sampling data regarding shpack dump, case # 01318

61
SHPACK DUMP CASE# 01318 LAB: COMPUCHEM LABS SAMPLING DATES: 09/?0/8? - 09/20/82 (PART 1 OF 1 ) _>. i n

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Page 1: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

SHPACK DUMP

CASE 01318

LAB COMPUCHEM LABS

SAMPLING DATES 0908 - 092082

(PART 1 OF 1 )

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jjB^BB IIS ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management HjcH[ampil ORGANICS TRAFFIC REPORT mm^mm^mmmm copy Case Number copy SAMPLE CC )NCENTRATION reg qvn TU- I i- f i snip 10 riff^l [Ct^AiC J- T

(Cl ieck One)

LOW CJoncentration ffjft ^ if^CJC^ t Sample Site NameCode Mediu im Concentration

Attn SEP 2 7 1982 copy SAMPLEM ATRIX

(Check One) bull Transfer

gt WaterSoiia sdiment Ship To TP

0^lt-AAJ copy Regional Office- copy Por each sample collected sp ecify number (u) AnalysraquoLab Sampling Personnel of containers used and markvolume level Recd byY iX^SSLCL

on each bottle )ate Reed- Cgt3OltS

3-pt 7ykfi sample Condition on Receipt (eg broken n r JNaine) Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

(Phone) Water j gt Sampling Date (Extractable)

Water (Begin (find) (VOA) j W copy Shipping Information Soil Sediment

Water (ExtVOA)

Name of Camer Other

3X f ^ Date Shipped

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media 7shy Ground Water Solids

I eachate Other (specify)

Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office -1 IBJB 1 i gt- H - bull bull - S Ai bull bull lt - bull V j i r n i Zii 3 7 M i i 4lt] bull IS 5V7 2490 Sample Number

m ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNsme QC REQUIREMENTS SAMPLE CONCENTRATION

Case No bull 3(b Designate below OC (Check One)

ST jraquoh Sample ID No

analysis selected (If Applicable)

Low Concentration Medium Concentration

QC Report No Dunlicate SAMPLE MATRIX n (Check ftfl) OlW

Matrix Spike Water Soil Sfidirnent

Description Technician Signature Detail Below Pertinent Information and or DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins)

Preparation(VGA)

XT

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number D O Box 88 Alexcundria Virginia 22313 -703 557-2490 -FTS557-2490

8tLj ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Cjifst Nn Df^ciignatfihfilow QC

Itnln Sample in NOanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report Nn HT mlirate 0 SAMPLE MATRIX V 09 (Check One)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1262 ORGANICSi TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office _JL Sampling Personnel

(Name) a ft i ~4

(Phone) Sampling Date

y(Begin) (End)

copy Shipping Information

Name of Garner

Date Shipped

Airbill Number

(f) Sample Description

Surf ace Water

^_ Ground Water

Leachate

copy SAMPLE CONCENTRATION Ship To bull (Check One)

Low Concentration Medium Concentration SEP2713tt

SAMPLE MATRIX Attn^ bull bull Lt 1

(Check One)

_ Water Transfer

SoilSediment

(D For each sample collected specify number Analjrsis Lab of containers used and mark volume level Recd on each bottle Date Recd

Sample Condition Oil Receipt (eg broken nNumber of Approximateice Chain-of-Custcdy etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Qo) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No _

gt Sample ID No

lo Designate below QC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check

Matrix Spike __ Water __ SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

(

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

-60 S US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO K c x H l H AV-varvlna Virginia22313 703557-249OFTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

HaseNo

Lah Sample ID No

r)pgtsigrifltlt=gt helow QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QT Report No HT inliratft flQi SAMPLE MATRIX OQ (Check One)

Matrix Spike Water

raquo lt

SoilSediment

D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins bull

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

(Name)

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

v M - V l ( ^ -raquogt

Name of Camer

Date Shipped

Airbill Number

(D Sample Description

Surface Water

Ground Water

Leachate

(D SAMPLE CC DNCENTRATION (Clieck One)

t

bull LowC Joncentration Mediu im Concentration

(D SAMPLEM ATRIX (Check One) bullraquo

Water Soila kliment

0 Ship To

SEP 2 7 1982 Attn ^ A (

Transfer _ ^

ShnpTo 3^3(jUcJ0 (D For each sample collected sp ecify number copy Analysis Lgb -

of containers used and mark volume level Rlaquor-H KyHy X Sk^vSOil

on each bottle Date RlaquovH ^ vQ^Roi Sample Condition

Number of Approximate on Receipt (eg broken no Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) J

Water (VOA)

^

Soil Sediment

Water (Ext VOA)

Other

Mixed Media

Solids

Other (specify)

V

lt r M

(D Sample Location

(jo) Special Handling Instructions (eg safety precautions hazardous nature)

| n| US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^m^mfHgmmm

^SlU ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HHHIi

T^hName I QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - Designate below QC analysis selected Low Conrpmtration

T rraquoh Sample ID No (Tf Applicable) Medium Concentration

QH Report No Di mlirate SAMPLE MATRIX (Check One) - ^

Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

f

f gtfExtractionPreparation(Dioxins)

f

Preparation(VGA)

t

f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

1TOCT| US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^mamtnteammm

Kii8 ORGANICS LABORATORY CHRONICLE (ANALYSIS) HUH

Lh NAme QH REQI IIREMENTS SAMPLE CONCENTRATION (Check One)

naseNrv D^RignatfihelowQC analysis performed Low Concentration

I rah Sample ID No (Tf Applicable) Medium Concentration

QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

i

Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

f Surface Water

ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

Water SoilSediment Ship To 223

C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

IECTI US ENVIRONMENTAL PROTECTION AGENCY HWISomi lpgt Mrrn^^ejmpnt Offirv^

Kiiijga ORGANICS LABORATORY CHRONICLE (E laquo

T^hNamJ 1 QC REQUIREMENTS -m -m SAMPLE CONCENTRATION (Check One)

Case No V Designate below OC

T Ah Sample ID Npanalysis selected

(Tf Applicable) Low Concentration Medium Cnnrfiritrfltion

QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

shyi iv M-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull bull A p bull bull bull bull bull -CJ IW bull TI 7 M9U Sample Number

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

^ t

Preparation -^ (VGA) f i

f f+V- r ttfs r

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BPH| US ENVIRONMENTAL PROTECnON AGENCY HWISomj iPiimISiigi ORGANICS LABORATORY CHRONICLE (j

mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) Cast Nrgt_ nosignate hfilow QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

y Ground Water

T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

i

i BB US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^ bullbullbullbullbullptrade

Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

i bull - Containers Total Volume ice Chain-of-Custody etc)

(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullB l US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^KpHHRjllMg

KM^ OHGANICS LABORATORY CHRONICLE (ANALYSIS) ^H^^l ^Ht^^^ijB bull

Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

y Ground Water

Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

lt Water Cl_- Tgt ^)gt O jf

SoilSi sdiment Ship To Jgt7 nf )f

copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

iB^ffi US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^BpBlaquoraquoiippM

KiBJgll ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) ^jjjjjlj^

I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

y LowC loncentration Mediu im Concentration SEP 27 1981

0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

bullV

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

T flb Sample TD Nn

Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

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0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

jMf^yampH(Phone)

Sampling Date

(Begin) (End)

copy Shipping Information

JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

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Airbill Number

copy Sample Description

Surface Water

V firoiinH Water

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ij|fimT3ft ^^oncntioii on Receipt (eg broken ac Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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T^HN^TTifi 1 QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

JB^JI ORGANICS LABORATORY CHRONICLE (j

T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

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(jj) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

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Sample Condition On Receipt

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Sample Description copy (Check One) bdquo Surface Water

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Low Conctjnlidliun

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(T) Shipping Information Name Of Carrier

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LAB FILE COPY

(4) Ship To ^ bdquo 4

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Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

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Sample Description copy (Check One) Surface Water

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Solids Other

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MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

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Water

(J) Shipping Information

Name Of Carrier

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Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FJLE COPY

(4) Ship To

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Transfer Ship To

(5) ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

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Sample Description copy (Check One) bdquo Surface Water

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(specify) MATCHES ORGANIC SAMPLE NO

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Low CoiicenlidLion

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Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

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Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

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Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Matrix Spike Water Soil Sfidirnent

Description Technician Signature Detail Below Pertinent Information and or DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins)

Preparation(VGA)

XT

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number D O Box 88 Alexcundria Virginia 22313 -703 557-2490 -FTS557-2490

8tLj ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Itnln Sample in NOanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report Nn HT mlirate 0 SAMPLE MATRIX V 09 (Check One)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1262 ORGANICSi TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office _JL Sampling Personnel

(Name) a ft i ~4

(Phone) Sampling Date

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Name of Garner

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Airbill Number

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Low Concentration Medium Concentration SEP2713tt

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SoilSediment

(D For each sample collected specify number Analjrsis Lab of containers used and mark volume level Recd on each bottle Date Recd

Sample Condition Oil Receipt (eg broken nNumber of Approximateice Chain-of-Custcdy etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Qo) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No _

gt Sample ID No

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(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check

Matrix Spike __ Water __ SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

(

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

-60 S US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO K c x H l H AV-varvlna Virginia22313 703557-249OFTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

HaseNo

Lah Sample ID No

r)pgtsigrifltlt=gt helow QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QT Report No HT inliratft flQi SAMPLE MATRIX OQ (Check One)

Matrix Spike Water

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SoilSediment

D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins bull

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

(Name)

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

v M - V l ( ^ -raquogt

Name of Camer

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Airbill Number

(D Sample Description

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Number of Approximate on Receipt (eg broken no Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) J

Water (VOA)

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Soil Sediment

Water (Ext VOA)

Other

Mixed Media

Solids

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V

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(D Sample Location

(jo) Special Handling Instructions (eg safety precautions hazardous nature)

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T^hName I QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - Designate below QC analysis selected Low Conrpmtration

T rraquoh Sample ID No (Tf Applicable) Medium Concentration

QH Report No Di mlirate SAMPLE MATRIX (Check One) - ^

Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

f

f gtfExtractionPreparation(Dioxins)

f

Preparation(VGA)

t

f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Lh NAme QH REQI IIREMENTS SAMPLE CONCENTRATION (Check One)

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I rah Sample ID No (Tf Applicable) Medium Concentration

QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

f Surface Water

ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

Water SoilSediment Ship To 223

C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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Case No V Designate below OC

T Ah Sample ID Npanalysis selected

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QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull bull A p bull bull bull bull bull -CJ IW bull TI 7 M9U Sample Number

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

^ t

Preparation -^ (VGA) f i

f f+V- r ttfs r

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BPH| US ENVIRONMENTAL PROTECnON AGENCY HWISomj iPiimISiigi ORGANICS LABORATORY CHRONICLE (j

mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) Cast Nrgt_ nosignate hfilow QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

y Ground Water

T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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KM^ OHGANICS LABORATORY CHRONICLE (ANALYSIS) ^H^^l ^Ht^^^ijB bull

Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

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Airbill Number

Sample Description

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Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

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SoilSi sdiment Ship To Jgt7 nf )f

copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

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0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

T flb Sample TD Nn

Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

r^sgt TSIn noltignfli-ft below QC

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

bull7 o gt z Date Snipped

Airbill Number

0 Sample Description

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Learhate

0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

bull Water SouS adiment

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0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

f

ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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Hi ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) BHDIi

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - ~- Designate below OC analysis selected Low Concentration

T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

- bull 1 t

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

~~| T Ah NATTIlaquo QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) HARA Nn Designate below QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

jMf^yampH(Phone)

Sampling Date

(Begin) (End)

copy Shipping Information

JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

poundC) ~j ltypound

Airbill Number

copy Sample Description

Surface Water

V firoiinH Water

Leachate

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Mixed Media

Solids

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Pesticides

Dioxins

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Page 3: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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Low Concentration Medium Concentration

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Matrix Spike Water Soil Sfidirnent

Description Technician Signature Detail Below Pertinent Information and or DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins)

Preparation(VGA)

XT

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number D O Box 88 Alexcundria Virginia 22313 -703 557-2490 -FTS557-2490

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QT Report Nn HT mlirate 0 SAMPLE MATRIX V 09 (Check One)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1262 ORGANICSi TRAFFIC REPORT T) Case Number

Sample Site NameCode

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(Name) a ft i ~4

(Phone) Sampling Date

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Name of Garner

Date Shipped

Airbill Number

(f) Sample Description

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SoilSediment

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Sample Condition Oil Receipt (eg broken nNumber of Approximateice Chain-of-Custcdy etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Qo) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No _

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Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check

Matrix Spike __ Water __ SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

(

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

-60 S US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO K c x H l H AV-varvlna Virginia22313 703557-249OFTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(If Applicable) Low Concentration Medium Concentration

QT Report No HT inliratft flQi SAMPLE MATRIX OQ (Check One)

Matrix Spike Water

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SoilSediment

D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins bull

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

(Name)

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

v M - V l ( ^ -raquogt

Name of Camer

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Airbill Number

(D Sample Description

Surface Water

Ground Water

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(D SAMPLE CC DNCENTRATION (Clieck One)

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Number of Approximate on Receipt (eg broken no Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) J

Water (VOA)

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Soil Sediment

Water (Ext VOA)

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Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

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Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

i

Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

f Surface Water

ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

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C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

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(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

(|) Sample Description

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T earhate

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LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

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Surface Water Mixed Media

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Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Begin) (End)

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

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Other

(D Sample Location

Mixed Media

Solids

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copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

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Airbill Number

0 Sample Description

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copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

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(Begin) (End)

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Leachate

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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Water (Extractable) f

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SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

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) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

