sample analysis s169096 esg environmental chemistry ... · pdf filewhere individual results...

221
Sample Analysis S169096 Customer Site Report No S169096 MethodID CustServ Dep.Opt ICPACIDS ICPBRE ICPWSS KONECL KoneNO3 TSBRE1 WSLM50 ID Number Description Sampled REPORT A DO Cl if pH<5.5 DO Mg if SO4(W)>3000 DO NO3 if pH<5.5 SO4-- (acid sol) Magnesium (BRE) SO4-- (H2O sol) mg/l Chloride:(2:1) Nitrate (BRE 2:1): mg/l Total Sulphur. pH (BS1377) CL/1636537 BH13 3.20-3.70 D D D D D D D D D D D D CL/1636538 BH02 1.20-1.60 D D D D D D D D D CL/1636539 BH15 2.50-3.00 D D D D D D D D D Deviating Sample Key A The sample was received in an inappropriate container for this analysis B The sample was received without the correct preservation for this analysis C Headspace present in the sample container D The sampling date was not supplied so holding time may be compromised - applicable to all analysis E Sample processing did not commence within the appropriate holding time F Sample processing did not commence within the appropriate handling time Requested Analysis Key Analysis Required Analysis dependant upon trigger result - Note: due date may be affected if triggered No analysis scheduled ^ Analysis Subcontracted - Note: due date may vary The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling. Report Due 14-Nov-2016 Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory. In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested. ESG Environmental Chemistry Analytical and Deviating Sample Overview ESG Limited Bridgend Consignment No S60609 Velindre Date Logged 07-Nov-2016 Page 3 of 5 Where individual results are flagged see report notes for status. EFS/169096 Ver. 1

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Page 1: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Sample Analysis S169096

CustomerSiteReport No S169096

MethodID

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

CL

KoneN

O3

TS

BR

E1

WS

LM50

ID Number Description Sampled

RE

PO

RT

A

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Chloride:(2:1)

Nitrate (B

RE

2:1): mg/l

Total S

ulphur.

pH (B

S1377)

� �

CL/1636537 BH13 3.20-3.70 D D D D D D D D D D D DCL/1636538 BH02 1.20-1.60 D D D D D D D D DCL/1636539 BH15 2.50-3.00 D D D D D D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 14-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60609

Velindre Date Logged 07-Nov-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/169096 Ver. 1

Page 2: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Oven Dried @ < 35°C

Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Oven Dried @ < 35°C

Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/169096

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/169096 Ver. 1

Page 3: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/169096 Ver. 1

Page 4: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1636537 BH13 D 3.20CL/1636538 BH02 D 1.20CL/1636539 BH15 D 2.50

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9096

Description

SILT SILT SILT

Appendix A Page 1 of 1 11/11/2016EFS/169096 Ver. 1

Page 5: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Our Ref: EFS/169140 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Amelia Gyngell-Jones Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendCF31 1JZ

For the attention of Amelia Gyngell-Jones

Dear Amelia Gyngell-Jones

Sample Analysis - Velindre Hospital

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 20/12/16 when they will be discarded. Please call 01283 554547 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

J ColbourneProject Co-ordinator01283 554547

November 14, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/169140 Ver. 1

Page 6: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendCF31 1JZ

Site: Velindre Hospital

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accredited.Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 14-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/169140 (Ver. 1)

The 11 samples described in this report were registered for analysis by ESG on 08-Nov-2016. This report supersedes any versions previously issued by the laboratory.

14-Nov-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/169140 Ver. 1

Page 7: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

SO

4-- (acid sol)

SO

4-- (H2O

sol) mg/l

Total S

ulphur.

pH (B

S1377)

1636724 TP09 D 5 2.00 04-Nov-16 224 18 0.017 8.5

1636725 TP03 D 5 2.00 04-Nov-16 169 <10 0.023 7.1

1636726 TP12 D 5 1.70 04-Nov-16 202 10 0.021 6.9

1636727 TP15 D 6 2.80 04-Nov-16 176 <10 0.020 8.3

1636728 TP21 D 5 1.50 04-Nov-16 247 12 0.021 6.6

1636729 TP13 D 4 0.70 04-Nov-16 219 <10 0.016 6.5

1636730 TP22 D 4 0.90 04-Nov-16 216 14 0.026 6.6

1636731 TP22 D 7 2.10 04-Nov-16 124 <10 0.021 8.0

1636732 TP23 D 6 1.50 04-Nov-16 222 21 0.019 6.4

1636733 TP24 D 6 1.70 04-Nov-16 340 65 0.026 8.0

1636734 TP24 D 8 2.50 04-Nov-16 206 14 0.019 7.9

Contact

Date Printed

Report Number EFS/169140

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Amelia Gyngell-Jones

14-Nov-2016

Velindre Hospital

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/169140 Ver. 1

Page 8: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Sample Analysis S169140

CustomerSiteReport No S169140

MethodID

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

CL

KoneN

O3

TS

BR

E1

WS

LM50

ID Number Description Sampled

RE

PO

RT

A

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Chloride:(2:1)

Nitrate (B

RE

2:1): mg/l

Total S

ulphur.

pH (B

S1377)

