sdms docid#1142198 test america …client: test america, inc. service request: p0904355 project: pga...

SDMS DOCID#1142198

Test America · ~~~~JT~H~E~L~E~AD~E~R:J~N~E~N~V~IR~O~N~M~E~N~TA~L:T~E;S~Tl~N;G~~~~mru~~~ffi~~~~~~ffiru~::::::~::::~~==::::::::~::::::::::::~::~ f%~f~

!j AMEC Geomatrix Consultants, Inc. - AZ - : Cl' t P. . tID· ~'·g· 7 E · d . 1en IOJec . ~~ 77 . V1a e Ventura, Smte 396

PGA North 14682.013

r, Scottsdale, AZ 85258 Attention: Brian Mcnamara

Report Number: PSL0870

CASE NARRATIVE

LABORATORY SAMPLE NUMBER DESCRIPTION

PSL0870-01 AB4-10-121509 PSL0870-02 AB4-20-121509 PSL0870-03 AB4-20-121509 DUP PSL0870-04 AB4-30-121509 PSL0870-05 AB4-FB3-121509 PSL0870-06 AB4-TB1-121509 PSL0870-07 AB4-40-121509 PSL0870-08 AB4-50-121509 PSL0870-09 AB4-60-1215 09 PSL0870-10 AB4-70-121509 PSL0870-11 AB4-70-121509 PSL0870-12 AB4-80-121509

Sampled: 12/15/09

TestAmeri~le~~8~albfl~~01 Pnc. fssued: 01!07/ 0

SAMPLE MATRIX

Air Air Air Air Air Air Air Air Air Air Air Air

SAMPLE RECEIPT: Samples were received intact, on ice, and with chain of custody documentation.

HQLDING TIMES: See attached report from subcontracted laboratory for holding time information.

' )?R£SERV ATION: Samples requiring preservation were verified prior to sample analysis.

QAJQC CRITERIA: See attached report from subcontracted laboratory for QA/QC information.

OBSERVATIONS: See attached report from subcontracted laboratory for observations made regarding this work order.

SUBCONTRACTED: One or more samples were subcontracted to Columbia Analytical Services-2655 Park Center Drive, Ste A-Simi Valley, CA 93065 for the requested analyses. Results are attached.

TEST AMERICA- PHOENIX, AZ (AZ0728)

j~?a&....;s.~ ·Tina Paulauskas

):1~oject Manager The results pertain only to the samples tested in the /aborat01y. This report shall not be reproduced, except in

full, without written permission from TestAmerica, Inc .

PSL0870

Page 1 of 1

. 4625 East Cotton Center Boulevard Suite 189 Phoenix, AZ 85040 tel602.437.3340 fax 602.454.9303 www.testamericainc.com ~,· !l

Air • Chain of Custody Record & Analytical Service Request

~Columbia 2655 Park Center Drive, Suite A . Simi Valley California 93065

Analytical ServicesK ' Phone (805) 526-7161 .1 Requested Turnaround Time in Business Days (Surcharges) please eire!~ :iCAS Project No. Fax (805) 526-7270 1 Day (1 00%) 2 Day (75%) 3 Day (50%)· 4 Day (35%) 5 Day (25%) 10 Da - a:nCJard ·. ·

CAS Contact

~Name & Address (Reporting Information) Project Name C:£l:>~t-'( . . PbAN~ Analysis Method and/or Analytes B 111 E-. v lA bf2. ViUl'rV"HI.- ~~

?Cb~~ ~-z.. 'bS-z.s~ Project Number P-!6~2. ,o(~

·'

Project Managert::£_,(Z,l[ Cf/..A.f;b . P.O.# I Billing Information

Comments ·e.g. Actual Preservative

Phone Fax or specific instru·ctions

l/;PP -??11!3 ~ 2..'-C '1 '-6'&> ~ 3 't ~ -. ~z c.t.S Email Address for Result Reporting ·

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BV~, filUJ~ C? I('I'£R.._ .. -rz • .soc:r "OuP po3oSS :z.ftS/c:Fr lo731.{ tl I Sc.oo I:J "Z- oAC071..JO. ~~ ------ 7) L.f Afbt.{-f6'!>- rusoc; ootf,t7tf f'l.b5/0'"( JD '-/5 II /sc.oa"JZ/ - !Q ----- '"DS' A-fj~ .... rez-rz.1so; · cD3S;t9' ----- L I"CP t( fsc oo)S'D - \£ ~ ---rJ~ Af3 l(- L/D-17...1 S" oC:., · oo3to8 l"t.jlfr/~ 1137 I l \sc:ocl8Y oAQJce.c:::.. l..Q ----- Z?l A5'1- So-1'i7 OAoJcE>9 t..Q ~ 12~ Af!Jtl-bo -ILJ$09 oe2.{:;.'2. '2. 1"~-bs/ot:r lt£05 H lsc&~t oA.bJ octo r..e ------- .hros.- -o4 A_~-1 o- ~ ""2..1 Sui) pu'{/80 -z..f es/r5t 15o3 t\. }sc:.oc7?.7 0Ace>70S I..(Y '---- JV•__.o~ -,o I-4Cl'i-70- r2.15o'i · DD316Cf . l?...fl'~lo"i ~s-o3 \.1 .. lscco'ZY3 OA.ool~l ~& ------- M sj /Vf.Sb ..:.)Q__I Af34- 8D-t"ZJ5o9 -CP3b'Z-8 vz.j rs/di lb:0:3 VI lscoc.t.fZ./ ()AO'D )t.:t. IQ ,.--------- ..,.. ll.. Report Tier Levels - please select Project Requirements (MRLs, QAPP) Tier I - (Results/Default if not specified) _ Tier Ill - (Data Validation Package) 1 O% Surcharge_· _ · EOD required Yes I No Tier II - (Results + QC) _ Tier V - {client speCified) _ Type:· EDD Units:

/1 ...... .Reli!1~n.!i'""-d b~ore) ~ A ?a~ot Tif'72__,7 Received by: (Signature) t::-e__' L~(..( D'ltt{tSl~t Time=nz7 ..... ....__ ,. ' Relinquished by: (Signatur1J1 · Date: Time: Received by: '(Signature) Date: Time: Cooler I Blank Z..O r D 1Cf lfv-z f:::. Relinquished by: (Signature) · Date: Time: Received by: (Signature) Date: Time: Temperature 2C

/A( Columbia . ~Analytical ServiceS'" 2G55 Park Center Drive, Suite/\ Simi Valley. CA 93065 805.526.7161 805 526.7270 fax www.caslab.com ·

' . . . . . . ' . . . . . . . . . . . . . . . . . . . . . ' . ' . . . . ' . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . : . . . . . ~ '

January 6, 2010

Tina Paulauskas Test Amelica, Inc.

LABORATORY REPORT

4625 E. Cotton Center Blvd., Suite 189 Phoenix, AZ 85040

RE: PGA North I 14682.013 (PSL0870)

Dear Tina:

Enclosed are the results of the samples submitted to our laboratory on December 18, 2009. For your reference, these analyses have been assigned our service request number P0904355.

All analyses were performed according to our laboratory's NELAP-approved quality assurance program. The test results meet requirements of the current NELAP standards, where applicable, and except as noted in the laboratory case narrative provided. For a specific list of NELAP-accredited analytes, refer to the certifications section at www.caslab.com. Results are intended to be considered in their entirety and apply only to the samples analyzed and repoi-ted herein .. Your repoti contains ? 5 pages.

Columbia Analytical Services, Inc. is certified by the California Department of Health Services, NELAP Laboratory Certificate No. 02115CA; Arizona Department of Health Services, Certificate No. AZ0694; Florida Department of Health, NELAP Cet-tification E871020; New Jersey Depmiment of Environmental Protection,

. NELAP Laboratory Certification ID #CA009; New York State Department of Health, NBLAP NY Lab ID No: 11221; Oregon Enviromnental Laboratory Accreditation Program, NELAP ID: CA20007; The American Industrial Hygiene Association, Laboratory #101661; Depmiment of the Navy (NFESC); Pennsylvania Registration No. 68-03307; TX Commission of Environmental Quality, NELAP ID T104704413-09-TX; Mim1esota Department of Health, Cet-tificate No. 11495.A.A. Each of the certifications listed above have an explicit Scope of Accreditation that applies to specific matrices/methods/analytes; therefore, please contact me for information corresponding to a particular certification. .

If you have any questions, please call me at (805) 526-7161.

Respectf1llly submitted,

Columbia Analytical Services, Inc.

·~~ _/~~~----·-_/t)f/U:: ~

Sue Anderson Project Manager

Page 1 of 55

••••••••••••• ' •• ' •••••••• < •••••• ' •••••••••••••••••••• ' •••••••• ' ••••••••••••••••••••••••••••••••••••••••••••••••••••••• " •••••• ' •••

c, 100% Rocyclud Papr

.... ...

~(Columbia ~Analytical ~ervices"' 2655 Park Canter DrivH, Suite A

Client: Test America, Inc. Project: PGA North /14682.013 (PSL0870)

Simi Valley, Ci\ 93065

CASE NARRATIVE

805.526.7161 805.526.72'70 fax www.caslab.corn · -·~·

CAS Project No: P0904355 Arizona License No: AZ0694

The samples were received intact under chain of custody on December 18, 2009 and were stored in accordance with the analytical method requirements. Please refer to the sample acceptance check fqrm for additional information. The ~·esults reported herein are applica~le only to the condition of the samples at the time of sample receipt. The laboratory is Arizona certified for EPA Method T0-15.

Volatile Organic Compound Analysis

The samples were analyzed for selected volatile organic compounds in accordance with EPA Method T0-15 from the CompendiumofMethods for the Determination of Toxic Organic Compounds in Ambient Air, Second Edition (EPA/625/R-96/0 1 Ob ), January, 1999. The analytical system was comprised of a gas chromatograph/mass spectrometer (GC/MS) interfaced to a whole-air preconcentrator.

The results of analyses are given in the attached laboratory report. All results are intended to be considered in their entirety, and Columbia Analytical Services, Inc. (CAS) is. not responsible for utilizatioli of less than the complete report.

~i 100% Hecyclod Paper

Client: Test America, Inc. Service Request: P0904355 Project: PGA North/14682.0 13 (PSL0870)

SAMPLE CROSS-REFERENCE

SAMPLE# CLIENT SAMPLE lD DATE TfMl~ P0904355-001 AB4-10-121509- Air 12/15/09 08:37 P0904355-002 AB4-20-121509- Air 12/15/09 09:34 P0904355-003 AB4-20-121509 DUP- Air 12/15/09 09:34 P0904355-004 AB4-30-121509- Air 12/15/09 10:24 1'0904355-005 AB4-FB3-121509- Air 12115/09 10:45 P0904355-006 AB4-TB1-121509- Air 12/15/09 11:00 P0904355-007 AB4-40-121509 - Air 12/15/09 11:37 P0904355-008 AB4-50-121509- Air 12/15/09 12:38 P0904355-009 AB4-60-121509- Air 12/15/09 14:05 P0904355-010 AB4-70-121509- Air 12/15/09 15:03

....

P0904355-011 AB4-70-121509 - Air 12115/09 15:03 P0904355-012 AB4-80-121509- Air 12/15/09 16:03

Printed 1/6/l 0 9:49 Sample Summary Page I ol' I .

