12:30409 85.6Di-n-octylphthalate ND ug/kg 1 09/18/10 14:02 117-84-009/13/10 12:30409 85.6bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 14:02 117-81-709/13/10 12:30409 112Fluoranthene ND ug/kg 1 09/18/10 14:02 206-44-009/13/10 12:30409 59.5Fluorene ND ug/kg 1 09/18/10 14:02 86-73-709/13/10 12:30409 84.3Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 14:02 87-68-309/13/10 12:30409 70.7Hexachlorobenzene ND ug/kg 1 09/18/10 14:02 118-74-109/13/10 12:30409 52.1Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 14:02 77-47-409/13/10 12:30409 75.7Hexachloroethane ND ug/kg 1 09/18/10 14:02 67-72-109/13/10 12:30409 108Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 14:02 193-39-509/13/10 12:30409 84.3Isophorone ND ug/kg 1 09/18/10 14:02 78-59-109/13/10 12:30409 91.82-Methylnaphthalene ND ug/kg 1 09/18/10 14:02 91-57-609/13/10 12:30409 88.12-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 14:02 95-48-709/13/10 12:30409 1243&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 14:0209/13/10 12:30409 161Naphthalene ND ug/kg 1 09/18/10 14:02 91-20-309/13/10 12:30409 1002-Nitroaniline ND ug/kg 1 09/18/10 14:02 88-74-409/13/10 12:302050 1273-Nitroaniline ND ug/kg 1 09/18/10 14:02 99-09-209/13/10 12:302050 1124-Nitroaniline ND ug/kg 1 09/18/10 14:02 100-01-609/13/10 12:30819 115Nitrobenzene ND ug/kg 1 09/18/10 14:02 98-95-309/13/10 12:30409 1122-Nitrophenol ND ug/kg 1 09/18/10 14:02 88-75-509/13/10 12:30409 99.24-Nitrophenol ND ug/kg 1 09/18/10 14:02 100-02-709/13/10 12:302050 73.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 14:02 621-64-709/13/10 12:30409 78.1N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 14:02 86-30-609/13/10 12:30409 122Pentachlorophenol ND ug/kg 1 09/18/10 14:02 87-86-509/13/10 12:302050 74.4Phenanthrene ND ug/kg 1 09/18/10 14:02 85-01-809/13/10 12:30409 68.2Phenol ND ug/kg 1 09/18/10 14:02 108-95-209/13/10 12:30409 123Pyrene ND ug/kg 1 09/18/10 14:02 129-00-009/13/10 12:30409 69.51,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 14:02 95-94-309/13/10 12:30409 1492,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 14:02 58-90-209/13/10 12:30409 1612,4,5-Trichlorophenol ND ug/kg 1 09/18/10 14:02 95-95-409/13/10 12:30409 1272,4,6-Trichlorophenol ND ug/kg 1 09/18/10 14:02 88-06-209/13/10 12:30409 90.52-Fluorobiphenyl (S) 47 % 1 09/18/10 14:02 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 44 % 1 09/18/10 14:02 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 33 % 1 09/18/10 14:02 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 35 % 1 09/18/10 14:02 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 43 % 1 09/18/10 14:02 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:48 PM Page 65 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 38 % 1 09/18/10 14:02 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:20 57-12-50.13 0.13





Date: 09/27/2010 06:48 PM Page 66 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: SS-110B Lab ID: 9276872002 Collected: 09/01/10 16:15 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "dry-weight" basis



Antimony ND mg/kg 10 09/22/10 18:39 7440-36-0 D309/08/10 15:405.4 3.0Arsenic ND mg/kg 10 09/22/10 18:39 7440-38-2 D309/08/10 15:405.4 3.5Beryllium 1.3 mg/kg 10 09/22/10 18:39 7440-41-709/08/10 15:401.1 0.22Cadmium ND mg/kg 10 09/22/10 18:39 7440-43-9 D309/08/10 15:401.1 0.65Chromium 18.4 mg/kg 10 09/22/10 18:39 7440-47-309/08/10 15:405.4 0.33Copper 0.51J mg/kg 10 09/22/10 18:39 7440-50-8 D309/08/10 15:405.4 0.43Lead ND mg/kg 10 09/22/10 18:39 7439-92-1 D309/08/10 15:405.4 5.2Manganese 221 mg/kg 10 09/22/10 18:39 7439-96-509/08/10 15:405.4 0.33Nickel 14.6 mg/kg 10 09/22/10 18:39 7440-02-009/08/10 15:405.4 2.0Selenium ND mg/kg 10 09/22/10 18:39 7782-49-2 D309/08/10 15:4010.8 4.1Silver ND mg/kg 10 09/22/10 18:39 7440-22-4 D309/08/10 15:405.4 0.33Thallium ND mg/kg 10 09/22/10 18:39 7440-28-0 D309/08/10 15:4010.8 2.8Zinc 84.1 mg/kg 10 09/22/10 18:39 7440-66-609/08/10 15:4010.8 2.8


Mercury 0.0031J mg/kg 1 09/10/10 12:39 7439-97-609/08/10 10:010.0045 0.000089





Date: 09/27/2010 06:48 PM Page 67 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 68 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 37 % 1 09/17/10 18:37 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:22 57-12-50.12 0.12





Date: 09/27/2010 06:48 PM Page 69 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: SS-110C Lab ID: 9276872003 Collected: 09/01/10 16:20 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "dry-weight" basis





Mercury 0.00047J mg/kg 1 09/10/10 12:42 7439-97-609/08/10 10:010.0042 0.000083





Date: 09/27/2010 06:48 PM Page 70 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/17/10 19:15 91-94-109/13/10 12:301970 86.02,4-Dichlorophenol ND ug/kg 1 09/17/10 19:15 120-83-209/13/10 12:30394 86.0Diethylphthalate ND ug/kg 1 09/17/10 19:15 84-66-209/13/10 12:30394 60.92,4-Dimethylphenol ND ug/kg 1 09/17/10 19:15 105-67-909/13/10 12:30394 155Dimethylphthalate ND ug/kg 1 09/17/10 19:15 131-11-309/13/10 12:30394 80.0Di-n-butylphthalate ND ug/kg 1 09/17/10 19:15 84-74-209/13/10 12:30394 64.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/17/10 19:15 534-52-109/13/10 12:30788 78.82,4-Dinitrophenol ND ug/kg 1 09/17/10 19:15 51-28-509/13/10 12:301970 64.52,4-Dinitrotoluene ND ug/kg 1 09/17/10 19:15 121-14-209/13/10 12:30394 74.02,6-Dinitrotoluene ND ug/kg 1 09/17/10 19:15 606-20-209/13/10 12:30394 82.4Di-n-octylphthalate ND ug/kg 1 09/17/10 19:15 117-84-009/13/10 12:30394 82.4bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/17/10 19:15 117-81-709/13/10 12:30394 107Fluoranthene ND ug/kg 1 09/17/10 19:15 206-44-009/13/10 12:30394 57.3Fluorene ND ug/kg 1 09/17/10 19:15 86-73-709/13/10 12:30394 81.2Hexachloro-1,3-butadiene ND ug/kg 1 09/17/10 19:15 87-68-309/13/10 12:30394 68.1Hexachlorobenzene ND ug/kg 1 09/17/10 19:15 118-74-109/13/10 12:30394 50.2Hexachlorocyclopentadiene ND ug/kg 1 09/17/10 19:15 77-47-409/13/10 12:30394 72.8Hexachloroethane ND ug/kg 1 09/17/10 19:15 67-72-109/13/10 12:30394 104Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/17/10 19:15 193-39-509/13/10 12:30394 81.2Isophorone ND ug/kg 1 09/17/10 19:15 78-59-109/13/10 12:30394 88.42-Methylnaphthalene ND ug/kg 1 09/17/10 19:15 91-57-609/13/10 12:30394 84.82-Methylphenol(o-Cresol) ND ug/kg 1 09/17/10 19:15 95-48-709/13/10 12:30394 1193&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/17/10 19:1509/13/10 12:30394 155Naphthalene ND ug/kg 1 09/17/10 19:15 91-20-309/13/10 12:30394 96.72-Nitroaniline ND ug/kg 1 09/17/10 19:15 88-74-409/13/10 12:301970 1223-Nitroaniline ND ug/kg 1 09/17/10 19:15 99-09-209/13/10 12:301970 1074-Nitroaniline ND ug/kg 1 09/17/10 19:15 100-01-609/13/10 12:30788 111Nitrobenzene ND ug/kg 1 09/17/10 19:15 98-95-309/13/10 12:30394 1072-Nitrophenol ND ug/kg 1 09/17/10 19:15 88-75-509/13/10 12:30394 95.54-Nitrophenol ND ug/kg 1 09/17/10 19:15 100-02-709/13/10 12:301970 70.5N-Nitroso-di-n-propylamine ND ug/kg 1 09/17/10 19:15 621-64-709/13/10 12:30394 75.2N-Nitrosodiphenylamine ND ug/kg 1 09/17/10 19:15 86-30-609/13/10 12:30394 117Pentachlorophenol ND ug/kg 1 09/17/10 19:15 87-86-509/13/10 12:301970 71.7Phenanthrene ND ug/kg 1 09/17/10 19:15 85-01-809/13/10 12:30394 65.7Phenol ND ug/kg 1 09/17/10 19:15 108-95-209/13/10 12:30394 118Pyrene ND ug/kg 1 09/17/10 19:15 129-00-009/13/10 12:30394 66.91,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/17/10 19:15 95-94-309/13/10 12:30394 1432,3,4,6-Tetrachlorophenol ND ug/kg 1 09/17/10 19:15 58-90-209/13/10 12:30394 1552,4,5-Trichlorophenol ND ug/kg 1 09/17/10 19:15 95-95-409/13/10 12:30394 1222,4,6-Trichlorophenol ND ug/kg 1 09/17/10 19:15 88-06-209/13/10 12:30394 87.22-Fluorobiphenyl (S) 28 % 1 09/17/10 19:15 321-60-8 S009/13/10 12:3030-110Terphenyl-d14 (S) 51 % 1 09/17/10 19:15 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 22 % 1 09/17/10 19:15 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 24 % 1 09/17/10 19:15 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 36 % 1 09/17/10 19:15 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:48 PM Page 71 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 27 % 1 09/17/10 19:15 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:22 57-12-50.11 0.11





Date: 09/27/2010 06:48 PM Page 72 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: SS-110D Lab ID: 9276872004 Collected: 09/01/10 16:25 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "dry-weight" basis





Mercury 0.00037J mg/kg 1 09/10/10 12:45 7439-97-609/08/10 10:010.0044 0.000088





Date: 09/27/2010 06:48 PM Page 73 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/17/10 19:52 91-94-109/13/10 12:301880 82.02,4-Dichlorophenol ND ug/kg 1 09/17/10 19:52 120-83-209/13/10 12:30376 82.0Diethylphthalate ND ug/kg 1 09/17/10 19:52 84-66-209/13/10 12:30376 58.12,4-Dimethylphenol ND ug/kg 1 09/17/10 19:52 105-67-909/13/10 12:30376 148Dimethylphthalate ND ug/kg 1 09/17/10 19:52 131-11-309/13/10 12:30376 76.3Di-n-butylphthalate ND ug/kg 1 09/17/10 19:52 84-74-209/13/10 12:30376 61.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/17/10 19:52 534-52-109/13/10 12:30751 75.12,4-Dinitrophenol ND ug/kg 1 09/17/10 19:52 51-28-509/13/10 12:301880 61.52,4-Dinitrotoluene ND ug/kg 1 09/17/10 19:52 121-14-209/13/10 12:30376 70.62,6-Dinitrotoluene ND ug/kg 1 09/17/10 19:52 606-20-209/13/10 12:30376 78.5Di-n-octylphthalate ND ug/kg 1 09/17/10 19:52 117-84-009/13/10 12:30376 78.5bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/17/10 19:52 117-81-709/13/10 12:30376 102Fluoranthene ND ug/kg 1 09/17/10 19:52 206-44-009/13/10 12:30376 54.6Fluorene ND ug/kg 1 09/17/10 19:52 86-73-709/13/10 12:30376 77.4Hexachloro-1,3-butadiene ND ug/kg 1 09/17/10 19:52 87-68-309/13/10 12:30376 64.9Hexachlorobenzene ND ug/kg 1 09/17/10 19:52 118-74-109/13/10 12:30376 47.8Hexachlorocyclopentadiene ND ug/kg 1 09/17/10 19:52 77-47-409/13/10 12:30376 69.4Hexachloroethane ND ug/kg 1 09/17/10 19:52 67-72-109/13/10 12:30376 99.0Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/17/10 19:52 193-39-509/13/10 12:30376 77.4Isophorone ND ug/kg 1 09/17/10 19:52 78-59-109/13/10 12:30376 84.22-Methylnaphthalene ND ug/kg 1 09/17/10 19:52 91-57-609/13/10 12:30376 80.82-Methylphenol(o-Cresol) ND ug/kg 1 09/17/10 19:52 95-48-709/13/10 12:30376 1143&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/17/10 19:5209/13/10 12:30376 148Naphthalene ND ug/kg 1 09/17/10 19:52 91-20-309/13/10 12:30376 92.22-Nitroaniline ND ug/kg 1 09/17/10 19:52 88-74-409/13/10 12:301880 1163-Nitroaniline ND ug/kg 1 09/17/10 19:52 99-09-209/13/10 12:301880 1024-Nitroaniline ND ug/kg 1 09/17/10 19:52 100-01-609/13/10 12:30751 106Nitrobenzene ND ug/kg 1 09/17/10 19:52 98-95-309/13/10 12:30376 1022-Nitrophenol ND ug/kg 1 09/17/10 19:52 88-75-509/13/10 12:30376 91.14-Nitrophenol ND ug/kg 1 09/17/10 19:52 100-02-709/13/10 12:301880 67.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/17/10 19:52 621-64-709/13/10 12:30376 71.7N-Nitrosodiphenylamine ND ug/kg 1 09/17/10 19:52 86-30-609/13/10 12:30376 112Pentachlorophenol ND ug/kg 1 09/17/10 19:52 87-86-509/13/10 12:301880 68.3Phenanthrene ND ug/kg 1 09/17/10 19:52 85-01-809/13/10 12:30376 62.6Phenol ND ug/kg 1 09/17/10 19:52 108-95-209/13/10 12:30376 113Pyrene ND ug/kg 1 09/17/10 19:52 129-00-009/13/10 12:30376 63.71,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/17/10 19:52 95-94-309/13/10 12:30376 1372,3,4,6-Tetrachlorophenol ND ug/kg 1 09/17/10 19:52 58-90-209/13/10 12:30376 1482,4,5-Trichlorophenol ND ug/kg 1 09/17/10 19:52 95-95-409/13/10 12:30376 1162,4,6-Trichlorophenol ND ug/kg 1 09/17/10 19:52 88-06-209/13/10 12:30376 83.12-Fluorobiphenyl (S) 32 % 1 09/17/10 19:52 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 49 % 1 09/17/10 19:52 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 27 % 1 09/17/10 19:52 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 28 % 1 09/17/10 19:52 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 38 % 1 09/17/10 19:52 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:48 PM Page 74 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 31 % 1 09/17/10 19:52 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:24 57-12-50.11 0.11





Date: 09/27/2010 06:48 PM Page 75 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: SS-110E Lab ID: 9276872005 Collected: 09/01/10 16:30 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "dry-weight" basis





Mercury 0.0021J mg/kg 1 09/13/10 13:22 7439-97-6 B09/13/10 09:380.0037 0.000075


Acenaphthene ND ug/kg 1 09/18/10 14:38 83-32-909/13/10 12:30370 85.3Acenaphthylene ND ug/kg 1 09/18/10 14:38 208-96-809/13/10 12:30370 87.5Acetophenone ND ug/kg 1 09/18/10 14:38 98-86-209/13/10 12:30370 191Anthracene ND ug/kg 1 09/18/10 14:38 120-12-709/13/10 12:30370 83.0Atrazine ND ug/kg 1 09/18/10 14:38 1912-24-909/13/10 12:30740 146Benzaldehyde ND ug/kg 1 09/18/10 14:38 100-52-709/13/10 12:30740 370Benzo(a)anthracene ND ug/kg 1 09/18/10 14:38 56-55-309/13/10 12:30370 68.4Benzo(a)pyrene ND ug/kg 1 09/18/10 14:38 50-32-809/13/10 12:30370 70.7Benzo(b)fluoranthene ND ug/kg 1 09/18/10 14:38 205-99-209/13/10 12:30370 63.9Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 14:38 191-24-209/13/10 12:30370 94.2Benzo(k)fluoranthene ND ug/kg 1 09/18/10 14:38 207-08-909/13/10 12:30370 72.9Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 14:38 92-52-409/13/10 12:30370 1174-Bromophenylphenyl ether ND ug/kg 1 09/18/10 14:38 101-55-309/13/10 12:30370 67.3Butylbenzylphthalate ND ug/kg 1 09/18/10 14:38 85-68-709/13/10 12:30370 78.5Caprolactam ND ug/kg 1 09/18/10 14:38 105-60-209/13/10 12:30370 63.9Carbazole ND ug/kg 1 09/18/10 14:38 86-74-809/13/10 12:30370 70.74-Chloro-3-methylphenol ND ug/kg 1 09/18/10 14:38 59-50-709/13/10 12:30740 76.34-Chloroaniline ND ug/kg 1 09/18/10 14:38 106-47-809/13/10 12:301850 103bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 14:38 111-91-109/13/10 12:30370 86.4bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 14:38 111-44-409/13/10 12:30370 94.2bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 14:38 108-60-109/13/10 12:30370 98.72-Chloronaphthalene ND ug/kg 1 09/18/10 14:38 91-58-709/13/10 12:30370 72.92-Chlorophenol ND ug/kg 1 09/18/10 14:38 95-57-809/13/10 12:30370 1014-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 14:38 7005-72-309/13/10 12:30370 76.3Chrysene ND ug/kg 1 09/18/10 14:38 218-01-909/13/10 12:30370 49.4Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 14:38 53-70-309/13/10 12:30370 78.5Dibenzofuran ND ug/kg 1 09/18/10 14:38 132-64-909/13/10 12:30370 60.6



Date: 09/27/2010 06:48 PM Page 76 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 14:38 91-94-109/13/10 12:301850 80.82,4-Dichlorophenol ND ug/kg 1 09/18/10 14:38 120-83-209/13/10 12:30370 80.8Diethylphthalate ND ug/kg 1 09/18/10 14:38 84-66-209/13/10 12:30370 57.22,4-Dimethylphenol ND ug/kg 1 09/18/10 14:38 105-67-909/13/10 12:30370 146Dimethylphthalate ND ug/kg 1 09/18/10 14:38 131-11-309/13/10 12:30370 75.2Di-n-butylphthalate ND ug/kg 1 09/18/10 14:38 84-74-209/13/10 12:30370 60.64,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 14:38 534-52-109/13/10 12:30740 74.02,4-Dinitrophenol ND ug/kg 1 09/18/10 14:38 51-28-509/13/10 12:301850 60.62,4-Dinitrotoluene ND ug/kg 1 09/18/10 14:38 121-14-209/13/10 12:30370 69.52,6-Dinitrotoluene ND ug/kg 1 09/18/10 14:38 606-20-209/13/10 12:30370 77.4Di-n-octylphthalate ND ug/kg 1 09/18/10 14:38 117-84-009/13/10 12:30370 77.4bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 14:38 117-81-709/13/10 12:30370 101Fluoranthene ND ug/kg 1 09/18/10 14:38 206-44-009/13/10 12:30370 53.8Fluorene ND ug/kg 1 09/18/10 14:38 86-73-709/13/10 12:30370 76.3Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 14:38 87-68-309/13/10 12:30370 63.9Hexachlorobenzene ND ug/kg 1 09/18/10 14:38 118-74-109/13/10 12:30370 47.1Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 14:38 77-47-409/13/10 12:30370 68.4Hexachloroethane ND ug/kg 1 09/18/10 14:38 67-72-109/13/10 12:30370 97.6Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 14:38 193-39-509/13/10 12:30370 76.3Isophorone ND ug/kg 1 09/18/10 14:38 78-59-109/13/10 12:30370 83.02-Methylnaphthalene ND ug/kg 1 09/18/10 14:38 91-57-609/13/10 12:30370 79.62-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 14:38 95-48-709/13/10 12:30370 1123&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 14:3809/13/10 12:30370 146Naphthalene ND ug/kg 1 09/18/10 14:38 91-20-309/13/10 12:30370 90.92-Nitroaniline ND ug/kg 1 09/18/10 14:38 88-74-409/13/10 12:301850 1143-Nitroaniline ND ug/kg 1 09/18/10 14:38 99-09-209/13/10 12:301850 1014-Nitroaniline ND ug/kg 1 09/18/10 14:38 100-01-609/13/10 12:30740 104Nitrobenzene ND ug/kg 1 09/18/10 14:38 98-95-309/13/10 12:30370 1012-Nitrophenol ND ug/kg 1 09/18/10 14:38 88-75-509/13/10 12:30370 89.74-Nitrophenol ND ug/kg 1 09/18/10 14:38 100-02-709/13/10 12:301850 66.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 14:38 621-64-709/13/10 12:30370 70.7N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 14:38 86-30-609/13/10 12:30370 110Pentachlorophenol ND ug/kg 1 09/18/10 14:38 87-86-509/13/10 12:301850 67.3Phenanthrene ND ug/kg 1 09/18/10 14:38 85-01-809/13/10 12:30370 61.7Phenol ND ug/kg 1 09/18/10 14:38 108-95-209/13/10 12:30370 111Pyrene ND ug/kg 1 09/18/10 14:38 129-00-009/13/10 12:30370 62.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 14:38 95-94-309/13/10 12:30370 1352,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 14:38 58-90-209/13/10 12:30370 1462,4,5-Trichlorophenol ND ug/kg 1 09/18/10 14:38 95-95-409/13/10 12:30370 1142,4,6-Trichlorophenol ND ug/kg 1 09/18/10 14:38 88-06-209/13/10 12:30370 81.92-Fluorobiphenyl (S) 29 % 1 09/18/10 14:38 321-60-8 S009/13/10 12:3030-110Terphenyl-d14 (S) 43 % 1 09/18/10 14:38 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 23 % 1 09/18/10 14:38 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 26 % 1 09/18/10 14:38 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 33 % 1 09/18/10 14:38 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:48 PM Page 77 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/18/10 14:38 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:24 57-12-50.13 0.13





Date: 09/27/2010 06:48 PM Page 78 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 2 09/22/10 18:53 7440-36-0 D309/08/10 15:401.1 0.60Arsenic ND mg/kg 2 09/22/10 18:53 7440-38-2 D309/08/10 15:401.1 0.69Beryllium 0.58 mg/kg 2 09/22/10 18:53 7440-41-709/08/10 15:400.21 0.043Cadmium 0.26 mg/kg 2 09/22/10 18:53 7440-43-909/08/10 15:400.21 0.13Chromium 19.9 mg/kg 2 09/22/10 18:53 7440-47-309/08/10 15:401.1 0.064Copper 5.3 mg/kg 2 09/22/10 18:53 7440-50-809/08/10 15:401.1 0.086Lead 11.8 mg/kg 2 09/22/10 18:53 7439-92-109/08/10 15:401.1 1.0Manganese 134 mg/kg 2 09/22/10 18:53 7439-96-509/08/10 15:401.1 0.064Nickel 6.1 mg/kg 2 09/22/10 18:53 7440-02-009/08/10 15:401.1 0.39Selenium ND mg/kg 2 09/22/10 18:53 7782-49-2 D309/08/10 15:402.1 0.81Silver ND mg/kg 2 09/22/10 18:53 7440-22-4 D309/08/10 15:401.1 0.064Thallium ND mg/kg 2 09/22/10 18:53 7440-28-0 D309/08/10 15:402.1 0.56Zinc 25.1 mg/kg 2 09/22/10 18:53 7440-66-609/08/10 15:402.1 0.56


Mercury 0.069 mg/kg 1 09/13/10 14:04 7439-97-6 B09/13/10 09:380.0030 0.000060


Acenaphthene ND ug/kg 1 09/18/10 15:15 83-32-909/13/10 12:30431 99.3Acenaphthylene ND ug/kg 1 09/18/10 15:15 208-96-809/13/10 12:30431 102Acetophenone ND ug/kg 1 09/18/10 15:15 98-86-209/13/10 12:30431 222Anthracene ND ug/kg 1 09/18/10 15:15 120-12-709/13/10 12:30431 96.7Atrazine ND ug/kg 1 09/18/10 15:15 1912-24-909/13/10 12:30862 170Benzaldehyde ND ug/kg 1 09/18/10 15:15 100-52-709/13/10 12:30862 431Benzo(a)anthracene ND ug/kg 1 09/18/10 15:15 56-55-309/13/10 12:30431 79.7Benzo(a)pyrene ND ug/kg 1 09/18/10 15:15 50-32-809/13/10 12:30431 82.3Benzo(b)fluoranthene ND ug/kg 1 09/18/10 15:15 205-99-209/13/10 12:30431 74.5Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 15:15 191-24-209/13/10 12:30431 110Benzo(k)fluoranthene ND ug/kg 1 09/18/10 15:15 207-08-909/13/10 12:30431 84.9Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 15:15 92-52-409/13/10 12:30431 1364-Bromophenylphenyl ether ND ug/kg 1 09/18/10 15:15 101-55-309/13/10 12:30431 78.4Butylbenzylphthalate ND ug/kg 1 09/18/10 15:15 85-68-709/13/10 12:30431 91.4Caprolactam ND ug/kg 1 09/18/10 15:15 105-60-209/13/10 12:30431 74.5Carbazole ND ug/kg 1 09/18/10 15:15 86-74-809/13/10 12:30431 82.34-Chloro-3-methylphenol ND ug/kg 1 09/18/10 15:15 59-50-709/13/10 12:30862 88.84-Chloroaniline ND ug/kg 1 09/18/10 15:15 106-47-809/13/10 12:302160 120bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 15:15 111-91-109/13/10 12:30431 101bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 15:15 111-44-409/13/10 12:30431 110bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 15:15 108-60-109/13/10 12:30431 1152-Chloronaphthalene ND ug/kg 1 09/18/10 15:15 91-58-709/13/10 12:30431 84.92-Chlorophenol ND ug/kg 1 09/18/10 15:15 95-57-809/13/10 12:30431 1184-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 15:15 7005-72-309/13/10 12:30431 88.8Chrysene ND ug/kg 1 09/18/10 15:15 218-01-909/13/10 12:30431 57.5Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 15:15 53-70-309/13/10 12:30431 91.4Dibenzofuran ND ug/kg 1 09/18/10 15:15 132-64-909/13/10 12:30431 70.5



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 15:15 91-94-109/13/10 12:302160 94.02,4-Dichlorophenol ND ug/kg 1 09/18/10 15:15 120-83-209/13/10 12:30431 94.0Diethylphthalate ND ug/kg 1 09/18/10 15:15 84-66-209/13/10 12:30431 66.62,4-Dimethylphenol ND ug/kg 1 09/18/10 15:15 105-67-909/13/10 12:30431 170Dimethylphthalate ND ug/kg 1 09/18/10 15:15 131-11-309/13/10 12:30431 87.5Di-n-butylphthalate ND ug/kg 1 09/18/10 15:15 84-74-209/13/10 12:30431 70.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 15:15 534-52-109/13/10 12:30862 86.22,4-Dinitrophenol ND ug/kg 1 09/18/10 15:15 51-28-509/13/10 12:302160 70.52,4-Dinitrotoluene ND ug/kg 1 09/18/10 15:15 121-14-209/13/10 12:30431 81.02,6-Dinitrotoluene ND ug/kg 1 09/18/10 15:15 606-20-209/13/10 12:30431 90.1Di-n-octylphthalate ND ug/kg 1 09/18/10 15:15 117-84-009/13/10 12:30431 90.1bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 15:15 117-81-709/13/10 12:30431 118Fluoranthene ND ug/kg 1 09/18/10 15:15 206-44-009/13/10 12:30431 62.7Fluorene ND ug/kg 1 09/18/10 15:15 86-73-709/13/10 12:30431 88.8Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 15:15 87-68-309/13/10 12:30431 74.5Hexachlorobenzene ND ug/kg 1 09/18/10 15:15 118-74-109/13/10 12:30431 54.9Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 15:15 77-47-409/13/10 12:30431 79.7Hexachloroethane ND ug/kg 1 09/18/10 15:15 67-72-109/13/10 12:30431 114Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 15:15 193-39-509/13/10 12:30431 88.8Isophorone ND ug/kg 1 09/18/10 15:15 78-59-109/13/10 12:30431 96.72-Methylnaphthalene ND ug/kg 1 09/18/10 15:15 91-57-609/13/10 12:30431 92.72-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 15:15 95-48-709/13/10 12:30431 1313&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 15:1509/13/10 12:30431 170Naphthalene ND ug/kg 1 09/18/10 15:15 91-20-309/13/10 12:30431 1062-Nitroaniline ND ug/kg 1 09/18/10 15:15 88-74-409/13/10 12:302160 1333-Nitroaniline ND ug/kg 1 09/18/10 15:15 99-09-209/13/10 12:302160 1184-Nitroaniline ND ug/kg 1 09/18/10 15:15 100-01-609/13/10 12:30862 121Nitrobenzene ND ug/kg 1 09/18/10 15:15 98-95-309/13/10 12:30431 1182-Nitrophenol ND ug/kg 1 09/18/10 15:15 88-75-509/13/10 12:30431 1044-Nitrophenol ND ug/kg 1 09/18/10 15:15 100-02-709/13/10 12:302160 77.1N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 15:15 621-64-709/13/10 12:30431 82.3N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 15:15 86-30-609/13/10 12:30431 128Pentachlorophenol ND ug/kg 1 09/18/10 15:15 87-86-509/13/10 12:302160 78.4Phenanthrene ND ug/kg 1 09/18/10 15:15 85-01-809/13/10 12:30431 71.8Phenol ND ug/kg 1 09/18/10 15:15 108-95-209/13/10 12:30431 129Pyrene ND ug/kg 1 09/18/10 15:15 129-00-009/13/10 12:30431 73.11,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 15:15 95-94-309/13/10 12:30431 1572,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 15:15 58-90-209/13/10 12:30431 1702,4,5-Trichlorophenol ND ug/kg 1 09/18/10 15:15 95-95-409/13/10 12:30431 1332,4,6-Trichlorophenol ND ug/kg 1 09/18/10 15:15 88-06-209/13/10 12:30431 95.42-Fluorobiphenyl (S) 36 % 1 09/18/10 15:15 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 46 % 1 09/18/10 15:15 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 27 % 1 09/18/10 15:15 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 32 % 1 09/18/10 15:15 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 37 % 1 09/18/10 15:15 118-79-609/13/10 12:3027-110



Date: 09/27/2010 06:48 PM Page 80 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 33 % 1 09/18/10 15:15 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:26 57-12-50.16 0.16





Date: 09/27/2010 06:48 PM Page 81 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/21/10 11:08 83-32-909/15/10 13:00380 87.4Acenaphthylene ND ug/kg 1 09/21/10 11:08 208-96-809/15/10 13:00380 89.7Acetophenone ND ug/kg 1 09/21/10 11:08 98-86-209/15/10 13:00380 196Anthracene ND ug/kg 1 09/21/10 11:08 120-12-709/15/10 13:00380 85.1Atrazine ND ug/kg 1 09/21/10 11:08 1912-24-909/15/10 13:00759 150Benzaldehyde ND ug/kg 1 09/21/10 11:08 100-52-709/15/10 13:00759 380Benzo(a)anthracene ND ug/kg 1 09/21/10 11:08 56-55-309/15/10 13:00380 70.2Benzo(a)pyrene ND ug/kg 1 09/21/10 11:08 50-32-809/15/10 13:00380 72.5Benzo(b)fluoranthene ND ug/kg 1 09/21/10 11:08 205-99-209/15/10 13:00380 65.6Benzo(g,h,i)perylene ND ug/kg 1 09/21/10 11:08 191-24-209/15/10 13:00380 96.6Benzo(k)fluoranthene ND ug/kg 1 09/21/10 11:08 207-08-909/15/10 13:00380 74.8Biphenyl (Diphenyl) ND ug/kg 1 09/21/10 11:08 92-52-409/15/10 13:00380 1204-Bromophenylphenyl ether ND ug/kg 1 09/21/10 11:08 101-55-309/15/10 13:00380 69.0Butylbenzylphthalate ND ug/kg 1 09/21/10 11:08 85-68-709/15/10 13:00380 80.5Caprolactam ND ug/kg 1 09/21/10 11:08 105-60-209/15/10 13:00380 65.6Carbazole ND ug/kg 1 09/21/10 11:08 86-74-809/15/10 13:00380 72.54-Chloro-3-methylphenol ND ug/kg 1 09/21/10 11:08 59-50-709/15/10 13:00759 78.24-Chloroaniline ND ug/kg 1 09/21/10 11:08 106-47-809/15/10 13:001900 106bis(2-Chloroethoxy)methane ND ug/kg 1 09/21/10 11:08 111-91-109/15/10 13:00380 88.6bis(2-Chloroethyl) ether ND ug/kg 1 09/21/10 11:08 111-44-409/15/10 13:00380 96.6bis(2-Chloroisopropyl) ether ND ug/kg 1 09/21/10 11:08 108-60-109/15/10 13:00380 1012-Chloronaphthalene ND ug/kg 1 09/21/10 11:08 91-58-709/15/10 13:00380 74.82-Chlorophenol ND ug/kg 1 09/21/10 11:08 95-57-809/15/10 13:00380 1044-Chlorophenylphenyl ether ND ug/kg 1 09/21/10 11:08 7005-72-309/15/10 13:00380 78.2Chrysene ND ug/kg 1 09/21/10 11:08 218-01-909/15/10 13:00380 50.6Dibenz(a,h)anthracene ND ug/kg 1 09/21/10 11:08 53-70-309/15/10 13:00380 80.5Dibenzofuran ND ug/kg 1 09/21/10 11:08 132-64-909/15/10 13:00380 62.13,3'-Dichlorobenzidine ND ug/kg 1 09/21/10 11:08 91-94-109/15/10 13:001900 82.82,4-Dichlorophenol ND ug/kg 1 09/21/10 11:08 120-83-209/15/10 13:00380 82.8Diethylphthalate ND ug/kg 1 09/21/10 11:08 84-66-209/15/10 13:00380 58.72,4-Dimethylphenol ND ug/kg 1 09/21/10 11:08 105-67-909/15/10 13:00380 150Dimethylphthalate ND ug/kg 1 09/21/10 11:08 131-11-309/15/10 13:00380 77.1Di-n-butylphthalate ND ug/kg 1 09/21/10 11:08 84-74-209/15/10 13:00380 62.14,6-Dinitro-2-methylphenol ND ug/kg 1 09/21/10 11:08 534-52-109/15/10 13:00759 75.92,4-Dinitrophenol ND ug/kg 1 09/21/10 11:08 51-28-509/15/10 13:001900 62.12,4-Dinitrotoluene ND ug/kg 1 09/21/10 11:08 121-14-209/15/10 13:00380 71.32,6-Dinitrotoluene ND ug/kg 1 09/21/10 11:08 606-20-209/15/10 13:00380 79.4Di-n-octylphthalate ND ug/kg 1 09/21/10 11:08 117-84-009/15/10 13:00380 79.4bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/21/10 11:08 117-81-709/15/10 13:00380 104Fluoranthene ND ug/kg 1 09/21/10 11:08 206-44-009/15/10 13:00380 55.2Fluorene ND ug/kg 1 09/21/10 11:08 86-73-709/15/10 13:00380 78.2Hexachloro-1,3-butadiene ND ug/kg 1 09/21/10 11:08 87-68-309/15/10 13:00380 65.6Hexachlorobenzene ND ug/kg 1 09/21/10 11:08 118-74-109/15/10 13:00380 48.3Hexachlorocyclopentadiene ND ug/kg 1 09/21/10 11:08 77-47-409/15/10 13:00380 70.2Hexachloroethane ND ug/kg 1 09/21/10 11:08 67-72-109/15/10 13:00380 100



Date: 09/27/2010 06:48 PM Page 82 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/21/10 11:08 193-39-509/15/10 13:00380 78.2Isophorone ND ug/kg 1 09/21/10 11:08 78-59-109/15/10 13:00380 85.12-Methylnaphthalene ND ug/kg 1 09/21/10 11:08 91-57-609/15/10 13:00380 81.72-Methylphenol(o-Cresol) ND ug/kg 1 09/21/10 11:08 95-48-709/15/10 13:00380 1153&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/21/10 11:0809/15/10 13:00380 150Naphthalene ND ug/kg 1 09/21/10 11:08 91-20-309/15/10 13:00380 93.22-Nitroaniline ND ug/kg 1 09/21/10 11:08 88-74-409/15/10 13:001900 1173-Nitroaniline ND ug/kg 1 09/21/10 11:08 99-09-209/15/10 13:001900 1044-Nitroaniline ND ug/kg 1 09/21/10 11:08 100-01-609/15/10 13:00759 107Nitrobenzene ND ug/kg 1 09/21/10 11:08 98-95-309/15/10 13:00380 1042-Nitrophenol ND ug/kg 1 09/21/10 11:08 88-75-509/15/10 13:00380 92.04-Nitrophenol ND ug/kg 1 09/21/10 11:08 100-02-709/15/10 13:001900 67.9N-Nitroso-di-n-propylamine ND ug/kg 1 09/21/10 11:08 621-64-709/15/10 13:00380 72.5N-Nitrosodiphenylamine ND ug/kg 1 09/21/10 11:08 86-30-609/15/10 13:00380 113Pentachlorophenol ND ug/kg 1 09/21/10 11:08 87-86-509/15/10 13:001900 69.0Phenanthrene ND ug/kg 1 09/21/10 11:08 85-01-809/15/10 13:00380 63.3Phenol ND ug/kg 1 09/21/10 11:08 108-95-209/15/10 13:00380 114Pyrene ND ug/kg 1 09/21/10 11:08 129-00-009/15/10 13:00380 64.41,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/21/10 11:08 95-94-309/15/10 13:00380 1382,3,4,6-Tetrachlorophenol ND ug/kg 1 09/21/10 11:08 58-90-209/15/10 13:00380 1502,4,5-Trichlorophenol ND ug/kg 1 09/21/10 11:08 95-95-409/15/10 13:00380 1172,4,6-Trichlorophenol ND ug/kg 1 09/21/10 11:08 88-06-209/15/10 13:00380 84.02-Fluorobiphenyl (S) 29 % 1 09/21/10 11:08 321-60-8 S009/15/10 13:0030-110Terphenyl-d14 (S) 39 % 1 09/21/10 11:08 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 17 % 1 09/21/10 11:08 13127-88-3 S009/15/10 13:0022-1102-Fluorophenol (S) 20 % 1 09/21/10 11:08 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 31 % 1 09/21/10 11:08 118-79-609/15/10 13:0027-110Nitrobenzene-d5 (S) 23 % 1 09/21/10 11:08 4165-60-009/15/10 13:0023-110





Date: 09/27/2010 06:48 PM Page 83 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.0031J mg/kg 1 09/15/10 11:59 7439-97-609/14/10 08:110.0052 0.00010




Cyanide ND mg/kg 1 09/12/10 16:26 57-12-50.11 0.11





Date: 09/27/2010 06:48 PM Page 84 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.0011J mg/kg 1 09/15/10 12:01 7439-97-609/14/10 08:110.0046 0.000093





Date: 09/27/2010 06:48 PM Page 85 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/18/10 15:51 83-32-909/13/10 12:30368 84.8Acenaphthylene ND ug/kg 1 09/18/10 15:51 208-96-809/13/10 12:30368 87.1Acetophenone ND ug/kg 1 09/18/10 15:51 98-86-209/13/10 12:30368 190Anthracene ND ug/kg 1 09/18/10 15:51 120-12-709/13/10 12:30368 82.6Atrazine ND ug/kg 1 09/18/10 15:51 1912-24-909/13/10 12:30737 145Benzaldehyde ND ug/kg 1 09/18/10 15:51 100-52-709/13/10 12:30737 368Benzo(a)anthracene ND ug/kg 1 09/18/10 15:51 56-55-309/13/10 12:30368 68.1Benzo(a)pyrene ND ug/kg 1 09/18/10 15:51 50-32-809/13/10 12:30368 70.3Benzo(b)fluoranthene ND ug/kg 1 09/18/10 15:51 205-99-209/13/10 12:30368 63.6Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 15:51 191-24-209/13/10 12:30368 93.8Benzo(k)fluoranthene ND ug/kg 1 09/18/10 15:51 207-08-909/13/10 12:30368 72.5Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 15:51 92-52-409/13/10 12:30368 1164-Bromophenylphenyl ether ND ug/kg 1 09/18/10 15:51 101-55-309/13/10 12:30368 67.0Butylbenzylphthalate ND ug/kg 1 09/18/10 15:51 85-68-709/13/10 12:30368 78.1Caprolactam ND ug/kg 1 09/18/10 15:51 105-60-209/13/10 12:30368 63.6Carbazole ND ug/kg 1 09/18/10 15:51 86-74-809/13/10 12:30368 70.34-Chloro-3-methylphenol ND ug/kg 1 09/18/10 15:51 59-50-709/13/10 12:30737 75.94-Chloroaniline ND ug/kg 1 09/18/10 15:51 106-47-809/13/10 12:301840 103bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 15:51 111-91-109/13/10 12:30368 85.9bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 15:51 111-44-409/13/10 12:30368 93.8bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 15:51 108-60-109/13/10 12:30368 98.22-Chloronaphthalene ND ug/kg 1 09/18/10 15:51 91-58-709/13/10 12:30368 72.52-Chlorophenol ND ug/kg 1 09/18/10 15:51 95-57-809/13/10 12:30368 1004-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 15:51 7005-72-309/13/10 12:30368 75.9Chrysene ND ug/kg 1 09/18/10 15:51 218-01-909/13/10 12:30368 49.1Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 15:51 53-70-309/13/10 12:30368 78.1Dibenzofuran ND ug/kg 1 09/18/10 15:51 132-64-909/13/10 12:30368 60.33,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 15:51 91-94-109/13/10 12:301840 80.42,4-Dichlorophenol ND ug/kg 1 09/18/10 15:51 120-83-209/13/10 12:30368 80.4Diethylphthalate ND ug/kg 1 09/18/10 15:51 84-66-209/13/10 12:30368 56.92,4-Dimethylphenol ND ug/kg 1 09/18/10 15:51 105-67-909/13/10 12:30368 145Dimethylphthalate ND ug/kg 1 09/18/10 15:51 131-11-309/13/10 12:30368 74.8Di-n-butylphthalate ND ug/kg 1 09/18/10 15:51 84-74-209/13/10 12:30368 60.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 15:51 534-52-109/13/10 12:30737 73.72,4-Dinitrophenol ND ug/kg 1 09/18/10 15:51 51-28-509/13/10 12:301840 60.32,4-Dinitrotoluene ND ug/kg 1 09/18/10 15:51 121-14-209/13/10 12:30368 69.22,6-Dinitrotoluene ND ug/kg 1 09/18/10 15:51 606-20-209/13/10 12:30368 77.0Di-n-octylphthalate ND ug/kg 1 09/18/10 15:51 117-84-009/13/10 12:30368 77.0bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 15:51 117-81-709/13/10 12:30368 100Fluoranthene ND ug/kg 1 09/18/10 15:51 206-44-009/13/10 12:30368 53.6Fluorene ND ug/kg 1 09/18/10 15:51 86-73-709/13/10 12:30368 75.9Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 15:51 87-68-309/13/10 12:30368 63.6Hexachlorobenzene ND ug/kg 1 09/18/10 15:51 118-74-109/13/10 12:30368 46.9Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 15:51 77-47-409/13/10 12:30368 68.1Hexachloroethane ND ug/kg 1 09/18/10 15:51 67-72-109/13/10 12:30368 97.1



Date: 09/27/2010 06:48 PM Page 86 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 15:51 193-39-509/13/10 12:30368 75.9Isophorone ND ug/kg 1 09/18/10 15:51 78-59-109/13/10 12:30368 82.62-Methylnaphthalene ND ug/kg 1 09/18/10 15:51 91-57-609/13/10 12:30368 79.22-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 15:51 95-48-709/13/10 12:30368 1123&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 15:5109/13/10 12:30368 145Naphthalene ND ug/kg 1 09/18/10 15:51 91-20-309/13/10 12:30368 90.42-Nitroaniline ND ug/kg 1 09/18/10 15:51 88-74-409/13/10 12:301840 1143-Nitroaniline ND ug/kg 1 09/18/10 15:51 99-09-209/13/10 12:301840 1004-Nitroaniline ND ug/kg 1 09/18/10 15:51 100-01-609/13/10 12:30737 104Nitrobenzene ND ug/kg 1 09/18/10 15:51 98-95-309/13/10 12:30368 1002-Nitrophenol ND ug/kg 1 09/18/10 15:51 88-75-509/13/10 12:30368 89.34-Nitrophenol ND ug/kg 1 09/18/10 15:51 100-02-709/13/10 12:301840 65.9N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 15:51 621-64-709/13/10 12:30368 70.3N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 15:51 86-30-609/13/10 12:30368 109Pentachlorophenol ND ug/kg 1 09/18/10 15:51 87-86-509/13/10 12:301840 67.0Phenanthrene ND ug/kg 1 09/18/10 15:51 85-01-809/13/10 12:30368 61.4Phenol ND ug/kg 1 09/18/10 15:51 108-95-209/13/10 12:30368 110Pyrene ND ug/kg 1 09/18/10 15:51 129-00-009/13/10 12:30368 62.51,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 15:51 95-94-309/13/10 12:30368 1342,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 15:51 58-90-209/13/10 12:30368 1452,4,5-Trichlorophenol ND ug/kg 1 09/18/10 15:51 95-95-409/13/10 12:30368 1142,4,6-Trichlorophenol ND ug/kg 1 09/18/10 15:51 88-06-209/13/10 12:30368 81.52-Fluorobiphenyl (S) 42 % 1 09/18/10 15:51 321-60-809/13/10 12:3030-110Terphenyl-d14 (S) 48 % 1 09/18/10 15:51 1718-51-009/13/10 12:3028-110Phenol-d6 (S) 32 % 1 09/18/10 15:51 13127-88-309/13/10 12:3022-1102-Fluorophenol (S) 37 % 1 09/18/10 15:51 367-12-409/13/10 12:3013-1102,4,6-Tribromophenol (S) 41 % 1 09/18/10 15:51 118-79-609/13/10 12:3027-110Nitrobenzene-d5 (S) 40 % 1 09/18/10 15:51 4165-60-009/13/10 12:3023-110




Cyanide ND mg/kg 1 09/12/10 16:27 57-12-50.11 0.11





Date: 09/27/2010 06:48 PM Page 87 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Cyanide ND mg/kg 1 09/12/10 16:29 57-12-50.11 0.11



Date: 09/27/2010 06:48 PM Page 88 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 19:20 7440-36-0 D309/08/10 15:404.0 2.3Arsenic 4.0 mg/kg 10 09/22/10 19:20 7440-38-209/08/10 15:404.0 2.6Beryllium 1.2 mg/kg 10 09/22/10 19:20 7440-41-709/08/10 15:400.81 0.16Cadmium ND mg/kg 10 09/22/10 19:20 7440-43-9 D309/08/10 15:400.81 0.48Chromium 16.4 mg/kg 10 09/22/10 19:20 7440-47-309/08/10 15:404.0 0.24Copper 13.5 mg/kg 10 09/22/10 19:20 7440-50-809/08/10 15:404.0 0.32Lead 4.0 mg/kg 10 09/22/10 19:20 7439-92-1 D309/08/10 15:404.0 3.9Manganese 304 mg/kg 10 09/22/10 19:20 7439-96-509/08/10 15:404.0 0.24Nickel 12.3 mg/kg 10 09/22/10 19:20 7440-02-009/08/10 15:404.0 1.5Selenium ND mg/kg 10 09/22/10 19:20 7782-49-2 D309/08/10 15:408.1 3.1Silver ND mg/kg 10 09/22/10 19:20 7440-22-4 D309/08/10 15:404.0 0.24Thallium 2.4J mg/kg 10 09/22/10 19:20 7440-28-0 D309/08/10 15:408.1 2.1Zinc 88.8 mg/kg 10 09/22/10 19:20 7440-66-609/08/10 15:408.1 2.1


Mercury 0.00066J mg/kg 1 09/15/10 12:09 7439-97-609/14/10 08:110.0041 0.000083





Date: 09/27/2010 06:48 PM Page 89 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 90 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 43 % 1 09/18/10 17:41 4165-60-009/13/10 18:3023-110







Date: 09/27/2010 06:48 PM Page 91 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744









Date: 09/27/2010 06:48 PM Page 92 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury ND mg/kg 1 09/15/10 12:15 7439-97-609/14/10 08:110.0053 0.00011





Date: 09/27/2010 06:48 PM Page 93 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 94 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 41 % 1 09/18/10 18:18 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:33 57-12-50.11 0.11



Date: 09/27/2010 06:48 PM Page 95 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 5 09/22/10 19:27 7440-36-0 D309/08/10 15:401.9 1.1Arsenic 1.4J mg/kg 5 09/22/10 19:27 7440-38-2 D309/08/10 15:401.9 1.2Beryllium 0.95 mg/kg 5 09/22/10 19:27 7440-41-709/08/10 15:400.38 0.077Cadmium ND mg/kg 5 09/22/10 19:27 7440-43-9 D309/08/10 15:400.38 0.23Chromium 16.7 mg/kg 5 09/22/10 19:27 7440-47-309/08/10 15:401.9 0.11Copper 12.4 mg/kg 5 09/22/10 19:27 7440-50-809/08/10 15:401.9 0.15Lead 7.8 mg/kg 5 09/22/10 19:27 7439-92-109/08/10 15:401.9 1.8Manganese 306 mg/kg 5 09/22/10 19:27 7439-96-509/08/10 15:401.9 0.11Nickel 9.1 mg/kg 5 09/22/10 19:27 7440-02-009/08/10 15:401.9 0.69Selenium ND mg/kg 5 09/22/10 19:27 7782-49-2 D309/08/10 15:403.8 1.5Silver 0.14J mg/kg 5 09/22/10 19:27 7440-22-4 D309/08/10 15:401.9 0.11Thallium ND mg/kg 5 09/22/10 19:27 7440-28-0 D309/08/10 15:403.8 1.0Zinc 47.8 mg/kg 5 09/22/10 19:27 7440-66-609/08/10 15:403.8 1.0


Mercury 0.022 mg/kg 1 09/15/10 12:18 7439-97-609/14/10 08:110.0046 0.000092


Acenaphthene ND ug/kg 1 09/18/10 18:54 83-32-909/13/10 18:30364 83.8Acenaphthylene ND ug/kg 1 09/18/10 18:54 208-96-809/13/10 18:30364 86.0Acetophenone ND ug/kg 1 09/18/10 18:54 98-86-209/13/10 18:30364 187Anthracene ND ug/kg 1 09/18/10 18:54 120-12-709/13/10 18:30364 81.6Atrazine ND ug/kg 1 09/18/10 18:54 1912-24-909/13/10 18:30728 143Benzaldehyde ND ug/kg 1 09/18/10 18:54 100-52-709/13/10 18:30728 364Benzo(a)anthracene ND ug/kg 1 09/18/10 18:54 56-55-309/13/10 18:30364 67.2Benzo(a)pyrene ND ug/kg 1 09/18/10 18:54 50-32-809/13/10 18:30364 69.5Benzo(b)fluoranthene ND ug/kg 1 09/18/10 18:54 205-99-209/13/10 18:30364 62.8Benzo(g,h,i)perylene ND ug/kg 1 09/18/10 18:54 191-24-209/13/10 18:30364 92.6Benzo(k)fluoranthene ND ug/kg 1 09/18/10 18:54 207-08-909/13/10 18:30364 71.7Biphenyl (Diphenyl) ND ug/kg 1 09/18/10 18:54 92-52-409/13/10 18:30364 1154-Bromophenylphenyl ether ND ug/kg 1 09/18/10 18:54 101-55-309/13/10 18:30364 66.1Butylbenzylphthalate ND ug/kg 1 09/18/10 18:54 85-68-709/13/10 18:30364 77.2Caprolactam ND ug/kg 1 09/18/10 18:54 105-60-209/13/10 18:30364 62.8Carbazole ND ug/kg 1 09/18/10 18:54 86-74-809/13/10 18:30364 69.54-Chloro-3-methylphenol ND ug/kg 1 09/18/10 18:54 59-50-709/13/10 18:30728 75.04-Chloroaniline ND ug/kg 1 09/18/10 18:54 106-47-809/13/10 18:301820 101bis(2-Chloroethoxy)methane ND ug/kg 1 09/18/10 18:54 111-91-109/13/10 18:30364 84.9bis(2-Chloroethyl) ether ND ug/kg 1 09/18/10 18:54 111-44-409/13/10 18:30364 92.6bis(2-Chloroisopropyl) ether ND ug/kg 1 09/18/10 18:54 108-60-109/13/10 18:30364 97.02-Chloronaphthalene ND ug/kg 1 09/18/10 18:54 91-58-709/13/10 18:30364 71.72-Chlorophenol ND ug/kg 1 09/18/10 18:54 95-57-809/13/10 18:30364 99.24-Chlorophenylphenyl ether ND ug/kg 1 09/18/10 18:54 7005-72-309/13/10 18:30364 75.0Chrysene ND ug/kg 1 09/18/10 18:54 218-01-909/13/10 18:30364 48.5Dibenz(a,h)anthracene ND ug/kg 1 09/18/10 18:54 53-70-309/13/10 18:30364 77.2Dibenzofuran ND ug/kg 1 09/18/10 18:54 132-64-909/13/10 18:30364 59.5



Date: 09/27/2010 06:48 PM Page 96 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 18:54 91-94-109/13/10 18:301820 79.42,4-Dichlorophenol ND ug/kg 1 09/18/10 18:54 120-83-209/13/10 18:30364 79.4Diethylphthalate ND ug/kg 1 09/18/10 18:54 84-66-209/13/10 18:30364 56.22,4-Dimethylphenol ND ug/kg 1 09/18/10 18:54 105-67-909/13/10 18:30364 143Dimethylphthalate ND ug/kg 1 09/18/10 18:54 131-11-309/13/10 18:30364 73.9Di-n-butylphthalate ND ug/kg 1 09/18/10 18:54 84-74-209/13/10 18:30364 59.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 18:54 534-52-109/13/10 18:30728 72.82,4-Dinitrophenol ND ug/kg 1 09/18/10 18:54 51-28-509/13/10 18:301820 59.52,4-Dinitrotoluene ND ug/kg 1 09/18/10 18:54 121-14-209/13/10 18:30364 68.32,6-Dinitrotoluene ND ug/kg 1 09/18/10 18:54 606-20-209/13/10 18:30364 76.1Di-n-octylphthalate ND ug/kg 1 09/18/10 18:54 117-84-009/13/10 18:30364 76.1bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 18:54 117-81-709/13/10 18:30364 99.2Fluoranthene ND ug/kg 1 09/18/10 18:54 206-44-009/13/10 18:30364 52.9Fluorene ND ug/kg 1 09/18/10 18:54 86-73-709/13/10 18:30364 75.0Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 18:54 87-68-309/13/10 18:30364 62.8Hexachlorobenzene ND ug/kg 1 09/18/10 18:54 118-74-109/13/10 18:30364 46.3Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 18:54 77-47-409/13/10 18:30364 67.2Hexachloroethane ND ug/kg 1 09/18/10 18:54 67-72-109/13/10 18:30364 95.9Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 18:54 193-39-509/13/10 18:30364 75.0Isophorone ND ug/kg 1 09/18/10 18:54 78-59-109/13/10 18:30364 81.62-Methylnaphthalene ND ug/kg 1 09/18/10 18:54 91-57-609/13/10 18:30364 78.32-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 18:54 95-48-709/13/10 18:30364 1103&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 18:5409/13/10 18:30364 143Naphthalene ND ug/kg 1 09/18/10 18:54 91-20-309/13/10 18:30364 89.32-Nitroaniline ND ug/kg 1 09/18/10 18:54 88-74-409/13/10 18:301820 1123-Nitroaniline ND ug/kg 1 09/18/10 18:54 99-09-209/13/10 18:301820 99.24-Nitroaniline ND ug/kg 1 09/18/10 18:54 100-01-609/13/10 18:30728 103Nitrobenzene ND ug/kg 1 09/18/10 18:54 98-95-309/13/10 18:30364 99.22-Nitrophenol ND ug/kg 1 09/18/10 18:54 88-75-509/13/10 18:30364 88.24-Nitrophenol ND ug/kg 1 09/18/10 18:54 100-02-709/13/10 18:301820 65.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 18:54 621-64-709/13/10 18:30364 69.5N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 18:54 86-30-609/13/10 18:30364 108Pentachlorophenol ND ug/kg 1 09/18/10 18:54 87-86-509/13/10 18:301820 66.1Phenanthrene ND ug/kg 1 09/18/10 18:54 85-01-809/13/10 18:30364 60.6Phenol ND ug/kg 1 09/18/10 18:54 108-95-209/13/10 18:30364 109Pyrene ND ug/kg 1 09/18/10 18:54 129-00-009/13/10 18:30364 61.71,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 18:54 95-94-309/13/10 18:30364 1322,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 18:54 58-90-209/13/10 18:30364 1432,4,5-Trichlorophenol ND ug/kg 1 09/18/10 18:54 95-95-409/13/10 18:30364 1122,4,6-Trichlorophenol ND ug/kg 1 09/18/10 18:54 88-06-209/13/10 18:30364 80.52-Fluorobiphenyl (S) 44 % 1 09/18/10 18:54 321-60-809/13/10 18:3030-110Terphenyl-d14 (S) 44 % 1 09/18/10 18:54 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 23 % 1 09/18/10 18:54 13127-88-309/13/10 18:3022-1102-Fluorophenol (S) 26 % 1 09/18/10 18:54 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 30 % 1 09/18/10 18:54 118-79-609/13/10 18:3027-110



Date: 09/27/2010 06:48 PM Page 97 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 36 % 1 09/18/10 18:54 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:33 57-12-50.12 0.12





Date: 09/27/2010 06:48 PM Page 98 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 19:30 7440-36-0 D309/08/10 15:403.8 2.1Arsenic ND mg/kg 10 09/22/10 19:30 7440-38-2 D309/08/10 15:403.8 2.4Beryllium 1.4 mg/kg 10 09/22/10 19:30 7440-41-709/08/10 15:400.76 0.15Cadmium ND mg/kg 10 09/22/10 19:30 7440-43-9 D309/08/10 15:400.76 0.46Chromium 20.2 mg/kg 10 09/22/10 19:30 7440-47-309/08/10 15:403.8 0.23Copper 8.5 mg/kg 10 09/22/10 19:30 7440-50-809/08/10 15:403.8 0.30Lead 5.3 mg/kg 10 09/22/10 19:30 7439-92-109/08/10 15:403.8 3.6Manganese 546 mg/kg 10 09/22/10 19:30 7439-96-509/08/10 15:403.8 0.23Nickel 10.9 mg/kg 10 09/22/10 19:30 7440-02-009/08/10 15:403.8 1.4Selenium ND mg/kg 10 09/22/10 19:30 7782-49-2 D309/08/10 15:407.6 2.9Silver ND mg/kg 10 09/22/10 19:30 7440-22-4 D309/08/10 15:403.8 0.23Thallium 2.4J mg/kg 10 09/22/10 19:30 7440-28-0 D309/08/10 15:407.6 2.0Zinc 85.8 mg/kg 10 09/22/10 19:30 7440-66-609/08/10 15:407.6 2.0


Mercury 0.0074 mg/kg 1 09/15/10 12:26 7439-97-609/14/10 08:110.0054 0.00011


Acenaphthene ND ug/kg 1 09/24/10 10:03 83-32-909/13/10 18:30356 82.0Acenaphthylene ND ug/kg 1 09/24/10 10:03 208-96-809/13/10 18:30356 84.1Acetophenone ND ug/kg 1 09/24/10 10:03 98-86-209/13/10 18:30356 183Anthracene ND ug/kg 1 09/24/10 10:03 120-12-709/13/10 18:30356 79.8Atrazine ND ug/kg 1 09/24/10 10:03 1912-24-909/13/10 18:30712 140Benzaldehyde ND ug/kg 1 09/24/10 10:03 100-52-709/13/10 18:30712 356Benzo(a)anthracene ND ug/kg 1 09/24/10 10:03 56-55-309/13/10 18:30356 65.8Benzo(a)pyrene ND ug/kg 1 09/24/10 10:03 50-32-809/13/10 18:30356 67.9Benzo(b)fluoranthene ND ug/kg 1 09/24/10 10:03 205-99-209/13/10 18:30356 61.5Benzo(g,h,i)perylene ND ug/kg 1 09/24/10 10:03 191-24-209/13/10 18:30356 90.6Benzo(k)fluoranthene ND ug/kg 1 09/24/10 10:03 207-08-909/13/10 18:30356 70.1Biphenyl (Diphenyl) ND ug/kg 1 09/24/10 10:03 92-52-409/13/10 18:30356 1124-Bromophenylphenyl ether ND ug/kg 1 09/24/10 10:03 101-55-309/13/10 18:30356 64.7Butylbenzylphthalate ND ug/kg 1 09/24/10 10:03 85-68-709/13/10 18:30356 75.5Caprolactam ND ug/kg 1 09/24/10 10:03 105-60-209/13/10 18:30356 61.5Carbazole ND ug/kg 1 09/24/10 10:03 86-74-809/13/10 18:30356 67.94-Chloro-3-methylphenol ND ug/kg 1 09/24/10 10:03 59-50-709/13/10 18:30712 73.34-Chloroaniline ND ug/kg 1 09/24/10 10:03 106-47-809/13/10 18:301780 99.2bis(2-Chloroethoxy)methane ND ug/kg 1 09/24/10 10:03 111-91-109/13/10 18:30356 83.0bis(2-Chloroethyl) ether ND ug/kg 1 09/24/10 10:03 111-44-409/13/10 18:30356 90.6bis(2-Chloroisopropyl) ether ND ug/kg 1 09/24/10 10:03 108-60-109/13/10 18:30356 94.92-Chloronaphthalene ND ug/kg 1 09/24/10 10:03 91-58-709/13/10 18:30356 70.12-Chlorophenol ND ug/kg 1 09/24/10 10:03 95-57-809/13/10 18:30356 97.04-Chlorophenylphenyl ether ND ug/kg 1 09/24/10 10:03 7005-72-309/13/10 18:30356 73.3Chrysene ND ug/kg 1 09/24/10 10:03 218-01-909/13/10 18:30356 47.4Dibenz(a,h)anthracene ND ug/kg 1 09/24/10 10:03 53-70-309/13/10 18:30356 75.5Dibenzofuran ND ug/kg 1 09/24/10 10:03 132-64-909/13/10 18:30356 58.2