0 Sample Description

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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Sampling Date

(Begin) (End)

copy Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

copy Sample Description

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V firoiinH Water

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Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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0 SAMPLE MATRIX (Check One)

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Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

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Attn

Transfer Ship To

0 ANALYSIS LAB

Rerrt hy ^

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Sample Condition On Receipt

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INORGANICS TRAFnC REPORT ltT) Case Number gt

Sample Site NameCode

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Sampling Personnel

(Name)

(Phone) Sampling Date

(Beam) _ - (End)

Sample Description copy (Check One) bdquo Surface Water

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____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

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Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

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Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

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Sample Condition On Receipt

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Sample Site NameCode

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Sampling Personnel

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Sample Description copy (Check One) Surface Water

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Solids Other

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MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

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(J) Shipping Information

Name Of Carrier

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Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FJLE COPY

(4) Ship To

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Transfer Ship To

(5) ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

Sampling Personnel

(Name-)

(Phone) Sampling Date

(Beam) (End) r

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Sample Description copy (Check One) bdquo Surface Water

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__ Solids nthpr

(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

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Transfer Ship To

0 ANALYSIS LAB

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

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Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

Ship To i

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

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(Phone) Sampling Date

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copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

^___ Solids OtVlfir

(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

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Water

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Sampling Personnel

(e) Shipping Information

Name Of Carrier

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(Phone) Sampling Date

(Beam) (End)

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Airhill Number-

copy Sample Description (Check One)

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_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

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LAB FILE COPY

(T) Ship To

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Transfer Ship To

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RwH Vy f i

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(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

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0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

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(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

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Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

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Surfflrp Wator Check Analysis required f mdash Ground Water

Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

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Attn

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(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Attnx i f r - ^ f lt Transfer Ship To

reg ANALYSIS LAB

R^Hhy - ^

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

-

gt W ~ f b

Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

- ^ - bull

Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 4: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number D O Box 88 Alexcundria Virginia 22313 -703 557-2490 -FTS557-2490

8tLj ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Itnln Sample in NOanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report Nn HT mlirate 0 SAMPLE MATRIX V 09 (Check One)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1262 ORGANICSi TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office _JL Sampling Personnel

(Name) a ft i ~4

(Phone) Sampling Date

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copy Shipping Information

Name of Garner

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Airbill Number

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Low Concentration Medium Concentration SEP2713tt

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(D For each sample collected specify number Analjrsis Lab of containers used and mark volume level Recd on each bottle Date Recd

Sample Condition Oil Receipt (eg broken nNumber of Approximateice Chain-of-Custcdy etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Qo) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No _

gt Sample ID No

lo Designate below QC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check

Matrix Spike __ Water __ SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

(

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

-60 S US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO K c x H l H AV-varvlna Virginia22313 703557-249OFTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

I ah Name QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

HaseNo

Lah Sample ID No

r)pgtsigrifltlt=gt helow QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QT Report No HT inliratft flQi SAMPLE MATRIX OQ (Check One)

Matrix Spike Water

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SoilSediment

D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins bull

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

(Name)

(Phone)

Sampling Date

(Begin) (End)

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(D SAMPLEM ATRIX (Check One) bullraquo

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on each bottle Date RlaquovH ^ vQ^Roi Sample Condition

Number of Approximate on Receipt (eg broken no Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) J

Water (VOA)

^

Soil Sediment

Water (Ext VOA)

Other

Mixed Media

Solids

Other (specify)

V

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(D Sample Location

(jo) Special Handling Instructions (eg safety precautions hazardous nature)

| n| US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^m^mfHgmmm

^SlU ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HHHIi

T^hName I QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - Designate below QC analysis selected Low Conrpmtration

T rraquoh Sample ID No (Tf Applicable) Medium Concentration

QH Report No Di mlirate SAMPLE MATRIX (Check One) - ^

Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

f

f gtfExtractionPreparation(Dioxins)

f

Preparation(VGA)

t

f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Kii8 ORGANICS LABORATORY CHRONICLE (ANALYSIS) HUH

Lh NAme QH REQI IIREMENTS SAMPLE CONCENTRATION (Check One)

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I rah Sample ID No (Tf Applicable) Medium Concentration

QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

i

Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

f Surface Water

ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

Water SoilSediment Ship To 223

C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

shyi iv M-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Name of Carrier

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Airbill Number

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LowC Concentration Mediu im Concentration

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

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Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Date

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Date Shipped

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Airbill Number

Sample Description

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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Attn ltbull v l copy SAMPLEM ATRIX

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

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(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

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Name of Carrier

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0 SAMPLEM ATRIX (Check One) 4

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

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QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

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Designate below OC analysis selected

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

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QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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Sampling Personnel

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(Begin) (End)

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( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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Water (Extractable) f

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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(Ijlame)

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Water (Extractable) o2 fraquol Water FP (VOA) 3

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Mixed Media

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Ship To If ft f

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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(Begin) (End)

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copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

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SoilSediment

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Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

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SoilSediment

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

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Mixed Media

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike O t i

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SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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Sampling Personnel

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(Phone) Sampling Date

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(specify) MATCHES ORGANir SAMPLF NO

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Name Of Carrier

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(B) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Site NameCode

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Sample Description copy (Check One) Si irface Wat^r

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Low Concentration

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

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(e) Shipping Information Name Of Carrier

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

() Ship To

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Transfer Ship To

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Sample Condition On Receipt

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- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Site NameCode

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Water (VOA)

SoilSediment

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Other

Sample Location

Mixed Media

Solids

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Qo) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No _

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QC Report No Duplicate SAMPLE MATRIX (Check

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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HaseNo

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D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins bull

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

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(Phone)

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(Begin) (End)

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Water (Extractable) J

Water (VOA)

^

Soil Sediment

Water (Ext VOA)

Other

Mixed Media

Solids

Other (specify)

V

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(D Sample Location

(jo) Special Handling Instructions (eg safety precautions hazardous nature)

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T rraquoh Sample ID No (Tf Applicable) Medium Concentration

QH Report No Di mlirate SAMPLE MATRIX (Check One) - ^

Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

f

f gtfExtractionPreparation(Dioxins)

f

Preparation(VGA)

t

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Kii8 ORGANICS LABORATORY CHRONICLE (ANALYSIS) HUH

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QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

i

Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

f Surface Water

ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

Water SoilSediment Ship To 223

C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

y Ground Water

T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

i

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Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Begin) (End)

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Sample Description

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copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

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(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

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Airbill Number

0 Sample Description

Surface Water

Ground Water

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

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(Begin) (End)

0 Shipping Information

Name of Carrier

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Airbill Number

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Leachate

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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Water (Extractable) f

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

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) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

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Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

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(Check One) HARA Nn Designate below QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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Sampling Date

(Begin) (End)

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JfoJWampi fjiampt faZ1

Name of Carrier

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Airbill Number

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V firoiinH Water

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Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

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T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

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Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

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Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

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LAB FILE COPY

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

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Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

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mdash Water

(T) Shipping Information Name Of Carrier

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Airhill Niimher

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Page 6: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No _

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Matrix Spike __ Water __ SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

(

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides)

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

-60 S US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO K c x H l H AV-varvlna Virginia22313 703557-249OFTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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SoilSediment

D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins bull

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

(Name)

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Sampling Date

(Begin) (End)

() Shipping Information

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Airbill Number

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Surface Water

Ground Water

Leachate

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Number of Approximate on Receipt (eg broken no Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) J

Water (VOA)

^

Soil Sediment

Water (Ext VOA)

Other

Mixed Media

Solids

Other (specify)

V

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(D Sample Location

(jo) Special Handling Instructions (eg safety precautions hazardous nature)

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T rraquoh Sample ID No (Tf Applicable) Medium Concentration

QH Report No Di mlirate SAMPLE MATRIX (Check One) - ^

Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

f

f gtfExtractionPreparation(Dioxins)

f

Preparation(VGA)

t

f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Kii8 ORGANICS LABORATORY CHRONICLE (ANALYSIS) HUH

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QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

i

Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

f Surface Water

ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

Water SoilSediment Ship To 223

C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

shyi iv M-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

f f+V- r ttfs r

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BPH| US ENVIRONMENTAL PROTECnON AGENCY HWISomj iPiimISiigi ORGANICS LABORATORY CHRONICLE (j

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r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

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0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

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Surface Water

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T earhate

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LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

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(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

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Airbill Number

Sample Description

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

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Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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0 SAMPLEM ATRIX (Check One) 4

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0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

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Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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(Tf Applicable) Low Concentration Medium Concentration

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Matrix Spike tty n (Check One)

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

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Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

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(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

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( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

0 Sample Description

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

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0 SAMPLE MATRIX (Check Otae) t

bull Water SouS adiment

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0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

f

ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - ~- Designate below OC analysis selected Low Concentration

T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

- bull 1 t

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

~~| T Ah NATTIlaquo QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) HARA Nn Designate below QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

jMf^yampH(Phone)

Sampling Date

(Begin) (End)

copy Shipping Information

JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

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Airbill Number

copy Sample Description

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V firoiinH Water

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Water (Extractable) a I11

Water (VOA) 2 ^lt

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Other

copy Sample Location

Mixed Media

Solids

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Page 7: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

-60 S US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO K c x H l H AV-varvlna Virginia22313 703557-249OFTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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D nnntion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

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VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

(B) Regional Office I Sampling Personnel

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Number of Approximate on Receipt (eg broken no Containers Total Volume ice Chain-of-Custody etc)

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Water (Ext VOA)

Other

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Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

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ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

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Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

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SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

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Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

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Preparation

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

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Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

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(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) Cast Nrgt_ nosignate hfilow QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

y Ground Water

T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

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(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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i BB US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^ bullbullbullbullbullptrade

Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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KM^ OHGANICS LABORATORY CHRONICLE (ANALYSIS) ^H^^l ^Ht^^^ijB bull

Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

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Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

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copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

T flb Sample TD Nn

Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

iBjjgsect ORGANICS LABORATORY CHRONICLE (j

T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

bull7 o gt z Date Snipped

Airbill Number

0 Sample Description

Surface Water bull Ground Water

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

bull Water SouS adiment

^^ A

0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

f

ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

y^ US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number A PO Box 818 AlexandriaVirginia22313-703557-249OFTS 557-2490 is

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

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ExtractionPreparation (Acid)

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ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation (BaseNeutral)

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Page 8: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1263 ORGANICS TRAFFIC REPORT (T) Case Number

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ExtractionPreparation(Pesticides)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

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0 Shipping Information

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Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

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C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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Case No V Designate below OC

T Ah Sample ID Npanalysis selected

(Tf Applicable) Low Concentration Medium Cnnrfiritrfltion

QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

shyi iv M-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

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reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

(|) Sample Description

Surface Water

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T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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r3laquo Nrraquo Designate helow OC

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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Sampling Date

(Begin) (End)

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

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0 Sample Description

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

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Airbill Number

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( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

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Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

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Craquolaquoe No

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ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Water (VGA)

SoilSediment

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Name of Carrier Other

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Surf ace Water Mixed Media

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(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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BaseNeutral

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Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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Sampling Personnel

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Name Of Carrier

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LAB FILE COPY

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Sample Condition On Receipt

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Sample Condition On Receipt

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Name Of Carrier

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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LAB FILE COPY

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Sampling Date Airhll Niimhpsr

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Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

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Sulfide Solids Cyanide OtVmr

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

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Sample Site NameCode

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Sample Description copy (Check One) Si irface Wat^r

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Low Concentration

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

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TOC _-_ Fluoride amp pH

LAB FILE COPY

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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(e) Shipping Information Name Of Carrier

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

() Ship To

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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(e) Shipping Information

Name Of Carrier

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_____ Solids Oth mshy

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(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

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LAB FILE COPY

(T) Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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Surfflrp Wator Check Analysis required f mdash Ground Water

Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

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LAB FILE COPY

(4) Ship To - 1 A

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

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(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

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SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

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(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

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Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

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Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Transfer Ship To

() ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

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Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

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(5) SAMPLE MATRIX (Check One)

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Name Of Carrier

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LAB FILE COPY

(5) Ship To v^1 A

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

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Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

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Sampling Date Airlr1 Niirphfir shy

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 9: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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T^hName I QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T rraquoh Sample ID No (Tf Applicable) Medium Concentration

QH Report No Di mlirate SAMPLE MATRIX (Check One) - ^

Matrix Spike Water HSJt ^ Soil Serhrn Pgtn t

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

f

f gtfExtractionPreparation(Dioxins)

f

Preparation(VGA)

t

f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

1TOCT| US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^mamtnteammm

Kii8 ORGANICS LABORATORY CHRONICLE (ANALYSIS) HUH

Lh NAme QH REQI IIREMENTS SAMPLE CONCENTRATION (Check One)

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QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

i

Sample Site NameCode

copy Regional Office Sampling Personnel

(Name) II- - (

(Phone) Sampling Date

(Begin) (End)

0 Shipping Information

A A f

Name of Carrier

Date Shipped

Airbill Number

(s) Sample Description

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ltL- Ground Water

Leachate

SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration

Attn pound SEP 27 SAMPLE MATRIX

(Check One) Transfer

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C For each sample collected specify number 1of containers used and mark volume level Recd by^ on each bottle hate R^

Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

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Preparation

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

(|) Sample Description

Surface Water

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T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

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Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

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Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

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Airbill Number

Sample Description

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

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Airbill Number

0 Sample Description

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copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

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(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

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( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

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(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

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Mixed Media

Solids

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Ship To If ft f

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

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Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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Sample Site NameCode

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Name of Carrier Other

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copy Sample Description

Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Mixed Media

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

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Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

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LAB FILE COPY

(T) Ship To

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Sample Site NameCode

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(Begin) (End)

copy Sample Description (Check One)