'

Client: Test America, Incorporated Folder: P0904355

Project: PGA North 14682.013 (PSL0870)

Detailed Sample Information

Pi2 Pi2 CAS Sample 10 Client Sample 10 Container Type _(JjgJ_ _{Q§jg)_ Pf2 Cant 10 Order# FC 10 _

P0904355-001.01 AB4-10-121509- Air 1.0 L-Summa Canister Source 0.5 1.2 1.1 10.7 1SC00621 15786 OA00706 ro9o4355-6o2~o1-- -AB4c2ocfi1569---Air -1 ~o-csurilriia canister-source----· ------o:2-- --o:1--- -f3---------1.2-- -1oA--- - -fscoo262- - -1578_6_-- -6A6oos6---------F>69o4355-6o3~0-1- - -A84c2oc fi1569-150P - 1 ~o -Lcsurilriia canister-source- - - - - - - - - -_·:(g- - - --0.9- - - -f6 - - - - - - - - -6.9 - - -1 o::f - - -1Sco613_2_ -- - -15786- - - -6i\Oo7 46 - - - - - - - - -

-Air F>o9o-4355-664~o-1-- -As4:3ocf21569--Air -1~o-ccsL!rilrTia canister-source---------- o~o---- o.o--- -fo-------- -6.7 ·- -1o:o--- -fscoo513--- -15786--- -6A61o93----- ··---F>69o4355-665~0-1-- ··As4cF83cf2-1569 --- -1~o-LcsL!rilriia canister-so-urce---------------- o2--- -fi---------1.6---10:3--- -fscoo7i1--- -15786-- ··----------------

Air F>o9o4355-666~61---A84cf81cf2-1569 ---- 1 :o-Lcsurilma canister-so-urce--------- --29.2-- c14~3-- -f,c-- 6.6----1.2-- -1o:O--- -fscoo35_o_-- - 1578_6_---------- --------

Air F>o9o-4355-6o7~6F- -AB44ocf2-1569---Air-1~o-Lcsurilrliacani5ter-so-urce · --- ·---- --0~4--- --o2 ___ -{6- --------6.9-- -1o~3--- -fsco0is4· --1578_6_-- -6i\01oso------- ··-F>o9o4355-6os~o-1-- -As4-5ocf21569---Air -1:o-c:su-rilma canister-source---- ------ --1~5--- --o.Y-- -ff---------f.-f-- -1o~3--- -fscooo4Y-- -1578_6_-- -6i\01o68---------F>o9o-4355-6og~o1- ·· -A84c6ocfz1569---Air -1~o-c:su-rilma canister-source---- ·---- ---1~2--- --o:6--- -{ 1----------f.6-- -1o§-- -fscoo652--- -1578_6_-- -6i\01o96---------F>o9o-4355-6fo~o1-- -A84ciocf21569---Air -1~o-C-st.lrilrlia canister-source-----------0~4--- --o.2--- -f f---------H-- -1o.o--- -fs-coo72Y--- -1578_6_-- ··aAoo765---------F>o9o-4355-6f1~o1-- -A84ciocf21569 --Air -1~o-Lcs_urilma canister-so-urce------------1~5--- --bY-- -fo---------6.8-- -10:1--- -fscoo2f3---- 1578_6_-- -6i\Oo71 f---------F>o9o4355-6f2~61-~ -As4:so:f21569--Air-1~o-L:surilriiacanister-source--------- ---1~4--- --o.Y-- -fo-------- -f.o-- -1o.s--- -1scoo4i1--- -15786--- -6i\Oo72i -----------------·--------------------------------------· ---------------------------------------------- ---- -------------------------

Miscellaneous Items - received

AVG00848 AVG00312 AVG01172 AVG00696 AVG00102 AVG01122 AVG00127 AVG00973 AVG01089 AVG00525

~/6/1.0 8:05 Page 1 of 1 ~ ! 1 1 ' ' 1 t L \• ··. f : ;

SENDING LABORATORY:

TestAmerica Phoenix

4625 East Cotton Center Blvd. Ste 18.9 Phoenix, AZ 85040 Phone: (602) 437-3340 Fax: (602)454-9303 Project Manager: Tina Paulauskas

SUBCONTRACT ORDER TestAmerica Phoenix

PSL0870

RECEIVING LABORATORY:

Columbia Analytical Services- Air

2655 Park Center Dr. Suite A Simi Valley, CA 93065 Phone :(805) 526-7161 Fax: (805) 526-7270 Project Location: AZ- ARIZONA Receipt Temperature: oc Ice: Y I N

Standard TAT is requested unless specific due date is requested. => Due Date: ---- Initials: ___ _

Analysis Units

Sample ID: PSL0870·01 (AB4·1 0-121509 ·Air)

T015 ppbv

Containers Supplied:

Air Canister (A)

Sample ID: PSL0870-02 (AB4-20-121509 ·Air)

T015 ppbv


Air Canister (A)

Sample ID: PSL0870-03 (AB4-20-121509 DUP- Air)

T015 ppbv


Air Canister (A)


T015 ppbv


Air Canister (A)

Sample ID: PSL0870-05 (AB4-FB3-121509 -Air)

T015 ppbv


Air Canister (A)

Sample ID: PSL0870-06 (AB4-TB1-121509- Air)

T015 ppbv


Air Canister (A)

__,___~1]_._. ~+--~!2//b_/ tf_i rfi'A4)~

Released By Date/Time

Released By Date/Time

Expires·

Sampled: 12/15/09 08:37 01/14/10 08:37

Sampled: 12/15109 09:34 01/14/10 09:34

Sampled: 12115/09 09:34 01/14/10 09:34

Sampled: 12/15/09 10:24 01/14/1010:24

Sampled: 12/15/09 10:45 01/14/10 10:45

Sampled: 12/15/09 11:00 01/14/1011:00

Comments

ICOC

ICOC

ICOC

ICOC

-o .. u ICOC

ICOC

--"~-· ·_x_· ----'-1211 &/ o 1 Received By Date!Tin\6 5 ~l-~li:J.,l.~b,I.!.~Ao&o· &J!QO~u::=:_j'~__!.._v_!JI?rlv Q f)qttu Received By· Date/Time Page 1 of 2

Analysis Units

Sample ID: PSL0870-07 (AB~-40-121509 ·Air)

T015 ppbv


Air Canister (A)

Sample ID: PSL0870-08 (AB4-50·121509 ·Air)

T015 ppbv


Air Canister (A)

Sample ID: PSL0870-09 (AB4·60·121509 ·Air)

T015 ppbv


Air Canister (A)

Sample ID: PSL0870-1 0 (AB4-70-121509 ·Air)

T015 ppbv


Air Canister (A)


T015 ppbv


Air Canister (A)

Sample ID: PSL0870-12 (AB4-80-121509 • Air)

T015 ppbv


Air Canister (A)

SUBCONTRACT ORDER TestAmerica Phoenix

PSL0870

Expires

Sampled: 12/15/09 11:37 01/14/1011:37

Sampled: 12/15/09 12:38 01/14/10 12:38

Sampled: 12/15/09 14:05 01/14/10 14:05

Sampled: 12/15/09 15:03 01/14/10 15:03

Sampled: 12/15/09 15:03 01/14/10 15:03

Sampled: 12/15/09 16:03 01/14/10 16:03

Comments

ICOC

ICOC

ICOC

ICOC

ICOC, MS/MSD

-1·1 ICOC

. 6. ~.

Page 2 of i

Air - Chain of Custody Record & Analytical Service Request Page _J_ of _L_

/;,{ Columbia !!:..~ Analytical Services~

2655 Park Center Drive, Suite A

Simi Valley, California 93065 Phone {805) 526-7161 Fax (805) 526-7270 !Requested Turnaround Time in Business Days (Surcharges) please eire~~~. -----..J. CAS Project No. 1 Day (1 00%) 2 Day (75%) 3 Day (50%) 4 Day (35%) 5 Day (25%) 10 Da~d __.-f ·

----------'---------~---------------..,----!CAS Contact c.o~p~ v~ 5117 E_. \J {;A bf2. VlUJ~ ;t;f:;7t:£ PbA-tJ~ Analysis Method and/or Ana/ytes 'Su:i['CfQ~ A.-2 ~ S LS -!b

Project Managert:1~\L C.f2A·H::::>

Email Address for Result Reporting

6VAt0*.MUJM1A'tA- (i? ~ "~&A

Client Sample 10 Laboratory Date 10 Number Collected

M Lj-JD-. I ?.J2::!j_ ~q3'3 17...f}$~

!+8 '/""'2v-J7.. ySo"j C>O~ZS'"

Columbia Analytical Services, Inc. Sample Acceptance Check Form

Client: Test America, Inc. Work order: P0904355 Project: PGA North I 14683.013 (PSL0870)

Sample(s) received on: ...:1.::2:.:../1::...:8:.:../0.::..;9:...:· --------- Date opened: 12/18/09 by: MZAMORA

Note: 'Il1i~ i'onn is used foti!_ll samples received by CAS. The u~e of this fom1 for cu~lody seals is slticlly meant to indicate presence/absence and no! as an indication or compliance or noncontbnnity. TI1ennal preservation and pH will only be evaluated either at the request oflhe client and/or as required by the method/SOP.

Yes Nc! ~A Were sample containers properly marked with client sample ID? [8] D D Container(s) supplied by CAS? [8] D D

". -~,.

2

3 Did sample containers anive in good condition? lliJ D D 4 Was a chain-of-custody provided? lEJ D D 5 Was the chain-of-custody properly completed? [}TI D D 6 Did sample c01itainer labels and/or tags agree with custody papers? [R] [] D 7 Was sample volunie received adequate for analysis? []] D D 8 Are samples within specified holding times? [8] D D 9 Was proper temperature (thermal preservation) of cooler at receipt aclherecl to? D D [R]

Cooler Temperature oc Blank Temperature oc 10 Was a trip blank received? [8] D D ... ~,;,:

Trip blank supplied by CAS: 1SC00350

11 Were custody seals on outside of cooler/Box? D ·[8] D Location of seal(s)? Sealing Lid? D D [8]' Were signature and elate included? D D [R] Were seals intact? D [] [ZJ

Were custody seals on outside of sample container? D [8] 0 Location ofseal(s)? Sealing Lid? D D lli.l Were signatme·ancl elate incluclecl? D D [8] Were seals intact'! D D rEl

12 Do containers have appropriate preservation, according to method/SOP or Client speciilecl infonnation? D D [g] Is there a client indication that the submitted samples are pH preserved? 0 D [2?] Were VOA vials checked for presence/absence of air bubbles? D D [8] Does the client/me~hoci/SOP require that the analyst check the sample pH and ifnecessmy alter it? D D [8]

13 Tubes: Are the tubes capped and intact? D D [8]

Do they contain moisture? D D llil 14 Badges: Are the badges properly capped and intact? llil

Are dual bed bad _,,..,,~.

Explain any discrepancies: (illclude lab sample ID numbers):

·~;;l-

Columbia Analytical Services, Inc. Sample Acceptance Check Form

Client: .I~st America, Inc. Work order:

Project: PGA North I 14683.013 (PSL0870) Sample(s) received on: 12118/09 Date opened: 12/18/09 ----------------------

II''''""'"'·' ''I '"'''' >.ill\ll!] ~~·:: t:~i1~1 ···-· ··_;:·:jTn:.I. 1 · ·:..• : .. ··r~;u' '~1:·:·:· I•}{\ tt- . •· •··•···············•···•·•···- .nr:.: ::::: 1(·}: .•• ·•······ ·········

IP0904355-007 .01 11.0 L Somce C•m IP0904355-008.01 11.0 L Source Can

IP0904355-009.01 11.0 L Source Can

IP0904355-010.01 11.0 L Source Can

IP09C)j}55-0ll.Ol 11.0 /.-Sourc(OCun

IP02Q4355-012.01 11.0 L Source Can

":•··· f:~\~f

• •••••

P0904355

by: MZAMORA

k·• .) •. _. {.~

~-i~i .•. 1·:: •. · ·-··· ~ . i ~- •• {_: .· .<

Explain any discrepancies: (incluc\e lab sample ID numbers): ~------------------------------

··---~------------~-------------------------

*Required pH: Phenols/COD/NH3/TOC/TOX/N03+N02/TKN/T.PHOS, H2S04 (pHl2); T. Sul!1cle, NHOI-1/ZnAc (ni-1>12) P09043SS_:rcst Amcnca, lnc.+)'C1/\ North_ 14683.013 ~Page 2 of'2

RSK- MEEPP, HCL (pH4) . . . 12119/09

COLUMBIA ANALYTICAL SERVICES, INC.