� �

CL/1636724 TP09 2.00-2.40 04/11/16CL/1636725 TP03 2.00 04/11/16CL/1636726 TP12 1.70-1.80 04/11/16CL/1636727 TP15 2.80-3.00 04/11/16CL/1636728 TP21 1.50-1.60 04/11/16CL/1636729 TP13 0.70-0.80 04/11/16CL/1636730 TP22 0.90-1.10 04/11/16CL/1636731 TP22 2.10-2.30 04/11/16CL/1636732 TP23 1.50-1.60 04/11/16CL/1636733 TP24 1.70-1.80 04/11/16CL/1636734 TP24 2.50-2.60 04/11/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 15-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60644

Velindre Hospital Date Logged 08-Nov-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/169140 Ver. 1

Page 9: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Oven Dried @ < 35°C

Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Oven Dried @ < 35°C

Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/169140

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/169140 Ver. 1

Page 10: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/169140 Ver. 1

Page 11: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1636724 TP09 D 5 2.00CL/1636725 TP03 D 5 2.00CL/1636726 TP12 D 5 1.70CL/1636727 TP15 D 6 2.80CL/1636728 TP21 D 5 1.50CL/1636729 TP13 D 4 0.70CL/1636730 TP22 D 4 0.90CL/1636731 TP22 D 7 2.10CL/1636732 TP23 D 6 1.50CL/1636733 TP24 D 6 1.70CL/1636734 TP24 D 8 2.50

Sample Descriptions

ESG Limited Bridgend

Velindre Hospital

S16_9140

Description

SILT CLAY SILT SILT SILT SILT SILT SILT CLAY CLAY CLAY

Appendix A Page 1 of 1 14/11/2016EFS/169140 Ver. 1

Page 12: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Our Ref: EFS/169274 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Amelia Gyngell-Jones Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Amelia Gyngell-Jones

Dear Amelia Gyngell-Jones

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 23/12/16 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

November 18, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/169274 Ver. 1

Page 13: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accredited.Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 18-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Subcontracted Analysis Reports (Pages 3 to 6) The accreditation status of subcontracted analysis is

displayed on the appended subcontracted analysis reports.Analytical and Deviating Sample Overview (Page 7)Table of Method Descriptions (Page 8)Table of Report Notes (Page 9)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/169274 (Ver. 1)

The 2 samples described in this report were registered for analysis by ESG on 11-Nov-2016. This report supersedes any versions previously issued by the laboratory.

18-Nov-2016

Page 1 of 9Where individual results are flagged see report notes for status.

EFS/169274 Ver. 1

Page 14: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

SO

4-- (acid sol)

SO

4-- (H2O

sol) mg/l

Total S

ulphur.

pH (B

S1377)

1637296 BH04S B 23 19.10 227 36 0.023 8.5

1637297 BH08S B 27 21.20 135 11 0.021 8.6

Contact

Date Printed

Report Number EFS/169274

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Amelia Gyngell-Jones

18-Nov-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 9Where individual results are flagged see report notes for status.

EFS/169274 Ver. 1

Page 15: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Sample Analysis S169274

CustomerSiteReport No S169274

MethodID

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

CL

KoneN

O3

TS

BR

E1

WS

LM50

ID Number Description Sampled

RE

PO

RT

A

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Chloride:(2:1)

Nitrate (B

RE

2:1): mg/l

Total S

ulphur.

pH (B

S1377)

� �

CL/1637296 BH04S 19.10-20.20CL/1637297 BH08S 21.20-22.30

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 18-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60737

Velindre Date Logged 11-Nov-2016

Page 7 of 9Where individual results are flagged see report notes for status.

EFS/169274 Ver. 1

Page 16: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Oven Dried @ < 35°C

Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Oven Dried @ < 35°C

Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/169274

Method Descriptions

Page 8 of 9Where individual results are flagged see report notes for status.

EFS/169274 Ver. 1

Page 17: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 9 of 9 EFS/169274 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1637296 BH04S B 23 19.10CL/1637297 BH08S B 27 21.20

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9274

Description

SILT SILT

Appendix A Page 1 of 1 18/11/2016EFS/169274 Ver. 1

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Our Ref: EFS/169570 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 03/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

November 28, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/169570 Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 28-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/169570 (Ver. 1)

The 2 samples described in this report were registered for analysis by ESG on 22-Nov-2016. This report supersedes any versions previously issued by the laboratory.

28-Nov-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/169570 Ver. 1

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Units : % M/M % M/MMethod Codes : FOCS WSLM59

Method Reporting Limits : 0.04 0.04

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

S.O

.M. %

(Calc)

Total O

rganic Carbon

1638438 BH9 D 2 2.00 1.10 0.64

1638439 BH9 D 3 3.00 1.00 0.58

Contact

Date Printed

Report Number EFS/169570

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Adam Putt

28-Nov-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/169570 Ver. 1

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Sample Analysis S169570

CustomerSiteReport No S169570

MethodID

CustS

erv

FO

CS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

Total O

rganic Carbon

CL/1638438 BH9 2.00 D D D DCL/1638439 BH9 3.00 D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 29-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61030

Velindre Date Logged 22-Nov-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/169570 Ver. 1

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Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/169570

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/169570 Ver. 1

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/169570 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1638438 BH9 D 2 2.00CL/1638439 BH9 D 3 3.00

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9570

Description

CLAY CLAY

Appendix A Page 1 of 1 28/11/2016EFS/169570 Ver. 1

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Our Ref: EFS/169572 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 03/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

November 28, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/169572 Ver. 1

Page 27: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 28-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/169572 (Ver. 1)

The 5 samples described in this report were registered for analysis by ESG on 22-Nov-2016. This report supersedes any versions previously issued by the laboratory.