Date: 09/27/2010 06:48 PM Page 99 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/24/10 10:03 91-94-109/13/10 18:301780 77.62,4-Dichlorophenol ND ug/kg 1 09/24/10 10:03 120-83-209/13/10 18:30356 77.6Diethylphthalate ND ug/kg 1 09/24/10 10:03 84-66-209/13/10 18:30356 55.02,4-Dimethylphenol ND ug/kg 1 09/24/10 10:03 105-67-909/13/10 18:30356 140Dimethylphthalate ND ug/kg 1 09/24/10 10:03 131-11-309/13/10 18:30356 72.2Di-n-butylphthalate ND ug/kg 1 09/24/10 10:03 84-74-209/13/10 18:30356 58.24,6-Dinitro-2-methylphenol ND ug/kg 1 09/24/10 10:03 534-52-109/13/10 18:30712 71.22,4-Dinitrophenol ND ug/kg 1 09/24/10 10:03 51-28-509/13/10 18:301780 58.22,4-Dinitrotoluene ND ug/kg 1 09/24/10 10:03 121-14-209/13/10 18:30356 66.92,6-Dinitrotoluene ND ug/kg 1 09/24/10 10:03 606-20-209/13/10 18:30356 74.4Di-n-octylphthalate ND ug/kg 1 09/24/10 10:03 117-84-009/13/10 18:30356 74.4bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/24/10 10:03 117-81-709/13/10 18:30356 97.0Fluoranthene ND ug/kg 1 09/24/10 10:03 206-44-009/13/10 18:30356 51.8Fluorene ND ug/kg 1 09/24/10 10:03 86-73-709/13/10 18:30356 73.3Hexachloro-1,3-butadiene ND ug/kg 1 09/24/10 10:03 87-68-309/13/10 18:30356 61.5Hexachlorobenzene ND ug/kg 1 09/24/10 10:03 118-74-109/13/10 18:30356 45.3Hexachlorocyclopentadiene ND ug/kg 1 09/24/10 10:03 77-47-409/13/10 18:30356 65.8Hexachloroethane ND ug/kg 1 09/24/10 10:03 67-72-109/13/10 18:30356 93.8Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/24/10 10:03 193-39-509/13/10 18:30356 73.3Isophorone ND ug/kg 1 09/24/10 10:03 78-59-109/13/10 18:30356 79.82-Methylnaphthalene ND ug/kg 1 09/24/10 10:03 91-57-609/13/10 18:30356 76.62-Methylphenol(o-Cresol) ND ug/kg 1 09/24/10 10:03 95-48-709/13/10 18:30356 1083&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/24/10 10:0309/13/10 18:30356 140Naphthalene ND ug/kg 1 09/24/10 10:03 91-20-309/13/10 18:30356 87.32-Nitroaniline ND ug/kg 1 09/24/10 10:03 88-74-409/13/10 18:301780 1103-Nitroaniline ND ug/kg 1 09/24/10 10:03 99-09-209/13/10 18:301780 97.04-Nitroaniline ND ug/kg 1 09/24/10 10:03 100-01-609/13/10 18:30712 100Nitrobenzene ND ug/kg 1 09/24/10 10:03 98-95-309/13/10 18:30356 97.02-Nitrophenol ND ug/kg 1 09/24/10 10:03 88-75-509/13/10 18:30356 86.34-Nitrophenol ND ug/kg 1 09/24/10 10:03 100-02-709/13/10 18:301780 63.6N-Nitroso-di-n-propylamine ND ug/kg 1 09/24/10 10:03 621-64-709/13/10 18:30356 67.9N-Nitrosodiphenylamine ND ug/kg 1 09/24/10 10:03 86-30-609/13/10 18:30356 106Pentachlorophenol ND ug/kg 1 09/24/10 10:03 87-86-509/13/10 18:301780 64.7Phenanthrene ND ug/kg 1 09/24/10 10:03 85-01-809/13/10 18:30356 59.3Phenol ND ug/kg 1 09/24/10 10:03 108-95-209/13/10 18:30356 107Pyrene ND ug/kg 1 09/24/10 10:03 129-00-009/13/10 18:30356 60.41,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/24/10 10:03 95-94-309/13/10 18:30356 1292,3,4,6-Tetrachlorophenol ND ug/kg 1 09/24/10 10:03 58-90-209/13/10 18:30356 1402,4,5-Trichlorophenol ND ug/kg 1 09/24/10 10:03 95-95-409/13/10 18:30356 1102,4,6-Trichlorophenol ND ug/kg 1 09/24/10 10:03 88-06-209/13/10 18:30356 78.72-Fluorobiphenyl (S) 15 % 1 09/24/10 10:03 321-60-8 S209/13/10 18:3030-110Terphenyl-d14 (S) 25 % 1 09/24/10 10:03 1718-51-0 S209/13/10 18:3028-110Phenol-d6 (S) 14 % 1 09/24/10 10:03 13127-88-3 S209/13/10 18:3022-1102-Fluorophenol (S) 12 % 1 09/24/10 10:03 367-12-4 S209/13/10 18:3013-1102,4,6-Tribromophenol (S) 21 % 1 09/24/10 10:03 118-79-6 S209/13/10 18:3027-110



Date: 09/27/2010 06:48 PM Page 100 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 11 % 1 09/24/10 10:03 4165-60-0 S209/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:35 57-12-50.12 0.12





Date: 09/27/2010 06:48 PM Page 101 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 19:34 7440-36-0 D309/08/10 15:404.5 2.5Arsenic ND mg/kg 10 09/22/10 19:34 7440-38-2 D309/08/10 15:404.5 2.9Beryllium 1.4 mg/kg 10 09/22/10 19:34 7440-41-709/08/10 15:400.90 0.18Cadmium ND mg/kg 10 09/22/10 19:34 7440-43-9 D309/08/10 15:400.90 0.54Chromium 16.3 mg/kg 10 09/22/10 19:34 7440-47-309/08/10 15:404.5 0.27Copper 3.5J mg/kg 10 09/22/10 19:34 7440-50-8 D309/08/10 15:404.5 0.36Lead 5.2 mg/kg 10 09/22/10 19:34 7439-92-109/08/10 15:404.5 4.3Manganese 354 mg/kg 10 09/22/10 19:34 7439-96-509/08/10 15:404.5 0.27Nickel 9.8 mg/kg 10 09/22/10 19:34 7440-02-009/08/10 15:404.5 1.6Selenium ND mg/kg 10 09/22/10 19:34 7782-49-2 D309/08/10 15:409.0 3.4Silver ND mg/kg 10 09/22/10 19:34 7440-22-4 D309/08/10 15:404.5 0.27Thallium ND mg/kg 10 09/22/10 19:34 7440-28-0 D309/08/10 15:409.0 2.3Zinc 75.4 mg/kg 10 09/22/10 19:34 7440-66-609/08/10 15:409.0 2.3


Mercury 0.00073J mg/kg 1 09/15/10 12:28 7439-97-609/14/10 08:110.0046 0.000092





Date: 09/27/2010 06:48 PM Page 102 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/18/10 21:31 91-94-109/13/10 18:301820 79.42,4-Dichlorophenol ND ug/kg 1 09/18/10 21:31 120-83-209/13/10 18:30364 79.4Diethylphthalate ND ug/kg 1 09/18/10 21:31 84-66-209/13/10 18:30364 56.22,4-Dimethylphenol ND ug/kg 1 09/18/10 21:31 105-67-909/13/10 18:30364 143Dimethylphthalate ND ug/kg 1 09/18/10 21:31 131-11-309/13/10 18:30364 73.8Di-n-butylphthalate ND ug/kg 1 09/18/10 21:31 84-74-209/13/10 18:30364 59.54,6-Dinitro-2-methylphenol ND ug/kg 1 09/18/10 21:31 534-52-109/13/10 18:30727 72.72,4-Dinitrophenol ND ug/kg 1 09/18/10 21:31 51-28-509/13/10 18:301820 59.52,4-Dinitrotoluene ND ug/kg 1 09/18/10 21:31 121-14-209/13/10 18:30364 68.32,6-Dinitrotoluene ND ug/kg 1 09/18/10 21:31 606-20-209/13/10 18:30364 76.0Di-n-octylphthalate ND ug/kg 1 09/18/10 21:31 117-84-009/13/10 18:30364 76.0bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/18/10 21:31 117-81-709/13/10 18:30364 99.2Fluoranthene ND ug/kg 1 09/18/10 21:31 206-44-009/13/10 18:30364 52.9Fluorene ND ug/kg 1 09/18/10 21:31 86-73-709/13/10 18:30364 74.9Hexachloro-1,3-butadiene ND ug/kg 1 09/18/10 21:31 87-68-309/13/10 18:30364 62.8Hexachlorobenzene ND ug/kg 1 09/18/10 21:31 118-74-109/13/10 18:30364 46.3Hexachlorocyclopentadiene ND ug/kg 1 09/18/10 21:31 77-47-409/13/10 18:30364 67.2Hexachloroethane ND ug/kg 1 09/18/10 21:31 67-72-109/13/10 18:30364 95.9Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/18/10 21:31 193-39-509/13/10 18:30364 74.9Isophorone ND ug/kg 1 09/18/10 21:31 78-59-109/13/10 18:30364 81.62-Methylnaphthalene ND ug/kg 1 09/18/10 21:31 91-57-609/13/10 18:30364 78.32-Methylphenol(o-Cresol) ND ug/kg 1 09/18/10 21:31 95-48-709/13/10 18:30364 1103&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/18/10 21:3109/13/10 18:30364 143Naphthalene ND ug/kg 1 09/18/10 21:31 91-20-309/13/10 18:30364 89.32-Nitroaniline ND ug/kg 1 09/18/10 21:31 88-74-409/13/10 18:301820 1123-Nitroaniline ND ug/kg 1 09/18/10 21:31 99-09-209/13/10 18:301820 99.24-Nitroaniline ND ug/kg 1 09/18/10 21:31 100-01-609/13/10 18:30727 102Nitrobenzene ND ug/kg 1 09/18/10 21:31 98-95-309/13/10 18:30364 99.22-Nitrophenol ND ug/kg 1 09/18/10 21:31 88-75-509/13/10 18:30364 88.24-Nitrophenol ND ug/kg 1 09/18/10 21:31 100-02-709/13/10 18:301820 65.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/18/10 21:31 621-64-709/13/10 18:30364 69.4N-Nitrosodiphenylamine ND ug/kg 1 09/18/10 21:31 86-30-609/13/10 18:30364 108Pentachlorophenol ND ug/kg 1 09/18/10 21:31 87-86-509/13/10 18:301820 66.1Phenanthrene ND ug/kg 1 09/18/10 21:31 85-01-809/13/10 18:30364 60.6Phenol ND ug/kg 1 09/18/10 21:31 108-95-209/13/10 18:30364 109Pyrene ND ug/kg 1 09/18/10 21:31 129-00-009/13/10 18:30364 61.71,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/18/10 21:31 95-94-309/13/10 18:30364 1322,3,4,6-Tetrachlorophenol ND ug/kg 1 09/18/10 21:31 58-90-209/13/10 18:30364 1432,4,5-Trichlorophenol ND ug/kg 1 09/18/10 21:31 95-95-409/13/10 18:30364 1122,4,6-Trichlorophenol ND ug/kg 1 09/18/10 21:31 88-06-209/13/10 18:30364 80.52-Fluorobiphenyl (S) 29 % 1 09/18/10 21:31 321-60-8 S009/13/10 18:3030-110Terphenyl-d14 (S) 44 % 1 09/18/10 21:31 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 19 % 1 09/18/10 21:31 13127-88-3 S009/13/10 18:3022-1102-Fluorophenol (S) 24 % 1 09/18/10 21:31 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 33 % 1 09/18/10 21:31 118-79-609/13/10 18:3027-110



Date: 09/27/2010 06:48 PM Page 103 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/18/10 21:31 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:35 57-12-50.12 0.12





Date: 09/27/2010 06:48 PM Page 104 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury ND mg/kg 1 09/15/10 12:31 7439-97-609/14/10 08:110.0046 0.000092





Date: 09/27/2010 06:48 PM Page 105 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 106 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 41 % 1 09/24/10 10:39 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:36 57-12-50.13 0.13





Date: 09/27/2010 06:48 PM Page 107 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.00014J mg/kg 1 09/15/10 12:34 7439-97-609/14/10 08:110.0037 0.000074





Date: 09/27/2010 06:48 PM Page 108 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 109 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 37 % 1 09/24/10 11:15 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:37 57-12-50.10 0.10





Date: 09/27/2010 06:48 PM Page 110 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 5 09/22/10 19:54 7440-36-0 D309/08/10 15:402.2 1.2Arsenic 1.9J mg/kg 5 09/22/10 19:54 7440-38-2 D309/08/10 15:402.2 1.4Beryllium 0.86 mg/kg 5 09/22/10 19:54 7440-41-709/08/10 15:400.43 0.087Cadmium 0.43 mg/kg 5 09/22/10 19:54 7440-43-909/08/10 15:400.43 0.26Chromium 14.7 mg/kg 5 09/22/10 19:54 7440-47-309/08/10 15:402.2 0.13Copper 9.4 mg/kg 5 09/22/10 19:54 7440-50-809/08/10 15:402.2 0.17Lead 10.9 mg/kg 5 09/22/10 19:54 7439-92-109/08/10 15:402.2 2.1Manganese 370 mg/kg 5 09/22/10 19:54 7439-96-509/08/10 15:402.2 0.13Nickel 8.6 mg/kg 5 09/22/10 19:54 7440-02-009/08/10 15:402.2 0.78Selenium ND mg/kg 5 09/22/10 19:54 7782-49-2 D309/08/10 15:404.3 1.7Silver ND mg/kg 5 09/22/10 19:54 7440-22-4 D309/08/10 15:402.2 0.13Thallium ND mg/kg 5 09/22/10 19:54 7440-28-0 D309/08/10 15:404.3 1.1Zinc 47.4 mg/kg 5 09/22/10 19:54 7440-66-609/08/10 15:404.3 1.1


Mercury 0.024 mg/kg 1 09/15/10 12:36 7439-97-609/14/10 08:110.0043 0.000086





Date: 09/27/2010 06:48 PM Page 111 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 112 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 29 % 1 09/18/10 23:19 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/12/10 16:38 57-12-50.13 0.13





Date: 09/27/2010 06:48 PM Page 113 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.010 mg/kg 1 09/15/10 12:39 7439-97-609/14/10 08:110.0041 0.000083





Date: 09/27/2010 06:48 PM Page 114 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 115 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 36 % 1 09/18/10 23:55 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/14/10 10:09 57-12-50.17 0.17





Date: 09/27/2010 06:48 PM Page 116 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 20:00 7440-36-0 D309/08/10 15:405.5 3.1Arsenic 6.1 mg/kg 10 09/22/10 20:00 7440-38-209/08/10 15:405.5 3.5Beryllium 2.5 mg/kg 10 09/22/10 20:00 7440-41-709/08/10 15:401.1 0.22Cadmium ND mg/kg 10 09/22/10 20:00 7440-43-9 D309/08/10 15:401.1 0.66Chromium 30.1 mg/kg 10 09/22/10 20:00 7440-47-309/08/10 15:405.5 0.33Copper 8.9 mg/kg 10 09/22/10 20:00 7440-50-809/08/10 15:405.5 0.44Lead 15.9 mg/kg 10 09/22/10 20:00 7439-92-109/08/10 15:405.5 5.3Manganese 3130 mg/kg 10 09/22/10 20:00 7439-96-509/08/10 15:405.5 0.33Nickel 24.6 mg/kg 10 09/22/10 20:00 7440-02-009/08/10 15:405.5 2.0Selenium ND mg/kg 10 09/22/10 20:00 7782-49-2 D309/08/10 15:4011.0 4.2Silver ND mg/kg 10 09/22/10 20:00 7440-22-4 D309/08/10 15:405.5 0.33Thallium ND mg/kg 10 09/22/10 20:00 7440-28-0 D309/08/10 15:4011.0 2.9Zinc 128 mg/kg 10 09/22/10 20:00 7440-66-609/08/10 15:4011.0 2.9


Mercury 0.0016J mg/kg 1 09/15/10 12:42 7439-97-609/14/10 08:110.0046 0.000091





Date: 09/27/2010 06:48 PM Page 117 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 118 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 56 % 1 09/24/10 11:51 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/14/10 10:09 57-12-50.20 0.20





Date: 09/27/2010 06:48 PM Page 119 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 20:04 7440-36-0 D309/08/10 15:404.4 2.5Arsenic ND mg/kg 10 09/22/10 20:04 7440-38-2 D309/08/10 15:404.4 2.8Beryllium 1.4 mg/kg 10 09/22/10 20:04 7440-41-709/08/10 15:400.88 0.18Cadmium ND mg/kg 10 09/22/10 20:04 7440-43-9 D309/08/10 15:400.88 0.53Chromium 12.8 mg/kg 10 09/22/10 20:04 7440-47-309/08/10 15:404.4 0.26Copper 7.1 mg/kg 10 09/22/10 20:04 7440-50-809/08/10 15:404.4 0.35Lead ND mg/kg 10 09/22/10 20:04 7439-92-1 D309/08/10 15:404.4 4.2Manganese 2030 mg/kg 10 09/22/10 20:04 7439-96-509/08/10 15:404.4 0.26Nickel 8.7 mg/kg 10 09/22/10 20:04 7440-02-009/08/10 15:404.4 1.6Selenium ND mg/kg 10 09/22/10 20:04 7782-49-2 D309/08/10 15:408.8 3.3Silver ND mg/kg 10 09/22/10 20:04 7440-22-4 D309/08/10 15:404.4 0.26Thallium 2.4J mg/kg 10 09/22/10 20:04 7440-28-0 D309/08/10 15:408.8 2.3Zinc 45.5 mg/kg 10 09/22/10 20:04 7440-66-609/08/10 15:408.8 2.3


Mercury ND mg/kg 1 09/15/10 12:44 7439-97-609/14/10 08:110.0043 0.000087





Date: 09/27/2010 06:48 PM Page 120 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/24/10 12:28 91-94-109/13/10 18:301910 83.22,4-Dichlorophenol ND ug/kg 1 09/24/10 12:28 120-83-209/13/10 18:30381 83.2Diethylphthalate ND ug/kg 1 09/24/10 12:28 84-66-209/13/10 18:30381 58.92,4-Dimethylphenol ND ug/kg 1 09/24/10 12:28 105-67-909/13/10 18:30381 150Dimethylphthalate ND ug/kg 1 09/24/10 12:28 131-11-309/13/10 18:30381 77.4Di-n-butylphthalate ND ug/kg 1 09/24/10 12:28 84-74-209/13/10 18:30381 62.44,6-Dinitro-2-methylphenol ND ug/kg 1 09/24/10 12:28 534-52-109/13/10 18:30762 76.22,4-Dinitrophenol ND ug/kg 1 09/24/10 12:28 51-28-509/13/10 18:301910 62.42,4-Dinitrotoluene ND ug/kg 1 09/24/10 12:28 121-14-209/13/10 18:30381 71.62,6-Dinitrotoluene ND ug/kg 1 09/24/10 12:28 606-20-209/13/10 18:30381 79.7Di-n-octylphthalate ND ug/kg 1 09/24/10 12:28 117-84-009/13/10 18:30381 79.7bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/24/10 12:28 117-81-709/13/10 18:30381 104Fluoranthene ND ug/kg 1 09/24/10 12:28 206-44-009/13/10 18:30381 55.5Fluorene ND ug/kg 1 09/24/10 12:28 86-73-709/13/10 18:30381 78.6Hexachloro-1,3-butadiene ND ug/kg 1 09/24/10 12:28 87-68-309/13/10 18:30381 65.9Hexachlorobenzene ND ug/kg 1 09/24/10 12:28 118-74-109/13/10 18:30381 48.5Hexachlorocyclopentadiene ND ug/kg 1 09/24/10 12:28 77-47-409/13/10 18:30381 70.5Hexachloroethane ND ug/kg 1 09/24/10 12:28 67-72-109/13/10 18:30381 101Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/24/10 12:28 193-39-509/13/10 18:30381 78.6Isophorone ND ug/kg 1 09/24/10 12:28 78-59-109/13/10 18:30381 85.52-Methylnaphthalene ND ug/kg 1 09/24/10 12:28 91-57-609/13/10 18:30381 82.02-Methylphenol(o-Cresol) ND ug/kg 1 09/24/10 12:28 95-48-709/13/10 18:30381 1163&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/24/10 12:2809/13/10 18:30381 150Naphthalene ND ug/kg 1 09/24/10 12:28 91-20-309/13/10 18:30381 93.62-Nitroaniline ND ug/kg 1 09/24/10 12:28 88-74-409/13/10 18:301910 1183-Nitroaniline ND ug/kg 1 09/24/10 12:28 99-09-209/13/10 18:301910 1044-Nitroaniline ND ug/kg 1 09/24/10 12:28 100-01-609/13/10 18:30762 107Nitrobenzene ND ug/kg 1 09/24/10 12:28 98-95-309/13/10 18:30381 1042-Nitrophenol ND ug/kg 1 09/24/10 12:28 88-75-509/13/10 18:30381 92.44-Nitrophenol ND ug/kg 1 09/24/10 12:28 100-02-709/13/10 18:301910 68.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/24/10 12:28 621-64-709/13/10 18:30381 72.8N-Nitrosodiphenylamine ND ug/kg 1 09/24/10 12:28 86-30-609/13/10 18:30381 113Pentachlorophenol ND ug/kg 1 09/24/10 12:28 87-86-509/13/10 18:301910 69.3Phenanthrene ND ug/kg 1 09/24/10 12:28 85-01-809/13/10 18:30381 63.5Phenol ND ug/kg 1 09/24/10 12:28 108-95-209/13/10 18:30381 114Pyrene ND ug/kg 1 09/24/10 12:28 129-00-009/13/10 18:30381 64.71,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/24/10 12:28 95-94-309/13/10 18:30381 1392,3,4,6-Tetrachlorophenol ND ug/kg 1 09/24/10 12:28 58-90-209/13/10 18:30381 1502,4,5-Trichlorophenol ND ug/kg 1 09/24/10 12:28 95-95-409/13/10 18:30381 1182,4,6-Trichlorophenol ND ug/kg 1 09/24/10 12:28 88-06-209/13/10 18:30381 84.32-Fluorobiphenyl (S) 32 % 1 09/24/10 12:28 321-60-809/13/10 18:3030-110Terphenyl-d14 (S) 49 % 1 09/24/10 12:28 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 14 % 1 09/24/10 12:28 13127-88-3 S209/13/10 18:3022-1102-Fluorophenol (S) 14 % 1 09/24/10 12:28 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 19 % 1 09/24/10 12:28 118-79-6 S009/13/10 18:3027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 23 % 1 09/24/10 12:28 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/14/10 10:10 57-12-50.20 0.20





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(704)875-9092


Asheville, NC 28804

(828)254-7176

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9276872MILLS GAP 6686081744




Antimony ND mg/kg 20 09/23/10 12:18 7440-36-0 D309/08/10 15:408.8 4.9Arsenic ND mg/kg 20 09/23/10 12:18 7440-38-2 D309/08/10 15:408.8 5.6Beryllium 1.5J mg/kg 20 09/23/10 12:18 7440-41-7 D309/08/10 15:401.8 0.35Cadmium ND mg/kg 20 09/23/10 12:18 7440-43-9 D309/08/10 15:401.8 1.1Chromium 14.3 mg/kg 20 09/23/10 12:18 7440-47-309/08/10 15:408.8 0.53Copper ND mg/kg 20 09/23/10 12:18 7440-50-8 D309/08/10 15:408.8 0.71Lead ND mg/kg 20 09/23/10 12:18 7439-92-1 D309/08/10 15:408.8 8.5Manganese 194 mg/kg 20 09/23/10 12:18 7439-96-509/08/10 15:408.8 0.53Nickel 6.8J mg/kg 20 09/23/10 12:18 7440-02-0 D309/08/10 15:408.8 3.2Selenium ND mg/kg 20 09/23/10 12:18 7782-49-2 D309/08/10 15:4017.6 6.7Silver ND mg/kg 20 09/23/10 12:18 7440-22-4 D309/08/10 15:408.8 0.53Thallium ND mg/kg 20 09/23/10 12:18 7440-28-0 D309/08/10 15:4017.6 4.6Zinc 45.9 mg/kg 20 09/23/10 12:18 7440-66-609/08/10 15:4017.6 4.6


Mercury ND mg/kg 1 09/15/10 12:47 7439-97-609/14/10 08:110.0041 0.000081





Date: 09/27/2010 06:48 PM Page 123 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 124 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 38 % 1 09/24/10 13:04 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/14/10 10:11 57-12-50.18 0.18





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 5 09/22/10 16:50 7440-36-0 D309/09/10 14:302.2 1.2Arsenic ND mg/kg 5 09/22/10 16:50 7440-38-2 D309/09/10 14:302.2 1.4Beryllium 0.91 mg/kg 5 09/22/10 16:50 7440-41-709/09/10 14:300.43 0.086Cadmium ND mg/kg 5 09/22/10 16:50 7440-43-9 D309/09/10 14:300.43 0.26Chromium 18.1 mg/kg 5 09/22/10 16:50 7440-47-309/09/10 14:302.2 0.13Copper 10.5 mg/kg 5 09/22/10 16:50 7440-50-809/09/10 14:302.2 0.17Lead 10.9 mg/kg 5 09/22/10 16:50 7439-92-109/09/10 14:302.2 2.1Manganese 290 mg/kg 5 09/22/10 16:50 7439-96-509/09/10 14:302.2 0.13Nickel 8.7 mg/kg 5 09/22/10 16:50 7440-02-009/09/10 14:302.2 0.78Selenium ND mg/kg 5 09/22/10 16:50 7782-49-2 D309/09/10 14:304.3 1.6Silver 1.3J mg/kg 5 09/22/10 16:50 7440-22-4 D309/09/10 14:302.2 0.13Thallium ND mg/kg 5 09/22/10 16:50 7440-28-0 D309/09/10 14:304.3 1.1Zinc 40.8 mg/kg 5 09/22/10 16:50 7440-66-609/09/10 14:304.3 1.1


Mercury 0.019 mg/kg 1 09/15/10 12:50 7439-97-6 M109/14/10 08:110.0054 0.00011





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/24/10 13:41 83-32-909/13/10 18:30349 80.3Acenaphthylene ND ug/kg 1 09/24/10 13:41 208-96-809/13/10 18:30349 82.4Acetophenone ND ug/kg 1 09/24/10 13:41 98-86-209/13/10 18:30349 180Anthracene ND ug/kg 1 09/24/10 13:41 120-12-709/13/10 18:30349 78.2Atrazine ND ug/kg 1 09/24/10 13:41 1912-24-909/13/10 18:30698 137Benzaldehyde ND ug/kg 1 09/24/10 13:41 100-52-709/13/10 18:30698 349Benzo(a)anthracene ND ug/kg 1 09/24/10 13:41 56-55-309/13/10 18:30349 64.5Benzo(a)pyrene ND ug/kg 1 09/24/10 13:41 50-32-809/13/10 18:30349 66.6Benzo(b)fluoranthene ND ug/kg 1 09/24/10 13:41 205-99-209/13/10 18:30349 60.2Benzo(g,h,i)perylene ND ug/kg 1 09/24/10 13:41 191-24-209/13/10 18:30349 88.8Benzo(k)fluoranthene ND ug/kg 1 09/24/10 13:41 207-08-909/13/10 18:30349 68.7Biphenyl (Diphenyl) ND ug/kg 1 09/24/10 13:41 92-52-409/13/10 18:30349 1104-Bromophenylphenyl ether ND ug/kg 1 09/24/10 13:41 101-55-309/13/10 18:30349 63.4Butylbenzylphthalate ND ug/kg 1 09/24/10 13:41 85-68-709/13/10 18:30349 74.0Caprolactam ND ug/kg 1 09/24/10 13:41 105-60-209/13/10 18:30349 60.2Carbazole ND ug/kg 1 09/24/10 13:41 86-74-809/13/10 18:30349 66.64-Chloro-3-methylphenol ND ug/kg 1 09/24/10 13:41 59-50-709/13/10 18:30698 71.94-Chloroaniline ND ug/kg 1 09/24/10 13:41 106-47-809/13/10 18:301740 97.2bis(2-Chloroethoxy)methane ND ug/kg 1 09/24/10 13:41 111-91-109/13/10 18:30349 81.4bis(2-Chloroethyl) ether ND ug/kg 1 09/24/10 13:41 111-44-409/13/10 18:30349 88.8bis(2-Chloroisopropyl) ether ND ug/kg 1 09/24/10 13:41 108-60-109/13/10 18:30349 93.02-Chloronaphthalene ND ug/kg 1 09/24/10 13:41 91-58-709/13/10 18:30349 68.72-Chlorophenol ND ug/kg 1 09/24/10 13:41 95-57-809/13/10 18:30349 95.14-Chlorophenylphenyl ether ND ug/kg 1 09/24/10 13:41 7005-72-309/13/10 18:30349 71.9Chrysene ND ug/kg 1 09/24/10 13:41 218-01-909/13/10 18:30349 46.5Dibenz(a,h)anthracene ND ug/kg 1 09/24/10 13:41 53-70-309/13/10 18:30349 74.0Dibenzofuran ND ug/kg 1 09/24/10 13:41 132-64-909/13/10 18:30349 57.13,3'-Dichlorobenzidine ND ug/kg 1 09/24/10 13:41 91-94-109/13/10 18:301740 76.12,4-Dichlorophenol ND ug/kg 1 09/24/10 13:41 120-83-209/13/10 18:30349 76.1Diethylphthalate ND ug/kg 1 09/24/10 13:41 84-66-209/13/10 18:30349 53.92,4-Dimethylphenol ND ug/kg 1 09/24/10 13:41 105-67-909/13/10 18:30349 137Dimethylphthalate ND ug/kg 1 09/24/10 13:41 131-11-309/13/10 18:30349 70.8Di-n-butylphthalate ND ug/kg 1 09/24/10 13:41 84-74-209/13/10 18:30349 57.14,6-Dinitro-2-methylphenol ND ug/kg 1 09/24/10 13:41 534-52-109/13/10 18:30698 69.82,4-Dinitrophenol ND ug/kg 1 09/24/10 13:41 51-28-509/13/10 18:301740 57.12,4-Dinitrotoluene ND ug/kg 1 09/24/10 13:41 121-14-209/13/10 18:30349 65.52,6-Dinitrotoluene ND ug/kg 1 09/24/10 13:41 606-20-209/13/10 18:30349 72.9Di-n-octylphthalate ND ug/kg 1 09/24/10 13:41 117-84-009/13/10 18:30349 72.9bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/24/10 13:41 117-81-709/13/10 18:30349 95.1Fluoranthene ND ug/kg 1 09/24/10 13:41 206-44-009/13/10 18:30349 50.7Fluorene ND ug/kg 1 09/24/10 13:41 86-73-709/13/10 18:30349 71.9Hexachloro-1,3-butadiene ND ug/kg 1 09/24/10 13:41 87-68-309/13/10 18:30349 60.2Hexachlorobenzene ND ug/kg 1 09/24/10 13:41 118-74-109/13/10 18:30349 44.4Hexachlorocyclopentadiene ND ug/kg 1 09/24/10 13:41 77-47-409/13/10 18:30349 64.5Hexachloroethane ND ug/kg 1 09/24/10 13:41 67-72-109/13/10 18:30349 91.9



Date: 09/27/2010 06:48 PM Page 127 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/24/10 13:41 193-39-509/13/10 18:30349 71.9Isophorone ND ug/kg 1 09/24/10 13:41 78-59-109/13/10 18:30349 78.22-Methylnaphthalene ND ug/kg 1 09/24/10 13:41 91-57-609/13/10 18:30349 75.02-Methylphenol(o-Cresol) ND ug/kg 1 09/24/10 13:41 95-48-709/13/10 18:30349 1063&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/24/10 13:4109/13/10 18:30349 137Naphthalene ND ug/kg 1 09/24/10 13:41 91-20-309/13/10 18:30349 85.62-Nitroaniline ND ug/kg 1 09/24/10 13:41 88-74-409/13/10 18:301740 1083-Nitroaniline ND ug/kg 1 09/24/10 13:41 99-09-209/13/10 18:301740 95.14-Nitroaniline ND ug/kg 1 09/24/10 13:41 100-01-609/13/10 18:30698 98.3Nitrobenzene ND ug/kg 1 09/24/10 13:41 98-95-309/13/10 18:30349 95.12-Nitrophenol ND ug/kg 1 09/24/10 13:41 88-75-509/13/10 18:30349 84.64-Nitrophenol ND ug/kg 1 09/24/10 13:41 100-02-709/13/10 18:301740 62.4N-Nitroso-di-n-propylamine ND ug/kg 1 09/24/10 13:41 621-64-709/13/10 18:30349 66.6N-Nitrosodiphenylamine ND ug/kg 1 09/24/10 13:41 86-30-609/13/10 18:30349 104Pentachlorophenol ND ug/kg 1 09/24/10 13:41 87-86-509/13/10 18:301740 63.4Phenanthrene ND ug/kg 1 09/24/10 13:41 85-01-809/13/10 18:30349 58.1Phenol ND ug/kg 1 09/24/10 13:41 108-95-209/13/10 18:30349 105Pyrene ND ug/kg 1 09/24/10 13:41 129-00-009/13/10 18:30349 59.21,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/24/10 13:41 95-94-309/13/10 18:30349 1272,3,4,6-Tetrachlorophenol ND ug/kg 1 09/24/10 13:41 58-90-209/13/10 18:30349 1372,4,5-Trichlorophenol ND ug/kg 1 09/24/10 13:41 95-95-409/13/10 18:30349 1082,4,6-Trichlorophenol ND ug/kg 1 09/24/10 13:41 88-06-209/13/10 18:30349 77.22-Fluorobiphenyl (S) 30 % 1 09/24/10 13:41 321-60-809/13/10 18:3030-110Terphenyl-d14 (S) 41 % 1 09/24/10 13:41 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 19 % 1 09/24/10 13:41 13127-88-3 S009/13/10 18:3022-1102-Fluorophenol (S) 21 % 1 09/24/10 13:41 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 37 % 1 09/24/10 13:41 118-79-609/13/10 18:3027-110Nitrobenzene-d5 (S) 23 % 1 09/24/10 13:41 4165-60-009/13/10 18:3023-110


Acetone 90.7J ug/kg 1 09/09/10 04:54 67-64-197.9 9.8Benzene ND ug/kg 1 09/09/10 04:54 71-43-24.9 1.6Bromochloromethane ND ug/kg 1 09/09/10 04:54 74-97-54.9 1.7Bromodichloromethane ND ug/kg 1 09/09/10 04:54 75-27-44.9 1.9Bromoform ND ug/kg 1 09/09/10 04:54 75-25-24.9 2.3Bromomethane ND ug/kg 1 09/09/10 04:54 74-83-99.8 2.42-Butanone (MEK) 2.9J ug/kg 1 09/09/10 04:54 78-93-397.9 2.8Carbon disulfide ND ug/kg 1 09/09/10 04:54 75-15-09.8 2.9Carbon tetrachloride ND ug/kg 1 09/09/10 04:54 56-23-54.9 2.5Chlorobenzene ND ug/kg 1 09/09/10 04:54 108-90-74.9 1.9Chloroethane ND ug/kg 1 09/09/10 04:54 75-00-39.8 2.3Chloroform ND ug/kg 1 09/09/10 04:54 67-66-34.9 1.6Chloromethane ND ug/kg 1 09/09/10 04:54 74-87-39.8 2.3Cyclohexane ND ug/kg 1 09/09/10 04:54 110-82-74.9 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 04:54 96-12-84.9 3.5



Date: 09/27/2010 06:48 PM Page 128 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Dibromochloromethane ND ug/kg 1 09/09/10 04:54 124-48-14.9 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 04:54 106-93-44.9 1.81,2-Dichlorobenzene ND ug/kg 1 09/09/10 04:54 95-50-14.9 1.91,3-Dichlorobenzene ND ug/kg 1 09/09/10 04:54 541-73-14.9 2.01,4-Dichlorobenzene ND ug/kg 1 09/09/10 04:54 106-46-74.9 1.7Dichlorodifluoromethane ND ug/kg 1 09/09/10 04:54 75-71-89.8 3.51,1-Dichloroethane ND ug/kg 1 09/09/10 04:54 75-34-34.9 1.51,2-Dichloroethane ND ug/kg 1 09/09/10 04:54 107-06-24.9 2.21,1-Dichloroethene ND ug/kg 1 09/09/10 04:54 75-35-44.9 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 04:54 156-59-24.9 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 04:54 156-60-54.9 1.91,2-Dichloropropane ND ug/kg 1 09/09/10 04:54 78-87-54.9 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 04:54 10061-01-54.9 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 04:54 10061-02-64.9 1.5Ethylbenzene ND ug/kg 1 09/09/10 04:54 100-41-44.9 1.82-Hexanone ND ug/kg 1 09/09/10 04:54 591-78-648.9 3.8Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 04:54 98-82-84.9 1.9Methyl acetate ND ug/kg 1 09/09/10 04:54 79-20-99.8 1.4Methylcyclohexane ND ug/kg 1 09/09/10 04:54 108-87-29.8 1.5Methylene Chloride ND ug/kg 1 09/09/10 04:54 75-09-219.6 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 04:54 108-10-148.9 3.6Methyl-tert-butyl ether ND ug/kg 1 09/09/10 04:54 1634-04-44.9 1.5Styrene ND ug/kg 1 09/09/10 04:54 100-42-54.9 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 04:54 79-34-54.9 1.9Tetrachloroethene ND ug/kg 1 09/09/10 04:54 127-18-44.9 1.7Toluene ND ug/kg 1 09/09/10 04:54 108-88-34.9 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 04:54 87-61-64.9 2.21,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 04:54 120-82-14.9 1.61,1,1-Trichloroethane ND ug/kg 1 09/09/10 04:54 71-55-64.9 1.81,1,2-Trichloroethane ND ug/kg 1 09/09/10 04:54 79-00-54.9 2.1Trichloroethene 28.0 ug/kg 1 09/09/10 04:54 79-01-64.9 2.1Trichlorofluoromethane ND ug/kg 1 09/09/10 04:54 75-69-44.9 2.21,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/09/10 04:54 76-13-14.9 1.9Vinyl chloride ND ug/kg 1 09/09/10 04:54 75-01-49.8 1.8Xylene (Total) ND ug/kg 1 09/09/10 04:54 1330-20-79.8 3.5m&p-Xylene ND ug/kg 1 09/09/10 04:54 179601-23-19.8 3.5o-Xylene ND ug/kg 1 09/09/10 04:54 95-47-64.9 1.9Dibromofluoromethane (S) 100 % 1 09/09/10 04:54 1868-53-770-130Toluene-d8 (S) 100 % 1 09/09/10 04:54 2037-26-570-1304-Bromofluorobenzene (S) 100 % 1 09/09/10 04:54 460-00-470-1301,2-Dichloroethane-d4 (S) 103 % 1 09/09/10 04:54 17060-07-070-132





Date: 09/27/2010 06:48 PM Page 129 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Cyanide ND mg/kg 1 09/14/10 10:16 57-12-50.14 0.14





Date: 09/27/2010 06:48 PM Page 130 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744









Date: 09/27/2010 06:48 PM Page 131 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 5 09/22/10 17:06 7440-36-0 D309/09/10 14:302.2 1.2Arsenic 1.4J mg/kg 5 09/22/10 17:06 7440-38-2 D309/09/10 14:302.2 1.4Beryllium 1.2 mg/kg 5 09/22/10 17:06 7440-41-709/09/10 14:300.44 0.088Cadmium ND mg/kg 5 09/22/10 17:06 7440-43-9 D309/09/10 14:300.44 0.27Chromium 13.3 mg/kg 5 09/22/10 17:06 7440-47-309/09/10 14:302.2 0.13Copper 2.7 mg/kg 5 09/22/10 17:06 7440-50-809/09/10 14:302.2 0.18Lead 11.3 mg/kg 5 09/22/10 17:06 7439-92-109/09/10 14:302.2 2.1Manganese 2510 mg/kg 5 09/22/10 17:06 7439-96-509/09/10 14:302.2 0.13Nickel 10.4 mg/kg 5 09/22/10 17:06 7440-02-009/09/10 14:302.2 0.80Selenium ND mg/kg 5 09/22/10 17:06 7782-49-2 D309/09/10 14:304.4 1.7Silver ND mg/kg 5 09/22/10 17:06 7440-22-4 D309/09/10 14:302.2 0.13Thallium 2.1J mg/kg 5 09/22/10 17:06 7440-28-0 D309/09/10 14:304.4 1.1Zinc 59.2 mg/kg 5 09/22/10 17:06 7440-66-609/09/10 14:304.4 1.1


Mercury 0.010 mg/kg 1 09/15/10 13:03 7439-97-609/14/10 08:110.0042 0.000083





Date: 09/27/2010 06:48 PM Page 132 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/24/10 14:18 91-94-109/13/10 18:301690 73.82,4-Dichlorophenol ND ug/kg 1 09/24/10 14:18 120-83-209/13/10 18:30338 73.8Diethylphthalate ND ug/kg 1 09/24/10 14:18 84-66-209/13/10 18:30338 52.32,4-Dimethylphenol ND ug/kg 1 09/24/10 14:18 105-67-909/13/10 18:30338 133Dimethylphthalate ND ug/kg 1 09/24/10 14:18 131-11-309/13/10 18:30338 68.7Di-n-butylphthalate ND ug/kg 1 09/24/10 14:18 84-74-209/13/10 18:30338 55.44,6-Dinitro-2-methylphenol ND ug/kg 1 09/24/10 14:18 534-52-109/13/10 18:30677 67.72,4-Dinitrophenol ND ug/kg 1 09/24/10 14:18 51-28-509/13/10 18:301690 55.42,4-Dinitrotoluene ND ug/kg 1 09/24/10 14:18 121-14-209/13/10 18:30338 63.62,6-Dinitrotoluene ND ug/kg 1 09/24/10 14:18 606-20-209/13/10 18:30338 70.8Di-n-octylphthalate ND ug/kg 1 09/24/10 14:18 117-84-009/13/10 18:30338 70.8bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/24/10 14:18 117-81-709/13/10 18:30338 92.3Fluoranthene ND ug/kg 1 09/24/10 14:18 206-44-009/13/10 18:30338 49.2Fluorene ND ug/kg 1 09/24/10 14:18 86-73-709/13/10 18:30338 69.7Hexachloro-1,3-butadiene ND ug/kg 1 09/24/10 14:18 87-68-309/13/10 18:30338 58.5Hexachlorobenzene ND ug/kg 1 09/24/10 14:18 118-74-109/13/10 18:30338 43.1Hexachlorocyclopentadiene ND ug/kg 1 09/24/10 14:18 77-47-409/13/10 18:30338 62.6Hexachloroethane ND ug/kg 1 09/24/10 14:18 67-72-109/13/10 18:30338 89.2Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/24/10 14:18 193-39-509/13/10 18:30338 69.7Isophorone ND ug/kg 1 09/24/10 14:18 78-59-109/13/10 18:30338 75.92-Methylnaphthalene ND ug/kg 1 09/24/10 14:18 91-57-609/13/10 18:30338 72.82-Methylphenol(o-Cresol) ND ug/kg 1 09/24/10 14:18 95-48-709/13/10 18:30338 1033&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/24/10 14:1809/13/10 18:30338 133Naphthalene ND ug/kg 1 09/24/10 14:18 91-20-309/13/10 18:30338 83.12-Nitroaniline ND ug/kg 1 09/24/10 14:18 88-74-409/13/10 18:301690 1053-Nitroaniline ND ug/kg 1 09/24/10 14:18 99-09-209/13/10 18:301690 92.34-Nitroaniline ND ug/kg 1 09/24/10 14:18 100-01-609/13/10 18:30677 95.4Nitrobenzene ND ug/kg 1 09/24/10 14:18 98-95-309/13/10 18:30338 92.32-Nitrophenol ND ug/kg 1 09/24/10 14:18 88-75-509/13/10 18:30338 82.04-Nitrophenol ND ug/kg 1 09/24/10 14:18 100-02-709/13/10 18:301690 60.5N-Nitroso-di-n-propylamine ND ug/kg 1 09/24/10 14:18 621-64-709/13/10 18:30338 64.6N-Nitrosodiphenylamine ND ug/kg 1 09/24/10 14:18 86-30-609/13/10 18:30338 101Pentachlorophenol ND ug/kg 1 09/24/10 14:18 87-86-509/13/10 18:301690 61.5Phenanthrene ND ug/kg 1 09/24/10 14:18 85-01-809/13/10 18:30338 56.4Phenol ND ug/kg 1 09/24/10 14:18 108-95-209/13/10 18:30338 102Pyrene ND ug/kg 1 09/24/10 14:18 129-00-009/13/10 18:30338 57.41,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/24/10 14:18 95-94-309/13/10 18:30338 1232,3,4,6-Tetrachlorophenol ND ug/kg 1 09/24/10 14:18 58-90-209/13/10 18:30338 1332,4,5-Trichlorophenol ND ug/kg 1 09/24/10 14:18 95-95-409/13/10 18:30338 1052,4,6-Trichlorophenol ND ug/kg 1 09/24/10 14:18 88-06-209/13/10 18:30338 74.92-Fluorobiphenyl (S) 29 % 1 09/24/10 14:18 321-60-8 S209/13/10 18:3030-110Terphenyl-d14 (S) 36 % 1 09/24/10 14:18 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 20 % 1 09/24/10 14:18 13127-88-3 S209/13/10 18:3022-1102-Fluorophenol (S) 20 % 1 09/24/10 14:18 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 29 % 1 09/24/10 14:18 118-79-609/13/10 18:3027-110



Date: 09/27/2010 06:48 PM Page 133 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Acetone ND ug/kg 1 09/09/10 05:13 67-64-196.0 9.6Benzene ND ug/kg 1 09/09/10 05:13 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/09/10 05:13 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/09/10 05:13 75-27-44.8 1.8Bromoform ND ug/kg 1 09/09/10 05:13 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/09/10 05:13 74-83-99.6 2.42-Butanone (MEK) ND ug/kg 1 09/09/10 05:13 78-93-396.0 2.8Carbon disulfide ND ug/kg 1 09/09/10 05:13 75-15-09.6 2.9Carbon tetrachloride ND ug/kg 1 09/09/10 05:13 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/09/10 05:13 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/09/10 05:13 75-00-39.6 2.3Chloroform ND ug/kg 1 09/09/10 05:13 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/09/10 05:13 74-87-39.6 2.3Cyclohexane ND ug/kg 1 09/09/10 05:13 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 05:13 96-12-84.8 3.5Dibromochloromethane ND ug/kg 1 09/09/10 05:13 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 05:13 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/09/10 05:13 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/09/10 05:13 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/09/10 05:13 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/09/10 05:13 75-71-89.6 3.51,1-Dichloroethane ND ug/kg 1 09/09/10 05:13 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/09/10 05:13 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/09/10 05:13 75-35-44.8 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 05:13 156-59-24.8 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 05:13 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/09/10 05:13 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 05:13 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 05:13 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/09/10 05:13 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/09/10 05:13 591-78-648.0 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 05:13 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/09/10 05:13 79-20-99.6 1.3Methylcyclohexane ND ug/kg 1 09/09/10 05:13 108-87-29.6 1.4Methylene Chloride ND ug/kg 1 09/09/10 05:13 75-09-219.2 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 05:13 108-10-148.0 3.6Methyl-tert-butyl ether ND ug/kg 1 09/09/10 05:13 1634-04-44.8 1.4Styrene ND ug/kg 1 09/09/10 05:13 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 05:13 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/09/10 05:13 127-18-44.8 1.6Toluene ND ug/kg 1 09/09/10 05:13 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 05:13 87-61-64.8 2.1



Date: 09/27/2010 06:48 PM Page 134 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




1,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 05:13 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/09/10 05:13 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/09/10 05:13 79-00-54.8 2.0Trichloroethene ND ug/kg 1 09/09/10 05:13 79-01-64.8 2.0Trichlorofluoromethane ND ug/kg 1 09/09/10 05:13 75-69-44.8 2.11,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/09/10 05:13 76-13-14.8 1.8Vinyl chloride ND ug/kg 1 09/09/10 05:13 75-01-49.6 1.7Xylene (Total) ND ug/kg 1 09/09/10 05:13 1330-20-79.6 3.5m&p-Xylene ND ug/kg 1 09/09/10 05:13 179601-23-19.6 3.5o-Xylene ND ug/kg 1 09/09/10 05:13 95-47-64.8 1.8Dibromofluoromethane (S) 104 % 1 09/09/10 05:13 1868-53-770-130Toluene-d8 (S) 101 % 1 09/09/10 05:13 2037-26-570-1304-Bromofluorobenzene (S) 99 % 1 09/09/10 05:13 460-00-470-1301,2-Dichloroethane-d4 (S) 108 % 1 09/09/10 05:13 17060-07-070-132




Cyanide ND mg/kg 1 09/14/10 10:18 57-12-50.16 0.16



Date: 09/27/2010 06:48 PM Page 135 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acetone ND ug/kg 1 09/09/10 05:31 67-64-1104 10.4Benzene ND ug/kg 1 09/09/10 05:31 71-43-25.2 1.7Bromochloromethane ND ug/kg 1 09/09/10 05:31 74-97-55.2 1.8Bromodichloromethane ND ug/kg 1 09/09/10 05:31 75-27-45.2 2.0Bromoform ND ug/kg 1 09/09/10 05:31 75-25-25.2 2.4Bromomethane ND ug/kg 1 09/09/10 05:31 74-83-910.4 2.62-Butanone (MEK) ND ug/kg 1 09/09/10 05:31 78-93-3104 3.0Carbon disulfide ND ug/kg 1 09/09/10 05:31 75-15-010.4 3.1Carbon tetrachloride ND ug/kg 1 09/09/10 05:31 56-23-55.2 2.7Chlorobenzene ND ug/kg 1 09/09/10 05:31 108-90-75.2 2.0Chloroethane ND ug/kg 1 09/09/10 05:31 75-00-310.4 2.5Chloroform ND ug/kg 1 09/09/10 05:31 67-66-35.2 1.7Chloromethane ND ug/kg 1 09/09/10 05:31 74-87-310.4 2.5Cyclohexane ND ug/kg 1 09/09/10 05:31 110-82-75.2 1.71,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 05:31 96-12-85.2 3.7Dibromochloromethane ND ug/kg 1 09/09/10 05:31 124-48-15.2 1.91,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 05:31 106-93-45.2 1.91,2-Dichlorobenzene ND ug/kg 1 09/09/10 05:31 95-50-15.2 2.01,3-Dichlorobenzene ND ug/kg 1 09/09/10 05:31 541-73-15.2 2.11,4-Dichlorobenzene ND ug/kg 1 09/09/10 05:31 106-46-75.2 1.8Dichlorodifluoromethane ND ug/kg 1 09/09/10 05:31 75-71-810.4 3.71,1-Dichloroethane ND ug/kg 1 09/09/10 05:31 75-34-35.2 1.61,2-Dichloroethane ND ug/kg 1 09/09/10 05:31 107-06-25.2 2.31,1-Dichloroethene ND ug/kg 1 09/09/10 05:31 75-35-45.2 1.9cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 05:31 156-59-25.2 1.5trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 05:31 156-60-55.2 2.01,2-Dichloropropane ND ug/kg 1 09/09/10 05:31 78-87-55.2 1.8cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 05:31 10061-01-55.2 1.9trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 05:31 10061-02-65.2 1.6Ethylbenzene ND ug/kg 1 09/09/10 05:31 100-41-45.2 1.92-Hexanone ND ug/kg 1 09/09/10 05:31 591-78-651.8 4.0Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 05:31 98-82-85.2 2.0Methyl acetate ND ug/kg 1 09/09/10 05:31 79-20-910.4 1.5Methylcyclohexane ND ug/kg 1 09/09/10 05:31 108-87-210.4 1.6Methylene Chloride ND ug/kg 1 09/09/10 05:31 75-09-220.7 3.14-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 05:31 108-10-151.8 3.8Methyl-tert-butyl ether ND ug/kg 1 09/09/10 05:31 1634-04-45.2 1.6Styrene ND ug/kg 1 09/09/10 05:31 100-42-55.2 1.91,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 05:31 79-34-55.2 2.0Tetrachloroethene ND ug/kg 1 09/09/10 05:31 127-18-45.2 1.8Toluene ND ug/kg 1 09/09/10 05:31 108-88-35.2 1.91,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 05:31 87-61-65.2 2.31,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 05:31 120-82-15.2 1.71,1,1-Trichloroethane ND ug/kg 1 09/09/10 05:31 71-55-65.2 1.91,1,2-Trichloroethane ND ug/kg 1 09/09/10 05:31 79-00-55.2 2.2



Date: 09/27/2010 06:48 PM Page 136 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Trichloroethene ND ug/kg 1 09/09/10 05:31 79-01-65.2 2.2Trichlorofluoromethane ND ug/kg 1 09/09/10 05:31 75-69-45.2 2.31,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/09/10 05:31 76-13-15.2 2.0Vinyl chloride ND ug/kg 1 09/09/10 05:31 75-01-410.4 1.9Xylene (Total) ND ug/kg 1 09/09/10 05:31 1330-20-710.4 3.7m&p-Xylene ND ug/kg 1 09/09/10 05:31 179601-23-110.4 3.7o-Xylene ND ug/kg 1 09/09/10 05:31 95-47-65.2 2.0Dibromofluoromethane (S) 102 % 1 09/09/10 05:31 1868-53-770-130Toluene-d8 (S) 101 % 1 09/09/10 05:31 2037-26-570-1304-Bromofluorobenzene (S) 98 % 1 09/09/10 05:31 460-00-470-1301,2-Dichloroethane-d4 (S) 106 % 1 09/09/10 05:31 17060-07-070-132





Date: 09/27/2010 06:48 PM Page 137 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.00018J mg/kg 1 09/15/10 13:05 7439-97-609/14/10 08:110.0057 0.00011





Date: 09/27/2010 06:48 PM Page 138 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 139 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/24/10 14:55 4165-60-009/13/10 18:3023-110




Cyanide ND mg/kg 1 09/14/10 10:18 57-12-50.11 0.11





Date: 09/27/2010 06:48 PM Page 140 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Cyanide ND mg/kg 1 09/14/10 10:19 57-12-50.17 0.17



Date: 09/27/2010 06:48 PM Page 141 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 17:21 7440-36-0 D309/09/10 14:305.4 3.1Arsenic ND mg/kg 10 09/22/10 17:21 7440-38-2 D309/09/10 14:305.4 3.5Beryllium 1.8 mg/kg 10 09/22/10 17:21 7440-41-709/09/10 14:301.1 0.22Cadmium ND mg/kg 10 09/22/10 17:21 7440-43-9 D309/09/10 14:301.1 0.65Chromium 19.5 mg/kg 10 09/22/10 17:21 7440-47-309/09/10 14:305.4 0.33Copper 7.3 mg/kg 10 09/22/10 17:21 7440-50-809/09/10 14:305.4 0.44Lead ND mg/kg 10 09/22/10 17:21 7439-92-1 D309/09/10 14:305.4 5.2Manganese 257 mg/kg 10 09/22/10 17:21 7439-96-509/09/10 14:305.4 0.33Nickel 11.8 mg/kg 10 09/22/10 17:21 7440-02-009/09/10 14:305.4 2.0Selenium ND mg/kg 10 09/22/10 17:21 7782-49-2 D309/09/10 14:3010.9 4.1Silver ND mg/kg 10 09/22/10 17:21 7440-22-4 D309/09/10 14:305.4 0.33Thallium ND mg/kg 10 09/22/10 17:21 7440-28-0 D309/09/10 14:3010.9 2.8Zinc 77.1 mg/kg 10 09/22/10 17:21 7440-66-609/09/10 14:3010.9 2.8


Mercury ND mg/kg 1 09/15/10 13:08 7439-97-609/14/10 08:110.0034 0.000068





Date: 09/27/2010 06:48 PM Page 142 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 143 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 30 % 1 09/19/10 04:05 4165-60-009/13/10 18:3023-110


Acetone 18.1J ug/kg 1 09/09/10 05:50 67-64-1102 10.2Benzene ND ug/kg 1 09/09/10 05:50 71-43-25.1 1.6Bromochloromethane ND ug/kg 1 09/09/10 05:50 74-97-55.1 1.7Bromodichloromethane ND ug/kg 1 09/09/10 05:50 75-27-45.1 1.9Bromoform ND ug/kg 1 09/09/10 05:50 75-25-25.1 2.3Bromomethane ND ug/kg 1 09/09/10 05:50 74-83-910.2 2.52-Butanone (MEK) ND ug/kg 1 09/09/10 05:50 78-93-3102 2.9Carbon disulfide ND ug/kg 1 09/09/10 05:50 75-15-010.2 3.0Carbon tetrachloride ND ug/kg 1 09/09/10 05:50 56-23-55.1 2.6Chlorobenzene ND ug/kg 1 09/09/10 05:50 108-90-75.1 1.9Chloroethane ND ug/kg 1 09/09/10 05:50 75-00-310.2 2.4Chloroform ND ug/kg 1 09/09/10 05:50 67-66-35.1 1.6Chloromethane ND ug/kg 1 09/09/10 05:50 74-87-310.2 2.4Cyclohexane ND ug/kg 1 09/09/10 05:50 110-82-75.1 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 05:50 96-12-85.1 3.7Dibromochloromethane ND ug/kg 1 09/09/10 05:50 124-48-15.1 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 05:50 106-93-45.1 1.81,2-Dichlorobenzene ND ug/kg 1 09/09/10 05:50 95-50-15.1 1.91,3-Dichlorobenzene ND ug/kg 1 09/09/10 05:50 541-73-15.1 2.01,4-Dichlorobenzene ND ug/kg 1 09/09/10 05:50 106-46-75.1 1.7Dichlorodifluoromethane ND ug/kg 1 09/09/10 05:50 75-71-810.2 3.71,1-Dichloroethane ND ug/kg 1 09/09/10 05:50 75-34-35.1 1.51,2-Dichloroethane ND ug/kg 1 09/09/10 05:50 107-06-25.1 2.21,1-Dichloroethene ND ug/kg 1 09/09/10 05:50 75-35-45.1 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 05:50 156-59-25.1 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 05:50 156-60-55.1 1.91,2-Dichloropropane ND ug/kg 1 09/09/10 05:50 78-87-55.1 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 05:50 10061-01-55.1 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 05:50 10061-02-65.1 1.5Ethylbenzene ND ug/kg 1 09/09/10 05:50 100-41-45.1 1.82-Hexanone ND ug/kg 1 09/09/10 05:50 591-78-650.8 4.0Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 05:50 98-82-85.1 1.9Methyl acetate ND ug/kg 1 09/09/10 05:50 79-20-910.2 1.4Methylcyclohexane ND ug/kg 1 09/09/10 05:50 108-87-210.2 1.5Methylene Chloride ND ug/kg 1 09/09/10 05:50 75-09-220.3 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 05:50 108-10-150.8 3.8Methyl-tert-butyl ether ND ug/kg 1 09/09/10 05:50 1634-04-45.1 1.5Styrene ND ug/kg 1 09/09/10 05:50 100-42-55.1 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 05:50 79-34-55.1 1.9Tetrachloroethene ND ug/kg 1 09/09/10 05:50 127-18-45.1 1.7Toluene ND ug/kg 1 09/09/10 05:50 108-88-35.1 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 05:50 87-61-65.1 2.2



Date: 09/27/2010 06:48 PM Page 144 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744











Date: 09/27/2010 06:48 PM Page 145 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/19/10 04:41 83-32-909/13/10 18:30414 95.4Acenaphthylene ND ug/kg 1 09/19/10 04:41 208-96-809/13/10 18:30414 97.9Acetophenone ND ug/kg 1 09/19/10 04:41 98-86-209/13/10 18:30414 213Anthracene ND ug/kg 1 09/19/10 04:41 120-12-709/13/10 18:30414 92.8Atrazine ND ug/kg 1 09/19/10 04:41 1912-24-909/13/10 18:30828 163Benzaldehyde ND ug/kg 1 09/19/10 04:41 100-52-709/13/10 18:30828 414Benzo(a)anthracene ND ug/kg 1 09/19/10 04:41 56-55-309/13/10 18:30414 76.5Benzo(a)pyrene ND ug/kg 1 09/19/10 04:41 50-32-809/13/10 18:30414 79.0Benzo(b)fluoranthene ND ug/kg 1 09/19/10 04:41 205-99-209/13/10 18:30414 71.5Benzo(g,h,i)perylene ND ug/kg 1 09/19/10 04:41 191-24-209/13/10 18:30414 105Benzo(k)fluoranthene ND ug/kg 1 09/19/10 04:41 207-08-909/13/10 18:30414 81.6Biphenyl (Diphenyl) ND ug/kg 1 09/19/10 04:41 92-52-409/13/10 18:30414 1304-Bromophenylphenyl ether ND ug/kg 1 09/19/10 04:41 101-55-309/13/10 18:30414 75.3Butylbenzylphthalate ND ug/kg 1 09/19/10 04:41 85-68-709/13/10 18:30414 87.8Caprolactam ND ug/kg 1 09/19/10 04:41 105-60-209/13/10 18:30414 71.5Carbazole ND ug/kg 1 09/19/10 04:41 86-74-809/13/10 18:30414 79.04-Chloro-3-methylphenol ND ug/kg 1 09/19/10 04:41 59-50-709/13/10 18:30828 85.34-Chloroaniline ND ug/kg 1 09/19/10 04:41 106-47-809/13/10 18:302070 115bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/10 04:41 111-91-109/13/10 18:30414 96.6bis(2-Chloroethyl) ether ND ug/kg 1 09/19/10 04:41 111-44-409/13/10 18:30414 105bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/10 04:41 108-60-109/13/10 18:30414 1102-Chloronaphthalene ND ug/kg 1 09/19/10 04:41 91-58-709/13/10 18:30414 81.62-Chlorophenol ND ug/kg 1 09/19/10 04:41 95-57-809/13/10 18:30414 1134-Chlorophenylphenyl ether ND ug/kg 1 09/19/10 04:41 7005-72-309/13/10 18:30414 85.3Chrysene ND ug/kg 1 09/19/10 04:41 218-01-909/13/10 18:30414 55.2Dibenz(a,h)anthracene ND ug/kg 1 09/19/10 04:41 53-70-309/13/10 18:30414 87.8Dibenzofuran ND ug/kg 1 09/19/10 04:41 132-64-909/13/10 18:30414 67.73,3'-Dichlorobenzidine ND ug/kg 1 09/19/10 04:41 91-94-109/13/10 18:302070 90.32,4-Dichlorophenol ND ug/kg 1 09/19/10 04:41 120-83-209/13/10 18:30414 90.3Diethylphthalate ND ug/kg 1 09/19/10 04:41 84-66-209/13/10 18:30414 64.02,4-Dimethylphenol ND ug/kg 1 09/19/10 04:41 105-67-909/13/10 18:30414 163Dimethylphthalate ND ug/kg 1 09/19/10 04:41 131-11-309/13/10 18:30414 84.1Di-n-butylphthalate ND ug/kg 1 09/19/10 04:41 84-74-209/13/10 18:30414 67.74,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/10 04:41 534-52-109/13/10 18:30828 82.82,4-Dinitrophenol ND ug/kg 1 09/19/10 04:41 51-28-509/13/10 18:302070 67.72,4-Dinitrotoluene ND ug/kg 1 09/19/10 04:41 121-14-209/13/10 18:30414 77.82,6-Dinitrotoluene ND ug/kg 1 09/19/10 04:41 606-20-209/13/10 18:30414 86.6Di-n-octylphthalate ND ug/kg 1 09/19/10 04:41 117-84-009/13/10 18:30414 86.6bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/10 04:41 117-81-709/13/10 18:30414 113Fluoranthene ND ug/kg 1 09/19/10 04:41 206-44-009/13/10 18:30414 60.2Fluorene ND ug/kg 1 09/19/10 04:41 86-73-709/13/10 18:30414 85.3Hexachloro-1,3-butadiene ND ug/kg 1 09/19/10 04:41 87-68-309/13/10 18:30414 71.5Hexachlorobenzene ND ug/kg 1 09/19/10 04:41 118-74-109/13/10 18:30414 52.7Hexachlorocyclopentadiene ND ug/kg 1 09/19/10 04:41 77-47-409/13/10 18:30414 76.5Hexachloroethane ND ug/kg 1 09/19/10 04:41 67-72-109/13/10 18:30414 109