RESULTS OF ANALYSIS

Page I of3

Client: Test America, Inc~ Client Sample ID: AB4-10-121509- Air CAS Project ID: P0904355

CAS Sample ID: P0904355-001 Client Project ID: PGA Nor.th I 14682.013 (PSL0870)

Test Code: Instrument ID: Analyst: Sampling Media: Test Notes: Container ID:

EPA T0-15 Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00621

Initial Pressure (psig):

Date Collected: 12/15/09 Date Received: 12/18/09 Date Analyzed: 12/21/09

Volume(s) Analyzed: 0.40 Liter(s)

Final Pressure (psig): 1.2 Initial Pressure 2 (psig):

0.5 1.1 Final Pressure 2 (psig): 10.7

Canister Dilution Factor: 1.68

CAS# Compound Result MRL Result MRL Data 11g/m3 j.Lg/m3 ppbV ppbV Qualifier

115-07-1 Propene 50 2.1 29 1.2 75-71-8 Dichlorodifluoromethane (CFC 12) 2.2 2.1 0.44 0.42 74-87-3 Chloromethane ND 2.1 ND 1.0

76-14-2 1 ,2-Dichloro-1,1 ,2,2-tetrafluoroethane ( CFC 114) ND 2.1 ND 0.30

75-01-4 Vinyl Chloride ND 2.1 ND 0.82 106-99-0 1,3-Butadiene 6.2 2.1 2.8 0.95 74-83-9 Bromo methane ND 2.1 ND 0.54 75-00-3 Chloroethane ND 2.1 ND 0.80 67-64-1 Acetone 890 21 380 8.8 75-69-4 Trichlorofluoromethane ND 2.1 ND 0.37 67-63-0 2-Propanol (Isopropyl Alcohol) ND 4.2 ND 1.7 75-35-4 1,1-Dichlproethene ND 2.1 ND 0.53 75-09-2 Methylene Chloride ND 2.1 ND 0.60 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.1 ND 0.67 76-13-1 Trichlorotrifluoroethane ND 2.1 ND 0.27 75-15-0 Carbon Disulfide ND 21 ND 6.7 156-60-5 trans-1 ,2-Dichloroethene ND 2.1 ND 0.53 75-34-3 1, 1-Dichloroethane ND 2.1 ND 0.52 1634-04-4 Methyl tert-Butyl Ether ND 2.1 ND 0.58 108-05-4 Vinyl Acetate ND 21 ND 6.0 78-93-3 2-Butanone (MEK) 29 21 9.8 7.1

ND = Compound was analyzed for, but not detected above the laborat01y reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

"-'·

.~ ... ~

P0904355_TOI5_0912301 144_SS.xls- Sample Verified By: __ .t.::?::>.e-


RESULTS OF ANALYSIS

Page2 of3

Client: Test America, Inc. Client Sample ID: AB4-10-121509- Air CAS Project ID: P0904355

CAS Sample ID: P0904355-001 Client Project ID: PGA North I 14682.013 (PSL0870)


EPA T0~15 Telanar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00621




Final Pressure (psig): 1.2

Initial Pressure 2 (psig):

0.5

1.1 Final Pressure 2 (psig): 10.7


CAS#. Compound Result MRL Result MRL Data ).lg/m3 l:!:g/m3 ppbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethe!le ND 2.1 ND 0.53 141-78-6 Ethyl .Acetate ND 4.2 ND 1.2 110-54-3 n-Hexan~ 4.4 2.1 1.2 0.60 67-66-3 Chloroform ND 2.1 ND 0.43 109-99-9 Tetrahydrofuran (THF) ND 2.1 ND 0.71 107-06-2 1 ,2-Dichloroethane ND 2.1 ND 0.52 71-55-6 1,1, 1-Trichloroethane ND 2.1 ND 0.39 71-43-2 Benzene 3.3 2.1 1.0 0.66 56-23-5 Carbon: T-etrachloride ND 2.1 ND 0.33 110-82-7 Cyclohexane · ND 4.2 ND 1.2 78-87-5 1,2-Dichloropropane ND 2.1 ND 0.45 75-27-4 Bromodichloromethane ND 2.1 ND 0.31 79-01-6 Trichloroethene 3.1 2.1 0.57 0.39 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 2.1 ND 0.45 142-82-5 n-Heptane 3.3 2.1 0.81 0.51 10061-01-5 cis-1 ,3-Dichloropropene ND 2.1 ND 0.46 108-10-1 4-Methyl-2-pentanone ND 2.1 ND 0.51 10061-02-6 trans-1 ,3-Dichloropropene ND 2.1 ND 0.46 79-00-5 1,1 ,2-Trichloroethane ND 2.1 ND 0.39 108-88-3 Toluene 13 2.1 3.4 0.56

ND == Compow1d was analyzed for, but not detected above the laboratmy reporting limit.

.... ".:.

MRL = Method Reporting l;imit- The mii1imum quantity of a target analyte that can be confidently detenninedby the referenced method. · ··

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RESULTS OF ANALYSIS

Page 3 of3

Client: Test America, Inc. Client Sample ID: AB4-10-121509- Air

CAS Project ID: P0904355 CAS Sample ID: P0904355-001

Client Project ID: PGA North I 14682.013 (PSL0870)



1SC00621


Date Colle.cted: 12/15/09 Date Received: 12118/09 Date Analyzed: 12/21/09



Initial Pressure 2 (psig):

0.5



CAS# Compound Result MRL Result MRL D.ata

~g/m3 f.!g/m3 ppbV ppbV Qualifiei·

591-78-6 2-Hexanone 5.0 2.1 1.2 0.51

124-48-1 Dibromochloromethane ND 2.1 ND 0.25 106-93-4 1,2-Dibromoethane ND 2.1 ND 0.27 127-18-4 Tetrach1oroethene ND 2.1 ND 0.31 108-90-7 Chloro benzene ND 2.1 ND 0.46 100-41-4 Ethylbenzene ND 2.1 ND 0.48 179601-23-1 m,p-Xy1enes ND 4.2 ND 0.97 75-25-2 Bromoform ND 2.1 ND 0.20 100-42-5 Styrene ND 2.1 ND 0.49 95-47-6 o-Xylene ND 2.1 ND 0.48 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.1 ND 0.31 622-96-8 4-Ethyltojuene ND 2.1 ND 0.43 108-67-8 1,3 ,5-Trimethylbenzene ND 2.1 ND 0.43 95-63-6 1 ,2,4-Trimethylbenzene ND 2.1 ND 0.43 100-44-7 Benzyl Chloride ND 2.1 ND 0.41 541-73-1 1,3-Dichlorobenzene ND 2.1 ND 0.35 106-46-7 1 ,4-Dich1orobenzene ND 2.1 ND 0.35 95-50-1 1 ,2-Dichlorobenzene ND 2.1 ND 0.3~ 120-82-1 1 ,2,4-Trichlorobenzene ND 2.1 ND 0.28 87-68-3 Hexachlorobutadiene ND 2.1 ND 0.20 593-60-2 Vinyl Bromide ND 2.1 ND 0.48

ND = Compound was analyzed for, but not detected above the laboratory repotiing limit. MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

P0904355_T015_0912301144_SS.xls ·Sample Verified By: __ ~~~-"_)L"-----'Date: 1! h \to 12 ...

T015scan.xls · NL· PageNo.:


RESULTS OF ANALYSIS

Page 1 of3

Client: Test America, Inc. Client Sample ID: AB4-20-121509 ~Air CAS Project ID: P0904355




1SC00262

Initial Pressure (psig): -0.1



Final Pressure (psig): 1.3 Initial Pressure 2 (psig): 1.2 Final Pressure 2 (psig): 10.4


CAS# Compound Result MRL Result MRL Data llgfm3 Jlg/m3 EPbV ppbV Qualifier

115-07-1 Propene 240 2.2 140 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) 2.2 2.2 0.44 0.44 74-87-3 Chloromethane 9.6 2.2 4.6 1.0

76-14-2 1,2-Dichloro-1 ,1 ,2,2-tetrafluoroethane (CFC 114) ND 2.2 ND 0.31

75-01-4 Vinyl Chloride ND 2.2 ND 0.85 ] 06-99-0 1,3-Butadiene 26 2.2 12 0.98 74-83-9 Bromomethane ND .2.2 ND 0.56 75-00-3 Chloroethane ND 2.2 ND 0.82 67-64-1 Acetone 520 22 220 9.1 75-69-4 Trichlorofluoromethane 8.8 2.2 1.6 0.38 67-63-0 2-Propanol (Isopropyl Alcohol) ND 4.3 ND 1.8 75-35-4 1,1-Di"chloroethene ND 2.2 ND 0.55 75-09-2 Methylene Chloride ND 2.2 ND 0.62 107-05-1 3-Chloro-1-pi'opene (Allyl Chloiide) ND 2.2 ND 0.69 76-13-1 Trichlorotrifluoroethane ND 2.2 ND 0.28 75-15-0 Carbon Disulfide ND 22 ND 6.9 156-60-5 trans-1 ,2-Dichloroethene ND 2.2 ND 0.55 75-34-3 1 ,1-Dichloroethane ND 2.2 ND 0.53 1634-04-4 Methyl tert-Butyl Ether ND 2.2 ND 0.60 108-05-4 Vinyl Acetate ND 22 ND 6.1 78-93-3 2-Butanone (MEK) 52 22 18 7.3

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

•'··

·-~"'

P0904355_T015_0912301144_SS.x~ ·Sample (2) Verified By:_(L.='-'. ___ __;Date: tl b \\12:> 13 -·

T015scan.xls · NL ~ PageNo.:


RESULTS OF ANALYSIS

Page 2 of3

Client: Test Am.erica, Inc. Client Sample ID: AB4-20-121509- Air CAS Project ID: P0904355




1SC00262




Final Pressure (psig):. 1.3

Initial Pressure 2 (psig): 1.2 Final Pressure 2 (psig): 10.4

Canister Dilution· Factor: 1. 73

CAS# Compound Result MRL Result MRL Data i-Lg/m3 f!g/m3 ppbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.2 ND 0.55 141-78-6 Ethyl Acetate ND 4.3 ND 1.2 110-54-3 n-Hexane 21 2.2 6.0 0.61 67-66-3 Chloroform ND 2.2 ND 0.44 109-99-9 Tetrahydrofuran (THF) ND 2.2 ND 0.73 107-06-2 1 ,2-Dichloroethane ND 2.2 ND 0.53 71-55-6 1,1,1-Trichloroethane ND 2.2 ND 0.40 71-43-2 Benzene 15 2.2 4.6 0.68 56-23-5 Carbon Tetrachloride 3.4 2.2 0.55 0.34 110-82-7 Cyclohexane ND 4.3 ND 1.3 78-87-5 1,2-Dichloropropane ND 2.2 ND 0.47 75-27-4 Bromodichlorbmethane ND 2.2 ND 0.32 79-01-6 Trichloroethene 4.9 2.2 0.92 0.40 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 2.2 ND 0.46 142-82-5 n-Heptane 13 2.2 3.2 0.53 10061-01-5 cis-1 ,3-Dichloropropene ND 2.2 ND 0.48 108-10-1 4-Methyl-2-pentanone ND 2.2 ND 0.53 10061-02-6 trans-1 ,3-Dichloropropene ND 2.2 ND 0.48 79-00-5 1,1 ,2-Trichloroethane ND 2.2 ND 0.40 108-88-3 Toluene 27 2.2 7.1 0.57

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit- The minimum quantity of a target analyte that can b~? confidently determined by the referenced method.

P0904355_T015_0912301144_SS.xls • Sample(2) VerifiedBy:_--'.~'=:...t:"'"'· '-----·Date: 1\ b\\o 14

TOI5scan.xls • NL • PageNo.:


RESULTS OF ANALYSIS Page 3 of3


· CAS Project ID: P0904355 CAS Sample ID: P090435?-002


Test Code: Instmment ID: Analyst: Sampling Media: Test Notes: Container ID:

EPA T0-15 Tekmar AUTO CAN/ Agilent 5973ineti/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00262

Irutial Pressure (psig): -0.1

Date Collected: 12/15/09 Date Received: 12118/09 Date Analyzed: 12/21/09




Canister Dilution Factor: 1. 73

CAS# Compoul).d Result MRL Result MRL Data ~-tg/m3 f.Lg/m3 . ppbV ppbV Qualifier

591-78-6 2-Hexanone 5.7 2.2 1.4 0.53 124-48-1 Dibromochloromethane ND 2.2 ND 0.25 106-93-4 1 ,2-Dibromoethane ND 2.2 ND 0.28 127-18-4 Tetrachloroethene ND 2.2 ND 0.32 108-90-7 Ch1orobenzene ND 2.2 ND 0.47 100-41-4 Ethylbenzene 3.2 2.2 0.74 0.50 179601-23-1 m,p-Xylenes 6.7 4.3 1.5 1.0 75-25-2 Bromofonn ND 2.2 ND 0.21 100-42-5 Styrene )\T]) 2.2 ND 0.51 95-47-6 o-Xylene 2.4 2.2 0.55 0.50 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.2 ND 0.32 622-96-8 4-Ethylto Juene ND 2.2 ND 0.44 108-67-8 1,3 ,5-Trimethylbenzene ND 2.2 ND 0.44 95-63-6 1 ,2,4-Tiimethylbenzene ND 2.2 ND 0.44 100-44-7 Benzyl Chloride ND 2.2 ND 0.42 541-73-1 1,3-Dichlorobenzene ND 2.2 ND 0.36 106-46-7 1 ,4-Dichlorobenzene ND 2.2 ND 0.36 95-50-1 1 ,2-Dichlorobenzene ND 2.2 ND 0.36 120-82-1 1 ,2,4-Trichlorobenzene ND 2.2 ND 0.29 87-68-3 Hexachlorobutadiene ND 2.2 ND 0.20 593-60-2 Vinyl Bromide ND 2.2 ND 0.49

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently detennined by the referenced method.