28-Nov-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/169572 Ver. 1

Page 28: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Units : % M/M % M/MMethod Codes : FOCS WSLM59

Method Reporting Limits : 0.04 0.04

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

S.O

.M. %

(Calc)

Total O

rganic Carbon

1638450 BH10 D 2.00 0.64 0.37

1638451 BH10 D 3.00 0.64 0.37

1638452 BH10 D 5.00 0.59 0.34

1638453 BH14 D 2.00 0.66 0.38

1638454 BH14 D 3.00 0.74 0.43

Contact

Date Printed

Report Number EFS/169572

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Adam Putt

28-Nov-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/169572 Ver. 1

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Sample Analysis S169572

CustomerSiteReport No S169572

MethodID

CustS

erv

FO

CS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

Total O

rganic Carbon

CL/1638450 BH10 2.00 D D D DCL/1638451 BH10 3.00 D D D DCL/1638452 BH10 5.00 D D D DCL/1638453 BH14 2.00 D D D DCL/1638454 BH14 3.00 D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 29-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61030

Velindre Date Logged 22-Nov-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/169572 Ver. 1

Page 30: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/169572

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/169572 Ver. 1

Page 31: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/169572 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1638450 BH10 D 2.00CL/1638451 BH10 D 3.00CL/1638452 BH10 D 5.00CL/1638453 BH14 D 2.00CL/1638454 BH14 D 3.00

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9572

Description

CLAY CLAY SILT SILT

MADE GROUND

Appendix A Page 1 of 1 28/11/2016EFS/169572 Ver. 1

Page 33: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Our Ref: EFS/169911 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 13/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 9, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/169911 Ver. 1

Page 34: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 09-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/169911 (Ver. 1)

The 2 samples described in this report were registered for analysis by ESG on 02-Dec-2016. This report supersedes any versions previously issued by the laboratory.

09-Dec-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/169911 Ver. 1

Page 35: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Units : % M/M % M/MMethod Codes : FOCS WSLM59

Method Reporting Limits : 0.04 0.04

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

S.O

.M. %

(Calc)

Total O

rganic Carbon

1639738 TP20 D 2.50 0.67 0.39

1639739 SA08 D 1.80 0.66 0.38

Contact

Date Printed

Report Number EFS/169911

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Adam Putt

09-Dec-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/169911 Ver. 1

Page 36: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Sample Analysis S169911

CustomerSiteReport No S169911

MethodID

CustS

erv

FO

CS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

Total O

rganic Carbon

CL/1639738 TP20 2.50 D D D DCL/1639739 SA08 1.80 D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 09-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61301

Velindre Date Logged 02-Dec-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/169911 Ver. 1

Page 37: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/169911

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/169911 Ver. 1

Page 38: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/169911 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1639738 TP20 D 2.50CL/1639739 SA08 D 1.80

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9911

Description

SILT SILT

Appendix A Page 1 of 1 09/12/2016EFS/169911 Ver. 1

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Our Ref: EFS/169912 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 13/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 9, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/169912 Ver. 1

Page 41: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 09-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/169912 (Ver. 1)

The 8 samples described in this report were registered for analysis by ESG on 02-Dec-2016. This report supersedes any versions previously issued by the laboratory.

09-Dec-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/169912 Ver. 1

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Units : % M/M % M/MMethod Codes : FOCS WSLM59

Method Reporting Limits : 0.04 0.01

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

S.O

.M. %

(Calc)

Total O

rganic Carbon

1639740 BH1 D 2.20 0.47 0.27

1639741 BH1 D 3.20 0.48 0.28

1639742 BH4 D 2.20 0.57 0.33

1639743 BH11 D 1.50 0.67 0.39

1639744 BH11 D 3.50 1.41 0.82

1639745 TP04 D 1.00 1.10 0.64

1639746 TP04 D 2.80 0.31 0.18

1639747 SA07 D 2.20 0.50 0.29

Contact

Date Printed

Report Number EFS/169912

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Adam Putt

09-Dec-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/169912 Ver. 1

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Sample Analysis S169912

CustomerSiteReport No S169912

MethodID

CustS

erv

FO

CS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

Total O

rganic Carbon

CL/1639740 BH1 2.20 D D D DCL/1639741 BH1 3.20 D D D DCL/1639742 BH4 2.20 D D D DCL/1639743 BH11 1.50 D D D DCL/1639744 BH11 3.50 D D D DCL/1639745 TP04 1.00 D D D DCL/1639746 TP04 2.80 D D D DCL/1639747 SA07 2.20-2.30 D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 09-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61300

Velindre Date Logged 02-Dec-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/169912 Ver. 1

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Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/169912