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/10 04:41 193-39-509/13/10 18:30414 85.3Isophorone ND ug/kg 1 09/19/10 04:41 78-59-109/13/10 18:30414 92.82-Methylnaphthalene ND ug/kg 1 09/19/10 04:41 91-57-609/13/10 18:30414 89.12-Methylphenol(o-Cresol) ND ug/kg 1 09/19/10 04:41 95-48-709/13/10 18:30414 1253&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/19/10 04:4109/13/10 18:30414 163Naphthalene ND ug/kg 1 09/19/10 04:41 91-20-309/13/10 18:30414 1022-Nitroaniline ND ug/kg 1 09/19/10 04:41 88-74-409/13/10 18:302070 1283-Nitroaniline ND ug/kg 1 09/19/10 04:41 99-09-209/13/10 18:302070 1134-Nitroaniline ND ug/kg 1 09/19/10 04:41 100-01-609/13/10 18:30828 117Nitrobenzene ND ug/kg 1 09/19/10 04:41 98-95-309/13/10 18:30414 1132-Nitrophenol ND ug/kg 1 09/19/10 04:41 88-75-509/13/10 18:30414 1004-Nitrophenol ND ug/kg 1 09/19/10 04:41 100-02-709/13/10 18:302070 74.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/10 04:41 621-64-709/13/10 18:30414 79.0N-Nitrosodiphenylamine ND ug/kg 1 09/19/10 04:41 86-30-609/13/10 18:30414 123Pentachlorophenol ND ug/kg 1 09/19/10 04:41 87-86-509/13/10 18:302070 75.3Phenanthrene ND ug/kg 1 09/19/10 04:41 85-01-809/13/10 18:30414 69.0Phenol ND ug/kg 1 09/19/10 04:41 108-95-209/13/10 18:30414 124Pyrene ND ug/kg 1 09/19/10 04:41 129-00-009/13/10 18:30414 70.31,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/19/10 04:41 95-94-309/13/10 18:30414 1512,3,4,6-Tetrachlorophenol ND ug/kg 1 09/19/10 04:41 58-90-209/13/10 18:30414 1632,4,5-Trichlorophenol ND ug/kg 1 09/19/10 04:41 95-95-409/13/10 18:30414 1282,4,6-Trichlorophenol ND ug/kg 1 09/19/10 04:41 88-06-209/13/10 18:30414 91.62-Fluorobiphenyl (S) 43 % 1 09/19/10 04:41 321-60-809/13/10 18:3030-110Terphenyl-d14 (S) 33 % 1 09/19/10 04:41 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 30 % 1 09/19/10 04:41 13127-88-309/13/10 18:3022-1102-Fluorophenol (S) 34 % 1 09/19/10 04:41 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 36 % 1 09/19/10 04:41 118-79-609/13/10 18:3027-110Nitrobenzene-d5 (S) 33 % 1 09/19/10 04:41 4165-60-009/13/10 18:3023-110





Date: 09/27/2010 06:48 PM Page 147 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury ND mg/kg 1 09/15/10 13:11 7439-97-609/14/10 08:110.0028 0.000056


Acetone ND ug/kg 1 09/09/10 06:08 67-64-199.9 10Benzene ND ug/kg 1 09/09/10 06:08 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/09/10 06:08 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/09/10 06:08 75-27-45.0 1.9Bromoform ND ug/kg 1 09/09/10 06:08 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/09/10 06:08 74-83-910 2.52-Butanone (MEK) ND ug/kg 1 09/09/10 06:08 78-93-399.9 2.9Carbon disulfide ND ug/kg 1 09/09/10 06:08 75-15-010 3.0Carbon tetrachloride ND ug/kg 1 09/09/10 06:08 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/09/10 06:08 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/09/10 06:08 75-00-310 2.4Chloroform ND ug/kg 1 09/09/10 06:08 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/09/10 06:08 74-87-310 2.4Cyclohexane ND ug/kg 1 09/09/10 06:08 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 06:08 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/09/10 06:08 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 06:08 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/09/10 06:08 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/09/10 06:08 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/09/10 06:08 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/09/10 06:08 75-71-810 3.61,1-Dichloroethane ND ug/kg 1 09/09/10 06:08 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/09/10 06:08 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/09/10 06:08 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 06:08 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 06:08 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/09/10 06:08 78-87-55.0 1.7



Date: 09/27/2010 06:48 PM Page 148 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 06:08 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 06:08 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/09/10 06:08 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/09/10 06:08 591-78-650.0 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 06:08 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/09/10 06:08 79-20-910 1.4Methylcyclohexane ND ug/kg 1 09/09/10 06:08 108-87-210 1.5Methylene Chloride ND ug/kg 1 09/09/10 06:08 75-09-220.0 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 06:08 108-10-150.0 3.7Methyl-tert-butyl ether ND ug/kg 1 09/09/10 06:08 1634-04-45.0 1.5Styrene ND ug/kg 1 09/09/10 06:08 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 06:08 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/09/10 06:08 127-18-45.0 1.7Toluene ND ug/kg 1 09/09/10 06:08 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 06:08 87-61-65.0 2.21,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 06:08 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/09/10 06:08 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/09/10 06:08 79-00-55.0 2.1Trichloroethene ND ug/kg 1 09/09/10 06:08 79-01-65.0 2.1Trichlorofluoromethane ND ug/kg 1 09/09/10 06:08 75-69-45.0 2.21,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/09/10 06:08 76-13-15.0 1.9Vinyl chloride ND ug/kg 1 09/09/10 06:08 75-01-410 1.8Xylene (Total) ND ug/kg 1 09/09/10 06:08 1330-20-710 3.6m&p-Xylene ND ug/kg 1 09/09/10 06:08 179601-23-110 3.6o-Xylene ND ug/kg 1 09/09/10 06:08 95-47-65.0 1.9Dibromofluoromethane (S) 103 % 1 09/09/10 06:08 1868-53-770-130Toluene-d8 (S) 99 % 1 09/09/10 06:08 2037-26-570-1304-Bromofluorobenzene (S) 96 % 1 09/09/10 06:08 460-00-470-1301,2-Dichloroethane-d4 (S) 109 % 1 09/09/10 06:08 17060-07-070-132




Cyanide ND mg/kg 1 09/14/10 10:22 57-12-50.15 0.15





Date: 09/27/2010 06:48 PM Page 149 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.0096 mg/kg 1 09/15/10 13:13 7439-97-609/14/10 08:110.0036 0.000072





Date: 09/27/2010 06:48 PM Page 150 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/19/10 06:28 91-94-109/13/10 18:301820 79.42,4-Dichlorophenol ND ug/kg 1 09/19/10 06:28 120-83-209/13/10 18:30364 79.4Diethylphthalate ND ug/kg 1 09/19/10 06:28 84-66-209/13/10 18:30364 56.32,4-Dimethylphenol ND ug/kg 1 09/19/10 06:28 105-67-909/13/10 18:30364 143Dimethylphthalate ND ug/kg 1 09/19/10 06:28 131-11-309/13/10 18:30364 73.9Di-n-butylphthalate ND ug/kg 1 09/19/10 06:28 84-74-209/13/10 18:30364 59.64,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/10 06:28 534-52-109/13/10 18:30728 72.82,4-Dinitrophenol ND ug/kg 1 09/19/10 06:28 51-28-509/13/10 18:301820 59.62,4-Dinitrotoluene ND ug/kg 1 09/19/10 06:28 121-14-209/13/10 18:30364 68.42,6-Dinitrotoluene ND ug/kg 1 09/19/10 06:28 606-20-209/13/10 18:30364 76.1Di-n-octylphthalate ND ug/kg 1 09/19/10 06:28 117-84-009/13/10 18:30364 76.1bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/10 06:28 117-81-709/13/10 18:30364 99.3Fluoranthene ND ug/kg 1 09/19/10 06:28 206-44-009/13/10 18:30364 52.9Fluorene ND ug/kg 1 09/19/10 06:28 86-73-709/13/10 18:30364 75.0Hexachloro-1,3-butadiene ND ug/kg 1 09/19/10 06:28 87-68-309/13/10 18:30364 62.9Hexachlorobenzene ND ug/kg 1 09/19/10 06:28 118-74-109/13/10 18:30364 46.3Hexachlorocyclopentadiene ND ug/kg 1 09/19/10 06:28 77-47-409/13/10 18:30364 67.3Hexachloroethane ND ug/kg 1 09/19/10 06:28 67-72-109/13/10 18:30364 96.0Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/10 06:28 193-39-509/13/10 18:30364 75.0Isophorone ND ug/kg 1 09/19/10 06:28 78-59-109/13/10 18:30364 81.62-Methylnaphthalene ND ug/kg 1 09/19/10 06:28 91-57-609/13/10 18:30364 78.32-Methylphenol(o-Cresol) ND ug/kg 1 09/19/10 06:28 95-48-709/13/10 18:30364 1103&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/19/10 06:2809/13/10 18:30364 143Naphthalene ND ug/kg 1 09/19/10 06:28 91-20-309/13/10 18:30364 89.32-Nitroaniline ND ug/kg 1 09/19/10 06:28 88-74-409/13/10 18:301820 1133-Nitroaniline ND ug/kg 1 09/19/10 06:28 99-09-209/13/10 18:301820 99.34-Nitroaniline ND ug/kg 1 09/19/10 06:28 100-01-609/13/10 18:30728 103Nitrobenzene ND ug/kg 1 09/19/10 06:28 98-95-309/13/10 18:30364 99.32-Nitrophenol ND ug/kg 1 09/19/10 06:28 88-75-509/13/10 18:30364 88.24-Nitrophenol ND ug/kg 1 09/19/10 06:28 100-02-709/13/10 18:301820 65.1N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/10 06:28 621-64-709/13/10 18:30364 69.5N-Nitrosodiphenylamine ND ug/kg 1 09/19/10 06:28 86-30-609/13/10 18:30364 108Pentachlorophenol ND ug/kg 1 09/19/10 06:28 87-86-509/13/10 18:301820 66.2Phenanthrene ND ug/kg 1 09/19/10 06:28 85-01-809/13/10 18:30364 60.7Phenol ND ug/kg 1 09/19/10 06:28 108-95-209/13/10 18:30364 109Pyrene ND ug/kg 1 09/19/10 06:28 129-00-009/13/10 18:30364 61.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/19/10 06:28 95-94-309/13/10 18:30364 1322,3,4,6-Tetrachlorophenol ND ug/kg 1 09/19/10 06:28 58-90-209/13/10 18:30364 1432,4,5-Trichlorophenol ND ug/kg 1 09/19/10 06:28 95-95-409/13/10 18:30364 1132,4,6-Trichlorophenol ND ug/kg 1 09/19/10 06:28 88-06-209/13/10 18:30364 80.52-Fluorobiphenyl (S) 28 % 1 09/19/10 06:28 321-60-8 S009/13/10 18:3030-110Terphenyl-d14 (S) 37 % 1 09/19/10 06:28 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 19 % 1 09/19/10 06:28 13127-88-3 S009/13/10 18:3022-1102-Fluorophenol (S) 21 % 1 09/19/10 06:28 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 33 % 1 09/19/10 06:28 118-79-609/13/10 18:3027-110



Date: 09/27/2010 06:48 PM Page 151 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/19/10 06:28 4165-60-009/13/10 18:3023-110


Acetone 41.9J ug/kg 1 09/09/10 17:54 67-64-1108 10.8Benzene ND ug/kg 1 09/09/10 17:54 71-43-25.4 1.7Bromochloromethane ND ug/kg 1 09/09/10 17:54 74-97-55.4 1.8Bromodichloromethane ND ug/kg 1 09/09/10 17:54 75-27-45.4 2.1Bromoform ND ug/kg 1 09/09/10 17:54 75-25-25.4 2.5Bromomethane ND ug/kg 1 09/09/10 17:54 74-83-910.8 2.72-Butanone (MEK) ND ug/kg 1 09/09/10 17:54 78-93-3108 3.1Carbon disulfide ND ug/kg 1 09/09/10 17:54 75-15-010.8 3.3Carbon tetrachloride ND ug/kg 1 09/09/10 17:54 56-23-55.4 2.8Chlorobenzene ND ug/kg 1 09/09/10 17:54 108-90-75.4 2.1Chloroethane ND ug/kg 1 09/09/10 17:54 75-00-310.8 2.6Chloroform ND ug/kg 1 09/09/10 17:54 67-66-35.4 1.7Chloromethane ND ug/kg 1 09/09/10 17:54 74-87-310.8 2.6Cyclohexane ND ug/kg 1 09/09/10 17:54 110-82-75.4 1.71,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 17:54 96-12-85.4 3.9Dibromochloromethane ND ug/kg 1 09/09/10 17:54 124-48-15.4 2.01,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 17:54 106-93-45.4 2.01,2-Dichlorobenzene ND ug/kg 1 09/09/10 17:54 95-50-15.4 2.11,3-Dichlorobenzene ND ug/kg 1 09/09/10 17:54 541-73-15.4 2.21,4-Dichlorobenzene ND ug/kg 1 09/09/10 17:54 106-46-75.4 1.8Dichlorodifluoromethane ND ug/kg 1 09/09/10 17:54 75-71-810.8 3.91,1-Dichloroethane ND ug/kg 1 09/09/10 17:54 75-34-35.4 1.61,2-Dichloroethane ND ug/kg 1 09/09/10 17:54 107-06-25.4 2.41,1-Dichloroethene ND ug/kg 1 09/09/10 17:54 75-35-45.4 2.0cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 17:54 156-59-25.4 1.5trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 17:54 156-60-55.4 2.11,2-Dichloropropane ND ug/kg 1 09/09/10 17:54 78-87-55.4 1.8cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 17:54 10061-01-55.4 2.0trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 17:54 10061-02-65.4 1.6Ethylbenzene ND ug/kg 1 09/09/10 17:54 100-41-45.4 2.02-Hexanone ND ug/kg 1 09/09/10 17:54 591-78-654.2 4.2Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 17:54 98-82-85.4 2.1Methyl acetate ND ug/kg 1 09/09/10 17:54 79-20-910.8 1.5Methylcyclohexane ND ug/kg 1 09/09/10 17:54 108-87-210.8 1.6Methylene Chloride 19.7J ug/kg 1 09/09/10 17:54 75-09-221.7 3.34-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 17:54 108-10-154.2 4.0Methyl-tert-butyl ether ND ug/kg 1 09/09/10 17:54 1634-04-45.4 1.6Styrene ND ug/kg 1 09/09/10 17:54 100-42-55.4 2.01,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 17:54 79-34-55.4 2.1Tetrachloroethene ND ug/kg 1 09/09/10 17:54 127-18-45.4 1.8Toluene ND ug/kg 1 09/09/10 17:54 108-88-35.4 2.01,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 17:54 87-61-65.4 2.4



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(828)254-7176

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Cyanide ND mg/kg 1 09/14/10 10:23 57-12-50.14 0.14





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Antimony ND mg/kg 10 09/22/10 17:41 7440-36-0 D309/09/10 14:303.2 1.8Arsenic ND mg/kg 10 09/22/10 17:41 7440-38-2 D309/09/10 14:303.2 2.1Beryllium 0.74 mg/kg 10 09/22/10 17:41 7440-41-709/09/10 14:300.65 0.13Cadmium ND mg/kg 10 09/22/10 17:41 7440-43-9 D309/09/10 14:300.65 0.39Chromium 15.7 mg/kg 10 09/22/10 17:41 7440-47-309/09/10 14:303.2 0.19Copper 11.4 mg/kg 10 09/22/10 17:41 7440-50-809/09/10 14:303.2 0.26Lead 6.3 mg/kg 10 09/22/10 17:41 7439-92-109/09/10 14:303.2 3.1Manganese 230 mg/kg 10 09/22/10 17:41 7439-96-509/09/10 14:303.2 0.19Nickel 10.1 mg/kg 10 09/22/10 17:41 7440-02-009/09/10 14:303.2 1.2Selenium ND mg/kg 10 09/22/10 17:41 7782-49-2 D309/09/10 14:306.5 2.5Silver ND mg/kg 10 09/22/10 17:41 7440-22-4 D309/09/10 14:303.2 0.19Thallium 2.0J mg/kg 10 09/22/10 17:41 7440-28-0 D309/09/10 14:306.5 1.7Zinc 73.6 mg/kg 10 09/22/10 17:41 7440-66-609/09/10 14:306.5 1.7


Mercury ND mg/kg 1 09/14/10 14:23 7439-97-6 M109/14/10 08:130.0034 0.000068





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(828)254-7176

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9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/24/10 15:32 91-94-109/13/10 18:301750 76.22,4-Dichlorophenol ND ug/kg 1 09/24/10 15:32 120-83-209/13/10 18:30349 76.2Diethylphthalate ND ug/kg 1 09/24/10 15:32 84-66-209/13/10 18:30349 54.02,4-Dimethylphenol ND ug/kg 1 09/24/10 15:32 105-67-909/13/10 18:30349 138Dimethylphthalate ND ug/kg 1 09/24/10 15:32 131-11-309/13/10 18:30349 70.9Di-n-butylphthalate ND ug/kg 1 09/24/10 15:32 84-74-209/13/10 18:30349 57.14,6-Dinitro-2-methylphenol ND ug/kg 1 09/24/10 15:32 534-52-109/13/10 18:30698 69.82,4-Dinitrophenol ND ug/kg 1 09/24/10 15:32 51-28-509/13/10 18:301750 57.12,4-Dinitrotoluene ND ug/kg 1 09/24/10 15:32 121-14-209/13/10 18:30349 65.62,6-Dinitrotoluene ND ug/kg 1 09/24/10 15:32 606-20-209/13/10 18:30349 73.0Di-n-octylphthalate ND ug/kg 1 09/24/10 15:32 117-84-009/13/10 18:30349 73.0bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/24/10 15:32 117-81-709/13/10 18:30349 95.2Fluoranthene ND ug/kg 1 09/24/10 15:32 206-44-009/13/10 18:30349 50.8Fluorene ND ug/kg 1 09/24/10 15:32 86-73-709/13/10 18:30349 72.0Hexachloro-1,3-butadiene ND ug/kg 1 09/24/10 15:32 87-68-309/13/10 18:30349 60.3Hexachlorobenzene ND ug/kg 1 09/24/10 15:32 118-74-109/13/10 18:30349 44.4Hexachlorocyclopentadiene ND ug/kg 1 09/24/10 15:32 77-47-409/13/10 18:30349 64.6Hexachloroethane ND ug/kg 1 09/24/10 15:32 67-72-109/13/10 18:30349 92.1Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/24/10 15:32 193-39-509/13/10 18:30349 72.0Isophorone ND ug/kg 1 09/24/10 15:32 78-59-109/13/10 18:30349 78.32-Methylnaphthalene ND ug/kg 1 09/24/10 15:32 91-57-609/13/10 18:30349 75.12-Methylphenol(o-Cresol) ND ug/kg 1 09/24/10 15:32 95-48-709/13/10 18:30349 1063&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/24/10 15:3209/13/10 18:30349 138Naphthalene ND ug/kg 1 09/24/10 15:32 91-20-309/13/10 18:30349 85.72-Nitroaniline ND ug/kg 1 09/24/10 15:32 88-74-409/13/10 18:301750 1083-Nitroaniline ND ug/kg 1 09/24/10 15:32 99-09-209/13/10 18:301750 95.24-Nitroaniline ND ug/kg 1 09/24/10 15:32 100-01-609/13/10 18:30698 98.4Nitrobenzene ND ug/kg 1 09/24/10 15:32 98-95-309/13/10 18:30349 95.22-Nitrophenol ND ug/kg 1 09/24/10 15:32 88-75-509/13/10 18:30349 84.74-Nitrophenol ND ug/kg 1 09/24/10 15:32 100-02-709/13/10 18:301750 62.4N-Nitroso-di-n-propylamine ND ug/kg 1 09/24/10 15:32 621-64-709/13/10 18:30349 66.7N-Nitrosodiphenylamine ND ug/kg 1 09/24/10 15:32 86-30-609/13/10 18:30349 104Pentachlorophenol ND ug/kg 1 09/24/10 15:32 87-86-509/13/10 18:301750 63.5Phenanthrene ND ug/kg 1 09/24/10 15:32 85-01-809/13/10 18:30349 58.2Phenol ND ug/kg 1 09/24/10 15:32 108-95-209/13/10 18:30349 105Pyrene ND ug/kg 1 09/24/10 15:32 129-00-009/13/10 18:30349 59.31,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/24/10 15:32 95-94-309/13/10 18:30349 1272,3,4,6-Tetrachlorophenol ND ug/kg 1 09/24/10 15:32 58-90-209/13/10 18:30349 1382,4,5-Trichlorophenol ND ug/kg 1 09/24/10 15:32 95-95-409/13/10 18:30349 1082,4,6-Trichlorophenol ND ug/kg 1 09/24/10 15:32 88-06-209/13/10 18:30349 77.22-Fluorobiphenyl (S) 34 % 1 09/24/10 15:32 321-60-809/13/10 18:3030-110Terphenyl-d14 (S) 48 % 1 09/24/10 15:32 1718-51-009/13/10 18:3028-110Phenol-d6 (S) 26 % 1 09/24/10 15:32 13127-88-309/13/10 18:3022-1102-Fluorophenol (S) 26 % 1 09/24/10 15:32 367-12-409/13/10 18:3013-1102,4,6-Tribromophenol (S) 39 % 1 09/24/10 15:32 118-79-609/13/10 18:3027-110



Date: 09/27/2010 06:48 PM Page 155 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 26 % 1 09/24/10 15:32 4165-60-009/13/10 18:3023-110





Date: 09/27/2010 06:48 PM Page 156 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/14/10 10:23 57-12-50.15 0.15





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury 0.00063J mg/kg 1 09/14/10 14:37 7439-97-609/14/10 08:130.0049 0.000098





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(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







Date: 09/27/2010 06:48 PM Page 159 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 30 % 1 09/24/10 16:09 4165-60-009/13/10 18:3023-110





Date: 09/27/2010 06:48 PM Page 160 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/14/10 10:27 57-12-50.12 0.12





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(704)875-9092


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(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury ND mg/kg 1 09/14/10 14:39 7439-97-609/14/10 08:130.0037 0.000074


Acenaphthene ND ug/kg 1 09/25/10 04:28 83-32-909/15/10 13:00350 80.7Acenaphthylene ND ug/kg 1 09/25/10 04:28 208-96-809/15/10 13:00350 82.8Acetophenone ND ug/kg 1 09/25/10 04:28 98-86-209/15/10 13:00350 181Anthracene ND ug/kg 1 09/25/10 04:28 120-12-709/15/10 13:00350 78.6Atrazine ND ug/kg 1 09/25/10 04:28 1912-24-909/15/10 13:00701 138Benzaldehyde ND ug/kg 1 09/25/10 04:28 100-52-709/15/10 13:00701 350Benzo(a)anthracene ND ug/kg 1 09/25/10 04:28 56-55-309/15/10 13:00350 64.8Benzo(a)pyrene ND ug/kg 1 09/25/10 04:28 50-32-809/15/10 13:00350 66.9Benzo(b)fluoranthene ND ug/kg 1 09/25/10 04:28 205-99-209/15/10 13:00350 60.5Benzo(g,h,i)perylene ND ug/kg 1 09/25/10 04:28 191-24-209/15/10 13:00350 89.2Benzo(k)fluoranthene ND ug/kg 1 09/25/10 04:28 207-08-909/15/10 13:00350 69.0Biphenyl (Diphenyl) ND ug/kg 1 09/25/10 04:28 92-52-409/15/10 13:00350 1104-Bromophenylphenyl ether ND ug/kg 1 09/25/10 04:28 101-55-309/15/10 13:00350 63.7Butylbenzylphthalate ND ug/kg 1 09/25/10 04:28 85-68-709/15/10 13:00350 74.3Caprolactam ND ug/kg 1 09/25/10 04:28 105-60-209/15/10 13:00350 60.5Carbazole ND ug/kg 1 09/25/10 04:28 86-74-809/15/10 13:00350 66.94-Chloro-3-methylphenol ND ug/kg 1 09/25/10 04:28 59-50-709/15/10 13:00701 72.24-Chloroaniline ND ug/kg 1 09/25/10 04:28 106-47-809/15/10 13:001750 97.7bis(2-Chloroethoxy)methane ND ug/kg 1 09/25/10 04:28 111-91-109/15/10 13:00350 81.8bis(2-Chloroethyl) ether ND ug/kg 1 09/25/10 04:28 111-44-409/15/10 13:00350 89.2bis(2-Chloroisopropyl) ether ND ug/kg 1 09/25/10 04:28 108-60-109/15/10 13:00350 93.52-Chloronaphthalene ND ug/kg 1 09/25/10 04:28 91-58-709/15/10 13:00350 69.02-Chlorophenol ND ug/kg 1 09/25/10 04:28 95-57-809/15/10 13:00350 95.64-Chlorophenylphenyl ether ND ug/kg 1 09/25/10 04:28 7005-72-309/15/10 13:00350 72.2Chrysene ND ug/kg 1 09/25/10 04:28 218-01-909/15/10 13:00350 46.7Dibenz(a,h)anthracene 78.2J ug/kg 1 09/25/10 04:28 53-70-309/15/10 13:00350 74.3Dibenzofuran ND ug/kg 1 09/25/10 04:28 132-64-909/15/10 13:00350 57.3



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/25/10 04:28 91-94-109/15/10 13:001750 76.52,4-Dichlorophenol ND ug/kg 1 09/25/10 04:28 120-83-209/15/10 13:00350 76.5Diethylphthalate ND ug/kg 1 09/25/10 04:28 84-66-209/15/10 13:00350 54.22,4-Dimethylphenol ND ug/kg 1 09/25/10 04:28 105-67-909/15/10 13:00350 138Dimethylphthalate ND ug/kg 1 09/25/10 04:28 131-11-309/15/10 13:00350 71.2Di-n-butylphthalate ND ug/kg 1 09/25/10 04:28 84-74-209/15/10 13:00350 57.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/25/10 04:28 534-52-109/15/10 13:00701 70.12,4-Dinitrophenol ND ug/kg 1 09/25/10 04:28 51-28-509/15/10 13:001750 57.32,4-Dinitrotoluene ND ug/kg 1 09/25/10 04:28 121-14-209/15/10 13:00350 65.82,6-Dinitrotoluene ND ug/kg 1 09/25/10 04:28 606-20-209/15/10 13:00350 73.3Di-n-octylphthalate ND ug/kg 1 09/25/10 04:28 117-84-009/15/10 13:00350 73.3bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/25/10 04:28 117-81-709/15/10 13:00350 95.6Fluoranthene ND ug/kg 1 09/25/10 04:28 206-44-009/15/10 13:00350 51.0Fluorene ND ug/kg 1 09/25/10 04:28 86-73-709/15/10 13:00350 72.2Hexachloro-1,3-butadiene ND ug/kg 1 09/25/10 04:28 87-68-309/15/10 13:00350 60.5Hexachlorobenzene ND ug/kg 1 09/25/10 04:28 118-74-109/15/10 13:00350 44.6Hexachlorocyclopentadiene ND ug/kg 1 09/25/10 04:28 77-47-409/15/10 13:00350 64.8Hexachloroethane ND ug/kg 1 09/25/10 04:28 67-72-109/15/10 13:00350 92.4Indeno(1,2,3-cd)pyrene 72.6J ug/kg 1 09/25/10 04:28 193-39-509/15/10 13:00350 72.2Isophorone ND ug/kg 1 09/25/10 04:28 78-59-109/15/10 13:00350 78.62-Methylnaphthalene ND ug/kg 1 09/25/10 04:28 91-57-609/15/10 13:00350 75.42-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 04:28 95-48-709/15/10 13:00350 1063&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 04:2809/15/10 13:00350 138Naphthalene ND ug/kg 1 09/25/10 04:28 91-20-309/15/10 13:00350 86.02-Nitroaniline ND ug/kg 1 09/25/10 04:28 88-74-409/15/10 13:001750 1083-Nitroaniline ND ug/kg 1 09/25/10 04:28 99-09-209/15/10 13:001750 95.64-Nitroaniline ND ug/kg 1 09/25/10 04:28 100-01-609/15/10 13:00701 98.8Nitrobenzene ND ug/kg 1 09/25/10 04:28 98-95-309/15/10 13:00350 95.62-Nitrophenol ND ug/kg 1 09/25/10 04:28 88-75-509/15/10 13:00350 85.04-Nitrophenol ND ug/kg 1 09/25/10 04:28 100-02-709/15/10 13:001750 62.7N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 04:28 621-64-709/15/10 13:00350 66.9N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 04:28 86-30-609/15/10 13:00350 104Pentachlorophenol ND ug/kg 1 09/25/10 04:28 87-86-509/15/10 13:001750 63.7Phenanthrene ND ug/kg 1 09/25/10 04:28 85-01-809/15/10 13:00350 58.4Phenol ND ug/kg 1 09/25/10 04:28 108-95-209/15/10 13:00350 105Pyrene ND ug/kg 1 09/25/10 04:28 129-00-009/15/10 13:00350 59.51,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 04:28 95-94-309/15/10 13:00350 1272,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 04:28 58-90-209/15/10 13:00350 1382,4,5-Trichlorophenol ND ug/kg 1 09/25/10 04:28 95-95-409/15/10 13:00350 1082,4,6-Trichlorophenol ND ug/kg 1 09/25/10 04:28 88-06-209/15/10 13:00350 77.52-Fluorobiphenyl (S) 38 % 1 09/25/10 04:28 321-60-809/15/10 13:0030-110Terphenyl-d14 (S) 58 % 1 09/25/10 04:28 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 27 % 1 09/25/10 04:28 13127-88-309/15/10 13:0022-1102-Fluorophenol (S) 29 % 1 09/25/10 04:28 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 57 % 1 09/25/10 04:28 118-79-609/15/10 13:0027-110



Date: 09/27/2010 06:48 PM Page 163 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 32 % 1 09/25/10 04:28 4165-60-009/15/10 13:0023-110





Date: 09/27/2010 06:48 PM Page 164 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/14/10 10:29 57-12-50.18 0.18





Date: 09/27/2010 06:48 PM Page 165 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Mercury ND mg/kg 1 09/14/10 14:42 7439-97-609/14/10 08:130.0050 0.00010





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(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/20/10 16:51 91-94-109/15/10 13:001820 79.52,4-Dichlorophenol ND ug/kg 1 09/20/10 16:51 120-83-209/15/10 13:00364 79.5Diethylphthalate ND ug/kg 1 09/20/10 16:51 84-66-209/15/10 13:00364 56.32,4-Dimethylphenol ND ug/kg 1 09/20/10 16:51 105-67-909/15/10 13:00364 144Dimethylphthalate ND ug/kg 1 09/20/10 16:51 131-11-309/15/10 13:00364 74.0Di-n-butylphthalate ND ug/kg 1 09/20/10 16:51 84-74-209/15/10 13:00364 59.64,6-Dinitro-2-methylphenol ND ug/kg 1 09/20/10 16:51 534-52-109/15/10 13:00729 72.92,4-Dinitrophenol ND ug/kg 1 09/20/10 16:51 51-28-509/15/10 13:001820 59.62,4-Dinitrotoluene ND ug/kg 1 09/20/10 16:51 121-14-209/15/10 13:00364 68.52,6-Dinitrotoluene ND ug/kg 1 09/20/10 16:51 606-20-209/15/10 13:00364 76.2Di-n-octylphthalate ND ug/kg 1 09/20/10 16:51 117-84-009/15/10 13:00364 76.2bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/20/10 16:51 117-81-709/15/10 13:00364 99.4Fluoranthene ND ug/kg 1 09/20/10 16:51 206-44-009/15/10 13:00364 53.0Fluorene ND ug/kg 1 09/20/10 16:51 86-73-709/15/10 13:00364 75.1Hexachloro-1,3-butadiene ND ug/kg 1 09/20/10 16:51 87-68-309/15/10 13:00364 62.9Hexachlorobenzene ND ug/kg 1 09/20/10 16:51 118-74-109/15/10 13:00364 46.4Hexachlorocyclopentadiene ND ug/kg 1 09/20/10 16:51 77-47-409/15/10 13:00364 67.4Hexachloroethane ND ug/kg 1 09/20/10 16:51 67-72-109/15/10 13:00364 96.1Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/20/10 16:51 193-39-509/15/10 13:00364 75.1Isophorone ND ug/kg 1 09/20/10 16:51 78-59-109/15/10 13:00364 81.72-Methylnaphthalene ND ug/kg 1 09/20/10 16:51 91-57-609/15/10 13:00364 78.42-Methylphenol(o-Cresol) ND ug/kg 1 09/20/10 16:51 95-48-709/15/10 13:00364 1103&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/20/10 16:5109/15/10 13:00364 144Naphthalene ND ug/kg 1 09/20/10 16:51 91-20-309/15/10 13:00364 89.42-Nitroaniline ND ug/kg 1 09/20/10 16:51 88-74-409/15/10 13:001820 1133-Nitroaniline ND ug/kg 1 09/20/10 16:51 99-09-209/15/10 13:001820 99.44-Nitroaniline ND ug/kg 1 09/20/10 16:51 100-01-609/15/10 13:00729 103Nitrobenzene ND ug/kg 1 09/20/10 16:51 98-95-309/15/10 13:00364 99.42-Nitrophenol ND ug/kg 1 09/20/10 16:51 88-75-509/15/10 13:00364 88.34-Nitrophenol ND ug/kg 1 09/20/10 16:51 100-02-709/15/10 13:001820 65.2N-Nitroso-di-n-propylamine ND ug/kg 1 09/20/10 16:51 621-64-709/15/10 13:00364 69.6N-Nitrosodiphenylamine ND ug/kg 1 09/20/10 16:51 86-30-609/15/10 13:00364 108Pentachlorophenol ND ug/kg 1 09/20/10 16:51 87-86-509/15/10 13:001820 66.3Phenanthrene ND ug/kg 1 09/20/10 16:51 85-01-809/15/10 13:00364 60.7Phenol ND ug/kg 1 09/20/10 16:51 108-95-209/15/10 13:00364 109Pyrene ND ug/kg 1 09/20/10 16:51 129-00-009/15/10 13:00364 61.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/20/10 16:51 95-94-309/15/10 13:00364 1332,3,4,6-Tetrachlorophenol ND ug/kg 1 09/20/10 16:51 58-90-209/15/10 13:00364 1442,4,5-Trichlorophenol ND ug/kg 1 09/20/10 16:51 95-95-409/15/10 13:00364 1132,4,6-Trichlorophenol ND ug/kg 1 09/20/10 16:51 88-06-209/15/10 13:00364 80.62-Fluorobiphenyl (S) 31 % 1 09/20/10 16:51 321-60-809/15/10 13:0030-110Terphenyl-d14 (S) 33 % 1 09/20/10 16:51 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 19 % 1 09/20/10 16:51 13127-88-3 S009/15/10 13:0022-1102-Fluorophenol (S) 24 % 1 09/20/10 16:51 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 31 % 1 09/20/10 16:51 118-79-609/15/10 13:0027-110



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(828)254-7176

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Nitrobenzene-d5 (S) 26 % 1 09/20/10 16:51 4165-60-009/15/10 13:0023-110





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Cyanide ND mg/kg 1 09/14/10 10:30 57-12-50.16 0.16





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Acetone 44.0J ug/kg 1 09/09/10 17:35 67-64-1119 11.9Benzene ND ug/kg 1 09/09/10 17:35 71-43-25.9 1.9Bromochloromethane ND ug/kg 1 09/09/10 17:35 74-97-55.9 2.0Bromodichloromethane ND ug/kg 1 09/09/10 17:35 75-27-45.9 2.3Bromoform ND ug/kg 1 09/09/10 17:35 75-25-25.9 2.7Bromomethane ND ug/kg 1 09/09/10 17:35 74-83-911.9 3.02-Butanone (MEK) ND ug/kg 1 09/09/10 17:35 78-93-3119 3.4Carbon disulfide ND ug/kg 1 09/09/10 17:35 75-15-011.9 3.6Carbon tetrachloride ND ug/kg 1 09/09/10 17:35 56-23-55.9 3.1Chlorobenzene ND ug/kg 1 09/09/10 17:35 108-90-75.9 2.3Chloroethane ND ug/kg 1 09/09/10 17:35 75-00-311.9 2.8Chloroform ND ug/kg 1 09/09/10 17:35 67-66-35.9 1.9Chloromethane ND ug/kg 1 09/09/10 17:35 74-87-311.9 2.8Cyclohexane ND ug/kg 1 09/09/10 17:35 110-82-75.9 1.91,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 17:35 96-12-85.9 4.3Dibromochloromethane ND ug/kg 1 09/09/10 17:35 124-48-15.9 2.11,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 17:35 106-93-45.9 2.11,2-Dichlorobenzene ND ug/kg 1 09/09/10 17:35 95-50-15.9 2.31,3-Dichlorobenzene ND ug/kg 1 09/09/10 17:35 541-73-15.9 2.41,4-Dichlorobenzene ND ug/kg 1 09/09/10 17:35 106-46-75.9 2.0Dichlorodifluoromethane ND ug/kg 1 09/09/10 17:35 75-71-811.9 4.31,1-Dichloroethane ND ug/kg 1 09/09/10 17:35 75-34-35.9 1.81,2-Dichloroethane ND ug/kg 1 09/09/10 17:35 107-06-25.9 2.61,1-Dichloroethene ND ug/kg 1 09/09/10 17:35 75-35-45.9 2.1cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 17:35 156-59-25.9 1.7trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 17:35 156-60-55.9 2.31,2-Dichloropropane ND ug/kg 1 09/09/10 17:35 78-87-55.9 2.0cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 17:35 10061-01-55.9 2.1trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 17:35 10061-02-65.9 1.8Ethylbenzene ND ug/kg 1 09/09/10 17:35 100-41-45.9 2.12-Hexanone ND ug/kg 1 09/09/10 17:35 591-78-659.4 4.6Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 17:35 98-82-85.9 2.3Methyl acetate ND ug/kg 1 09/09/10 17:35 79-20-911.9 1.7Methylcyclohexane ND ug/kg 1 09/09/10 17:35 108-87-211.9 1.8Methylene Chloride ND ug/kg 1 09/09/10 17:35 75-09-223.7 3.64-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 17:35 108-10-159.4 4.4Methyl-tert-butyl ether ND ug/kg 1 09/09/10 17:35 1634-04-45.9 1.8Styrene ND ug/kg 1 09/09/10 17:35 100-42-55.9 2.11,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 17:35 79-34-55.9 2.3Tetrachloroethene ND ug/kg 1 09/09/10 17:35 127-18-45.9 2.0Toluene ND ug/kg 1 09/09/10 17:35 108-88-35.9 2.11,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 17:35 87-61-65.9 2.61,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 17:35 120-82-15.9 1.91,1,1-Trichloroethane ND ug/kg 1 09/09/10 17:35 71-55-65.9 2.11,1,2-Trichloroethane ND ug/kg 1 09/09/10 17:35 79-00-55.9 2.5



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(828)254-7176

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(704)875-9092


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Mercury 0.051 mg/kg 1 09/14/10 14:44 7439-97-609/14/10 08:130.0051 0.00010





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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/26/10 00:15 91-94-109/23/10 16:201790 78.12,4-Dichlorophenol ND ug/kg 1 09/26/10 00:15 120-83-209/23/10 16:20358 78.1Diethylphthalate ND ug/kg 1 09/26/10 00:15 84-66-209/23/10 16:20358 55.32,4-Dimethylphenol ND ug/kg 1 09/26/10 00:15 105-67-909/23/10 16:20358 141Dimethylphthalate ND ug/kg 1 09/26/10 00:15 131-11-309/23/10 16:20358 72.7Di-n-butylphthalate ND ug/kg 1 09/26/10 00:15 84-74-209/23/10 16:20358 58.64,6-Dinitro-2-methylphenol ND ug/kg 1 09/26/10 00:15 534-52-109/23/10 16:20716 71.62,4-Dinitrophenol ND ug/kg 1 09/26/10 00:15 51-28-509/23/10 16:201790 58.62,4-Dinitrotoluene ND ug/kg 1 09/26/10 00:15 121-14-209/23/10 16:20358 67.32,6-Dinitrotoluene ND ug/kg 1 09/26/10 00:15 606-20-209/23/10 16:20358 74.9Di-n-octylphthalate ND ug/kg 1 09/26/10 00:15 117-84-009/23/10 16:20358 74.9bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/26/10 00:15 117-81-709/23/10 16:20358 97.7Fluoranthene ND ug/kg 1 09/26/10 00:15 206-44-009/23/10 16:20358 52.1Fluorene ND ug/kg 1 09/26/10 00:15 86-73-709/23/10 16:20358 73.8Hexachloro-1,3-butadiene ND ug/kg 1 09/26/10 00:15 87-68-309/23/10 16:20358 61.9Hexachlorobenzene ND ug/kg 1 09/26/10 00:15 118-74-109/23/10 16:20358 45.6Hexachlorocyclopentadiene ND ug/kg 1 09/26/10 00:15 77-47-409/23/10 16:20358 66.2Hexachloroethane ND ug/kg 1 09/26/10 00:15 67-72-109/23/10 16:20358 94.4Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/26/10 00:15 193-39-509/23/10 16:20358 73.8Isophorone ND ug/kg 1 09/26/10 00:15 78-59-109/23/10 16:20358 80.32-Methylnaphthalene ND ug/kg 1 09/26/10 00:15 91-57-609/23/10 16:20358 77.02-Methylphenol(o-Cresol) ND ug/kg 1 09/26/10 00:15 95-48-709/23/10 16:20358 1093&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/26/10 00:1509/23/10 16:20358 141Naphthalene ND ug/kg 1 09/26/10 00:15 91-20-309/23/10 16:20358 87.92-Nitroaniline ND ug/kg 1 09/26/10 00:15 88-74-409/23/10 16:201790 1113-Nitroaniline ND ug/kg 1 09/26/10 00:15 99-09-209/23/10 16:201790 97.74-Nitroaniline ND ug/kg 1 09/26/10 00:15 100-01-609/23/10 16:20716 101Nitrobenzene ND ug/kg 1 09/26/10 00:15 98-95-309/23/10 16:20358 97.72-Nitrophenol ND ug/kg 1 09/26/10 00:15 88-75-509/23/10 16:20358 86.84-Nitrophenol ND ug/kg 1 09/26/10 00:15 100-02-709/23/10 16:201790 64.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/26/10 00:15 621-64-709/23/10 16:20358 68.4N-Nitrosodiphenylamine ND ug/kg 1 09/26/10 00:15 86-30-609/23/10 16:20358 106Pentachlorophenol ND ug/kg 1 09/26/10 00:15 87-86-509/23/10 16:201790 65.1Phenanthrene ND ug/kg 1 09/26/10 00:15 85-01-809/23/10 16:20358 59.7Phenol ND ug/kg 1 09/26/10 00:15 108-95-2 H509/23/10 16:20358 107Pyrene ND ug/kg 1 09/26/10 00:15 129-00-009/23/10 16:20358 60.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/26/10 00:15 95-94-309/23/10 16:20358 1302,3,4,6-Tetrachlorophenol ND ug/kg 1 09/26/10 00:15 58-90-209/23/10 16:20358 1412,4,5-Trichlorophenol ND ug/kg 1 09/26/10 00:15 95-95-409/23/10 16:20358 1112,4,6-Trichlorophenol ND ug/kg 1 09/26/10 00:15 88-06-209/23/10 16:20358 79.22-Fluorobiphenyl (S) 31 % 1 09/26/10 00:15 321-60-809/23/10 16:2030-110Terphenyl-d14 (S) 41 % 1 09/26/10 00:15 1718-51-009/23/10 16:2028-110Phenol-d6 (S) 20 % 1 09/26/10 00:15 13127-88-3 S209/23/10 16:2022-1102-Fluorophenol (S) 20 % 1 09/26/10 00:15 367-12-409/23/10 16:2013-1102,4,6-Tribromophenol (S) 38 % 1 09/26/10 00:15 118-79-609/23/10 16:2027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/26/10 00:15 4165-60-009/23/10 16:2023-110




Cyanide ND mg/kg 1 09/14/10 10:31 57-12-50.18 0.18





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Cyanide ND mg/kg 1 09/14/10 10:32 57-12-50.14 0.14



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Antimony ND mg/kg 10 09/22/10 17:59 7440-36-0 D309/09/10 14:304.0 2.2Arsenic ND mg/kg 10 09/22/10 17:59 7440-38-2 D309/09/10 14:304.0 2.6Beryllium 1.5 mg/kg 10 09/22/10 17:59 7440-41-709/09/10 14:300.80 0.16Cadmium ND mg/kg 10 09/22/10 17:59 7440-43-9 D309/09/10 14:300.80 0.48Chromium 20.2 mg/kg 10 09/22/10 17:59 7440-47-309/09/10 14:304.0 0.24Copper 9.7 mg/kg 10 09/22/10 17:59 7440-50-809/09/10 14:304.0 0.32Lead 9.5 mg/kg 10 09/22/10 17:59 7439-92-109/09/10 14:304.0 3.8Manganese 393 mg/kg 10 09/22/10 17:59 7439-96-509/09/10 14:304.0 0.24Nickel 17.6 mg/kg 10 09/22/10 17:59 7440-02-009/09/10 14:304.0 1.4Selenium ND mg/kg 10 09/22/10 17:59 7782-49-2 D309/09/10 14:308.0 3.0Silver ND mg/kg 10 09/22/10 17:59 7440-22-4 D309/09/10 14:304.0 0.24Thallium ND mg/kg 10 09/22/10 17:59 7440-28-0 D309/09/10 14:308.0 2.1Zinc 115 mg/kg 10 09/22/10 17:59 7440-66-609/09/10 14:308.0 2.1


Mercury 0.0075 mg/kg 1 09/14/10 14:47 7439-97-609/14/10 08:130.0035 0.000070





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9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/25/10 05:04 91-94-109/15/10 13:001720 75.12,4-Dichlorophenol ND ug/kg 1 09/25/10 05:04 120-83-209/15/10 13:00344 75.1Diethylphthalate ND ug/kg 1 09/25/10 05:04 84-66-209/15/10 13:00344 53.22,4-Dimethylphenol ND ug/kg 1 09/25/10 05:04 105-67-909/15/10 13:00344 136Dimethylphthalate ND ug/kg 1 09/25/10 05:04 131-11-309/15/10 13:00344 69.9Di-n-butylphthalate ND ug/kg 1 09/25/10 05:04 84-74-209/15/10 13:00344 56.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/25/10 05:04 534-52-109/15/10 13:00688 68.82,4-Dinitrophenol ND ug/kg 1 09/25/10 05:04 51-28-509/15/10 13:001720 56.32,4-Dinitrotoluene ND ug/kg 1 09/25/10 05:04 121-14-209/15/10 13:00344 64.62,6-Dinitrotoluene ND ug/kg 1 09/25/10 05:04 606-20-209/15/10 13:00344 71.9Di-n-octylphthalate ND ug/kg 1 09/25/10 05:04 117-84-009/15/10 13:00344 71.9bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/25/10 05:04 117-81-709/15/10 13:00344 93.8Fluoranthene ND ug/kg 1 09/25/10 05:04 206-44-009/15/10 13:00344 50.0Fluorene ND ug/kg 1 09/25/10 05:04 86-73-709/15/10 13:00344 70.9Hexachloro-1,3-butadiene ND ug/kg 1 09/25/10 05:04 87-68-309/15/10 13:00344 59.4Hexachlorobenzene ND ug/kg 1 09/25/10 05:04 118-74-109/15/10 13:00344 43.8Hexachlorocyclopentadiene ND ug/kg 1 09/25/10 05:04 77-47-409/15/10 13:00344 63.6Hexachloroethane ND ug/kg 1 09/25/10 05:04 67-72-109/15/10 13:00344 90.7Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/25/10 05:04 193-39-509/15/10 13:00344 70.9Isophorone ND ug/kg 1 09/25/10 05:04 78-59-109/15/10 13:00344 77.22-Methylnaphthalene ND ug/kg 1 09/25/10 05:04 91-57-609/15/10 13:00344 74.02-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 05:04 95-48-709/15/10 13:00344 1043&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 05:0409/15/10 13:00344 136Naphthalene ND ug/kg 1 09/25/10 05:04 91-20-309/15/10 13:00344 84.52-Nitroaniline ND ug/kg 1 09/25/10 05:04 88-74-409/15/10 13:001720 1063-Nitroaniline ND ug/kg 1 09/25/10 05:04 99-09-209/15/10 13:001720 93.84-Nitroaniline ND ug/kg 1 09/25/10 05:04 100-01-609/15/10 13:00688 97.0Nitrobenzene ND ug/kg 1 09/25/10 05:04 98-95-309/15/10 13:00344 93.82-Nitrophenol ND ug/kg 1 09/25/10 05:04 88-75-509/15/10 13:00344 83.44-Nitrophenol ND ug/kg 1 09/25/10 05:04 100-02-709/15/10 13:001720 61.5N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 05:04 621-64-709/15/10 13:00344 65.7N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 05:04 86-30-609/15/10 13:00344 102Pentachlorophenol ND ug/kg 1 09/25/10 05:04 87-86-509/15/10 13:001720 62.6Phenanthrene ND ug/kg 1 09/25/10 05:04 85-01-809/15/10 13:00344 57.3Phenol ND ug/kg 1 09/25/10 05:04 108-95-209/15/10 13:00344 103Pyrene ND ug/kg 1 09/25/10 05:04 129-00-009/15/10 13:00344 58.41,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 05:04 95-94-309/15/10 13:00344 1252,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 05:04 58-90-209/15/10 13:00344 1362,4,5-Trichlorophenol ND ug/kg 1 09/25/10 05:04 95-95-409/15/10 13:00344 1062,4,6-Trichlorophenol ND ug/kg 1 09/25/10 05:04 88-06-209/15/10 13:00344 76.12-Fluorobiphenyl (S) 10 % 1 09/25/10 05:04 321-60-8 S209/15/10 13:0030-110Terphenyl-d14 (S) 17 % 1 09/25/10 05:04 1718-51-0 S209/15/10 13:0028-110Phenol-d6 (S) 9 % 1 09/25/10 05:04 13127-88-3 S209/15/10 13:0022-1102-Fluorophenol (S) 7 % 1 09/25/10 05:04 367-12-4 S209/15/10 13:0013-1102,4,6-Tribromophenol (S) 12 % 1 09/25/10 05:04 118-79-6 S209/15/10 13:0027-110



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(828)254-7176

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(828)254-7176

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(828)254-7176

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ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 18:02 7440-36-0 D309/09/10 14:305.1 2.8Arsenic 4.6J mg/kg 10 09/22/10 18:02 7440-38-2 D309/09/10 14:305.1 3.3Beryllium 1.8 mg/kg 10 09/22/10 18:02 7440-41-709/09/10 14:301.0 0.20Cadmium ND mg/kg 10 09/22/10 18:02 7440-43-9 D309/09/10 14:301.0 0.61Chromium 27.3 mg/kg 10 09/22/10 18:02 7440-47-309/09/10 14:305.1 0.31Copper 4.3J mg/kg 10 09/22/10 18:02 7440-50-8 D309/09/10 14:305.1 0.41Lead 9.5 mg/kg 10 09/22/10 18:02 7439-92-109/09/10 14:305.1 4.9Manganese 664 mg/kg 10 09/22/10 18:02 7439-96-509/09/10 14:305.1 0.31Nickel 17.5 mg/kg 10 09/22/10 18:02 7440-02-009/09/10 14:305.1 1.8Selenium ND mg/kg 10 09/22/10 18:02 7782-49-2 D309/09/10 14:3010.2 3.9Silver ND mg/kg 10 09/22/10 18:02 7440-22-4 D309/09/10 14:305.1 0.31Thallium ND mg/kg 10 09/22/10 18:02 7440-28-0 D309/09/10 14:3010.2 2.6Zinc 93.5 mg/kg 10 09/22/10 18:02 7440-66-609/09/10 14:3010.2 2.6


Mercury 0.0046 mg/kg 1 09/14/10 14:50 7439-97-609/14/10 08:130.0045 0.000091





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/20/10 18:43 91-94-109/15/10 13:001850 80.62,4-Dichlorophenol ND ug/kg 1 09/20/10 18:43 120-83-209/15/10 13:00369 80.6Diethylphthalate ND ug/kg 1 09/20/10 18:43 84-66-209/15/10 13:00369 57.12,4-Dimethylphenol ND ug/kg 1 09/20/10 18:43 105-67-909/15/10 13:00369 145Dimethylphthalate ND ug/kg 1 09/20/10 18:43 131-11-309/15/10 13:00369 75.0Di-n-butylphthalate ND ug/kg 1 09/20/10 18:43 84-74-209/15/10 13:00369 60.44,6-Dinitro-2-methylphenol ND ug/kg 1 09/20/10 18:43 534-52-109/15/10 13:00738 73.82,4-Dinitrophenol ND ug/kg 1 09/20/10 18:43 51-28-509/15/10 13:001850 60.42,4-Dinitrotoluene ND ug/kg 1 09/20/10 18:43 121-14-209/15/10 13:00369 69.42,6-Dinitrotoluene ND ug/kg 1 09/20/10 18:43 606-20-209/15/10 13:00369 77.2Di-n-octylphthalate ND ug/kg 1 09/20/10 18:43 117-84-009/15/10 13:00369 77.2bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/20/10 18:43 117-81-709/15/10 13:00369 101Fluoranthene ND ug/kg 1 09/20/10 18:43 206-44-009/15/10 13:00369 53.7Fluorene ND ug/kg 1 09/20/10 18:43 86-73-709/15/10 13:00369 76.1Hexachloro-1,3-butadiene ND ug/kg 1 09/20/10 18:43 87-68-309/15/10 13:00369 63.8Hexachlorobenzene ND ug/kg 1 09/20/10 18:43 118-74-109/15/10 13:00369 47.0Hexachlorocyclopentadiene ND ug/kg 1 09/20/10 18:43 77-47-409/15/10 13:00369 68.2Hexachloroethane ND ug/kg 1 09/20/10 18:43 67-72-109/15/10 13:00369 97.3Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/20/10 18:43 193-39-509/15/10 13:00369 76.1Isophorone ND ug/kg 1 09/20/10 18:43 78-59-109/15/10 13:00369 82.82-Methylnaphthalene ND ug/kg 1 09/20/10 18:43 91-57-609/15/10 13:00369 79.42-Methylphenol(o-Cresol) ND ug/kg 1 09/20/10 18:43 95-48-709/15/10 13:00369 1123&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/20/10 18:4309/15/10 13:00369 145Naphthalene ND ug/kg 1 09/20/10 18:43 91-20-309/15/10 13:00369 90.62-Nitroaniline ND ug/kg 1 09/20/10 18:43 88-74-409/15/10 13:001850 1143-Nitroaniline ND ug/kg 1 09/20/10 18:43 99-09-209/15/10 13:001850 1014-Nitroaniline ND ug/kg 1 09/20/10 18:43 100-01-609/15/10 13:00738 104Nitrobenzene ND ug/kg 1 09/20/10 18:43 98-95-309/15/10 13:00369 1012-Nitrophenol ND ug/kg 1 09/20/10 18:43 88-75-509/15/10 13:00369 89.54-Nitrophenol ND ug/kg 1 09/20/10 18:43 100-02-709/15/10 13:001850 66.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/20/10 18:43 621-64-709/15/10 13:00369 70.5N-Nitrosodiphenylamine ND ug/kg 1 09/20/10 18:43 86-30-609/15/10 13:00369 110Pentachlorophenol ND ug/kg 1 09/20/10 18:43 87-86-509/15/10 13:001850 67.1Phenanthrene ND ug/kg 1 09/20/10 18:43 85-01-809/15/10 13:00369 61.5Phenol ND ug/kg 1 09/20/10 18:43 108-95-209/15/10 13:00369 111Pyrene ND ug/kg 1 09/20/10 18:43 129-00-009/15/10 13:00369 62.71,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/20/10 18:43 95-94-309/15/10 13:00369 1342,3,4,6-Tetrachlorophenol ND ug/kg 1 09/20/10 18:43 58-90-209/15/10 13:00369 1452,4,5-Trichlorophenol ND ug/kg 1 09/20/10 18:43 95-95-409/15/10 13:00369 1142,4,6-Trichlorophenol ND ug/kg 1 09/20/10 18:43 88-06-209/15/10 13:00369 81.72-Fluorobiphenyl (S) 31 % 1 09/20/10 18:43 321-60-809/15/10 13:0030-110Terphenyl-d14 (S) 36 % 1 09/20/10 18:43 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 21 % 1 09/20/10 18:43 13127-88-3 S009/15/10 13:0022-1102-Fluorophenol (S) 22 % 1 09/20/10 18:43 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 28 % 1 09/20/10 18:43 118-79-609/15/10 13:0027-110



Date: 09/27/2010 06:48 PM Page 182 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 25 % 1 09/20/10 18:43 4165-60-009/15/10 13:0023-110


Acetone ND ug/kg 1 09/09/10 07:59 67-64-1106 10.6Benzene ND ug/kg 1 09/09/10 07:59 71-43-25.3 1.7Bromochloromethane ND ug/kg 1 09/09/10 07:59 74-97-55.3 1.8Bromodichloromethane ND ug/kg 1 09/09/10 07:59 75-27-45.3 2.0Bromoform ND ug/kg 1 09/09/10 07:59 75-25-25.3 2.4Bromomethane ND ug/kg 1 09/09/10 07:59 74-83-910.6 2.72-Butanone (MEK) ND ug/kg 1 09/09/10 07:59 78-93-3106 3.1Carbon disulfide ND ug/kg 1 09/09/10 07:59 75-15-010.6 3.2Carbon tetrachloride ND ug/kg 1 09/09/10 07:59 56-23-55.3 2.8Chlorobenzene ND ug/kg 1 09/09/10 07:59 108-90-75.3 2.0Chloroethane ND ug/kg 1 09/09/10 07:59 75-00-310.6 2.5Chloroform ND ug/kg 1 09/09/10 07:59 67-66-35.3 1.7Chloromethane ND ug/kg 1 09/09/10 07:59 74-87-310.6 2.5Cyclohexane ND ug/kg 1 09/09/10 07:59 110-82-75.3 1.71,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 07:59 96-12-85.3 3.8Dibromochloromethane ND ug/kg 1 09/09/10 07:59 124-48-15.3 1.91,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 07:59 106-93-45.3 1.91,2-Dichlorobenzene ND ug/kg 1 09/09/10 07:59 95-50-15.3 2.01,3-Dichlorobenzene ND ug/kg 1 09/09/10 07:59 541-73-15.3 2.11,4-Dichlorobenzene ND ug/kg 1 09/09/10 07:59 106-46-75.3 1.8Dichlorodifluoromethane ND ug/kg 1 09/09/10 07:59 75-71-810.6 3.81,1-Dichloroethane ND ug/kg 1 09/09/10 07:59 75-34-35.3 1.61,2-Dichloroethane ND ug/kg 1 09/09/10 07:59 107-06-25.3 2.31,1-Dichloroethene ND ug/kg 1 09/09/10 07:59 75-35-45.3 1.9cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 07:59 156-59-25.3 1.5trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 07:59 156-60-55.3 2.01,2-Dichloropropane ND ug/kg 1 09/09/10 07:59 78-87-55.3 1.8cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 07:59 10061-01-55.3 1.9trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 07:59 10061-02-65.3 1.6Ethylbenzene ND ug/kg 1 09/09/10 07:59 100-41-45.3 1.92-Hexanone ND ug/kg 1 09/09/10 07:59 591-78-653.1 4.1Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 07:59 98-82-85.3 2.0Methyl acetate ND ug/kg 1 09/09/10 07:59 79-20-910.6 1.5Methylcyclohexane ND ug/kg 1 09/09/10 07:59 108-87-210.6 1.6Methylene Chloride ND ug/kg 1 09/09/10 07:59 75-09-221.2 3.24-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 07:59 108-10-153.1 3.9Methyl-tert-butyl ether ND ug/kg 1 09/09/10 07:59 1634-04-45.3 1.6Styrene ND ug/kg 1 09/09/10 07:59 100-42-55.3 1.91,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 07:59 79-34-55.3 2.0Tetrachloroethene ND ug/kg 1 09/09/10 07:59 127-18-45.3 1.8Toluene ND ug/kg 1 09/09/10 07:59 108-88-35.3 1.91,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 07:59 87-61-65.3 2.3



Date: 09/27/2010 06:48 PM Page 183 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/14/10 10:34 57-12-50.15 0.15



Date: 09/27/2010 06:48 PM Page 184 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/14/10 14:55 7440-36-0 D309/10/10 15:154.0 2.2Arsenic 2.9J mg/kg 10 09/14/10 14:55 7440-38-2 D309/10/10 15:154.0 2.5Beryllium 1.8 mg/kg 10 09/14/10 14:55 7440-41-7 D309/10/10 15:150.79 0.16Cadmium ND mg/kg 10 09/14/10 14:55 7440-43-9 D309/10/10 15:150.79 0.48Chromium 23.6 mg/kg 10 09/14/10 14:55 7440-47-3 D309/10/10 15:154.0 0.24Copper 7.0 mg/kg 10 09/14/10 14:55 7440-50-8 D309/10/10 15:154.0 0.32Lead 4.1 mg/kg 10 09/14/10 14:55 7439-92-1 D309/10/10 15:154.0 3.8Manganese 509 mg/kg 10 09/14/10 14:55 7439-96-5 D309/10/10 15:154.0 0.24Nickel 16.0 mg/kg 10 09/14/10 14:55 7440-02-0 D309/10/10 15:154.0 1.4Selenium 3.5J mg/kg 10 09/14/10 14:55 7782-49-2 D309/10/10 15:157.9 3.0Silver ND mg/kg 10 09/14/10 14:55 7440-22-4 D309/10/10 15:154.0 0.24Thallium 17.5 mg/kg 10 09/14/10 14:55 7440-28-0 D309/10/10 15:157.9 2.1Zinc 88.0 mg/kg 10 09/14/10 14:55 7440-66-6 D309/10/10 15:157.9 2.1