Verified By: __ __.\2.'--'e..,-"""' _-____ .Date: il b \1 o P0904355_T015_0912301144_SS.xls- Sample (2) TOISscan.xls- NL- PageNo.:


RESULTS OF ANALYSIS

Page 1 of3

Client: Test America, Inc. Client Sample ID: AB4-20-121509 DUP- Air Client Project ID: PGA North I 14682.013 (PSL0870)



1SC00132


CAS ProjectiD: P0904355 CAS Sample ID: P0904355-003

Date Collected: 12/15/09 Date Received: 12/18/09 Date Analyzed: 12/21109


Final Pressure (psig):. 1.0 Initial Pressure 2 (psig): 0.9 Final Pressure 2 (psig): 10.3


CAS# Compound Result MRL Result MRL Data )lg/m3 f.lg/m3 ppbV ppbV Qualifier

115-07-1 Propene 220 2.3 130 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) ND 2.3 ND 0.46 74-87-3 Chloromethane 9.2 2.3 4.5 1.1

76-14-2 1 ,2-Di~hloro-1 ,1 ,2,2~ tetrafluoroethane (CFC 114) ND 2.3 ND 0.33

75-01-4 Vinyl Chloride ND 2.3 ND 0.89 106-99-0 1,3-Butadiene 26 2.3 12 1.0 74-83-9 Bromomethane ND 2.3 ND 0.59 75-00-3 Chloroethane ND 2.3 ND 0.86 67-64-1 Acetone 480 23 200 9.6 75-69-4 Trichl()rQfluoromethane 9.0 2.3 1.6 0.40 67-63-0 2-Propanol (Isopropyl Alcohol) ND 4.6 ND 1.9 75-35-4 1,1-Dichloroethene ND 2.3 ND 0.57 75-09-2 Methylene Chloride ND 2.3 ND 0.66 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.3 ND 0.73 76-13-1 Trichlorotrifluoroethane ND 2.3 ND 0.30 75-15-0 Carbon Disulfide ND 23 ND 7.3. 156-60-5 trans-1 ,2-Dichloroethene ND 2.3 ND 0.57 75-34-3 1,1-Dichloroethane ND 2.3 ND 0.56 1634-04-4 Methyl tert-Butyl Ether ND 2.3 ND 0.63 108-05-4 Vinyl Acetate ND 23 ND 6.5 78-93-3 2-Butanone (MEK) 50 23 17 7.7

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method ..

Verified By: ___ _,_\2-"'e:,_,--_-------'Date: ll b \ l a 16 P0904355_T015_0912301144_SS.xls- Sample (3) T015scan,xls- NL- PageNo.:

...

'""'"'


Client: Test America, Inc. Client Sample ID: AB4-20-121509 DUP- Air Client Project ID: PGA North I 14682.013 (PSL0870)

Test Code: EPA T0-15

RESULTS OF ANALYSIS

Page2 of3

Instrument ID: Analyst:

Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng

Sampling Media: 1.0 L Suriuna Canister Test Notes: Container ID: 1SC00132




Initial Pressure (psig): -0.9 Final Pressure (psig): l.O Initial Pressure 2 (psig): 0.9 Final Pressure 2 (psig):· 10.3

Canister Diluti011 Factor: 1.82

CAS# Compound Result MRL Result MRL Data· f.Lg/m3 f.Lg/m3 ppbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.3 . ND 0.57 141-78-6 Ethyl Acetate ND 4.6 ND 1.3 110-54-3 n-Hexane 21 2.3 5.9 0.65 67-66-3 Chloroform ND 2.3 ND 0.47 109-99-9 Tetrahydrofuran (THF) ND 2.3 ND 0.77 107-06-2 1 ,2-Dichloroethane ND 2.3 ND 0.56 71-55-6 1,1, 1-Trichloroethane ND . 2.3 ND 0.42 71-43-2 Benzene 15 2.3 4.7 0.71 56-23-5 Carbon Tetrachloride 3.6 2.3 0.57 0.36 110-82-7 Cyclohexane ND 4.6 ND 1.3 78-87-5 1 ,2-Dichloropropane ND 2.3 ND 0.49 75-27-4 Bromodichlorometbane ND 2.3 ND 0.34 79-01-6 Trichloroethene 4.8 2.3 0.90 0.42 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 2.3 ND 0.49 142-82-5 n-Heptane 13 2.3 3.2 0.56 10061-01-5 cis-1 ,3-Dichloropropene ND 2.3 ND 0.50 108-10-1 4-Methyl-2-pentanone ND 2.3 ND 0.56 10061-02-6 trans-1 ,~-Dich1oropropene ND 2.3 ND 0.50 79-00-5 1,1 ,2-Trichloroethane ND 2.3 ND 0.42 108-88-3 Toluene 28 2.3 7.4 0.60

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently detem1ined by the referenced method.

Verified By:. __ _,_~L=t.r'"'-' ____ Date: lib\ l o 17 P0904355_T015_0912301144_SS.xls • Sample(3) TOISscan.xls • NL. PageNo.:

........


RESULTS OF ANALYSIS

Page 3 of3

Client: Test America, Inc. . CAS Project ID: P0904355 CAS Sample ID: P090435.5-003 Client Sample ID: AB4-20-121509 DUP- Air




1SC00132







CAS# Compound Result MRL Result MRL Data 11-g/m3 IJ.g/m3 ppbV ppbV Qualifi~r

591-78-6 2-Hexanone 6.1 2.3 1.5 0.56 124-48-'l Dibromochloromethane ND 2.3 ND 0.27 106-93-4 1,2-Dibromoethane ND 2.3 ND 0.30 127-18-4 Tetrachloroethene ND 2.3 ND 0.34 108-90-7 Chlorobenzene ND 2.3 ND 0.49 100-41-4 Ethylbenzene 3.4 2.3 0.77 0.52 179601-23-1 m,p-Xylenes 7.2 4.6 1.7 1.0 75-25-2 Bromoform ND 2.3 ND 0.22 100-42-5 Styrene ND 2.3 ND 0.53 95-47-6 o-Xylene 2.6 2.3 0.59 . 0.52 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.3 ND 0.33 622-96-8 4-Ethyltoluene ND 2.3 ND 0.46 108-67-8 1,3 ,5-Trimethylbenzene ND 2.3 ND 0.46 95-63-6 1 ,2,4-Ti·imethylbenzene ND 2.3 ND 0.46 100-44-7 Benzyl Chloride ND 2.3 ND 0.44 541-73-1 1 ,3-Dichlorobenzene ND 2.3 ND 0.38 106-46-7 1 ,4-Dichlorobenzene ND 2.3 ND 0.38 95-50-1 1,2-Dichlorobenzene ND 2.3 ND 0.38 120-82-1 1,2 ,4-Trichlorobenzene ND 2.3 ND 0.31 87-68-3 Hexachlorobutadiene ND 2_.3 ND 0.21 593-60-2 Vinyl Bromide ND 2.3 ND 0.52

ND = Compound was analyzed for, but not detected above the laboratory repmting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

P0904355_T015_0912301144_SS.xls ·Sample (3) VerifiedBy:._---+=~=.l'.l._s: ___ _.;Date: llb\ 1 D 18.

T015scan.x!s • :NL- PageNo.:


Client: Test America, Inc. Client Sample ID: AB4-30-121509- Air Client Project ID: PGA North I 14682.013 (PSL0870)


RESULTS OF ANALYSIS Page 1 of3

Instmment ID: Analyst:

Tekmar AUTOCAN/Agilent 5973inertJ6890N/MS8 WidaAng

Sampling Media: 1.0 L Summa Canister Test Notes: Container ID: 1SC00513

CAS Project ID: P0904355 ·CAS Sample ID: P0904355-004

Date Collected: 12/15/09 Date Received: 12118/09 Date Analyzed: 12/21 - 12/22/09

Volume(s) Analyzed: 0.40 Liter(s) 0.10 Liter(s)

Initial Pressure (psig): 0.0 0.7

Final Pressure (psig): · 1.0 Initial Pressure 2 (psig): Final Pressure 2 (psig): 10.0

Canister Dilution Factor: 1. 71 ·

CAS# Compound Result MRL Result MRL Data ~-tg/m3 f.Lg/m3 ppbV ppbV Qualifier

115-07-1 Propene 780 8.6 450 5.0 D2 75-71-8 Dichlorodifluor6methane (CFC 12) ND 2.1 ND 0.43 74-87-3 Chloromethane 2.4 2.1 1.2 1.0

76-14-2 1 ,2-Diehl oro-1 , 1 ,2 ,2-tetrafluoroethane (CFC 114) ND 2.1 ND 0.31

75-01-4 Vinyl Chloride ND 2.1 ND 0.84 106-99-0 1,3-Butadiene 59 2.1 27 0.97 74-83-9 Bromo methane ND 2.1 ND 0.55 75-00-3 Chloroethane ND 2.1 ND 0.81 67-64-1 Acetone 1,200 21 530 9.0 75-69-4 Trichlorofluoromethane 12 2.1 2.1 0.38 67-63-0 2-Propanol (Isopropyl Alcohol) 13 4.3 5.5 1.7 75-35-4 1,1-Dichloroethene · ND 2.1 ND 0.54 75-09-2 Methylene Chloride ND 2.1 ND 0.62 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.1 ND 0.68 76-13-1 Trichlorotrifluoroethane ND 2.1 ND 0.28 75-15-0 Carbon Disulfide 27 21 8.6 6.9 156-60-5 trans-1 ,2-Dichloroethene ND 2.1 ND 0.54 75-34-3 1, 1-Dichloroethane · ND 2.1 ND 0.53 1634-04-4 Methyl teit-Butyl Ether ND 2.1 ND 0.59 108-05-4 Vinyl Acetate ND 21 ND 6.1 78-93-3 2-Butanone (MEK) 120 21 41 7.3

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method. D2 =Sample required dilution due to high concentration of target analyte.

Verified By: __ ---'1'-"~'-'-----Date: \I b\ 1 o 19 P0904355_T015_0912301144_SS.xls ·Sample (4) T015scnn.xls · NL- PageNo.:




RESULTS OF ANALYSIS

Page 2 of3


Tekmar AUTOCAN/Agilent 5973inert/6890N!MS8 WidaAng



Date Collected: 12/15/09. Date Received: 12/18/09 Date Analyzed: 12/21 - 12/22/09


Initial Pressure (psig): 0.0

0.7


Initial Pressure 2 (psig): Final Pressure 2 (psig): 10.0


CAS# Compound Result MRL Result MRL Data 11g/m3 i:!;glm3 ppbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.1 ND 0.54 141-78-6 Ethyl Acetate ND 4.3 ND 1.2 110-54-3 n-Hexane 40 2.1 11 0.61 67-66-3 Chloroform ND 2.1 ND 0.44 109-99-9 Tetrahydrofuran (THF) ND 2.1 ND 0.73 107-06-2 1 ,2-Dichloroethane ND 2.1 ND 0.53 71-55-6 1 ,1,1-Trichloroethane ND 2.1 ND 0.39 71-43'-2 Benzene 17 2.1 5.3 0.67 56-23-5 Carbon Tetrachloride ND 2.1 ND 0.34 110-82-7 Cyclohexane ND 4.3 ND 1.2 78-87-5 1 ,2-Dichloropropane ND 2.1 ND 0.46 75-27-4 Bromodichloromethane ND 2.1 ND 0.32 79-01-6 Trichloroethene ND 2.1 ND 0.40 540-84-1 2,2,4-Trimethylpentane (Isooctane) 2.9 2.1 0.62 0.46 142-82-5 n-Heptane 22 2.1 5.4 0.52 10061-01-5 cis-1 ,3-Dichloropropene ND 2.1 ND 0.47 108-10-1 4-Metliyl-2-pentanone 3.0 2.1 0.73 0.52 10061-02-6 trans-1 ,3-Dichloropropene ND 2.1 ND 0.47 79-00-5 1,1 ,2-Trichloroethane ND 2.1 ND 0.39 108-88-3 Toluene 35 2.1 9.2 0.57

ND =Compound was analyzed for, but not detected above the laboratoty reporting limit. MRL = Method Reporting Liii)it- The minimum quantity of a target analyte that can be confidently determined by the referenced niethod.