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/169912 Ver. 1

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/169912 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1639740 BH1 D 2.20CL/1639741 BH1 D 3.20CL/1639742 BH4 D 2.20CL/1639743 BH11 D 1.50CL/1639744 BH11 D 3.50CL/1639745 TP04 D 1.00CL/1639746 TP04 D 2.80CL/1639747 SA07 D 2.20

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9912

Description

SILT SILT SILT SILT

STONE SILT

STONE SILT

Appendix A Page 1 of 1 09/12/2016EFS/169912 Ver. 1

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Our Ref: EFS/169916M (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 13/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 9, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Laboratory and Analytical) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501

EFS/169916M Ver. 1

Page 48: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accredited.Any opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 09-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

TEST REPORT

Report No. EFS/169916M (Ver. 1)

The 4 samples described in this report were registered for analysis by ESG on 02-Dec-2016. This report supersedes any versions previously issued by the laboratory.

09-Dec-2016

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

ESG accepts no responsibility for any sampling not carried out by our personnel.

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)Tests marked '^' have been subcontracted to another laboratory.

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/169916M Ver. 1Page 1 of 5

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Units : % % M/M % M/MMethod Codes : TMSS FOCS WSLM59

Method Reporting Limits : 0.1 0.04 0.04Accreditation Code: U N N

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

Tot.M

oisture @ 105C

S.O

.M. %

(Calc)

Total O

rganic Carbon

1639771 BH4 D 2.20 12.5 0.51 0.30

1639772 BH16 D 1.70 15.9 0.90 0.52

1639773 BH17 D 2.00 14.9 1.17 0.68

1639774 BH17 D 4.00 10.5 0.85 0.49

Contact

Date Printed

Report Number EFS/169916M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Adam Putt

09-Dec-2016

Velindre

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/169916M Ver. 1Page 2 of 5

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Sample Analysis S169916M

CustomerSiteReport No S169916M

MethodID

CustS

erv

FO

CS

MC

ertS

TM

SS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

MC

ertS A

nalysis

Tot.M

oisture @ 105C

Total O

rganic Carbon

CL/1639771 BH4 2.20 D D D D D DCL/1639772 BH16 1.70 D D D D D DCL/1639773 BH17 2.00 D D D D D DCL/1639774 BH17 4.00 D D D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 09-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61314

Velindre Date Logged 02-Dec-2016

Where individual results are flagged see report notes for status.EFS/169916M Ver. 1Page 3 of 5

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Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on oven drying gravimetric analysis (% based upon wet weight)

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/169916M

Method Descriptions

Where individual results are flagged see report notes for status.EFS/169916M Ver. 1Page 4 of 5

Page 52: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/169916M Ver. 1Page 5 of 5

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1639771 BH4 D 2.20CL/1639772 BH16 D 1.70CL/1639773 BH17 D 2.00CL/1639774 BH17 D 4.00

Brown Stone CLAY Brown Stone CLAY Brown Stone SILT

Sample Descriptions

ESG Limited Bridgend

Velindre

S16_9916

Description

Brown Stone CLAY

EFS/169916M Ver. 1Appendix A Page 1 of 1

Page 54: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Our Ref: EFS/170081M (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 19/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 14, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Laboratory and Analytical) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501

EFS/170081M Ver. 1

Page 55: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accredited.Any opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 14-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

TEST REPORT

Report No. EFS/170081M (Ver. 1)

The 8 samples described in this report were registered for analysis by ESG on 08-Dec-2016. This report supersedes any versions previously issued by the laboratory.

14-Dec-2016

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

ESG accepts no responsibility for any sampling not carried out by our personnel.

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)Tests marked '^' have been subcontracted to another laboratory.

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/170081M Ver. 1Page 1 of 5

Page 56: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Units : % % M/M % M/MMethod Codes : TMSS FOCS WSLM59

Method Reporting Limits : 0.1 0.04 0.01Accreditation Code: U N N

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

Tot.M

oisture @ 105C

S.O

.M. %

(Calc)

Total O

rganic Carbon

1640498 BH10 D 2.00 (NVM) 4.1 § 0.45 0.26

1640499 BH10 D 3.00 6.7 1.20 0.69

1640500 BH10 D 5.00 10.2 1.63 0.94

1640501 BH14 D 2.00 15.0 0.71 0.41

1640502 BH14 D 3.00 9.4 0.71 0.41

1640503 BH16 D 1.70 11.1 1.13 0.66

1640504 BH17 D 2.00 16.8 0.90 0.52

1640505 BH17 D 4.00 9.6 0.60 0.35

Contact

Date Printed

Report Number EFS/170081M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Adam Putt

14-Dec-2016

Velindre

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/170081M Ver. 1Page 2 of 5

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Sample Analysis S170081M

CustomerSiteReport No S170081M

MethodID

CustS

erv

FO

CS

MC

ertS

TM

SS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

MC

ertS A

nalysis

Tot.M

oisture @ 105C

Total O

rganic Carbon

CL/1640498 BH10 2.00CL/1640499 BH10 3.00CL/1640500 BH10 5.00CL/1640501 BH14 2.00CL/1640502 BH14 3.00CL/1640503 BH16 1.70CL/1640504 BH17 2.00CL/1640505 BH17 4.00

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 14-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61443