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Solids Othmshy

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Low Concentration

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Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

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(specify) MATCHES ORGANIC S AMPI K NO

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(5) SAMPLE MATRIX (Check One)

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Name Of Carrier

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LAB FILE COPY

(5) Ship To v^1 A

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier it

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

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Tflsk 3 Ammonia Sulfide Solids

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TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

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Kii8 ORGANICS LABORATORY CHRONICLE (ANALYSIS) HUH

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QC Report No Hi mlirwta ^ SAMPLE MATRIX

Matrix Spike V 9 7n (Check One)

WQg Water SoilSediment

Df^rTintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

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Sample Site NameCode

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(Begin) (End)

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Name of Carrier

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Sample Condition on Receipt (eg broken nNumber of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

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Sample Location

Mixed Media

Solids

Other (specify)

Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

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(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

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LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

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Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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Sampling Date

(Begin) (End)

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Airbill Number

Sample Description

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

0 Sample Description

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Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

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Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

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SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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tt7 $~poundgt6amp (Phone)

(Begin) (End)

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Name of Carrier

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Airbill Number

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( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

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(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

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Mixed Media

Solids

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Ship To If ft f

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Craquolaquoe No

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

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Name of Carrier Other

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Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Pesticides

Dioxins

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

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Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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(e) Shipping Information Name Of Carrier

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(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

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Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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Task 1 amp 2 Task 3 Ammnnifl

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Airbill MiimhfiTshy

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

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Low CunceutidLiou

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Sample Site NameCode

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(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

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Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Page 11: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1264 ORGANICS TRAFFIC REPORT J) Case Number

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Sample Site NameCode

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

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Preparation

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

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(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

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Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

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Water (ExtVOA)

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Sample Location

Mixed Media

Solids K

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(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Name of Carrier

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Airbill Number

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Water (VOA) shy

SoilSediment

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Other

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Mixed Media

Solids

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(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

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Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

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Matrix Spike MQV ) laquo (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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(Begin) (End)

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Airbill Number

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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Water (Extractable)

Water (VOA)

SoilSediment

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Other

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Mixed Media

Solids

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copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

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Airbill Number

0 Sample Description

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Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

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Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

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QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

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SAMPLE MATRIX (Check One)

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For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

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(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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Sampling Personnel

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(Begin) (End)

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Name of Carrier

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Airbill Number

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( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

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(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

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Mixed Media

Solids

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Ship To If ft f

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Craquolaquoe No

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

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Name of Carrier Other

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Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Pesticides

Dioxins

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

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Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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(e) Shipping Information Name Of Carrier

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(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

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Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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Task 1 amp 2 Task 3 Ammnnifl

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Airbill MiimhfiTshy

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

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Low CunceutidLiou

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Sample Site NameCode

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(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

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Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

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Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

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(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

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D^tfi RViippesfi t

Airhill Number

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LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

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(Check One) f Attn - Water

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Sampling Personnel Name Of Carrier it

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Tflsk 3 Ammonia Sulfide Solids

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TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 12: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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QC Report N^ Hi mliratfi SAMPLE MATRIX (Check One)

Matrix Spike WatorSoilSediment W ^n

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

ExtractionPreparation (Dioxins)

i

Preparation

(VOA) lt f

shyi iv M-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) Cast Nrgt_ nosignate hfilow QC

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reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

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T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

y Ground Water

Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

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Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

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Mixed Media

Solids

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Ship To If ft f

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

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Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Lab Sample ID Nltraquo

Designate below QC analysis performed

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Name of Carrier Other

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(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Sample Site NameCode

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Mixed Media

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Name Of Carrier

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LAB FILE COPY

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(e) Shipping Information

Name Of Carrier

Date Shipped

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(J) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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(e) Shipping Information Name Of Carrier

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

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LAB FILE COPY

Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Condition On Receipt

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LAB FILE COPY

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

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Low CunceutidLiou

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

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Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

0 Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

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(5) SAMPLE MATRIX (Check One)

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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LAB FILE COPY

Page 13: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number IO Rox8i8 AIexltir1riu Virginia 22313 703557 2490 ITS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

Lab Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case Nomdash

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike nWater deg 9 ty SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

(Phone) Sampling Date

(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

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Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

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T earhate

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LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

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Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

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I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

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Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

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Airbill Number

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Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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Sampling Date

(Begin) (End)

(T) Shipping Information

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Airbill Number

Sample Description

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

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Airbill Number

0 Sample Description

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

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(Begin) (End)

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Name of Carrier

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Airbill Number

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( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

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Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

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Craquolaquoe No

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Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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SoilSediment

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Name of Carrier Other

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Surf ace Water Mixed Media

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ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Pesticides

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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(e) Shipping Information

Name Of Carrier

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(J) Mark Volume Level On Sample Bottle Check Analysis required

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

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Sample Condition On Receipt

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Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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(4) Ship To - 1 A

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

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(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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(5) SAMPLE MATRIX (Check One)

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(5) Ship To v^1 A

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

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Sampling Personnel Name Of Carrier it

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 14: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1265 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office -pound Sampling Personnel

(Name) I I bull l t - bull (

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(Begin) (End)

(T) Shipping Information

Name of Carrier

Date Shipped

Airbill Number

Sample Description

Surf ace Water

Ground Water

Leachate

SAMPLE CONCENTRATION (pound) Ship To (Check One)

Low Concentration Medium Concentration

SEP 2 7 1981 Attn i

SAMPLE MATRIX (Check One)

Transfer 1 Water

Ship To SoilSediment

Por each sample collected specify number 1(0) AnalyBfflj[ ab of containers used and mark volume level Rec on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nc

ice Chain-of-Custody eta) Containers Total Volume

Water i(Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids K

Other (specify)

(To) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull bull A p bull bull bull bull bull -CJ IW bull TI 7 M9U Sample Number

ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

^ t

Preparation -^ (VGA) f i

f f+V- r ttfs r

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BPH| US ENVIRONMENTAL PROTECnON AGENCY HWISomj iPiimISiigi ORGANICS LABORATORY CHRONICLE (j

mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) Cast Nrgt_ nosignate hfilow QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

y Ground Water

T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

i

i BB US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^ bullbullbullbullbullptrade

Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

i bull - Containers Total Volume ice Chain-of-Custody etc)

(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullB l US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^KpHHRjllMg

KM^ OHGANICS LABORATORY CHRONICLE (ANALYSIS) ^H^^l ^Ht^^^ijB bull

Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

y Ground Water

Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

lt Water Cl_- Tgt ^)gt O jf

SoilSi sdiment Ship To Jgt7 nf )f

copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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KiBJgll ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) ^jjjjjlj^

I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

y LowC loncentration Mediu im Concentration SEP 27 1981

0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

HAQA Nrt ppHsignatfi below QC

T ah Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

bullV

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

T flb Sample TD Nn

Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

iBjjgsect ORGANICS LABORATORY CHRONICLE (j

T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

r^sgt TSIn noltignfli-ft below QC

I ah Sample in NOanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

bull7 o gt z Date Snipped

Airbill Number

0 Sample Description

Surface Water bull Ground Water

Learhate

0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

bull Water SouS adiment

^^ A

0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

f

ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

i bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

y^ US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number A PO Box 818 AlexandriaVirginia22313-703557-249OFTS 557-2490 is

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

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copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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(Begin) (End)

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copy Sample Description

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ij|fimT3ft ^^oncntioii on Receipt (eg broken ac Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

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MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

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Sample Condition On Receipt

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0 SAMPLE CONCENTRATION (Check One)

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0 SAMPLE MATRIX (Check One)

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(T) Shipping Information Name Of Carrier

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Datp SViipppfi

Airhill Niimher

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Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

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Sample Site NameCode

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Sample Description copy (Check One) Surface Water

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Solids Other

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MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

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(J) Shipping Information

Name Of Carrier

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

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Sample Description copy (Check One) bdquo Surface Water

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Sulfide Cyanide

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LAB FILE COPY

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

A i (Name) J

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Sampling Date Airhll Niimhpsr

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Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

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TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

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Sample Site NameCode

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Sample Description copy (Check One) Si irface Wat^r

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(specify) MATCHES ORGANIC S AMPT K NO

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Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

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LAB FILE COPY

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Sample Condition On Receipt

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Sample Site NameCode

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Sampling Personnel

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(specify)

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Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

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(e) Shipping Information

Name Of Carrier

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Sampling Personnel Name Of Carrier

(Name)

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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LAB FILE COPY

0 Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

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(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

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Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

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Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Sample Site NameCode

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Sampling Personnel

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(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

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Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

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(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

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D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

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Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

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(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 15: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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ORGAN1CS LABORATORY CHRONICLE (EXTRACTIONS)

T ah Name QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No gt v Designate below OC analysis selected Low Concentration

Lab Sample ID No (If Applicable) Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX (Check One)

Matrix Spike Water WN 01laquo SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) lt

ExtractionPreparation (Dioxins) bull

^ t

Preparation -^ (VGA) f i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BPH| US ENVIRONMENTAL PROTECnON AGENCY HWISomj iPiimISiigi ORGANICS LABORATORY CHRONICLE (j

mdash| T h Namlaquo i - QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) Cast Nrgt_ nosignate hfilow QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

r SAMPLE MATRIX

reg19Q$Matrix Spike Water SoilSediment

D^a^rrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

j

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

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T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

i

i BB US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^ bullbullbullbullbullptrade

Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullB l US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^KpHHRjllMg

KM^ OHGANICS LABORATORY CHRONICLE (ANALYSIS) ^H^^l ^Ht^^^ijB bull

Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

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Airbill Number

Sample Description

Surf are Water

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Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

lt Water Cl_- Tgt ^)gt O jf

SoilSi sdiment Ship To Jgt7 nf )f

copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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KiBJgll ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) ^jjjjjlj^

I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

y LowC loncentration Mediu im Concentration SEP 27 1981

0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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T ah Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

T flb Sample TD Nn

Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

r^sgt TSIn noltignfli-ft below QC

I ah Sample in NOanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

bull7 o gt z Date Snipped

Airbill Number

0 Sample Description

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Learhate

0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

bull Water SouS adiment

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0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

f

ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

y^ US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number A PO Box 818 AlexandriaVirginia22313-703557-249OFTS 557-2490 is

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

ltc M SVC lt r J

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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Hi ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) BHDIi

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - ~- Designate below OC analysis selected Low Concentration

T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

- bull 1 t

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

~~| T Ah NATTIlaquo QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) HARA Nn Designate below QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

jMf^yampH(Phone)

Sampling Date

(Begin) (End)

copy Shipping Information

JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

poundC) ~j ltypound

Airbill Number

copy Sample Description

Surface Water

V firoiinH Water

Leachate

copy SAMPLE C( DNCENTRATION copy Ship To Of bull tlt (Cl leckOne) bullgtbull V C( ty finlt- ty

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Complete section below only if sample is to be used for duplicate or spike analyses

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ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

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QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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Page 16: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

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ExtractionPreparation T j l

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Matrix Spike - t

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SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Shipping Iniormation SoiV Sediment

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Name of Carrier Other

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Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

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Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

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Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

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(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

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Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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(Begin) (End)

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Sample Description

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

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(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

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Name of Carrier

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Surface Water

Ground Water

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

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Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

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(Begin) (End)

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Name of Carrier

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Airbill Number

reg Sample Description

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( Omiind Water

Leachate

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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Water (Extractable) f

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

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Sample Condittom on Receipt (eg broken nc Number of Approximate

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Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

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0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

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Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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Other

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Mixed Media

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

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T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

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(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

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Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

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Low Cuuctmlidliuii

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Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

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(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

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LAB FILE COPY

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Sample Condition On Receipt

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

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Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

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INORGANICS TRAFnC REPORT ltT) Case Number gt

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Q Samplina Office

Sampling Personnel

(Name)

(Phone) Sampling Date

(Beam) _ - (End)

Sample Description copy (Check One) bdquo Surface Water

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____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

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TOC J_- _ FluondeamppH

LAB FILE COPY

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Attn

Transfer Ship To

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natBRlaquofH- y

Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

M90-FTS 55

IMA 8872 bulllaquo PRO^

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Sample Site NameCode

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Sampling Personnel

(Nflmf)

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Sample Description copy (Check One) Surface Water

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Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

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Water

(J) Shipping Information

Name Of Carrier

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Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

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Attn

Transfer Ship To

(5) ANALYSIS LAB

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DateRfir-rf ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

)7-2490-FTS 5572490

IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

Sampling Personnel

(Name-)

(Phone) Sampling Date

(Beam) (End) r

f

Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

__ Solids nthpr

(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

shy bull

Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

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Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

Ship To i

bullv

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Transfer Ship To

0 ANALYSIS LAB

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Sample Condition On Receipt

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bdquo - f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

natfiRfir-H 2

Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

- -1 i

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

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(specify)

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Low CuiiceiilidLiuii

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Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

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- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

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(e) Shipping Information

Name Of Carrier

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(Beam) (End)

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Airhill Number-

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_____ Solids Oth mshy

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(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

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(T) Ship To

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Transfer Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

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Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

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(Name) -

(Phone) Sampling Date

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

(T) Ship To

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INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

0 Ship To

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Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

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LAB FILE COPY

(5) Ship To v^1 A

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Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 17: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Oifice Sample Number

A 1266 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office _Z Sampling Personnel

( j JName)

(Phone)

Sampling Date

(Begin) (End)

0 Shipping Information

1 K i t bull (t

Name of Carrier

Date Shipped

j i

Airbill Number

(|) Sample Description

Surface Water

y Ground Water

T earhate

copy SAMPLE C( DNCENTRATION 0 Ship To (Cl ieck One)

LowC Concentration Mediu im Concentration

Attn ^gt t r v l xy (f) SAMPLEM ATRIX

(Check Craquone) v Transfer

Water SoilS sdiment Ship To Lj r ^ )