Verified By: __ ___:\) ___ _.·_,_-____ Date: \\ 6\ 1 o 20 .... P0904355_T015_0912301144_SS.xls- Sample (4) TOISscan.xls- NL- PageNo.;




RESULTS OF ANALYSIS

Page 3 of3


Telanar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng


CAS Project ID: P0904355 ·CAS Sample ID: P0904355-004

Date Collected: 12115/09 Datct Received: 12/18/09 Date Analyzed: 12/21 - 12/22/09


Initial Pressure (psig): 0.0

0.7


Initial Pressure 2 (psig): Final Pressure 2 (psig): 10.0


CAS# Compound Result MRL Result MRL Data ~-tg/m3 f.Lg/m3 ppbV ppbV Qualifier

591-78-6 2-Hexanone 12 2.1 2.8 0.52 124-48-1 Dibromochlot:omethane ND 2.1 ND 0.25 106-93-4 1,2-Dibromoethane ND 2.1 ND 0.28 127-18-4 Tetrachloroethene ND 2.1 ND 0.32 108-90-7 Chlorobenzene ND 2.1 ND 0.46 100-41-4 Ethylbenzerie 3.1 2.1 0.71 0.49 179601-23-1 m,p-Xyleues 6.4 4.3 1.5 0.98 75-25-2 Bromoform ND 2.1 ND 0.21 100-42-5 Styrene ND 2.1 ND 0.50 95-47-6 o-Xylene 2.3 2.1 0.53 0.49

79-34-5 1 , 1 ,2 ,2-Tetrachloroethane ND 2.1 ND 0.31 622-96-8 4-Ethyltoluene ND 2.1 ND 0.43 108-67-8 1,3 ,5-Trimethylbenzene ND 2.1 ND 0.43 95-63-6 1 ,2,4-Tdmethylbenzene ND 2.1 ND 0.43 100-44-7 Benzyl Chloride ND 2.1 ND 0.41

541-73-1 1,3-Dichlorobenzene ND 2.1 ND 0.36 106-46-7 1,4-Dichlorobenzene ND 2.1 ND 0.36 95-50-1 1 ,2-Dichlorobenzene ND 2.1 1\TD 0.36 120-82-1 1 ,2,4-Trichlorobenzene ND 2.1 :ND 0.29 87-68-3 Hexachlorobutadiene ND 2.1 ND 0.20 593-60-2 Vinyl "Bromide ND 2.1 ND 0.49

ND ==Compound was analyzed for; but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently detennined by the referenced method.

Verified By: _ __:'{!_=-) t:""· '=-" _____ Date:___L\_blll"l 21 P0904355_TOI5_0912301144_SS.xls ·Sample (4) TOI5scan.xls. NL • PageNo.:

-~'"


RESULTS OF ANALYSIS

Page 1 of3

Client: Test America, Inc. Client Sample ID: AB4-FB3-121509 -Air Client Project ID: PGA North I 14682.013 (PSL0870)


EPA T0-15 Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Smmna Canister

1SC00721

Initial Pressme (psig):


Date Collected: 12/15/09 Date Received: 12/18/09 DateAnalyzed: 12/21/09


Final Pressure (psig): 1.2 Initial Pressure 2 (psig):

0.2 1.0 Final Pressure 2 (psig): 10.3


CAS# Compound Result MRL Result MRL Data 11g/m3 flg/m3 ppbV EEbV Qualifier

115-07-1 Propene ND 2.1 ND 1.2 75-71-8 Dichlorodifluoromethane (CFC 12) 2.3 2.1 0.46 0.43 74-87-3 Chloromethane ND 2.1 ND 1.0

76-14-2 1 ,2-Dichloro-1, 1 ,2,2-tett·afluoroethane ( CFC 114) ND 2.1 ND 0.30

75-01-4 Vinyl Chloride ND 2.1 ND 0.83 106-99-0 1 ,3-Butadiene ND 2.1 ND 0.96 74-83-9 Bromomethane ND 2.1 ND 0.55 75-00-3 Chloroethane ND 2.1 ND 0.81 67-64-1 Acetone ND 21 ND 8.9 75-69-4 Trichlorofluoromethane ND 2.1 ND 0.38 67-63-0 2-Propanol (Isopropyl Alcohol) ND 4.3 ND 1.7 75-35-4 1, 1-Dichloroethene ND 2.1 ND 0.54 75-09-2 Methylene Chloride ND 2.1 ND 0.61 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.1 ND 0.68 76-13-1 Trichlorotrifluoroethane ND 2.1 ND 0.28 75-15-0 Carbon Disulfide ND 21 ND 6.8 156-60-5 trans-1 ,2-Dichloroethene ND 2.1 ND 0.54 75-34-3 1, 1-Dichloroethane ND 2.1 ND 0.53 1634-04-4 Methyl tert-Butyl Ether ND 2.1 ND 0.59 108-05-4 Vinyl Acetate ND 21 ND 6.0 78-93-3 2-Butanone (MEK} ND 21 ND 7.2

l\TD = Compotmd was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The 1i1inimum quantity of a target analyte that can be confidently determined by the referenced method.

) Verified By: __ \_"---


RESULTS OF ANALYSIS

Page 2 of3

Client: Test America, Inc. Client Sample ID: AB4-FB3-121509- Air Client Project ID: PGA North I 14682.013 (PSL0870)


EPA T0-15 Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Sununa Canister

1SC00721






Initiiil Pressure 2 (psig):

0.2



CAS# Compound Result MRL Result MRL Data flg/m3 flg/m3 ppbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.1 ND 0.54 141-78-6 Ethyl Acetate ND 4.3 ND 1.2 110-54-3 n-Hexane ND 2.1 ND 0.60 67-66-3 Chlorofmm ND 2.1 ND 0.44 109-99-9 Tetrahydrofuran (TI:j:F) ND 2.1 ND 0.72 107-06-2 1 ,2-Dichloroethane ND 2.1 ND 0.53 71-55-6 1,1, 1-Trichloroethane ND 2.1 ND 0.39 71-43-2 Benzene ND 2.1 ND 0.67 56-23-5 Carbon Tetrachloride ND 2.1 ND 0.34 110-82-7 Cyclohexane ND 4.3 ND 1.2 78-87-5 1,2-Dichloropropane ND 2.1 ND 0.46 75-27-4 Bromodichloromethane ND 2.1 ND 0.32 79-01-6 Trichloroethene ND 2.1 ND 0.40 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 2.1 ND 0.46 142-82-5 n-Heptane ND 2.1 ND 0.52 10061-01-5 cis-1 ,3-Dichloropropene ND 2.1 ND 0.47 108-10-1 4-Methyl-2-pentanone ND 2.1 ND 0.52 10061-02-6 trans-1 ,3-Dichloropropene ND 2.1 ND 0.47 79-00-5 1,1 ,2-Trichloroethane ND 2.1 ND 0.39 108-88-3 Toluene 2.7 2.1 0.71 0.56

ND = Compound was analyzed for, but ·not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

P0904355_T015_0912301144_SS.xls- Satwle (5)

0 I I Verified By: __ I"--'---"·(~·,-------'Date~01 ~sc~~xl! ~NL _ PageNo.: 23


RESULTS OF ANALYSIS

Page 3 of3

Client: Test America, Inc. CAS Project ID: P0904355 CAS Sample ID: P0904355-005 Client Sample ID: AB4-FB3-121509- Air



EPA T0-15 Tekmar AUTOCAN/Agilent 5973ineli/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00721

Initial Pressure (psi g):




Initial Pressure 2 (psi g):

0.2



CAS# Compound Result MRL Result MRL Data llg/m' f.lg/m' ppbV ppbV Qualifier

591-78-6 2-Hexanone ND 2.1 ND 0.52 124-48-1 Dibromochloromethane ND 2.1 ND 0.25 106-93-4 1 ,2-Dibromoethane ND 2.1 ND 0.28 127-18-4 Tetrachloroethene ND 2.1 ND 0.31 108-90-7 Chloro benzene ND 2.1 ND 0.46 100-41-4 Ethylbenzene ND 2.1 ND 0.49 179601-23-1 m,p-Xylenes ND 4.3 ND 0.98 75-25-2 Bromofom1 ND 2.1 ND 0.21 100-42-5 Styrene ND 2.1 ND 0.50 95-47-6 o-Xylene ND 2.1 ND 0.49 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.1 ND 0.31 622-96-8 4-Ethyltoluene ND 2.1 ND 0.43 108-67-8 1,3,5-Trimethylbenzene ND 2.1 ND 0.43 95-63-6 1 ,2,4-Trimethy1benzene ND 2.1 ND 0.43 100-44-7 Benzyl Chloride ND 2.1 ND 0.41 541-73-1 1,3-Dichlorobenzene . ND 2.1 ND 0.35 106-46-7 1,4-Dichlorobenzene ND 2.1 ND 0.35 95-50-1 1 ,2-Di?hloro benzene ND 2.1 ND 0.35 120-82-1 1 ,2,4-Trichlorobenzene ND 2.1 ND 0.29 87-68-3 Hexachloro butadiene ND 2.1 ND 0.20 593-60-2 Vinx:l Bromide ND 2.1 ND 0.49

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.'

\() I Verified By: __ \(.____,lo_r _____ Date: ~ !:o / ( o '24" P0904355_T015_09!230!144_SS.xls ·Sample (5) T0!5scan.xls • NL. PagcNo.:


Client: Test America, Inc. Client Sample ID: AB4-TB1-121509- Air Client Project ID: PGA North I 14682.013 (PSL0870)


RESULTS OF ANALYSIS

Page 1 of3




CAS# Compound Result MRL ltgfm3 [:!:g/m3

115-07-1 Propene ND 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) ND 1.3 74-87-3 Chloromethane ND 1.3

76-14-2 1 ,2-Dichloro-1,1,2,2-tetrafluoroethane (CFC 114) ND 1.3

75-01-4 Vinyl Chloride ND 1.3 106-99-0 1,3-Butadiene ND 1.3 74-83-9 Brotnomethane ND 1.3 75-00-3 Chloroethane ND 1.3 67-64-1 Acetone ND 13 75-69-4 Trichlorofluoromethane ND 1.3 67-63-0 2-Propanol (Isopropyl Alcohol) ND 2.5 75-35-4 1,1-Dichloroethene ND 1.3 75-09-2 Methyl~ne Chloride ND 1.3 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 1.3 76-13-1 Trichlorotrifluoroethane ND 1.3 75-15-0 Carbon Disulfide ND 13 156-60-5 trans-1 ,2-Dichloroethene ND 1.3 75-34-3 1, 1-Dichloroethane ND 1.3 1634-04-4 Methyl tert-Butyl Ether ND 1.3 108-05-4 Vinyl Acetate ND 13 78-93-3 2-Butanone (MEK) ND 13

ND = Compound was analyzed for, but not detected above the laboratory repmting limit.

CAS Project ID: P0904355 CAS Sample ID: P090435.5-006

Date Collected: 12/15/09 Date Received: 12118/09 Date Analyzed: 12/21109



Result MRL Data ppbV ppbV Qualifier.

ND 0.73 ND 0.25 ND 0.61

ND 0.18 ND 0.49 ND 0.57 ND 0.32 ND 0.47 ND 5.3 ND 0.22 ND 1.0 ND 0.32 ND 0.36 ND 0.40 ND 0.16 ND 4.0 ND 0.32 ND 0.31 ND 0.35 ND 3.6 ND 4.2

MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Verified By: __ ___,_'\?""-(""',...._. __ ____;Date: _ _.l-~.l-'-'b...ll_,_,l D""'---P0904355_TOI5_0912301144_S,S.xls. Sample (6) roisscan.xls · NL· PngeNo.:

·-'""'

.... ~.

. COLUMBIA ANALYTICAL SERVICES, INC.