Velindre Date Logged 08-Dec-2016

Where individual results are flagged see report notes for status.EFS/170081M Ver. 1Page 3 of 5

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Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on oven drying gravimetric analysis (% based upon wet weight)

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/170081M

Method Descriptions

Where individual results are flagged see report notes for status.EFS/170081M Ver. 1Page 4 of 5

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/170081M Ver. 1Page 5 of 5

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1640498 BH10 D 2.00 (NVM)CL/1640499 BH10 D 3.00CL/1640500 BH10 D 5.00CL/1640501 BH14 D 2.00CL/1640502 BH14 D 3.00CL/1640503 BH16 D 1.70CL/1640504 BH17 D 2.00CL/1640505 BH17 D 4.00 Brown Stone SILT

Brown CLAY Brown CLAY

Brown Stone SILT Brown Stone CLAY Brown Stone CLAY Brown Stone CLAY

Sample Descriptions

ESG Limited Bridgend

Velindre

S17_0081

Description

Brown STONE

EFS/170081M Ver. 1Appendix A Page 1 of 1

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Our Ref: EFS/170083 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 19/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 14, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/170083 Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accredited.Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 14-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/170083 (Ver. 1)

The 2 samples described in this report were registered for analysis by ESG on 08-Dec-2016. This report supersedes any versions previously issued by the laboratory.

14-Dec-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/170083 Ver. 1

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Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

SO

4-- (acid sol)

SO

4-- (H2O

sol) mg/l

Total S

ulphur.

pH (B

S1377)

1640509 BH12 D 3.20 28-Oct-16 511 17 0.039 8.2

1640510 BH17 D 1.20 28-Oct-16 276 28 0.030 6.5

Contact

Date Printed

Report Number EFS/170083

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Adam Putt

14-Dec-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/170083 Ver. 1

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Sample Analysis S170083

CustomerSiteReport No S170083

MethodID

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

CL

KoneN

O3

TS

BR

E1

WS

LM50

ID Number Description Sampled

RE

PO

RT

A

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Chloride:(2:1)

Nitrate (B

RE

2:1): mg/l

Total S

ulphur.

pH (B

S1377)

� �

CL/1640509 BH12 3.20-3.70 28/10/16 ECL/1640510 BH17 1.20-1.70 28/10/16 E

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 14-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61438

Velindre Date Logged 08-Dec-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/170083 Ver. 1

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Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Oven Dried @ < 35°C

Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Oven Dried @ < 35°C

Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/170083

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/170083 Ver. 1

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/170083 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1640509 BH12 D 3.20CL/1640510 BH17 D 1.20

Sample Descriptions

ESG Limited Bridgend

Velindre

S17_0083

Description

MADE GROUND MADE GROUND

Appendix A Page 1 of 1 14/12/2016EFS/170083 Ver. 1

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Our Ref: EFS/170084 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Adam Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 19/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 14, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/170084 Ver. 1

Page 69: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 14-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/170084 (Ver. 1)

The 2 samples described in this report were registered for analysis by ESG on 08-Dec-2016. This report supersedes any versions previously issued by the laboratory.

14-Dec-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/170084 Ver. 1

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Units : % M/M % M/MMethod Codes : FOCS WSLM59

Method Reporting Limits : 0.04 0.01

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

S.O

.M. %

(Calc)

Total O

rganic Carbon

1640511 BH9 D 2.00 0.64 0.37

1640512 BH9 D 3.00 0.57 0.33

Contact

Date Printed

Report Number EFS/170084

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Adam Putt

14-Dec-2016

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/170084 Ver. 1

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Sample Analysis S170084

CustomerSiteReport No S170084

MethodID

CustS

erv

FO

CS

WS

LM59

ID Number Description Sampled

RE

PO

RT

A

S.O

.M. %

(Calc)

Total O

rganic Carbon

CL/1640511 BH9 2.00 D D D DCL/1640512 BH9 3.00 D D D D

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 14-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61441

Velindre Date Logged 08-Dec-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/170084 Ver. 1

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Matrix MethodID Analysis Basis

Method Description

Soil FOCS Oven Dried @ < 35°C

Calculation of Soil Organic Matter content from Organic Carbon content of soil samples

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/170084

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/170084 Ver. 1

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/170084 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1640511 BH9 D 2.00CL/1640512 BH9 D 3.00

Sample Descriptions

ESG Limited Bridgend

Velindre

S17_0084

Description

STONE STONE

Appendix A Page 1 of 1 14/12/2016EFS/170084 Ver. 1

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Our Ref: EFS/170161 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESGBretby Business ParkAshby RoadBurton-on-Trent

Adam Putt StaffordshireESG Limited Bridgend DE15 0YZESG BridgendUnit 15 Telephone: 01283 554400Crosby Yard Facsimile: 01283 554422WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Adam Putt

Dear Adam Putt

Sample Analysis - Velindre

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 20/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 16, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/170161 Ver. 1

Page 76: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accredited.Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 16-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

Tests marked '^' have been subcontracted to another laboratory.Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/170161 (Ver. 1)

The 1 sample described in this report were registered for analysis by ESG on 09-Dec-2016. This report supersedes any versions previously issued by the laboratory.