Mercury ND mg/kg 1 09/14/10 14:52 7439-97-6 M109/14/10 08:130.0043 0.000087





Date: 09/27/2010 06:48 PM Page 185 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/25/10 05:40 83-32-909/15/10 13:00362 83.3Acenaphthylene ND ug/kg 1 09/25/10 05:40 208-96-809/15/10 13:00362 85.5Acetophenone ND ug/kg 1 09/25/10 05:40 98-86-209/15/10 13:00362 186Anthracene ND ug/kg 1 09/25/10 05:40 120-12-709/15/10 13:00362 81.1Atrazine ND ug/kg 1 09/25/10 05:40 1912-24-909/15/10 13:00723 142Benzaldehyde ND ug/kg 1 09/25/10 05:40 100-52-709/15/10 13:00723 362Benzo(a)anthracene ND ug/kg 1 09/25/10 05:40 56-55-309/15/10 13:00362 66.8Benzo(a)pyrene ND ug/kg 1 09/25/10 05:40 50-32-809/15/10 13:00362 69.0Benzo(b)fluoranthene ND ug/kg 1 09/25/10 05:40 205-99-209/15/10 13:00362 62.5Benzo(g,h,i)perylene ND ug/kg 1 09/25/10 05:40 191-24-209/15/10 13:00362 92.0Benzo(k)fluoranthene ND ug/kg 1 09/25/10 05:40 207-08-909/15/10 13:00362 71.2Biphenyl (Diphenyl) ND ug/kg 1 09/25/10 05:40 92-52-409/15/10 13:00362 1144-Bromophenylphenyl ether ND ug/kg 1 09/25/10 05:40 101-55-309/15/10 13:00362 65.7Butylbenzylphthalate ND ug/kg 1 09/25/10 05:40 85-68-709/15/10 13:00362 76.7Caprolactam ND ug/kg 1 09/25/10 05:40 105-60-209/15/10 13:00362 62.5Carbazole ND ug/kg 1 09/25/10 05:40 86-74-809/15/10 13:00362 69.04-Chloro-3-methylphenol ND ug/kg 1 09/25/10 05:40 59-50-709/15/10 13:00723 74.54-Chloroaniline ND ug/kg 1 09/25/10 05:40 106-47-809/15/10 13:001810 101bis(2-Chloroethoxy)methane ND ug/kg 1 09/25/10 05:40 111-91-109/15/10 13:00362 84.4bis(2-Chloroethyl) ether ND ug/kg 1 09/25/10 05:40 111-44-409/15/10 13:00362 92.0bis(2-Chloroisopropyl) ether ND ug/kg 1 09/25/10 05:40 108-60-109/15/10 13:00362 96.42-Chloronaphthalene ND ug/kg 1 09/25/10 05:40 91-58-709/15/10 13:00362 71.22-Chlorophenol ND ug/kg 1 09/25/10 05:40 95-57-809/15/10 13:00362 98.64-Chlorophenylphenyl ether ND ug/kg 1 09/25/10 05:40 7005-72-309/15/10 13:00362 74.5Chrysene ND ug/kg 1 09/25/10 05:40 218-01-909/15/10 13:00362 48.2Dibenz(a,h)anthracene ND ug/kg 1 09/25/10 05:40 53-70-309/15/10 13:00362 76.7Dibenzofuran ND ug/kg 1 09/25/10 05:40 132-64-909/15/10 13:00362 59.23,3'-Dichlorobenzidine ND ug/kg 1 09/25/10 05:40 91-94-109/15/10 13:001810 78.92,4-Dichlorophenol ND ug/kg 1 09/25/10 05:40 120-83-209/15/10 13:00362 78.9Diethylphthalate ND ug/kg 1 09/25/10 05:40 84-66-209/15/10 13:00362 55.92,4-Dimethylphenol ND ug/kg 1 09/25/10 05:40 105-67-909/15/10 13:00362 142Dimethylphthalate ND ug/kg 1 09/25/10 05:40 131-11-309/15/10 13:00362 73.4Di-n-butylphthalate ND ug/kg 1 09/25/10 05:40 84-74-209/15/10 13:00362 59.24,6-Dinitro-2-methylphenol ND ug/kg 1 09/25/10 05:40 534-52-109/15/10 13:00723 72.32,4-Dinitrophenol ND ug/kg 1 09/25/10 05:40 51-28-509/15/10 13:001810 59.22,4-Dinitrotoluene ND ug/kg 1 09/25/10 05:40 121-14-209/15/10 13:00362 67.92,6-Dinitrotoluene ND ug/kg 1 09/25/10 05:40 606-20-209/15/10 13:00362 75.6Di-n-octylphthalate ND ug/kg 1 09/25/10 05:40 117-84-009/15/10 13:00362 75.6bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/25/10 05:40 117-81-709/15/10 13:00362 98.6Fluoranthene ND ug/kg 1 09/25/10 05:40 206-44-009/15/10 13:00362 52.6Fluorene ND ug/kg 1 09/25/10 05:40 86-73-709/15/10 13:00362 74.5Hexachloro-1,3-butadiene ND ug/kg 1 09/25/10 05:40 87-68-309/15/10 13:00362 62.5Hexachlorobenzene ND ug/kg 1 09/25/10 05:40 118-74-109/15/10 13:00362 46.0Hexachlorocyclopentadiene ND ug/kg 1 09/25/10 05:40 77-47-409/15/10 13:00362 66.8Hexachloroethane ND ug/kg 1 09/25/10 05:40 67-72-109/15/10 13:00362 95.3



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/25/10 05:40 193-39-509/15/10 13:00362 74.5Isophorone ND ug/kg 1 09/25/10 05:40 78-59-109/15/10 13:00362 81.12-Methylnaphthalene ND ug/kg 1 09/25/10 05:40 91-57-609/15/10 13:00362 77.82-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 05:40 95-48-709/15/10 13:00362 1103&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 05:4009/15/10 13:00362 142Naphthalene ND ug/kg 1 09/25/10 05:40 91-20-309/15/10 13:00362 88.82-Nitroaniline ND ug/kg 1 09/25/10 05:40 88-74-409/15/10 13:001810 1123-Nitroaniline ND ug/kg 1 09/25/10 05:40 99-09-209/15/10 13:001810 98.64-Nitroaniline ND ug/kg 1 09/25/10 05:40 100-01-609/15/10 13:00723 102Nitrobenzene ND ug/kg 1 09/25/10 05:40 98-95-309/15/10 13:00362 98.62-Nitrophenol ND ug/kg 1 09/25/10 05:40 88-75-509/15/10 13:00362 87.74-Nitrophenol ND ug/kg 1 09/25/10 05:40 100-02-709/15/10 13:001810 64.6N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 05:40 621-64-709/15/10 13:00362 69.0N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 05:40 86-30-609/15/10 13:00362 107Pentachlorophenol ND ug/kg 1 09/25/10 05:40 87-86-509/15/10 13:001810 65.7Phenanthrene ND ug/kg 1 09/25/10 05:40 85-01-809/15/10 13:00362 60.3Phenol ND ug/kg 1 09/25/10 05:40 108-95-209/15/10 13:00362 108Pyrene ND ug/kg 1 09/25/10 05:40 129-00-009/15/10 13:00362 61.41,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 05:40 95-94-309/15/10 13:00362 1312,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 05:40 58-90-209/15/10 13:00362 1422,4,5-Trichlorophenol ND ug/kg 1 09/25/10 05:40 95-95-409/15/10 13:00362 1122,4,6-Trichlorophenol ND ug/kg 1 09/25/10 05:40 88-06-209/15/10 13:00362 80.02-Fluorobiphenyl (S) 20 % 1 09/25/10 05:40 321-60-8 S209/15/10 13:0030-110Terphenyl-d14 (S) 31 % 1 09/25/10 05:40 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 15 % 1 09/25/10 05:40 13127-88-3 S209/15/10 13:0022-1102-Fluorophenol (S) 15 % 1 09/25/10 05:40 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 27 % 1 09/25/10 05:40 118-79-609/15/10 13:0027-110Nitrobenzene-d5 (S) 15 % 1 09/25/10 05:40 4165-60-0 S209/15/10 13:0023-110


Acetone ND ug/kg 1 09/09/10 08:17 67-64-199.4 9.9Benzene ND ug/kg 1 09/09/10 08:17 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/09/10 08:17 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/09/10 08:17 75-27-45.0 1.9Bromoform ND ug/kg 1 09/09/10 08:17 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/09/10 08:17 74-83-99.9 2.52-Butanone (MEK) ND ug/kg 1 09/09/10 08:17 78-93-399.4 2.9Carbon disulfide ND ug/kg 1 09/09/10 08:17 75-15-09.9 3.0Carbon tetrachloride ND ug/kg 1 09/09/10 08:17 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/09/10 08:17 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/09/10 08:17 75-00-39.9 2.4Chloroform ND ug/kg 1 09/09/10 08:17 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/09/10 08:17 74-87-39.9 2.4Cyclohexane ND ug/kg 1 09/09/10 08:17 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 08:17 96-12-85.0 3.6



Date: 09/27/2010 06:48 PM Page 187 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Dibromochloromethane ND ug/kg 1 09/09/10 08:17 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 08:17 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/09/10 08:17 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/09/10 08:17 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/09/10 08:17 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/09/10 08:17 75-71-89.9 3.61,1-Dichloroethane ND ug/kg 1 09/09/10 08:17 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/09/10 08:17 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/09/10 08:17 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 08:17 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 08:17 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/09/10 08:17 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 08:17 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 08:17 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/09/10 08:17 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/09/10 08:17 591-78-649.7 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 08:17 98-82-85.0 1.9Methyl acetate ND ug/kg 1 09/09/10 08:17 79-20-99.9 1.4Methylcyclohexane ND ug/kg 1 09/09/10 08:17 108-87-29.9 1.5Methylene Chloride ND ug/kg 1 09/09/10 08:17 75-09-219.9 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 08:17 108-10-149.7 3.7Methyl-tert-butyl ether ND ug/kg 1 09/09/10 08:17 1634-04-45.0 1.5Styrene ND ug/kg 1 09/09/10 08:17 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 08:17 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/09/10 08:17 127-18-45.0 1.7Toluene ND ug/kg 1 09/09/10 08:17 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 08:17 87-61-65.0 2.21,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 08:17 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/09/10 08:17 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/09/10 08:17 79-00-55.0 2.1Trichloroethene ND ug/kg 1 09/09/10 08:17 79-01-65.0 2.1Trichlorofluoromethane ND ug/kg 1 09/09/10 08:17 75-69-45.0 2.21,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/09/10 08:17 76-13-15.0 1.9Vinyl chloride ND ug/kg 1 09/09/10 08:17 75-01-49.9 1.8Xylene (Total) ND ug/kg 1 09/09/10 08:17 1330-20-79.9 3.6m&p-Xylene ND ug/kg 1 09/09/10 08:17 179601-23-19.9 3.6o-Xylene ND ug/kg 1 09/09/10 08:17 95-47-65.0 1.9Dibromofluoromethane (S) 101 % 1 09/09/10 08:17 1868-53-770-130Toluene-d8 (S) 100 % 1 09/09/10 08:17 2037-26-570-1304-Bromofluorobenzene (S) 97 % 1 09/09/10 08:17 460-00-470-1301,2-Dichloroethane-d4 (S) 103 % 1 09/09/10 08:17 17060-07-070-132





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Cyanide ND mg/kg 1 09/14/10 10:38 57-12-50.16 0.16





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/19/10 13:16 83-32-909/16/10 08:45376 86.6Acenaphthylene ND ug/kg 1 09/19/10 13:16 208-96-809/16/10 08:45376 88.9Acetophenone ND ug/kg 1 09/19/10 13:16 98-86-209/16/10 08:45376 194Anthracene ND ug/kg 1 09/19/10 13:16 120-12-709/16/10 08:45376 84.4Atrazine ND ug/kg 1 09/19/10 13:16 1912-24-909/16/10 08:45752 148Benzaldehyde ND ug/kg 1 09/19/10 13:16 100-52-709/16/10 08:45752 376Benzo(a)anthracene ND ug/kg 1 09/19/10 13:16 56-55-309/16/10 08:45376 69.5Benzo(a)pyrene ND ug/kg 1 09/19/10 13:16 50-32-809/16/10 08:45376 71.8Benzo(b)fluoranthene ND ug/kg 1 09/19/10 13:16 205-99-209/16/10 08:45376 65.0Benzo(g,h,i)perylene ND ug/kg 1 09/19/10 13:16 191-24-209/16/10 08:45376 95.8Benzo(k)fluoranthene ND ug/kg 1 09/19/10 13:16 207-08-909/16/10 08:45376 74.1Biphenyl (Diphenyl) ND ug/kg 1 09/19/10 13:16 92-52-409/16/10 08:45376 1194-Bromophenylphenyl ether ND ug/kg 1 09/19/10 13:16 101-55-309/16/10 08:45376 68.4Butylbenzylphthalate ND ug/kg 1 09/19/10 13:16 85-68-709/16/10 08:45376 79.8Caprolactam ND ug/kg 1 09/19/10 13:16 105-60-209/16/10 08:45376 65.0Carbazole ND ug/kg 1 09/19/10 13:16 86-74-809/16/10 08:45376 71.84-Chloro-3-methylphenol ND ug/kg 1 09/19/10 13:16 59-50-709/16/10 08:45752 77.54-Chloroaniline ND ug/kg 1 09/19/10 13:16 106-47-809/16/10 08:451880 105bis(2-Chloroethoxy)methane ND ug/kg 1 09/19/10 13:16 111-91-109/16/10 08:45376 87.8bis(2-Chloroethyl) ether ND ug/kg 1 09/19/10 13:16 111-44-409/16/10 08:45376 95.8bis(2-Chloroisopropyl) ether ND ug/kg 1 09/19/10 13:16 108-60-109/16/10 08:45376 1002-Chloronaphthalene ND ug/kg 1 09/19/10 13:16 91-58-709/16/10 08:45376 74.12-Chlorophenol ND ug/kg 1 09/19/10 13:16 95-57-809/16/10 08:45376 1034-Chlorophenylphenyl ether ND ug/kg 1 09/19/10 13:16 7005-72-309/16/10 08:45376 77.5Chrysene ND ug/kg 1 09/19/10 13:16 218-01-909/16/10 08:45376 50.2Dibenz(a,h)anthracene ND ug/kg 1 09/19/10 13:16 53-70-309/16/10 08:45376 79.8Dibenzofuran ND ug/kg 1 09/19/10 13:16 132-64-909/16/10 08:45376 61.63,3'-Dichlorobenzidine ND ug/kg 1 09/19/10 13:16 91-94-109/16/10 08:451880 82.12,4-Dichlorophenol ND ug/kg 1 09/19/10 13:16 120-83-209/16/10 08:45376 82.1Diethylphthalate ND ug/kg 1 09/19/10 13:16 84-66-209/16/10 08:45376 58.12,4-Dimethylphenol ND ug/kg 1 09/19/10 13:16 105-67-909/16/10 08:45376 148Dimethylphthalate ND ug/kg 1 09/19/10 13:16 131-11-309/16/10 08:45376 76.4Di-n-butylphthalate ND ug/kg 1 09/19/10 13:16 84-74-209/16/10 08:45376 61.64,6-Dinitro-2-methylphenol ND ug/kg 1 09/19/10 13:16 534-52-109/16/10 08:45752 75.22,4-Dinitrophenol ND ug/kg 1 09/19/10 13:16 51-28-509/16/10 08:451880 61.62,4-Dinitrotoluene ND ug/kg 1 09/19/10 13:16 121-14-209/16/10 08:45376 70.72,6-Dinitrotoluene ND ug/kg 1 09/19/10 13:16 606-20-209/16/10 08:45376 78.7Di-n-octylphthalate ND ug/kg 1 09/19/10 13:16 117-84-009/16/10 08:45376 78.7bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/19/10 13:16 117-81-709/16/10 08:45376 103Fluoranthene ND ug/kg 1 09/19/10 13:16 206-44-009/16/10 08:45376 54.7Fluorene ND ug/kg 1 09/19/10 13:16 86-73-709/16/10 08:45376 77.5Hexachloro-1,3-butadiene ND ug/kg 1 09/19/10 13:16 87-68-309/16/10 08:45376 65.0Hexachlorobenzene ND ug/kg 1 09/19/10 13:16 118-74-109/16/10 08:45376 47.9Hexachlorocyclopentadiene ND ug/kg 1 09/19/10 13:16 77-47-409/16/10 08:45376 69.5Hexachloroethane ND ug/kg 1 09/19/10 13:16 67-72-109/16/10 08:45376 99.2



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/19/10 13:16 193-39-509/16/10 08:45376 77.5Isophorone ND ug/kg 1 09/19/10 13:16 78-59-109/16/10 08:45376 84.42-Methylnaphthalene ND ug/kg 1 09/19/10 13:16 91-57-609/16/10 08:45376 80.92-Methylphenol(o-Cresol) ND ug/kg 1 09/19/10 13:16 95-48-709/16/10 08:45376 1143&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/19/10 13:1609/16/10 08:45376 148Naphthalene ND ug/kg 1 09/19/10 13:16 91-20-309/16/10 08:45376 92.32-Nitroaniline ND ug/kg 1 09/19/10 13:16 88-74-409/16/10 08:451880 1163-Nitroaniline ND ug/kg 1 09/19/10 13:16 99-09-209/16/10 08:451880 1034-Nitroaniline ND ug/kg 1 09/19/10 13:16 100-01-609/16/10 08:45752 106Nitrobenzene ND ug/kg 1 09/19/10 13:16 98-95-309/16/10 08:45376 1032-Nitrophenol ND ug/kg 1 09/19/10 13:16 88-75-509/16/10 08:45376 91.24-Nitrophenol ND ug/kg 1 09/19/10 13:16 100-02-709/16/10 08:451880 67.3N-Nitroso-di-n-propylamine ND ug/kg 1 09/19/10 13:16 621-64-709/16/10 08:45376 71.8N-Nitrosodiphenylamine ND ug/kg 1 09/19/10 13:16 86-30-609/16/10 08:45376 112Pentachlorophenol ND ug/kg 1 09/19/10 13:16 87-86-509/16/10 08:451880 68.4Phenanthrene ND ug/kg 1 09/19/10 13:16 85-01-809/16/10 08:45376 62.7Phenol ND ug/kg 1 09/19/10 13:16 108-95-209/16/10 08:45376 113Pyrene ND ug/kg 1 09/19/10 13:16 129-00-009/16/10 08:45376 63.81,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/19/10 13:16 95-94-309/16/10 08:45376 1372,3,4,6-Tetrachlorophenol ND ug/kg 1 09/19/10 13:16 58-90-209/16/10 08:45376 1482,4,5-Trichlorophenol ND ug/kg 1 09/19/10 13:16 95-95-409/16/10 08:45376 1162,4,6-Trichlorophenol ND ug/kg 1 09/19/10 13:16 88-06-209/16/10 08:45376 83.22-Fluorobiphenyl (S) 32 % 1 09/19/10 13:16 321-60-809/16/10 08:4530-110Terphenyl-d14 (S) 46 % 1 09/19/10 13:16 1718-51-009/16/10 08:4528-110Phenol-d6 (S) 19 % 1 09/19/10 13:16 13127-88-3 S009/16/10 08:4522-1102-Fluorophenol (S) 26 % 1 09/19/10 13:16 367-12-409/16/10 08:4513-1102,4,6-Tribromophenol (S) 34 % 1 09/19/10 13:16 118-79-609/16/10 08:4527-110Nitrobenzene-d5 (S) 27 % 1 09/19/10 13:16 4165-60-009/16/10 08:4523-110





Date: 09/27/2010 06:48 PM Page 191 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 10 09/22/10 18:05 7440-36-0 D309/09/10 14:304.3 2.4Arsenic 4.0J mg/kg 10 09/22/10 18:05 7440-38-2 D309/09/10 14:304.3 2.7Beryllium 1.5 mg/kg 10 09/22/10 18:05 7440-41-709/09/10 14:300.86 0.17Cadmium ND mg/kg 10 09/22/10 18:05 7440-43-9 D309/09/10 14:300.86 0.51Chromium 17.5 mg/kg 10 09/22/10 18:05 7440-47-309/09/10 14:304.3 0.26Copper 2.4J mg/kg 10 09/22/10 18:05 7440-50-8 D309/09/10 14:304.3 0.34Lead 7.4 mg/kg 10 09/22/10 18:05 7439-92-109/09/10 14:304.3 4.1Manganese 502 mg/kg 10 09/22/10 18:05 7439-96-509/09/10 14:304.3 0.26Nickel 15.5 mg/kg 10 09/22/10 18:05 7440-02-009/09/10 14:304.3 1.5Selenium ND mg/kg 10 09/22/10 18:05 7782-49-2 D309/09/10 14:308.6 3.3Silver ND mg/kg 10 09/22/10 18:05 7440-22-4 D309/09/10 14:304.3 0.26Thallium ND mg/kg 10 09/22/10 18:05 7440-28-0 D309/09/10 14:308.6 2.2Zinc 61.4 mg/kg 10 09/22/10 18:05 7440-66-609/09/10 14:308.6 2.2


Mercury ND mg/kg 1 09/14/10 15:06 7439-97-609/14/10 08:130.0053 0.00011


Acetone ND ug/kg 1 09/09/10 08:35 67-64-1104 10.4Benzene ND ug/kg 1 09/09/10 08:35 71-43-25.2 1.7Bromochloromethane ND ug/kg 1 09/09/10 08:35 74-97-55.2 1.8Bromodichloromethane ND ug/kg 1 09/09/10 08:35 75-27-45.2 2.0Bromoform ND ug/kg 1 09/09/10 08:35 75-25-25.2 2.4Bromomethane ND ug/kg 1 09/09/10 08:35 74-83-910.4 2.62-Butanone (MEK) ND ug/kg 1 09/09/10 08:35 78-93-3104 3.0Carbon disulfide ND ug/kg 1 09/09/10 08:35 75-15-010.4 3.1Carbon tetrachloride ND ug/kg 1 09/09/10 08:35 56-23-55.2 2.7Chlorobenzene ND ug/kg 1 09/09/10 08:35 108-90-75.2 2.0Chloroethane ND ug/kg 1 09/09/10 08:35 75-00-310.4 2.5Chloroform ND ug/kg 1 09/09/10 08:35 67-66-35.2 1.7Chloromethane ND ug/kg 1 09/09/10 08:35 74-87-310.4 2.5Cyclohexane ND ug/kg 1 09/09/10 08:35 110-82-75.2 1.71,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 08:35 96-12-85.2 3.7Dibromochloromethane ND ug/kg 1 09/09/10 08:35 124-48-15.2 1.91,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 08:35 106-93-45.2 1.91,2-Dichlorobenzene ND ug/kg 1 09/09/10 08:35 95-50-15.2 2.01,3-Dichlorobenzene ND ug/kg 1 09/09/10 08:35 541-73-15.2 2.11,4-Dichlorobenzene ND ug/kg 1 09/09/10 08:35 106-46-75.2 1.8Dichlorodifluoromethane ND ug/kg 1 09/09/10 08:35 75-71-810.4 3.71,1-Dichloroethane ND ug/kg 1 09/09/10 08:35 75-34-35.2 1.61,2-Dichloroethane ND ug/kg 1 09/09/10 08:35 107-06-25.2 2.31,1-Dichloroethene ND ug/kg 1 09/09/10 08:35 75-35-45.2 1.9cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 08:35 156-59-25.2 1.5trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 08:35 156-60-55.2 2.01,2-Dichloropropane ND ug/kg 1 09/09/10 08:35 78-87-55.2 1.8



Date: 09/27/2010 06:48 PM Page 192 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 08:35 10061-01-55.2 1.9trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 08:35 10061-02-65.2 1.6Ethylbenzene ND ug/kg 1 09/09/10 08:35 100-41-45.2 1.92-Hexanone ND ug/kg 1 09/09/10 08:35 591-78-651.9 4.0Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 08:35 98-82-85.2 2.0Methyl acetate ND ug/kg 1 09/09/10 08:35 79-20-910.4 1.5Methylcyclohexane ND ug/kg 1 09/09/10 08:35 108-87-210.4 1.6Methylene Chloride ND ug/kg 1 09/09/10 08:35 75-09-220.8 3.14-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 08:35 108-10-151.9 3.8Methyl-tert-butyl ether ND ug/kg 1 09/09/10 08:35 1634-04-45.2 1.6Styrene ND ug/kg 1 09/09/10 08:35 100-42-55.2 1.91,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 08:35 79-34-55.2 2.0Tetrachloroethene ND ug/kg 1 09/09/10 08:35 127-18-45.2 1.8Toluene ND ug/kg 1 09/09/10 08:35 108-88-35.2 1.91,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 08:35 87-61-65.2 2.31,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 08:35 120-82-15.2 1.71,1,1-Trichloroethane ND ug/kg 1 09/09/10 08:35 71-55-65.2 1.91,1,2-Trichloroethane ND ug/kg 1 09/09/10 08:35 79-00-55.2 2.2Trichloroethene ND ug/kg 1 09/09/10 08:35 79-01-65.2 2.2Trichlorofluoromethane ND ug/kg 1 09/09/10 08:35 75-69-45.2 2.31,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/09/10 08:35 76-13-15.2 2.0Vinyl chloride ND ug/kg 1 09/09/10 08:35 75-01-410.4 1.9Xylene (Total) ND ug/kg 1 09/09/10 08:35 1330-20-710.4 3.7m&p-Xylene ND ug/kg 1 09/09/10 08:35 179601-23-110.4 3.7o-Xylene ND ug/kg 1 09/09/10 08:35 95-47-65.2 2.0Dibromofluoromethane (S) 100 % 1 09/09/10 08:35 1868-53-770-130Toluene-d8 (S) 100 % 1 09/09/10 08:35 2037-26-570-1304-Bromofluorobenzene (S) 96 % 1 09/09/10 08:35 460-00-470-1301,2-Dichloroethane-d4 (S) 99 % 1 09/09/10 08:35 17060-07-070-132




Cyanide ND mg/kg 1 09/14/10 10:38 57-12-50.17 0.17





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 20 09/22/10 18:09 7440-36-0 D309/09/10 14:307.0 3.9Arsenic 5.3J mg/kg 20 09/22/10 18:09 7440-38-2 D309/09/10 14:307.0 4.5Beryllium 4.0 mg/kg 20 09/22/10 18:09 7440-41-709/09/10 14:301.4 0.28Cadmium 1.4 mg/kg 20 09/22/10 18:09 7440-43-909/09/10 14:301.4 0.84Chromium 34.3 mg/kg 20 09/22/10 18:09 7440-47-309/09/10 14:307.0 0.42Copper 44.1 mg/kg 20 09/22/10 18:09 7440-50-809/09/10 14:307.0 0.56Lead 31.5 mg/kg 20 09/22/10 18:09 7439-92-109/09/10 14:307.0 6.8Manganese 739 mg/kg 20 09/22/10 18:09 7439-96-509/09/10 14:307.0 0.42Nickel 82.5 mg/kg 20 09/22/10 18:09 7440-02-009/09/10 14:307.0 2.5Selenium ND mg/kg 20 09/22/10 18:09 7782-49-2 D309/09/10 14:3014.1 5.3Silver 101 mg/kg 20 09/22/10 18:09 7440-22-409/09/10 14:307.0 0.42Thallium ND mg/kg 20 09/22/10 18:09 7440-28-0 D309/09/10 14:3014.1 3.7Zinc 515 mg/kg 20 09/22/10 18:09 7440-66-609/09/10 14:3014.1 3.7


Mercury 0.010 mg/kg 1 09/14/10 15:08 7439-97-609/14/10 08:130.0037 0.000075





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/25/10 06:16 91-94-109/21/10 14:201810 79.12,4-Dichlorophenol ND ug/kg 1 09/25/10 06:16 120-83-209/21/10 14:20362 79.1Diethylphthalate ND ug/kg 1 09/25/10 06:16 84-66-209/21/10 14:20362 56.02,4-Dimethylphenol ND ug/kg 1 09/25/10 06:16 105-67-909/21/10 14:20362 143Dimethylphthalate ND ug/kg 1 09/25/10 06:16 131-11-309/21/10 14:20362 73.6Di-n-butylphthalate ND ug/kg 1 09/25/10 06:16 84-74-209/21/10 14:20362 59.34,6-Dinitro-2-methylphenol ND ug/kg 1 09/25/10 06:16 534-52-109/21/10 14:20725 72.52,4-Dinitrophenol ND ug/kg 1 09/25/10 06:16 51-28-509/21/10 14:201810 59.32,4-Dinitrotoluene ND ug/kg 1 09/25/10 06:16 121-14-209/21/10 14:20362 68.12,6-Dinitrotoluene ND ug/kg 1 09/25/10 06:16 606-20-209/21/10 14:20362 75.8Di-n-octylphthalate ND ug/kg 1 09/25/10 06:16 117-84-009/21/10 14:20362 75.8bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/25/10 06:16 117-81-709/21/10 14:20362 98.8Fluoranthene ND ug/kg 1 09/25/10 06:16 206-44-009/21/10 14:20362 52.7Fluorene ND ug/kg 1 09/25/10 06:16 86-73-709/21/10 14:20362 74.7Hexachloro-1,3-butadiene ND ug/kg 1 09/25/10 06:16 87-68-309/21/10 14:20362 62.6Hexachlorobenzene ND ug/kg 1 09/25/10 06:16 118-74-109/21/10 14:20362 46.1Hexachlorocyclopentadiene ND ug/kg 1 09/25/10 06:16 77-47-409/21/10 14:20362 67.0Hexachloroethane ND ug/kg 1 09/25/10 06:16 67-72-109/21/10 14:20362 95.5Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/25/10 06:16 193-39-509/21/10 14:20362 74.7Isophorone ND ug/kg 1 09/25/10 06:16 78-59-109/21/10 14:20362 81.32-Methylnaphthalene ND ug/kg 1 09/25/10 06:16 91-57-609/21/10 14:20362 78.02-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 06:16 95-48-709/21/10 14:20362 1103&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 06:1609/21/10 14:20362 143Naphthalene ND ug/kg 1 09/25/10 06:16 91-20-309/21/10 14:20362 88.92-Nitroaniline ND ug/kg 1 09/25/10 06:16 88-74-409/21/10 14:201810 1123-Nitroaniline ND ug/kg 1 09/25/10 06:16 99-09-209/21/10 14:201810 98.84-Nitroaniline ND ug/kg 1 09/25/10 06:16 100-01-609/21/10 14:20725 102Nitrobenzene ND ug/kg 1 09/25/10 06:16 98-95-309/21/10 14:20362 98.82-Nitrophenol ND ug/kg 1 09/25/10 06:16 88-75-509/21/10 14:20362 87.84-Nitrophenol ND ug/kg 1 09/25/10 06:16 100-02-709/21/10 14:201810 64.8N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 06:16 621-64-709/21/10 14:20362 69.2N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 06:16 86-30-609/21/10 14:20362 108Pentachlorophenol ND ug/kg 1 09/25/10 06:16 87-86-509/21/10 14:201810 65.9Phenanthrene ND ug/kg 1 09/25/10 06:16 85-01-809/21/10 14:20362 60.4Phenol ND ug/kg 1 09/25/10 06:16 108-95-2 H509/21/10 14:20362 109Pyrene ND ug/kg 1 09/25/10 06:16 129-00-009/21/10 14:20362 61.51,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 06:16 95-94-309/21/10 14:20362 1322,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 06:16 58-90-209/21/10 14:20362 1432,4,5-Trichlorophenol ND ug/kg 1 09/25/10 06:16 95-95-409/21/10 14:20362 1122,4,6-Trichlorophenol ND ug/kg 1 09/25/10 06:16 88-06-209/21/10 14:20362 80.22-Fluorobiphenyl (S) 38 % 1 09/25/10 06:16 321-60-809/21/10 14:2030-110Terphenyl-d14 (S) 41 % 1 09/25/10 06:16 1718-51-009/21/10 14:2028-110Phenol-d6 (S) 22 % 1 09/25/10 06:16 13127-88-309/21/10 14:2022-1102-Fluorophenol (S) 22 % 1 09/25/10 06:16 367-12-409/21/10 14:2013-1102,4,6-Tribromophenol (S) 35 % 1 09/25/10 06:16 118-79-609/21/10 14:2027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 27 % 1 09/25/10 06:16 4165-60-009/21/10 14:2023-110


Acetone 51.5J ug/kg 1 09/09/10 08:54 67-64-1101 10.1Benzene ND ug/kg 1 09/09/10 08:54 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/09/10 08:54 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/09/10 08:54 75-27-45.0 1.9Bromoform ND ug/kg 1 09/09/10 08:54 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/09/10 08:54 74-83-910.1 2.52-Butanone (MEK) 6.1J ug/kg 1 09/09/10 08:54 78-93-3101 2.9Carbon disulfide ND ug/kg 1 09/09/10 08:54 75-15-010.1 3.0Carbon tetrachloride ND ug/kg 1 09/09/10 08:54 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/09/10 08:54 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/09/10 08:54 75-00-310.1 2.4Chloroform ND ug/kg 1 09/09/10 08:54 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/09/10 08:54 74-87-310.1 2.4Cyclohexane ND ug/kg 1 09/09/10 08:54 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 08:54 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/09/10 08:54 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 08:54 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/09/10 08:54 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/09/10 08:54 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/09/10 08:54 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/09/10 08:54 75-71-810.1 3.61,1-Dichloroethane ND ug/kg 1 09/09/10 08:54 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/09/10 08:54 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/09/10 08:54 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/09/10 08:54 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 08:54 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/09/10 08:54 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 08:54 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 08:54 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/09/10 08:54 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/09/10 08:54 591-78-650.5 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 08:54 98-82-85.0 1.9Methyl acetate 85.7 ug/kg 1 09/09/10 08:54 79-20-910.1 1.4Methylcyclohexane ND ug/kg 1 09/09/10 08:54 108-87-210.1 1.5Methylene Chloride ND ug/kg 1 09/09/10 08:54 75-09-220.2 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 08:54 108-10-150.5 3.7Methyl-tert-butyl ether ND ug/kg 1 09/09/10 08:54 1634-04-45.0 1.5Styrene ND ug/kg 1 09/09/10 08:54 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 08:54 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/09/10 08:54 127-18-45.0 1.7Toluene ND ug/kg 1 09/09/10 08:54 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 08:54 87-61-65.0 2.2



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/14/10 10:39 57-12-50.14 0.14





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 5 09/22/10 18:12 7440-36-0 D309/09/10 14:302.6 1.4Arsenic 2.7 mg/kg 5 09/22/10 18:12 7440-38-209/09/10 14:302.6 1.6Beryllium 3.0 mg/kg 5 09/22/10 18:12 7440-41-709/09/10 14:300.52 0.10Cadmium ND mg/kg 5 09/22/10 18:12 7440-43-9 D309/09/10 14:300.52 0.31Chromium 42.1 mg/kg 5 09/22/10 18:12 7440-47-309/09/10 14:302.6 0.15Copper 25.6 mg/kg 5 09/22/10 18:12 7440-50-809/09/10 14:302.6 0.21Lead 8.8 mg/kg 5 09/22/10 18:12 7439-92-109/09/10 14:302.6 2.5Manganese 446 mg/kg 5 09/22/10 18:12 7439-96-509/09/10 14:302.6 0.15Nickel 25.9 mg/kg 5 09/22/10 18:12 7440-02-009/09/10 14:302.6 0.93Selenium ND mg/kg 5 09/22/10 18:12 7782-49-2 D309/09/10 14:305.2 2.0Silver 72.1 mg/kg 5 09/22/10 18:12 7440-22-409/09/10 14:302.6 0.15Thallium 1.7J mg/kg 5 09/22/10 18:12 7440-28-0 D309/09/10 14:305.2 1.3Zinc 106 mg/kg 5 09/22/10 18:12 7440-66-609/09/10 14:305.2 1.3


Mercury 0.0061 mg/kg 1 09/14/10 15:11 7439-97-609/14/10 08:130.0051 0.00010





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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




3,3'-Dichlorobenzidine ND ug/kg 1 09/25/10 06:53 91-94-109/21/10 14:201840 80.12,4-Dichlorophenol ND ug/kg 1 09/25/10 06:53 120-83-209/21/10 14:20367 80.1Diethylphthalate ND ug/kg 1 09/25/10 06:53 84-66-209/21/10 14:20367 56.72,4-Dimethylphenol ND ug/kg 1 09/25/10 06:53 105-67-909/21/10 14:20367 145Dimethylphthalate ND ug/kg 1 09/25/10 06:53 131-11-309/21/10 14:20367 74.5Di-n-butylphthalate ND ug/kg 1 09/25/10 06:53 84-74-209/21/10 14:20367 60.14,6-Dinitro-2-methylphenol ND ug/kg 1 09/25/10 06:53 534-52-109/21/10 14:20734 73.42,4-Dinitrophenol ND ug/kg 1 09/25/10 06:53 51-28-509/21/10 14:201840 60.12,4-Dinitrotoluene ND ug/kg 1 09/25/10 06:53 121-14-209/21/10 14:20367 69.02,6-Dinitrotoluene ND ug/kg 1 09/25/10 06:53 606-20-209/21/10 14:20367 76.8Di-n-octylphthalate ND ug/kg 1 09/25/10 06:53 117-84-009/21/10 14:20367 76.8bis(2-Ethylhexyl)phthalate 144J ug/kg 1 09/25/10 06:53 117-81-709/21/10 14:20367 100Fluoranthene 75.9J ug/kg 1 09/25/10 06:53 206-44-009/21/10 14:20367 53.4Fluorene ND ug/kg 1 09/25/10 06:53 86-73-709/21/10 14:20367 75.7Hexachloro-1,3-butadiene ND ug/kg 1 09/25/10 06:53 87-68-309/21/10 14:20367 63.4Hexachlorobenzene ND ug/kg 1 09/25/10 06:53 118-74-109/21/10 14:20367 46.7Hexachlorocyclopentadiene ND ug/kg 1 09/25/10 06:53 77-47-409/21/10 14:20367 67.9Hexachloroethane ND ug/kg 1 09/25/10 06:53 67-72-109/21/10 14:20367 96.8Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/25/10 06:53 193-39-509/21/10 14:20367 75.7Isophorone ND ug/kg 1 09/25/10 06:53 78-59-109/21/10 14:20367 82.32-Methylnaphthalene ND ug/kg 1 09/25/10 06:53 91-57-609/21/10 14:20367 79.02-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 06:53 95-48-709/21/10 14:20367 1113&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 06:5309/21/10 14:20367 145Naphthalene ND ug/kg 1 09/25/10 06:53 91-20-309/21/10 14:20367 90.12-Nitroaniline ND ug/kg 1 09/25/10 06:53 88-74-409/21/10 14:201840 1133-Nitroaniline ND ug/kg 1 09/25/10 06:53 99-09-209/21/10 14:201840 1004-Nitroaniline ND ug/kg 1 09/25/10 06:53 100-01-609/21/10 14:20734 103Nitrobenzene ND ug/kg 1 09/25/10 06:53 98-95-309/21/10 14:20367 1002-Nitrophenol ND ug/kg 1 09/25/10 06:53 88-75-509/21/10 14:20367 89.04-Nitrophenol ND ug/kg 1 09/25/10 06:53 100-02-709/21/10 14:201840 65.6N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 06:53 621-64-709/21/10 14:20367 70.1N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 06:53 86-30-609/21/10 14:20367 109Pentachlorophenol ND ug/kg 1 09/25/10 06:53 87-86-509/21/10 14:201840 66.8Phenanthrene ND ug/kg 1 09/25/10 06:53 85-01-809/21/10 14:20367 61.2Phenol ND ug/kg 1 09/25/10 06:53 108-95-2 H509/21/10 14:20367 110Pyrene ND ug/kg 1 09/25/10 06:53 129-00-009/21/10 14:20367 62.31,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 06:53 95-94-309/21/10 14:20367 1342,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 06:53 58-90-209/21/10 14:20367 1452,4,5-Trichlorophenol ND ug/kg 1 09/25/10 06:53 95-95-409/21/10 14:20367 1132,4,6-Trichlorophenol ND ug/kg 1 09/25/10 06:53 88-06-209/21/10 14:20367 81.22-Fluorobiphenyl (S) 48 % 1 09/25/10 06:53 321-60-809/21/10 14:2030-110Terphenyl-d14 (S) 51 % 1 09/25/10 06:53 1718-51-009/21/10 14:2028-110Phenol-d6 (S) 29 % 1 09/25/10 06:53 13127-88-309/21/10 14:2022-1102-Fluorophenol (S) 29 % 1 09/25/10 06:53 367-12-409/21/10 14:2013-1102,4,6-Tribromophenol (S) 51 % 1 09/25/10 06:53 118-79-609/21/10 14:2027-110



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Nitrobenzene-d5 (S) 33 % 1 09/25/10 06:53 4165-60-009/21/10 14:2023-110


Acetone 153 ug/kg 1 09/10/10 01:20 67-64-1 C9129 12.9Benzene ND ug/kg 1 09/10/10 01:20 71-43-26.4 2.1Bromochloromethane ND ug/kg 1 09/10/10 01:20 74-97-56.4 2.2Bromodichloromethane ND ug/kg 1 09/10/10 01:20 75-27-46.4 2.4Bromoform ND ug/kg 1 09/10/10 01:20 75-25-26.4 3.0Bromomethane ND ug/kg 1 09/10/10 01:20 74-83-912.9 3.22-Butanone (MEK) 12.7J ug/kg 1 09/10/10 01:20 78-93-3129 3.7Carbon disulfide 5.2J ug/kg 1 09/10/10 01:20 75-15-012.9 3.9Carbon tetrachloride ND ug/kg 1 09/10/10 01:20 56-23-56.4 3.3Chlorobenzene ND ug/kg 1 09/10/10 01:20 108-90-76.4 2.4Chloroethane ND ug/kg 1 09/10/10 01:20 75-00-312.9 3.1Chloroform ND ug/kg 1 09/10/10 01:20 67-66-36.4 2.1Chloromethane ND ug/kg 1 09/10/10 01:20 74-87-312.9 3.1Cyclohexane ND ug/kg 1 09/10/10 01:20 110-82-76.4 2.11,2-Dibromo-3-chloropropane ND ug/kg 1 09/10/10 01:20 96-12-86.4 4.6Dibromochloromethane ND ug/kg 1 09/10/10 01:20 124-48-16.4 2.31,2-Dibromoethane (EDB) ND ug/kg 1 09/10/10 01:20 106-93-46.4 2.31,2-Dichlorobenzene ND ug/kg 1 09/10/10 01:20 95-50-16.4 2.41,3-Dichlorobenzene ND ug/kg 1 09/10/10 01:20 541-73-16.4 2.61,4-Dichlorobenzene ND ug/kg 1 09/10/10 01:20 106-46-76.4 2.2Dichlorodifluoromethane ND ug/kg 1 09/10/10 01:20 75-71-812.9 4.61,1-Dichloroethane ND ug/kg 1 09/10/10 01:20 75-34-36.4 1.91,2-Dichloroethane ND ug/kg 1 09/10/10 01:20 107-06-26.4 2.81,1-Dichloroethene ND ug/kg 1 09/10/10 01:20 75-35-46.4 2.3cis-1,2-Dichloroethene ND ug/kg 1 09/10/10 01:20 156-59-26.4 1.8trans-1,2-Dichloroethene ND ug/kg 1 09/10/10 01:20 156-60-56.4 2.41,2-Dichloropropane ND ug/kg 1 09/10/10 01:20 78-87-56.4 2.2cis-1,3-Dichloropropene ND ug/kg 1 09/10/10 01:20 10061-01-56.4 2.3trans-1,3-Dichloropropene ND ug/kg 1 09/10/10 01:20 10061-02-66.4 1.9Ethylbenzene ND ug/kg 1 09/10/10 01:20 100-41-46.4 2.32-Hexanone ND ug/kg 1 09/10/10 01:20 591-78-664.4 5.0Isopropylbenzene (Cumene) ND ug/kg 1 09/10/10 01:20 98-82-86.4 2.4Methyl acetate ND ug/kg 1 09/10/10 01:20 79-20-912.9 1.8Methylcyclohexane ND ug/kg 1 09/10/10 01:20 108-87-212.9 1.9Methylene Chloride ND ug/kg 1 09/10/10 01:20 75-09-225.8 3.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/10/10 01:20 108-10-164.4 4.8Methyl-tert-butyl ether ND ug/kg 1 09/10/10 01:20 1634-04-46.4 1.9Styrene ND ug/kg 1 09/10/10 01:20 100-42-56.4 2.31,1,2,2-Tetrachloroethane ND ug/kg 1 09/10/10 01:20 79-34-56.4 2.4Tetrachloroethene ND ug/kg 1 09/10/10 01:20 127-18-46.4 2.2Toluene ND ug/kg 1 09/10/10 01:20 108-88-36.4 2.31,2,3-Trichlorobenzene ND ug/kg 1 09/10/10 01:20 87-61-66.4 2.8



Date: 09/27/2010 06:48 PM Page 200 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744








Cyanide ND mg/kg 1 09/14/10 10:40 57-12-50.19 0.19





Date: 09/27/2010 06:48 PM Page 201 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 5 09/22/10 18:25 7440-36-0 D309/09/10 14:302.7 1.5Arsenic 2.7 mg/kg 5 09/22/10 18:25 7440-38-2 D309/09/10 14:302.7 1.7Beryllium 1.7 mg/kg 5 09/22/10 18:25 7440-41-709/09/10 14:300.54 0.11Cadmium ND mg/kg 5 09/22/10 18:25 7440-43-9 D309/09/10 14:300.54 0.33Chromium 33.1 mg/kg 5 09/22/10 18:25 7440-47-309/09/10 14:302.7 0.16Copper 27.3 mg/kg 5 09/22/10 18:25 7440-50-809/09/10 14:302.7 0.22Lead 12.6 mg/kg 5 09/22/10 18:25 7439-92-109/09/10 14:302.7 2.6Manganese 433 mg/kg 5 09/22/10 18:25 7439-96-509/09/10 14:302.7 0.16Nickel 16.4 mg/kg 5 09/22/10 18:25 7440-02-009/09/10 14:302.7 0.98Selenium ND mg/kg 5 09/22/10 18:25 7782-49-2 D309/09/10 14:305.4 2.1Silver 0.22J mg/kg 5 09/22/10 18:25 7440-22-4 D309/09/10 14:302.7 0.16Thallium ND mg/kg 5 09/22/10 18:25 7440-28-0 D309/09/10 14:305.4 1.4Zinc 65.7 mg/kg 5 09/22/10 18:25 7440-66-609/09/10 14:305.4 1.4


Mercury 0.070 mg/kg 1 09/14/10 15:14 7439-97-609/14/10 08:130.0064 0.00013







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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 2 09/22/10 18:29 7440-36-0 D309/09/10 14:301.2 0.68Arsenic 1.2 mg/kg 2 09/22/10 18:29 7440-38-2 D309/09/10 14:301.2 0.77Beryllium 1.2 mg/kg 2 09/22/10 18:29 7440-41-709/09/10 14:300.24 0.048Cadmium ND mg/kg 2 09/22/10 18:29 7440-43-9 D309/09/10 14:300.24 0.14Chromium 24.6 mg/kg 2 09/22/10 18:29 7440-47-309/09/10 14:301.2 0.072Copper 18.9 mg/kg 2 09/22/10 18:29 7440-50-809/09/10 14:301.2 0.097Lead 9.9 mg/kg 2 09/22/10 18:29 7439-92-109/09/10 14:301.2 1.2Manganese 150 mg/kg 2 09/22/10 18:29 7439-96-509/09/10 14:301.2 0.072Nickel 11.9 mg/kg 2 09/22/10 18:29 7440-02-009/09/10 14:301.2 0.43Selenium ND mg/kg 2 09/22/10 18:29 7782-49-2 D309/09/10 14:302.4 0.92Silver ND mg/kg 2 09/22/10 18:29 7440-22-4 D309/09/10 14:301.2 0.072Thallium ND mg/kg 2 09/22/10 18:29 7440-28-0 D309/09/10 14:302.4 0.63Zinc 45.4 mg/kg 2 09/22/10 18:29 7440-66-609/09/10 14:302.4 0.63


Mercury 0.040 mg/kg 1 09/14/10 15:16 7439-97-609/14/10 08:130.0050 0.000099







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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: FD-16 Lab ID: 9276872054 Collected: 09/01/10 00:00 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "dry-weight" basis






Date: 09/27/2010 06:48 PM Page 204 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/25/10 07:29 193-39-509/15/10 13:00371 76.5Isophorone ND ug/kg 1 09/25/10 07:29 78-59-109/15/10 13:00371 83.22-Methylnaphthalene ND ug/kg 1 09/25/10 07:29 91-57-609/15/10 13:00371 79.92-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 07:29 95-48-709/15/10 13:00371 1123&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 07:2909/15/10 13:00371 146Naphthalene ND ug/kg 1 09/25/10 07:29 91-20-309/15/10 13:00371 91.12-Nitroaniline ND ug/kg 1 09/25/10 07:29 88-74-409/15/10 13:001860 1153-Nitroaniline ND ug/kg 1 09/25/10 07:29 99-09-209/15/10 13:001860 1014-Nitroaniline ND ug/kg 1 09/25/10 07:29 100-01-609/15/10 13:00742 105Nitrobenzene ND ug/kg 1 09/25/10 07:29 98-95-309/15/10 13:00371 1012-Nitrophenol ND ug/kg 1 09/25/10 07:29 88-75-509/15/10 13:00371 90.04-Nitrophenol ND ug/kg 1 09/25/10 07:29 100-02-709/15/10 13:001860 66.4N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 07:29 621-64-709/15/10 13:00371 70.9N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 07:29 86-30-609/15/10 13:00371 110Pentachlorophenol ND ug/kg 1 09/25/10 07:29 87-86-509/15/10 13:001860 67.5Phenanthrene ND ug/kg 1 09/25/10 07:29 85-01-809/15/10 13:00371 61.9Phenol ND ug/kg 1 09/25/10 07:29 108-95-209/15/10 13:00371 111Pyrene ND ug/kg 1 09/25/10 07:29 129-00-009/15/10 13:00371 63.01,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 07:29 95-94-309/15/10 13:00371 1352,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 07:29 58-90-209/15/10 13:00371 1462,4,5-Trichlorophenol ND ug/kg 1 09/25/10 07:29 95-95-409/15/10 13:00371 1152,4,6-Trichlorophenol ND ug/kg 1 09/25/10 07:29 88-06-209/15/10 13:00371 82.12-Fluorobiphenyl (S) 25 % 1 09/25/10 07:29 321-60-8 S209/15/10 13:0030-110Terphenyl-d14 (S) 37 % 1 09/25/10 07:29 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 16 % 1 09/25/10 07:29 13127-88-3 S209/15/10 13:0022-1102-Fluorophenol (S) 17 % 1 09/25/10 07:29 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 29 % 1 09/25/10 07:29 118-79-609/15/10 13:0027-110Nitrobenzene-d5 (S) 19 % 1 09/25/10 07:29 4165-60-0 S209/15/10 13:0023-110





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Asheville, NC 28804

(828)254-7176

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Mercury 0.0061 mg/kg 1 09/14/10 15:19 7439-97-609/14/10 08:130.0042 0.000084





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(828)254-7176

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Asheville, NC 28804

(828)254-7176

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9276872MILLS GAP 6686081744






Cyanide ND mg/kg 1 09/14/10 10:12 57-12-50.14 0.14



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(828)254-7176

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Acenaphthene ND ug/kg 1 09/25/10 08:05 83-32-909/21/10 14:20402 92.5Acenaphthylene ND ug/kg 1 09/25/10 08:05 208-96-809/21/10 14:20402 94.9Acetophenone ND ug/kg 1 09/25/10 08:05 98-86-209/21/10 14:20402 207Anthracene ND ug/kg 1 09/25/10 08:05 120-12-709/21/10 14:20402 90.0Atrazine ND ug/kg 1 09/25/10 08:05 1912-24-909/21/10 14:20803 158Benzaldehyde ND ug/kg 1 09/25/10 08:05 100-52-709/21/10 14:20803 402Benzo(a)anthracene ND ug/kg 1 09/25/10 08:05 56-55-309/21/10 14:20402 74.2Benzo(a)pyrene ND ug/kg 1 09/25/10 08:05 50-32-809/21/10 14:20402 76.7Benzo(b)fluoranthene ND ug/kg 1 09/25/10 08:05 205-99-209/21/10 14:20402 69.4Benzo(g,h,i)perylene ND ug/kg 1 09/25/10 08:05 191-24-209/21/10 14:20402 102Benzo(k)fluoranthene ND ug/kg 1 09/25/10 08:05 207-08-909/21/10 14:20402 79.1Biphenyl (Diphenyl) ND ug/kg 1 09/25/10 08:05 92-52-409/21/10 14:20402 1274-Bromophenylphenyl ether ND ug/kg 1 09/25/10 08:05 101-55-309/21/10 14:20402 73.0Butylbenzylphthalate ND ug/kg 1 09/25/10 08:05 85-68-709/21/10 14:20402 85.2Caprolactam ND ug/kg 1 09/25/10 08:05 105-60-209/21/10 14:20402 69.4Carbazole ND ug/kg 1 09/25/10 08:05 86-74-809/21/10 14:20402 76.74-Chloro-3-methylphenol ND ug/kg 1 09/25/10 08:05 59-50-709/21/10 14:20803 82.74-Chloroaniline ND ug/kg 1 09/25/10 08:05 106-47-809/21/10 14:202010 112bis(2-Chloroethoxy)methane ND ug/kg 1 09/25/10 08:05 111-91-109/21/10 14:20402 93.7bis(2-Chloroethyl) ether ND ug/kg 1 09/25/10 08:05 111-44-409/21/10 14:20402 102bis(2-Chloroisopropyl) ether ND ug/kg 1 09/25/10 08:05 108-60-109/21/10 14:20402 1072-Chloronaphthalene ND ug/kg 1 09/25/10 08:05 91-58-709/21/10 14:20402 79.12-Chlorophenol ND ug/kg 1 09/25/10 08:05 95-57-809/21/10 14:20402 1104-Chlorophenylphenyl ether ND ug/kg 1 09/25/10 08:05 7005-72-309/21/10 14:20402 82.7Chrysene ND ug/kg 1 09/25/10 08:05 218-01-909/21/10 14:20402 53.5Dibenz(a,h)anthracene ND ug/kg 1 09/25/10 08:05 53-70-309/21/10 14:20402 85.2Dibenzofuran ND ug/kg 1 09/25/10 08:05 132-64-909/21/10 14:20402 65.73,3'-Dichlorobenzidine ND ug/kg 1 09/25/10 08:05 91-94-109/21/10 14:202010 87.62,4-Dichlorophenol ND ug/kg 1 09/25/10 08:05 120-83-209/21/10 14:20402 87.6Diethylphthalate ND ug/kg 1 09/25/10 08:05 84-66-209/21/10 14:20402 62.12,4-Dimethylphenol ND ug/kg 1 09/25/10 08:05 105-67-909/21/10 14:20402 158Dimethylphthalate ND ug/kg 1 09/25/10 08:05 131-11-309/21/10 14:20402 81.5Di-n-butylphthalate ND ug/kg 1 09/25/10 08:05 84-74-209/21/10 14:20402 65.74,6-Dinitro-2-methylphenol ND ug/kg 1 09/25/10 08:05 534-52-109/21/10 14:20803 80.32,4-Dinitrophenol ND ug/kg 1 09/25/10 08:05 51-28-509/21/10 14:202010 65.72,4-Dinitrotoluene ND ug/kg 1 09/25/10 08:05 121-14-209/21/10 14:20402 75.42,6-Dinitrotoluene ND ug/kg 1 09/25/10 08:05 606-20-209/21/10 14:20402 84.0Di-n-octylphthalate ND ug/kg 1 09/25/10 08:05 117-84-009/21/10 14:20402 84.0bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/25/10 08:05 117-81-709/21/10 14:20402 110Fluoranthene ND ug/kg 1 09/25/10 08:05 206-44-009/21/10 14:20402 58.4Fluorene ND ug/kg 1 09/25/10 08:05 86-73-709/21/10 14:20402 82.7Hexachloro-1,3-butadiene ND ug/kg 1 09/25/10 08:05 87-68-309/21/10 14:20402 69.4Hexachlorobenzene ND ug/kg 1 09/25/10 08:05 118-74-109/21/10 14:20402 51.1Hexachlorocyclopentadiene ND ug/kg 1 09/25/10 08:05 77-47-409/21/10 14:20402 74.2Hexachloroethane ND ug/kg 1 09/25/10 08:05 67-72-109/21/10 14:20402 106



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/25/10 08:05 193-39-509/21/10 14:20402 82.7Isophorone ND ug/kg 1 09/25/10 08:05 78-59-109/21/10 14:20402 90.02-Methylnaphthalene ND ug/kg 1 09/25/10 08:05 91-57-609/21/10 14:20402 86.42-Methylphenol(o-Cresol) ND ug/kg 1 09/25/10 08:05 95-48-709/21/10 14:20402 1223&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/25/10 08:0509/21/10 14:20402 158Naphthalene ND ug/kg 1 09/25/10 08:05 91-20-309/21/10 14:20402 98.62-Nitroaniline ND ug/kg 1 09/25/10 08:05 88-74-409/21/10 14:202010 1243-Nitroaniline ND ug/kg 1 09/25/10 08:05 99-09-209/21/10 14:202010 1104-Nitroaniline ND ug/kg 1 09/25/10 08:05 100-01-609/21/10 14:20803 113Nitrobenzene ND ug/kg 1 09/25/10 08:05 98-95-309/21/10 14:20402 1102-Nitrophenol ND ug/kg 1 09/25/10 08:05 88-75-509/21/10 14:20402 97.34-Nitrophenol ND ug/kg 1 09/25/10 08:05 100-02-709/21/10 14:202010 71.8N-Nitroso-di-n-propylamine ND ug/kg 1 09/25/10 08:05 621-64-709/21/10 14:20402 76.7N-Nitrosodiphenylamine ND ug/kg 1 09/25/10 08:05 86-30-609/21/10 14:20402 119Pentachlorophenol ND ug/kg 1 09/25/10 08:05 87-86-509/21/10 14:202010 73.0Phenanthrene ND ug/kg 1 09/25/10 08:05 85-01-809/21/10 14:20402 66.9Phenol ND ug/kg 1 09/25/10 08:05 108-95-2 H509/21/10 14:20402 120Pyrene ND ug/kg 1 09/25/10 08:05 129-00-009/21/10 14:20402 68.11,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/25/10 08:05 95-94-309/21/10 14:20402 1462,3,4,6-Tetrachlorophenol ND ug/kg 1 09/25/10 08:05 58-90-209/21/10 14:20402 1582,4,5-Trichlorophenol ND ug/kg 1 09/25/10 08:05 95-95-409/21/10 14:20402 1242,4,6-Trichlorophenol ND ug/kg 1 09/25/10 08:05 88-06-209/21/10 14:20402 88.82-Fluorobiphenyl (S) 40 % 1 09/25/10 08:05 321-60-809/21/10 14:2030-110Terphenyl-d14 (S) 50 % 1 09/25/10 08:05 1718-51-009/21/10 14:2028-110Phenol-d6 (S) 27 % 1 09/25/10 08:05 13127-88-309/21/10 14:2022-1102-Fluorophenol (S) 31 % 1 09/25/10 08:05 367-12-409/21/10 14:2013-1102,4,6-Tribromophenol (S) 46 % 1 09/25/10 08:05 118-79-609/21/10 14:2027-110Nitrobenzene-d5 (S) 31 % 1 09/25/10 08:05 4165-60-009/21/10 14:2023-110





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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Antimony ND mg/kg 20 09/14/10 15:40 7440-36-0 D309/10/10 15:157.9 4.4Arsenic ND mg/kg 20 09/14/10 15:40 7440-38-2 D309/10/10 15:157.9 5.1Beryllium 1.4J mg/kg 20 09/14/10 15:40 7440-41-7 D309/10/10 15:151.6 0.32Cadmium ND mg/kg 20 09/14/10 15:40 7440-43-9 D309/10/10 15:151.6 0.95Chromium 18.0 mg/kg 20 09/14/10 15:40 7440-47-3 D309/10/10 15:157.9 0.47Copper 1.6J mg/kg 20 09/14/10 15:40 7440-50-8 D309/10/10 15:157.9 0.63Lead ND mg/kg 20 09/14/10 15:40 7439-92-1 D309/10/10 15:157.9 7.6Manganese 249 mg/kg 20 09/14/10 15:40 7439-96-5 D309/10/10 15:157.9 0.47Nickel 14.6 mg/kg 20 09/14/10 15:40 7440-02-0 D309/10/10 15:157.9 2.8Selenium ND mg/kg 20 09/14/10 15:40 7782-49-2 D309/10/10 15:1515.8 6.0Silver ND mg/kg 20 09/14/10 15:40 7440-22-4 D309/10/10 15:157.9 0.47Thallium ND mg/kg 20 09/14/10 15:40 7440-28-0 D309/10/10 15:1515.8 4.1Zinc 90.1 mg/kg 20 09/14/10 15:40 7440-66-609/10/10 15:1515.8 4.1


Mercury 0.0010J mg/kg 1 09/14/10 15:22 7439-97-609/14/10 08:130.0031 0.000062





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(704)875-9092


Asheville, NC 28804

(828)254-7176

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9276872MILLS GAP 6686081744









Date: 09/27/2010 06:48 PM Page 212 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744