RESULTS OF ANALYSIS

Page 2 of3




CAS# Compound Result MRL 11-g/m3 ~-tg/ma

156-59-2 cis-1 ,2~Dichloroethene ND 1.3 141-78-6 Ethyl Acetate ND 2.5 110-54-3 n-Hexane ND 1.3 67-66-3 Chlorofonn ND 1.3 109-99-9 Tetrahydrofuran (THF) ND 1.3 107-06-2 1,2-Dichloroethane ND 1.3 71-55-6 1,1, 1-Trichloroethane ND 1.3 71-43-2 Benzene' ND 1.3 56-23-5 Carbon Tetrachloride ND 1.3 110-82-7 Cyclohexane ND 2.5 78-87-5 1 ,2-Dichloropropane ND 1.3 75-27-4 Bromodichloromethane ND 1.3 79-01-6 Trichloroethene ND 1.3 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 1.3 142-82-5 n-Heptane ND 1.3 10061-01-5 cis-1 ,3-Dichloropropene ND 1.3 108-10-1 4-Methyl-2-pentanone ND 1.3 10061-02-6 trans-1 ,3-Dichloropropene ND 1.3 79-00-5 1,1 ,2-Trichloroethane ND 1.3 108-88-3 Toluene ND 1.3

ND = Compound was analyzed for, .but not detected above the laborat01y reporting limit.





Result MRL Data ppbV ppbV Qualifier

ND 0.32 ND 0.69 ND 0.35 ND 0.26 ND 0.42 ND 0.31 ND 0.23 ND 0.39 ND 0.20

ND 0.73 ND 0.27 ND 0.19 ND 0.23 ND 0.27 ND 0.31 ND 0.28 ND 0.31 ND 0.28 ND 0.23 ND 0.33

MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

.. ~-~-

Verified By: ___ ~l--'-.--""'0---------'Date: II b I 10 26 __ _ P0904355_TOI5_0912301 144_SS.xls- Sample (6) T015scnn.xls ~ NL- PageNo.:




RESULTS OF ANALYSIS

Page 3 of3




CAS# Compound Result MRL ).lg/m3 J.lg/m3

591-78-6 2-Hexanone ND 1.3 124-48-1 Dibromochloromethane ND 1.3 106-93-4 1,2-Dibromoethane ND L3 127-18-4 Tetrachloroethene ND 1.3 108-90-7 Chlorobenzene ND 1.3 100-41-4 Ethylbenzene ND 1.3 179601-23-1 m,p-Xylenes ND 2.5 75-25-2 Bromoform ND 1.3 100-42-5 Styrene ND 1.3 95-47-6 a-Xylene ND 1.3 79-34-5 1,1 ,2,2-Tetrachloroethane ND 1.3 622-96-8 4-Ethyl toluene ND 1.3 108-67-8 1,3 ,5-Trimethylbenzene ND 1.3 95-63-6 1 ,2,4-Trimethylbenzene ND 1.3 100-44-7 Benzyl Chloride ND 1.3 541-73-1 1 ,3-Dichlorobenzene ND 1.3 106-46-7 1,4-Dic~1lorobenzene ND 1.3 95-50-1 1,2-Dichlorobenzene ND 1.3 120-82-1 1,2,4-Trichlorobenzene ND 1.3 87-68-3 Hexachlorobutadiene ND 1.3 593-60-2 Vinyl Bromide ND 1.3

ND = Compound was analyzed for, but not detected above the laboratory reporting limit.


Date Collected: 12115/09 Date Received: 12/18/09· Date Analyzed: .12/21/09



Result MRL Data· . ppbV ppbV Qualifier

ND 0.31 ND 0.15 ND 0.16 ND 0.18 ND 0.27 ND 0.29 ND 0.58 ND 0.12 ND 0.29 ND 0.29 ND 0.18 ND 0.25 ND 0.25 ND 0.25 ND 0.24 ND 0.21 ND 0.21 ND 0.21 ND 0.17 ND 0.12 ND 0.29

MRL = Method Reporting Limit - The minimum quantity of a target anal)ite that can: be confidently detennined by the referenced method.

Verified By: ___ \2-,___,\:J-,_· ___ Date:. _ __,\L'..l ~6'-'-\ ..__,l o"'---P0904355_T015_0912301144_SS.xls- Sample (6) TOJSscan.xls- NL • PageNo.:

... ..


RESULTS OF ANALYSIS

Page I of3





1SC00184


Date Collected: 12115/09 Date Received: 12/18/09 Date Analyzed: 12/21/09



Canister Dilution Factor: 1.7 4

CAS# Compound Result MRL Result MRL Data IJ.g/m3 ~Lg/m3 ppbV ppbV Qualifier

115-07-1 Propene 140 2.2 84 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) 2.3 2.2 0.47 0.44 74-87-3 Chloromethane ND 2.2 ND 1.1

76-14-2 1 ,2-Dichloro-1, 1 ,2,2-tetrafluoroethane (CFC 114) ND 2.2 ND 0.31

75-01-4 Vinyl Chloride ND 2.2 ND 0.85 106-99-0 1,3-Butadiene 17 2.2 7.9 0.98 74-83-9 Bromo methane ND 2.2 ND 0.56 75-00-3 Chloroethane ND 2.2 ND 0.82 67-64-1 Acetone 1,900 22 790 9.2 75-69-4 TrichlorQfluoromethane 23 2.2 4.1 0.39 67-63-0 2-Propanol (Isopropyl Alcohol) 4.4 4.4 1.8 1.8 75-35-4 1,1-Dichloroethene · ND 2.2 ND 0.55 75-09-2 Methylene Chloride ND 2.2 ND 0.63 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.2 ND 0.70 76-13-1 Trichlorotrifluoroethane ND 2.2 ND 0.28 75-15-0 Carbon Disulfide ND 22 ND 7.0 156-60-5 trans-1 ,2-Dichloroethene ND 2.2 ND 0.55 75-34-3 1,1-Dichloroethane ND 2.2 ND 0.54 1634-04-4 Methyl tert-Butyl Ether ND 2.2 ND 0.60 108-05-4 Vinyl Acetate ND 22 ND 6.2 78-93-3 2-Butanone (MEK) 34 22 11 7.4

ND = Compound was analyzed for, but not detected above the laborat01y reporting limit. _ MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

.. ~ ..

.. , ...

Verified By: __ __:__)2._--\:.J"""' _---·--~-Date: '\ I 6 \ 1 o 28··· P0904355_TOI5_0912301 144_SS.xls- Sample (7) T015scan.xls- NL- PageNo.:


RESULTS OF ANALYSIS

Page 2 of3





1SC00184


Date Collected: 12/15/09 Date Received: 12118/09 Date Analyzed: 12/21109'



Initial :Pressure 2 (psig): 0.9 Final Pressure 2 (psig): 10.3

Canister Dilution Factor: 1. 7 4

CAS# Compound Result MRL Result MRL Data llgfm3 J.tg/m3 _epbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.2 ND 0.55 141-78-6 Ethyl Acetate ND 4.4 ND 1.2 110-54-3 n-Hexane 11 2.2 3.2 0.62 67-66-3 Chlorofo'rm 4.3 2.2 0.87 0.45 109-99-9 Tetrahydrofiiran (THF) ND 2.2 ND 0.74 107-06-2 1 ,2-Dichloroethane ND 2.2 ND 0.54 71-55-6 1,1, 1-Trichloroethane ND 2.2 ND 0.40 71-43-2 Benzene 6.0 2.2 1.9 0.68 56-23-5 Carbon Tetrachloride ND 2.2 ND 0.35 110-82-7 Cyclohexane ND 4.4 ND 1.3 78-87-5 1,2-Dichloropropane ND 2.2 ND 0.47 75-27-4 Bromodichloromethane ND 2.2 ND 0.32 79-01-6 Trichloroethene 9.1 2.2 1.7 0.40 540-84-1 2,2,4-Trimethy1pentane (Isooctane) ND 2.2 ND 0.47 142-82-5 n-Heptane 9.3 2.2 2.3 0.53 10061-01-5 cis-1 ,3-Dichloropropene ND 2.2 ND 0.48 108-10-1 4-Methyl-2-pentanone ND 2.2 ND 0.53 10061-02-6 trans-1 ;3~Dich1oropropene ND 2.2 ND 0.48 79-00-5 1,1 ,2-Trichloroethane ND 2.2 ND 0.40 108-88-3 Toluene 38 2.2 10 0.58

ND = Compound was analyzed for, but not detected above the laboratory repmting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confiqently determined by the referenced method ..

--~···--

Verified By: __ ~~="='· ,___ __ __;Date: J l6 \ l o 2 9 -··-'-P0904355_TOI5_0912301144_SS.xls ·Sample (7) TOI5scan.xls ~ NL. PageNo.:



EPA T0-15

RESULTS OF ANALYSIS

Page 3 of3

Test Code: lnstmment ID: Analyst:

Tekmar AUTOCAN/Agilent 5973inert/6890NIMS8 WidaAng



Date Collected: 12115/09 Date Received: 12/18/09 Date Analyzed: 12/21/09


Initial Pressure (psig): -0.2 .Final Pressure (psig): 1.0

.Initial Pressure 2 (psig): 0.9 Final Pressure 2 (psig): 10.3


CAS# Compound Result MRL Result MRL Data p,g/m3 11g/m3 ppbV ppbV Qualifier

591-78-6 2-Hexanone 8.0 2.2 2.0 0.53 124-48-1 Dibromochloromethane ND 2.2 ND 0.26 106-93-4 1 ,2-Dibromoethane ND 2.2 ND 0.28 127-18-4 Tetrachloroethene ND 2.2 ND 0.32 108-90-7 Chloro benzene ND 2.2 ND 0.47 100-41-4 Ethylbenzene 3.1 2.2 0.72 0.50 179601-23-1 m,p-Xylenes 7.3 4.4 1.7 1.0 75-25-2 Bromoform ND 2.2 ND 0.21 100-42-5 Styrene ND 2.2 ND 0.51 95-47-6 o-Xylene 2.5 2.2 0.58 0.50 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.2 ND 0.32 622-96-8 4-Ethylto1uene ND 2.2 ND 0.44 108-67-8 1,3 ,5-Trimethylbenzene ND 2.2 ND 0.44 95-63-6 1 ,2,4-Trimethylbenzene ND 2.2 ND 0.44 100-44-7 Benzyl Chloride ND 2.2 ND 0.42 541-73-1 1 ,3-Dichlorobenzene ND 2.2 1\TD 0.36 106-46-7 1 ,4-Dichlorobenzene ND 2.2 ND 0.36 95-50-1 1 ,2-Dichlorobenzene ND 2.2 ND 0.36 120-82-1 1 ,2,4-Trichlorobenzene ND 2.2 ND 0.29 87-68-3 Hexachlorobutadiene ND 2.2 ND 0.20 593-60-2 Vinyl Bromide ND 2.2 ND 0.50

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

P0904355_T015_09!2301144_SS.xls- Sample (7) Verified By: __ ____,_~_·~_-___ Date::-::-:-c:---"\--'-:\ =.6:---'\.L.:I a"'-----

Totsscan.xts- NL- PageNo.: 30'


RESULTS OF ANALYSIS

Page 1 of3



Test Code: InstrumentiD: Analyst: Sampling Media: Test Notes: Container ID:

EPA T0-15 Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 Wida Ang 1.0 L Sununa Canister

1SC00047




Final Pressure (psig); 1.1 Initial Pressure 2 (psig): 1.1 Final Pressure 2 (psig):. 1b.3


CAS# Compound Result MRL Result MRL Data IJ.g/m3 Jlg/m3 ppbV ppbV Qualifier

115-07-1 Propene 290 2.2 170 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) ND 2.2 ND 0.45 74-87-3 Chloromethane ND 2.2 ND 1.1

76-14-2 1 ,2-Dichloro-1 ,1 ,2,2-tetrafluroethane (CF·c 114) ND 2.2 ND 0.32

75-01-4 Vinyl Chloride ND 2.2 ND 0.88 106-99-0 1,3-Butadiene 26 2.2 12 1.0 74-83-9 Bromomethane ND 2.2 ND 0.58 75-00-3 Chloroethane ND 2.2 ND 0.85 67-64-1 Acetone 2,700 90 1,100 38 D2 75-69-4 Trichlorofluoromethane 19 2.2 3.4 0.40 67-63-0 2-Propanol (Isopropyl Alcohol) 6.1 4;5 2.5 1.8 75-35-4 1,1-Dichloroethene ND 2.2 ND 0.56 75-09-2 Methylene Chloride ND 2.2 ND 0.64 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.2 ND 0.72 76-13-1 Trichlorotrifluoroethane ND 2.2 ND 0.29 75-15-0 Carbon Disulfide ND 22 ND 7.2 156-60-5 trans-1 ,2-Dichloroethene ND 2.2 ND 0.56 75-34-3 1,1-Dichloroethane ND 2.2 ND 0.55 1634-04-4 Methyl tert-Butyl Ether ND 2.2 ND 0.62 108-05-4 Vinyl Acetate ND 22 ND 6.4 78-93-3 2-Butanone (MEK) 51 22 17 7.6

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently dete1mined by the referenced method. D2 =Sample required.dilution due to high' concentration of target analyte.