(D For each sample collected sp ecify number (n) AnalysisLab i of containers used and markvolume level FWd Ky ^njc^KcL on each bottle DateRecd- ^^^-^J

on Receipt (sfj hmkm no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water -(Extractable)

Water (VOA) shy

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

(jo) Special Handling Instructions (e g safety precautions hazardous nature)

i

i BB US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^ bullbullbullbullbullptrade

Hl^f ORGANICS LABORATORY CHRONICLE (EXTRACTIONS) HUH i-V

T ah Name f QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No bull_ V Designate below OC analysis selected Low Concentration

I ah Sample ID No (If Applicable) Medium Concentration

QT Report No Dunlicate SAMPLE MATRIX (Check One)

Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullB l US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^KpHHRjllMg

KM^ OHGANICS LABORATORY CHRONICLE (ANALYSIS) ^H^^l ^Ht^^^ijB bull

Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

Casft No Dp-RirjnatA helow QC analysis performed Low Concentration

Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

y Ground Water

Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

lt Water Cl_- Tgt ^)gt O jf

SoilSi sdiment Ship To Jgt7 nf )f

copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

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Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

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For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

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Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

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(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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(If Applicable) Low Concentration Medium Concentration

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Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

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Craquolaquoe No

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ExtractionPreparation (BaseNeutral)

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Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

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Sampling Personnel Name Of Carrier

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Name Of Carrier s

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Name Of Carrier f t flt f raquo - f

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(specify) MATCHES ORGANIC S AMPI K NO

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Name Of Carrier

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Sampling Personnel Name Of Carrier it

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(Nam)

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Sampling Date Airlr1 Niirphfir shy

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Matrix Spike Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparationf(Pesticides)

1 f

ExtractionPreparation T j l

(Dioxins)

Preparation(VOA) j

f

f sOti i

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

^L Water SoiVS sdiment ShipTo $J(0

copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

(Name) Approximate On Receipt (eg broken no 1 Number of

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(Phone) Water j 1 bull Sampling Date (Extractable) gt bull Water

J (Begin) (End) (VOA) v

Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

1

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

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Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

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copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

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0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

bullV

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

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(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

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(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

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Water (ExtVOA)

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Mixed Media

Solids

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Ship To If ft f

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Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

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Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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Sample Site NameCode

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(Begin) (End)

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(3) SAMPLE MATRIX (Check One)

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Water (VGA)

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Name of Carrier Other

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Airbill Number

copy Sample Description

Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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copy Sample Location

Mixed Media

Solids

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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Name Of Carrier

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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LAB FILE COPY

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Low Concentration

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

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TOC _-_ Fluoride amp pH

LAB FILE COPY

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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(e) Shipping Information Name Of Carrier

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(e) Shipping Information

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_____ Solids Oth mshy

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(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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Task 1 amp 2 Tank 3 Ammonia

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Sample Site NameCode

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Sampling Personnel

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(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Transfer Ship To

() ANALYSIS LAB

R0H hy f

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Sample Condition On Receipt

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v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

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(5) SAMPLE MATRIX (Check One)

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() Shipping Information

Name Of Carrier

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LAB FILE COPY

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TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number gt T+bull Ai-ri-bjVirqinj22313- 703557-2490-FTS557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

LabName__L QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No

Lab Sample ID No

Designate below QC analysis performed

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate ^ SAMPLE MATRIX

Matrix Spike - t

Water

f (Check One)

SoilSediment

Analyst Signature Detail Below Pertinent Information andor Description DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

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Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

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(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

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Airbill Number

Sample Description

Surf are Water

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Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

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0 SAMPLEM ATRIX (Check One) 4

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

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(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

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Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

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Airbill Number

0 Sample Description

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

bull Water SouS adiment

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0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

f

ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

ltc M SVC lt r J

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

bullH l US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^^gmmimfim

Hi ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) BHDIi

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No - ~- Designate below OC analysis selected Low Concentration

T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

- bull 1 t

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

~~| T Ah NATTIlaquo QC REQUIREMENTS SAMPLE CONCENTRATION

(Check One) HARA Nn Designate below QC

analysis performed Low Concentration Lab Sample ID No (Tf Applicable) Medium Concentration

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

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Name of Carrier

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copy Sample Description

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Containers Total Volume ice Chain-of-Custody etc)

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Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

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Surface Water r Ground Water

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(specify) MATCHES ORGANir SAMPLF NO

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Low Cuuctmlidliuii

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0 Shipping Information

Name Of Carrier

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(B) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

(4) Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

(Name)

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Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

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MATCHES ORGANIC SAMPLE NO -t-ii

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Site NameCode

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(e) Shipping Information

Name Of Carrier

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(J) Mark Volume Level On Sample Bottle Check Analysis required

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

(Name)

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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LAB FILE COPY

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

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Solids Othmshy

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Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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(a) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

0 Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Name) -

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(5) SAMPLE MATRIX (Check One)

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Name Of Carrier

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

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Sampling Personnel Name Of Carrier it

Ror-H Ky - -

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 20: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

a A 1267 ORGANICS TRAFFIC REPORT copy Case Number copy SAMPLE CC DNCENTRATIC )N 0 Ship To V ^

(Cl ieck One) -

LowC loncentration Sample Site NameCode Mediu im Concentratic gt SEP 27 1982

Attn K bull - copy SAMPLEM ATRIX

(Check One) Transfer

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copy Regional Office 4- copy For each sample collected sp ecify number copy Analysis Lab j Sainpling Personnel of containers used and mark volume level Rlaquonrl Hy^T) l^^S^lu

on each bottle Date R^rl-^-jfD^^ L bull ^ ( Sample Condition

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Shipping Iniormation SoiV Sediment

Water bull bull r t shy (ExtVOA)

Name of Carrier Other

Date Shipped

h

Airbill Number

reg Sample Description copy Sample Location

Surface Water Mixed Media

firmrnri Water Sohds

Leachate Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PC rxvcHht Vxin-n t V i ru in i Z3 i i 703 ^77490-ITo SIv90 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T jh Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No shy Designate below CXI (Check One)

Lab Sraquonpllaquo TD Noanalysis selected

(Tf Applicable) Low Concentration Medium Concentration

QC Report No Di mlirate SAMPLE MATRIX

Matrix Spike Water

(Check One) _ HQV Ol W

Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

i bullbull

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Lab Name QH RFQI IIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Nn (Tf Applirahle) Medium Concentration

QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

y Ground Water

Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Matrix Spike QV ft n (Check One)

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Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

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(Phone) Sampling Date y i i gt

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Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

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Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

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Designate below OC analysis selected

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

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QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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Water (Extractable) f

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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Sample Condittom on Receipt (eg broken nc Number of Approximate

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Water (Extractable) o2 fraquol Water FP (VOA) 3

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Water (ExtVOA)

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Mixed Media

Solids

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Ship To If ft f

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

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Matrix Spike Water

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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(Begin) (End)

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(3) SAMPLE MATRIX (Check One)

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

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Water (VOA) 2 ^lt

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Mixed Media

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

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QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

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Water

0 Shipping Information

Name Of Carrier

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(B) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Name Of Carrier

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Water

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Page 21: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

1

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Soil Sediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA) r

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation (Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No

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ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

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Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Date

(Begin) (End)

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Sample Description

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Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

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Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Matrix Spike QV ft n (Check One)

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Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

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(Phone) Sampling Date y i i gt

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0 Shipping Information

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

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Mixed Media

Solid

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QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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SoilSediment

Water (ExtVOA)

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Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

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(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

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Mixed Media

Solids

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Ship To If ft f

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

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Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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Sample Site NameCode

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Name of Carrier Other

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copy Sample Description

Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Mixed Media

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

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Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

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LAB FILE COPY

(T) Ship To

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Sample Site NameCode

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(Begin) (End)

copy Sample Description (Check One)

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Solids Othmshy

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Low Concentration

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Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

0 Ship To

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

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(specify) MATCHES ORGANIC S AMPI K NO

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(5) SAMPLE MATRIX (Check One)

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Name Of Carrier

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LAB FILE COPY

(5) Ship To v^1 A

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QT Report Nr Hi mlir^t^ SAMPLE MATRIX ^p (Check One)

r c v ils i) i Matrix Spike y (too

SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

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(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No

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Designate below OC analysis selected

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Low Concentration Medium Concentration

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Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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(Begin) (End)

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Airbill Number

Sample Description

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(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

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on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

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Name of Carrier

Date Shipped

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Airbill Number

0 Sample Description

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0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

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(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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(Begin) (End)

0 Shipping Information

Name of Carrier

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Airbill Number

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( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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Water (Extractable) f

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SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

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) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Sample Condittom on Receipt (eg broken nc Number of Approximate

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Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

Ship To If ft f

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Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

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Mixed Media

Solids

Other (specify)

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

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T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

(laquoraquo Mr Dfisignate helow QC

T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

(Name)

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Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

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(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Name Of Carrier

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Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

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(Name-)

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Sample Description copy (Check One) bdquo Surface Water

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Transfer Ship To

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Sample Condition On Receipt

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J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Luw Cuiiceiilidliua

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Sampling Personnel Name Of Carrier

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

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Sample Site NameCode

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Low Concentration

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

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TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

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Transfer Ship To

0 ANALYSIS LAB if

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

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Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

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Attn

Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Water _ SoilSedimpnt

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Sampling Personnel Name Of Carrier

(Name)

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

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Sulhde Solids Cyanide Other Tor (specify)

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LAB FILE COPY

(4) Ship To - 1 A

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Attn

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(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

DatftRprHshy

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

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SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Attnx i f r - ^ f lt Transfer Ship To

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R^Hhy - ^

natfiRp-rrl lt ^ ^

Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

-

gt W ~ f b

Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

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Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

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Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 23: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1268 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

copy Regional Office_ Sampling Personnel

(Name) bull -

(Phone)

Sampling Date

(Begin) (End)

(D Shipping Information

Name of Carrier

Date Shipped

Airbill Number

copy Sample Description

Surf ace Water

L Ground Water

Leachate

(D SAMPLE CONCENTRATION Ship To (Check One)

Low Concentration Medium Concentration SEP 2 7 1982

Attn SAMPLE MATRIX

(Check One)

Water SoilSediment

Transfer ShipTo

Por each sample collected specify number 0) Anal of containers used and mark volume level Recdby dL on each bottle Pate Recd

amide Condition on Receipt (eg broken mNumber of Approximate ice Chaunrf-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number bullbullbullOYX bull- A-vr v Wi i ru- i fOi 03 bv 4iO P fgt Jib 2490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

ThNwne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

I flh Sample TO No

Designate below OC analysis selected

(Tf Applicable)

(Check One)

Low Concentration Medium Concentration

Qlt~ Report No Duplicate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN Oi2

SoilSediment t [

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

f

ExtractionPreparation^

(Dioxins) i

Preparation(VGA) gt A

S f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

r3laquo Nrraquo Designate helow OC

Lab Sample ID No analysis performed

(Tf Applicable) Low Concentration Medium Concentration

DT Praquoprraquorf Nn HT mlirflte SAMPLE MATRIX

Matrix Spike MQV ) laquo (Check One)

(9 Water SoilSediment

Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

copy Regional Office- bull Sampling Personnel

-7 J i bull bull (Name)

(Phone)

Sampling Date

(Begin) (End)

(T) Shipping Information

Tc i bull i v i Name of Carrier

Date Shipped

t 4 i

Airbill Number

Sample Description

Surf are Water

y Ground Water

Leachate

(D SAMPLE CC 3NCENTRATIC )N copy Ship To (Ci ieck One)

LowC loncentration __ Mediu m Concentratio m SEP 2 7 190

Attn ltbull v l copy SAMPLEM ATRIX

(Check One) Transfer

lt Water Cl_- Tgt ^)gt O jf

SoilSi sdiment Ship To Jgt7 nf )f

copy For each sample collected sp ecify number (n) Analysis Lab of containers used and markvolume level RlaquooH hy ^JVj (^5Scdj

on each bottle Date Rlaquocri- 9 P3- f ^jarnpjp Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

iB^ffi US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^BpBlaquoraquoiippM

KiBJgll ORGANTCS LABORATORY CHRONICLE (EXTRACTIONS) ^jjjjjlj^

I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

y LowC loncentration Mediu im Concentration SEP 27 1981

0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

bullV

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

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0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

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Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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(Begin) (End)

copy Shipping Information

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Name of Carrier

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copy Sample Description

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Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

JB^JI ORGANICS LABORATORY CHRONICLE (j

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(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

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Sampling Personnel Name Of Carrier

(Name)

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Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

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Transfer Ship To

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Rerrt hy ^

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Sample Condition On Receipt

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0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

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(T) Shipping Information Name Of Carrier

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Airhill Niimher

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Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

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M90-FTS 55

IMA 8872 bulllaquo PRO^

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Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

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Sample Description copy (Check One) Surface Water

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Solids Other

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MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

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Water

(J) Shipping Information

Name Of Carrier

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Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FJLE COPY

(4) Ship To

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(5) ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

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(Name-)

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(Beam) (End) r

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Sample Description copy (Check One) bdquo Surface Water

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Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

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Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

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Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

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LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

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Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

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Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

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(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

0 SAMPLE MATRIX fPViorlr Onal

Water

Q Samplina Office

Sampling Personnel

(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

Date Shipped

Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

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LAB FILE COPY

(T) Ship To

Attn

Transfer Ship To

() ANALYSIS LAB

RwH Vy f i

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(eg broken leakage chain of custody etc )

bull bull - raquo bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

1 LuW CoilUtillLldtlOll

0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

DateRfirH- ^ ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

Water

(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

(Phone) t~ Dfltp- SViipppri

Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

fi Sample Description ^5) Mark Volume Level ^-J (Check One) On Sample Bottle

Surfflrp Wator Check Analysis required f mdash Ground Water

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) i

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ExtractionPreparation^

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Preparation(VGA) gt A

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

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ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