Cyanide ND mg/kg 1 09/14/10 10:13 57-12-50.12 0.12



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(704)875-9092


Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Acenaphthene ND ug/kg 1 09/20/10 22:24 83-32-909/15/10 13:00430 99.1Acenaphthylene ND ug/kg 1 09/20/10 22:24 208-96-809/15/10 13:00430 102Acetophenone ND ug/kg 1 09/20/10 22:24 98-86-209/15/10 13:00430 222Anthracene ND ug/kg 1 09/20/10 22:24 120-12-709/15/10 13:00430 96.5Atrazine ND ug/kg 1 09/20/10 22:24 1912-24-909/15/10 13:00860 169Benzaldehyde ND ug/kg 1 09/20/10 22:24 100-52-709/15/10 13:00860 430Benzo(a)anthracene ND ug/kg 1 09/20/10 22:24 56-55-309/15/10 13:00430 79.5Benzo(a)pyrene ND ug/kg 1 09/20/10 22:24 50-32-809/15/10 13:00430 82.1Benzo(b)fluoranthene ND ug/kg 1 09/20/10 22:24 205-99-209/15/10 13:00430 74.3Benzo(g,h,i)perylene ND ug/kg 1 09/20/10 22:24 191-24-209/15/10 13:00430 110Benzo(k)fluoranthene ND ug/kg 1 09/20/10 22:24 207-08-909/15/10 13:00430 84.7Biphenyl (Diphenyl) ND ug/kg 1 09/20/10 22:24 92-52-409/15/10 13:00430 1364-Bromophenylphenyl ether ND ug/kg 1 09/20/10 22:24 101-55-309/15/10 13:00430 78.2Butylbenzylphthalate ND ug/kg 1 09/20/10 22:24 85-68-709/15/10 13:00430 91.3Caprolactam ND ug/kg 1 09/20/10 22:24 105-60-209/15/10 13:00430 74.3Carbazole ND ug/kg 1 09/20/10 22:24 86-74-809/15/10 13:00430 82.14-Chloro-3-methylphenol ND ug/kg 1 09/20/10 22:24 59-50-709/15/10 13:00860 88.74-Chloroaniline ND ug/kg 1 09/20/10 22:24 106-47-809/15/10 13:002150 120bis(2-Chloroethoxy)methane ND ug/kg 1 09/20/10 22:24 111-91-109/15/10 13:00430 100bis(2-Chloroethyl) ether ND ug/kg 1 09/20/10 22:24 111-44-409/15/10 13:00430 110bis(2-Chloroisopropyl) ether ND ug/kg 1 09/20/10 22:24 108-60-109/15/10 13:00430 1152-Chloronaphthalene ND ug/kg 1 09/20/10 22:24 91-58-709/15/10 13:00430 84.72-Chlorophenol ND ug/kg 1 09/20/10 22:24 95-57-809/15/10 13:00430 1174-Chlorophenylphenyl ether ND ug/kg 1 09/20/10 22:24 7005-72-309/15/10 13:00430 88.7Chrysene ND ug/kg 1 09/20/10 22:24 218-01-909/15/10 13:00430 57.4Dibenz(a,h)anthracene ND ug/kg 1 09/20/10 22:24 53-70-309/15/10 13:00430 91.3Dibenzofuran ND ug/kg 1 09/20/10 22:24 132-64-909/15/10 13:00430 70.43,3'-Dichlorobenzidine ND ug/kg 1 09/20/10 22:24 91-94-109/15/10 13:002150 93.92,4-Dichlorophenol ND ug/kg 1 09/20/10 22:24 120-83-209/15/10 13:00430 93.9Diethylphthalate ND ug/kg 1 09/20/10 22:24 84-66-209/15/10 13:00430 66.52,4-Dimethylphenol ND ug/kg 1 09/20/10 22:24 105-67-909/15/10 13:00430 169Dimethylphthalate ND ug/kg 1 09/20/10 22:24 131-11-309/15/10 13:00430 87.3Di-n-butylphthalate ND ug/kg 1 09/20/10 22:24 84-74-209/15/10 13:00430 70.44,6-Dinitro-2-methylphenol ND ug/kg 1 09/20/10 22:24 534-52-109/15/10 13:00860 86.02,4-Dinitrophenol ND ug/kg 1 09/20/10 22:24 51-28-509/15/10 13:002150 70.42,4-Dinitrotoluene ND ug/kg 1 09/20/10 22:24 121-14-209/15/10 13:00430 80.82,6-Dinitrotoluene ND ug/kg 1 09/20/10 22:24 606-20-209/15/10 13:00430 90.0Di-n-octylphthalate ND ug/kg 1 09/20/10 22:24 117-84-009/15/10 13:00430 90.0bis(2-Ethylhexyl)phthalate ND ug/kg 1 09/20/10 22:24 117-81-709/15/10 13:00430 117Fluoranthene ND ug/kg 1 09/20/10 22:24 206-44-009/15/10 13:00430 62.6Fluorene ND ug/kg 1 09/20/10 22:24 86-73-709/15/10 13:00430 88.7Hexachloro-1,3-butadiene ND ug/kg 1 09/20/10 22:24 87-68-309/15/10 13:00430 74.3Hexachlorobenzene ND ug/kg 1 09/20/10 22:24 118-74-109/15/10 13:00430 54.8Hexachlorocyclopentadiene ND ug/kg 1 09/20/10 22:24 77-47-409/15/10 13:00430 79.5Hexachloroethane ND ug/kg 1 09/20/10 22:24 67-72-109/15/10 13:00430 113



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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744




Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/20/10 22:24 193-39-509/15/10 13:00430 88.7Isophorone ND ug/kg 1 09/20/10 22:24 78-59-109/15/10 13:00430 96.52-Methylnaphthalene ND ug/kg 1 09/20/10 22:24 91-57-609/15/10 13:00430 92.62-Methylphenol(o-Cresol) ND ug/kg 1 09/20/10 22:24 95-48-709/15/10 13:00430 1303&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/20/10 22:2409/15/10 13:00430 169Naphthalene ND ug/kg 1 09/20/10 22:24 91-20-309/15/10 13:00430 1062-Nitroaniline ND ug/kg 1 09/20/10 22:24 88-74-409/15/10 13:002150 1333-Nitroaniline ND ug/kg 1 09/20/10 22:24 99-09-209/15/10 13:002150 1174-Nitroaniline ND ug/kg 1 09/20/10 22:24 100-01-609/15/10 13:00860 121Nitrobenzene ND ug/kg 1 09/20/10 22:24 98-95-309/15/10 13:00430 1172-Nitrophenol ND ug/kg 1 09/20/10 22:24 88-75-509/15/10 13:00430 1044-Nitrophenol ND ug/kg 1 09/20/10 22:24 100-02-709/15/10 13:002150 76.9N-Nitroso-di-n-propylamine ND ug/kg 1 09/20/10 22:24 621-64-709/15/10 13:00430 82.1N-Nitrosodiphenylamine ND ug/kg 1 09/20/10 22:24 86-30-609/15/10 13:00430 128Pentachlorophenol ND ug/kg 1 09/20/10 22:24 87-86-509/15/10 13:002150 78.2Phenanthrene ND ug/kg 1 09/20/10 22:24 85-01-809/15/10 13:00430 71.7Phenol ND ug/kg 1 09/20/10 22:24 108-95-209/15/10 13:00430 129Pyrene ND ug/kg 1 09/20/10 22:24 129-00-009/15/10 13:00430 73.01,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/20/10 22:24 95-94-309/15/10 13:00430 1562,3,4,6-Tetrachlorophenol ND ug/kg 1 09/20/10 22:24 58-90-209/15/10 13:00430 1692,4,5-Trichlorophenol ND ug/kg 1 09/20/10 22:24 95-95-409/15/10 13:00430 1332,4,6-Trichlorophenol ND ug/kg 1 09/20/10 22:24 88-06-209/15/10 13:00430 95.22-Fluorobiphenyl (S) 35 % 1 09/20/10 22:24 321-60-809/15/10 13:0030-110Terphenyl-d14 (S) 31 % 1 09/20/10 22:24 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 25 % 1 09/20/10 22:24 13127-88-309/15/10 13:0022-1102-Fluorophenol (S) 30 % 1 09/20/10 22:24 367-12-409/15/10 13:0013-1102,4,6-Tribromophenol (S) 28 % 1 09/20/10 22:24 118-79-609/15/10 13:0027-110Nitrobenzene-d5 (S) 31 % 1 09/20/10 22:24 4165-60-009/15/10 13:0023-110





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Asheville, NC 28804

(828)254-7176

ANALYTICAL RESULTS


9276872MILLS GAP 6686081744







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(828)254-7176

ANALYTICAL RESULTS


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(704)875-9092


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(828)254-7176

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Antimony ND mg/kg 5 09/14/10 15:47 7440-36-0 D309/10/10 15:152.4 1.3Arsenic ND mg/kg 5 09/14/10 15:47 7440-38-2 D309/10/10 15:152.4 1.5Beryllium 1.1 mg/kg 5 09/14/10 15:47 7440-41-7 D309/10/10 15:150.48 0.096Cadmium ND mg/kg 5 09/14/10 15:47 7440-43-9 D309/10/10 15:150.48 0.29Chromium 12.6 mg/kg 5 09/14/10 15:47 7440-47-3 D309/10/10 15:152.4 0.14Copper 13.3 mg/kg 5 09/14/10 15:47 7440-50-8 D309/10/10 15:152.4 0.19Lead 5.0 mg/kg 5 09/14/10 15:47 7439-92-1 D309/10/10 15:152.4 2.3Manganese 681 mg/kg 5 09/14/10 15:47 7439-96-5 D309/10/10 15:152.4 0.14Nickel 8.7 mg/kg 5 09/14/10 15:47 7440-02-0 D309/10/10 15:152.4 0.86Selenium ND mg/kg 5 09/14/10 15:47 7782-49-2 D309/10/10 15:154.8 1.8Silver ND mg/kg 5 09/14/10 15:47 7440-22-4 D309/10/10 15:152.4 0.14Thallium 1.5J mg/kg 5 09/14/10 15:47 7440-28-0 D309/10/10 15:154.8 1.2Zinc 82.5 mg/kg 5 09/14/10 15:47 7440-66-6 D309/10/10 15:154.8 1.2


Mercury ND mg/kg 1 09/14/10 15:24 7439-97-609/14/10 08:130.0043 0.000086





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Cyanide ND mg/kg 1 09/14/10 10:16 57-12-50.16 0.16



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Indeno(1,2,3-cd)pyrene ND ug/kg 1 09/23/10 18:37 193-39-509/15/10 13:00369 76.0Isophorone ND ug/kg 1 09/23/10 18:37 78-59-109/15/10 13:00369 82.72-Methylnaphthalene ND ug/kg 1 09/23/10 18:37 91-57-609/15/10 13:00369 79.42-Methylphenol(o-Cresol) ND ug/kg 1 09/23/10 18:37 95-48-709/15/10 13:00369 1123&4-Methylphenol(m&p Cresol) ND ug/kg 1 09/23/10 18:3709/15/10 13:00369 145Naphthalene ND ug/kg 1 09/23/10 18:37 91-20-309/15/10 13:00369 90.62-Nitroaniline ND ug/kg 1 09/23/10 18:37 88-74-409/15/10 13:001840 1143-Nitroaniline ND ug/kg 1 09/23/10 18:37 99-09-209/15/10 13:001840 1014-Nitroaniline ND ug/kg 1 09/23/10 18:37 100-01-609/15/10 13:00738 104Nitrobenzene ND ug/kg 1 09/23/10 18:37 98-95-309/15/10 13:00369 1012-Nitrophenol ND ug/kg 1 09/23/10 18:37 88-75-509/15/10 13:00369 89.54-Nitrophenol ND ug/kg 1 09/23/10 18:37 100-02-709/15/10 13:001840 66.0N-Nitroso-di-n-propylamine ND ug/kg 1 09/23/10 18:37 621-64-709/15/10 13:00369 70.4N-Nitrosodiphenylamine ND ug/kg 1 09/23/10 18:37 86-30-609/15/10 13:00369 110Pentachlorophenol ND ug/kg 1 09/23/10 18:37 87-86-509/15/10 13:001840 67.1Phenanthrene ND ug/kg 1 09/23/10 18:37 85-01-809/15/10 13:00369 61.5Phenol ND ug/kg 1 09/23/10 18:37 108-95-209/15/10 13:00369 111Pyrene ND ug/kg 1 09/23/10 18:37 129-00-009/15/10 13:00369 62.61,2,4,5-Tetrachlorobenzene ND ug/kg 1 09/23/10 18:37 95-94-309/15/10 13:00369 1342,3,4,6-Tetrachlorophenol ND ug/kg 1 09/23/10 18:37 58-90-209/15/10 13:00369 1452,4,5-Trichlorophenol ND ug/kg 1 09/23/10 18:37 95-95-409/15/10 13:00369 1142,4,6-Trichlorophenol ND ug/kg 1 09/23/10 18:37 88-06-209/15/10 13:00369 81.62-Fluorobiphenyl (S) 18 % 1 09/23/10 18:37 321-60-8 S209/15/10 13:0030-110Terphenyl-d14 (S) 34 % 1 09/23/10 18:37 1718-51-009/15/10 13:0028-110Phenol-d6 (S) 12 % 1 09/23/10 18:37 13127-88-3 S209/15/10 13:0022-1102-Fluorophenol (S) 11 % 1 09/23/10 18:37 367-12-4 S209/15/10 13:0013-1102,4,6-Tribromophenol (S) 24 % 1 09/23/10 18:37 118-79-6 S209/15/10 13:0027-110Nitrobenzene-d5 (S) 11 % 1 09/23/10 18:37 4165-60-0 S209/15/10 13:0023-110





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Antimony 0.76J mg/kg 2 09/14/10 15:50 7440-36-0 D309/10/10 15:151.2 0.65Arsenic 1.3 mg/kg 2 09/14/10 15:50 7440-38-2 D309/10/10 15:151.2 0.75Beryllium 1.4 mg/kg 2 09/14/10 15:50 7440-41-7 D309/10/10 15:150.23 0.047Cadmium 0.18J mg/kg 2 09/14/10 15:50 7440-43-9 D309/10/10 15:150.23 0.14Chromium 24.3 mg/kg 2 09/14/10 15:50 7440-47-3 D309/10/10 15:151.2 0.070Copper 21.0 mg/kg 2 09/14/10 15:50 7440-50-8 D309/10/10 15:151.2 0.094Lead 9.4 mg/kg 2 09/14/10 15:50 7439-92-1 D309/10/10 15:151.2 1.1Manganese 171 mg/kg 2 09/14/10 15:50 7439-96-5 D309/10/10 15:151.2 0.070Nickel 11.0 mg/kg 2 09/14/10 15:50 7440-02-0 D309/10/10 15:151.2 0.42Selenium ND mg/kg 2 09/14/10 15:50 7782-49-2 D309/10/10 15:152.3 0.89Silver ND mg/kg 2 09/14/10 15:50 7440-22-4 D309/10/10 15:151.2 0.070Thallium ND mg/kg 2 09/14/10 15:50 7440-28-0 D309/10/10 15:152.3 0.61Zinc 46.5 mg/kg 2 09/14/10 15:50 7440-66-6 D309/10/10 15:152.3 0.61


Mercury 0.026 mg/kg 1 09/16/10 12:22 7439-97-6 B09/15/10 15:390.0056 0.00011





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Sample: TB-06 Lab ID: 9276872070 Collected: 09/01/10 00:00 Received: 09/02/10 16:22 Matrix: SolidResults reported on a "wet-weight" basis






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Acetone 12.1J ug/kg 1 09/08/10 04:57 67-64-1100 10.0Benzene ND ug/kg 1 09/08/10 04:57 71-43-25.0 1.6Bromochloromethane ND ug/kg 1 09/08/10 04:57 74-97-55.0 1.7Bromodichloromethane ND ug/kg 1 09/08/10 04:57 75-27-45.0 1.9Bromoform ND ug/kg 1 09/08/10 04:57 75-25-25.0 2.3Bromomethane ND ug/kg 1 09/08/10 04:57 74-83-910.0 2.52-Butanone (MEK) ND ug/kg 1 09/08/10 04:57 78-93-3100 2.9Carbon disulfide ND ug/kg 1 09/08/10 04:57 75-15-010.0 3.0Carbon tetrachloride ND ug/kg 1 09/08/10 04:57 56-23-55.0 2.6Chlorobenzene ND ug/kg 1 09/08/10 04:57 108-90-75.0 1.9Chloroethane ND ug/kg 1 09/08/10 04:57 75-00-310.0 2.4Chloroform ND ug/kg 1 09/08/10 04:57 67-66-35.0 1.6Chloromethane ND ug/kg 1 09/08/10 04:57 74-87-310.0 2.4Cyclohexane ND ug/kg 1 09/08/10 04:57 110-82-75.0 1.61,2-Dibromo-3-chloropropane ND ug/kg 1 09/08/10 04:57 96-12-85.0 3.6Dibromochloromethane ND ug/kg 1 09/08/10 04:57 124-48-15.0 1.81,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 04:57 106-93-45.0 1.81,2-Dichlorobenzene ND ug/kg 1 09/08/10 04:57 95-50-15.0 1.91,3-Dichlorobenzene ND ug/kg 1 09/08/10 04:57 541-73-15.0 2.01,4-Dichlorobenzene ND ug/kg 1 09/08/10 04:57 106-46-75.0 1.7Dichlorodifluoromethane ND ug/kg 1 09/08/10 04:57 75-71-810.0 3.61,1-Dichloroethane ND ug/kg 1 09/08/10 04:57 75-34-35.0 1.51,2-Dichloroethane ND ug/kg 1 09/08/10 04:57 107-06-25.0 2.21,1-Dichloroethene ND ug/kg 1 09/08/10 04:57 75-35-45.0 1.8cis-1,2-Dichloroethene ND ug/kg 1 09/08/10 04:57 156-59-25.0 1.4trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 04:57 156-60-55.0 1.91,2-Dichloropropane ND ug/kg 1 09/08/10 04:57 78-87-55.0 1.7cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 04:57 10061-01-55.0 1.8trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 04:57 10061-02-65.0 1.5Ethylbenzene ND ug/kg 1 09/08/10 04:57 100-41-45.0 1.82-Hexanone ND ug/kg 1 09/08/10 04:57 591-78-650.1 3.9Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 04:57 98-82-85.0 1.9Methyl acetate 1.7J ug/kg 1 09/08/10 04:57 79-20-910.0 1.4Methylcyclohexane ND ug/kg 1 09/08/10 04:57 108-87-210.0 1.5Methylene Chloride ND ug/kg 1 09/08/10 04:57 75-09-220.1 3.04-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 04:57 108-10-150.1 3.7Methyl-tert-butyl ether ND ug/kg 1 09/08/10 04:57 1634-04-45.0 1.5Styrene ND ug/kg 1 09/08/10 04:57 100-42-55.0 1.81,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 04:57 79-34-55.0 1.9Tetrachloroethene ND ug/kg 1 09/08/10 04:57 127-18-45.0 1.7Toluene ND ug/kg 1 09/08/10 04:57 108-88-35.0 1.81,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 04:57 87-61-65.0 2.21,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 04:57 120-82-15.0 1.61,1,1-Trichloroethane ND ug/kg 1 09/08/10 04:57 71-55-65.0 1.81,1,2-Trichloroethane ND ug/kg 1 09/08/10 04:57 79-00-55.0 2.1



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Acetone ND ug/kg 1 09/08/10 05:54 67-64-195.5 9.5Benzene ND ug/kg 1 09/08/10 05:54 71-43-24.8 1.5Bromochloromethane ND ug/kg 1 09/08/10 05:54 74-97-54.8 1.6Bromodichloromethane ND ug/kg 1 09/08/10 05:54 75-27-44.8 1.8Bromoform ND ug/kg 1 09/08/10 05:54 75-25-24.8 2.2Bromomethane ND ug/kg 1 09/08/10 05:54 74-83-99.5 2.42-Butanone (MEK) ND ug/kg 1 09/08/10 05:54 78-93-395.5 2.8Carbon disulfide ND ug/kg 1 09/08/10 05:54 75-15-09.5 2.9Carbon tetrachloride ND ug/kg 1 09/08/10 05:54 56-23-54.8 2.5Chlorobenzene ND ug/kg 1 09/08/10 05:54 108-90-74.8 1.8Chloroethane ND ug/kg 1 09/08/10 05:54 75-00-39.5 2.3Chloroform ND ug/kg 1 09/08/10 05:54 67-66-34.8 1.5Chloromethane ND ug/kg 1 09/08/10 05:54 74-87-39.5 2.3Cyclohexane ND ug/kg 1 09/08/10 05:54 110-82-74.8 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/08/10 05:54 96-12-84.8 3.4Dibromochloromethane ND ug/kg 1 09/08/10 05:54 124-48-14.8 1.71,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 05:54 106-93-44.8 1.71,2-Dichlorobenzene ND ug/kg 1 09/08/10 05:54 95-50-14.8 1.81,3-Dichlorobenzene ND ug/kg 1 09/08/10 05:54 541-73-14.8 1.91,4-Dichlorobenzene ND ug/kg 1 09/08/10 05:54 106-46-74.8 1.6Dichlorodifluoromethane ND ug/kg 1 09/08/10 05:54 75-71-89.5 3.41,1-Dichloroethane ND ug/kg 1 09/08/10 05:54 75-34-34.8 1.41,2-Dichloroethane ND ug/kg 1 09/08/10 05:54 107-06-24.8 2.11,1-Dichloroethene ND ug/kg 1 09/08/10 05:54 75-35-44.8 1.7cis-1,2-Dichloroethene ND ug/kg 1 09/08/10 05:54 156-59-24.8 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 05:54 156-60-54.8 1.81,2-Dichloropropane ND ug/kg 1 09/08/10 05:54 78-87-54.8 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 05:54 10061-01-54.8 1.7trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 05:54 10061-02-64.8 1.4Ethylbenzene ND ug/kg 1 09/08/10 05:54 100-41-44.8 1.72-Hexanone ND ug/kg 1 09/08/10 05:54 591-78-647.7 3.7Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 05:54 98-82-84.8 1.8Methyl acetate ND ug/kg 1 09/08/10 05:54 79-20-99.5 1.3Methylcyclohexane ND ug/kg 1 09/08/10 05:54 108-87-29.5 1.4Methylene Chloride ND ug/kg 1 09/08/10 05:54 75-09-219.1 2.94-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 05:54 108-10-147.7 3.5Methyl-tert-butyl ether ND ug/kg 1 09/08/10 05:54 1634-04-44.8 1.4Styrene ND ug/kg 1 09/08/10 05:54 100-42-54.8 1.71,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 05:54 79-34-54.8 1.8Tetrachloroethene ND ug/kg 1 09/08/10 05:54 127-18-44.8 1.6Toluene ND ug/kg 1 09/08/10 05:54 108-88-34.8 1.71,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 05:54 87-61-64.8 2.11,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 05:54 120-82-14.8 1.51,1,1-Trichloroethane ND ug/kg 1 09/08/10 05:54 71-55-64.8 1.71,1,2-Trichloroethane ND ug/kg 1 09/08/10 05:54 79-00-54.8 2.0



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Trichloroethene 2.6J ug/kg 1 09/08/10 06:12 79-01-65.1 2.2Trichlorofluoromethane ND ug/kg 1 09/08/10 06:12 75-69-45.1 2.31,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/08/10 06:12 76-13-15.1 1.9Vinyl chloride ND ug/kg 1 09/08/10 06:12 75-01-410.3 1.8Xylene (Total) ND ug/kg 1 09/08/10 06:12 1330-20-710.3 3.7m&p-Xylene ND ug/kg 1 09/08/10 06:12 179601-23-110.3 3.7o-Xylene ND ug/kg 1 09/08/10 06:12 95-47-65.1 1.9Dibromofluoromethane (S) 101 % 1 09/08/10 06:12 1868-53-770-130Toluene-d8 (S) 100 % 1 09/08/10 06:12 2037-26-570-1304-Bromofluorobenzene (S) 98 % 1 09/08/10 06:12 460-00-470-1301,2-Dichloroethane-d4 (S) 103 % 1 09/08/10 06:12 17060-07-070-132





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Acetone 71.2J ug/kg 1 09/08/10 21:32 67-64-191.3 9.1Benzene ND ug/kg 1 09/08/10 21:32 71-43-24.6 1.5Bromochloromethane ND ug/kg 1 09/08/10 21:32 74-97-54.6 1.6Bromodichloromethane ND ug/kg 1 09/08/10 21:32 75-27-44.6 1.7Bromoform ND ug/kg 1 09/08/10 21:32 75-25-24.6 2.1Bromomethane ND ug/kg 1 09/08/10 21:32 74-83-99.1 2.32-Butanone (MEK) ND ug/kg 1 09/08/10 21:32 78-93-391.3 2.6Carbon disulfide ND ug/kg 1 09/08/10 21:32 75-15-09.1 2.7Carbon tetrachloride ND ug/kg 1 09/08/10 21:32 56-23-54.6 2.4Chlorobenzene ND ug/kg 1 09/08/10 21:32 108-90-74.6 1.7Chloroethane ND ug/kg 1 09/08/10 21:32 75-00-39.1 2.2Chloroform ND ug/kg 1 09/08/10 21:32 67-66-34.6 1.5Chloromethane ND ug/kg 1 09/08/10 21:32 74-87-39.1 2.2Cyclohexane ND ug/kg 1 09/08/10 21:32 110-82-74.6 1.51,2-Dibromo-3-chloropropane ND ug/kg 1 09/08/10 21:32 96-12-84.6 3.3Dibromochloromethane ND ug/kg 1 09/08/10 21:32 124-48-14.6 1.61,2-Dibromoethane (EDB) ND ug/kg 1 09/08/10 21:32 106-93-44.6 1.61,2-Dichlorobenzene ND ug/kg 1 09/08/10 21:32 95-50-14.6 1.71,3-Dichlorobenzene ND ug/kg 1 09/08/10 21:32 541-73-14.6 1.81,4-Dichlorobenzene ND ug/kg 1 09/08/10 21:32 106-46-74.6 1.6Dichlorodifluoromethane ND ug/kg 1 09/08/10 21:32 75-71-89.1 3.31,1-Dichloroethane ND ug/kg 1 09/08/10 21:32 75-34-34.6 1.41,2-Dichloroethane ND ug/kg 1 09/08/10 21:32 107-06-24.6 2.01,1-Dichloroethene ND ug/kg 1 09/08/10 21:32 75-35-44.6 1.6cis-1,2-Dichloroethene 2.1J ug/kg 1 09/08/10 21:32 156-59-24.6 1.3trans-1,2-Dichloroethene ND ug/kg 1 09/08/10 21:32 156-60-54.6 1.71,2-Dichloropropane ND ug/kg 1 09/08/10 21:32 78-87-54.6 1.6cis-1,3-Dichloropropene ND ug/kg 1 09/08/10 21:32 10061-01-54.6 1.6trans-1,3-Dichloropropene ND ug/kg 1 09/08/10 21:32 10061-02-64.6 1.4Ethylbenzene ND ug/kg 1 09/08/10 21:32 100-41-44.6 1.62-Hexanone ND ug/kg 1 09/08/10 21:32 591-78-645.7 3.6Isopropylbenzene (Cumene) ND ug/kg 1 09/08/10 21:32 98-82-84.6 1.7Methyl acetate 2.2J ug/kg 1 09/08/10 21:32 79-20-99.1 1.3Methylcyclohexane ND ug/kg 1 09/08/10 21:32 108-87-29.1 1.4Methylene Chloride ND ug/kg 1 09/08/10 21:32 75-09-218.3 2.74-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/08/10 21:32 108-10-145.7 3.4Methyl-tert-butyl ether ND ug/kg 1 09/08/10 21:32 1634-04-44.6 1.4Styrene ND ug/kg 1 09/08/10 21:32 100-42-54.6 1.61,1,2,2-Tetrachloroethane ND ug/kg 1 09/08/10 21:32 79-34-54.6 1.7Tetrachloroethene ND ug/kg 1 09/08/10 21:32 127-18-44.6 1.6Toluene ND ug/kg 1 09/08/10 21:32 108-88-34.6 1.61,2,3-Trichlorobenzene ND ug/kg 1 09/08/10 21:32 87-61-64.6 2.01,2,4-Trichlorobenzene ND ug/kg 1 09/08/10 21:32 120-82-14.6 1.51,1,1-Trichloroethane ND ug/kg 1 09/08/10 21:32 71-55-64.6 1.61,1,2-Trichloroethane ND ug/kg 1 09/08/10 21:32 79-00-54.6 1.9



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Trichloroethene 15.2 ug/kg 1 09/08/10 21:32 79-01-64.6 1.9Trichlorofluoromethane ND ug/kg 1 09/08/10 21:32 75-69-44.6 2.01,1,2-Trichlorotrifluoroethane ND ug/kg 1 09/08/10 21:32 76-13-14.6 1.7Vinyl chloride ND ug/kg 1 09/08/10 21:32 75-01-49.1 1.6Xylene (Total) ND ug/kg 1 09/08/10 21:32 1330-20-79.1 3.3m&p-Xylene ND ug/kg 1 09/08/10 21:32 179601-23-19.1 3.3o-Xylene ND ug/kg 1 09/08/10 21:32 95-47-64.6 1.7Dibromofluoromethane (S) 100 % 1 09/08/10 21:32 1868-53-770-130Toluene-d8 (S) 100 % 1 09/08/10 21:32 2037-26-570-1304-Bromofluorobenzene (S) 96 % 1 09/08/10 21:32 460-00-470-1301,2-Dichloroethane-d4 (S) 101 % 1 09/08/10 21:32 17060-07-070-132





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Acetone 81.3J ug/kg 1 09/09/10 03:59 67-64-188.6 8.9Benzene ND ug/kg 1 09/09/10 03:59 71-43-24.4 1.4Bromochloromethane ND ug/kg 1 09/09/10 03:59 74-97-54.4 1.5Bromodichloromethane ND ug/kg 1 09/09/10 03:59 75-27-44.4 1.7Bromoform ND ug/kg 1 09/09/10 03:59 75-25-24.4 2.0Bromomethane ND ug/kg 1 09/09/10 03:59 74-83-98.9 2.22-Butanone (MEK) 5.4J ug/kg 1 09/09/10 03:59 78-93-388.6 2.6Carbon disulfide ND ug/kg 1 09/09/10 03:59 75-15-08.9 2.7Carbon tetrachloride ND ug/kg 1 09/09/10 03:59 56-23-54.4 2.3Chlorobenzene ND ug/kg 1 09/09/10 03:59 108-90-74.4 1.7Chloroethane ND ug/kg 1 09/09/10 03:59 75-00-38.9 2.1Chloroform ND ug/kg 1 09/09/10 03:59 67-66-34.4 1.4Chloromethane ND ug/kg 1 09/09/10 03:59 74-87-38.9 2.1Cyclohexane ND ug/kg 1 09/09/10 03:59 110-82-74.4 1.41,2-Dibromo-3-chloropropane ND ug/kg 1 09/09/10 03:59 96-12-84.4 3.2Dibromochloromethane ND ug/kg 1 09/09/10 03:59 124-48-14.4 1.61,2-Dibromoethane (EDB) ND ug/kg 1 09/09/10 03:59 106-93-44.4 1.61,2-Dichlorobenzene ND ug/kg 1 09/09/10 03:59 95-50-14.4 1.71,3-Dichlorobenzene ND ug/kg 1 09/09/10 03:59 541-73-14.4 1.81,4-Dichlorobenzene ND ug/kg 1 09/09/10 03:59 106-46-74.4 1.5Dichlorodifluoromethane ND ug/kg 1 09/09/10 03:59 75-71-88.9 3.21,1-Dichloroethane ND ug/kg 1 09/09/10 03:59 75-34-34.4 1.31,2-Dichloroethane ND ug/kg 1 09/09/10 03:59 107-06-24.4 1.91,1-Dichloroethene ND ug/kg 1 09/09/10 03:59 75-35-44.4 1.6cis-1,2-Dichloroethene 2.4J ug/kg 1 09/09/10 03:59 156-59-24.4 1.2trans-1,2-Dichloroethene ND ug/kg 1 09/09/10 03:59 156-60-54.4 1.71,2-Dichloropropane ND ug/kg 1 09/09/10 03:59 78-87-54.4 1.5cis-1,3-Dichloropropene ND ug/kg 1 09/09/10 03:59 10061-01-54.4 1.6trans-1,3-Dichloropropene ND ug/kg 1 09/09/10 03:59 10061-02-64.4 1.3Ethylbenzene ND ug/kg 1 09/09/10 03:59 100-41-44.4 1.62-Hexanone ND ug/kg 1 09/09/10 03:59 591-78-644.3 3.5Isopropylbenzene (Cumene) ND ug/kg 1 09/09/10 03:59 98-82-84.4 1.7Methyl acetate 3.8J ug/kg 1 09/09/10 03:59 79-20-98.9 1.2Methylcyclohexane ND ug/kg 1 09/09/10 03:59 108-87-28.9 1.3Methylene Chloride ND ug/kg 1 09/09/10 03:59 75-09-217.7 2.74-Methyl-2-pentanone (MIBK) ND ug/kg 1 09/09/10 03:59 108-10-144.3 3.3Methyl-tert-butyl ether ND ug/kg 1 09/09/10 03:59 1634-04-44.4 1.3Styrene ND ug/kg 1 09/09/10 03:59 100-42-54.4 1.61,1,2,2-Tetrachloroethane ND ug/kg 1 09/09/10 03:59 79-34-54.4 1.7Tetrachloroethene ND ug/kg 1 09/09/10 03:59 127-18-44.4 1.5Toluene ND ug/kg 1 09/09/10 03:59 108-88-34.4 1.61,2,3-Trichlorobenzene ND ug/kg 1 09/09/10 03:59 87-61-64.4 1.91,2,4-Trichlorobenzene ND ug/kg 1 09/09/10 03:59 120-82-14.4 1.41,1,1-Trichloroethane ND ug/kg 1 09/09/10 03:59 71-55-64.4 1.61,1,2-Trichloroethane ND ug/kg 1 09/09/10 03:59 79-00-54.4 1.9



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9276872MILLS GAP 6686081744

Sample: EB-02 Lab ID: 9276872093 Collected: 09/01/10 17:15 Received: 09/03/10 08:00 Matrix: Water


6010 MET ICP, 3030C Analytical Method: EPA 6010 Preparation Method: SM 3030C

Antimony ND ug/L 1 09/10/10 19:51 7440-36-009/04/10 09:005.0 2.6Arsenic 5.4 ug/L 1 09/10/10 19:51 7440-38-209/04/10 09:005.0 2.7Beryllium ND ug/L 1 09/10/10 19:51 7440-41-709/04/10 09:001.0 0.10Cadmium ND ug/L 1 09/10/10 19:51 7440-43-909/04/10 09:001.0 0.50Chromium 0.53J ug/L 1 09/10/10 19:51 7440-47-309/04/10 09:005.0 0.40Copper ND ug/L 1 09/10/10 19:51 7440-50-809/04/10 09:005.0 0.30Lead ND ug/L 1 09/10/10 19:51 7439-92-109/04/10 09:005.0 4.0Manganese ND ug/L 1 09/10/10 19:51 7439-96-509/04/10 09:005.0 0.30Nickel ND ug/L 1 09/10/10 19:51 7440-02-009/04/10 09:005.0 1.7Selenium 11.9 ug/L 1 09/10/10 19:51 7782-49-209/04/10 09:0010.0 3.8Silver ND ug/L 1 09/10/10 19:51 7440-22-409/04/10 09:005.0 0.10Thallium ND ug/L 1 09/13/10 15:12 7440-28-009/04/10 09:0010.0 3.0Zinc 1.9J ug/L 1 09/10/10 19:51 7440-66-609/04/10 09:0010.0 0.40


Mercury 0.11J ug/L 1 09/16/10 14:17 7439-97-6 B09/15/10 15:370.20 0.070

8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510

Acenaphthene ND ug/L 1 09/25/10 02:40 83-32-909/08/10 14:3010.0 1.9Acenaphthylene ND ug/L 1 09/25/10 02:40 208-96-809/08/10 14:3010.0 3.2Acetophenone ND ug/L 1 09/25/10 02:40 98-86-209/08/10 14:3010.0 3.7Anthracene ND ug/L 1 09/25/10 02:40 120-12-709/08/10 14:3010.0 2.5Atrazine ND ug/L 1 09/25/10 02:40 1912-24-909/08/10 14:3020.0 6.5Benzaldehyde ND ug/L 1 09/25/10 02:40 100-52-709/08/10 14:3020.0 12.0Benzo(a)anthracene ND ug/L 1 09/25/10 02:40 56-55-309/08/10 14:3010.0 2.3Benzo(a)pyrene ND ug/L 1 09/25/10 02:40 50-32-809/08/10 14:3010.0 2.0Benzo(b)fluoranthene ND ug/L 1 09/25/10 02:40 205-99-209/08/10 14:3010.0 1.8Benzo(g,h,i)perylene 4.1J ug/L 1 09/25/10 02:40 191-24-209/08/10 14:3010.0 2.6Benzo(k)fluoranthene ND ug/L 1 09/25/10 02:40 207-08-909/08/10 14:3010.0 2.0Biphenyl (Diphenyl) ND ug/L 1 09/25/10 02:40 92-52-409/08/10 14:3010.0 3.24-Bromophenylphenyl ether ND ug/L 1 09/25/10 02:40 101-55-309/08/10 14:3010.0 3.1Butylbenzylphthalate ND ug/L 1 09/25/10 02:40 85-68-709/08/10 14:3010.0 2.0Caprolactam ND ug/L 1 09/25/10 02:40 105-60-209/08/10 14:3010.0 2.1Carbazole ND ug/L 1 09/25/10 02:40 86-74-809/08/10 14:3010.0 2.44-Chloro-3-methylphenol ND ug/L 1 09/25/10 02:40 59-50-709/08/10 14:3020.0 8.14-Chloroaniline ND ug/L 1 09/25/10 02:40 106-47-809/08/10 14:3020.0 17.0bis(2-Chloroethoxy)methane ND ug/L 1 09/25/10 02:40 111-91-109/08/10 14:3010.0 3.2bis(2-Chloroethyl) ether ND ug/L 1 09/25/10 02:40 111-44-409/08/10 14:3010.0 3.5bis(2-Chloroisopropyl) ether ND ug/L 1 09/25/10 02:40 108-60-109/08/10 14:3010.0 2.92-Chloronaphthalene ND ug/L 1 09/25/10 02:40 91-58-709/08/10 14:3010.0 3.62-Chlorophenol ND ug/L 1 09/25/10 02:40 95-57-809/08/10 14:3010.0 3.54-Chlorophenylphenyl ether ND ug/L 1 09/25/10 02:40 7005-72-309/08/10 14:3010.0 3.5Chrysene ND ug/L 1 09/25/10 02:40 218-01-909/08/10 14:3010.0 2.3Dibenz(a,h)anthracene 3.7J ug/L 1 09/25/10 02:40 53-70-309/08/10 14:3010.0 2.8Dibenzofuran ND ug/L 1 09/25/10 02:40 132-64-909/08/10 14:3010.0 3.33,3'-Dichlorobenzidine ND ug/L 1 09/25/10 02:40 91-94-109/08/10 14:3020.0 9.5



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8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510

2,4-Dichlorophenol ND ug/L 1 09/25/10 02:40 120-83-209/08/10 14:3010.0 4.4Diethylphthalate ND ug/L 1 09/25/10 02:40 84-66-209/08/10 14:3010.0 2.72,4-Dimethylphenol ND ug/L 1 09/25/10 02:40 105-67-909/08/10 14:3010.0 9.0Dimethylphthalate ND ug/L 1 09/25/10 02:40 131-11-309/08/10 14:3010.0 2.3Di-n-butylphthalate ND ug/L 1 09/25/10 02:40 84-74-209/08/10 14:3010.0 2.04,6-Dinitro-2-methylphenol ND ug/L 1 09/25/10 02:40 534-52-109/08/10 14:3020.0 3.82,4-Dinitrophenol ND ug/L 1 09/25/10 02:40 51-28-509/08/10 14:3050.0 8.82,4-Dinitrotoluene ND ug/L 1 09/25/10 02:40 121-14-209/08/10 14:3010.0 2.52,6-Dinitrotoluene ND ug/L 1 09/25/10 02:40 606-20-209/08/10 14:3010.0 2.5Di-n-octylphthalate ND ug/L 1 09/25/10 02:40 117-84-009/08/10 14:3010.0 1.5bis(2-Ethylhexyl)phthalate ND ug/L 1 09/25/10 02:40 117-81-709/08/10 14:306.0 2.2Fluoranthene ND ug/L 1 09/25/10 02:40 206-44-009/08/10 14:3010.0 2.4Fluorene ND ug/L 1 09/25/10 02:40 86-73-709/08/10 14:3010.0 3.1Hexachloro-1,3-butadiene ND ug/L 1 09/25/10 02:40 87-68-309/08/10 14:3010.0 2.9Hexachlorobenzene ND ug/L 1 09/25/10 02:40 118-74-109/08/10 14:3010.0 3.2Hexachlorocyclopentadiene ND ug/L 1 09/25/10 02:40 77-47-409/08/10 14:3010.0 2.3Hexachloroethane ND ug/L 1 09/25/10 02:40 67-72-109/08/10 14:3010.0 2.7Indeno(1,2,3-cd)pyrene 3.5J ug/L 1 09/25/10 02:40 193-39-509/08/10 14:3010.0 2.7Isophorone ND ug/L 1 09/25/10 02:40 78-59-109/08/10 14:3010.0 3.32-Methylnaphthalene ND ug/L 1 09/25/10 02:40 91-57-609/08/10 14:3010.0 4.22-Methylphenol(o-Cresol) ND ug/L 1 09/25/10 02:40 95-48-709/08/10 14:3010.0 3.63&4-Methylphenol(m&p Cresol) ND ug/L 1 09/25/10 02:4009/08/10 14:3010.0 3.3Naphthalene ND ug/L 1 09/25/10 02:40 91-20-309/08/10 14:3010.0 4.02-Nitroaniline ND ug/L 1 09/25/10 02:40 88-74-409/08/10 14:3050.0 13.03-Nitroaniline ND ug/L 1 09/25/10 02:40 99-09-209/08/10 14:3050.0 13.04-Nitroaniline ND ug/L 1 09/25/10 02:40 100-01-609/08/10 14:3020.0 14.0Nitrobenzene ND ug/L 1 09/25/10 02:40 98-95-309/08/10 14:3010.0 3.52-Nitrophenol ND ug/L 1 09/25/10 02:40 88-75-509/08/10 14:3010.0 3.44-Nitrophenol ND ug/L 1 09/25/10 02:40 100-02-709/08/10 14:3050.0 4.9N-Nitroso-di-n-propylamine ND ug/L 1 09/25/10 02:40 621-64-709/08/10 14:3010.0 3.7N-Nitrosodiphenylamine ND ug/L 1 09/25/10 02:40 86-30-609/08/10 14:3010.0 3.0Pentachlorophenol ND ug/L 1 09/25/10 02:40 87-86-509/08/10 14:3025.0 18.0Phenanthrene ND ug/L 1 09/25/10 02:40 85-01-809/08/10 14:3010.0 2.5Phenol ND ug/L 1 09/25/10 02:40 108-95-209/08/10 14:3010.0 1.6Pyrene ND ug/L 1 09/25/10 02:40 129-00-009/08/10 14:3010.0 2.11,2,4,5-Tetrachlorobenzene ND ug/L 1 09/25/10 02:40 95-94-309/08/10 14:3010.0 4.02,3,4,6-Tetrachlorophenol ND ug/L 1 09/25/10 02:40 58-90-209/08/10 14:3010.0 1.62,4,5-Trichlorophenol ND ug/L 1 09/25/10 02:40 95-95-409/08/10 14:3010.0 2.12,4,6-Trichlorophenol ND ug/L 1 09/25/10 02:40 88-06-209/08/10 14:3010.0 1.8Nitrobenzene-d5 (S) 33 % 1 09/25/10 02:40 4165-60-009/08/10 14:3021-1102-Fluorobiphenyl (S) 41 % 1 09/25/10 02:40 321-60-809/08/10 14:3027-110Terphenyl-d14 (S) 50 % 1 09/25/10 02:40 1718-51-009/08/10 14:3031-107Phenol-d6 (S) 10 % 1 09/25/10 02:40 13127-88-309/08/10 14:3010-1102-Fluorophenol (S) 17 % 1 09/25/10 02:40 367-12-409/08/10 14:3012-1102,4,6-Tribromophenol (S) 48 % 1 09/25/10 02:40 118-79-609/08/10 14:3027-110



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ANALYTICAL RESULTS


9276872MILLS GAP 6686081744



8260 MSV Low Level Analytical Method: EPA 8260

Acetone 6.3J ug/L 1 09/08/10 01:29 67-64-125.0 2.2Benzene ND ug/L 1 09/08/10 01:29 71-43-21.0 0.25Bromochloromethane ND ug/L 1 09/08/10 01:29 74-97-51.0 0.17Bromodichloromethane ND ug/L 1 09/08/10 01:29 75-27-41.0 0.18Bromoform ND ug/L 1 09/08/10 01:29 75-25-21.0 0.26Bromomethane ND ug/L 1 09/08/10 01:29 74-83-92.0 0.292-Butanone (MEK) ND ug/L 1 09/08/10 01:29 78-93-35.0 0.96Carbon disulfide ND ug/L 1 09/08/10 01:29 75-15-02.0 1.2Carbon tetrachloride ND ug/L 1 09/08/10 01:29 56-23-51.0 0.25Chlorobenzene ND ug/L 1 09/08/10 01:29 108-90-71.0 0.23Chloroethane ND ug/L 1 09/08/10 01:29 75-00-31.0 0.54Chloroform ND ug/L 1 09/08/10 01:29 67-66-31.0 0.14Chloromethane ND ug/L 1 09/08/10 01:29 74-87-31.0 0.11Cyclohexane ND ug/L 1 09/08/10 01:29 110-82-71.0 0.361,2-Dibromo-3-chloropropane ND ug/L 1 09/08/10 01:29 96-12-85.0 2.5Dibromochloromethane ND ug/L 1 09/08/10 01:29 124-48-11.0 0.211,2-Dibromoethane (EDB) ND ug/L 1 09/08/10 01:29 106-93-41.0 0.271,2-Dichlorobenzene ND ug/L 1 09/08/10 01:29 95-50-11.0 0.301,3-Dichlorobenzene ND ug/L 1 09/08/10 01:29 541-73-11.0 0.241,4-Dichlorobenzene ND ug/L 1 09/08/10 01:29 106-46-71.0 0.33Dichlorodifluoromethane ND ug/L 1 09/08/10 01:29 75-71-81.0 0.211,1-Dichloroethane ND ug/L 1 09/08/10 01:29 75-34-31.0 0.321,2-Dichloroethane ND ug/L 1 09/08/10 01:29 107-06-21.0 0.121,1-Dichloroethene ND ug/L 1 09/08/10 01:29 75-35-41.0 0.56cis-1,2-Dichloroethene ND ug/L 1 09/08/10 01:29 156-59-21.0 0.19trans-1,2-Dichloroethene ND ug/L 1 09/08/10 01:29 156-60-51.0 0.491,2-Dichloropropane ND ug/L 1 09/08/10 01:29 78-87-51.0 0.27cis-1,3-Dichloropropene ND ug/L 1 09/08/10 01:29 10061-01-51.0 0.13trans-1,3-Dichloropropene ND ug/L 1 09/08/10 01:29 10061-02-61.0 0.26Ethylbenzene ND ug/L 1 09/08/10 01:29 100-41-41.0 0.302-Hexanone ND ug/L 1 09/08/10 01:29 591-78-65.0 0.46Isopropylbenzene (Cumene) ND ug/L 1 09/08/10 01:29 98-82-81.0 0.40Methyl acetate ND ug/L 1 09/08/10 01:29 79-20-910.0 0.82Methylcyclohexane ND ug/L 1 09/08/10 01:29 108-87-210.0 1.9Methylene Chloride ND ug/L 1 09/08/10 01:29 75-09-22.0 0.974-Methyl-2-pentanone (MIBK) ND ug/L 1 09/08/10 01:29 108-10-15.0 0.33Methyl-tert-butyl ether ND ug/L 1 09/08/10 01:29 1634-04-41.0 0.21Styrene ND ug/L 1 09/08/10 01:29 100-42-51.0 0.261,1,2,2-Tetrachloroethane ND ug/L 1 09/08/10 01:29 79-34-51.0 0.40Tetrachloroethene ND ug/L 1 09/08/10 01:29 127-18-41.0 0.46Toluene ND ug/L 1 09/08/10 01:29 108-88-31.0 0.261,2,3-Trichlorobenzene ND ug/L 1 09/08/10 01:29 87-61-61.0 0.331,2,4-Trichlorobenzene ND ug/L 1 09/08/10 01:29 120-82-11.0 0.351,1,1-Trichloroethane ND ug/L 1 09/08/10 01:29 71-55-61.0 0.481,1,2-Trichloroethane ND ug/L 1 09/08/10 01:29 79-00-51.0 0.29Trichloroethene ND ug/L 1 09/08/10 01:29 79-01-61.0 0.47



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Trichlorofluoromethane ND ug/L 1 09/08/10 01:29 75-69-41.0 0.201,1,2-Trichlorotrifluoroethane ND ug/L 1 09/08/10 01:29 76-13-11.0 0.19Vinyl chloride ND ug/L 1 09/08/10 01:29 75-01-41.0 0.62Xylene (Total) ND ug/L 1 09/08/10 01:29 1330-20-72.0 0.66m&p-Xylene ND ug/L 1 09/08/10 01:29 179601-23-12.0 0.66o-Xylene ND ug/L 1 09/08/10 01:29 95-47-61.0 0.234-Bromofluorobenzene (S) 101 % 1 09/08/10 01:29 460-00-470-130Dibromofluoromethane (S) 110 % 1 09/08/10 01:29 1868-53-770-1301,2-Dichloroethane-d4 (S) 116 % 1 09/08/10 01:29 17060-07-070-130Toluene-d8 (S) 97 % 1 09/08/10 01:29 2037-26-570-130


Cyanide ND mg/L 1 09/05/10 14:26 57-12-50.0050 0.0050



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ANALYTICAL RESULTS


9276872MILLS GAP 6686081744

Sample: TB-05 Lab ID: 9276872095 Collected: 09/01/10 00:00 Received: 09/03/10 08:00 Matrix: Water



Acetone ND ug/L 1 09/08/10 01:54 67-64-125.0 2.2Benzene ND ug/L 1 09/08/10 01:54 71-43-21.0 0.25Bromochloromethane ND ug/L 1 09/08/10 01:54 74-97-51.0 0.17Bromodichloromethane ND ug/L 1 09/08/10 01:54 75-27-41.0 0.18Bromoform ND ug/L 1 09/08/10 01:54 75-25-21.0 0.26Bromomethane ND ug/L 1 09/08/10 01:54 74-83-92.0 0.292-Butanone (MEK) ND ug/L 1 09/08/10 01:54 78-93-35.0 0.96Carbon disulfide ND ug/L 1 09/08/10 01:54 75-15-02.0 1.2Carbon tetrachloride ND ug/L 1 09/08/10 01:54 56-23-51.0 0.25Chlorobenzene ND ug/L 1 09/08/10 01:54 108-90-71.0 0.23Chloroethane ND ug/L 1 09/08/10 01:54 75-00-31.0 0.54Chloroform ND ug/L 1 09/08/10 01:54 67-66-31.0 0.14Chloromethane ND ug/L 1 09/08/10 01:54 74-87-31.0 0.11Cyclohexane ND ug/L 1 09/08/10 01:54 110-82-71.0 0.361,2-Dibromo-3-chloropropane ND ug/L 1 09/08/10 01:54 96-12-85.0 2.5Dibromochloromethane ND ug/L 1 09/08/10 01:54 124-48-11.0 0.211,2-Dibromoethane (EDB) ND ug/L 1 09/08/10 01:54 106-93-41.0 0.271,2-Dichlorobenzene ND ug/L 1 09/08/10 01:54 95-50-11.0 0.301,3-Dichlorobenzene ND ug/L 1 09/08/10 01:54 541-73-11.0 0.241,4-Dichlorobenzene ND ug/L 1 09/08/10 01:54 106-46-71.0 0.33Dichlorodifluoromethane ND ug/L 1 09/08/10 01:54 75-71-81.0 0.211,1-Dichloroethane ND ug/L 1 09/08/10 01:54 75-34-31.0 0.321,2-Dichloroethane ND ug/L 1 09/08/10 01:54 107-06-21.0 0.121,1-Dichloroethene ND ug/L 1 09/08/10 01:54 75-35-41.0 0.56cis-1,2-Dichloroethene ND ug/L 1 09/08/10 01:54 156-59-21.0 0.19trans-1,2-Dichloroethene ND ug/L 1 09/08/10 01:54 156-60-51.0 0.491,2-Dichloropropane ND ug/L 1 09/08/10 01:54 78-87-51.0 0.27cis-1,3-Dichloropropene ND ug/L 1 09/08/10 01:54 10061-01-51.0 0.13trans-1,3-Dichloropropene ND ug/L 1 09/08/10 01:54 10061-02-61.0 0.26Ethylbenzene ND ug/L 1 09/08/10 01:54 100-41-41.0 0.302-Hexanone ND ug/L 1 09/08/10 01:54 591-78-65.0 0.46Isopropylbenzene (Cumene) ND ug/L 1 09/08/10 01:54 98-82-81.0 0.40Methyl acetate ND ug/L 1 09/08/10 01:54 79-20-910.0 0.82Methylcyclohexane ND ug/L 1 09/08/10 01:54 108-87-210.0 1.9Methylene Chloride 1.9J ug/L 1 09/08/10 01:54 75-09-22.0 0.974-Methyl-2-pentanone (MIBK) ND ug/L 1 09/08/10 01:54 108-10-15.0 0.33Methyl-tert-butyl ether ND ug/L 1 09/08/10 01:54 1634-04-41.0 0.21Styrene ND ug/L 1 09/08/10 01:54 100-42-51.0 0.261,1,2,2-Tetrachloroethane ND ug/L 1 09/08/10 01:54 79-34-51.0 0.40Tetrachloroethene ND ug/L 1 09/08/10 01:54 127-18-41.0 0.46Toluene ND ug/L 1 09/08/10 01:54 108-88-31.0 0.261,2,3-Trichlorobenzene ND ug/L 1 09/08/10 01:54 87-61-61.0 0.331,2,4-Trichlorobenzene ND ug/L 1 09/08/10 01:54 120-82-11.0 0.351,1,1-Trichloroethane ND ug/L 1 09/08/10 01:54 71-55-61.0 0.481,1,2-Trichloroethane ND ug/L 1 09/08/10 01:54 79-00-51.0 0.29Trichloroethene ND ug/L 1 09/08/10 01:54 79-01-61.0 0.47



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Sample: TB-05 Lab ID: 9276872095 Collected: 09/01/10 00:00 Received: 09/03/10 08:00 Matrix: Water



Trichlorofluoromethane ND ug/L 1 09/08/10 01:54 75-69-41.0 0.201,1,2-Trichlorotrifluoroethane ND ug/L 1 09/08/10 01:54 76-13-11.0 0.19Vinyl chloride ND ug/L 1 09/08/10 01:54 75-01-41.0 0.62Xylene (Total) ND ug/L 1 09/08/10 01:54 1330-20-72.0 0.66m&p-Xylene ND ug/L 1 09/08/10 01:54 179601-23-12.0 0.66o-Xylene ND ug/L 1 09/08/10 01:54 95-47-61.0 0.234-Bromofluorobenzene (S) 102 % 1 09/08/10 01:54 460-00-470-130Dibromofluoromethane (S) 110 % 1 09/08/10 01:54 1868-53-770-1301,2-Dichloroethane-d4 (S) 115 % 1 09/08/10 01:54 17060-07-070-130Toluene-d8 (S) 98 % 1 09/08/10 01:54 2037-26-570-130



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9276872MILLS GAP 6686081744



MPRP/7031EPA 3050

EPA 60106010 MET

Associated Lab Samples: 9276872001, 9276872002, 9276872003, 9276872004, 9276872005, 9276872006, 9276872008, 9276872009,9276872012, 9276872014, 9276872015, 9276872016, 9276872017, 9276872018, 9276872019, 9276872020,9276872021, 9276872022, 9276872023, 9276872024





Matrix: Solid

Analyzed

Antimony mg/kg ND 0.50 09/16/10 05:23Arsenic mg/kg ND 0.50 09/16/10 05:23Beryllium mg/kg ND 0.10 09/16/10 05:23Cadmium mg/kg ND 0.10 09/16/10 05:23Chromium mg/kg 0.15J 0.50 09/16/10 05:23Copper mg/kg ND 0.50 09/16/10 05:23Lead mg/kg ND 0.50 09/16/10 05:23Manganese mg/kg 0.16J 0.50 09/16/10 05:23Nickel mg/kg ND 0.50 09/16/10 05:23Selenium mg/kg ND 1.0 09/16/10 05:23Silver mg/kg ND 0.50 09/16/10 05:23Thallium mg/kg ND 1.0 09/16/10 05:23Zinc mg/kg 0.40J 1.0 09/16/10 05:23

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9276872009

494456

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Antimony mg/kg M0,R144.3 38 75-12542 30 2053.6ND 16.7 22.7



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Parameter UnitsMS



MSSpikeResult

9276872009

494456

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg M0,R144.3 50 75-12555 28 2053.61.8J 23.7 31.5Beryllium mg/kg R144.3 84 75-12587 23 2053.60.86 37.9 47.7Cadmium mg/kg R144.3 82 75-12585 23 2053.6ND 36.2 45.7Chromium mg/kg 44.3 81 75-12586 17 2053.616.8 52.7 62.7Copper mg/kg R144.3 80 75-12583 21 2053.62.5 38.1 46.9Lead mg/kg R144.3 81 75-12585 21 2053.66.4 42.3 52.0Manganese mg/kg M044.3 135 75-125116 1 2053.6269 329 331Nickel mg/kg 44.3 85 75-12589 19 2053.612.2 49.6 60.1Selenium mg/kg M0,R144.3 53 75-12562 32 2053.6ND 25.0 34.6Silver mg/kg R122.1 76 75-12580 23 2026.8ND 16.9 21.4Thallium mg/kg M0,R144.3 73 75-12580 27 2053.6ND 33.5 44.1Zinc mg/kg 44.3 79 75-12595 13 2053.678.9 114 130



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9276872MILLS GAP 6686081744



MPRP/7040EPA 3050

EPA 60106010 MET

Associated Lab Samples: 9276872025, 9276872028, 9276872030, 9276872032, 9276872034, 9276872035, 9276872036, 9276872037,9276872038, 9276872039, 9276872041, 9276872043, 9276872045, 9276872049, 9276872050, 9276872051,9276872052, 9276872053, 9276872055





Matrix: Solid

Analyzed

Antimony mg/kg ND 0.50 09/16/10 02:58Arsenic mg/kg ND 0.50 09/16/10 02:58Beryllium mg/kg ND 0.10 09/16/10 02:58Cadmium mg/kg ND 0.10 09/16/10 02:58Chromium mg/kg 0.038J 0.50 09/16/10 02:58Copper mg/kg 0.20J 0.50 09/16/10 12:18Lead mg/kg ND 0.50 09/16/10 02:58Manganese mg/kg 0.089J 0.50 09/16/10 02:58Nickel mg/kg ND 0.50 09/16/10 02:58Selenium mg/kg ND 1.0 09/16/10 02:58Silver mg/kg ND 0.50 09/16/10 02:58Thallium mg/kg ND 1.0 09/16/10 02:58Zinc mg/kg ND 1.0 09/16/10 02:58

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9276872025

495086

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Antimony mg/kg M056.6 41 75-12539 14 2051.5ND 23.3 20.4



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Parameter UnitsMS



MSSpikeResult

9276872025

495086

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Arsenic mg/kg M056.6 69 75-12562 20 2051.5ND 39.4 32.4Beryllium mg/kg 56.6 95 75-12594 10 2051.50.91 54.5 49.5Cadmium mg/kg 56.6 93 75-12591 11 2051.5ND 52.7 47.1Chromium mg/kg M0,R156.6 88 75-125129 22 2051.518.1 68.0 84.6Copper mg/kg 56.6 93 75-12596 5 2051.510.5 62.9 59.8Lead mg/kg 56.6 90 75-12593 5 2051.510.9 61.7 58.8Manganese mg/kg M056.6 68 75-125154 12 2051.5290 328 369Nickel mg/kg 56.6 95 75-12595 8 2051.58.7 62.3 57.8Selenium mg/kg M056.6 67 75-12571 3 2051.5ND 37.8 36.6Silver mg/kg 28.3 91 75-12592 8 2025.81.3J 27.0 24.9Thallium mg/kg 56.6 88 75-12589 8 2051.5ND 49.8 46.2Zinc mg/kg 56.6 96 75-125109 2 2051.540.8 95.1 97.0



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MPRP/7046EPA 3050

EPA 60106010 MET






Matrix: Solid

Analyzed

Antimony mg/kg ND 0.50 09/14/10 14:49Arsenic mg/kg ND 0.50 09/14/10 14:49Beryllium mg/kg ND 0.10 09/14/10 14:49Cadmium mg/kg ND 0.10 09/14/10 14:49Chromium mg/kg 0.10J 0.50 09/14/10 14:49Copper mg/kg 0.058J 0.50 09/14/10 14:49Lead mg/kg ND 0.50 09/14/10 14:49Manganese mg/kg 0.16J 0.50 09/14/10 14:49Nickel mg/kg ND 0.50 09/14/10 14:49Selenium mg/kg ND 1.0 09/14/10 14:49Silver mg/kg ND 0.50 09/14/10 14:49Thallium mg/kg ND 1.0 09/14/10 14:49Zinc mg/kg ND 1.0 09/14/10 14:49

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9276872046

495774

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Antimony mg/kg M056.7 45 75-12544 12 2051.7ND 26.7 23.6Arsenic mg/kg M056.7 68 75-12567 10 2051.72.9J 41.3 37.5Beryllium mg/kg 56.7 93 75-12590 12 2051.71.8 54.5 48.3Cadmium mg/kg 56.7 83 75-12580 13 2051.7ND 47.0 41.3Chromium mg/kg 56.7 89 75-12587 7 2051.723.6 73.8 68.8



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Parameter UnitsMS



MSSpikeResult

9276872046

495774

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Copper mg/kg 56.7 92 75-12590 10 2051.77.0 59.3 53.4Lead mg/kg 56.7 85 75-12589 4 2051.74.1 52.5 50.4Manganese mg/kg M0,R156.7 517 75-1251431 44 2051.7509 803 1250Nickel mg/kg 56.7 87 75-12589 6 2051.716.0 65.5 61.8Selenium mg/kg M056.7 76 75-12574 11 2051.73.5J 46.4 41.8Silver mg/kg 28.4 82 75-12579 13 2025.8ND 23.3 20.5Thallium mg/kg M056.7 58 75-12558 6 2051.717.5 50.5 47.4Zinc mg/kg 56.7 99 75-12598 4 2051.788.0 144 139



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MPRP/7016SM 3030C

EPA 60106010 MET 3030C






Matrix: Water

Analyzed

Antimony ug/L ND 5.0 09/10/10 19:34Arsenic ug/L ND 5.0 09/10/10 19:34Beryllium ug/L ND 1.0 09/10/10 19:34Cadmium ug/L ND 1.0 09/10/10 19:34Chromium ug/L ND 5.0 09/10/10 19:34Copper ug/L ND 5.0 09/10/10 19:34Lead ug/L ND 5.0 09/10/10 19:34Manganese ug/L ND 5.0 09/10/10 19:34Nickel ug/L ND 5.0 09/10/10 19:34Selenium ug/L ND 10.0 09/10/10 19:34Silver ug/L ND 5.0 09/10/10 19:34Thallium ug/L ND 10.0 09/10/10 19:34Zinc ug/L ND 10.0 09/10/10 19:34

Parameter UnitsLCS



Antimony ug/L 529500 106 80-120Arsenic ug/L 546500 109 80-120Beryllium ug/L 554500 111 80-120Cadmium ug/L 530500 106 80-120Chromium ug/L 499500 100 80-120Copper ug/L 514500 103 80-120Lead ug/L 522500 104 80-120Manganese ug/L 501500 100 80-120Nickel ug/L 514500 103 80-120Selenium ug/L 523500 105 80-120Silver ug/L 247250 99 80-120Thallium ug/L 462500 92 80-120Zinc ug/L 577500 115 80-120