P0904355_T015_0912301144_SS.xls. Sample (8) Verified By: __ _l€~b''-~-----'Date: _ __,1'-"l-=6'-\'-'l"""O"---

Toisscan.xis. NL. PageNo.:

Client: Client Sample ID: Client Project ID:



Test Americ·a, Inc. AB4-50-121509- Air PGA North I 14682.013 (PSL0870)

EPA T0-15

RESULTS OF ANALYSIS

Page 2 of3

Telm1ar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00047




Initial Pressure (psig): -0.7 Final Pressure (psig): 1.1



CAS# Compound Result MRL Result MRL Data !:!;g/m3 f.tg/m3 ppbV. ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.2 ND 0.56 I41-78-6 Ethyl Acetate ND 4.5 ND 1.2 110-54-3 n-Hexane

. ' 21 2.2 6.0 0.64

67-66-3 Chloroform 4.9 2.2 1.0 0.46 109-99-9 Tetra~ydrofuran (THF) ND 2.2 ND 0.76 107-06-2 I ,2-Dichloroethane ND 2.2 ND 0.55 71-55-6 1, I, 1-Trichloroethane ND 2.2 ND 0.41 71-43-2 Benzene 8.7 2.2 2.7 0.70 56-23-5 Carbon Tetrachloride ND 2.2 ND 0.36 110-82-7 Cyclohexane ND 4.5 ND 1.3 78-87-5 1,2-Dichloropropane ND 2.2 ND 0.48 75-27-4 Bromodichloromethane ND 2.2 ND 0.33 79-01-6 Trichloroethene 13 2.2 2.4 0.42 540-84-I 2,2,4-Trimethylpentane (Isooctane) ND 2.2 ND 0.48 142-82-5 ll-Heptane 17 2.2 4.1 0.55 10061-0I-5 cis-1 ,3-Dichloropropene ND 2.2 ND 0.49 108-10-1 4-Methyl-2-pentanone 2.5 2.2 0.61 0.55 I0061-02-6 trans-1 ,3-Dichloropropene ND 2.2 ND 0.49 79-00-5 1,1 ,2-Trichloroethane ND 2.2 ND 0.41 108-88-3 Toluene 41 2.2 11 0.59


Verified By: __ --'X=L.=E._,_r ____ .Date: _ __,_l _,__j ,..,b,__,_\_,_1 -=0'---_ 32···=· P09043SS_TOIS_0912301144_SS.xls • S•mple (8) T015scan.xls ~ NL- PageNo.:


RESULTS OF ANALYSIS

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EPA T0-15 Tekmar AUTOCAN(Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00047





Final Pressure (psig): 1.1 Initial Pressure 2 (psig): 1.1 Final Pressure 2 (psi g): 10.3

Canister Dilution Factor: I. 79

P0904355_T015_0912301144_SS.xls- Sample (8) Verified By: __ ____,_\2-_...,c.,L..------'Date: db J1 o

T015scan.x!S ~ NL- PageNo.:

33 ...... ..


RESULTS OF ANALYSIS

Page I of3





1SC00052



Volume(s) Analyzed: 0.40 Lite_r(s)



CAS# Compound Result MRL Result MRL Data 1-1-glm3 ~-tg/m3 ppbV PEbV Qualifier

115-07-1 Propene 77 2.3 . 45 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) ND 2.3 ND 0.46 74-87-3 Chloromethane ND 2.3 ND 1.1

76-14-2 1 ,2-Dichloro-1, 1 ,2,2-tetrafluorqethane (CFC 114) ND 2.3 ND 0.33

75-01-4 Vinyl Chloriqe ND 2.3 ND 0.90 106-99-0 1,3-Butadiene 12 2.3 5.5 1.0 74-83-9 Bromomethane ND 2.3 ND 0.59 75-00-3 Chloroethane ND 2.3 ND 0.87 67-64-1 Acetone 2,200 23 930 9.6 75-69-4 Trichlorofluoromethane 9.7 2.3 1.7 0.41 67-63-0 2-Propanol (Isopropyl Alcohol) 6.6 4.6 2.7 1.9 75-35-4 1,1-Dichloroethene ND 2.3 ND 0.58 75-09-2 Methylene Chloride ND 2.3 ND 0.66 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.3 ND 0.73 76-13-1 Trichlorotrifluoroethane 2.9 2.3 0.37 0.30 75-15-0 Carbon Disulfide ND 23 ND 7.3 156-60-5 trans- I ,2-Dichloroethene ND 2.3 ND 0.58 75-34-3 I, 1-Dichloroethane ND 2.3 ND 0.57 1634-04-4 Methyl lett-Butyl Ether ND 2.3 ND. 0.63 108-05-4 Vinyl Acetate ND 23 ND 6.5 78-93-3 2-Butanone (MEK) 56 23 19 7.8

ND = Compound was analyzed for, but not detected above the laboratoty reporting limit. MRL = Method Reporting ~imit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

.. ., ....

Verified By: __ -"'.\L=>...;· •.-=--· ___ Date:_--"-'ll"""'b'-'\-'-'1 c,_,_:;, __ -34 '" P0904355_T015_0912301144_SS.xls ·Sample (9) T015scan.xls · NL- PageNo.:

Client: Client Sample ID: Client Project ID:


CAS#

156-59-2 141-78-6 110-54-3 67-66-3 109-99-9 107-06-2 71-55-6 71-43-2 56-23-5 110-82-7 78-87-5 75-27-4 79-01-6 540-84-1 142-82-5 10061-01-5 108-10-1 10061-02-6 79-00-5 108-88-3

COLUJ\1BIA ANALYTICAL SERVICES, INC.

Test America, Inc. AB4-60-121509- Air PGA North I 14682.013 (PSL0870)

EPA T0-15

RESULTS OF ANALYSIS

Page2 of3

Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Summa Canister

1SC00052


Date Collected: 12/15/09 pate Received: 12/18/09 Date Analyzed: 12/21/09


Initial Pressure (psig): -0.6 Final Pressure (psig): 1.1



Compound .Result MRL Result MRL Data ).lg/m3 )Lg/m3 ppbV ppbV Qualifier

cis-1 ,2-Dichloroethene ND 2.3 ND 0.58 Ethyl Acetate ND 4.6 ND 1.3 n-Hexane 12 2.3 3.3 0.65 Chloroform 23 2.3 4.7 . 0.47 Tetrahydrofuran (THF) ND 2.3 ND 0.78 1,2-Dichloroethane ND 2.3 ND. 0.57 1,1, 1-Tric.hloroethane ND 2.3 ND 0.42 Benzene 7.9 2.3 2.5 0.72 Carbon Tetrachloride ND 2.3 ND 0.36 Cyclohexane ND 4.6 ND 1.3 1 ,2-Dichloropropane ND 2.3 ND 0.50 Bromodichloromethane ND 2.3 ND 0.34 Trichlon~ethene 100 2.3 19 0.43 2,2,4-Trimethylpentane (lsooctane) ND 2.3 ND 0.49 n-Heptane 12 2.3 3.0 0.56 cis-1 ,3-Dichloropropene ND 2.3 ND 0.50 4-Methyl-2-pentanone ND 2.3 ND 0.56 trans-1 ,3-Dichloropropene ND 2.3 ND 0.50 1,1 ,2-Trichloroethane ND 2.3 ND 0.42 Toluene 45 2.3 12 0.61

ND = Compound was analyzed for, but not detected above the laboratory repo1ting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently determined by the referenced method.

Verified By: ___ g"--'=z.,_--____ D.ate: _ ___.~'-"-[_,b'-'-1 _,_( D:::::' __ 35 P0904355_T015_0912301144_SS.xls- Sample (9) T015scan.xls • NL· PngeNo.:

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-


RESULTS OF ANALYSIS

Page 3 of3






1SC00052


Date Collected; 12/15/09 Date Received: 12/18/09 Date Analyzed: 12/21/09





CAS# Comp'ound Result MRL Result MRL Data 11glm3 f.Lg/m3 ppbV ppbV Qualifier.

591-78-6 2-Hexanone 8.2 2.3 2.0 0.56 124-48-1 Dibromochloromethane ND 2.3 ND 0.27 106-93-4 1,2-Dibromoethane ND 2.3 ND 0.30 127-18-4 Tetrachloroethene ND 2.3 ND 0.34 108-90-7 Chlorobenzene ND 2.3 ND 0.50 100-41-4 Ethylbenzene 3.9 2.3 0.90 0.53 179601-23-1 m,p-Xylenes 9.5 4.6 2.2 1.1 75-25-2 Bromoform ND 2.3 ND 0.22 100-42-5 Styrene ND 2.3 ND 0.54 95-47-6 o-Xylene 3.3 2.3 0.76 0.53 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.3 ND 0.33 622-96-8 4-Ethyltoluene ND 2.3 ND 0.47 108-67-8 1,3 ,5-Trimethylbenzene ND 2.3 ND 0.47 95-63-6 1 ,2,4-Trimethylbenzene ND 2.3 ND 0.47 100-44-7 Benzyl Chloride ND 2.3 ND 0.44 541-73-1 1 ,3-Dichlorobenzene ND 2.3 ND 0.38 106-46-7 1 A-Dichlorobenzene ND 2.3 ND 0.38 95-50-1 1 ,2-Dichlorobenzene ND 2.3 ND 0.38 120-82-1 1 ,2,4-Trichlorobenzene ND 2.3 ND 0.31 87-68-3 Hexachlorobutadiene ND 2.3 ND 0.21 593-60-2 Vinyl Bromide ND 2.3 ND 0.52

ND = Compound was analyzed for, but not detected above the laboratOJy reporting limit. MRL = Method Rep01ting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

P0904355_T015_0912301144_SS.xls- Sample (9) Verified By: __ __,__-H-'-'-" _____ Date: ll 6\ I D 36 ·

T015scan.xls- NL- PageNo.:

-··•··"

COLUMBIA ANALYTICAL SERVICES, INC ..

RESULTS OF ANALYSIS

Page 1 of3





1SC00727


Date Collected: 12/15/09 Date Received: 12/18/09 Date Analyzed: 12121/09


Final Pressure (psig): 1.1 Initial Pressure 2 (psig): · 1.1 Final Pressure 2 (psig): 10.0


CAS# Compound Result MRL Result MRL Data f.\cg/m3 l-lg/m3 ppbV ppbV Qualifier

115-07-1 Propene 110 2.1 61 1.2 75-71-8 Dichlorodifluoromethane (CFC 12) ND 2.1 ND 0.43 74-87-3 Chloromethane ND 2.1 ND 1.0

76-14-2 1 ,2-Dichloro-1, 1 ,2,2-tetrafluoroethane ( CFC 114) ND 2.1 ND 0.30

75-01-4 Vinyl Chloride ND 2.1 ND 0.83 106-99-0 1,3-Butadiene 19 2.1 8.7 0.96 74-83-9 Bromomethane ND 2.1 ND 0.55 75-00-3 Chloroethane ND 2.1 ND 0.81 67-64-1 Acetone 780 21 330 8.9 75-69-4 Trichlorofluoromethane 3.1 2.1 0.56 0.38 67-63-0 2-Propanol (Isopropyl Alcohol) 4.5 4.3 1.8 1.7 75-35-4 1,1-Dichloroethene - ND 2.1 ND 0.54 75-09-2 Methylene Chloride ND 2.1 ND 0.61 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.1 ND 0.68 76-13-1 Trichlorotrifluoroethane 7.9 2.1 1.0 0.28 75-15-0 Carbon D,isulfide ND 21 ND 6.8 156-60-5 trans-1 ,2-Dichloroethene ND 2.1 ND 0.54 75-34-3 1,1-Dichloroethane ND 2.1 ND 0.53 1634-04-4 Methyl tert-Butyl Ether ND 2.1 ND 0.59 108-05-4 ·Vinyl Acetate ND 21 ND 6.0 78-93-3 2-Butanone (MEK) 45 21 15 7.2

ND =Compound was analyzed for, but not detected above the laboratory reporting limit. MRL =Method Rep01ting Limit- The minimum quantity of a target analyte that can be confidently detennined by the referenced metho~.