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Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

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ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Site NameCode

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For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

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Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

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Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

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Water (Extractable) o2 fraquol Water FP (VOA) 3

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Mixed Media

Solids

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(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Craquolaquoe No

Iflb Sample ID No

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Low Concentration Medium Concentration

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Matrix Spike Water

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Lab Sample ID Nltraquo

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(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

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Sampling Date

(Begin) (End)

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(3) SAMPLE MATRIX (Check One)

Water SoilSediment

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

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Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

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Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Name Of Carrier s

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

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TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 25: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

i PO Box 818 AlexandriaVirginia 22313-703 557-2490 -FTS 557-2490

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

T ah Nilaquoe QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Draquolaquorrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1269 ORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Water (Extractable)

Water (VOA)

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

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SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Matrix Spike QV ft n (Check One)

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Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

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Surface Water

Ground Water

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Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

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Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

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(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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iBjjgsect ORGANICS LABORATORY CHRONICLE (j

T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

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0 SAMPLE MATRIX (Check Otae) t

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

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Mixed Media

Solids

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Ship To If ft f

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Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

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copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

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QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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(Begin) (End)

copy Shipping Information

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copy Sample Description

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Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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T^HN^TTifi 1 QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

JB^JI ORGANICS LABORATORY CHRONICLE (j

T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

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Sampling Personnel Name Of Carrier

(Name)

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Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

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Rerrt hy ^

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Sample Condition On Receipt

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0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

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(T) Shipping Information Name Of Carrier

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Airhill Niimher

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Sulhde Cyanide

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LAB FILE COPY

(4) Ship To ^ bdquo 4

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M90-FTS 55

IMA 8872 bulllaquo PRO^

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Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

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Sample Description copy (Check One) Surface Water

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Water

(J) Shipping Information

Name Of Carrier

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(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FJLE COPY

(4) Ship To

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(5) ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

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Low CoiicenlidLion

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Water

0 Shipping Information

Name Of Carrier - - tx

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Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FILE COPY

0 Ship To ft

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Transfer Ship To

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PPCT) by -

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

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Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

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Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

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Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

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Low CuiiceiilidLiuii

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Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

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Water

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(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

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Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

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LAB FILE COPY

(T) Ship To

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Transfer Ship To

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RwH Vy f i

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(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

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Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

DateRfirH- ^ ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

Water

(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

(Phone) t~ Dfltp- SViipppri

Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

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Surfflrp Wator Check Analysis required f mdash Ground Water

Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

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Attn

Transfer Ship To

(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

DatftRprHshy

(fo) C 1 f --raquoraquo-

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ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

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Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Acid

Pesticides

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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Mixed Media

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(10) Special HandUng Instructions (eg safety precautions hazardous nature)

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ExtractionPreparation (Pesticides)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

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ExtractionPreparation (BaseNeutral)

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ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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Name of Carrier Other

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Airbill Number

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Surf ace Water Mixed Media

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

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Matrix Spike HOV Olfltt Water SoilSediment

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike O t i

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BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

-bull 5

Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

i k

Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

X^ ixxdi= Alexandra VA 22313 703 557 2490 -FTS 5572490 IMA 8870 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

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Sampling Personnel Name Of Carrier

(Name)

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Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

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Transfer Ship To

0 ANALYSIS LAB

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Sample Condition On Receipt

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(Name)

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Sample Description copy (Check One) bdquo Surface Water

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____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

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Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

M90-FTS 55

IMA 8872 bulllaquo PRO^

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Sample Site NameCode

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Sample Description copy (Check One) Surface Water

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(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FJLE COPY

(4) Ship To

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

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(Name-)

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(Beam) (End) r

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Sample Description copy (Check One) bdquo Surface Water

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Low CoiicenlidLion

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Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

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Transfer Ship To

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Sample Condition On Receipt

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J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Luw Cuiiceiilidliua

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Sampling Personnel Name Of Carrier

A i (Name) J

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Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

(Namfil

(Phone) Sampling Date

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Low CuiiceiilidLiuii

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Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(e) Shipping Information

Name Of Carrier

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(Beam) (End)

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Airhill Number-

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_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

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LAB FILE COPY

(T) Ship To

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RwH Vy f i

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

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Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

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Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sulfide Solids Cyanide nthfir

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INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

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(5) Sampling Office lt (e) Shipping Information

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Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

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LAB FILE COPY

(4) Ship To - 1 A

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Attn

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(9) ANALYSIS LAB

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

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Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

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Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 27: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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I ah Name QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ah Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC Rlaquoprgtrf No Dunlicate SAMPLE MATRIX

Matrix Spike Water

(Check One) UQMUN Oil

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation(BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides) gt

ExtractionPreparation(Dioxins)

Preparation(VGA)

-

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation(VGA) QC

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

ORGAN1CS LABORATORY CHRONICLE (ANALYSIS)

T Ah Nam QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

faisraquo No n^Rignatp hfilow QC

Lab Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT Report No Hi ml irate SAMPLE MATRIX

Matrix Spike QV ft n (Check One)

t V if VA-

Wflter SoilSediment

Doerrinti on Aivaljrst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode

0 Region Office- i Sampling Personnel

- - - A i (Name)

(Phone) Sampling Date y i i gt

(Begin) (End)

0 Shipping Information

| gt i t

Name of Carrier

Date Shipped

--

Airbill Number

0 Sample Description

Surface Water

Ground Water

Leachate

copy SAMPLE CC gtNCENTRATION 0 Ship To (Cl ieck One)

y LowC loncentration Mediu im Concentration SEP 27 1981

0 SAMPLEM ATRIX (Check One) 4

Transfer gt Water

SoilSlt adiment

0 For each sample collected sp ecify number AnalysisLab of containers used and mark volume level on each bottle Date Rflcd- lt poundyenpound

Sample Condition on Receipt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable)

Water (VOA) _ j Soil Sediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solid

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

HAQA Nrt ppHsignatfi below QC

T ah Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

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Ship To If ft f

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Water (VGA)

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Name of Carrier Other

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Airbill Number

copy Sample Description

Surf ace Water Mixed Media

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(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

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Low Concentration

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(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

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TOC _-_ Fluoride amp pH

LAB FILE COPY

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Sample Condition On Receipt

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(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

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Transfer Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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Name Of Carrier

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(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

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LAB FILE COPY

(4) Ship To - 1 A

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(9) ANALYSIS LAB

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KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

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(jj) Sampling Office

Sampling Personnel

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Sample Description copy (Check One) Surface Water OiroTinH Writer

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Low CunceutidLiou

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

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(Begin) (End)

copy Sample Description (Check One)

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Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

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Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

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Transfer Ship To

() ANALYSIS LAB

R0H hy f

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

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Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

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(5) SAMPLE MATRIX (Check One)

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Name Of Carrier

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LAB FILE COPY

(5) Ship To v^1 A

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Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

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Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

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Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 28: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box818 Alexandria Virginia 22313-703557-2490 FTS 557-2490

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BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1270 ORGANICS TRAFFIC REPORT 0 Case Number

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ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

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ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

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ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

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QC (Acid)

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QC (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

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(T) Shipping Information

Name of Carrier

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(s) Sample Description

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SAMPLE CONCENTRATION S Ship To (Check One)

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SAMPLE MATRIX (Check One)

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For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

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Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No

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Designate below OC analysis selected

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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LowrC Concentration Mediu im Concentration

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SoilSediment

Water (ExtVOA)

Other

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Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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0 Shipping Information

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

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Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Lab Sample ID Nltraquo

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(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

jMf^yampH(Phone)

Sampling Date

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JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

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Airbill Number

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Surface Water

V firoiinH Water

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Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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T^HN^TTifi 1 QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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JB^JI ORGANICS LABORATORY CHRONICLE (j

T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

(laquoraquo Mr Dfisignate helow QC

T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

y Water

(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

-bull 5

Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

i k

Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

X^ ixxdi= Alexandra VA 22313 703 557 2490 -FTS 5572490 IMA 8870 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

J Water

(jj) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

bulllt f t ~ J

Attn

Transfer Ship To

0 ANALYSIS LAB

Rerrt hy ^

DatfiRprH- ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f f

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INORGANICS TRAFnC REPORT ltT) Case Number gt

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Name)

(Phone) Sampling Date

(Beam) _ - (End)

Sample Description copy (Check One) bdquo Surface Water

_fc^mdash Ground Water

____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

_raquopound Task 1 amp 2 Task 3 Ammonia

Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

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Attn

Transfer Ship To

0 ANALYSIS LAB

PPI-H -vy r

natBRlaquofH- y

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

M bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

M90-FTS 55

IMA 8872 bulllaquo PRO^

bullV INORGANICS TRAFFIC REPORT reg Case Number-

Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

(Nflmf)

(Phone)

Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water

f mdash Ground Water

Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 - Task 3 Ammonia

Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

jf S -J i jr

Attn

Transfer Ship To

(5) ANALYSIS LAB

R0nHhy ^^^

DateRfir-rf ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

^

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

Sampling Personnel

(Name-)

(Phone) Sampling Date

(Beam) (End) r

f

Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

__ Solids nthpr

(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

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Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

DatfiRfirH l

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

Q Samohna Office 0 Shipping Information

Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

Ship To i

bullv

Attn

Transfer Ship To

0 ANALYSIS LAB

f f ftYlt4 Pm~r) by

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

bdquo - f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

natfiRfir-H 2

Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

- -1 i

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

^___ Solids OtVlfir

(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

0 SAMPLE MATRIX fPViorlr Onal

Water

Q Samplina Office

Sampling Personnel

(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

Date Shipped

Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

_ FlnonH^^pH

LAB FILE COPY

(T) Ship To

Attn

Transfer Ship To

() ANALYSIS LAB

RwH Vy f i

DatfiRficHshy

^^^ f 1 ^ J ^AM

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

1 LuW CoilUtillLldtlOll

0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

DateRfirH- ^ ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

Water

(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

(Phone) t~ Dfltp- SViipppri

Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

fi Sample Description ^5) Mark Volume Level ^-J (Check One) On Sample Bottle

Surfflrp Wator Check Analysis required f mdash Ground Water

Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

f

Attn

Transfer Ship To

(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

DatftRprHshy

(fo) C 1 f --raquoraquo-

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

f V -

Attnx i f r - ^ f lt Transfer Ship To

reg ANALYSIS LAB

R^Hhy - ^

natfiRp-rrl lt ^ ^

Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

-

gt W ~ f b

Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

- ^ - bull

Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 30: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office bull bull y Ai gt ci V r IK H ij K7 Xvjl l - i l V b)7 2490 Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATtifi I ) QC REQUIREMENTS SAMPLE CONCENTRATION i (Check One)

Case No Designate below OC analysis selected Low Concentration

I^h Sample TO No (Tf Applicable) Medium Concentration

QC PfraquopoH- No D iplirate SAMPLE MATRIX (Check One)

Matrix Spike Water laquoN ^ Soil Sediment

Description TechniciaGCl Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation(Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation ft (Dioxins)

Preparation(VGA) lt i

- V

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

T ah Nmlaquo QT REQUIREMENTS SAMPLE CONCENTRATION (Check One)

HAQA Nrt ppHsignatfi below QC

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No HT mlirota ^ SAMPLE MATRIX

Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

iBjjgsect ORGANICS LABORATORY CHRONICLE (j

T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

r^sgt TSIn noltignfli-ft below QC

I ah Sample in NOanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

bull7 o gt z Date Snipped

Airbill Number

0 Sample Description

Surface Water bull Ground Water

Learhate

0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

0 SAMPLE MATRIX (Check Otae) t

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Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

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ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Pesticides

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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Sample Site NameCode

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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(e) Shipping Information

Name Of Carrier

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(J) Mark Volume Level On Sample Bottle Check Analysis required

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

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LAB FILE COPY

Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

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(s) Mark Volume Level On Sample Bottle Check Analysis required

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 31: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

BSHB US ENVIRONMENTAL PROTECnON AGENCY HWISomi BrlB PO Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 PTS -557 2490 fHfH ~~JSi a ORGANICS LABORATORY CHRONICLE ( bull

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Matrix Spike tty n (Check One)

9 Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1271 ORGANICS TRAFFIC REPORT T) Case Number

Sample Site NameCode

0 Regional Office Z Sampling Personnel

(Phone)

Sampling Date hfiA

(T) Shipping Information

Name of Carrier

Date Snipped

Airbill Number

(s) Sample Description

Surface Water

Ground Water

Leachate

SAMPLE CONCENTRATION S Ship To (Check One)

f Low Concentration Medium Concentration

SAMPLE MATRIX (Check One)

_bull Water SoiVSediment

Transfer Ship To

For each sample collected specify number Icopy Analysis Lab of containers used and mark volume level Recd hy-f H O on each bottle

Sample Condition Number of Approximate on Receipt (eg broken nt

Total Volume ice Chain-of-Custody etc) Containers Water (Extractable)

Water (VGA)

SoiVSediment

Water (ExtVOA)

Other

Sample Location

Mixed Media

Solids

Other (specify)

(10) Special HandUng Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number PO Box 818 dew maiia Virginia 22313 703 557490 laquoFiT b 72490

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hName QC REQUIREMENTS SAMPLE CONCENTRATION

Case No

T ab Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

OT Report No Duplicate SAMPLE MATRIX (Chec^eOlW

Matrix Spike Water SoilSediment f

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

bullV

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

fSBffii US ENVIRONMENTAL PROTECTION AGENCY HWISomi BKlia PO Box 818 Alexandra Virginia 223 13-703 557-2490 -FTS 557-2490

iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

(Check One) CflS^No

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Plaquotignfltfi hfilowQC analysis performed