16-Dec-2016

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/170161 Ver. 1

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Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LA

B ID

Nu

mb

er C

L/

Client Sample Description

Sa

mp

le D

ate

SO

4-- (a

cid

so

l)

SO

4-- (H

2O

so

l) mg

/l

To

tal S

ulp

hu

r.

pH

(BS

137

7)

1640791 TP19 - 1.30-1.60 1710 39 0.095 7.8

Contact

Date Printed

Report Number EFS/170161

Table Number 1

Fax +44 (0) 1283 554422

Velindre

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend Sample Analysis

Adam Putt

16-Dec-2016

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/170161 Ver. 1

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Sample Analysis S170161

Customer

Site

Report No S170161

MethodID

Cu

stS

erv

De

p.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

CL

Ko

ne

NO

3

TS

BR

E1

WS

LM

50

ID Number Description Sampled

RE

PO

RT

A

DO

Cl if p

H<

5.5

DO

Mg

if SO

4(W

)>3000

DO

NO

3 if p

H<

5.5

SO

4-- (a

cid

so

l)

Mag

nesiu

m (B

RE

)

SO

4-- (H

2O

so

l) mg

/l

Ch

lorid

e:(2

:1)

Nitra

te (B

RE

2:1

): mg

/l

To

tal S

ulp

hu

r.

pH

(BS

1377)

CL/1640791 TP19 - 1.30-1.60 D D D D D D D D D D D D

Deviating Sample Key

A The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggered

No analysis scheduled^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 16-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the

holding time we will do our utmost to prioritise these samples. However,

it is possible that samples could become deviant whilst being processed

in the laboratory.

In this instance please contact the laboratory immediately should you

wish to discuss how you would like us to proceed. If you do not respond

within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61443Velindre Date Logged 09-Dec-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/170161 Ver. 1

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Matrix MethodID Analysis

Basis

Method Description

Soil ICPACIDS Oven Dried @ < 35°C

Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Oven Dried @ < 35°C

Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/170161

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/170161 Ver. 1

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters Analysis

Unless stated otherwise results are expressed as mg/lNil: Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/170161 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1640791 TP19 - 1.30-1.60

Sample Descriptions

ESG Limited Bridgend

Velindre

S17_0161

Description

SILT

Appendix A Page 1 of 1 16/12/2016EFS/170161 Ver. 1

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Our Ref: EFS/170377 (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Amelia Gyngell-Jones Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Amelia Gyngell-Jones

Dear Amelia Gyngell-Jones

Sample Analysis - Velindre Hospital

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 30/01/17 when they will be discarded. Please call 01283 554463 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

K SpencerProject Co-ordinator01283 554463

December 23, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Multi-Sector Services) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501 EFS/170377 Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre Hospital

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accredited.Opinions and interpretations expressed herein are outside the scope of UKAS accreditation.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 23-Dec-2016Tim Barnes Operations Director

Energy & Waste Services

Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)Table of Sample Descriptions (Appendix A Page 1 of 1)

Tests marked '^' have been subcontracted to another laboratory.

Where samples have been flagged as deviant on the Analytical and Deviating Sample Overview, for any reason, the data may not be representative of the sample at the point of sampling and the validity of the data may be affected.

ESG accepts no responsibility for any sampling not carried out by our personnel.

TEST REPORT

Report No. EFS/170377 (Ver. 1)

The 9 samples described in this report were registered for analysis by ESG on 19-Dec-2016. This report supersedes any versions previously issued by the laboratory.

23-Dec-2016

Page 1 of 5Where individual results are flagged see report notes for status.

EFS/170377 Ver. 1

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Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50

Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

SO

4-- (acid sol)

SO

4-- (H2O

sol) mg/l

Total S

ulphur.

pH (B

S1377)

1641733 SA03 D 3 1.90 04-Nov-16 267 21 0.025 8.0

1641734 TP05 D 6 2.00 04-Nov-16 275 <10 0.027 8.4

1641735 TP07 D 6 2.00 04-Nov-16 252 18 0.024 8.5

1641736 TP07 D 7 2.80 04-Nov-16 278 16 0.021 8.4

1641737 TP12 D 7 2.50 04-Nov-16 240 11 0.020 8.1

1641738 TP14 D 6 2.30 04-Nov-16 179 <10 0.020 7.9

1641739 TP15 D 3 0.80 04-Nov-16 297 <10 0.026 7.5

1641740 TP21 D 6 2.30 04-Nov-16 184 <10 0.019 7.6

1641741 TP23 D 9 2.80 04-Nov-16 433 17 0.029 8.3

Contact

Date Printed

Report Number EFS/170377

Table Number 1

Fax +44 (0) 1283 554422

Sample Analysis

Amelia Gyngell-Jones

23-Dec-2016

Velindre Hospital

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name ESG Limited Bridgend

Page 2 of 5Where individual results are flagged see report notes for status.