Verified By: __ .xl?:::;'..:.z· =--------:--D.ate: ll bi I. D 37 P0904355_T015_0912301144_SS.x!s- Sample (10) T015scnn.xls- NL- PageNo.:

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RESULTS OF ANALYSIS

Page 2 of3


CAS Sample ID: P0904355-010 Client Project ID: PGANorth I 14682.013 (PSL0870)



1SC00727


Date Collected: 12/15/09 Date Received: 12/18/09 Date Analyzed: 12/21/09·



Initial ]:>ressure 2 (psig): 1.1 Final Pressure 2 (psig): 10.0


CAS# Compound Result MRL Result MRL Data )lg/m3 ~g/m3 ppbV ppbV Qualiffer

156-59-2 · cis-1 ,2-Dichloroethene ND 2.1 ND 0.54 141-78-6 Ethyl Acetate ND 4.3 ND 1.2 110-54-3 n-He:X:ane 13 2.1 3.7 0.60 67-66-3 Chloroform 25 2.1 5.2 0.44 109-99-9 Tetrahydrofuran (THF) ND 2.1 ND 0.72 107-06-2 1,2-Dichloroethane ND 2.1 ND 0.53 71-55-6 1,1, 1-Trichloroethane ND 2.1 ND 0.39 71-43-2 Benzene 10 2.1 3.2 0.67 56-23-5 Carbon Tetrachloride ND 2.1 ND 0.34 110-82-7 Cyclohexane ND 4.3 ND 1.2 78-87-5 1 ,2-Dichloropropane ND 2.1 ND 0.46 75-27-4 Bromodichloromethane ND 2.1 ND 0.32 79-01-6 Trichloroethene 170 2.1 32 0.40 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 2.1 ND 0.46 142-82-5 n-Heptane 15 2.1 3.6 0.52 10061-01-5 cis-1 ,3-Dichloropropene ND 2.1 ND 0.47 108-10-1 4-Methyl-2-pentanon~ ND 2.1 ND 0.52 10061-02-6 trans-1 ,3-Dichloropropene ND 2.1 ND 0.47 79-00-5 1,1 ,2-Trichloroethane ND 2.1 ND 0.39 108-88-3 Toluene 44 2.1 12 0.56

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL = Method Reporting Limit - The minimum quantity of a target analyte that can be confidently detem1ined by the referenced method.

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Verified By: ____ \'-) _:,.,;__ ____ D.ate: I ->· T~O~lSs-cM~t_~x:~_l~l~?~Pa-ge-No-.:

38 ,;., P0904355_T015_0912301144_SS.xl' ·Sample (10)


RESULTS OF ANALYSIS

Page 3 of3


. CAS Project ID: P0904355 CAS Sample ID: P090435~-010



EPA T0-15 Tekmar-AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1 .0 L Summa Canister

1SC00727





Initial Pressure 2 (psig): 1 . 1 Final Pressure 2 (psig): 10.0


CAS# CompomJd Result MRL Result MRL Data ltg/m3 f.lg/m3 ppbV ppbV Qualifier

591-78-6 2-Hexanone 7.1 2.1 1.7 0.52 124-48-1 Dibromochloromethane ·ND 2.1 l'ID 0.25 106-93-4 1 ,2-Dibromoethane ND 2.1 ND 0.28 127-18-4 Tetrachloroethene ND 2.1 ND 0.31 108-90-7 Chi oro benzene ND 2.1 ND 0.46 100-41-4 Ethylbenzene 3.7 2.1 0.86 0.49 179601-23-1 . m,p-Xylenes 8.8 4.3 2.0 0.98 75-25-2 Bromoform ND 2.1 ND 0.21 100-42-5 Styrene ND 2.1 ND 0.50 95-47-6 o-Xylene 3.1 2.1 0.71 0.49 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.1 ND 0.31 622-96-8 4-Ethyltpluene ND 2.1 ND 0.43 108-67-8 1,3 ,5-Trimethylbenzene ND 2.1 ND 0.43 95-63-6 1 ,2,4-Ti-imethylbenzene ND 2.1 ND 0.43 100-44-7 Benzyl Chloride ND 2.1 ND 0.41 541-73-1 1 ,3-Dichloro benzene ND 2.1 ND 0.35 106-46-7 1 ,4-Dichlorobenzene ND 2.1 ND 0.35 95-50-1 1 ,2-Dichlorobenzene ND 2.1 ND 0.35 120-82-1 1 ,2,4-Trichlorobenzene ND 2.1 ND 0.29 87-68-3 Hexachlorobutadiene ND 2.1 ND 0.20 593-60-2 Vinyl Bromide ND 2.1 ND 0.49


P0904355_T015_0912301144_SS,xls ·Sample (I 0) Verified By: __ _,'l:..1' ..>..L..L ______ D.ate: ll bIt o

£::f. T-0-15-scan--'-.+-)u.=. N'-'-L-'-'-=Pa-ge-No-.:

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RESULTS OF ANALYSIS

Page I of3

Client: Test America, Inc. Client Sample ID: AB4-70-121509- Air CAS ProjectiD: P0904355


Test Code: Instmment ID: Analyst: Sampling Media: Test Notes: Container ID:


1SC00213






CAS# Compound Result MRL Result MRL Data ~-tg/m3 !:!:g/m3 ppbV ppbV Qualifier

115-07-1 Propene po 2.2 62 1.3 75-71-8 Dichlorodifluoromethane (CFC 12) ND 2.2 ND 0.45 74-87-3 Chloromethane ND 2.2 ND 1.1

76-14-2 1 ,2-Dichloro-1, 1 ,2,2-tetrafluoroethane (CFC 114) ND 2.2 ND 0.32

75-01-4 Vinyl Chloride ND 2.2 ND 0.88 106-99-0 1,3-Butadiene 20 2.2 8.8 1.0 74-83-9 B romomethane ND 2.2 ND 0.58 75-00-3 Chloroethane ND 2.2 ND 0.85 67-64-1 Aceton·e 770 22 320 9.4 75-69-4 Trichlorofluoromethane 3.1 2.2 0.56 0.40 67-63-0 2-Propanol (Isopropyl Alcohol) ND 4.5 ND 1.8 75-35-4 1,1-Dichloroethene ND 2.2 ND 0.56 75-09-2 Methylene Chloride ND 2.2 ND 0.64 107-05-1 3-Chloro-1-propene (Allyl Chloride) ND 2.2 ND 0.72 76-13-1 Trichlorotrifluoroethane 8.0 2.2 1.0 0.29 75-15-0 Carbon Disulfide ND 22 ND 7.2 156-60-5 trans-1 ,2-Dichloroethene ND 2.2 ND 0.56 75-34-3 1, 1-Dichloroethane ND 2.2 ND 0.55 1634-04-4 Methyl tert-Butyl Ether ND 2.2 ND 0.62 108-05-4 Vinyl Acetate ND 22 ND 6.4 78-93-3 2-Butanone (MEK) 44 22 15 7.6

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL =Method Reporting Limit- The minimum quantity of a target analyte that can be confidently detetmined by the referenced method.

VerifiedBy: __ _,_,!(>-U,-c-:__ __ _;Date: l/6\lo 40 P0904355_T015_0912301144_SS.xls- Srunple (I I) T015scan.xl'- NL- PageNo.:


RESULTS OF ANALYSIS

Page2 of3




EPA T0-15 Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1 .0 L Summa Canister

1SC00213


Date Collected: 12/15/09 Date Received: 12/18/09. Date Analyzed: 12/21/09





CAS# Compound Result MRL Result MRL Data-M-glm3 M-glm3 ppbV ppbV Qualifier

156-59-2 cis-1 ,2-Dichloroethene ND 2.2 ND 0.56 141-78-6 Ethyl Acetate ND 4.5. ND 1.2 110-~4-3 n-Hexane 13 2.2 3.8 0.64 67-66-3 Chloroform 26 2.2 5.3 0.46 109-99-9 Tetrahydrofuran ·(THF) ND 2.2 ND 0.76 107-06-2 1 ,2-Dichloroethane ND 2.2 ND 0.55 71-55-6 1,1, 1-Trichloroethane ND 2.2 ND 0.41 71-43-2 Benzene 10 2.2 3.2 0;70 56-23-5 Carbon Tetrachloride ND 2.2 ND 0.36 110-82-7 Cyclohexane ND 4.5 ND 1.3 78-87-5 1,2-Dichloropropane ND 2.2 ND 0.48 75-27-4 Bromodichloromethane ND 2.2 ND 0.33 79-01-6 Trichloroethene 170 2.2 32 0.42 540-84-1 2,2,4-Trimethylpentane (Isooctane) ND 2.2 ND 0.48 142-82-5 n-Heptane 15 2.2 3.7 0.55 10061-01-5 cis-1 ,3 -Dichloropropene ND 2.2 ND 0.49 108-10-1 4-Methyl-2-pentanone ND 2.2 ND 0.55 10061-02-6 trans-1 ,3-Dichloropropene ND 2.2 ND 0.49 79-00-5 1,1 ,2-Trichloroethane ND 2.2 ND 0.41 108-88-3 Toluene 45 2.2 12 0.59


Verified By: __ ....l':t=oc..>==· _· ------'Date: L lb \ I D 41 ... ~.:. P0904355_T015_0912301144_SS.xls- Sample (II) T015scan.xls- NL- PageNo.:


RESULTS OF ANALYSIS

Page 3 of3


CAS Project ID: P0904355 CAS Sample ID: P090435.5-011



EPA T0-15 Tekmar AUTOCAN/Agilent 5973inert/6890N/MS8 WidaAng 1.0 L Summa Canist~r

1SC00213






Canister Dilution Factor: 1. 79 .

CAS# Compound Result MRL Result MRL Data' IJ-g/m3 !J-g/1113 ppbV ppbV Qualifier·

591-78-6 2-Hexanone 6.7 2.2 1.6 0.55 124A8-1 Dibrotnochloromethane ND 2.2 ND 0.26 106-93-4 1,2-Dibromoethane ND 2.2 ND 0.29 127-18-4 Tetrachloroethene ND 2.2 ND 0.33 108-90-7 Chlorobenzene ND 2.2 ND b.49 100-41-4 Ethylbenzene 3.8 2.2 0.88 0.52 179601-23-1 m,p-Xyfenes 8.9 4.5 2.0 l.O 75-25-2 Bromofonn ND 2.2 ND 0.22 100-42-5 ·Styrene ND 2.2 ND 0.53 95-47-6 o-X~lene 3.1 2.2 0.72 0.52 79-34-5 1,1 ,2,2-Tetrachloroethane ND 2.2 ND 0.33 622-96-8 4-Ethyltoluene ND 2.2 ND 0.46 108-67-8 1,3 ,5-Trimethylbenzene ND 2:2 ND 0.46 95-63-6 1 ,2,4-Trimethylbenzene ND 2.2 ND 0.46 100-44-7 Benzyl Chlmide ND 2.2 ND 0.43 541-73-1 1 ,3-Dich1orobenzene ND 2.2 ND 0.37 106-46-7 1 A-Dichlorobenzene ND 2.2 ND 0.37 95-50-1 1,2-Dichlorobenzene ND 2.2 ND 0.37 120-82-1 1,2,4-'rrichlorobenzene ND 2.2 ND 0.30 87-68-3 Hexachlo'robutadiene ND 2.2 ND 0.21 593-60-2 Vinyl Bromide ND 2.2 ND 0.51

ND = Compound was analyzed for, but not detected above the laboratory reporting limit. MRL =Method Reporting Limit- The minimum quantity of a target analyte that can be confidently determined by the referenced method.

... ,.,:

.....

P0904355_T015_0912301144_SS.xls ·Sample (11) VerifiedBy: __ ---"~=·-·-___ Date: i\ hi (Q 42

sdms docid#1142198 test america …client: test america, inc. service request: p0904355 project: pga...

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