(Tf Applirahle^ Low Concentration Medium Concentration

QT RlaquopoH- TMo Hi mlirata SAMPLE MATRIX titty g j^CheckOne)

Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

- Sa^SiteNan-eCode

(s) RecriorM Offiw ^ff ^ bull^-s if

Sampling Personnel

tt7 $~poundgt6amp (Phone)

(Begin) (End)

0 Shipping Information

Name of Carrier

asf-z Date Shipped

Airbill Number

reg Sample Description

Surf are Water

( Omiind Water

Leachate

copy SAMPLE CC DNCENTRATION 0 Ship Toy Ir stf (gflpi C (Cl ieck One)

LowrC Concentration Mediu im Concentration

Q) SAMPLEM ATRIX (Check One)

Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

CvJi^shy

(D For each sample collected sp ecify number copy AnfllyRJsLrab of containers used and mark volume level R^cd byM raquo 0 55 yn on each bottle nate RLpound5 SS- 1

Sftrnplfl Condition OXI Receipt (e ltj brokfln no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

(D Sample Location

Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

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0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

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n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

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(3) SAMPLE MATRIX (Check One)

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Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

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T ah Sample ID No (If Applicable^ Medium Concentration

QT Report No Dnnlicate SAMPLE MATRIX (Check One)

Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

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(Begin) (End)

copy Shipping Information

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Name of Carrier

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copy Sample Description

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Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

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(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Low ConctJiiUdlion

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Sampling Personnel Name Of Carrier

(Name)

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Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

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(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

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Transfer Ship To

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Sample Condition On Receipt

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Sample Description copy (Check One) bdquo Surface Water

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0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

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(T) Shipping Information Name Of Carrier

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(4) Ship To ^ bdquo 4

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M90-FTS 55

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Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

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Sample Description copy (Check One) Surface Water

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Solids Other

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MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

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Water

(J) Shipping Information

Name Of Carrier

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Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

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LAB FJLE COPY

(4) Ship To

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(5) ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

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(Name-)

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(Beam) (End) r

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Sample Description copy (Check One) bdquo Surface Water

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Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

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Sulfide Cyanide

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LAB FILE COPY

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Transfer Ship To

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

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Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

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TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

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Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

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Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

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(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

0 SAMPLE MATRIX fPViorlr Onal

Water

Q Samplina Office

Sampling Personnel

(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

Date Shipped

Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

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LAB FILE COPY

(T) Ship To

Attn

Transfer Ship To

() ANALYSIS LAB

RwH Vy f i

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(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

1 LuW CoilUtillLldtlOll

0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

DateRfirH- ^ ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

Water

(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

(Phone) t~ Dfltp- SViipppri

Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

ExtractionPreparation (Dioxins) bull ) 4gt

Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

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Complete section below only if sample is to be used for duplicate or spike analyses

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ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

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(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Mixed Media

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike O t i

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

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Sampling Personnel

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(Phone) Sampling Date

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Surface Water r Ground Water

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(specify) MATCHES ORGANir SAMPLF NO

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Low Cuuctmlidliuii

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0 Shipping Information

Name Of Carrier

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(B) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

(4) Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides)

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Preparation (VGA) ji

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Name of Carrier

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LowrC Concentration Mediu im Concentration

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SoilSediment

Water (ExtVOA)

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Mixed Media

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(If Applicable) Low Concentration Medium Concentration

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Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

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Mixed Media

Solids

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Craquolaquoe No

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Designate below OC analysis selected

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Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

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Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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(Begin) (End)

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(3) SAMPLE MATRIX (Check One)

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For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

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Name of Carrier Other

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Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

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Sample Site NameCode

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Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

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Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

JB^JI ORGANICS LABORATORY CHRONICLE (j

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(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

-bull 5

Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

X^ ixxdi= Alexandra VA 22313 703 557 2490 -FTS 5572490 IMA 8870 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Low ConctJiiUdlion

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 34: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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iSJggJI ORGAN1CS LABORATORY CHRONICLE C^ZZr ^H| T h Nlaquomlaquo OH RFQT ITREMENTS SAMPLE CONCENTRATION

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC(Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

A 1272 ORGAN1CS TRAFFIC REPORT 0 Case Number

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(Begin) (End)

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Name of Carrier

asf-z Date Shipped

Airbill Number

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Surf are Water

( Omiind Water

Leachate

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LowrC Concentration Mediu im Concentration

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Transfer ~ Water ampt 2s~ CJ SoiVS adiment Ship To v d

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Water (Extractable) f

^ Water J F^raquoV (VGA)

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

) Special Handling Instructions (e g safety precautions hazardous nature)

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

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Airbill Number

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

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bull Water SouS adiment

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0 For each sample collected sp ecify number (TT) Analynifi LiAb i of containers used and mark volume level pLrl hyy^7-^ltSr flL on each bottle Date R H- 9 -f^^

Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

XV tf^ 4 ]d| ^ ^ fe rn

Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

^ Ground Water Solids

Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

le Condition On iteoapt (eg broken no Number of Approximateice Chain-of-Custody etc) Containers Total Volume

Sample Location

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T ah Sample ID No (If Applicable^ Medium Concentration

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Matrix Spike _ Water flOl

SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

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copy Shipping Information

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Name of Carrier

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copy Sample Description

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Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

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QC (Acid)

QC (Pesticides)

QC (Dioxins)

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Page 35: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Matrix Spike WN 01W Water SoilSediment

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

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Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

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ExtractionPreparation (BaseNeutral)

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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ORGANICS LABORATORY CHRONICLE (ANALYSIS)

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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(Phone)

Sampling Date

(Begin) (End)

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Name of Carrier Other

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Airbill Number

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Surf ace Water Mixed Media

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(10) Special Handling Instructions (e g safety precautions hazardous nature)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Sample Site NameCode

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(Begin) (End)

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Water (VOA) 2 ^lt

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Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

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Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

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copy Sample Description (Check One)

Surface Water r Ground Water

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(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

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Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

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(B) Mark Volume Level On Sample Bottle Check Analysis required

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Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

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MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Site NameCode

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(e) Shipping Information

Name Of Carrier

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(J) Mark Volume Level On Sample Bottle Check Analysis required

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(e) Shipping Information Name Of Carrier

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Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

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Sample Condition On Receipt

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(Check One) Sample Site NameCode Luw Cuiicenlidliou

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LAB FILE COPY

(4) Ship To - 1 A

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Sample Description copy (Check One) Surface Water OiroTinH Writer

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Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

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Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

(T) Ship To

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(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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(a) Mark Volume Level On Sample Bottle Check Analysis required

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LAB FILE COPY

0 Ship To

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Transfer Ship To

() ANALYSIS LAB

R0H hy f

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

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Name Of Carrier

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LAB FILE COPY

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

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Sampling Personnel Name Of Carrier it

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Sampling Date Airlr1 Niirphfir shy

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Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 36: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office lt gt xV A v gt r Yrlt nmj 7H3 5b7 2490 -HS raquo7149G Sample Number

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^hNATne QC REQUIREMENTS SAMPLE CONCENTRATION

Case No Designate below OC (Check One)

T jraquoh Sample ID Noanalysis selected

(If Applicable) Low Concentration Medium Concentration

QC Report No Duplicate SAMPLE MATRIX (Check OneL eamp)

Matrix Spike WN 01W Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) gt

ExtractionPreparation (Dioxins)

Preparation (VGA)

- J i f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation (BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

bullbullbull US ENVIRONMENTAL PROTECTION AGENCY HWISomf BtlaquolH PO Box 8 1 8 Alexandria Virginia 223 13-703 557-2490 FTS 557-2490 mmn ~

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T^h Name QH REQT IIREMENTS SAMPLE CONCENTRATION (Check One)

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(Tf Applicable) Low Concentration Medium Concentration

QC Report No T^1 mlirata - SAMPLE MATRIX fy y (Check One)

Matrix Spike Water ^ SoilSediment

D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

ORGANICS TRAFFIC REPORT 0 Case Number

Sample Site NameCode i

0 Regional Office A^9 Sampling Personnel

(Ijlame)

(Phone) Sampling Date 7v 7^7 f^c^

(Begin) (End)

0 Shipping Information

fatffft pound5ltpj res Name of Camer

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Airbill Number

0 Sample Description

Surface Water bull Ground Water

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0 SAMPLE CC 3NCENTRATION (Cl ieck One)

LowC Concentration Mediu m Concentration

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Sample Condittom on Receipt (eg broken nc Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) o2 fraquol Water FP (VOA) 3

SoiVSediment

Water (ExtVOA)

Other

0 Sample Location

Mixed Media

Solids

Other (specify)

Ship To If ft f

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Transfer

(To) Special Handling Instructions (e g safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T-ahNatne QC REQUIREMENTS SAMPLE CONCENTRATION

Craquolaquoe No

Iflb Sample ID No

Designate below OC analysis selected

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QC RlaquopJt No Duplicate SAMPLE MATRIX

Matrix Spike Water

(Check One)

wnM 01 W WW v SoilSediment JAgt i

n y^- Description Technician Signature Detail Below Pertinent Information andor

Date Time ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

I

i bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

y^ US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number A PO Box 818 AlexandriaVirginia22313-703557-249OFTS 557-2490 is

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

rc^M^

Lab Sample ID Nltraquo

Designate below QC analysis performed

(If Applicable)

(Check One)

Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

i gt I ltI -gt I

Sample Site NameCode

copy Regional Office Sampling Personnel

(Phone)

Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

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ExtractionPreparation (Acid)

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ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Pesticides

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Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

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Sample Site NameCode

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Sampling Personnel

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(Phone) Sampling Date

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Name Of Carrier

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LAB FILE COPY

(4) Ship To

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Sample Condition On Receipt

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(e) Shipping Information

Name Of Carrier s

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(s) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

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TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 37: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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D srrintion Anal^t Signature Detail Below Pertinent Information and or DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC(Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office

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Sample Site NameCode i

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Water (Extractable) o2 fraquol Water FP (VOA) 3

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Mixed Media

Solids

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number 1 u b v v - Abullraquo a iri Viiqinia gtpound-ni 703 557-M9j bullIIS 49J

ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides) J

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

y^ US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number A PO Box 818 AlexandriaVirginia22313-703557-249OFTS 557-2490 is

ORGANICS LABORATORY CHRONICLE (ANALYSIS)

ThNtrade QC REQUIREMENTS SAMPLE CONCENTRATION

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Low Concentration Medium Concentration

QT Rlaquoprraquor+ No SAMPLE MATRIX

Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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Sampling Date

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

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QC (Acid)

QC(Pesticides)

QC (Dioxins)

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ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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Sample Site NameCode

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Page 38: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

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Craquolaquoe No

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Low Concentration Medium Concentration

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ExtractionPreparation (Dioxins) bullill

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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copy Regional Office Sampling Personnel

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Sampling Date

(Begin) (End)

() Shipping Information

copy SAMPLE CONCENTRATION (Check One)

__ Low Concentration Medium Concentration

(3) SAMPLE MATRIX (Check One)

Water SoilSediment

Ship To irraquof jgtr~

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Transfer SEP 2 Ship To

For each sample collected specify number (n) Anal of containers used and mark volume level Recd by on each bottle

Water (Extractable)

Water (VGA)

SoilSediment

I jpoundffre Water (ExtVOA)

Name of Carrier Other

-t-f-Date Shipped

Airbill Number

copy Sample Description

Surf ace Water Mixed Media

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ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

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QC (Acid)

QC(Pesticides)

QC (Dioxins)

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ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

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Page 39: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

y^ US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number A PO Box 818 AlexandriaVirginia22313-703557-249OFTS 557-2490 is

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Low Concentration Medium Concentration

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Matrix Spike Water SoilSediment

Draquolaquocrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

A 1274 ORGANICS TRAFFIC REPORT T) Case Number

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Sample Site NameCode

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Name of Carrier Other

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Airbill Number

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Leachate Other (specify)

(10) Special Handling Instructions (e g safety precautions hazardous nature)

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Sample Location

bullH l US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office ^^gmmimfim

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Matrix Spike _ Water flOl

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Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

BfBBB US ENVIRONMENTAL PROTECTION AGENCY HWISomi Qfrly PO Box 818 Alexandria Virginia 223 13-703 557-2490 -FTS -557-2490 miimJSJBijgil ORGANICS LABORATORY CHRONICLE (j bull

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Matrix Spike Water SoilSediment

Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

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Complete section below only if sample is to be used for duplicate or spike analyses

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ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

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Page 40: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC (VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI SoiTiple Management Office Sample Number

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Name of Carrier Other

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Airbill Number

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Surf ace Water Mixed Media

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

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Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office IO I- bullbullbullbull c bullbull Agtxlaquoina Vnyimu22313 703 S57 2490 bullIV1 gt7 2490 Sample Number i ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^HN^TTifi 1 QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No Designate below OC analysis selected Low Concentration

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

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T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

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Name Of Carrier

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LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(J) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Name of Carrier Other

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Airbill Number

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

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Sample Site NameCode

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Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

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Matrix Spike HOV Olfltt Water SoilSediment

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

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(specify) MATCHES ORGANir SAMPLF NO

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0 Shipping Information

Name Of Carrier

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(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

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MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

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(T) Shipping Information Name Of Carrier

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Sulhde Cyanide

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LAB FILE COPY

(4) Ship To ^ bdquo 4

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0 ANALYSIS LAB

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Description copy (Check One) Surface Water

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Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 - Task 3 Ammonia

Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

jf S -J i jr

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Transfer Ship To

(5) ANALYSIS LAB

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

)7-2490-FTS 5572490

IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

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(Name-)

(Phone) Sampling Date

(Beam) (End) r

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Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

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Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

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0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

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Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

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Sampling Personnel Name Of Carrier

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Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

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Sulfide Solids Cyanide OtVmr