Parameter UnitsMS



Result9276872093

Antimony ug/L 522500 104 75-125NDArsenic ug/L 530500 105 75-1255.4Beryllium ug/L 544500 109 75-125NDCadmium ug/L 523500 105 75-125NDChromium ug/L 494500 99 75-1250.53JCopper ug/L 509500 102 75-125ND



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Parameter UnitsMS



Result9276872093

Lead ug/L 515500 103 75-125NDManganese ug/L 495500 99 75-125NDNickel ug/L 506500 101 75-125NDSelenium ug/L 606500 119 75-12511.9Silver ug/L 246250 98 75-125NDThallium ug/L 366 M0500 73 75-125NDZinc ug/L 560500 112 75-1251.9J

Parameter UnitsDup



Antimony ug/L ND 20NDArsenic ug/L 5.5 10 206.1Beryllium ug/L ND 20NDCadmium ug/L ND 20NDChromium ug/L ND 20NDCopper ug/L ND 20NDLead ug/L ND 20NDManganese ug/L 17.8 1 2017.9Nickel ug/L ND 20NDSelenium ug/L ND 20NDSilver ug/L 0.10J 20NDThallium ug/L 9.1J 2028.0Zinc ug/L ND 20ND



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MERP/3015EPA 7470







Matrix: Water

Analyzed

Mercury ug/L 0.13J 0.20 09/16/10 13:45

Parameter UnitsLCS



Mercury ug/L 2.62.5 106 80-120

Parameter UnitsMS



MSSpikeResult

9276650031

497300

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L M12.5 68 75-12568 0 252.5ND 1.8 1.8

Parameter UnitsMS



MSSpikeResult

9276650042

497302

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury ug/L M12.5 74 75-12573 1 252.5ND 1.9 1.9



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MERP/3004EPA 7471







Matrix: Solid

Analyzed

Mercury mg/kg ND 0.0050 09/10/10 11:28

Parameter UnitsLCS



Mercury mg/kg 0.062.067 93 80-120

Parameter UnitsMS



MSSpikeResult

9276750026

494572

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .058 85 75-12595 10 20.060.018 0.067 0.074

Parameter UnitsMS



MSSpikeResult

9276872001

494718

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M1.069 58 75-12549 9 20.0670.041 0.080 0.074



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MERP/3006EPA 7471


Associated Lab Samples: 9276872005, 9276872006





Matrix: Solid

Analyzed

Mercury mg/kg 0.0023J 0.0050 09/13/10 11:11

Parameter UnitsLCS



Mercury mg/kg 0.067.067 100 80-120

Parameter UnitsMS



MSSpikeResult

9276916001

495890

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M6.07 17966 75-125-12891 19 20.06105 117 97.0

Parameter UnitsMS



MSSpikeResult

9276916011

495892

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M6.048 -12667 75-125-35167 9 20.046124 118 108



Date: 09/27/2010 06:48 PM Page 289 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MERP/3010EPA 7471







Matrix: Solid

Analyzed

Mercury mg/kg ND 0.0050 09/15/10 11:54

Parameter UnitsLCS



Mercury mg/kg 0.068.067 102 80-120

Parameter UnitsMS



MSSpikeResult

9276872009

496424

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .075 75 75-12579 5 20.0750.0011J 0.057 0.060

Parameter UnitsMS



MSSpikeResult

9276872025

496426

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M1.058 67 75-12557 6 20.0620.019 0.058 0.054



Date: 09/27/2010 06:48 PM Page 290 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MERP/3011EPA 7471


Associated Lab Samples: 9276872036, 9276872037, 9276872038, 9276872039, 9276872041, 9276872043, 9276872045, 9276872046,9276872049, 9276872050, 9276872051, 9276872052, 9276872053, 9276872055, 9276872059, 9276872064





Matrix: Solid

Analyzed

Mercury mg/kg ND 0.0050 09/14/10 14:18

Parameter UnitsLCS



Mercury mg/kg 0.057.067 85 80-120

Parameter UnitsMS



MSSpikeResult

9276872036

496430

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg M1.057 80 75-12570 2 20.066ND 0.046 0.047

Parameter UnitsMS



MSSpikeResult

9276872046

496432

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg D6,M1.049 65 75-12572 49 20.072ND 0.031 0.052



Date: 09/27/2010 06:48 PM Page 291 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MERP/3013EPA 7471







Matrix: Solid

Analyzed

Mercury mg/kg 0.0023J 0.0050 09/16/10 12:17

Parameter UnitsLCS



Mercury mg/kg 0.066.067 98 80-120

Parameter UnitsMS



MSSpikeResult

9276872069

496688

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg .055 89 75-12586 12 20.0470.026 0.075 0.066

Parameter UnitsMS



MSSpikeResult

9276981008

496690

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Mercury mg/kg D6,M1.062 -4 75-1251 27 20.0790.013 0.010 0.014



Date: 09/27/2010 06:48 PM Page 292 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11146EPA 3546


Associated Lab Samples: 9276872001, 9276872002, 9276872003, 9276872004, 9276872005, 9276872006, 9276872010





Matrix: Solid

Analyzed




Date: 09/27/2010 06:48 PM Page 293 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS






Date: 09/27/2010 06:48 PM Page 294 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 8291670 50 39-1122-Methylphenol(o-Cresol) ug/kg 9031670 54 39-1012-Nitroaniline ug/kg 18203330 55 44-1112-Nitrophenol ug/kg 7581670 45 41-1003&4-Methylphenol(m&p Cresol) ug/kg 9391670 56 43-1033,3'-Dichlorobenzidine ug/kg 25003330 75 10-1503-Nitroaniline ug/kg 17703330 53 35-1104,6-Dinitro-2-methylphenol ug/kg 23103330 69 38-1184-Bromophenylphenyl ether ug/kg 12501670 75 47-1154-Chloro-3-methylphenol ug/kg 18603330 56 43-1274-Chloroaniline ug/kg 1620J3330 49 34-1094-Chlorophenylphenyl ether ug/kg 11901670 72 44-1154-Nitroaniline ug/kg 18703330 56 37-1114-Nitrophenol ug/kg 60608330 73 21-152Acenaphthene ug/kg 10501670 63 38-117Acenaphthylene ug/kg 10201670 61 46-107Acetophenone ug/kg 917 L23330 28 39-112Anthracene ug/kg 10101670 61 50-110Atrazine ug/kg 15301670 92 39-112Benzaldehyde ug/kg 628J L21670 38 39-112Benzo(a)anthracene ug/kg 13201670 79 47-116Benzo(a)pyrene ug/kg 10501670 63 47-106Benzo(b)fluoranthene ug/kg 12401670 74 47-109Benzo(g,h,i)perylene ug/kg 11401670 68 39-115Benzo(k)fluoranthene ug/kg 11301670 68 45-117Biphenyl (Diphenyl) ug/kg 9961670 60 39-112bis(2-Chloroethoxy)methane ug/kg 9491670 57 39-110bis(2-Chloroethyl) ether ug/kg 8141670 49 19-119bis(2-Chloroisopropyl) ether ug/kg 6471670 39 21-110bis(2-Ethylhexyl)phthalate ug/kg 3320 L31670 199 35-116Butylbenzylphthalate ug/kg 9641670 58 38-110Caprolactam ug/kg 8351670 50 39-112Carbazole ug/kg 9831670 59 39-112Chrysene ug/kg 10701670 64 49-110Di-n-butylphthalate ug/kg 9961670 60 43-109Di-n-octylphthalate ug/kg 9441670 57 37-109Dibenz(a,h)anthracene ug/kg 12701670 76 43-116Dibenzofuran ug/kg 10801670 65 45-106Diethylphthalate ug/kg 10601670 63 41-114Dimethylphthalate ug/kg 10301670 62 43-110Fluoranthene ug/kg 10501670 63 50-114Fluorene ug/kg 11601670 70 46-114Hexachloro-1,3-butadiene ug/kg 8841670 53 28-111Hexachlorobenzene ug/kg 12401670 74 46-120Hexachlorocyclopentadiene ug/kg 10001670 60 18-119Hexachloroethane ug/kg 9651670 58 33-110Indeno(1,2,3-cd)pyrene ug/kg 11901670 71 42-115Isophorone ug/kg 7681670 46 44-109



Date: 09/27/2010 06:48 PM Page 295 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9276750026

496479

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 16 30ND 967 8262,3,4,6-Tetrachlorophenol ug/kg 1790 125 50-15094 28 301790ND 2230 16802,4,5-Trichlorophenol ug/kg 1790 61 28-11051 18 301790ND 1090 9092,4,6-Trichlorophenol ug/kg 1790 63 17-11754 17 301790ND 1130 9542,4-Dichlorophenol ug/kg 1790 53 21-12845 15 301790ND 937 8072,4-Dimethylphenol ug/kg 1790 43 10-12040 9 301790ND 772 7092,4-Dinitrophenol ug/kg 8910 49 10-10741 17 308910ND 4370 36902,4-Dinitrotoluene ug/kg 1790 58 36-10954 6 301790ND 1030 9712,6-Dinitrotoluene ug/kg 1790 57 32-11054 5 301790ND 1010 9602-Chloronaphthalene ug/kg 1790 68 30-10764 6 301790ND 1210 11502-Chlorophenol ug/kg 1790 54 14-10646 16 301790ND 958 8192-Methylnaphthalene ug/kg 1790 49 10-13547 5 301790ND 876 8312-Methylphenol(o-Cresol) ug/kg 1790 51 10-12445 13 301790ND 917 8072-Nitroaniline ug/kg 3560 50 26-11652 3 303560ND 1790 18402-Nitrophenol ug/kg 1790 47 28-10343 9 301790ND 837 7623&4-Methylphenol(m&pCresol)

ug/kg 1790 54 10-10942 25 301790ND 964 747

3,3'-Dichlorobenzidine ug/kg 3560 52 10-15040 303560ND 1840 1430J3-Nitroaniline ug/kg 3560 43 22-11049 303560ND 1530J 1730J4,6-Dinitro-2-methylphenol ug/kg 3560 57 13-12147 19 303560ND 2020 16704-Bromophenylphenyl ether ug/kg 1790 66 31-10953 23 301790ND 1180 9414-Chloro-3-methylphenol ug/kg 3560 51 13-12847 8 303560ND 1820 16804-Chloroaniline ug/kg 3560 41 18-10242 303560ND 1470J 1490J4-Chlorophenylphenyl ether ug/kg 1790 66 29-11256 16 301790ND 1180 10004-Nitroaniline ug/kg 3560 48 16-11151 6 303560ND 1720 18204-Nitrophenol ug/kg 8910 63 14-13556 11 308910ND 5600 5030Acenaphthene ug/kg 1790 59 26-11458 2 301790ND 1060 1040Acenaphthylene ug/kg 1790 57 32-10857 0 301790ND 1020 1020



Date: 09/27/2010 06:48 PM Page 296 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276750026

496479

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg 3560 28 50-15025 14 303560ND 1010 878Anthracene ug/kg 1790 54 32-11153 2 301790ND 955 939Atrazine ug/kg R11790 66 50-150117 55 301790ND 1180 2090Benzaldehyde ug/kg M01790 33 50-15039 301790ND 584J 693JBenzo(a)anthracene ug/kg 1790 67 25-11751 26 301790ND 1190 915Benzo(a)pyrene ug/kg 1790 55 25-10650 9 301790ND 973 892Benzo(b)fluoranthene ug/kg 1790 69 24-11051 30 301790ND 1230 912Benzo(g,h,i)perylene ug/kg 1790 58 19-11254 8 301790ND 1100 1010Benzo(k)fluoranthene ug/kg 1790 54 24-11455 2 301790ND 969 988Biphenyl (Diphenyl) ug/kg 1790 58 50-15057 1 301790ND 1030 1010bis(2-Chloroethoxy)methane ug/kg 1790 57 13-11952 10 301790ND 1020 919bis(2-Chloroethyl) ether ug/kg 1790 51 10-13449 4 301790ND 904 870bis(2-Chloroisopropyl) ether ug/kg 1790 40 10-11342 5 301790ND 712 751bis(2-Ethylhexyl)phthalate ug/kg R11790 165 10-125110 40 301790ND 2940 1960Butylbenzylphthalate ug/kg 1790 49 18-11042 15 301790ND 867 749Caprolactam ug/kg M0,

M1,R11790 41 50-15058 35 301790ND 729 1040

Carbazole ug/kg 1790 52 50-15055 7 301790ND 919 981Chrysene ug/kg 1790 56 30-11053 6 301790ND 999 939Di-n-butylphthalate ug/kg 1790 51 19-11244 14 301790ND 908 789Di-n-octylphthalate ug/kg R11790 49 17-10535 35 301790ND 880 616Dibenz(a,h)anthracene ug/kg 1790 64 23-11153 18 301790ND 1200 1000Dibenzofuran ug/kg 1790 60 35-10359 3 301790ND 1080 1050Diethylphthalate ug/kg 1790 57 27-11352 10 301790ND 1020 926Dimethylphthalate ug/kg 1790 57 26-11155 4 301790ND 1010 972Fluoranthene ug/kg 1790 54 33-10953 2 301790ND 956 938Fluorene ug/kg 1790 63 32-11356 12 301790ND 1130 995Hexachloro-1,3-butadiene ug/kg 1790 56 16-11652 8 301790ND 1000 922Hexachlorobenzene ug/kg 1790 66 27-12055 18 301790ND 1180 989Hexachlorocyclopentadiene ug/kg R11790 68 10-10844 43 301790ND 1210 776Hexachloroethane ug/kg 1790 60 10-11755 8 301790ND 1060 976Indeno(1,2,3-cd)pyrene ug/kg 1790 60 10-12251 16 301790ND 1130 969Isophorone ug/kg 1790 45 28-11445 0 301790ND 802 805N-Nitroso-di-n-propylamine ug/kg 1790 53 27-11346 15 301790ND 946 816N-Nitrosodiphenylamine ug/kg 1790 57 10-12851 12 301790ND 1020 906Naphthalene ug/kg 1790 49 25-11049 1 301790ND 866 871Nitrobenzene ug/kg 1790 46 18-11446 2 301790ND 812 825Pentachlorophenol ug/kg 3560 68 10-12243 303560ND 2420 1520JPhenanthrene ug/kg 1790 57 30-11454 6 301790ND 1020 960Phenol ug/kg 1790 52 11-10246 12 301790ND 931 825Pyrene ug/kg 1790 52 25-11653 2 301790ND 927 9442,4,6-Tribromophenol (S) % 69 27-110572-Fluorobiphenyl (S) % 62 30-110612-Fluorophenol (S) % 50 13-11049Nitrobenzene-d5 (S) % 44 23-11047Phenol-d6 (S) % 49 22-11047Terphenyl-d14 (S) % 56 28-11054



Date: 09/27/2010 06:48 PM Page 297 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11153EPA 3546


Associated Lab Samples: 9276872012, 9276872014, 9276872015, 9276872016, 9276872017, 9276872018, 9276872019, 9276872020,9276872021, 9276872022, 9276872023, 9276872024, 9276872026




Associated Lab Samples: 9276872012, 9276872014, 9276872015, 9276872017, 9276872020, 9276872021, 9276872032, 9276872033,9276872035

Matrix: Solid

Analyzed

1,2,4,5-Tetrachlorobenzene ug/kg ND 330 09/18/10 16:282,3,4,6-Tetrachlorophenol ug/kg ND 330 09/18/10 16:282,4,5-Trichlorophenol ug/kg ND 330 09/18/10 16:282,4,6-Trichlorophenol ug/kg ND 330 09/18/10 16:282,4-Dichlorophenol ug/kg ND 330 09/18/10 16:282,4-Dimethylphenol ug/kg ND 330 09/18/10 16:282,4-Dinitrophenol ug/kg ND 1650 09/18/10 16:282,4-Dinitrotoluene ug/kg ND 330 09/18/10 16:282,6-Dinitrotoluene ug/kg ND 330 09/18/10 16:282-Chloronaphthalene ug/kg ND 330 09/18/10 16:282-Chlorophenol ug/kg ND 330 09/18/10 16:282-Methylnaphthalene ug/kg ND 330 09/18/10 16:282-Methylphenol(o-Cresol) ug/kg ND 330 09/18/10 16:282-Nitroaniline ug/kg ND 1650 09/18/10 16:282-Nitrophenol ug/kg ND 330 09/18/10 16:283&4-Methylphenol(m&p Cresol) ug/kg ND 330 09/18/10 16:283,3'-Dichlorobenzidine ug/kg ND 1650 09/18/10 16:283-Nitroaniline ug/kg ND 1650 09/18/10 16:284,6-Dinitro-2-methylphenol ug/kg ND 660 09/18/10 16:284-Bromophenylphenyl ether ug/kg ND 330 09/18/10 16:284-Chloro-3-methylphenol ug/kg ND 660 09/18/10 16:284-Chloroaniline ug/kg ND 1650 09/18/10 16:284-Chlorophenylphenyl ether ug/kg ND 330 09/18/10 16:284-Nitroaniline ug/kg ND 660 09/18/10 16:284-Nitrophenol ug/kg ND 1650 09/18/10 16:28Acenaphthene ug/kg ND 330 09/18/10 16:28Acenaphthylene ug/kg ND 330 09/18/10 16:28Acetophenone ug/kg ND 330 09/18/10 16:28Anthracene ug/kg ND 330 09/18/10 16:28Atrazine ug/kg ND 660 09/18/10 16:28Benzaldehyde ug/kg ND 660 09/18/10 16:28Benzo(a)anthracene ug/kg ND 330 09/18/10 16:28Benzo(a)pyrene ug/kg ND 330 09/18/10 16:28Benzo(b)fluoranthene ug/kg ND 330 09/18/10 16:28Benzo(g,h,i)perylene ug/kg ND 330 09/18/10 16:28Benzo(k)fluoranthene ug/kg ND 330 09/18/10 16:28Biphenyl (Diphenyl) ug/kg ND 330 09/18/10 16:28bis(2-Chloroethoxy)methane ug/kg ND 330 09/18/10 16:28bis(2-Chloroethyl) ether ug/kg ND 330 09/18/10 16:28bis(2-Chloroisopropyl) ether ug/kg ND 330 09/18/10 16:28bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/18/10 16:28



Date: 09/27/2010 06:48 PM Page 298 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed

Butylbenzylphthalate ug/kg ND 330 09/18/10 16:28Caprolactam ug/kg ND 330 09/18/10 16:28Carbazole ug/kg ND 330 09/18/10 16:28Chrysene ug/kg ND 330 09/18/10 16:28Di-n-butylphthalate ug/kg ND 330 09/18/10 16:28Di-n-octylphthalate ug/kg ND 330 09/18/10 16:28Dibenz(a,h)anthracene ug/kg ND 330 09/18/10 16:28Dibenzofuran ug/kg ND 330 09/18/10 16:28Diethylphthalate ug/kg ND 330 09/18/10 16:28Dimethylphthalate ug/kg ND 330 09/18/10 16:28Fluoranthene ug/kg ND 330 09/18/10 16:28Fluorene ug/kg ND 330 09/18/10 16:28Hexachloro-1,3-butadiene ug/kg ND 330 09/18/10 16:28Hexachlorobenzene ug/kg ND 330 09/18/10 16:28Hexachlorocyclopentadiene ug/kg ND 330 09/18/10 16:28Hexachloroethane ug/kg ND 330 09/18/10 16:28Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/18/10 16:28Isophorone ug/kg ND 330 09/18/10 16:28N-Nitroso-di-n-propylamine ug/kg ND 330 09/18/10 16:28N-Nitrosodiphenylamine ug/kg ND 330 09/18/10 16:28Naphthalene ug/kg ND 330 09/18/10 16:28Nitrobenzene ug/kg ND 330 09/18/10 16:28Pentachlorophenol ug/kg ND 1650 09/18/10 16:28Phenanthrene ug/kg ND 330 09/18/10 16:28Phenol ug/kg ND 330 09/18/10 16:28Pyrene ug/kg ND 330 09/18/10 16:282,4,6-Tribromophenol (S) % 53 27-110 09/18/10 16:282-Fluorobiphenyl (S) % 57 30-110 09/18/10 16:282-Fluorophenol (S) % 52 13-110 09/18/10 16:28Nitrobenzene-d5 (S) % 54 23-110 09/18/10 16:28Phenol-d6 (S) % 47 22-110 09/18/10 16:28Terphenyl-d14 (S) % 58 28-110 09/18/10 16:28

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/kg 9722,3,4,6-Tetrachlorophenol ug/kg 2140 L31670 129 39-1122,4,5-Trichlorophenol ug/kg 10901670 65 48-1092,4,6-Trichlorophenol ug/kg 11501670 69 45-1112,4-Dichlorophenol ug/kg 9531670 57 51-1162,4-Dimethylphenol ug/kg 9621670 58 42-1032,4-Dinitrophenol ug/kg 47408330 57 28-1032,4-Dinitrotoluene ug/kg 11101670 67 46-114



Date: 09/27/2010 06:48 PM Page 299 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2,6-Dinitrotoluene ug/kg 11101670 67 48-1122-Chloronaphthalene ug/kg 12801670 77 44-1052-Chlorophenol ug/kg 9681670 58 36-1102-Methylnaphthalene ug/kg 8901670 53 39-1122-Methylphenol(o-Cresol) ug/kg 10201670 61 39-1012-Nitroaniline ug/kg 21603330 65 44-1112-Nitrophenol ug/kg 8131670 49 41-1003&4-Methylphenol(m&p Cresol) ug/kg 10001670 60 43-1033,3'-Dichlorobenzidine ug/kg 18103330 54 10-1503-Nitroaniline ug/kg 20003330 60 35-1104,6-Dinitro-2-methylphenol ug/kg 19803330 59 38-1184-Bromophenylphenyl ether ug/kg 10801670 65 47-1154-Chloro-3-methylphenol ug/kg 20003330 60 43-1274-Chloroaniline ug/kg 16703330 50 34-1094-Chlorophenylphenyl ether ug/kg 11601670 70 44-1154-Nitroaniline ug/kg 20903330 63 37-1114-Nitrophenol ug/kg 67808330 81 21-152Acenaphthene ug/kg 11301670 68 38-117Acenaphthylene ug/kg 11201670 67 46-107Acetophenone ug/kg 1010 L23330 30 39-112Anthracene ug/kg 10701670 64 50-110Atrazine ug/kg 2460 L31670 148 39-112Benzaldehyde ug/kg 584J L21670 35 39-112Benzo(a)anthracene ug/kg 10801670 65 47-116Benzo(a)pyrene ug/kg 10601670 64 47-106Benzo(b)fluoranthene ug/kg 11101670 67 47-109Benzo(g,h,i)perylene ug/kg 12001670 72 39-115Benzo(k)fluoranthene ug/kg 11601670 69 45-117Biphenyl (Diphenyl) ug/kg 10901670 65 39-112bis(2-Chloroethoxy)methane ug/kg 10101670 60 39-110bis(2-Chloroethyl) ether ug/kg 9541670 57 19-119bis(2-Chloroisopropyl) ether ug/kg 8371670 50 21-110bis(2-Ethylhexyl)phthalate ug/kg 2580 L31670 155 35-116Butylbenzylphthalate ug/kg 9191670 55 38-110Caprolactam ug/kg 12101670 73 39-112Carbazole ug/kg 11001670 66 39-112Chrysene ug/kg 10601670 64 49-110Di-n-butylphthalate ug/kg 9621670 58 43-109Di-n-octylphthalate ug/kg 7821670 47 37-109Dibenz(a,h)anthracene ug/kg 11701670 70 43-116Dibenzofuran ug/kg 11401670 68 45-106Diethylphthalate ug/kg 10701670 64 41-114Dimethylphthalate ug/kg 11001670 66 43-110Fluoranthene ug/kg 11001670 66 50-114Fluorene ug/kg 11401670 68 46-114Hexachloro-1,3-butadiene ug/kg 9381670 56 28-111Hexachlorobenzene ug/kg 11401670 69 46-120Hexachlorocyclopentadiene ug/kg 8991670 54 18-119



Date: 09/27/2010 06:48 PM Page 300 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



Hexachloroethane ug/kg 11201670 67 33-110Indeno(1,2,3-cd)pyrene ug/kg 11501670 69 42-115Isophorone ug/kg 8581670 51 44-109N-Nitroso-di-n-propylamine ug/kg 9831670 59 43-104N-Nitrosodiphenylamine ug/kg 10501670 63 48-113Naphthalene ug/kg 8911670 53 41-110Nitrobenzene ug/kg 8621670 52 38-110Pentachlorophenol ug/kg 21203330 64 32-128Phenanthrene ug/kg 10801670 65 50-110Phenol ug/kg 10101670 61 28-106Pyrene ug/kg 10501670 63 45-1142,4,6-Tribromophenol (S) % 67 27-1102-Fluorobiphenyl (S) % 65 30-1102-Fluorophenol (S) % 56 13-110Nitrobenzene-d5 (S) % 49 23-110Phenol-d6 (S) % 57 22-110Terphenyl-d14 (S) % 60 28-110

Parameter UnitsMS



MSSpikeResult

9276872033

496653

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 5 30ND 1290 13502,3,4,6-Tetrachlorophenol ug/kg 2100 121 50-150133 9 302100ND 2530 27802,4,5-Trichlorophenol ug/kg 2100 66 28-11065 1 302100ND 1380 13702,4,6-Trichlorophenol ug/kg 2100 69 17-11772 5 302100ND 1430 15102,4-Dichlorophenol ug/kg 2100 54 21-12858 6 302100ND 1140 12102,4-Dimethylphenol ug/kg 2100 54 10-12055 1 302100ND 1140 11502,4-Dinitrophenol ug/kg 10500 37 10-10746 22 3010500ND 3850 47802,4-Dinitrotoluene ug/kg 2100 63 36-10967 6 302100ND 1310 14002,6-Dinitrotoluene ug/kg 2100 70 32-11067 5 302100ND 1470 13902-Chloronaphthalene ug/kg 2100 81 30-10782 1 302100ND 1680 17002-Chlorophenol ug/kg 2100 54 14-10660 11 302100ND 1130 12602-Methylnaphthalene ug/kg 2100 51 10-13556 10 302100ND 1060 11702-Methylphenol(o-Cresol) ug/kg 2100 55 10-12461 11 302100ND 1140 12802-Nitroaniline ug/kg 4180 64 26-11661 6 304180ND 2700 25402-Nitrophenol ug/kg 2100 47 28-10352 10 302100ND 974 10803&4-Methylphenol(m&pCresol)

ug/kg 2100 55 10-10956 4 302100ND 1140 1180

3,3'-Dichlorobenzidine ug/kg 4180 55 10-15054 1 304180ND 2290 22603-Nitroaniline ug/kg 4180 48 22-11055 304180ND 2030J 22904,6-Dinitro-2-methylphenol ug/kg 4180 51 13-12157 11 304180ND 2140 23804-Bromophenylphenyl ether ug/kg 2100 62 31-10968 9 302100ND 1300 14204-Chloro-3-methylphenol ug/kg 4180 55 13-12857 5 304180ND 2290 23904-Chloroaniline ug/kg 4180 46 18-10248 304180ND 1920J 2020J4-Chlorophenylphenyl ether ug/kg 2100 67 29-11273 8 302100ND 1410 15204-Nitroaniline ug/kg 4180 49 16-11157 14 304180ND 2070 2370



Date: 09/27/2010 06:48 PM Page 301 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276872033

496653

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

4-Nitrophenol ug/kg 10500 56 14-13567 18 3010500ND 5870 7000Acenaphthene ug/kg 2100 65 26-11470 7 302100ND 1350 1450Acenaphthylene ug/kg 2100 70 32-10869 2 302100ND 1470 1440Acetophenone ug/kg M04180 28 50-15032 11 304180ND 1190 1320Anthracene ug/kg 2100 59 32-11164 9 302100ND 1230 1340Atrazine ug/kg M02100 144 50-150158 9 302100ND 3000 3300Benzaldehyde ug/kg 2100 54 50-15066 19 302100ND 1140 1370Benzo(a)anthracene ug/kg 2100 59 25-11762 4 302100ND 1230 1290Benzo(a)pyrene ug/kg 2100 57 25-10662 9 302100ND 1180 1290Benzo(b)fluoranthene ug/kg 2100 60 24-11065 8 302100ND 1250 1360Benzo(g,h,i)perylene ug/kg 2100 64 19-11270 8 302100ND 1350 1460Benzo(k)fluoranthene ug/kg 2100 62 24-11467 8 302100ND 1290 1410Biphenyl (Diphenyl) ug/kg 2100 67 50-15068 2 302100ND 1400 1420bis(2-Chloroethoxy)methane ug/kg 2100 57 13-11962 8 302100ND 1190 1290bis(2-Chloroethyl) ether ug/kg 2100 52 10-13459 12 302100ND 1090 1230bis(2-Chloroisopropyl) ether ug/kg 2100 44 10-11349 11 302100ND 919 1030bis(2-Ethylhexyl)phthalate ug/kg M02100 133 10-125134 0 302100ND 2790 2800Butylbenzylphthalate ug/kg 2100 48 18-11048 1 302100ND 1010 1010Caprolactam ug/kg 2100 63 50-15065 3 302100ND 1320 1360Carbazole ug/kg 2100 59 50-15065 9 302100ND 1240 1350Chrysene ug/kg 2100 61 30-11062 1 302100ND 1280 1300Di-n-butylphthalate ug/kg 2100 50 19-11253 5 302100ND 1040 1100Di-n-octylphthalate ug/kg 2100 36 17-10538 5 302100ND 760 797Dibenz(a,h)anthracene ug/kg 2100 64 23-11168 6 302100ND 1330 1410Dibenzofuran ug/kg 2100 65 35-10369 6 302100ND 1370 1450Diethylphthalate ug/kg 2100 60 27-11365 8 302100ND 1250 1350Dimethylphthalate ug/kg 2100 68 26-11166 3 302100ND 1420 1380Fluoranthene ug/kg 2100 61 33-10963 4 302100ND 1270 1320Fluorene ug/kg 2100 63 32-11367 7 302100ND 1310 1410Hexachloro-1,3-butadiene ug/kg 2100 59 16-11666 12 302100ND 1230 1380Hexachlorobenzene ug/kg 2100 67 27-12074 10 302100ND 1390 1540Hexachlorocyclopentadiene ug/kg 2100 64 10-10868 5 302100ND 1340 1420Hexachloroethane ug/kg 2100 60 10-11768 13 302100ND 1250 1420Indeno(1,2,3-cd)pyrene ug/kg 2100 63 10-12267 7 302100ND 1310 1400Isophorone ug/kg 2100 48 28-11451 5 302100ND 1010 1060N-Nitroso-di-n-propylamine ug/kg 2100 54 27-11359 10 302100ND 1120 1240N-Nitrosodiphenylamine ug/kg 2100 57 10-12863 9 302100ND 1200 1320Naphthalene ug/kg 2100 52 25-11058 10 302100ND 1090 1210Nitrobenzene ug/kg 2100 50 18-11452 4 302100ND 1050 1090Pentachlorophenol ug/kg 4180 56 10-12259 5 304180ND 2340 2470Phenanthrene ug/kg 2100 59 30-11465 9 302100ND 1230 1350Phenol ug/kg 2100 53 11-10258 9 302100ND 1110 1210Pyrene ug/kg 2100 56 25-11660 7 302100ND 1180 12602,4,6-Tribromophenol (S) % 66 27-110712-Fluorobiphenyl (S) % 66 30-110692-Fluorophenol (S) % 49 13-11057Nitrobenzene-d5 (S) % 47 23-11051



Date: 09/27/2010 06:48 PM Page 302 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276872033

496653

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Phenol-d6 (S) % 50 22-11055Terphenyl-d14 (S) % 53 28-11057



Date: 09/27/2010 06:48 PM Page 303 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11170EPA 3546







Matrix: Solid

Analyzed

1,2,4,5-Tetrachlorobenzene ug/kg ND 330 09/20/10 13:102,3,4,6-Tetrachlorophenol ug/kg ND 330 09/20/10 13:102,4,5-Trichlorophenol ug/kg ND 330 09/20/10 13:102,4,6-Trichlorophenol ug/kg ND 330 09/20/10 13:102,4-Dichlorophenol ug/kg ND 330 09/20/10 13:102,4-Dimethylphenol ug/kg ND 330 09/20/10 13:102,4-Dinitrophenol ug/kg ND 1650 09/20/10 13:102,4-Dinitrotoluene ug/kg ND 330 09/20/10 13:102,6-Dinitrotoluene ug/kg ND 330 09/20/10 13:102-Chloronaphthalene ug/kg ND 330 09/20/10 13:102-Chlorophenol ug/kg ND 330 09/20/10 13:102-Methylnaphthalene ug/kg ND 330 09/20/10 13:102-Methylphenol(o-Cresol) ug/kg ND 330 09/20/10 13:102-Nitroaniline ug/kg ND 1650 09/20/10 13:102-Nitrophenol ug/kg ND 330 09/20/10 13:103&4-Methylphenol(m&p Cresol) ug/kg ND 330 09/20/10 13:103,3'-Dichlorobenzidine ug/kg ND 1650 09/20/10 13:103-Nitroaniline ug/kg ND 1650 09/20/10 13:104,6-Dinitro-2-methylphenol ug/kg ND 660 09/20/10 13:104-Bromophenylphenyl ether ug/kg 75.4J 330 09/20/10 13:104-Chloro-3-methylphenol ug/kg ND 660 09/20/10 13:104-Chloroaniline ug/kg ND 1650 09/20/10 13:104-Chlorophenylphenyl ether ug/kg ND 330 09/20/10 13:104-Nitroaniline ug/kg ND 660 09/20/10 13:104-Nitrophenol ug/kg ND 1650 09/20/10 13:10Acenaphthene ug/kg ND 330 09/20/10 13:10Acenaphthylene ug/kg ND 330 09/20/10 13:10Acetophenone ug/kg ND 330 09/20/10 13:10Anthracene ug/kg ND 330 09/20/10 13:10Atrazine ug/kg ND 660 09/20/10 13:10Benzaldehyde ug/kg ND 660 09/20/10 13:10Benzo(a)anthracene ug/kg ND 330 09/20/10 13:10Benzo(a)pyrene ug/kg ND 330 09/20/10 13:10Benzo(b)fluoranthene ug/kg ND 330 09/20/10 13:10Benzo(g,h,i)perylene ug/kg ND 330 09/20/10 13:10Benzo(k)fluoranthene ug/kg ND 330 09/20/10 13:10Biphenyl (Diphenyl) ug/kg ND 330 09/20/10 13:10bis(2-Chloroethoxy)methane ug/kg ND 330 09/20/10 13:10bis(2-Chloroethyl) ether ug/kg ND 330 09/20/10 13:10bis(2-Chloroisopropyl) ether ug/kg ND 330 09/20/10 13:10bis(2-Ethylhexyl)phthalate ug/kg ND 330 09/20/10 13:10Butylbenzylphthalate ug/kg ND 330 09/20/10 13:10



Date: 09/27/2010 06:48 PM Page 304 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed

Caprolactam ug/kg ND 330 09/20/10 13:10Carbazole ug/kg ND 330 09/20/10 13:10Chrysene ug/kg ND 330 09/20/10 13:10Di-n-butylphthalate ug/kg ND 330 09/20/10 13:10Di-n-octylphthalate ug/kg ND 330 09/20/10 13:10Dibenz(a,h)anthracene ug/kg ND 330 09/20/10 13:10Dibenzofuran ug/kg ND 330 09/20/10 13:10Diethylphthalate ug/kg ND 330 09/20/10 13:10Dimethylphthalate ug/kg ND 330 09/20/10 13:10Fluoranthene ug/kg ND 330 09/20/10 13:10Fluorene ug/kg ND 330 09/20/10 13:10Hexachloro-1,3-butadiene ug/kg ND 330 09/20/10 13:10Hexachlorobenzene ug/kg ND 330 09/20/10 13:10Hexachlorocyclopentadiene ug/kg ND 330 09/20/10 13:10Hexachloroethane ug/kg ND 330 09/20/10 13:10Indeno(1,2,3-cd)pyrene ug/kg ND 330 09/20/10 13:10Isophorone ug/kg ND 330 09/20/10 13:10N-Nitroso-di-n-propylamine ug/kg ND 330 09/20/10 13:10N-Nitrosodiphenylamine ug/kg ND 330 09/20/10 13:10Naphthalene ug/kg ND 330 09/20/10 13:10Nitrobenzene ug/kg ND 330 09/20/10 13:10Pentachlorophenol ug/kg ND 1650 09/20/10 13:10Phenanthrene ug/kg ND 330 09/20/10 13:10Phenol ug/kg ND 330 09/20/10 13:10Pyrene ug/kg ND 330 09/20/10 13:102,4,6-Tribromophenol (S) % 84 27-110 09/20/10 13:102-Fluorobiphenyl (S) % 66 30-110 09/20/10 13:102-Fluorophenol (S) % 52 13-110 09/20/10 13:10Nitrobenzene-d5 (S) % 52 23-110 09/20/10 13:10Phenol-d6 (S) % 48 22-110 09/20/10 13:10Terphenyl-d14 (S) % 72 28-110 09/20/10 13:10

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/kg 14302,3,4,6-Tetrachlorophenol ug/kg 3140 L31670 189 39-1122,4,5-Trichlorophenol ug/kg 15401670 92 48-1092,4,6-Trichlorophenol ug/kg 16401670 98 45-1112,4-Dichlorophenol ug/kg 11801670 71 51-1162,4-Dimethylphenol ug/kg 10901670 66 42-1032,4-Dinitrophenol ug/kg 65208330 78 28-1032,4-Dinitrotoluene ug/kg 14901670 90 46-1142,6-Dinitrotoluene ug/kg 14701670 88 48-1122-Chloronaphthalene ug/kg 17301670 104 44-105



Date: 09/27/2010 06:48 PM Page 305 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2-Chlorophenol ug/kg 13101670 79 36-1102-Methylnaphthalene ug/kg 11101670 67 39-1122-Methylphenol(o-Cresol) ug/kg 12301670 74 39-1012-Nitroaniline ug/kg 23803330 72 44-1112-Nitrophenol ug/kg 10601670 64 41-1003&4-Methylphenol(m&p Cresol) ug/kg 12101670 73 43-1033,3'-Dichlorobenzidine ug/kg 23503330 70 10-1503-Nitroaniline ug/kg 24403330 73 35-1104,6-Dinitro-2-methylphenol ug/kg 27103330 81 38-1184-Bromophenylphenyl ether ug/kg 15801670 95 47-1154-Chloro-3-methylphenol ug/kg 22303330 67 43-1274-Chloroaniline ug/kg 18403330 55 34-1094-Chlorophenylphenyl ether ug/kg 16601670 100 44-1154-Nitroaniline ug/kg 25003330 75 37-1114-Nitrophenol ug/kg 76808330 92 21-152Acenaphthene ug/kg 14701670 88 38-117Acenaphthylene ug/kg 14601670 88 46-107Acetophenone ug/kg 1270 L23330 38 39-112Anthracene ug/kg 13901670 83 50-110Atrazine ug/kg 3320 L31670 199 39-112Benzaldehyde ug/kg 542J L21670 33 39-112Benzo(a)anthracene ug/kg 14201670 85 47-116Benzo(a)pyrene ug/kg 13601670 82 47-106Benzo(b)fluoranthene ug/kg 14501670 87 47-109Benzo(g,h,i)perylene ug/kg 16401670 99 39-115Benzo(k)fluoranthene ug/kg 14901670 90 45-117Biphenyl (Diphenyl) ug/kg 14201670 85 39-112bis(2-Chloroethoxy)methane ug/kg 11201670 67 39-110bis(2-Chloroethyl) ether ug/kg 11401670 68 19-119bis(2-Chloroisopropyl) ether ug/kg 8101670 49 21-110bis(2-Ethylhexyl)phthalate ug/kg 2970 L31670 178 35-116Butylbenzylphthalate ug/kg 10401670 62 38-110Caprolactam ug/kg 13201670 79 39-112Carbazole ug/kg 13601670 82 39-112Chrysene ug/kg 14001670 84 49-110Di-n-butylphthalate ug/kg 11601670 70 43-109Di-n-octylphthalate ug/kg 8981670 54 37-109Dibenz(a,h)anthracene ug/kg 16101670 96 43-116Dibenzofuran ug/kg 15201670 91 45-106Diethylphthalate ug/kg 13601670 82 41-114Dimethylphthalate ug/kg 14201670 85 43-110Fluoranthene ug/kg 14601670 88 50-114Fluorene ug/kg 15001670 90 46-114Hexachloro-1,3-butadiene ug/kg 14201670 85 28-111Hexachlorobenzene ug/kg 17301670 104 46-120Hexachlorocyclopentadiene ug/kg 17401670 104 18-119Hexachloroethane ug/kg 14301670 86 33-110Indeno(1,2,3-cd)pyrene ug/kg 16001670 96 42-115



Date: 09/27/2010 06:48 PM Page 306 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



Isophorone ug/kg 9171670 55 44-109N-Nitroso-di-n-propylamine ug/kg 10601670 64 43-104N-Nitrosodiphenylamine ug/kg 13501670 81 48-113Naphthalene ug/kg 11201670 67 41-110Nitrobenzene ug/kg 9921670 60 38-110Pentachlorophenol ug/kg 32303330 97 32-128Phenanthrene ug/kg 13901670 83 50-110Phenol ug/kg 11801670 71 28-106Pyrene ug/kg 13301670 80 45-1142,4,6-Tribromophenol (S) % 101 27-1102-Fluorobiphenyl (S) % 85 30-1102-Fluorophenol (S) % 69 13-110Nitrobenzene-d5 (S) % 55 23-110Phenol-d6 (S) % 65 22-110Terphenyl-d14 (S) % 79 28-110

Parameter UnitsMS



MSSpikeResult

9276872007

497435

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg R148 30ND 773 4722,3,4,6-Tetrachlorophenol ug/kg R11920 80 50-15053 41 301920ND 1530 10102,4,5-Trichlorophenol ug/kg M0,

M1,R11920 37 28-11026 35 301920ND 708 496

2,4,6-Trichlorophenol ug/kg R11920 39 17-11727 35 301920ND 748 5262,4-Dichlorophenol ug/kg R11920 33 21-12822 41 301920ND 627 4142,4-Dimethylphenol ug/kg 1920 27 10-12018 301920ND 514 355J2,4-Dinitrophenol ug/kg 9580 32 10-10723 30 309580ND 3020 22302,4-Dinitrotoluene ug/kg M0,

M1,R11920 37 36-10927 31 301920ND 706 517

2,6-Dinitrotoluene ug/kg M0,M1,R1

1920 37 32-11027 32 301920ND 703 511

2-Chloronaphthalene ug/kg R11920 44 30-10730 37 301920ND 837 5772-Chlorophenol ug/kg R11920 33 14-10620 48 301920ND 624 3822-Methylnaphthalene ug/kg R11920 32 10-13522 37 301920ND 620 4282-Methylphenol(o-Cresol) ug/kg 1920 30 10-12419 301920ND 569 355J2-Nitroaniline ug/kg M0,M13830 29 26-11621 303830ND 1130J 817J2-Nitrophenol ug/kg M0,

M1,R11920 31 28-10319 301920ND 587 363J

3&4-Methylphenol(m&pCresol)

ug/kg 1920 28 10-10918 301920ND 538 336J

3,3'-Dichlorobenzidine ug/kg 3830 27 10-15020 303830ND 1050J 749J3-Nitroaniline ug/kg 3830 29 22-11022 303830ND 1130J 843J4,6-Dinitro-2-methylphenol ug/kg R13830 32 13-12123 33 303830ND 1240 8894-Bromophenylphenyl ether ug/kg M0,

M1,R11920 38 31-10928 31 301920ND 727 529

4-Chloro-3-methylphenol ug/kg R13830 31 13-12822 33 303830ND 1190 8554-Chloroaniline ug/kg 3830 26 18-10218 303830ND 996J 692J



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(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276872007

497435

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

4-Chlorophenylphenyl ether ug/kg R11920 41 29-11229 34 301920ND 785 5554-Nitroaniline ug/kg 3830 32 16-11124 30 303830ND 1240 9184-Nitrophenol ug/kg R19580 37 14-13526 35 309580ND 3500 2450Acenaphthene ug/kg R11920 37 26-11426 34 301920ND 705 501Acenaphthylene ug/kg M0,

M1,R11920 37 32-10825 37 301920ND 702 484

Acetophenone ug/kg M0,R13830 17 50-15010 47 303830ND 633 393Anthracene ug/kg M0,M11920 34 32-11125 28 301920ND 646 486Atrazine ug/kg 1920 87 50-15066 28 301920ND 1670 1260Benzaldehyde ug/kg M01920 28 50-15017 301920ND 546J NDBenzo(a)anthracene ug/kg R11920 34 25-11725 33 301920ND 656 470Benzo(a)pyrene ug/kg M0,

M1,R11920 33 25-10624 33 301920ND 636 455

Benzo(b)fluoranthene ug/kg R11920 34 24-11025 31 301920ND 657 481Benzo(g,h,i)perylene ug/kg R11920 39 19-11228 35 301920ND 756 530Benzo(k)fluoranthene ug/kg M0,

M1,R11920 38 24-11427 34 301920ND 730 518

Biphenyl (Diphenyl) ug/kg M0,M1,R1

1920 36 50-15025 37 301920ND 683 471

bis(2-Chloroethoxy)methane ug/kg R11920 34 13-11922 43 301920ND 644 417bis(2-Chloroethyl) ether ug/kg 1920 29 10-13418 301920ND 553 353Jbis(2-Chloroisopropyl) ether ug/kg 1920 21 10-11313 301920ND 399 242Jbis(2-Ethylhexyl)phthalate ug/kg R11920 76 10-12549 42 301920ND 1450 948Butylbenzylphthalate ug/kg M0,M11920 25 18-11017 301920ND 475 334JCaprolactam ug/kg M0,M11920 43 50-15034 21 301920ND 816 660Carbazole ug/kg M0,M11920 33 50-15025 27 301920ND 637 487Chrysene ug/kg M0,

M1,R11920 34 30-11024 33 301920ND 656 468

Di-n-butylphthalate ug/kg 1920 28 19-11221 30 301920ND 533 394Di-n-octylphthalate ug/kg M0,M11920 20 17-10514 301920ND 391 261JDibenz(a,h)anthracene ug/kg R11920 39 23-11127 36 301920ND 752 525Dibenzofuran ug/kg M0,

M1,R11920 38 35-10327 33 301920ND 736 526

Diethylphthalate ug/kg M0,M1,R1

1920 35 27-11325 31 301920ND 662 483

Dimethylphthalate ug/kg R11920 36 26-11126 32 301920ND 692 501Fluoranthene ug/kg M0,M11920 36 33-10927 28 301920ND 682 513Fluorene ug/kg M0,

M1,R11920 37 32-11327 33 301920ND 716 512

Hexachloro-1,3-butadiene ug/kg R11920 40 16-11627 38 301920ND 770 522Hexachlorobenzene ug/kg R11920 43 27-12031 34 301920ND 825 586Hexachlorocyclopentadiene ug/kg R11920 41 10-10825 47 301920ND 786 487Hexachloroethane ug/kg R11920 37 10-11723 48 301920ND 713 438Indeno(1,2,3-cd)pyrene ug/kg R11920 37 10-12226 35 301920ND 716 503Isophorone ug/kg M0,

M1,R11920 27 28-11418 301920ND 516 350J

N-Nitroso-di-n-propylamine ug/kg M0,M1,R1

1920 28 27-11317 301920ND 545 330J

N-Nitrosodiphenylamine ug/kg 1920 32 10-12824 29 301920ND 608 453



Date: 09/27/2010 06:48 PM Page 308 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276872007

497435

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Naphthalene ug/kg M0,M1,R1

1920 33 25-11022 40 301920ND 625 415

Nitrobenzene ug/kg 1920 29 18-11419 301920ND 547 374JPentachlorophenol ug/kg 3830 36 10-12224 303830ND 1370J 921JPhenanthrene ug/kg M0,M11920 34 30-11426 29 301920ND 657 491Phenol ug/kg 1920 30 11-10219 301920ND 573 359JPyrene ug/kg M0,

M1,R11920 32 25-11623 33 301920ND 621 447

2,4,6-Tribromophenol (S) % 48 27-110392-Fluorobiphenyl (S) % 44 30-110332-Fluorophenol (S) % 34 13-11024Nitrobenzene-d5 (S) % 33 23-11024Phenol-d6 (S) % S033 22-11021Terphenyl-d14 (S) % 39 28-11031



Date: 09/27/2010 06:48 PM Page 309 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11177EPA 3546







Matrix: Solid

Analyzed




Date: 09/27/2010 06:48 PM Page 310 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS






Date: 09/27/2010 06:48 PM Page 311 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 10701670 64 39-1122-Methylphenol(o-Cresol) ug/kg 11801670 71 39-1012-Nitroaniline ug/kg 26203330 79 44-1112-Nitrophenol ug/kg 10101670 60 41-1003&4-Methylphenol(m&p Cresol) ug/kg 11701670 70 43-1033,3'-Dichlorobenzidine ug/kg 22303330 67 10-1503-Nitroaniline ug/kg 25003330 75 35-1104,6-Dinitro-2-methylphenol ug/kg 23803330 71 38-1184-Bromophenylphenyl ether ug/kg 13901670 83 47-1154-Chloro-3-methylphenol ug/kg 23603330 71 43-1274-Chloroaniline ug/kg 18903330 57 34-1094-Chlorophenylphenyl ether ug/kg 15001670 90 44-1154-Nitroaniline ug/kg 25203330 76 37-1114-Nitrophenol ug/kg 86108330 103 21-152Acenaphthene ug/kg 14701670 88 38-117Acenaphthylene ug/kg 14501670 87 46-107Acetophenone ug/kg 1240 L23330 37 39-112Anthracene ug/kg 13601670 81 50-110Atrazine ug/kg 3420 L31670 205 39-112Benzaldehyde ug/kg 13501670 81 39-112Benzo(a)anthracene ug/kg 13301670 80 47-116Benzo(a)pyrene ug/kg 13001670 78 47-106Benzo(b)fluoranthene ug/kg 14001670 84 47-109Benzo(g,h,i)perylene ug/kg 15201670 91 39-115Benzo(k)fluoranthene ug/kg 15001670 90 45-117Biphenyl (Diphenyl) ug/kg 13801670 83 39-112bis(2-Chloroethoxy)methane ug/kg 11801670 71 39-110bis(2-Chloroethyl) ether ug/kg 11501670 69 19-119bis(2-Chloroisopropyl) ether ug/kg 9771670 59 21-110bis(2-Ethylhexyl)phthalate ug/kg 2860 L31670 172 35-116Butylbenzylphthalate ug/kg 9881670 59 38-110Caprolactam ug/kg 14501670 87 39-112Carbazole ug/kg 13101670 79 39-112Chrysene ug/kg 13501670 81 49-110Di-n-butylphthalate ug/kg 10801670 65 43-109Di-n-octylphthalate ug/kg 7661670 46 37-109Dibenz(a,h)anthracene ug/kg 15101670 91 43-116Dibenzofuran ug/kg 15101670 91 45-106Diethylphthalate ug/kg 12401670 74 41-114Dimethylphthalate ug/kg 12901670 77 43-110Fluoranthene ug/kg 13901670 84 50-114Fluorene ug/kg 14401670 86 46-114Hexachloro-1,3-butadiene ug/kg 12501670 75 28-111Hexachlorobenzene ug/kg 14401670 87 46-120Hexachlorocyclopentadiene ug/kg 13301670 80 18-119Hexachloroethane ug/kg 13301670 80 33-110Indeno(1,2,3-cd)pyrene ug/kg 14601670 88 42-115Isophorone ug/kg 9981670 60 44-109



Date: 09/27/2010 06:48 PM Page 312 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9276872048

497677

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 10 30ND 1230 13602,3,4,6-Tetrachlorophenol ug/kg M01900 137 50-150155 13 301900ND 2600 29502,4,5-Trichlorophenol ug/kg 1900 67 28-11074 9 301900ND 1280 14102,4,6-Trichlorophenol ug/kg 1900 73 17-11778 7 301900ND 1390 14902,4-Dichlorophenol ug/kg 1900 55 21-12862 11 301900ND 1050 11702,4-Dimethylphenol ug/kg 1900 50 10-12054 7 301900ND 944 10202,4-Dinitrophenol ug/kg 9500 53 10-10763 18 309500ND 5020 60002,4-Dinitrotoluene ug/kg 1900 69 36-10976 10 301900ND 1310 14502,6-Dinitrotoluene ug/kg 1900 68 32-11074 10 301900ND 1280 14102-Chloronaphthalene ug/kg 1900 85 30-10788 4 301900ND 1610 16802-Chlorophenol ug/kg 1900 52 14-10663 18 301900ND 997 11902-Methylnaphthalene ug/kg 1900 60 10-13559 1 301900ND 1140 11202-Methylphenol(o-Cresol) ug/kg 1900 55 10-12462 13 301900ND 1040 11802-Nitroaniline ug/kg 3800 66 26-11670 5 303800ND 2520 26402-Nitrophenol ug/kg 1900 52 28-10358 12 301900ND 982 11003&4-Methylphenol(m&pCresol)

ug/kg 1900 53 10-10959 10 301900ND 1010 1120

3,3'-Dichlorobenzidine ug/kg 3800 51 10-15056 10 303800ND 1930 21403-Nitroaniline ug/kg 3800 63 22-11065 3 303800ND 2390 24704,6-Dinitro-2-methylphenol ug/kg 3800 58 13-12161 6 303800ND 2190 23204-Bromophenylphenyl ether ug/kg 1900 67 31-10971 6 301900ND 1280 13504-Chloro-3-methylphenol ug/kg 3800 64 13-12864 1 303800ND 2450 24304-Chloroaniline ug/kg 3800 48 18-10251 303800ND 1840J 19404-Chlorophenylphenyl ether ug/kg 1900 76 29-11281 7 301900ND 1440 15404-Nitroaniline ug/kg 3800 66 16-11171 8 303800ND 2490 26904-Nitrophenol ug/kg 9500 84 14-13593 10 309500ND 7960 8840Acenaphthene ug/kg 1900 78 26-11479 2 301900ND 1480 1510Acenaphthylene ug/kg 1900 73 32-10879 8 301900ND 1390 1500



Date: 09/27/2010 06:48 PM Page 313 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276872048

497677

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg M03800 30 50-15033 10 303800ND 1140 1250Anthracene ug/kg 1900 69 32-11175 9 301900ND 1300 1430Atrazine ug/kg M01900 175 50-150189 8 301900ND 3320 3590Benzaldehyde ug/kg 1900 101 50-150106 5 301900ND 1930 2010Benzo(a)anthracene ug/kg 1900 66 25-11773 10 301900ND 1260 1390Benzo(a)pyrene ug/kg 1900 65 25-10673 12 301900ND 1230 1390Benzo(b)fluoranthene ug/kg 1900 70 24-11076 8 301900ND 1330 1440Benzo(g,h,i)perylene ug/kg 1900 76 19-11282 7 301900ND 1440 1550Benzo(k)fluoranthene ug/kg 1900 74 24-11482 10 301900ND 1400 1550Biphenyl (Diphenyl) ug/kg 1900 70 50-15075 6 301900ND 1340 1420bis(2-Chloroethoxy)methane ug/kg 1900 62 13-11969 11 301900ND 1180 1310bis(2-Chloroethyl) ether ug/kg 1900 52 10-13462 18 301900ND 981 1170bis(2-Chloroisopropyl) ether ug/kg 1900 44 10-11353 18 301900ND 838 1000bis(2-Ethylhexyl)phthalate ug/kg M01900 139 10-125156 12 301900ND 2640 2970Butylbenzylphthalate ug/kg 1900 50 18-11055 10 301900ND 944 1050Caprolactam ug/kg 1900 72 50-15079 10 301900ND 1360 1500Carbazole ug/kg 1900 64 50-15074 14 301900ND 1220 1400Chrysene ug/kg 1900 67 30-11073 9 301900ND 1270 1390Di-n-butylphthalate ug/kg 1900 54 19-11255 3 301900ND 1020 1050Di-n-octylphthalate ug/kg 1900 39 17-10539 1 301900ND 740 734Dibenz(a,h)anthracene ug/kg 1900 76 23-11183 9 301900ND 1450 1580Dibenzofuran ug/kg 1900 78 35-10380 3 301900ND 1480 1520Diethylphthalate ug/kg 1900 62 27-11368 10 301900ND 1180 1300Dimethylphthalate ug/kg 1900 64 26-11169 8 301900ND 1210 1320Fluoranthene ug/kg 1900 70 33-10978 10 301900ND 1330 1480Fluorene ug/kg 1900 76 32-11379 3 301900ND 1450 1500Hexachloro-1,3-butadiene ug/kg 1900 60 16-11669 15 301900ND 1130 1320Hexachlorobenzene ug/kg 1900 75 27-12078 5 301900ND 1420 1490Hexachlorocyclopentadiene ug/kg 1900 61 10-10875 21 301900ND 1160 1430Hexachloroethane ug/kg 1900 57 10-11770 20 301900ND 1090 1330Indeno(1,2,3-cd)pyrene ug/kg 1900 74 10-12281 10 301900ND 1400 1540Isophorone ug/kg 1900 51 28-11455 6 301900ND 978 1040N-Nitroso-di-n-propylamine ug/kg 1900 57 27-11364 12 301900ND 1080 1220N-Nitrosodiphenylamine ug/kg 1900 67 10-12865 2 301900ND 1270 1240Naphthalene ug/kg 1900 57 25-11063 9 301900ND 1080 1190Nitrobenzene ug/kg 1900 50 18-11460 20 301900ND 942 1150Pentachlorophenol ug/kg 3800 59 10-12271 19 303800ND 2230 2700Phenanthrene ug/kg 1900 70 30-11475 6 301900ND 1330 1420Phenol ug/kg 1900 56 11-10261 9 301900ND 1060 1160Pyrene ug/kg 1900 67 25-11673 9 301900ND 1270 13902,4,6-Tribromophenol (S) % 73 27-110752-Fluorobiphenyl (S) % 75 30-110782-Fluorophenol (S) % 50 13-11059Nitrobenzene-d5 (S) % 51 23-11061Phenol-d6 (S) % 54 22-11060Terphenyl-d14 (S) % 65 28-11071



Date: 09/27/2010 06:48 PM Page 314 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276981018

497679

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 9 30ND 965 10502,3,4,6-Tetrachlorophenol ug/kg 1830 114 50-150133 15 301830ND 2070 24202,4,5-Trichlorophenol ug/kg 1830 56 28-11065 15 301830ND 1020 11802,4,6-Trichlorophenol ug/kg 1830 53 17-11766 21 301830ND 975 12002,4-Dichlorophenol ug/kg 1830 46 21-12861 29 301830ND 838 11202,4-Dimethylphenol ug/kg 1830 43 10-12055 24 301830ND 787 10002,4-Dinitrophenol ug/kg R19120 42 10-10760 34 309120ND 3870 54502,4-Dinitrotoluene ug/kg 1830 56 36-10968 20 301830ND 1020 12402,6-Dinitrotoluene ug/kg 1830 51 32-11067 27 301830ND 938 12302-Chloronaphthalene ug/kg 1830 65 30-10774 13 301830ND 1180 13402-Chlorophenol ug/kg 1830 48 14-10660 23 301830ND 878 11002-Methylnaphthalene ug/kg 1830 43 10-13557 28 301830ND 790 10402-Methylphenol(o-Cresol) ug/kg R11830 45 10-12463 34 301830ND 821 11502-Nitroaniline ug/kg 3640 53 26-11665 20 303640ND 1950 23802-Nitrophenol ug/kg 1830 40 28-10355 30 301830ND 735 9953&4-Methylphenol(m&pCresol)

ug/kg 1830 43 10-10951 17 301830ND 781 930

3,3'-Dichlorobenzidine ug/kg 3640 42 10-15052 303640ND 1550J 19103-Nitroaniline ug/kg 3640 49 22-11061 303640ND 1810 22404,6-Dinitro-2-methylphenol ug/kg R13640 44 13-12163 36 303640ND 1600 23104-Bromophenylphenyl ether ug/kg 1830 56 31-10970 22 301830ND 1030 12804-Chloro-3-methylphenol ug/kg 3640 47 13-12862 27 303640ND 1710 22604-Chloroaniline ug/kg 3640 39 18-10249 303640ND 1430J 1770J4-Chlorophenylphenyl ether ug/kg 1830 60 29-11276 22 301830ND 1100 13804-Nitroaniline ug/kg 3640 50 16-11164 24 303640ND 1830 23304-Nitrophenol ug/kg 9120 65 14-13580 21 309120ND 5920 7300Acenaphthene ug/kg 1830 59 26-11475 23 301830ND 1090 1370Acenaphthylene ug/kg 1830 56 32-10872 25 301830ND 1030 1320Acetophenone ug/kg M03640 23 50-15027 17 303640ND 845 1000Anthracene ug/kg 1830 55 32-11169 23 301830ND 1010 1270Atrazine ug/kg M01830 136 50-150160 16 301830ND 2480 2910Benzaldehyde ug/kg 1830 102 50-150115 13 301830ND 1850 2100Benzo(a)anthracene ug/kg 1830 55 25-11770 24 301830ND 1000 1280Benzo(a)pyrene ug/kg R11830 51 25-10669 31 301830ND 931 1270Benzo(b)fluoranthene ug/kg 1830 58 24-11073 22 301830ND 1060 1320Benzo(g,h,i)perylene ug/kg 1830 63 19-11282 26 301830ND 1150 1500Benzo(k)fluoranthene ug/kg 1830 60 24-11477 25 301830ND 1100 1410Biphenyl (Diphenyl) ug/kg 1830 57 50-15062 8 301830ND 1040 1120bis(2-Chloroethoxy)methane ug/kg 1830 51 13-11962 21 301830ND 924 1140bis(2-Chloroethyl) ether ug/kg 1830 48 10-13458 20 301830ND 872 1070bis(2-Chloroisopropyl) ether ug/kg 1830 40 10-11353 28 301830ND 738 975bis(2-Ethylhexyl)phthalate ug/kg M01830 121 10-125152 23 301830ND 2200 2770Butylbenzylphthalate ug/kg 1830 49 18-11059 20 301830ND 889 1080Caprolactam ug/kg M0,M11830 56 50-15079 33 301830ND 1030 1440Carbazole ug/kg M0,

M1,R11830 47 50-15065 32 301830ND 857 1190

Chrysene ug/kg 1830 55 30-11067 19 301830ND 1000 1220Di-n-butylphthalate ug/kg 1830 44 19-11256 24 301830ND 806 1030



Date: 09/27/2010 06:48 PM Page 315 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276981018

