seiko group. ・ sample: azoxyanisole ・ dsc : dsc6200 ・ sample :5 mg ・ scan rate : 20...

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SEIKO GROUP

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Page 1: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

SEIKO GROUP

Page 2: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

・ Sample: Azoxyanisole

・ DSC : DSC6200・ Sample :5 mg・ Scan Rate : 20 ゚

C/min

DSCDSC

Page 3: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

Prensinhas e CadinhosPrensinhas e CadinhosSample Pan1-7 Sealed Type8-15 Open Type16-17 Hermetic Type

Panelinhas para alta pressão

DSCDSC

Page 4: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

Modelo DSC 7020 DSC 6100 DSC 6220 DSC 6300

Tipo de DSC Heat Flux DSC

Faixa de Temperatura -170 ~ 725°C -170 ~ 500°C -170 ~ 725°C Ambiente ~ 1500°C

Ruído Médio 0.1µW 0.1µW 0.2µW 10µW

Sensibilidade 0.2µW 0.2µW 0.4µW 20µW

Taxa de Aquecimento 0.01 ~ 100°C/min 0.01 ~ 20°C/min 0.01 ~ 100°C/min 0.01 ~ 100°C/min

Amostrador Automático Opcional Opcional Opcional Indisponível

Controlador de Gás de Purga Opcional Opcional Opcional Opcional

Capacidade Máxima: Open Pan 100µL 100µL 100µL 50µL

Capacidade Máxima: Hermetic Sealed 15µL 70µL 15µL

Capacidade Máxima: Sealed 15µL 15µL

Sistema Automático de Resfriamento com LN2

(Opcional)

-150 ~ 500°C -150 ~ 500°C -170 ~ 725°C Indisponível

Sistema Eletrônico de Resfriamento(Opcional)

-70 ~ 420°C C Type: -75 ~ 210°CD Type: -30 ~ 250°C

C Type: -75 ~ 470°CD Type: -30 ~ 380°C

Indisponível

Cooling Can (Opcional) -170 ~ 725°C -170 ~ 500°C -170 ~ 725°C Indisponível

DSCDSC

Page 5: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

DSCDSC

Page 6: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

DSC OVAL SENSORDSC OVAL SENSOR

Main Heat SinkMain Heat Sink

Oval Sensor PlateOval Sensor Plate

Sample PanSample PanReference Pan Reference Pan

Oval DSC DiagramOval DSC Diagram

Heater Heater

Oval Sensor PlateOval Sensor Plate

Main Heat SinkMain Heat Sink

Heat FilterHeat Filter

Lead WireLead Wire

Sub Heat Sink Sub Heat Sink

Oval DSC Cross SectionOval DSC Cross Section

・ ・ High Resolution (Quick responsibility)High Resolution (Quick responsibility)   ・・ Low thermal resistance by 2nd dimension thermo flow Low thermal resistance by 2nd dimension thermo flow ・・ The shortest heat flow between sample and referenceThe shortest heat flow between sample and reference

・ ・ Protect the sensitivity down (by reducing noise lever)Protect the sensitivity down (by reducing noise lever)・ ・ Heat sink substrate used as sensor holder alsoHeat sink substrate used as sensor holder also・ ・ Filter stored inside sensor in order to cut the noise.Filter stored inside sensor in order to cut the noise.

DSCDSC

Page 7: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

• Os DSCs da SII NanoTechnology – Seiko são os únicos DSCs com forno Elipsoidal.

• Melhor resolução, alta sensibilidade e excelente planicidade da linha base.

Exclusividade da SEIKO SII NanoTechnology

DSCDSC

Page 8: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

Full range Cooling system

Electronic Cooling System, Automatic LN2

cooling system

Robust Auto-sampler

DSCDSC

Page 9: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

Research & Development Application ー DTG(TG) and DSC peak separation. ( for reaction of different activation energies ) ー Data simulation of measurements that are difficult

such as extremely high ( ex. 106℃/min ) or extremely low heating rates ( ex. 10-3℃/min ) .

Reduced measurement time for Quality Control ー Measurement time → 1/2~1/10

Application of Highway TAApplication of Highway TATG/DTATG/DTA

Page 10: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

Measured Data

Separated Peak

Synthetic Peak

Peak SeparationPeak Separation

DSCDSC

Page 11: SEIKO GROUP. ・ Sample: Azoxyanisole ・ DSC : DSC6200 ・ Sample :5 mg ・ Scan Rate : 20 ゚ C/min DSC

High and Low Heating Rate SimulationHigh and Low Heating Rate Simulation

DSCDSC

Temp Cel280.0260.0240.0220.0200.0180.0160.0140.0120.0

DSC

mW

0.00

-5.00

-10.00

-15.00

-20.00

Poliamida5ºC/min

10ºC/min

15ºC/min

20ºC/min25ºC/min