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LAB FILE COPY

Ship To i

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Transfer Ship To

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

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Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

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Low CuiiceiilidLiuii

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(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

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Airbill MiimhfiTshy

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LAB FILE COPY

(4) Ship To - 1 A

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(e) Shipping Information

Name Of Carrier s

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(e) Shipping Information

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation (Pesticides) tf

ExtractionPreparation (Dioxins)

Preparation(VGA) i bull

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation

ExtractionPreparation(Dioxins) QC

Preparation (VOA)QC

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Descrintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Acid

Pesticides

Dioxins

VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

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Sample Site NameCode

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Sampling Date

(Begin) (End)

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JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

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ij|fimT3ft ^^oncntioii on Receipt (eg broken ac Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

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Mixed Media

Solids

Other (specify)

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QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

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Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

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Matrix Spike O t i

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

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Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

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Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

J Water

(jj) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

bulllt f t ~ J

Attn

Transfer Ship To

0 ANALYSIS LAB

Rerrt hy ^

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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(Phone) Sampling Date

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Sample Description copy (Check One) bdquo Surface Water

_fc^mdash Ground Water

____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

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Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

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PPI-H -vy r

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M bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

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(Phone)

Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water

f mdash Ground Water

Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 - Task 3 Ammonia

Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

jf S -J i jr

Attn

Transfer Ship To

(5) ANALYSIS LAB

R0nHhy ^^^

DateRfir-rf ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

^

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

)7-2490-FTS 5572490

IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

Sampling Personnel

(Name-)

(Phone) Sampling Date

(Beam) (End) r

f

Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

__ Solids nthpr

(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

shy bull

Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

DatfiRfirH l

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

Q Samohna Office 0 Shipping Information

Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

Ship To i

bullv

Attn

Transfer Ship To

0 ANALYSIS LAB

f f ftYlt4 Pm~r) by

gt v 2 Datfi Rpgtr-H

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

bdquo - f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

natfiRfir-H 2

Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

- -1 i

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

^___ Solids OtVlfir

(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Acid

Pesticides

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VOA

Complete section below only if sample is used for duplicate or spike analyses

QC (BaseNeutral)

QC (Acid)

QC(Pesticides)

QC (Dioxins)

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Complete section below only if sample is used for duplicate or spike analyses

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QC (Acid)

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

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LAB FILE COPY

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0 ANALYSIS LAB if

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Sample Condition On Receipt

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Sample Site NameCode

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Low CuiiceiilidLiuii

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Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

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LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

0 SAMPLE MATRIX fPViorlr Onal

Water

Q Samplina Office

Sampling Personnel

(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

Date Shipped

Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

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LAB FILE COPY

(T) Ship To

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Transfer Ship To

() ANALYSIS LAB

RwH Vy f i

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

1 LuW CoilUtillLldtlOll

0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

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Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

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Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

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(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

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Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

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Attn

Transfer Ship To

(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

DatftRprHshy

(fo) C 1 f --raquoraquo-

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(ltv

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

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reg ANALYSIS LAB

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

-

gt W ~ f b

Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

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Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

- ^ - bull

Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 44: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HW1 Sample Management Office

ORGANICS TRAFFIC REPORT copy Case Number

Sample Site NameCode

() Regional QfPw^9 Sampling Personnel

jMf^yampH(Phone)

Sampling Date

(Begin) (End)

copy Shipping Information

JfoJWampi fjiampt faZ1

Name of Carrier

Date Shipped

poundC) ~j ltypound

Airbill Number

copy Sample Description

Surface Water

V firoiinH Water

Leachate

copy SAMPLE C( DNCENTRATION copy Ship To Of bull tlt (Cl leckOne) bullgtbull V C( ty finlt- ty

Y LowC Concentration ^ ^JfX J r Mediu im Concentration rr ^riy ^ A ^ ^ bull lfr ~ lt ^

AC Q^o

copy SAMPLEM ATRIX ^mmmm^fpoundmmampltmm JCheck O

Transfer SEP 27 I9ff V Water Cl_ bull T1 ^T l 1 ^bhlP rdegSoilS ediment ^ff 0 j I

copy For each sample collected sp ecify number (n) AnalysisLab bullbull of containers used and mark volume level on each bottle Date RACU- 7^5SJ

ij|fimT3ft ^^oncntioii on Receipt (eg broken ac Number of Approximate

Containers Total Volume ice Chain-of-Custody etc)

Water (Extractable) a I11

Water (VOA) 2 ^lt

SoilSediment

Water (ExtVOA)

Other

copy Sample Location

Mixed Media

Solids

Other (specify)

copy Special Handling Instructions (eg safety precautions hazardous nature)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office IO I- bullbullbullbull c bullbull Agtxlaquoina Vnyimu22313 703 S57 2490 bullIV1 gt7 2490 Sample Number i ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^HN^TTifi 1 QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

JB^JI ORGANICS LABORATORY CHRONICLE (j

T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

(laquoraquo Mr Dfisignate helow QC

T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

y Water

(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

-bull 5

Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

i k

Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

X^ ixxdi= Alexandra VA 22313 703 557 2490 -FTS 5572490 IMA 8870 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

J Water

(jj) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

bulllt f t ~ J

Attn

Transfer Ship To

0 ANALYSIS LAB

Rerrt hy ^

DatfiRprH- ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f f

Alaquopounddeg sgt US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office -2490 -F

INORGANICS TRAFnC REPORT ltT) Case Number gt

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Name)

(Phone) Sampling Date

(Beam) _ - (End)

Sample Description copy (Check One) bdquo Surface Water

_fc^mdash Ground Water

____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

_raquopound Task 1 amp 2 Task 3 Ammonia

Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

- 11 bull i

Attn

Transfer Ship To

0 ANALYSIS LAB

PPI-H -vy r

natBRlaquofH- y

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

M bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

M90-FTS 55

IMA 8872 bulllaquo PRO^

bullV INORGANICS TRAFFIC REPORT reg Case Number-

Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

(Nflmf)

(Phone)

Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water

f mdash Ground Water

Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 - Task 3 Ammonia

Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

jf S -J i jr

Attn

Transfer Ship To

(5) ANALYSIS LAB

R0nHhy ^^^

DateRfir-rf ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

^

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

)7-2490-FTS 5572490

IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

Sampling Personnel

(Name-)

(Phone) Sampling Date

(Beam) (End) r

f

Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

__ Solids nthpr

(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

shy bull

Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

DatfiRfirH l

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

Q Samohna Office 0 Shipping Information

Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

Ship To i

bullv

Attn

Transfer Ship To

0 ANALYSIS LAB

f f ftYlt4 Pm~r) by

gt v 2 Datfi Rpgtr-H

Sample Condition On Receipt

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bdquo - f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

natfiRfir-H 2

Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

- -1 i

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

^___ Solids OtVlfir

(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

0 SAMPLE MATRIX fPViorlr Onal

Water

Q Samplina Office

Sampling Personnel

(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

Date Shipped

Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

_ FlnonH^^pH

LAB FILE COPY

(T) Ship To

Attn

Transfer Ship To

() ANALYSIS LAB

RwH Vy f i

DatfiRficHshy

^^^ f 1 ^ J ^AM

(eg broken leakage chain of custody etc )

bull bull - raquo bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

1 LuW CoilUtillLldtlOll

0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

DateRfirH- ^ ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

Water

(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

(Phone) t~ Dfltp- SViipppri

Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

fi Sample Description ^5) Mark Volume Level ^-J (Check One) On Sample Bottle

Surfflrp Wator Check Analysis required f mdash Ground Water

Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

f

Attn

Transfer Ship To

(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

DatftRprHshy

(fo) C 1 f --raquoraquo-

(eg broken leakage chain of custody etc )

(ltv

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

f V -

Attnx i f r - ^ f lt Transfer Ship To

reg ANALYSIS LAB

R^Hhy - ^

natfiRp-rrl lt ^ ^

Sample Condition On Receipt

(eg broken leakage qham of custody etc )

I

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

-

gt W ~ f b

Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

- ^ - bull

Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 45: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office IO I- bullbullbullbull c bullbull Agtxlaquoina Vnyimu22313 703 S57 2490 bullIV1 gt7 2490 Sample Number i ORGANICS LABORATORY CHRONICLE (EXTRACTIONS)

T^HN^TTifi 1 QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

Case No Designate below OC analysis selected Low Concentration

I h Sample TO No (If Applicable) Medium Concentration

QC RepoH- NO Duplicate SAMPLE MATRIX (Check One) _ laquolaquoAA

Matrix Spike HOV Olfltt Water SoilSediment

Description Technician Signature Detail Below Pertinent Information andor DateTime ExtractionPreparation Completed Problems Associated with ExtractionPreparation

ExtractionPreparation (BaseNeutral)

ExtractionPreparation (Acid)

ExtractionPreparation(Pesticides)

ExtractionPreparation (Dioxins)

Preparation(VGA)

bull f

Complete section below only if sample is to be used for duplicate or spike analyses

ExtractionPreparation(BaseNeutral) QC

ExtractionPreparation(Acid)QC

ExtractionPreparation(Pesticides) QC

ExtractionPreparation(Dioxins) QC

Preparation(VOA)QC

bullFBtCT| US ENVIRONMENTAL PROTECTION AGENCY HWISomi raquomdash degK~|mj|BTlaquolH P-O Box 8 1 8 Alexandria Virginia 223 1 3 -703 557-2490 -FTS 5575490

JB^JI ORGANICS LABORATORY CHRONICLE (j

T h Nmlaquo QC REQUIREMENTS SAMPLE CONCENTRATION (Check One)

(laquoraquo Mr Dfisignate helow QC

T ^Vgt Sample ID Noanalysis performed

(Tf Applicable) Low Concentration Medium Concentration

QT RlaquoraquoprtT+ Nn Hi mlirfltplaquo yenn SAMPLE MATRIX

Matrix Spike O t i

y Water

(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

-bull 5

Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

i k

Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

X^ ixxdi= Alexandra VA 22313 703 557 2490 -FTS 5572490 IMA 8870 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

J Water

(jj) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

bulllt f t ~ J

Attn

Transfer Ship To

0 ANALYSIS LAB

Rerrt hy ^

DatfiRprH- ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f f

Alaquopounddeg sgt US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office -2490 -F

INORGANICS TRAFnC REPORT ltT) Case Number gt

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Name)

(Phone) Sampling Date

(Beam) _ - (End)

Sample Description copy (Check One) bdquo Surface Water

_fc^mdash Ground Water

____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

_raquopound Task 1 amp 2 Task 3 Ammonia

Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

- 11 bull i

Attn

Transfer Ship To

0 ANALYSIS LAB

PPI-H -vy r

natBRlaquofH- y

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

M90-FTS 55

IMA 8872 bulllaquo PRO^

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Sample Site NameCode

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Sampling Personnel

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(Phone)

Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water

f mdash Ground Water

Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 - Task 3 Ammonia

Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

jf S -J i jr

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(5) ANALYSIS LAB

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

)7-2490-FTS 5572490

IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

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(Name-)

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Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

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(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

shy bull

Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

DatfiRfirH l

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

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Sampling Personnel Name Of Carrier

A i (Name) J

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(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

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Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

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Transfer Ship To

0 ANALYSIS LAB

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

bdquo - f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

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Sample Condition On Receipt

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US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

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Sample Site NameCode

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(Phone) Sampling Date

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Surf tiro WatPT f-JronnH W^t^r

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Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

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Sample Condition On Receipt

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

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(e) Shipping Information

Name Of Carrier

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(Beam) (End)

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Airhill Number-

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(a) Mark Volume Level On Sample Bottle Check Analysis required

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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Sampling Personnel Name Of Carrier

(Name)

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Airbill MiimhfiTshy

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Sample Condition On Receipt

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LAB FILE COPY

(4) Ship To - 1 A

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Name) -

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Sample Description copy (Check One) Surface Water OiroTinH Writer

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(e) Shipping Information

Name Of Carrier s

lt- i

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Airhill Niimhfir

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Solids Othmshy

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Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

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Airbil l NiimhRr

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LAB FILE COPY

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

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Sample Site NameCode

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(Name) -

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(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

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(specify) MATCHES ORGANIC S AMPI K NO

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(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

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Airhill Number

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Sulfide Cyanide

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LAB FILE COPY

(5) Ship To v^1 A

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Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

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US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

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Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

Page 46: SAMPLING DATA REGARDING SHPACK DUMP, CASE # 01318

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(Check One)

SoilSediment

D^Qr-rintion Analyst Signature Detail Below Pertinent Information andor DateTime Analysis Completed Problems Associated with Analysis

BaseNeutral

Add

Pesticides

Dioxins

VGA

Complete section below only if sample is used for duplicate or spike analyses

QC(BaseNeutral)

QC (Acid)

QC (Pesticides)

QC (Dioxins)

QC(VOA)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office axels Alexc

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

Q Samolina Office

Sampling Personnel

(NfliTifgt)

(Phone) Sampling Date

(Beam) (End)

copy Sample Description (Check One)

Surface Water r Ground Water

__^_ Solids Othpr

(specify) MATCHES ORGANir SAMPLF NO

0 SAMPLE CONCENTRATION (Check One)

Low Cuuctmlidliuii

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier

-bull 5

Datp Rhippfirf-

Airbill NTnb(=gtr

(B) Mark Volume Level On Sample Bottle Check Analysis required

-_ Task 1 amp 2 Taltlf 3 Ammnrna

Sulfide Cyanide

TOC Fluoride amp pH

LAB FILE COPY

(4) Ship To

i

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Attn

Transfer Ship To

0 ANALYSIS LAB

Perrj by

DarfiRfirH- ~~

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

V

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

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(Check One) Sample Site NameCode Low ConctJiiUdlion