497679

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Di-n-octylphthalate ug/kg 1830 33 17-10535 7 301830ND 595 640Dibenz(a,h)anthracene ug/kg 1830 63 23-11181 24 301830ND 1160 1470Dibenzofuran ug/kg 1830 60 35-10374 21 301830ND 1090 1350Diethylphthalate ug/kg 1830 50 27-11362 21 301830ND 919 1140Dimethylphthalate ug/kg 1830 52 26-11164 19 301830ND 956 1160Fluoranthene ug/kg 1830 57 33-10972 24 301830ND 1030 1320Fluorene ug/kg 1830 58 32-11371 19 301830ND 1060 1290Hexachloro-1,3-butadiene ug/kg 1830 50 16-11667 29 301830ND 906 1220Hexachlorobenzene ug/kg 1830 60 27-12075 21 301830ND 1100 1370Hexachlorocyclopentadiene ug/kg 1830 53 10-10866 21 301830ND 968 1200Hexachloroethane ug/kg 1830 56 10-11757 3 301830ND 1020 1050Indeno(1,2,3-cd)pyrene ug/kg 1830 60 10-12277 25 301830ND 1090 1400Isophorone ug/kg 1830 40 28-11451 24 301830ND 736 934N-Nitroso-di-n-propylamine ug/kg 1830 44 27-11349 11 301830ND 803 892N-Nitrosodiphenylamine ug/kg R11830 48 10-12867 34 301830ND 870 1220Naphthalene ug/kg 1830 46 25-11060 25 301830ND 848 1090Nitrobenzene ug/kg 1830 41 18-11453 25 301830ND 745 960Pentachlorophenol ug/kg 3640 47 10-12266 303640ND 1720J 2410Phenanthrene ug/kg 1830 57 30-11471 22 301830ND 1040 1300Phenol ug/kg R11830 46 11-10263 31 301830ND 836 1140Pyrene ug/kg R11830 51 25-11671 32 301830ND 934 12902,4,6-Tribromophenol (S) % 58 27-110792-Fluorobiphenyl (S) % 60 30-110672-Fluorophenol (S) % 48 13-11060Nitrobenzene-d5 (S) % 43 23-11055Phenol-d6 (S) % 46 22-11062Terphenyl-d14 (S) % 56 28-11072



Date: 09/27/2010 06:48 PM Page 316 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11234EPA 3546


Associated Lab Samples: 9276872050, 9276872051, 9276872058





Matrix: Solid

Analyzed




Date: 09/27/2010 06:48 PM Page 317 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS






Date: 09/27/2010 06:48 PM Page 318 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 9881670 59 39-1122-Methylphenol(o-Cresol) ug/kg 10601670 63 39-1012-Nitroaniline ug/kg 20303330 61 44-1112-Nitrophenol ug/kg 10301670 62 41-1003&4-Methylphenol(m&p Cresol) ug/kg 10601670 63 43-1033,3'-Dichlorobenzidine ug/kg 16803330 51 10-1503-Nitroaniline ug/kg 21703330 65 35-1104,6-Dinitro-2-methylphenol ug/kg 23403330 70 38-1184-Bromophenylphenyl ether ug/kg 13201670 79 47-1154-Chloro-3-methylphenol ug/kg 20303330 61 43-1274-Chloroaniline ug/kg 16903330 51 34-1094-Chlorophenylphenyl ether ug/kg 14401670 86 44-1154-Nitroaniline ug/kg 22003330 66 37-1114-Nitrophenol ug/kg 65908330 79 21-152Acenaphthene ug/kg 13101670 79 38-117Acenaphthylene ug/kg 12901670 77 46-107Acetophenone ug/kg 1080 L03330 32 39-112Anthracene ug/kg 12001670 72 50-110Atrazine ug/kg 3200 L01670 192 39-112Benzaldehyde ug/kg 6801670 41 39-112Benzo(a)anthracene ug/kg 12801670 77 47-116Benzo(a)pyrene ug/kg 11901670 71 47-106Benzo(b)fluoranthene ug/kg 13001670 78 47-109Benzo(g,h,i)perylene ug/kg 12201670 73 39-115Benzo(k)fluoranthene ug/kg 14201670 85 45-117Biphenyl (Diphenyl) ug/kg 12501670 75 39-112bis(2-Chloroethoxy)methane ug/kg 10801670 65 39-110bis(2-Chloroethyl) ether ug/kg 9841670 59 19-119bis(2-Chloroisopropyl) ether ug/kg 6811670 41 21-110bis(2-Ethylhexyl)phthalate ug/kg 2700 L01670 162 35-116Butylbenzylphthalate ug/kg 9451670 57 38-110Caprolactam ug/kg 10901670 65 39-112Carbazole ug/kg 11101670 67 39-112Chrysene ug/kg 12301670 74 49-110Di-n-butylphthalate ug/kg 9131670 55 43-109Di-n-octylphthalate ug/kg 6811670 41 37-109Dibenz(a,h)anthracene ug/kg 12201670 73 43-116Dibenzofuran ug/kg 13401670 80 45-106Diethylphthalate ug/kg 10601670 64 41-114Dimethylphthalate ug/kg 11301670 68 43-110Fluoranthene ug/kg 12401670 75 50-114Fluorene ug/kg 13301670 80 46-114Hexachloro-1,3-butadiene ug/kg 12801670 77 28-111Hexachlorobenzene ug/kg 14701670 88 46-120Hexachlorocyclopentadiene ug/kg 14701670 88 18-119Hexachloroethane ug/kg 12301670 74 33-110Indeno(1,2,3-cd)pyrene ug/kg 11901670 72 42-115Isophorone ug/kg 8251670 49 44-109



Date: 09/27/2010 06:48 PM Page 319 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9277975005

500224

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 2 30ND 1280 12602,3,4,6-Tetrachlorophenol ug/kg M0,M11810 159 50-150161 1 301810ND 2880 29102,4,5-Trichlorophenol ug/kg 1810 74 28-11076 2 301810ND 1340 13702,4,6-Trichlorophenol ug/kg 1810 77 17-11779 2 301810ND 1390 14202,4-Dichlorophenol ug/kg 1810 65 21-12864 2 301810ND 1170 11502,4-Dimethylphenol ug/kg 1810 58 10-12059 1 301810ND 1050 10602,4-Dinitrophenol ug/kg 9050 64 10-10767 4 309050ND 5780 60402,4-Dinitrotoluene ug/kg 1810 68 36-10968 0 301810ND 1240 12402,6-Dinitrotoluene ug/kg 1810 69 32-11069 0 301810ND 1250 12502-Chloronaphthalene ug/kg 1810 81 30-10781 1 301810ND 1470 14702-Chlorophenol ug/kg 1810 66 14-10659 12 301810ND 1200 10602-Methylnaphthalene ug/kg 1810 55 10-13554 1 301810ND 997 9842-Methylphenol(o-Cresol) ug/kg 1810 64 10-12460 7 301810ND 1160 10802-Nitroaniline ug/kg 3620 53 26-11654 2 303620ND 1920 19602-Nitrophenol ug/kg 1810 56 28-10354 4 301810ND 1020 9783&4-Methylphenol(m&pCresol)

ug/kg 1810 62 10-10962 1 301810ND 1130 1110

3,3'-Dichlorobenzidine ug/kg 3620 61 10-15060 2 303620ND 2210 21603-Nitroaniline ug/kg 3620 60 22-11060 0 303620ND 2160 21604,6-Dinitro-2-methylphenol ug/kg 3620 64 13-12165 2 303620ND 2330 23604-Bromophenylphenyl ether ug/kg 1810 71 31-10973 2 301810ND 1290 13104-Chloro-3-methylphenol ug/kg 3620 57 13-12858 2 303620ND 2050 20904-Chloroaniline ug/kg 3620 51 18-10249 303620ND 1850 1760J4-Chlorophenylphenyl ether ug/kg 1810 77 29-11276 1 301810ND 1390 13804-Nitroaniline ug/kg 3620 61 16-11160 1 303620ND 2200 21904-Nitrophenol ug/kg 9050 71 14-13572 2 309050ND 6400 6540Acenaphthene ug/kg 1810 70 26-11470 0 301810ND 1270 1280Acenaphthylene ug/kg 1810 69 32-10870 1 301810ND 1260 1260



Date: 09/27/2010 06:48 PM Page 320 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9277975005

500224

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg M0,M13620 31 50-15029 9 303620ND 1130 1030Anthracene ug/kg 1810 65 32-11165 1 301810ND 1170 1180Atrazine ug/kg 1810 99 50-150100 1 301810ND 1790 1810Benzaldehyde ug/kg M0,

M1,R11810 49 50-15067 31 301810ND 894 1220

Benzo(a)anthracene ug/kg 1810 65 25-11764 1 301810ND 1180 1170Benzo(a)pyrene ug/kg 1810 61 25-10663 3 301810ND 1110 1140Benzo(b)fluoranthene ug/kg 1810 64 24-11064 0 301810ND 1150 1150Benzo(g,h,i)perylene ug/kg 1810 74 19-11274 1 301810ND 1330 1350Benzo(k)fluoranthene ug/kg 1810 69 24-11471 4 301810ND 1240 1290Biphenyl (Diphenyl) ug/kg 1810 67 50-15067 1 301810ND 1220 1210bis(2-Chloroethoxy)methane ug/kg 1810 61 13-11957 6 301810ND 1110 1040bis(2-Chloroethyl) ether ug/kg 1810 58 10-13449 16 301810ND 1040 886bis(2-Chloroisopropyl) ether ug/kg 1810 40 10-11334 16 301810ND 723 615bis(2-Ethylhexyl)phthalate ug/kg R11810 125 10-12543 98 301810ND 2270 776Butylbenzylphthalate ug/kg 1810 45 18-11045 0 301810ND 808 810Caprolactam ug/kg 1810 71 50-15071 1 301810ND 1280 1290Carbazole ug/kg 1810 62 50-15063 1 301810ND 1130 1140Chrysene ug/kg 1810 64 30-11065 2 301810ND 1150 1180Di-n-butylphthalate ug/kg 1810 49 19-11250 1 301810ND 887 897Di-n-octylphthalate ug/kg 1810 38 17-10538 1 301810ND 688 683Dibenz(a,h)anthracene ug/kg 1810 72 23-11175 4 301810ND 1300 1350Dibenzofuran ug/kg 1810 72 35-10372 1 301810ND 1300 1310Diethylphthalate ug/kg 1810 59 27-11359 0 301810ND 1060 1060Dimethylphthalate ug/kg 1810 62 26-11162 0 301810ND 1120 1130Fluoranthene ug/kg 1810 68 33-10968 0 301810ND 1230 1230Fluorene ug/kg 1810 71 32-11371 1 301810ND 1290 1280Hexachloro-1,3-butadiene ug/kg 1810 68 16-11660 14 301810ND 1240 1080Hexachlorobenzene ug/kg 1810 78 27-12080 2 301810ND 1420 1450Hexachlorocyclopentadiene ug/kg 1810 75 10-10872 4 301810ND 1360 1300Hexachloroethane ug/kg 1810 70 10-11758 20 301810ND 1270 1040Indeno(1,2,3-cd)pyrene ug/kg 1810 71 10-12273 3 301810ND 1280 1320Isophorone ug/kg 1810 46 28-11447 2 301810ND 828 843N-Nitroso-di-n-propylamine ug/kg 1810 54 27-11350 7 301810ND 972 906N-Nitrosodiphenylamine ug/kg 1810 63 10-12865 2 301810ND 1150 1170Naphthalene ug/kg 1810 59 25-11055 7 301810ND 1070 990Nitrobenzene ug/kg 1810 48 18-11445 7 301810ND 869 808Pentachlorophenol ug/kg 3620 80 10-12282 2 303620ND 2900 2970Phenanthrene ug/kg 1810 66 30-11466 1 301810ND 1190 1200Phenol ug/kg 1810 61 11-10257 7 301810ND 1100 1030Pyrene ug/kg 1810 62 25-11663 2 301810ND 1120 11302,4,6-Tribromophenol (S) % 85 27-110842-Fluorobiphenyl (S) % 68 30-110652-Fluorophenol (S) % 59 13-11049Nitrobenzene-d5 (S) % 49 23-11045Phenol-d6 (S) % 57 22-11052Terphenyl-d14 (S) % 58 28-11056



Date: 09/27/2010 06:48 PM Page 321 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11277EPA 3546







Matrix: Solid

Analyzed




Date: 09/27/2010 06:48 PM Page 322 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS






Date: 09/27/2010 06:48 PM Page 323 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/kg 11101670 67 39-1122-Methylphenol(o-Cresol) ug/kg 11601670 70 39-1012-Nitroaniline ug/kg 21603330 65 44-1112-Nitrophenol ug/kg 11201670 67 41-1003&4-Methylphenol(m&p Cresol) ug/kg 11801670 71 43-1033,3'-Dichlorobenzidine ug/kg 23903330 72 10-1503-Nitroaniline ug/kg 24103330 72 35-1104,6-Dinitro-2-methylphenol ug/kg 26403330 79 38-1184-Bromophenylphenyl ether ug/kg 15201670 91 47-1154-Chloro-3-methylphenol ug/kg 22403330 67 43-1274-Chloroaniline ug/kg 19503330 59 34-1094-Chlorophenylphenyl ether ug/kg 16001670 96 44-1154-Nitroaniline ug/kg 25403330 76 37-1114-Nitrophenol ug/kg 73408330 88 21-152Acenaphthene ug/kg 14301670 86 38-117Acenaphthylene ug/kg 14301670 86 46-107Acetophenone ug/kg 1190 L03330 36 39-112Anthracene ug/kg 13701670 82 50-110Atrazine ug/kg 3680 L01670 221 39-112Benzaldehyde ug/kg 8981670 54 39-112Benzo(a)anthracene ug/kg 13701670 82 47-116Benzo(a)pyrene ug/kg 13301670 80 47-106Benzo(b)fluoranthene ug/kg 14101670 85 47-109Benzo(g,h,i)perylene ug/kg 15701670 94 39-115Benzo(k)fluoranthene ug/kg 14701670 88 45-117Biphenyl (Diphenyl) ug/kg 13401670 80 39-112bis(2-Chloroethoxy)methane ug/kg 11701670 70 39-110bis(2-Chloroethyl) ether ug/kg 10301670 62 19-119bis(2-Chloroisopropyl) ether ug/kg 7271670 44 21-110bis(2-Ethylhexyl)phthalate ug/kg 8671670 52 35-116Butylbenzylphthalate ug/kg 9501670 57 38-110Caprolactam ug/kg 13701670 82 39-112Carbazole ug/kg 13101670 78 39-112Chrysene ug/kg 13801670 83 49-110Di-n-butylphthalate ug/kg 10401670 62 43-109Di-n-octylphthalate ug/kg 7691670 46 37-109Dibenz(a,h)anthracene ug/kg 15501670 93 43-116Dibenzofuran ug/kg 14801670 89 45-106Diethylphthalate ug/kg 12201670 73 41-114Dimethylphthalate ug/kg 12701670 76 43-110Fluoranthene ug/kg 14501670 87 50-114Fluorene ug/kg 14801670 89 46-114Hexachloro-1,3-butadiene ug/kg 13501670 81 28-111Hexachlorobenzene ug/kg 16801670 101 46-120Hexachlorocyclopentadiene ug/kg 14501670 87 18-119Hexachloroethane ug/kg 12801670 77 33-110Indeno(1,2,3-cd)pyrene ug/kg 15501670 93 42-115Isophorone ug/kg 8961670 54 44-109



Date: 09/27/2010 06:48 PM Page 324 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9278153009

502118

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/kg 4 30ND 1610 15402,3,4,6-Tetrachlorophenol ug/kg M01910 191 50-150193 1 301910ND 3640 36902,4,5-Trichlorophenol ug/kg 1910 87 28-11090 3 301910ND 1670 17202,4,6-Trichlorophenol ug/kg 1910 95 17-11794 1 301910ND 1810 17902,4-Dichlorophenol ug/kg 1910 70 21-12872 3 301910ND 1340 13802,4-Dimethylphenol ug/kg 1910 66 10-12066 0 301910ND 1250 12602,4-Dinitrophenol ug/kg 9540 61 10-10767 10 309540ND 5790 63802,4-Dinitrotoluene ug/kg 1910 81 36-10982 1 301910ND 1550 15602,6-Dinitrotoluene ug/kg 1910 82 32-11081 1 301910ND 1560 15502-Chloronaphthalene ug/kg 1910 98 30-10795 3 301910ND 1870 18202-Chlorophenol ug/kg 1910 73 14-10668 7 301910ND 1400 13002-Methylnaphthalene ug/kg 1910 65 10-13563 3 301910ND 1240 12002-Methylphenol(o-Cresol) ug/kg 1910 71 10-12467 6 301910ND 1360 12902-Nitroaniline ug/kg 3810 63 26-11662 2 303810ND 2390 23502-Nitrophenol ug/kg 1910 61 28-10362 1 301910ND 1170 11903&4-Methylphenol(m&pCresol)

ug/kg 1910 72 10-10969 5 301910ND 1380 1310

3,3'-Dichlorobenzidine ug/kg 3810 67 10-15069 3 303810ND 2550 26203-Nitroaniline ug/kg 3810 62 22-11066 6 303810ND 2370 25004,6-Dinitro-2-methylphenol ug/kg 3810 72 13-12176 5 303810ND 2750 28904-Bromophenylphenyl ether ug/kg 1910 87 31-10983 4 301910ND 1660 15904-Chloro-3-methylphenol ug/kg 3810 68 13-12866 2 303810ND 2580 25304-Chloroaniline ug/kg 3810 53 18-10255 3 303810ND 2030 21004-Chlorophenylphenyl ether ug/kg 1910 93 29-11289 4 301910ND 1770 17004-Nitroaniline ug/kg 3810 64 16-11168 6 303810ND 2440 25904-Nitrophenol ug/kg 9540 73 14-13577 5 309540ND 7010 7350Acenaphthene ug/kg 1910 85 26-11483 2 301910ND 1620 1590Acenaphthylene ug/kg 1910 83 32-10882 1 301910ND 1580 1560



Date: 09/27/2010 06:48 PM Page 325 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9278153009

502118

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Acetophenone ug/kg M03810 36 50-15034 4 303810ND 1360 1300Anthracene ug/kg 1910 78 32-11177 2 301910ND 1490 1460Atrazine ug/kg 1910 137 50-150103 28 301910ND 2610 1970Benzaldehyde ug/kg 1910 95 50-15083 14 301910ND 1810 1580Benzo(a)anthracene ug/kg 1910 78 25-11774 4 301910ND 1480 1420Benzo(a)pyrene ug/kg 1910 76 25-10675 2 301910ND 1460 1430Benzo(b)fluoranthene ug/kg 1910 82 24-11077 6 301910ND 1570 1470Benzo(g,h,i)perylene ug/kg 1910 92 19-11287 6 301910ND 1770 1670Benzo(k)fluoranthene ug/kg 1910 82 24-11483 1 301910ND 1570 1580Biphenyl (Diphenyl) ug/kg 1910 81 50-15078 3 301910ND 1540 1490bis(2-Chloroethoxy)methane ug/kg 1910 67 13-11966 2 301910ND 1290 1270bis(2-Chloroethyl) ether ug/kg 1910 64 10-13458 10 301910ND 1220 1100bis(2-Chloroisopropyl) ether ug/kg 1910 44 10-11340 10 301910ND 849 770bis(2-Ethylhexyl)phthalate ug/kg 1910 50 10-12548 3 301910ND 947 917Butylbenzylphthalate ug/kg 1910 53 18-11052 2 301910ND 1010 990Caprolactam ug/kg 1910 74 50-15074 1 30191093.8J 1520 1500Carbazole ug/kg 1910 74 50-15075 2 301910ND 1410 1430Chrysene ug/kg 1910 78 30-11074 5 301910ND 1490 1420Di-n-butylphthalate ug/kg 1910 59 19-11258 3 301910ND 1130 1100Di-n-octylphthalate ug/kg 1910 45 17-10544 2 301910ND 854 836Dibenz(a,h)anthracene ug/kg 1910 91 23-11187 5 301910ND 1740 1650Dibenzofuran ug/kg 1910 87 35-10385 3 301910ND 1670 1630Diethylphthalate ug/kg 1910 72 27-11372 0 301910ND 1370 1370Dimethylphthalate ug/kg 1910 75 26-11175 0 301910ND 1430 1440Fluoranthene ug/kg 1910 81 33-10980 1 301910ND 1550 1540Fluorene ug/kg 1910 86 32-11384 3 301910ND 1640 1600Hexachloro-1,3-butadiene ug/kg 1910 77 16-11672 6 301910ND 1460 1380Hexachlorobenzene ug/kg 1910 96 27-12093 3 301910ND 1830 1780Hexachlorocyclopentadiene ug/kg 1910 96 10-10895 2 301910ND 1840 1800Hexachloroethane ug/kg 1910 78 10-11770 11 301910ND 1500 1340Indeno(1,2,3-cd)pyrene ug/kg 1910 90 10-12286 4 301910ND 1710 1640Isophorone ug/kg 1910 53 28-11453 0 301910ND 1010 1010N-Nitroso-di-n-propylamine ug/kg 1910 61 27-11357 6 301910ND 1160 1090N-Nitrosodiphenylamine ug/kg 1910 76 10-12875 0 301910ND 1440 1440Naphthalene ug/kg 1910 67 25-11066 1 301910ND 1280 1260Nitrobenzene ug/kg 1910 53 18-11452 1 301910ND 1010 999Pentachlorophenol ug/kg 3810 96 10-12298 2 303810ND 3680 3750Phenanthrene ug/kg 1910 79 30-11478 1 301910ND 1500 1480Phenol ug/kg 1910 69 11-10265 7 301910ND 1330 1240Pyrene ug/kg 1910 74 25-11672 3 301910ND 1420 13702,4,6-Tribromophenol (S) % 101 27-1101012-Fluorobiphenyl (S) % 81 30-110772-Fluorophenol (S) % 65 13-11060Nitrobenzene-d5 (S) % 52 23-11052Phenol-d6 (S) % 63 22-11060Terphenyl-d14 (S) % 70 28-11066



Date: 09/27/2010 06:48 PM Page 326 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



OEXT/11099EPA 3510

EPA 82708270 Water MSSV






Matrix: Water

Analyzed

1,2,4,5-Tetrachlorobenzene ug/L ND 10.0 09/24/10 18:372,3,4,6-Tetrachlorophenol ug/L ND 10.0 09/24/10 18:372,4,5-Trichlorophenol ug/L ND 10.0 09/24/10 18:372,4,6-Trichlorophenol ug/L ND 10.0 09/24/10 18:372,4-Dichlorophenol ug/L ND 10.0 09/24/10 18:372,4-Dimethylphenol ug/L ND 10.0 09/24/10 18:372,4-Dinitrophenol ug/L ND 50.0 09/24/10 18:372,4-Dinitrotoluene ug/L ND 10.0 09/24/10 18:372,6-Dinitrotoluene ug/L ND 10.0 09/24/10 18:372-Chloronaphthalene ug/L ND 10.0 09/24/10 18:372-Chlorophenol ug/L ND 10.0 09/24/10 18:372-Methylnaphthalene ug/L ND 10.0 09/24/10 18:372-Methylphenol(o-Cresol) ug/L ND 10.0 09/24/10 18:372-Nitroaniline ug/L ND 50.0 09/24/10 18:372-Nitrophenol ug/L ND 10.0 09/24/10 18:373&4-Methylphenol(m&p Cresol) ug/L ND 10.0 09/24/10 18:373,3'-Dichlorobenzidine ug/L ND 20.0 09/24/10 18:373-Nitroaniline ug/L ND 50.0 09/24/10 18:374,6-Dinitro-2-methylphenol ug/L ND 20.0 09/24/10 18:374-Bromophenylphenyl ether ug/L ND 10.0 09/24/10 18:374-Chloro-3-methylphenol ug/L ND 20.0 09/24/10 18:374-Chloroaniline ug/L ND 20.0 09/24/10 18:374-Chlorophenylphenyl ether ug/L ND 10.0 09/24/10 18:374-Nitroaniline ug/L ND 20.0 09/24/10 18:374-Nitrophenol ug/L ND 50.0 09/24/10 18:37Acenaphthene ug/L ND 10.0 09/24/10 18:37Acenaphthylene ug/L ND 10.0 09/24/10 18:37Acetophenone ug/L ND 10.0 09/24/10 18:37Anthracene ug/L ND 10.0 09/24/10 18:37Atrazine ug/L ND 20.0 09/24/10 18:37Benzaldehyde ug/L ND 20.0 09/24/10 18:37Benzo(a)anthracene ug/L ND 10.0 09/24/10 18:37Benzo(a)pyrene ug/L ND 10.0 09/24/10 18:37Benzo(b)fluoranthene ug/L ND 10.0 09/24/10 18:37Benzo(g,h,i)perylene ug/L ND 10.0 09/24/10 18:37Benzo(k)fluoranthene ug/L ND 10.0 09/24/10 18:37Biphenyl (Diphenyl) ug/L ND 10.0 09/24/10 18:37bis(2-Chloroethoxy)methane ug/L ND 10.0 09/24/10 18:37bis(2-Chloroethyl) ether ug/L ND 10.0 09/24/10 18:37bis(2-Chloroisopropyl) ether ug/L ND 10.0 09/24/10 18:37bis(2-Ethylhexyl)phthalate ug/L ND 6.0 09/24/10 18:37Butylbenzylphthalate ug/L ND 10.0 09/24/10 18:37Caprolactam ug/L ND 10.0 09/24/10 18:37



Date: 09/27/2010 06:48 PM Page 327 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Water

Analyzed

Carbazole ug/L ND 10.0 09/24/10 18:37Chrysene ug/L ND 10.0 09/24/10 18:37Di-n-butylphthalate ug/L ND 10.0 09/24/10 18:37Di-n-octylphthalate ug/L ND 10.0 09/24/10 18:37Dibenz(a,h)anthracene ug/L ND 10.0 09/24/10 18:37Dibenzofuran ug/L ND 10.0 09/24/10 18:37Diethylphthalate ug/L ND 10.0 09/24/10 18:37Dimethylphthalate ug/L ND 10.0 09/24/10 18:37Fluoranthene ug/L ND 10.0 09/24/10 18:37Fluorene ug/L ND 10.0 09/24/10 18:37Hexachloro-1,3-butadiene ug/L ND 10.0 09/24/10 18:37Hexachlorobenzene ug/L ND 10.0 09/24/10 18:37Hexachlorocyclopentadiene ug/L ND 10.0 09/24/10 18:37Hexachloroethane ug/L ND 10.0 09/24/10 18:37Indeno(1,2,3-cd)pyrene ug/L ND 10.0 09/24/10 18:37Isophorone ug/L ND 10.0 09/24/10 18:37N-Nitroso-di-n-propylamine ug/L ND 10.0 09/24/10 18:37N-Nitrosodiphenylamine ug/L ND 10.0 09/24/10 18:37Naphthalene ug/L ND 10.0 09/24/10 18:37Nitrobenzene ug/L ND 10.0 09/24/10 18:37Pentachlorophenol ug/L ND 25.0 09/24/10 18:37Phenanthrene ug/L ND 10.0 09/24/10 18:37Phenol ug/L ND 10.0 09/24/10 18:37Pyrene ug/L ND 10.0 09/24/10 18:372,4,6-Tribromophenol (S) % 84 27-110 09/24/10 18:372-Fluorobiphenyl (S) % 65 27-110 09/24/10 18:372-Fluorophenol (S) % 29 12-110 09/24/10 18:37Nitrobenzene-d5 (S) % 52 21-110 09/24/10 18:37Phenol-d6 (S) % 17 10-110 09/24/10 18:37Terphenyl-d14 (S) % 80 31-107 09/24/10 18:37

Parameter UnitsLCS



1,2,4,5-Tetrachlorobenzene ug/L 32.350 65 17-1152,3,4,6-Tetrachlorophenol ug/L 84.9 L050 170 17-1152,4,5-Trichlorophenol ug/L 42.250 84 23-1162,4,6-Trichlorophenol ug/L 43.450 87 21-1142,4-Dichlorophenol ug/L 33.750 67 22-1202,4-Dimethylphenol ug/L 28.550 57 15-1092,4-Dinitrophenol ug/L 95.2250 38 10-1032,4-Dinitrotoluene ug/L 39.950 80 24-1192,6-Dinitrotoluene ug/L 40.450 81 25-1162-Chloronaphthalene ug/L 42.950 86 18-1102-Chlorophenol ug/L 31.150 62 10-104



Date: 09/27/2010 06:48 PM Page 328 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



2-Methylnaphthalene ug/L 27.250 54 16-1102-Methylphenol(o-Cresol) ug/L 26.550 53 13-1102-Nitroaniline ug/L 61.3250 25 20-1172-Nitrophenol ug/L 30.850 62 16-1083&4-Methylphenol(m&p Cresol) ug/L 24.650 49 14-1103,3'-Dichlorobenzidine ug/L 57.1250 23 13-1313-Nitroaniline ug/L 67.2250 27 15-1174,6-Dinitro-2-methylphenol ug/L 64.7100 65 13-1194-Bromophenylphenyl ether ug/L 40.550 81 23-1204-Chloro-3-methylphenol ug/L 58.4100 58 21-1194-Chloroaniline ug/L 55.8250 22 10-1224-Chlorophenylphenyl ether ug/L 43.750 87 22-1124-Nitroaniline ug/L 64.8250 26 14-1184-Nitrophenol ug/L 76.9250 31 10-110Acenaphthene ug/L 38.350 77 20-105Acenaphthylene ug/L 37.550 75 23-106Acetophenone ug/L 32.550 65 17-115Anthracene ug/L 35.750 71 25-120Atrazine ug/L 85.0 L050 170 17-115Benzaldehyde ug/L ND50 22 17-115Benzo(a)anthracene ug/L 40.150 80 21-128Benzo(a)pyrene ug/L 36.350 73 25-116Benzo(b)fluoranthene ug/L 37.850 76 23-117Benzo(g,h,i)perylene ug/L 40.150 80 17-128Benzo(k)fluoranthene ug/L 41.350 83 25-127Biphenyl (Diphenyl) ug/L 35.350 71 17-115bis(2-Chloroethoxy)methane ug/L 32.250 64 19-107bis(2-Chloroethyl) ether ug/L 28.850 58 10-108bis(2-Chloroisopropyl) ether ug/L 19.750 39 10-108Butylbenzylphthalate ug/L 28.850 58 20-118Caprolactam ug/L 10.450 21 17-115Carbazole ug/L 35.350 71 17-115Chrysene ug/L 35.250 70 24-125Di-n-butylphthalate ug/L 30.950 62 23-115Di-n-octylphthalate ug/L 22.750 45 20-115Dibenz(a,h)anthracene ug/L 40.250 80 18-131Dibenzofuran ug/L 39.750 79 23-106Diethylphthalate ug/L 36.050 72 24-115Dimethylphthalate ug/L 37.550 75 22-113Fluoranthene ug/L 37.450 75 24-125Fluorene ug/L 39.750 79 24-114Hexachloro-1,3-butadiene ug/L 24.750 49 10-110Hexachlorobenzene ug/L 45.250 90 22-127Hexachlorocyclopentadiene ug/L 36.650 73 10-110Hexachloroethane ug/L 22.050 44 10-110Indeno(1,2,3-cd)pyrene ug/L 39.550 79 18-130Isophorone ug/L 25.550 51 23-114N-Nitroso-di-n-propylamine ug/L 25.550 51 21-114



Date: 09/27/2010 06:48 PM Page 329 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



N-Nitrosodiphenylamine ug/L 34.350 69 24-123Naphthalene ug/L 27.850 56 14-110Nitrobenzene ug/L 27.750 55 16-106Pentachlorophenol ug/L 70.9250 28 10-123Phenanthrene ug/L 36.250 72 25-119Phenol ug/L 14.350 29 10-110Pyrene ug/L 39.350 79 22-1272,4,6-Tribromophenol (S) % 95 27-1102-Fluorobiphenyl (S) % 80 27-1102-Fluorophenol (S) % 36 12-110Nitrobenzene-d5 (S) % 53 21-110Phenol-d6 (S) % 23 10-110Terphenyl-d14 (S) % 83 31-107

Parameter UnitsMS



MSSpikeResult

9276872093

494468

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,2,4,5-Tetrachlorobenzene ug/L 100 76 50-15079 4 30100ND 75.9 79.02,3,4,6-Tetrachlorophenol ug/L M0,M1100 189 50-150185 2 30100ND 189 1852,4,5-Trichlorophenol ug/L 100 89 19-10587 3 30100ND 89.4 86.52,4,6-Trichlorophenol ug/L 100 93 13-10894 1 30100ND 92.5 93.72,4-Dichlorophenol ug/L 100 69 29-11170 2 30100ND 69.0 70.42,4-Dimethylphenol ug/L 100 59 21-10363 7 30100ND 59.2 63.22,4-Dinitrophenol ug/L 500 85 10-10983 3 30500ND 424 4132,4-Dinitrotoluene ug/L 100 86 27-10484 2 30100ND 86.2 84.42,6-Dinitrotoluene ug/L 100 86 28-10184 2 30100ND 85.9 84.42-Chloronaphthalene ug/L 100 94 14-10297 4 30100ND 93.7 97.12-Chlorophenol ug/L 100 64 16-11065 2 30100ND 64.3 65.52-Methylnaphthalene ug/L 100 60 13-11063 4 30100ND 60.3 62.82-Methylphenol(o-Cresol) ug/L 100 60 19-11061 2 30100ND 60.2 61.22-Nitroaniline ug/L 500 27 26-10326 2 30500ND 134 1312-Nitrophenol ug/L 100 61 20-11064 4 30100ND 61.2 64.03&4-Methylphenol(m&pCresol)

ug/L 100 60 20-11061 2 30100ND 59.6 61.0

3,3'-Dichlorobenzidine ug/L M0,M1500 24 25-11224 2 30500ND 124 1213-Nitroaniline ug/L M0,M1500 29 29-11028 3 30500ND 143 1394,6-Dinitro-2-methylphenol ug/L 200 78 10-11780 2 30200ND 157 1594-Bromophenylphenyl ether ug/L 100 86 20-10586 0 30100ND 87.1 87.44-Chloro-3-methylphenol ug/L 200 65 22-11063 3 30200ND 129 1264-Chloroaniline ug/L 500 22 20-10023 2 30500ND 111 1134-Chlorophenylphenyl ether ug/L 100 94 19-10291 3 30100ND 93.9 91.24-Nitroaniline ug/L M0,M1500 30 29-11028 4 30500ND 148 1424-Nitrophenol ug/L 500 59 10-11057 4 30500ND 297 286Acenaphthene ug/L 100 83 17-10082 1 30100ND 82.6 81.9Acenaphthylene ug/L 100 79 21-10079 0 30100ND 79.3 79.4Acetophenone ug/L 100 65 50-15066 2 30100ND 65.3 66.4



Date: 09/27/2010 06:48 PM Page 330 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276872093

494468

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

Anthracene ug/L 100 77 24-10977 0 30100ND 77.1 77.1Atrazine ug/L 100 127 50-150127 0 30100ND 127 127Benzaldehyde ug/L M0,M1100 14 50-15013 30100ND ND NDBenzo(a)anthracene ug/L 100 86 22-11787 1 30100ND 85.8 86.7Benzo(a)pyrene ug/L 100 76 23-10479 5 30100ND 75.8 79.4Benzo(b)fluoranthene ug/L 100 82 23-10384 3 30100ND 81.6 83.9Benzo(g,h,i)perylene ug/L 100 81 18-11182 2 301004.1J 84.7 86.5Benzo(k)fluoranthene ug/L 100 85 22-11392 8 30100ND 84.6 91.9Biphenyl (Diphenyl) ug/L 100 78 50-15079 1 30100ND 77.6 78.8bis(2-Chloroethoxy)methane ug/L 100 65 22-11067 3 30100ND 65.2 67.0bis(2-Chloroethyl) ether ug/L 100 58 16-11058 1 30100ND 58.0 57.7bis(2-Chloroisopropyl) ether ug/L 100 40 14-11041 1 30100ND 40.3 40.8Butylbenzylphthalate ug/L 100 61 25-11060 3 30100ND 61.4 59.9Caprolactam ug/L M0,M1100 34 50-15033 3 30100ND 33.9 32.7Carbazole ug/L 100 76 50-15076 1 30100ND 75.6 76.0Chrysene ug/L 100 77 23-11576 1 30100ND 77.0 76.2Di-n-butylphthalate ug/L 100 66 26-11065 1 30100ND 65.5 65.1Di-n-octylphthalate ug/L 100 49 22-11048 1 30100ND 48.9 48.5Dibenz(a,h)anthracene ug/L 100 82 21-11284 2 301003.7J 85.2 87.3Dibenzofuran ug/L 100 85 19-10284 1 30100ND 85.3 84.3Diethylphthalate ug/L 100 77 29-11075 2 30100ND 76.8 74.9Dimethylphthalate ug/L 100 81 27-11079 2 30100ND 80.7 78.8Fluoranthene ug/L 100 82 23-11281 0 30100ND 81.7 81.3Fluorene ug/L 100 85 22-10484 2 30100ND 85.1 83.7Hexachloro-1,3-butadiene ug/L 100 60 10-11065 9 30100ND 59.5 65.2Hexachlorobenzene ug/L 100 98 21-11697 1 30100ND 98.3 97.1Hexachlorocyclopentadiene ug/L 100 86 10-11093 8 30100ND 86.1 92.9Hexachloroethane ug/L 100 55 10-11056 2 30100ND 55.1 56.4Indeno(1,2,3-cd)pyrene ug/L 100 80 20-11381 1 301003.5J 83.6 84.6Isophorone ug/L 100 53 50-15053 1 30100ND 52.9 53.2N-Nitroso-di-n-propylamine ug/L 100 53 21-10553 0 30100ND 52.9 53.0N-Nitrosodiphenylamine ug/L 100 74 23-10774 0 30100ND 74.0 74.1Naphthalene ug/L 100 59 10-11062 5 30100ND 58.8 61.5Nitrobenzene ug/L 100 54 20-11056 3 30100ND 54.0 55.5Pentachlorophenol ug/L 500 38 10-11838 1 30500ND 190 189Phenanthrene ug/L 100 79 24-10678 1 30100ND 78.8 78.2Phenol ug/L 100 41 12-11041 1 30100ND 41.4 41.0Pyrene ug/L 100 84 24-11482 2 30100ND 84.2 82.12,4,6-Tribromophenol (S) % 104 27-1101022-Fluorobiphenyl (S) % 83 27-110832-Fluorophenol (S) % 47 12-11047Nitrobenzene-d5 (S) % 52 21-11055Phenol-d6 (S) % 36 10-11036Terphenyl-d14 (S) % 87 31-10786



Date: 09/27/2010 06:48 PM Page 331 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12147EPA 8260

EPA 82608260 MSV Low Level






Matrix: Water

Analyzed

1,1,1-Trichloroethane ug/L ND 1.0 09/07/10 23:471,1,2,2-Tetrachloroethane ug/L ND 1.0 09/07/10 23:471,1,2-Trichloroethane ug/L ND 1.0 09/07/10 23:471,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/07/10 23:471,1-Dichloroethane ug/L ND 1.0 09/07/10 23:471,1-Dichloroethene ug/L ND 1.0 09/07/10 23:471,2,3-Trichlorobenzene ug/L 0.44J 1.0 09/07/10 23:471,2,4-Trichlorobenzene ug/L ND 1.0 09/07/10 23:471,2-Dibromo-3-chloropropane ug/L ND 5.0 09/07/10 23:471,2-Dibromoethane (EDB) ug/L ND 1.0 09/07/10 23:471,2-Dichlorobenzene ug/L ND 1.0 09/07/10 23:471,2-Dichloroethane ug/L ND 1.0 09/07/10 23:471,2-Dichloropropane ug/L ND 1.0 09/07/10 23:471,3-Dichlorobenzene ug/L ND 1.0 09/07/10 23:471,4-Dichlorobenzene ug/L ND 1.0 09/07/10 23:472-Butanone (MEK) ug/L ND 5.0 09/07/10 23:472-Hexanone ug/L ND 5.0 09/07/10 23:474-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/07/10 23:47Acetone ug/L ND 25.0 09/07/10 23:47Benzene ug/L ND 1.0 09/07/10 23:47Bromochloromethane ug/L ND 1.0 09/07/10 23:47Bromodichloromethane ug/L ND 1.0 09/07/10 23:47Bromoform ug/L ND 1.0 09/07/10 23:47Bromomethane ug/L ND 2.0 09/07/10 23:47Carbon disulfide ug/L ND 2.0 09/07/10 23:47Carbon tetrachloride ug/L ND 1.0 09/07/10 23:47Chlorobenzene ug/L ND 1.0 09/07/10 23:47Chloroethane ug/L ND 1.0 09/07/10 23:47Chloroform ug/L ND 1.0 09/07/10 23:47Chloromethane ug/L ND 1.0 09/07/10 23:47cis-1,2-Dichloroethene ug/L ND 1.0 09/07/10 23:47cis-1,3-Dichloropropene ug/L ND 1.0 09/07/10 23:47Cyclohexane ug/L ND 1.0 09/07/10 23:47Dibromochloromethane ug/L ND 1.0 09/07/10 23:47Dichlorodifluoromethane ug/L ND 1.0 09/07/10 23:47Ethylbenzene ug/L ND 1.0 09/07/10 23:47Isopropylbenzene (Cumene) ug/L ND 1.0 09/07/10 23:47m&p-Xylene ug/L ND 2.0 09/07/10 23:47Methyl acetate ug/L ND 10.0 09/07/10 23:47Methyl-tert-butyl ether ug/L ND 1.0 09/07/10 23:47Methylcyclohexane ug/L ND 10.0 09/07/10 23:47Methylene Chloride ug/L ND 2.0 09/07/10 23:47o-Xylene ug/L ND 1.0 09/07/10 23:47



Date: 09/27/2010 06:48 PM Page 332 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Water

Analyzed

Styrene ug/L ND 1.0 09/07/10 23:47Tetrachloroethene ug/L ND 1.0 09/07/10 23:47Toluene ug/L ND 1.0 09/07/10 23:47trans-1,2-Dichloroethene ug/L ND 1.0 09/07/10 23:47trans-1,3-Dichloropropene ug/L ND 1.0 09/07/10 23:47Trichloroethene ug/L ND 1.0 09/07/10 23:47Trichlorofluoromethane ug/L ND 1.0 09/07/10 23:47Vinyl chloride ug/L ND 1.0 09/07/10 23:47Xylene (Total) ug/L ND 2.0 09/07/10 23:471,2-Dichloroethane-d4 (S) % 112 70-130 09/07/10 23:474-Bromofluorobenzene (S) % 103 70-130 09/07/10 23:47Dibromofluoromethane (S) % 108 70-130 09/07/10 23:47Toluene-d8 (S) % 98 70-130 09/07/10 23:47





Matrix: Water

Analyzed

1,1,1-Trichloroethane ug/L ND 1.0 09/08/10 11:541,1,2,2-Tetrachloroethane ug/L ND 1.0 09/08/10 11:541,1,2-Trichloroethane ug/L ND 1.0 09/08/10 11:541,1,2-Trichlorotrifluoroethane ug/L ND 1.0 09/08/10 11:541,1-Dichloroethane ug/L ND 1.0 09/08/10 11:541,1-Dichloroethene ug/L ND 1.0 09/08/10 11:541,2,3-Trichlorobenzene ug/L ND 1.0 09/08/10 11:541,2,4-Trichlorobenzene ug/L ND 1.0 09/08/10 11:541,2-Dibromo-3-chloropropane ug/L ND 5.0 09/08/10 11:541,2-Dibromoethane (EDB) ug/L ND 1.0 09/08/10 11:541,2-Dichlorobenzene ug/L ND 1.0 09/08/10 11:541,2-Dichloroethane ug/L ND 1.0 09/08/10 11:541,2-Dichloropropane ug/L ND 1.0 09/08/10 11:541,3-Dichlorobenzene ug/L ND 1.0 09/08/10 11:541,4-Dichlorobenzene ug/L ND 1.0 09/08/10 11:542-Butanone (MEK) ug/L ND 5.0 09/08/10 11:542-Hexanone ug/L ND 5.0 09/08/10 11:544-Methyl-2-pentanone (MIBK) ug/L ND 5.0 09/08/10 11:54Acetone ug/L ND 25.0 09/08/10 11:54Benzene ug/L ND 1.0 09/08/10 11:54Bromochloromethane ug/L ND 1.0 09/08/10 11:54Bromodichloromethane ug/L ND 1.0 09/08/10 11:54Bromoform ug/L ND 1.0 09/08/10 11:54Bromomethane ug/L ND 2.0 09/08/10 11:54Carbon disulfide ug/L ND 2.0 09/08/10 11:54Carbon tetrachloride ug/L ND 1.0 09/08/10 11:54Chlorobenzene ug/L ND 1.0 09/08/10 11:54



Date: 09/27/2010 06:48 PM Page 333 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Water

Analyzed

Chloroethane ug/L ND 1.0 09/08/10 11:54Chloroform ug/L ND 1.0 09/08/10 11:54Chloromethane ug/L ND 1.0 09/08/10 11:54cis-1,2-Dichloroethene ug/L ND 1.0 09/08/10 11:54cis-1,3-Dichloropropene ug/L ND 1.0 09/08/10 11:54Cyclohexane ug/L ND 1.0 09/08/10 11:54Dibromochloromethane ug/L ND 1.0 09/08/10 11:54Dichlorodifluoromethane ug/L ND 1.0 09/08/10 11:54Ethylbenzene ug/L ND 1.0 09/08/10 11:54Isopropylbenzene (Cumene) ug/L ND 1.0 09/08/10 11:54m&p-Xylene ug/L ND 2.0 09/08/10 11:54Methyl acetate ug/L ND 10.0 09/08/10 11:54Methyl-tert-butyl ether ug/L ND 1.0 09/08/10 11:54Methylcyclohexane ug/L ND 10.0 09/08/10 11:54Methylene Chloride ug/L ND 2.0 09/08/10 11:54o-Xylene ug/L ND 1.0 09/08/10 11:54Styrene ug/L ND 1.0 09/08/10 11:54Tetrachloroethene ug/L ND 1.0 09/08/10 11:54Toluene ug/L ND 1.0 09/08/10 11:54trans-1,2-Dichloroethene ug/L ND 1.0 09/08/10 11:54trans-1,3-Dichloropropene ug/L ND 1.0 09/08/10 11:54Trichloroethene ug/L ND 1.0 09/08/10 11:54Trichlorofluoromethane ug/L ND 1.0 09/08/10 11:54Vinyl chloride ug/L ND 1.0 09/08/10 11:54Xylene (Total) ug/L ND 2.0 09/08/10 11:541,2-Dichloroethane-d4 (S) % 95 70-130 09/08/10 11:544-Bromofluorobenzene (S) % 99 70-130 09/08/10 11:54Dibromofluoromethane (S) % 99 70-130 09/08/10 11:54Toluene-d8 (S) % 100 70-130 09/08/10 11:54

Parameter UnitsLCS



1,1,1-Trichloroethane ug/L 50.550 101 70-1301,1,2,2-Tetrachloroethane ug/L 51.350 103 70-1301,1,2-Trichloroethane ug/L 51.650 103 70-1301,1,2-Trichlorotrifluoroethane ug/L 50.850 102 70-1301,1-Dichloroethane ug/L 49.850 100 70-1301,1-Dichloroethene ug/L 53.050 106 70-1321,2,3-Trichlorobenzene ug/L 52.350 105 70-1351,2,4-Trichlorobenzene ug/L 53.450 107 70-1341,2-Dibromo-3-chloropropane ug/L 53.350 107 70-1301,2-Dibromoethane (EDB) ug/L 52.250 104 70-1301,2-Dichlorobenzene ug/L 50.450 101 70-1301,2-Dichloroethane ug/L 51.250 102 70-130



Date: 09/27/2010 06:48 PM Page 334 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



1,2-Dichloropropane ug/L 47.250 94 70-1301,3-Dichlorobenzene ug/L 50.050 100 70-1301,4-Dichlorobenzene ug/L 49.050 98 70-1302-Butanone (MEK) ug/L 93.6100 94 70-1452-Hexanone ug/L 108100 108 70-1444-Methyl-2-pentanone (MIBK) ug/L 108100 108 70-140Acetone ug/L 102100 102 50-175Benzene ug/L 50.250 100 70-130Bromochloromethane ug/L 50.050 100 70-130Bromodichloromethane ug/L 50.750 101 70-130Bromoform ug/L 53.350 107 70-130Bromomethane ug/L 55.550 111 54-130Carbon disulfide ug/L 52.450 105 70-131Carbon tetrachloride ug/L 55.650 111 70-132Chlorobenzene ug/L 51.350 103 70-130Chloroethane ug/L 54.650 109 64-134Chloroform ug/L 49.250 98 70-130Chloromethane ug/L 54.350 109 64-130cis-1,2-Dichloroethene ug/L 49.750 99 70-131cis-1,3-Dichloropropene ug/L 50.450 101 70-130Cyclohexane ug/L 47.450 95 70-130Dibromochloromethane ug/L 51.150 102 70-130Dichlorodifluoromethane ug/L 47.250 94 56-130Ethylbenzene ug/L 52.350 105 70-130Isopropylbenzene (Cumene) ug/L 56.250 112 70-130m&p-Xylene ug/L 105100 105 70-130Methyl acetate ug/L 37.950 76 70-130Methyl-tert-butyl ether ug/L 49.750 99 70-130Methylcyclohexane ug/L 55.750 111 70-130Methylene Chloride ug/L 52.350 105 63-130o-Xylene ug/L 55.450 111 70-130Styrene ug/L 53.250 106 70-130Tetrachloroethene ug/L 50.450 101 70-130Toluene ug/L 51.850 104 70-130trans-1,2-Dichloroethene ug/L 50.050 100 70-130trans-1,3-Dichloropropene ug/L 52.750 105 70-132Trichloroethene ug/L 51.850 104 70-130Trichlorofluoromethane ug/L 52.050 104 62-133Vinyl chloride ug/L 51.350 103 69-130Xylene (Total) ug/L 160150 107 70-1301,2-Dichloroethane-d4 (S) % 100 70-1304-Bromofluorobenzene (S) % 103 70-130Dibromofluoromethane (S) % 100 70-130Toluene-d8 (S) % 102 70-130



Date: 09/27/2010 06:48 PM Page 335 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



MSSpikeResult

9276650039

493818

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/L 50 101 70-166102 0 3050ND 51.3 51.4Benzene ug/L 50 121 70-148122 1 3050ND 60.5 61.2Chlorobenzene ug/L 50 109 70-146109 0 3050ND 54.4 54.3Toluene ug/L 50 116 70-155115 1 3050ND 58.1 57.7Trichloroethene ug/L 50 103 69-15199 3 305010.8 62.1 60.31,2-Dichloroethane-d4 (S) % 93 70-130894-Bromofluorobenzene (S) % 95 70-13095Dibromofluoromethane (S) % 100 70-13097Toluene-d8 (S) % 98 70-13096



Date: 09/27/2010 06:48 PM Page 336 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12151EPA 8260


Associated Lab Samples: 9276872063, 9276872070, 9276872071, 9276872072, 9276872073, 9276872074, 9276872075, 9276872076,9276872077, 9276872078





Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/08/10 00:391,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/08/10 00:391,1,2-Trichloroethane ug/kg ND 5.0 09/08/10 00:391,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/08/10 00:391,1-Dichloroethane ug/kg ND 5.0 09/08/10 00:391,1-Dichloroethene ug/kg ND 5.0 09/08/10 00:391,2,3-Trichlorobenzene ug/kg ND 5.0 09/08/10 00:391,2,4-Trichlorobenzene ug/kg ND 5.0 09/08/10 00:391,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/08/10 00:391,2-Dibromoethane (EDB) ug/kg ND 5.0 09/08/10 00:391,2-Dichlorobenzene ug/kg ND 5.0 09/08/10 00:391,2-Dichloroethane ug/kg ND 5.0 09/08/10 00:391,2-Dichloropropane ug/kg ND 5.0 09/08/10 00:391,3-Dichlorobenzene ug/kg ND 5.0 09/08/10 00:391,4-Dichlorobenzene ug/kg ND 5.0 09/08/10 00:392-Butanone (MEK) ug/kg ND 100 09/08/10 00:392-Hexanone ug/kg ND 50.0 09/08/10 00:394-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/08/10 00:39Acetone ug/kg ND 100 09/08/10 00:39Benzene ug/kg ND 5.0 09/08/10 00:39Bromochloromethane ug/kg ND 5.0 09/08/10 00:39Bromodichloromethane ug/kg ND 5.0 09/08/10 00:39Bromoform ug/kg ND 5.0 09/08/10 00:39Bromomethane ug/kg ND 10.0 09/08/10 00:39Carbon disulfide ug/kg ND 10.0 09/08/10 00:39Carbon tetrachloride ug/kg ND 5.0 09/08/10 00:39Chlorobenzene ug/kg ND 5.0 09/08/10 00:39Chloroethane ug/kg ND 10.0 09/08/10 00:39Chloroform ug/kg ND 5.0 09/08/10 00:39Chloromethane ug/kg ND 10.0 09/08/10 00:39cis-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 00:39cis-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 00:39Cyclohexane ug/kg ND 5.0 09/08/10 00:39Dibromochloromethane ug/kg ND 5.0 09/08/10 00:39Dichlorodifluoromethane ug/kg ND 10.0 09/08/10 00:39Ethylbenzene ug/kg ND 5.0 09/08/10 00:39Isopropylbenzene (Cumene) ug/kg ND 5.0 09/08/10 00:39m&p-Xylene ug/kg ND 10.0 09/08/10 00:39Methyl acetate ug/kg ND 10.0 09/08/10 00:39Methyl-tert-butyl ether ug/kg ND 5.0 09/08/10 00:39Methylcyclohexane ug/kg ND 10.0 09/08/10 00:39



Date: 09/27/2010 06:48 PM Page 337 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed

Methylene Chloride ug/kg ND 20.0 09/08/10 00:39o-Xylene ug/kg ND 5.0 09/08/10 00:39Styrene ug/kg ND 5.0 09/08/10 00:39Tetrachloroethene ug/kg ND 5.0 09/08/10 00:39Toluene ug/kg ND 5.0 09/08/10 00:39trans-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 00:39trans-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 00:39Trichloroethene ug/kg ND 5.0 09/08/10 00:39Trichlorofluoromethane ug/kg ND 5.0 09/08/10 00:39Vinyl chloride ug/kg ND 10.0 09/08/10 00:39Xylene (Total) ug/kg ND 10.0 09/08/10 00:391,2-Dichloroethane-d4 (S) % 99 70-132 09/08/10 00:394-Bromofluorobenzene (S) % 96 70-130 09/08/10 00:39Dibromofluoromethane (S) % 99 70-130 09/08/10 00:39Toluene-d8 (S) % 101 70-130 09/08/10 00:39

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 61.550 123 70-1411,1,2,2-Tetrachloroethane ug/kg 63.550 127 70-1301,1,2-Trichloroethane ug/kg 61.750 123 70-1321,1,2-Trichlorotrifluoroethane ug/kg 57.650 115 70-1301,1-Dichloroethane ug/kg 61.650 123 70-1431,1-Dichloroethene ug/kg 56.850 114 70-1371,2,3-Trichlorobenzene ug/kg 59.050 118 69-1531,2,4-Trichlorobenzene ug/kg 55.850 112 55-1711,2-Dibromo-3-chloropropane ug/kg 62.250 124 68-1411,2-Dibromoethane (EDB) ug/kg 59.550 119 70-1301,2-Dichlorobenzene ug/kg 58.550 117 70-1401,2-Dichloroethane ug/kg 61.850 124 70-1371,2-Dichloropropane ug/kg 59.950 120 70-1331,3-Dichlorobenzene ug/kg 56.650 113 70-1441,4-Dichlorobenzene ug/kg 56.950 114 70-1422-Butanone (MEK) ug/kg 128100 128 70-1492-Hexanone ug/kg 131100 131 70-1494-Methyl-2-pentanone (MIBK) ug/kg 126100 126 70-153Acetone ug/kg 126100 126 70-157Benzene ug/kg 61.350 123 70-130Bromochloromethane ug/kg 64.350 129 70-149Bromodichloromethane ug/kg 61.550 123 70-130Bromoform ug/kg 57.250 114 70-131Bromomethane ug/kg 79.0 L350 158 64-136Carbon disulfide ug/kg 58.750 117 70-130



Date: 09/27/2010 06:48 PM Page 338 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



Carbon tetrachloride ug/kg 62.650 125 70-154Chlorobenzene ug/kg 60.850 122 70-135Chloroethane ug/kg 61.550 123 68-151Chloroform ug/kg 61.250 122 70-130Chloromethane ug/kg 58.050 116 70-132cis-1,2-Dichloroethene ug/kg 60.250 120 70-140cis-1,3-Dichloropropene ug/kg 56.550 113 70-137Cyclohexane ug/kg 57.450 115 70-130Dibromochloromethane ug/kg 60.050 120 70-130Dichlorodifluoromethane ug/kg 50.950 102 36-148Ethylbenzene ug/kg 59.050 118 70-137Isopropylbenzene (Cumene) ug/kg 60.850 122 70-141m&p-Xylene ug/kg 120100 120 70-140Methyl acetate ug/kg 19.3 L050 39 70-130Methyl-tert-butyl ether ug/kg 58.350 117 45-150Methylcyclohexane ug/kg 58.650 117 70-130Methylene Chloride ug/kg 62.650 125 70-133o-Xylene ug/kg 61.350 123 70-141Styrene ug/kg 57.450 115 70-138Tetrachloroethene ug/kg 57.750 115 70-140Toluene ug/kg 59.150 118 70-130trans-1,2-Dichloroethene ug/kg 57.650 115 70-136trans-1,3-Dichloropropene ug/kg 56.250 112 70-138Trichloroethene ug/kg 59.850 120 70-132Trichlorofluoromethane ug/kg 57.250 114 69-134Vinyl chloride ug/kg 60.450 121 55-140Xylene (Total) ug/kg 181150 121 70-1411,2-Dichloroethane-d4 (S) % 102 70-1324-Bromofluorobenzene (S) % 102 70-130Dibromofluoromethane (S) % 100 70-130Toluene-d8 (S) % 100 70-130

Parameter UnitsMS



MSSpikeResult

9276750025

493936

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/kg 53 155 49-180131 16 3053.3ND 82.1 70.0Benzene ug/kg 53 148 50-166127 14 3053.3ND 78.2 67.8Chlorobenzene ug/kg 53 147 43-169122 18 3053.3ND 77.9 64.8Toluene ug/kg 53 146 52-163125 15 3053.3ND 77.4 66.7Trichloroethene ug/kg R153 133 49-167382 34 3053.3258 329 4621,2-Dichloroethane-d4 (S) % 99 70-132984-Bromofluorobenzene (S) % 100 70-13098Dibromofluoromethane (S) % 97 70-13099Toluene-d8 (S) % 98 70-13099



Date: 09/27/2010 06:48 PM Page 339 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12152EPA 8260







Matrix: Solid

Analyzed




Date: 09/27/2010 06:48 PM Page 340 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed






Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/08/10 13:491,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/08/10 13:491,1,2-Trichloroethane ug/kg ND 5.0 09/08/10 13:491,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/08/10 13:491,1-Dichloroethane ug/kg ND 5.0 09/08/10 13:491,1-Dichloroethene ug/kg ND 5.0 09/08/10 13:491,2,3-Trichlorobenzene ug/kg ND 5.0 09/08/10 13:491,2,4-Trichlorobenzene ug/kg ND 5.0 09/08/10 13:491,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/08/10 13:491,2-Dibromoethane (EDB) ug/kg ND 5.0 09/08/10 13:491,2-Dichlorobenzene ug/kg ND 5.0 09/08/10 13:491,2-Dichloroethane ug/kg ND 5.0 09/08/10 13:491,2-Dichloropropane ug/kg ND 5.0 09/08/10 13:491,3-Dichlorobenzene ug/kg ND 5.0 09/08/10 13:491,4-Dichlorobenzene ug/kg ND 5.0 09/08/10 13:492-Butanone (MEK) ug/kg ND 100 09/08/10 13:492-Hexanone ug/kg ND 50.0 09/08/10 13:494-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/08/10 13:49Acetone ug/kg ND 100 09/08/10 13:49Benzene ug/kg ND 5.0 09/08/10 13:49Bromochloromethane ug/kg ND 5.0 09/08/10 13:49Bromodichloromethane ug/kg ND 5.0 09/08/10 13:49Bromoform ug/kg ND 5.0 09/08/10 13:49Bromomethane ug/kg ND 10.0 09/08/10 13:49Carbon disulfide ug/kg ND 10.0 09/08/10 13:49Carbon tetrachloride ug/kg ND 5.0 09/08/10 13:49Chlorobenzene ug/kg ND 5.0 09/08/10 13:49



Date: 09/27/2010 06:48 PM Page 341 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed

Chloroethane ug/kg ND 10.0 09/08/10 13:49Chloroform ug/kg ND 5.0 09/08/10 13:49Chloromethane ug/kg ND 10.0 09/08/10 13:49cis-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 13:49cis-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 13:49Cyclohexane ug/kg ND 5.0 09/08/10 13:49Dibromochloromethane ug/kg ND 5.0 09/08/10 13:49Dichlorodifluoromethane ug/kg ND 10.0 09/08/10 13:49Ethylbenzene ug/kg ND 5.0 09/08/10 13:49Isopropylbenzene (Cumene) ug/kg ND 5.0 09/08/10 13:49m&p-Xylene ug/kg ND 10.0 09/08/10 13:49Methyl acetate ug/kg ND 10.0 09/08/10 13:49Methyl-tert-butyl ether ug/kg ND 5.0 09/08/10 13:49Methylcyclohexane ug/kg ND 10.0 09/08/10 13:49Methylene Chloride ug/kg 4.1J 20.0 09/08/10 13:49o-Xylene ug/kg ND 5.0 09/08/10 13:49Styrene ug/kg ND 5.0 09/08/10 13:49Tetrachloroethene ug/kg ND 5.0 09/08/10 13:49Toluene ug/kg ND 5.0 09/08/10 13:49trans-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 13:49trans-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 13:49Trichloroethene ug/kg ND 5.0 09/08/10 13:49Trichlorofluoromethane ug/kg ND 5.0 09/08/10 13:49Vinyl chloride ug/kg ND 10.0 09/08/10 13:49Xylene (Total) ug/kg ND 10.0 09/08/10 13:491,2-Dichloroethane-d4 (S) % 98 70-132 09/08/10 13:494-Bromofluorobenzene (S) % 95 70-130 09/08/10 13:49Dibromofluoromethane (S) % 98 70-130 09/08/10 13:49Toluene-d8 (S) % 101 70-130 09/08/10 13:49

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 64.550 129 70-1411,1,2,2-Tetrachloroethane ug/kg 63.950 128 70-1301,1,2-Trichloroethane ug/kg 62.550 125 70-1321,1,2-Trichlorotrifluoroethane ug/kg 61.650 123 70-1301,1-Dichloroethane ug/kg 64.850 130 70-1431,1-Dichloroethene ug/kg 60.650 121 70-1371,2,3-Trichlorobenzene ug/kg 64.250 128 69-1531,2,4-Trichlorobenzene ug/kg 61.150 122 55-1711,2-Dibromo-3-chloropropane ug/kg 60.050 120 68-1411,2-Dibromoethane (EDB) ug/kg 60.450 121 70-1301,2-Dichlorobenzene ug/kg 62.550 125 70-1401,2-Dichloroethane ug/kg 62.550 125 70-137



Date: 09/27/2010 06:48 PM Page 342 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