EFS/170377 Ver. 1

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Sample Analysis S170377

CustomerSiteReport No S170377

MethodID

CustS

erv

Dep.O

pt

ICP

AC

IDS

ICP

BR

E

ICP

WS

S

KO

NE

CL

KoneN

O3

TS

BR

E1

WS

LM50

ID Number Description Sampled

RE

PO

RT

A

DO

Cl if pH

<5.5

DO

Mg if S

O4(W

)>3000

DO

NO

3 if pH<5.5

SO

4-- (acid sol)

Magnesium

(BR

E)

SO

4-- (H2O

sol) mg/l

Chloride:(2:1)

Nitrate (B

RE

2:1): mg/l

Total S

ulphur.

pH (B

S1377)

� �

CL/1641733 SA03 1.90-2.40 04/11/16 ECL/1641734 TP05 2.00-2.30 04/11/16 ECL/1641735 TP07 2.00-2.30 04/11/16 ECL/1641736 TP07 2.80-3.00 04/11/16 ECL/1641737 TP12 2.50-2.70 04/11/16 ECL/1641738 TP14 2.30-2.50 04/11/16 ECL/1641739 TP15 0.80-1.00 04/11/16 ECL/1641740 TP21 2.30-2.50 04/11/16 ECL/1641741 TP23 2.80-3.00 04/11/16 E

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 28-Dec-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S61725

Velindre Hospital Date Logged 19-Dec-2016

Page 3 of 5Where individual results are flagged see report notes for status.

EFS/170377 Ver. 1

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Matrix MethodID Analysis Basis

Method Description

Soil ICPACIDS Oven Dried @ < 35°C

Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil WSLM50 Oven Dried @ < 35°C

Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Report Number: EFS/170377

Method Descriptions

Page 4 of 5Where individual results are flagged see report notes for status.

EFS/170377 Ver. 1

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Page 5 of 5 EFS/170377 Ver. 1

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1641733 SA03 D 3 1.90CL/1641734 TP05 D 6 2.00CL/1641735 TP07 D 6 2.00CL/1641736 TP07 D 7 2.80CL/1641737 TP12 D 7 2.50CL/1641738 TP14 D 6 2.30CL/1641739 TP15 D 3 0.80CL/1641740 TP21 D 6 2.30CL/1641741 TP23 D 9 2.80

Sample Descriptions

ESG Limited Bridgend

Velindre Hospital

S17_0377

Description

CLAY SILT

SAND SILT SILT CLAY SILT SILT SILT

Appendix A Page 1 of 1 23/12/2016EFS/170377 Ver. 1

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January 2017 Report No H6108-16 Issue 1 Appendix F

APPENDIX F

GEOENVIRONMENTAL LABORATORY TEST RESULTS

Soil Sample Analysis Test Reports

EFS/168756 EFS/168759 EFS/168766 EFS/168767

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Our Ref: EFS/168756M (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Mr A Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Mr A Putt

Dear Mr Putt

Sample Analysis - Velindre Cancer Hospital

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 07/12/16 when they will be discarded. Please call 01283 554547 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

J ColbourneProject Co-ordinator01283 554547

November 7, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Laboratory and Analytical) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501

EFS/168756M Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre Cancer Hospital

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accredited.Any opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 07-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

TEST REPORT

Report No. EFS/168756M (Ver. 1)

The 1 sample described in this report were registered for analysis by ESG on 26-Oct-2016. This report supersedes any versions previously issued by the laboratory.

07-Nov-2016

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Page 4)Table of GRO Results (Page 5)Table of TPH (Si) banding (std) (Page 6)GC-FID Chromatograms (Pages 7 to 8)Table of VOC (HSA) Results (Page 9)Subcontracted Analysis Reports (Pages 10 to 11) The accreditation status of subcontracted analysis is

displayed on the appended subcontracted analysis reports.Analytical and Deviating Sample Overview (Pages 12 to 13)Table of Method Descriptions (Page 14)Table of Report Notes (Page 15)Table of Sample Descriptions (Appendix A Page 1 of 1)

ESG accepts no responsibility for any sampling not carried out by our personnel.

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)Tests marked '^' have been subcontracted to another laboratory.

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/168756M Ver. 1Page 1 of 15

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Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg pH Units mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL ICPWSS PHSOIL SFAPI

Method Reporting Limits : 0.2 0.5 0.3 0.2 1.6 0.7 0.5 2 0.5 16 0.5 0.1 36 10 0.5Accreditation Code: UM UM UM UM UM UM UM UM UM UM UM UM UM UM UM

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

1635093 TP23 ES 3 0.50 20-Oct-16 Req <0.5 10.2 0.26 15.3 22 <0.5 31.0 1.0 103.5 115 0.994 53400 185 6.5 <0.6

Contact

Date Printed

Report Number EFS/168756M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 2 of 15

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Units : mg/kg mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : SFAPI SFAPI SFAPI Sub020 TMSS TPHUSSI VOCHSAS ICPMSS KONECR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 0.5 0.5 2 0.1 20 0.6 0.1 0.005 0.04Accreditation Code: UM U UM U U N N N N

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Vanadium

(MS

)

Chrom

ium vi:

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1635093 TP23 ES 3 0.50 20-Oct-16 <0.6 <0.6 <0.3 NAIIS 21.7 Req Req 35.4 <0.1 0.031 0.59 Req

Contact

Date Printed

Report Number EFS/168756M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 3 of 15

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Limited Bridgend: Velindre Cancer HospitalSample Details: TP23 ES 3 0.50 Job Number: S16_8756MLIMS ID Number: CL1635093 Date Booked in: 26-Oct-16QC Batch Number: 161229 Date Extracted: 27-Oct-16

Quantitation File: Initial Calibration Date Analysed: 29-Oct-16Directory: 6\102816GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.63 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 102 2-Fluorobiphenyl 102Acenaphthene-d10 109 Terphenyl-d14 87Phenanthrene-d10 107Chrysene-d12 111Perylene-d12 109

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 4 of 15

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Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: Soil

Job Number: S16_8756 Date Booked in: 26-Oct-16

Directory: E:\TES\DATA\2016\1027HSA_GC9\102716 2016-10-27 13-27-48\123B2301.D Date extracted: 27-Oct-16

Method: Headspace GCFID Date Analysed: 27-Oct-16, 20:02:22Accreditation Code: UM

y * Sample data with an asterisk are not UKAS accredite d.