0 SAMPLE MATRIX (Check One)

J Water

(jj) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) - - Dfltfi Shipper Sampling Date

Airbill NiiTnh^ishy(Beoin) bdquo (End) k

Sample Description (ipound Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required (Ground Watpr

Tact 1 amp 9

Task 3 Ammonia

Sulfide __^_ Solids Cyanide Oth sr TOf1

(specify) ^_ Fluoride amp pH

MATCHES ORGANIC SAMPLE NO -t-ii

LAB FILE COPY

0 Ship To - gt

bulllt f t ~ J

Attn

Transfer Ship To

0 ANALYSIS LAB

Rerrt hy ^

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Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f f

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Sampling Personnel

(Name)

(Phone) Sampling Date

(Beam) _ - (End)

Sample Description copy (Check One) bdquo Surface Water

_fc^mdash Ground Water

____ Solids nth^r

(specify) MATCHES ORGANIC SAMPLE NOshy

0 SAMPLE CONCENTRATION (Check One)

Low Conctjnlidliun

0 SAMPLE MATRIX (Check One)

mdash Water

(T) Shipping Information Name Of Carrier

- raquo

Datp SViipppfi

Airhill Niimher

0 Mark Volume Level On Sample Bottle Check Analysis required

_raquopound Task 1 amp 2 Task 3 Ammonia

Sulhde Cyanide

TOC J_- _ FluondeamppH

LAB FILE COPY

(4) Ship To ^ bdquo 4

- 11 bull i

Attn

Transfer Ship To

0 ANALYSIS LAB

PPI-H -vy r

natBRlaquofH- y

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

M bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

M90-FTS 55

IMA 8872 bulllaquo PRO^

bullV INORGANICS TRAFFIC REPORT reg Case Number-

Sample Site NameCode

(ji) Sampling Office

Sampling Personnel

(Nflmf)

(Phone)

Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water

f mdash Ground Water

Solids Other

(specify)

MATCHES ORGANIC SAMPLE NOmdashimdash mdashgtshy

SAMPLE CONCENTRATION (Check One) mdash Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(J) Shipping Information

Name Of Carrier

- fiflt^ Shipped

Airbil Nimher lt bdquo

(a) Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 - Task 3 Ammonia

Sulfide Cyanide

TOC FlnnrHeamppH

LAB FJLE COPY

(4) Ship To

jf S -J i jr

Attn

Transfer Ship To

(5) ANALYSIS LAB

R0nHhy ^^^

DateRfir-rf ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

^

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

)7-2490-FTS 5572490

IA 8873 INORGANICS TRAFFIC REPORT reg Case Numher

Sample Site NameCode

(cpound) Samplina Office

Sampling Personnel

(Name-)

(Phone) Sampling Date

(Beam) (End) r

f

Sample Description copy (Check One) bdquo Surface Water

(Ground Wfltor

__ Solids nthpr

(specify) MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CoiicenlidLion

0 SAMPLE MATRIX (Check One)

Water

0 Shipping Information

Name Of Carrier - - tx

Datp Shipper)

Airhill Niimhfir bdquo

(J) Mark Volume Level On Sample Bottle Check Analysis required

_ Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

TOC T - - Fluoride amp pH

LAB FILE COPY

0 Ship To ft

shy bull

Attn

Transfer Ship To

0 ANALYSIS LAB

PPCT) by -

DatfiRfirH l

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

J -1

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

AJexandnc IMA 8874 INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION (T) Case Number

(Check One) Sample Site NameCode Luw Cuiiceiilidliua

0 SAMPLE MATRIX (Check One)

Water

Q Samohna Office 0 Shipping Information

Sampling Personnel Name Of Carrier

A i (Name) J

(Phone) f DstB RmppeH t

Sampling Date Airhll Niimhpsr

(Beam) (End)

Sample Description (a) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required GSronnd Water

Ta=lr 1 K

Taslf S Ammonia

Sulfide Solids Cyanide OtVmr

TOC (specify) f ^ - - Fluoride amp pH MATCHES ORGANIC SAMPI K MO 1

LAB FILE COPY

Ship To i

bullv

Attn

Transfer Ship To

0 ANALYSIS LAB

f f ftYlt4 Pm~r) by

gt v 2 Datfi Rpgtr-H

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

bdquo - f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office 2490-ITS 557249C

INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(5) Sampling Office

Sampling Personnel

(NflTTiegt)

(Phone) Sampling Date

(Begin) (End)

Sample Description copy (Check One) Si irface Wat^r

Ground Wfltor

Solids Othpr

(specify) MATCHES ORGANIC S AMPT K NO

0 SAMPLE CONCENTRATION (Check One)

Low Concentration

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier

Date Shipped

Airbill NiimhfiT

(J) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Taslr 3 Ammnnia

Sulfide Cyanide

TOC _-_ Fluoride amp pH

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB if

Ro^hy H

natfiRfir-H 2

Sample Condition On Receipt

(eg broken leakage chain of custody etc ) I

- -1 i

US ENVmONMENTAL PROTECTION AGENCY HWI Sample Management Office M90-FTS 5572490

SB- ^ INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Namfil

(Phone) Sampling Date

(Beoin) (End)

copy Sample Description (Check One)

Surf tiro WatPT f-JronnH W^t^r

^___ Solids OtVlfir

(specify)

MATCHES ORGANIC SAMPLE NO

0 SAMPLE CONCENTRATION (Check One)

Low CuiiceiilidLiuii

0 SAMPLE MATRIX (Check One)

Water

(e) Shipping Information Name Of Carrier

Datlt=gt Shipped

Airhill Niimhfir-

(Y) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammonia

Sulfade Cyanide

fnr FlnnnHoamppH

LAB FILE COPY

Sample Number

IMA 8876

() Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rlaquov1hy bull mdash f 1 ^ i

DateRfirH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

- -

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO Bo

IA 8877 INORGANICS TRAFFIC REPORT reg Case Number

Sample Site NameCode

(2) SAMPLE CONCENTRATION (Check One)

Low ConceuUdhun

0 SAMPLE MATRIX fPViorlr Onal

Water

Q Samplina Office

Sampling Personnel

(e) Shipping Information

Name Of Carrier

(NaiTIA)

(Phone) Sampling Date

(Beam) (End)

Date Shipped

Airhill Number-

copy Sample Description (Check One)

- SurfsrB Water Glround Writer

_____ Solids Oth mshy

(specify) MATCHES ORGANICSAMPTF NO _ mdash

(a) Mark Volume Level On Sample Bottle Check Analysis required

Task 1 amp 2 Task 3 Ammnnifl

Sulfide Cyanide

Tor1

_ FlnonH^^pH

LAB FILE COPY

(T) Ship To

Attn

Transfer Ship To

() ANALYSIS LAB

RwH Vy f i

DatfiRficHshy

^^^ f 1 ^ J ^AM

(eg broken leakage chain of custody etc )

bull bull - raquo bull

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

rub^vcU Alexandria VA22313 703 557-2490-FTS 5572490 IMA SSTS PRddeg INORGANICS TRAFHC REPORT

0 SAMPLE CONCENTRATION reg Case Number (Check One) Sample Site NameCode

1 LuW CoilUtillLldtlOll

0 SAMPLE MATRIX (Check One)

Water _ SoilSedimpnt

(5) Sampling Office 0 Shipping Information

Sampling Personnel Name Of Carrier

(Name)

(Phone) Datfi Shipped Sampling Date

Airbill MiimhfiTshy

(Becrin) (End)

Sample Description (J) Mark Volume Level copy (Check One) On Sample Bottle Surface Water Check Analysis required fiTrgtunH Watdegr

Task 1 amp 2 Task 3 Ammnnia

Sulfide Solids Cyanide nthfir

TOG (specify) FliirHlaquo pH

MATPHRS ORGANIC SAMPIR MO --

LAB FILE COPY

0 Ship To

Attn

Transfer Ship To

0 ANALYSIS LAB

Rpr-H hy - ltbull bull I

DateRfirH- ^ ^

Sample Condition On Receipt

(eg broken leakage chain of custody etc)

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office PO Bo

INORGANICS TRAFFIC REPORT 0 SAMPLE CONCENTRATION reg Case Number

(Check One) Sample Site NameCode Luw Cuiicenlidliou

reg SAMPLE MATRIX (CViprk Onp)

Water

(5) Sampling Office lt (e) Shipping Information

Sampling Personnel Name Of Carrier

(Nnmlt=gt) rshy

(Phone) t~ Dfltp- SViipppri

Sampling Date Airhill Niimhfir

(Beam) (End) bull shy

fi Sample Description ^5) Mark Volume Level ^-J (Check One) On Sample Bottle

Surfflrp Wator Check Analysis required f mdash Ground Water

Task 1 amp 2 Tank 3 Ammonia

Sulhde Solids Cyanide Other Tor (specify)

_ FtiirH^pH MATCHES ORGANIC S AMPT R NO _

LAB FILE COPY

(4) Ship To - 1 A

f

Attn

Transfer Ship To

(9) ANALYSIS LAB

Rlaquorrl Vy - gt ^

DatftRprHshy

(fo) C 1 f --raquoraquo-

(eg broken leakage chain of custody etc )

(ltv

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

KG i^xdo Alexandria VA22313 703 557-2490-FTS 5572490 IMA 8880 INORGANICS TRAFFIC REPORT

reg Case Number Sample Site NameCode

(jj) Sampling Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Beam) (End)

Sample Description copy (Check One) Surface Water OiroTinH Writer

_____ Solids OHi(=r

(specify) MATCHES ORGANIC SAMPLK MO

SAMPLE CONCENTRATION (Check One)

Low CunceutidLiou

0 SAMPLE MATRIX (Check One)

Water SoilSedirnpnt

(e) Shipping Information

Name Of Carrier s

lt- i

DatR SViipppr)

Airhill Niimhfir

(s) Mark Volume Level On Sample Bottle Check Analysis required

i_ Task 1 amp 2 Tsslf 3 Ammonia

Sulfide Cyanide

TOC Fl^^nHo laquor pH

LAB FILE COPY

(T) Ship To

f V -

Attnx i f r - ^ f lt Transfer Ship To

reg ANALYSIS LAB

R^Hhy - ^

natfiRp-rrl lt ^ ^

Sample Condition On Receipt

(eg broken leakage qham of custody etc )

I

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office POBox818Alexc

INORGANICS TRAFFIC REPORT (T) Case Number

Sample Site NameCode

Q Samplina Office

Sampling Personnel

(Nflmp)

(Phone) Sampling Date

(Begin) (End)

copy Sample Description (Check One)

M Surface Water _ (Ground Wfltpt

Solids Othmshy

(specify)

MATCHES ORGANIC SAMPLE NO

SAMPLE CONCENTRATION (Check One)

Low Concentration

reg SAMPLE MATRIX (Check One)

Water

(e) Shipping Information

Name Of Carrier f t flt f raquo - f

Dfltp Shipped

Airbil l NiimhRr

(a) Mark Volume Level On Sample Bottle Check Analysis required

^ Task 1 amp 2 _ Task 3 Ammnma

Sulfide Cyanide

TOG Jmdash- Fluoride amp pH

LAB FILE COPY

0 Ship To

-

gt W ~ f b

Attn^ gt i lt- lt

Transfer Ship To

() ANALYSIS LAB

R0H hy f

DatfiRflcH i

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

v

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

PO boxdib Alexandria VA22313 703 557-2490-FTS 557 249G

IMA 8882 INORGANICS TRAFFIC REPORT reg Case Number lt

Sample Site NameCode

(j Satnplina Office

Sampling Personnel

(Name) -

(Phone) Sampling Date

(Begin) (End) J shy

Sample Description copy (Check One) Surface Water

mdash jmdash Ground Water

Solids Othpr

(specify) MATCHES ORGANIC S AMPI K NO

SAMPLE CONCENTRATION (Check One)

mdash Low Concentration

(5) SAMPLE MATRIX (Check One)

f Water

() Shipping Information

Name Of Carrier

_^

D^tfi RViippesfi t

Airhill Number

Q Mark Volume Level On Sample Bottle Check Analysis required

_L Task 1 amp 2 Task 3 Ammonia

Sulfide Cyanide

Tnr raquo__ FlnrHlaquo amp pH

LAB FILE COPY

(5) Ship To v^1 A

- ^ - bull

Attn

Transfer Ship To

() ANALYSIS LAB

TD u raquo A r lt pprrl hy

DateRttrH

Sample Condition On Receipt

(eg broken leakage chain of custody etc )

f

US ENVIRONMENTAL PROTECTION AGENCY HWI Sample Management Office Sample Number

557 2490-FTS 5572490

SSJ IA 8883 INORGANICS TRAFnC REPORT 0 SAMPLE CONCENTRATION (T) Case Number _ bdquo 0 Ship To shy

(Check One) Sample Site NameCode f mdash Low Concentration ^

-y - gt yen 0 SAMPLE MATRIX

(Check One) f Attn - Water

Transfer Ship To

(5) Sampling Office 0 Shipping Information 0 ANALYSIS LAB

Sampling Personnel Name Of Carrier it

Ror-H Ky - -

(Nam)

DatpR^rH C ^ ^(Phone) Datfi Shipped

Sampling Date Airlr1 Niirphfir shy

(Beam) (End)

Sample Condition On Receipt Sample Description (^ Mark Volume Level copy (Check One) On Sample Bottle (eg broken leakage chain of custody etc )

Burfarp Water Check Analysis required laquo GifounH Wfltpr - lt - Cs_i_ Task 1 amp 2

Tflsk 3 Ammonia Sulfide Solids

OtW Cyanide

TOC (specify) L - Fluoride amp pH

MATCHES ORGANIC SAMPLE NO

LAB FILE COPY

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