1,2-Dichloropropane ug/kg 63.250 126 70-1331,3-Dichlorobenzene ug/kg 60.950 122 70-1441,4-Dichlorobenzene ug/kg 61.050 122 70-1422-Butanone (MEK) ug/kg 118100 118 70-1492-Hexanone ug/kg 127100 127 70-1494-Methyl-2-pentanone (MIBK) ug/kg 121100 121 70-153Acetone ug/kg 122100 122 70-157Benzene ug/kg 64.250 128 70-130Bromochloromethane ug/kg 67.050 134 70-149Bromodichloromethane ug/kg 64.250 128 70-130Bromoform ug/kg 57.750 115 70-131Bromomethane ug/kg 83.5 L350 167 64-136Carbon disulfide ug/kg 61.950 124 70-130Carbon tetrachloride ug/kg 76.950 154 70-154Chlorobenzene ug/kg 65.050 130 70-135Chloroethane ug/kg 65.550 131 68-151Chloroform ug/kg 64.050 128 70-130Chloromethane ug/kg 61.050 122 70-132cis-1,2-Dichloroethene ug/kg 63.550 127 70-140cis-1,3-Dichloropropene ug/kg 59.350 119 70-137Cyclohexane ug/kg 60.950 122 70-130Dibromochloromethane ug/kg 62.450 125 70-130Dichlorodifluoromethane ug/kg 53.450 107 36-148Ethylbenzene ug/kg 63.650 127 70-137Isopropylbenzene (Cumene) ug/kg 64.650 129 70-141m&p-Xylene ug/kg 128100 128 70-140Methyl acetate ug/kg 19.7 L050 39 70-130Methyl-tert-butyl ether ug/kg 59.550 119 45-150Methylcyclohexane ug/kg 61.750 123 70-130Methylene Chloride ug/kg 69.4 L050 139 70-133o-Xylene ug/kg 66.150 132 70-141Styrene ug/kg 60.950 122 70-138Tetrachloroethene ug/kg 62.750 125 70-140Toluene ug/kg 62.550 125 70-130trans-1,2-Dichloroethene ug/kg 60.450 121 70-136trans-1,3-Dichloropropene ug/kg 59.250 118 70-138Trichloroethene ug/kg 62.850 126 70-132Trichlorofluoromethane ug/kg 61.650 123 69-134Vinyl chloride ug/kg 63.350 127 55-140Xylene (Total) ug/kg 194150 129 70-1411,2-Dichloroethane-d4 (S) % 95 70-1324-Bromofluorobenzene (S) % 102 70-130Dibromofluoromethane (S) % 98 70-130Toluene-d8 (S) % 99 70-130



Date: 09/27/2010 06:48 PM Page 343 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsMS



Result9276872080

1,1-Dichloroethene ug/kg 64.050 128 49-180NDBenzene ug/kg 60.650 121 50-166NDChlorobenzene ug/kg 60.650 121 43-169NDToluene ug/kg 60.950 122 52-163NDTrichloroethene ug/kg 60.650 121 49-167ND1,2-Dichloroethane-d4 (S) % 101 70-1324-Bromofluorobenzene (S) % 98 70-130Dibromofluoromethane (S) % 100 70-130Toluene-d8 (S) % 100 70-130

Parameter UnitsDup



1,1,1-Trichloroethane ug/kg ND 30ND1,1,2,2-Tetrachloroethane ug/kg ND 30ND1,1,2-Trichloroethane ug/kg ND 30ND1,1,2-Trichlorotrifluoroethane ug/kg ND 30ND1,1-Dichloroethane ug/kg ND 30ND1,1-Dichloroethene ug/kg ND 30ND1,2,3-Trichlorobenzene ug/kg ND 30ND1,2,4-Trichlorobenzene ug/kg ND 30ND1,2-Dibromo-3-chloropropane ug/kg ND 30ND1,2-Dibromoethane (EDB) ug/kg ND 30ND1,2-Dichlorobenzene ug/kg ND 30ND1,2-Dichloroethane ug/kg ND 30ND1,2-Dichloropropane ug/kg ND 30ND1,3-Dichlorobenzene ug/kg ND 30ND1,4-Dichlorobenzene ug/kg ND 30ND2-Butanone (MEK) ug/kg ND 30ND2-Hexanone ug/kg ND 30ND4-Methyl-2-pentanone (MIBK) ug/kg ND 30NDAcetone ug/kg ND 30NDBenzene ug/kg ND 30NDBromochloromethane ug/kg ND 30NDBromodichloromethane ug/kg ND 30NDBromoform ug/kg ND 30NDBromomethane ug/kg ND 30NDCarbon disulfide ug/kg ND 30NDCarbon tetrachloride ug/kg ND 30NDChlorobenzene ug/kg ND 30NDChloroethane ug/kg ND 30NDChloroform ug/kg ND 30NDChloromethane ug/kg ND 30NDcis-1,2-Dichloroethene ug/kg ND 30NDcis-1,3-Dichloropropene ug/kg ND 30NDCyclohexane ug/kg ND 30NDDibromochloromethane ug/kg ND 30ND



Date: 09/27/2010 06:48 PM Page 344 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsDup



Dichlorodifluoromethane ug/kg ND 30NDEthylbenzene ug/kg ND 30NDIsopropylbenzene (Cumene) ug/kg ND 30NDm&p-Xylene ug/kg ND 30NDMethyl acetate ug/kg ND 30NDMethyl-tert-butyl ether ug/kg ND 30NDMethylcyclohexane ug/kg ND 30NDMethylene Chloride ug/kg ND 30NDo-Xylene ug/kg ND 30NDStyrene ug/kg ND 30NDTetrachloroethene ug/kg ND 30NDToluene ug/kg ND 30NDtrans-1,2-Dichloroethene ug/kg ND 30NDtrans-1,3-Dichloropropene ug/kg ND 30NDTrichloroethene ug/kg ND 30NDTrichlorofluoromethane ug/kg ND 30NDVinyl chloride ug/kg ND 30NDXylene (Total) ug/kg ND 30ND1,2-Dichloroethane-d4 (S) % 105 81054-Bromofluorobenzene (S) % 96 499Dibromofluoromethane (S) % 100 5102Toluene-d8 (S) % 101 8101



Date: 09/27/2010 06:48 PM Page 345 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12162EPA 8260


Associated Lab Samples: 9276872083, 9276872084, 9276872085, 9276872086, 9276872087, 9276872088





Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/08/10 14:071,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/08/10 14:071,1,2-Trichloroethane ug/kg ND 5.0 09/08/10 14:071,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/08/10 14:071,1-Dichloroethane ug/kg ND 5.0 09/08/10 14:071,1-Dichloroethene ug/kg ND 5.0 09/08/10 14:071,2,3-Trichlorobenzene ug/kg ND 5.0 09/08/10 14:071,2,4-Trichlorobenzene ug/kg ND 5.0 09/08/10 14:071,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/08/10 14:071,2-Dibromoethane (EDB) ug/kg ND 5.0 09/08/10 14:071,2-Dichlorobenzene ug/kg ND 5.0 09/08/10 14:071,2-Dichloroethane ug/kg ND 5.0 09/08/10 14:071,2-Dichloropropane ug/kg ND 5.0 09/08/10 14:071,3-Dichlorobenzene ug/kg ND 5.0 09/08/10 14:071,4-Dichlorobenzene ug/kg ND 5.0 09/08/10 14:072-Butanone (MEK) ug/kg ND 100 09/08/10 14:072-Hexanone ug/kg ND 50.0 09/08/10 14:074-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/08/10 14:07Acetone ug/kg ND 100 09/08/10 14:07Benzene ug/kg ND 5.0 09/08/10 14:07Bromochloromethane ug/kg ND 5.0 09/08/10 14:07Bromodichloromethane ug/kg ND 5.0 09/08/10 14:07Bromoform ug/kg ND 5.0 09/08/10 14:07Bromomethane ug/kg ND 10.0 09/08/10 14:07Carbon disulfide ug/kg ND 10.0 09/08/10 14:07Carbon tetrachloride ug/kg ND 5.0 09/08/10 14:07Chlorobenzene ug/kg ND 5.0 09/08/10 14:07Chloroethane ug/kg ND 10.0 09/08/10 14:07Chloroform ug/kg ND 5.0 09/08/10 14:07Chloromethane ug/kg ND 10.0 09/08/10 14:07cis-1,2-Dichloroethene ug/kg ND 5.0 09/08/10 14:07cis-1,3-Dichloropropene ug/kg ND 5.0 09/08/10 14:07Cyclohexane ug/kg ND 5.0 09/08/10 14:07Dibromochloromethane ug/kg ND 5.0 09/08/10 14:07Dichlorodifluoromethane ug/kg ND 10.0 09/08/10 14:07Ethylbenzene ug/kg ND 5.0 09/08/10 14:07Isopropylbenzene (Cumene) ug/kg ND 5.0 09/08/10 14:07m&p-Xylene ug/kg ND 10.0 09/08/10 14:07Methyl acetate ug/kg ND 10.0 09/08/10 14:07Methyl-tert-butyl ether ug/kg ND 5.0 09/08/10 14:07Methylcyclohexane ug/kg ND 10.0 09/08/10 14:07Methylene Chloride ug/kg 5.1J 20.0 09/08/10 14:07o-Xylene ug/kg ND 5.0 09/08/10 14:07



Date: 09/27/2010 06:48 PM Page 346 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 53.350 107 70-1411,1,2,2-Tetrachloroethane ug/kg 53.250 106 70-1301,1,2-Trichloroethane ug/kg 54.250 108 70-1321,1,2-Trichlorotrifluoroethane ug/kg 55.650 111 70-1301,1-Dichloroethane ug/kg 53.050 106 70-1431,1-Dichloroethene ug/kg 52.650 105 70-1371,2,3-Trichlorobenzene ug/kg 60.750 121 69-1531,2,4-Trichlorobenzene ug/kg 59.950 120 55-1711,2-Dibromo-3-chloropropane ug/kg 52.650 105 68-1411,2-Dibromoethane (EDB) ug/kg 50.850 102 70-1301,2-Dichlorobenzene ug/kg 54.450 109 70-1401,2-Dichloroethane ug/kg 52.950 106 70-1371,2-Dichloropropane ug/kg 51.150 102 70-1331,3-Dichlorobenzene ug/kg 55.050 110 70-1441,4-Dichlorobenzene ug/kg 55.850 112 70-1422-Butanone (MEK) ug/kg 116100 116 70-1492-Hexanone ug/kg 107100 107 70-1494-Methyl-2-pentanone (MIBK) ug/kg 108100 108 70-153Acetone ug/kg 107100 107 70-157Benzene ug/kg 53.150 106 70-130Bromochloromethane ug/kg 53.750 107 70-149Bromodichloromethane ug/kg 53.650 107 70-130Bromoform ug/kg 49.650 99 70-131Bromomethane ug/kg 63.450 127 64-136Carbon disulfide ug/kg 51.850 104 70-130Carbon tetrachloride ug/kg 55.950 112 70-154Chlorobenzene ug/kg 54.050 108 70-135Chloroethane ug/kg 50.850 102 68-151



Date: 09/27/2010 06:48 PM Page 347 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS




Parameter UnitsMS



Result9276872083




Date: 09/27/2010 06:48 PM Page 348 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsDup



1,1,1-Trichloroethane ug/kg ND 30ND1,1,2,2-Tetrachloroethane ug/kg ND 30ND1,1,2-Trichloroethane ug/kg ND 30ND1,1,2-Trichlorotrifluoroethane ug/kg ND 30ND1,1-Dichloroethane ug/kg ND 30ND1,1-Dichloroethene ug/kg ND 30ND1,2,3-Trichlorobenzene ug/kg ND 30ND1,2,4-Trichlorobenzene ug/kg ND 30ND1,2-Dibromo-3-chloropropane ug/kg ND 30ND1,2-Dibromoethane (EDB) ug/kg ND 30ND1,2-Dichlorobenzene ug/kg ND 30ND1,2-Dichloroethane ug/kg ND 30ND1,2-Dichloropropane ug/kg ND 30ND1,3-Dichlorobenzene ug/kg ND 30ND1,4-Dichlorobenzene ug/kg ND 30ND2-Butanone (MEK) ug/kg ND 30ND2-Hexanone ug/kg ND 30ND4-Methyl-2-pentanone (MIBK) ug/kg ND 30NDAcetone ug/kg ND 30NDBenzene ug/kg ND 30NDBromochloromethane ug/kg ND 30NDBromodichloromethane ug/kg ND 30NDBromoform ug/kg ND 30NDBromomethane ug/kg ND 30NDCarbon disulfide ug/kg ND 30NDCarbon tetrachloride ug/kg ND 30NDChlorobenzene ug/kg ND 30NDChloroethane ug/kg ND 30NDChloroform ug/kg ND 30NDChloromethane ug/kg ND 30NDcis-1,2-Dichloroethene ug/kg ND 30NDcis-1,3-Dichloropropene ug/kg ND 30NDCyclohexane ug/kg ND 30NDDibromochloromethane ug/kg ND 30NDDichlorodifluoromethane ug/kg ND 30NDEthylbenzene ug/kg ND 30NDIsopropylbenzene (Cumene) ug/kg ND 30NDm&p-Xylene ug/kg ND 30NDMethyl acetate ug/kg ND 30NDMethyl-tert-butyl ether ug/kg ND 30NDMethylcyclohexane ug/kg ND 30NDMethylene Chloride ug/kg ND 30NDo-Xylene ug/kg ND 30NDStyrene ug/kg ND 30NDTetrachloroethene ug/kg ND 30NDToluene ug/kg ND 30NDtrans-1,2-Dichloroethene ug/kg ND 30NDtrans-1,3-Dichloropropene ug/kg ND 30ND



Date: 09/27/2010 06:48 PM Page 349 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsDup



Trichloroethene ug/kg ND 30NDTrichlorofluoromethane ug/kg ND 30NDVinyl chloride ug/kg ND 30NDXylene (Total) ug/kg ND 30ND1,2-Dichloroethane-d4 (S) % 98 101034-Bromofluorobenzene (S) % 95 1397Dibromofluoromethane (S) % 98 12101Toluene-d8 (S) % 101 16100



Date: 09/27/2010 06:48 PM Page 350 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12168EPA 8260







Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/09/10 02:461,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/09/10 02:461,1,2-Trichloroethane ug/kg ND 5.0 09/09/10 02:461,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/09/10 02:461,1-Dichloroethane ug/kg ND 5.0 09/09/10 02:461,1-Dichloroethene ug/kg ND 5.0 09/09/10 02:461,2,3-Trichlorobenzene ug/kg ND 5.0 09/09/10 02:461,2,4-Trichlorobenzene ug/kg ND 5.0 09/09/10 02:461,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/09/10 02:461,2-Dibromoethane (EDB) ug/kg ND 5.0 09/09/10 02:461,2-Dichlorobenzene ug/kg ND 5.0 09/09/10 02:461,2-Dichloroethane ug/kg ND 5.0 09/09/10 02:461,2-Dichloropropane ug/kg ND 5.0 09/09/10 02:461,3-Dichlorobenzene ug/kg ND 5.0 09/09/10 02:461,4-Dichlorobenzene ug/kg ND 5.0 09/09/10 02:462-Butanone (MEK) ug/kg ND 100 09/09/10 02:462-Hexanone ug/kg ND 50.0 09/09/10 02:464-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/09/10 02:46Acetone ug/kg ND 100 09/09/10 02:46Benzene ug/kg ND 5.0 09/09/10 02:46Bromochloromethane ug/kg ND 5.0 09/09/10 02:46Bromodichloromethane ug/kg ND 5.0 09/09/10 02:46Bromoform ug/kg ND 5.0 09/09/10 02:46Bromomethane ug/kg ND 10.0 09/09/10 02:46Carbon disulfide ug/kg ND 10.0 09/09/10 02:46Carbon tetrachloride ug/kg ND 5.0 09/09/10 02:46Chlorobenzene ug/kg ND 5.0 09/09/10 02:46Chloroethane ug/kg ND 10.0 09/09/10 02:46Chloroform ug/kg ND 5.0 09/09/10 02:46Chloromethane ug/kg ND 10.0 09/09/10 02:46cis-1,2-Dichloroethene ug/kg ND 5.0 09/09/10 02:46cis-1,3-Dichloropropene ug/kg ND 5.0 09/09/10 02:46Cyclohexane ug/kg ND 5.0 09/09/10 02:46Dibromochloromethane ug/kg ND 5.0 09/09/10 02:46Dichlorodifluoromethane ug/kg ND 10.0 09/09/10 02:46Ethylbenzene ug/kg ND 5.0 09/09/10 02:46Isopropylbenzene (Cumene) ug/kg ND 5.0 09/09/10 02:46m&p-Xylene ug/kg ND 10.0 09/09/10 02:46Methyl acetate ug/kg ND 10.0 09/09/10 02:46



Date: 09/27/2010 06:48 PM Page 351 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed

Methyl-tert-butyl ether ug/kg ND 5.0 09/09/10 02:46Methylcyclohexane ug/kg ND 10.0 09/09/10 02:46Methylene Chloride ug/kg ND 20.0 09/09/10 02:46o-Xylene ug/kg ND 5.0 09/09/10 02:46Styrene ug/kg ND 5.0 09/09/10 02:46Tetrachloroethene ug/kg ND 5.0 09/09/10 02:46Toluene ug/kg ND 5.0 09/09/10 02:46trans-1,2-Dichloroethene ug/kg ND 5.0 09/09/10 02:46trans-1,3-Dichloropropene ug/kg ND 5.0 09/09/10 02:46Trichloroethene ug/kg ND 5.0 09/09/10 02:46Trichlorofluoromethane ug/kg ND 5.0 09/09/10 02:46Vinyl chloride ug/kg ND 10.0 09/09/10 02:46Xylene (Total) ug/kg ND 10.0 09/09/10 02:461,2-Dichloroethane-d4 (S) % 96 70-132 09/09/10 02:464-Bromofluorobenzene (S) % 97 70-130 09/09/10 02:46Dibromofluoromethane (S) % 100 70-130 09/09/10 02:46Toluene-d8 (S) % 100 70-130 09/09/10 02:46

Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 61.350 123 70-1411,1,2,2-Tetrachloroethane ug/kg 60.350 121 70-1301,1,2-Trichloroethane ug/kg 59.450 119 70-1321,1,2-Trichlorotrifluoroethane ug/kg 55.850 112 70-1301,1-Dichloroethane ug/kg 60.750 121 70-1431,1-Dichloroethene ug/kg 56.550 113 70-1371,2,3-Trichlorobenzene ug/kg 57.150 114 69-1531,2,4-Trichlorobenzene ug/kg 51.850 104 55-1711,2-Dibromo-3-chloropropane ug/kg 58.650 117 68-1411,2-Dibromoethane (EDB) ug/kg 57.350 115 70-1301,2-Dichlorobenzene ug/kg 55.550 111 70-1401,2-Dichloroethane ug/kg 60.050 120 70-1371,2-Dichloropropane ug/kg 59.450 119 70-1331,3-Dichlorobenzene ug/kg 53.150 106 70-1441,4-Dichlorobenzene ug/kg 53.950 108 70-1422-Butanone (MEK) ug/kg 120100 120 70-1492-Hexanone ug/kg 122100 122 70-1494-Methyl-2-pentanone (MIBK) ug/kg 119100 119 70-153Acetone ug/kg 114100 114 70-157Benzene ug/kg 60.350 121 70-130Bromochloromethane ug/kg 65.450 131 70-149Bromodichloromethane ug/kg 60.750 121 70-130Bromoform ug/kg 54.550 109 70-131



Date: 09/27/2010 06:48 PM Page 352 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS



Bromomethane ug/kg 75.9 L350 152 64-136Carbon disulfide ug/kg 58.250 116 70-130Carbon tetrachloride ug/kg 72.950 146 70-154Chlorobenzene ug/kg 59.150 118 70-135Chloroethane ug/kg 61.550 123 68-151Chloroform ug/kg 60.750 121 70-130Chloromethane ug/kg 53.750 107 70-132cis-1,2-Dichloroethene ug/kg 59.550 119 70-140cis-1,3-Dichloropropene ug/kg 55.750 111 70-137Cyclohexane ug/kg 56.250 112 70-130Dibromochloromethane ug/kg 58.450 117 70-130Dichlorodifluoromethane ug/kg 51.350 103 36-148Ethylbenzene ug/kg 58.050 116 70-137Isopropylbenzene (Cumene) ug/kg 60.250 120 70-141m&p-Xylene ug/kg 117100 117 70-140Methyl acetate ug/kg 13.7 L050 27 70-130Methyl-tert-butyl ether ug/kg 56.350 113 45-150Methylcyclohexane ug/kg 57.050 114 70-130Methylene Chloride ug/kg 59.050 118 70-133o-Xylene ug/kg 59.850 120 70-141Styrene ug/kg 55.750 111 70-138Tetrachloroethene ug/kg 56.350 113 70-140Toluene ug/kg 59.150 118 70-130trans-1,2-Dichloroethene ug/kg 55.750 111 70-136trans-1,3-Dichloropropene ug/kg 55.850 112 70-138Trichloroethene ug/kg 59.050 118 70-132Trichlorofluoromethane ug/kg 56.450 113 69-134Vinyl chloride ug/kg 58.350 117 55-140Xylene (Total) ug/kg 176150 118 70-1411,2-Dichloroethane-d4 (S) % 99 70-1324-Bromofluorobenzene (S) % 102 70-130Dibromofluoromethane (S) % 98 70-130Toluene-d8 (S) % 99 70-130

Parameter UnitsMS



MSSpikeResult

9276872029

494509

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/kg 50 139 49-180157 13 3050.3ND 69.3 79.1Benzene ug/kg 50 130 50-166154 17 3050.3ND 65.0 77.5Chlorobenzene ug/kg 50 122 43-169145 18 3050.3ND 60.7 73.0Toluene ug/kg 50 128 52-163152 18 3050.3ND 64.0 76.5Trichloroethene ug/kg 50 130 49-167152 16 3050.3ND 65.0 76.41,2-Dichloroethane-d4 (S) % 104 70-1321024-Bromofluorobenzene (S) % 99 70-13097Dibromofluoromethane (S) % 101 70-130101Toluene-d8 (S) % 100 70-130100



Date: 09/27/2010 06:48 PM Page 353 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12175EPA 8260







Matrix: Solid

Analyzed

1,1,1-Trichloroethane ug/kg ND 5.0 09/09/10 12:071,1,2,2-Tetrachloroethane ug/kg ND 5.0 09/09/10 12:071,1,2-Trichloroethane ug/kg ND 5.0 09/09/10 12:071,1,2-Trichlorotrifluoroethane ug/kg ND 5.0 09/09/10 12:071,1-Dichloroethane ug/kg ND 5.0 09/09/10 12:071,1-Dichloroethene ug/kg ND 5.0 09/09/10 12:071,2,3-Trichlorobenzene ug/kg ND 5.0 09/09/10 12:071,2,4-Trichlorobenzene ug/kg ND 5.0 09/09/10 12:071,2-Dibromo-3-chloropropane ug/kg ND 5.0 09/09/10 12:071,2-Dibromoethane (EDB) ug/kg ND 5.0 09/09/10 12:071,2-Dichlorobenzene ug/kg ND 5.0 09/09/10 12:071,2-Dichloroethane ug/kg ND 5.0 09/09/10 12:071,2-Dichloropropane ug/kg ND 5.0 09/09/10 12:071,3-Dichlorobenzene ug/kg ND 5.0 09/09/10 12:071,4-Dichlorobenzene ug/kg ND 5.0 09/09/10 12:072-Butanone (MEK) ug/kg ND 100 09/09/10 12:072-Hexanone ug/kg ND 50.0 09/09/10 12:074-Methyl-2-pentanone (MIBK) ug/kg ND 50.0 09/09/10 12:07Acetone ug/kg ND 100 09/09/10 12:07Benzene ug/kg ND 5.0 09/09/10 12:07Bromochloromethane ug/kg ND 5.0 09/09/10 12:07Bromodichloromethane ug/kg ND 5.0 09/09/10 12:07Bromoform ug/kg ND 5.0 09/09/10 12:07Bromomethane ug/kg ND 10.0 09/09/10 12:07Carbon disulfide ug/kg ND 10.0 09/09/10 12:07Carbon tetrachloride ug/kg ND 5.0 09/09/10 12:07Chlorobenzene ug/kg ND 5.0 09/09/10 12:07Chloroethane ug/kg ND 10.0 09/09/10 12:07Chloroform ug/kg ND 5.0 09/09/10 12:07Chloromethane ug/kg ND 10.0 09/09/10 12:07cis-1,2-Dichloroethene ug/kg ND 5.0 09/09/10 12:07cis-1,3-Dichloropropene ug/kg ND 5.0 09/09/10 12:07Cyclohexane ug/kg ND 5.0 09/09/10 12:07Dibromochloromethane ug/kg ND 5.0 09/09/10 12:07Dichlorodifluoromethane ug/kg ND 10.0 09/09/10 12:07Ethylbenzene ug/kg ND 5.0 09/09/10 12:07Isopropylbenzene (Cumene) ug/kg ND 5.0 09/09/10 12:07m&p-Xylene ug/kg ND 10.0 09/09/10 12:07Methyl acetate ug/kg ND 10.0 09/09/10 12:07Methyl-tert-butyl ether ug/kg ND 5.0 09/09/10 12:07Methylcyclohexane ug/kg ND 10.0 09/09/10 12:07Methylene Chloride ug/kg 5.0J 20.0 09/09/10 12:07o-Xylene ug/kg ND 5.0 09/09/10 12:07



Date: 09/27/2010 06:48 PM Page 354 of 383



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(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 51.750 103 70-1411,1,2,2-Tetrachloroethane ug/kg 52.450 105 70-1301,1,2-Trichloroethane ug/kg 50.750 101 70-1321,1,2-Trichlorotrifluoroethane ug/kg 53.750 107 70-1301,1-Dichloroethane ug/kg 50.950 102 70-1431,1-Dichloroethene ug/kg 51.050 102 70-1371,2,3-Trichlorobenzene ug/kg 60.050 120 69-1531,2,4-Trichlorobenzene ug/kg 58.950 118 55-1711,2-Dibromo-3-chloropropane ug/kg 50.250 100 68-1411,2-Dibromoethane (EDB) ug/kg 50.850 102 70-1301,2-Dichlorobenzene ug/kg 56.550 113 70-1401,2-Dichloroethane ug/kg 49.950 100 70-1371,2-Dichloropropane ug/kg 50.550 101 70-1331,3-Dichlorobenzene ug/kg 56.750 113 70-1441,4-Dichlorobenzene ug/kg 57.450 115 70-1422-Butanone (MEK) ug/kg 92.2J100 92 70-1492-Hexanone ug/kg 99.9100 100 70-1494-Methyl-2-pentanone (MIBK) ug/kg 96.6100 97 70-153Acetone ug/kg 88.4J100 88 70-157Benzene ug/kg 53.050 106 70-130Bromochloromethane ug/kg 51.350 103 70-149Bromodichloromethane ug/kg 52.350 105 70-130Bromoform ug/kg 50.450 101 70-131Bromomethane ug/kg 62.550 125 64-136Carbon disulfide ug/kg 51.350 103 70-130Carbon tetrachloride ug/kg 58.650 117 70-154Chlorobenzene ug/kg 56.350 113 70-135Chloroethane ug/kg 50.750 101 68-151



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(828)254-7176



9276872MILLS GAP 6686081744

Parameter UnitsLCS




Parameter UnitsMS



MSSpikeResult

9276872040

494962

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/kg R182.4 120 49-180106 40 3062ND 98.6 65.6Benzene ug/kg R182.4 125 50-166111 40 3062ND 103 68.6Chlorobenzene ug/kg R182.4 131 43-169116 40 3062ND 108 71.8Toluene ug/kg R182.4 123 52-163109 40 3062ND 102 67.9Trichloroethene ug/kg R182.4 127 49-167114 39 3062ND 105 70.61,2-Dichloroethane-d4 (S) % 99 70-1321024-Bromofluorobenzene (S) % 97 70-13096Dibromofluoromethane (S) % 97 70-13098Toluene-d8 (S) % 98 70-13098



Date: 09/27/2010 06:48 PM Page 356 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



MSV/12185EPA 8260







Matrix: Solid

Analyzed




Date: 09/27/2010 06:48 PM Page 357 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Matrix: Solid

Analyzed


Parameter UnitsLCS



1,1,1-Trichloroethane ug/kg 62.250 124 70-1411,1,2,2-Tetrachloroethane ug/kg 64.150 128 70-1301,1,2-Trichloroethane ug/kg 62.450 125 70-1321,1,2-Trichlorotrifluoroethane ug/kg 58.250 116 70-1301,1-Dichloroethane ug/kg 62.850 126 70-1431,1-Dichloroethene ug/kg 58.350 117 70-1371,2,3-Trichlorobenzene ug/kg 64.150 128 69-1531,2,4-Trichlorobenzene ug/kg 57.150 114 55-1711,2-Dibromo-3-chloropropane ug/kg 62.150 124 68-1411,2-Dibromoethane (EDB) ug/kg 62.550 125 70-1301,2-Dichlorobenzene ug/kg 64.850 130 70-1401,2-Dichloroethane ug/kg 61.450 123 70-1371,2-Dichloropropane ug/kg 63.450 127 70-1331,3-Dichlorobenzene ug/kg 63.150 126 70-1441,4-Dichlorobenzene ug/kg 62.150 124 70-1422-Butanone (MEK) ug/kg 113100 113 70-1492-Hexanone ug/kg 125100 125 70-1494-Methyl-2-pentanone (MIBK) ug/kg 116100 116 70-153Acetone ug/kg 109100 109 70-157Benzene ug/kg 65.050 130 70-130Bromochloromethane ug/kg 64.150 128 70-149Bromodichloromethane ug/kg 66.0 L350 132 70-130Bromoform ug/kg 59.150 118 70-131Bromomethane ug/kg 77.2 L350 154 64-136Carbon disulfide ug/kg 59.150 118 70-130Carbon tetrachloride ug/kg 68.950 138 70-154Chlorobenzene ug/kg 68.6 L350 137 70-135Chloroethane ug/kg 62.950 126 68-151



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9276872MILLS GAP 6686081744

Parameter UnitsLCS



Chloroform ug/kg 61.250 122 70-130Chloromethane ug/kg 52.150 104 70-132cis-1,2-Dichloroethene ug/kg 60.750 121 70-140cis-1,3-Dichloropropene ug/kg 60.450 121 70-137Cyclohexane ug/kg 58.950 118 70-130Dibromochloromethane ug/kg 65.5 L350 131 70-130Dichlorodifluoromethane ug/kg 49.750 99 36-148Ethylbenzene ug/kg 66.550 133 70-137Isopropylbenzene (Cumene) ug/kg 69.150 138 70-141m&p-Xylene ug/kg 133100 133 70-140Methyl acetate ug/kg 7.7J L050 15 70-130Methyl-tert-butyl ether ug/kg 56.850 114 45-150Methylcyclohexane ug/kg 60.950 122 70-130Methylene Chloride ug/kg 54.650 109 70-133o-Xylene ug/kg 70.250 140 70-141Styrene ug/kg 63.450 127 70-138Tetrachloroethene ug/kg 65.550 131 70-140Toluene ug/kg 63.550 127 70-130trans-1,2-Dichloroethene ug/kg 56.850 114 70-136trans-1,3-Dichloropropene ug/kg 58.350 117 70-138Trichloroethene ug/kg 64.150 128 70-132Trichlorofluoromethane ug/kg 58.750 117 69-134Vinyl chloride ug/kg 59.250 118 55-140Xylene (Total) ug/kg 203150 135 70-1411,2-Dichloroethane-d4 (S) % 94 70-1324-Bromofluorobenzene (S) % 100 70-130Dibromofluoromethane (S) % 94 70-130Toluene-d8 (S) % 98 70-130

Parameter UnitsMS



MSSpikeResult

9276981018

495148

MSDResult

MSD% Rec RPD RPD

MaxMSDMSSpikeConc.

1,1-Dichloroethene ug/kg 58.6 115 49-180114 2 3058.1ND 67.5 66.3Benzene ug/kg 58.6 119 50-166116 4 3058.1ND 69.7 67.2Chlorobenzene ug/kg 58.6 121 43-169120 2 3058.1ND 70.8 69.5Toluene ug/kg 58.6 118 52-163116 3 3058.1ND 69.0 67.3Trichloroethene ug/kg 58.6 120 49-167119 2 3058.1ND 70.6 69.01,2-Dichloroethane-d4 (S) % 103 70-1321034-Bromofluorobenzene (S) % 97 70-13097Dibromofluoromethane (S) % 98 70-13098Toluene-d8 (S) % 98 70-13098



Date: 09/27/2010 06:48 PM Page 359 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744






Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 360 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Associated Lab Samples: 9276872006, 9276872007, 9276872008, 9276872009, 9276872010, 9276872011, 9276872012, 9276872013,9276872014, 9276872015, 9276872016, 9276872017, 9276872018, 9276872019, 9276872020, 9276872021,9276872022

Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 361 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744






Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 362 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744






Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 363 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Associated Lab Samples: 9276872045, 9276872046, 9276872047, 9276872048, 9276872049, 9276872050, 9276872051, 9276872052,9276872053, 9276872054, 9276872055, 9276872056

Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 364 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744






Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 365 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Associated Lab Samples: 9276872071, 9276872072, 9276872073, 9276872074, 9276872075, 9276872076, 9276872077, 9276872078,9276872079, 9276872080, 9276872081, 9276872082, 9276872083, 9276872084, 9276872085, 9276872086,9276872087

Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 366 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744






Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 367 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744










Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/12/10 16:15

Parameter UnitsLCS



Cyanide mg/kg 3.23 108 80-120

Parameter UnitsMS



Result9276872011

Cyanide mg/kg 2.32.5 87 75-125ND

Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 368 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744





Associated Lab Samples: 9276872021, 9276872022, 9276872023, 9276872024, 9276872026, 9276872028, 9276872030, 9276872031,9276872034, 9276872035, 9276872036, 9276872037, 9276872057, 9276872061, 9276872066




Associated Lab Samples: 9276872021, 9276872022, 9276872023, 9276872024, 9276872026, 9276872028, 9276872030, 9276872031,9276872034, 9276872035, 9276872036, 9276872037, 9276872057, 9276872061, 9276872066

Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/14/10 10:07

Parameter UnitsLCS



Cyanide mg/kg 3.63 120 80-120

Parameter UnitsMS



Result9276872031

Cyanide mg/kg 4.54.3 104 75-125ND

Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 369 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744










Matrix: Solid

Analyzed

Cyanide mg/kg ND 0.15 09/14/10 10:27

Parameter UnitsLCS



Cyanide mg/kg 3.63 120 80-120

Parameter UnitsMS



Result9276872042

Cyanide mg/kg 3.83.3 114 75-125ND

Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 370 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744










Matrix: Water

Analyzed

Cyanide mg/L ND 0.0050 09/05/10 14:08

Parameter UnitsLCS



Cyanide mg/L 0.11.1 108 80-120

Parameter UnitsMS



Result9276599001

Cyanide mg/L 0.11.1 107 75-125ND

Parameter UnitsDup



Cyanide mg/L ND 20ND



Date: 09/27/2010 06:48 PM Page 371 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



WETA/8098EPA 7196







Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



Result9276833001

Chromium, Hexavalent mg/kg ND M147.7 0 75-125ND

Parameter UnitsMS



Result9276872013


Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 372 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



WETA/8100EPA 7196







Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



Result9276872015


Parameter UnitsMS



Result9276872027


Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 373 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744



WETA/8137EPA 7196







Matrix: Solid

Analyzed


Parameter UnitsLCS




Parameter UnitsMS



Result9276872041

Chromium, Hexavalent mg/kg 13.4 M127.1 49 75-125ND

Parameter UnitsMS



Result9276872044


Parameter UnitsDup




Parameter UnitsDup






Date: 09/27/2010 06:48 PM Page 374 of 383



(704)875-9092


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(828)254-7176

QUALIFIERS


9276872MILLS GAP 6686081744

DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution ofthe sample aliquot, or moisture content.ND - Not Detected at or above adjusted reporting limit.J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.MDL - Adjusted Method Detection Limit.S - Surrogate1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.LCS(D) - Laboratory Control Sample (Duplicate)MS(D) - Matrix Spike (Duplicate)DUP - Sample DuplicateRPD - Relative Percent DifferenceNC - Not Calculable.U - Indicates the compound was analyzed for, but not detected.N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported foreach analyte is a combined concentration.Pace Analytical is NELAP accredited. Contact your Pace PM for the current list of accredited analytes.

ANALYTE QUALIFIERS

Analyte was detected in the associated method blank.BCommon Laboratory Contaminant.C9Sample was diluted due to the presence of high levels of non-target analytes or other matrix interference.D3The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.D6Reanalysis conducted in excess of EPA method holding time. Results confirm original analysis performed in hold time.H5Analyte recovery in the laboratory control sample (LCS) was outside QC limits.L0Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associatedsamples may be biased low.

L2

Analyte recovery in the laboratory control sample (LCS) exceeded QC limits. Analyte presence below reporting limits inassociated samples. Results unaffected by high bias.

L3

Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.M0Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.M6RPD value was outside control limits.R1Surrogate recovery outside laboratory control limits.S0Surrogate recovery outside laboratory control limits due to matrix interferences (confirmed by similar results from samplere-analysis).

S2



Date: 09/27/2010 06:48 PM Page 375 of 383



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9276872MILLS GAP 6686081744


9276872001 MPRP/7031 ICP/6480SS-110A EPA 3050 EPA 60109276872002 MPRP/7031 ICP/6480SS-110B EPA 3050 EPA 60109276872003 MPRP/7031 ICP/6480SS-110C EPA 3050 EPA 60109276872004 MPRP/7031 ICP/6480SS-110D EPA 3050 EPA 60109276872005 MPRP/7031 ICP/6480SS-110E EPA 3050 EPA 60109276872006 MPRP/7031 ICP/6480SS-111A EPA 3050 EPA 60109276872008 MPRP/7031 ICP/6480SS-111B EPA 3050 EPA 60109276872009 MPRP/7031 ICP/6480SS-111C EPA 3050 EPA 60109276872012 MPRP/7031 ICP/6480SS-111E EPA 3050 EPA 60109276872014 MPRP/7031 ICP/6480SS-111D EPA 3050 EPA 60109276872015 MPRP/7031 ICP/6480SS-106A EPA 3050 EPA 60109276872016 MPRP/7031 ICP/6480SS-106B EPA 3050 EPA 60109276872017 MPRP/7031 ICP/6480SS-106C EPA 3050 EPA 60109276872018 MPRP/7031 ICP/6480SS-106D EPA 3050 EPA 60109276872019 MPRP/7031 ICP/6480SS-106E EPA 3050 EPA 60109276872020 MPRP/7031 ICP/6480SS-105A EPA 3050 EPA 60109276872021 MPRP/7031 ICP/6480SS-105B EPA 3050 EPA 60109276872022 MPRP/7031 ICP/6480SS-105C EPA 3050 EPA 60109276872023 MPRP/7031 ICP/6480SS-105D EPA 3050 EPA 60109276872024 MPRP/7031 ICP/6480SS-105E EPA 3050 EPA 6010

9276872025 MPRP/7040 ICP/6491SS-107A EPA 3050 EPA 60109276872028 MPRP/7040 ICP/6491SS-107B EPA 3050 EPA 60109276872030 MPRP/7040 ICP/6491SS-107C EPA 3050 EPA 60109276872032 MPRP/7040 ICP/6491SS-107D EPA 3050 EPA 60109276872034 MPRP/7040 ICP/6491SS-107E EPA 3050 EPA 60109276872035 MPRP/7040 ICP/6491SS-112A EPA 3050 EPA 60109276872036 MPRP/7040 ICP/6491SS-112B EPA 3050 EPA 60109276872037 MPRP/7040 ICP/6491SS-112C EPA 3050 EPA 60109276872038 MPRP/7040 ICP/6491SS-112D EPA 3050 EPA 60109276872039 MPRP/7040 ICP/6491SS-112E EPA 3050 EPA 60109276872041 MPRP/7040 ICP/6491SS-108A EPA 3050 EPA 60109276872043 MPRP/7040 ICP/6491SS-108B EPA 3050 EPA 60109276872045 MPRP/7040 ICP/6491SS-108C EPA 3050 EPA 6010

9276872046 MPRP/7046 ICP/6497SS-108D EPA 3050 EPA 6010

9276872049 MPRP/7040 ICP/6491SS-108E EPA 3050 EPA 60109276872050 MPRP/7040 ICP/6491SS-114A EPA 3050 EPA 60109276872051 MPRP/7040 ICP/6491SS-114B EPA 3050 EPA 60109276872052 MPRP/7040 ICP/6491SS-131 EPA 3050 EPA 60109276872053 MPRP/7040 ICP/6491SS-132 EPA 3050 EPA 60109276872055 MPRP/7040 ICP/6491FD-17 EPA 3050 EPA 6010

9276872059 MPRP/7046 ICP/6497FD-22 EPA 3050 EPA 60109276872064 MPRP/7046 ICP/6497FD-28 EPA 3050 EPA 60109276872069 MPRP/7046 ICP/6497FD-33 EPA 3050 EPA 6010

9276872093 MPRP/7016 ICP/6465EB-02 SM 3030C EPA 6010

9276872093 MERP/3015 MERC/2972EB-02 EPA 7470 EPA 7470



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9276872MILLS GAP 6686081744


9276872001 MERP/3004 MERC/2962SS-110A EPA 7471 EPA 74719276872002 MERP/3004 MERC/2962SS-110B EPA 7471 EPA 74719276872003 MERP/3004 MERC/2962SS-110C EPA 7471 EPA 74719276872004 MERP/3004 MERC/2962SS-110D EPA 7471 EPA 7471

9276872005 MERP/3006 MERC/2964SS-110E EPA 7471 EPA 74719276872006 MERP/3006 MERC/2964SS-111A EPA 7471 EPA 7471

9276872008 MERP/3010 MERC/2968SS-111B EPA 7471 EPA 74719276872009 MERP/3010 MERC/2968SS-111C EPA 7471 EPA 74719276872012 MERP/3010 MERC/2968SS-111E EPA 7471 EPA 74719276872014 MERP/3010 MERC/2968SS-111D EPA 7471 EPA 74719276872015 MERP/3010 MERC/2968SS-106A EPA 7471 EPA 74719276872016 MERP/3010 MERC/2968SS-106B EPA 7471 EPA 74719276872017 MERP/3010 MERC/2968SS-106C EPA 7471 EPA 74719276872018 MERP/3010 MERC/2968SS-106D EPA 7471 EPA 74719276872019 MERP/3010 MERC/2968SS-106E EPA 7471 EPA 74719276872020 MERP/3010 MERC/2968SS-105A EPA 7471 EPA 74719276872021 MERP/3010 MERC/2968SS-105B EPA 7471 EPA 74719276872022 MERP/3010 MERC/2968SS-105C EPA 7471 EPA 74719276872023 MERP/3010 MERC/2968SS-105D EPA 7471 EPA 74719276872024 MERP/3010 MERC/2968SS-105E EPA 7471 EPA 74719276872025 MERP/3010 MERC/2968SS-107A EPA 7471 EPA 74719276872028 MERP/3010 MERC/2968SS-107B EPA 7471 EPA 74719276872030 MERP/3010 MERC/2968SS-107C EPA 7471 EPA 74719276872032 MERP/3010 MERC/2968SS-107D EPA 7471 EPA 74719276872034 MERP/3010 MERC/2968SS-107E EPA 7471 EPA 74719276872035 MERP/3010 MERC/2968SS-112A EPA 7471 EPA 7471

9276872036 MERP/3011 MERC/2969SS-112B EPA 7471 EPA 74719276872037 MERP/3011 MERC/2969SS-112C EPA 7471 EPA 74719276872038 MERP/3011 MERC/2969SS-112D EPA 7471 EPA 74719276872039 MERP/3011 MERC/2969SS-112E EPA 7471 EPA 74719276872041 MERP/3011 MERC/2969SS-108A EPA 7471 EPA 74719276872043 MERP/3011 MERC/2969SS-108B EPA 7471 EPA 74719276872045 MERP/3011 MERC/2969SS-108C EPA 7471 EPA 74719276872046 MERP/3011 MERC/2969SS-108D EPA 7471 EPA 74719276872049 MERP/3011 MERC/2969SS-108E EPA 7471 EPA 74719276872050 MERP/3011 MERC/2969SS-114A EPA 7471 EPA 74719276872051 MERP/3011 MERC/2969SS-114B EPA 7471 EPA 74719276872052 MERP/3011 MERC/2969SS-131 EPA 7471 EPA 74719276872053 MERP/3011 MERC/2969SS-132 EPA 7471 EPA 74719276872055 MERP/3011 MERC/2969FD-17 EPA 7471 EPA 74719276872059 MERP/3011 MERC/2969FD-22 EPA 7471 EPA 74719276872064 MERP/3011 MERC/2969FD-28 EPA 7471 EPA 7471

9276872069 MERP/3013 MERC/2974FD-33 EPA 7471 EPA 7471

9276872001 OEXT/11146 MSSV/4003SS-110A EPA 3546 EPA 82709276872002 OEXT/11146 MSSV/4003SS-110B EPA 3546 EPA 82709276872003 OEXT/11146 MSSV/4003SS-110C EPA 3546 EPA 8270



Date: 09/27/2010 06:48 PM Page 377 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872004 OEXT/11146 MSSV/4003SS-110D EPA 3546 EPA 82709276872005 OEXT/11146 MSSV/4003SS-110E EPA 3546 EPA 82709276872006 OEXT/11146 MSSV/4003SS-111A EPA 3546 EPA 8270

9276872007 OEXT/11170 MSSV/4013SS-111B EPA 3546 EPA 8270

9276872010 OEXT/11146 MSSV/4003SS-111C EPA 3546 EPA 8270

9276872012 OEXT/11153 MSSV/4010SS-111E EPA 3546 EPA 82709276872014 OEXT/11153 MSSV/4010SS-111D EPA 3546 EPA 82709276872015 OEXT/11153 MSSV/4010SS-106A EPA 3546 EPA 82709276872016 OEXT/11153 MSSV/4035SS-106B EPA 3546 EPA 82709276872017 OEXT/11153 MSSV/4010SS-106C EPA 3546 EPA 82709276872018 OEXT/11153 MSSV/4035SS-106D EPA 3546 EPA 82709276872019 OEXT/11153 MSSV/4035SS-106E EPA 3546 EPA 82709276872020 OEXT/11153 MSSV/4010SS-105A EPA 3546 EPA 82709276872021 OEXT/11153 MSSV/4010SS-105B EPA 3546 EPA 82709276872022 OEXT/11153 MSSV/4035SS-105C EPA 3546 EPA 82709276872023 OEXT/11153 MSSV/4035SS-105D EPA 3546 EPA 82709276872024 OEXT/11153 MSSV/4035SS-105E EPA 3546 EPA 82709276872026 OEXT/11153 MSSV/4035SS-107A EPA 3546 EPA 82709276872028 OEXT/11153 MSSV/4035SS-107B EPA 3546 EPA 82709276872030 OEXT/11153 MSSV/4035SS-107C EPA 3546 EPA 82709276872032 OEXT/11153 MSSV/4010SS-107D EPA 3546 EPA 82709276872033 OEXT/11153 MSSV/4010SS-107E EPA 3546 EPA 82709276872035 OEXT/11153 MSSV/4010SS-112A EPA 3546 EPA 82709276872036 OEXT/11153 MSSV/4035SS-112B EPA 3546 EPA 82709276872037 OEXT/11153 MSSV/4035SS-112C EPA 3546 EPA 8270

9276872038 OEXT/11170 MSSV/4040SS-112D EPA 3546 EPA 82709276872039 OEXT/11170 MSSV/4013SS-112E EPA 3546 EPA 8270

9276872041 OEXT/11277 MSSV/4039SS-108A EPA 3546 EPA 8270

9276872043 OEXT/11170 MSSV/4040SS-108B EPA 3546 EPA 82709276872045 OEXT/11170 MSSV/4013SS-108C EPA 3546 EPA 82709276872047 OEXT/11170 MSSV/4040SS-108D EPA 3546 EPA 8270

9276872048 OEXT/11177 MSSV/4012SS-108E EPA 3546 EPA 8270

9276872050 OEXT/11234 MSSV/4040SS-114A EPA 3546 EPA 82709276872051 OEXT/11234 MSSV/4040SS-114B EPA 3546 EPA 8270

9276872054 OEXT/11170 MSSV/4040FD-16 EPA 3546 EPA 8270

9276872058 OEXT/11234 MSSV/4040FD-21 EPA 3546 EPA 8270

9276872062 OEXT/11170 MSSV/4013FD-26 EPA 3546 EPA 82709276872067 OEXT/11170 MSSV/4013FD-31 EPA 3546 EPA 8270

9276872093 OEXT/11099 MSSV/4045EB-02 EPA 3510 EPA 8270

9276872093 MSV/12147EB-02 EPA 82609276872095 MSV/12147TB-05 EPA 8260

9276872026 MSV/12168SS-107A EPA 8260



Date: 09/27/2010 06:48 PM Page 378 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872028 MSV/12168SS-107B EPA 82609276872029 MSV/12168SS-107C EPA 82609276872032 MSV/12168SS-107D EPA 82609276872034 MSV/12168SS-107E EPA 8260

9276872035 MSV/12175SS-112A EPA 8260

9276872036 MSV/12168SS-112B EPA 82609276872037 MSV/12168SS-112C EPA 82609276872038 MSV/12168SS-112D EPA 82609276872039 MSV/12168SS-112E EPA 8260

9276872040 MSV/12175SS-108A EPA 8260

9276872043 MSV/12168SS-108B EPA 82609276872045 MSV/12168SS-108C EPA 82609276872047 MSV/12168SS-108D EPA 82609276872049 MSV/12168SS-108E EPA 82609276872050 MSV/12168SS-114A EPA 8260

9276872051 MSV/12185SS-114B EPA 8260

9276872063 MSV/12151FD-27 EPA 82609276872070 MSV/12151TB-06 EPA 82609276872071 MSV/12151SS-110A EPA 82609276872072 MSV/12151SS-110B EPA 82609276872073 MSV/12151SS-110C EPA 82609276872074 MSV/12151SS-110D EPA 82609276872075 MSV/12151SS-110E EPA 82609276872076 MSV/12151SS-111A EPA 82609276872077 MSV/12151SS-111B EPA 82609276872078 MSV/12151SS-111C EPA 8260

9276872079 MSV/12152SS-111E EPA 82609276872080 MSV/12152SS-111D EPA 82609276872081 MSV/12152SS-106A EPA 82609276872082 MSV/12152SS-106B EPA 8260

9276872083 MSV/12162SS-106C EPA 82609276872084 MSV/12162SS-106D EPA 82609276872085 MSV/12162SS-106E EPA 82609276872086 MSV/12162SS-105A EPA 82609276872087 MSV/12162SS-105B EPA 82609276872088 MSV/12162SS-105C EPA 8260

9276872089 MSV/12168SS-105D EPA 82609276872090 MSV/12168SS-105E EPA 82609276872091 MSV/12168FD-20 EPA 82609276872092 MSV/12168FD-23 EPA 82609276872094 MSV/12168TB-04 EPA 8260

9276872001 PMST/3398SS-110A ASTM D2974-879276872002 PMST/3398SS-110B ASTM D2974-879276872003 PMST/3398SS-110C ASTM D2974-87



Date: 09/27/2010 06:48 PM Page 379 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872004 PMST/3398SS-110D ASTM D2974-879276872005 PMST/3398SS-110E ASTM D2974-87

9276872006 PMST/3408SS-111A ASTM D2974-879276872007 PMST/3408SS-111B ASTM D2974-879276872008 PMST/3408SS-111B ASTM D2974-879276872009 PMST/3408SS-111C ASTM D2974-879276872010 PMST/3408SS-111C ASTM D2974-879276872011 PMST/3408SS-111E ASTM D2974-879276872012 PMST/3408SS-111E ASTM D2974-879276872013 PMST/3408SS-111D ASTM D2974-879276872014 PMST/3408SS-111D ASTM D2974-879276872015 PMST/3408SS-106A ASTM D2974-879276872016 PMST/3408SS-106B ASTM D2974-879276872017 PMST/3408SS-106C ASTM D2974-879276872018 PMST/3408SS-106D ASTM D2974-879276872019 PMST/3408SS-106E ASTM D2974-879276872020 PMST/3408SS-105A ASTM D2974-879276872021 PMST/3408SS-105B ASTM D2974-879276872022 PMST/3408SS-105C ASTM D2974-87

9276872023 PMST/3411SS-105D ASTM D2974-879276872024 PMST/3411SS-105E ASTM D2974-87

9276872025 PMST/3412SS-107A ASTM D2974-879276872026 PMST/3412SS-107A ASTM D2974-879276872027 PMST/3412SS-107B ASTM D2974-879276872028 PMST/3412SS-107B ASTM D2974-879276872029 PMST/3412SS-107C ASTM D2974-879276872030 PMST/3412SS-107C ASTM D2974-879276872031 PMST/3412SS-107D ASTM D2974-879276872032 PMST/3412SS-107D ASTM D2974-879276872033 PMST/3412SS-107E ASTM D2974-879276872034 PMST/3412SS-107E ASTM D2974-879276872035 PMST/3412SS-112A ASTM D2974-879276872036 PMST/3412SS-112B ASTM D2974-879276872037 PMST/3412SS-112C ASTM D2974-879276872038 PMST/3412SS-112D ASTM D2974-879276872039 PMST/3412SS-112E ASTM D2974-879276872040 PMST/3412SS-108A ASTM D2974-879276872041 PMST/3412SS-108A ASTM D2974-879276872042 PMST/3412SS-108B ASTM D2974-879276872043 PMST/3412SS-108B ASTM D2974-879276872044 PMST/3412SS-108C ASTM D2974-87

9276872045 PMST/3414SS-108C ASTM D2974-879276872046 PMST/3414SS-108D ASTM D2974-879276872047 PMST/3414SS-108D ASTM D2974-879276872048 PMST/3414SS-108E ASTM D2974-879276872049 PMST/3414SS-108E ASTM D2974-879276872050 PMST/3414SS-114A ASTM D2974-87



Date: 09/27/2010 06:48 PM Page 380 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872051 PMST/3414SS-114B ASTM D2974-879276872052 PMST/3414SS-131 ASTM D2974-879276872053 PMST/3414SS-132 ASTM D2974-879276872054 PMST/3414FD-16 ASTM D2974-879276872055 PMST/3414FD-17 ASTM D2974-879276872056 PMST/3414FD-18 ASTM D2974-87

9276872057 PMST/3415FD-19 ASTM D2974-879276872058 PMST/3415FD-21 ASTM D2974-879276872059 PMST/3415FD-22 ASTM D2974-879276872060 PMST/3415FD-24 ASTM D2974-879276872061 PMST/3415FD-25 ASTM D2974-879276872062 PMST/3415FD-26 ASTM D2974-879276872063 PMST/3415FD-27 ASTM D2974-879276872064 PMST/3415FD-28 ASTM D2974-879276872065 PMST/3415FD-29 ASTM D2974-879276872066 PMST/3415FD-30 ASTM D2974-879276872067 PMST/3415FD-31 ASTM D2974-879276872068 PMST/3415FD-32 ASTM D2974-879276872069 PMST/3415FD-33 ASTM D2974-87

9276872071 PMST/3418SS-110A ASTM D2974-879276872072 PMST/3418SS-110B ASTM D2974-879276872073 PMST/3418SS-110C ASTM D2974-879276872074 PMST/3418SS-110D ASTM D2974-879276872075 PMST/3418SS-110E ASTM D2974-879276872076 PMST/3418SS-111A ASTM D2974-879276872077 PMST/3418SS-111B ASTM D2974-879276872078 PMST/3418SS-111C ASTM D2974-879276872079 PMST/3418SS-111E ASTM D2974-879276872080 PMST/3418SS-111D ASTM D2974-879276872081 PMST/3418SS-106A ASTM D2974-879276872082 PMST/3418SS-106B ASTM D2974-879276872083 PMST/3418SS-106C ASTM D2974-879276872084 PMST/3418SS-106D ASTM D2974-879276872085 PMST/3418SS-106E ASTM D2974-879276872086 PMST/3418SS-105A ASTM D2974-879276872087 PMST/3418SS-105B ASTM D2974-87

9276872088 PMST/3420SS-105C ASTM D2974-879276872089 PMST/3420SS-105D ASTM D2974-879276872090 PMST/3420SS-105E ASTM D2974-879276872091 PMST/3420FD-20 ASTM D2974-879276872092 PMST/3420FD-23 ASTM D2974-87

9276872001 WETA/8135SS-110A SM 4500-CN-E9276872002 WETA/8135SS-110B SM 4500-CN-E9276872003 WETA/8135SS-110C SM 4500-CN-E9276872004 WETA/8135SS-110D SM 4500-CN-E9276872005 WETA/8135SS-110E SM 4500-CN-E9276872006 WETA/8135SS-111A SM 4500-CN-E



Date: 09/27/2010 06:48 PM Page 381 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872008 WETA/8135SS-111B SM 4500-CN-E9276872010 WETA/8135SS-111C SM 4500-CN-E9276872011 WETA/8135SS-111E SM 4500-CN-E9276872014 WETA/8135SS-111D SM 4500-CN-E9276872015 WETA/8135SS-106A SM 4500-CN-E9276872016 WETA/8135SS-106B SM 4500-CN-E9276872017 WETA/8135SS-106C SM 4500-CN-E9276872018 WETA/8135SS-106D SM 4500-CN-E9276872019 WETA/8135SS-106E SM 4500-CN-E9276872020 WETA/8135SS-105A SM 4500-CN-E

9276872021 WETA/8142SS-105B SM 4500-CN-E9276872022 WETA/8142SS-105C SM 4500-CN-E9276872023 WETA/8142SS-105D SM 4500-CN-E9276872024 WETA/8142SS-105E SM 4500-CN-E9276872026 WETA/8142SS-107A SM 4500-CN-E9276872028 WETA/8142SS-107B SM 4500-CN-E9276872030 WETA/8142SS-107C SM 4500-CN-E9276872031 WETA/8142SS-107D SM 4500-CN-E9276872034 WETA/8142SS-107E SM 4500-CN-E9276872035 WETA/8142SS-112A SM 4500-CN-E9276872036 WETA/8142SS-112B SM 4500-CN-E9276872037 WETA/8142SS-112C SM 4500-CN-E

9276872038 WETA/8143SS-112D SM 4500-CN-E9276872039 WETA/8143SS-112E SM 4500-CN-E9276872041 WETA/8143SS-108A SM 4500-CN-E9276872042 WETA/8143SS-108B SM 4500-CN-E9276872045 WETA/8143SS-108C SM 4500-CN-E9276872047 WETA/8143SS-108D SM 4500-CN-E9276872049 WETA/8143SS-108E SM 4500-CN-E9276872050 WETA/8143SS-114A SM 4500-CN-E9276872051 WETA/8143SS-114B SM 4500-CN-E

9276872057 WETA/8142FD-19 SM 4500-CN-E9276872061 WETA/8142FD-25 SM 4500-CN-E9276872066 WETA/8142FD-30 SM 4500-CN-E

9276872093 WETA/8111EB-02 SM 4500-CN-E

9276872001 WETA/8098 WETA/8104SS-110A EPA 7196 EPA 71969276872002 WETA/8098 WETA/8104SS-110B EPA 7196 EPA 71969276872003 WETA/8098 WETA/8104SS-110C EPA 7196 EPA 71969276872004 WETA/8098 WETA/8104SS-110D EPA 7196 EPA 71969276872005 WETA/8098 WETA/8104SS-110E EPA 7196 EPA 71969276872006 WETA/8098 WETA/8104SS-111A EPA 7196 EPA 71969276872008 WETA/8098 WETA/8104SS-111B EPA 7196 EPA 71969276872010 WETA/8098 WETA/8104SS-111C EPA 7196 EPA 71969276872012 WETA/8098 WETA/8104SS-111E EPA 7196 EPA 71969276872013 WETA/8098 WETA/8104SS-111D EPA 7196 EPA 7196

9276872015 WETA/8100 WETA/8105SS-106A EPA 7196 EPA 7196



Date: 09/27/2010 06:48 PM Page 382 of 383



(704)875-9092


Asheville, NC 28804

(828)254-7176



9276872MILLS GAP 6686081744


9276872016 WETA/8100 WETA/8105SS-106B EPA 7196 EPA 71969276872017 WETA/8100 WETA/8105SS-106C EPA 7196 EPA 71969276872018 WETA/8100 WETA/8105SS-106D EPA 7196 EPA 71969276872019 WETA/8100 WETA/8105SS-106E EPA 7196 EPA 71969276872020 WETA/8100 WETA/8105SS-105A EPA 7196 EPA 71969276872021 WETA/8100 WETA/8105SS-105B EPA 7196 EPA 71969276872022 WETA/8100 WETA/8105SS-105C EPA 7196 EPA 71969276872023 WETA/8100 WETA/8105SS-105D EPA 7196 EPA 71969276872024 WETA/8100 WETA/8105SS-105E EPA 7196 EPA 71969276872026 WETA/8100 WETA/8105SS-107A EPA 7196 EPA 71969276872027 WETA/8100 WETA/8105SS-107B EPA 7196 EPA 71969276872030 WETA/8100 WETA/8105SS-107C EPA 7196 EPA 71969276872032 WETA/8100 WETA/8105SS-107D EPA 7196 EPA 71969276872034 WETA/8100 WETA/8105SS-107E EPA 7196 EPA 71969276872035 WETA/8100 WETA/8105SS-112A EPA 7196 EPA 71969276872036 WETA/8100 WETA/8105SS-112B EPA 7196 EPA 71969276872037 WETA/8100 WETA/8105SS-112C EPA 7196 EPA 71969276872038 WETA/8100 WETA/8105SS-112D EPA 7196 EPA 71969276872039 WETA/8100 WETA/8105SS-112E EPA 7196 EPA 7196

9276872041 WETA/8137 WETA/8153SS-108A EPA 7196 EPA 71969276872043 WETA/8137 WETA/8153SS-108B EPA 7196 EPA 71969276872044 WETA/8137 WETA/8153SS-108C EPA 7196 EPA 71969276872047 WETA/8137 WETA/8153SS-108D EPA 7196 EPA 71969276872049 WETA/8137 WETA/8153SS-108E EPA 7196 EPA 71969276872050 WETA/8137 WETA/8153SS-114A EPA 7196 EPA 71969276872051 WETA/8137 WETA/8153SS-114B EPA 7196 EPA 71969276872052 WETA/8137 WETA/8153SS-131 EPA 7196 EPA 71969276872053 WETA/8137 WETA/8153SS-132 EPA 7196 EPA 71969276872056 WETA/8137 WETA/8153FD-18 EPA 7196 EPA 71969276872060 WETA/8137 WETA/8153FD-24 EPA 7196 EPA 71969276872065 WETA/8137 WETA/8153FD-29 EPA 7196 EPA 71969276872068 WETA/8137 WETA/8153FD-32 EPA 7196 EPA 7196



Date: 09/27/2010 06:48 PM Page 383 of 383



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(828)254-7176

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