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1635093 TP23 ES 3 0.50 <0.013 <0.013 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 5 of 15

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ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: SoilJob Number: S16_8756M Separation: Silica gel Date Booked in: 26-Oct-16QC Batch Number: 161229 Eluents: Hexane, DCM Date Extracted: 27-Oct-16Directory: D:\TES\DATA\Y2016\102716TPH_GC14\102716 2016-10-27 14-34-41\074B2601.D Date Analysed: 27-Oct-16, 19:41:23Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

CL1635093 TP23 ES 3 0.50 <5 <5 <5 <5 <5 <5 <5 8.38 <11.19 <11.19 <26 <26

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 6 of 15

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1635093ALI Job Number: S16_8756MMultiplier: 15.2 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP23 ES 3 0.50Acquisition Date/Time: 27-Oct-16, 19:41:23Datafile: D:\TES\DATA\Y2016\102716TPH_GC14\102716 2016-10-27 14-34-41\024F2601.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, Front Signal (024F2601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 7 of 15

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1635093ARO Job Number: S16_8756MMultiplier: 11.2 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP23 ES 3 0.50Acquisition Date/Time: 27-Oct-16, 19:41:23Datafile: D:\TES\DATA\Y2016\102716TPH_GC14\102716 2016-10-27 14-34-41\074B2601.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID2 B, Back Signal (074B2601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 8 of 15

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Limited Bridgend: Velindre Cancer Hospital Directory/Quant file: 027VOC.MS19\ Initial Calibration Matrix: SoilSample Details: TP23 ES 3 0.50 Date Booked in: 26-Oct-16 Method: HeadspaceLIMS ID Number: CL1635093 Date Analysed: 27-Oct-16 Multiplier: 0.94Job Number: S16_8756M Operator: PR Position: 11

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 * - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 - < 4 - U Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 * - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 - < 1 - U Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 - < 1 - U

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 * - < 1 - N 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 - < 4 - U

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 * - < 3 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked * are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Received' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.01 99 Dibromofluoromethane 1071,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.36 102 Toluene-d8 97

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.47 94Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.86 891,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.25 83m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.09 68

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 9 of 15

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Sample Analysis S168756M

CustomerSiteReport No S168756M

MethodID

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL

SF

AP

I

Sub020

ID Number Description Sampled

RE

PO

RT

A

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

Cyanide(F

ree) (AR

)

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

� � � � � � � � � � � � � � � � � � � � �

CL/1635093 TP23 0.50 20/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60296

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168756M Ver. 1Page 12 of 15

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Sample Analysis S168756M

CustomerSiteReport No S168756M

MethodID

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59

ID Number Description Sampled

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

� � �

CL/1635093 TP23 0.50 20/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental Chemistry

Analytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60296

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168756M Ver. 1Page 13 of 15

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Matrix MethodID Analysis Basis

Method Description

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Oven Dried @ < 35°C

Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Oven Dried @ < 35°C

Determination of Metals in Marine Sediments and Soil samples by aqua regia digestion followed by ICPMS detection

Soil ICPSOIL Oven Dried @ < 35°C

Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil KONECR Oven Dried @ < 35°C

Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysis (% based upon wet weight)Soil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/168756M

Method Descriptions

Where individual results are flagged see report notes for status.EFS/168756M Ver. 1Page 14 of 15

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168756M Ver. 1Page 15 of 15

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1635093 TP23 ES 3 0.50

Sample Descriptions

ESG Limited Bridgend

Velindre Cancer Hospital

S16_8756

Description

Brown Stone SILT

EFS/168756M Ver. 1Appendix A Page 1 of 1

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Our Ref: EFS/168759M (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Mr A Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Mr A Putt

Dear Mr Putt

Sample Analysis - Velindre Cancer Hospital

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 07/12/16 when they will be discarded. Please call 01283 554547 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

J ColbourneProject Co-ordinator01283 554547

November 7, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Laboratory and Analytical) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501

EFS/168759M Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre Cancer Hospital

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accredited.Any opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 07-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

TEST REPORT

Report No. EFS/168759M (Ver. 1)

The 2 samples described in this report were registered for analysis by ESG on 26-Oct-2016. This report supersedes any versions previously issued by the laboratory.

07-Nov-2016

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 5)Table of GRO Results (Page 6)Table of TPH (Si) banding (std) (Page 7)GC-FID Chromatograms (Pages 8 to 11)Table of VOC (HSA) Results (Pages 12 to 13)Subcontracted Analysis Reports (Pages 14 to 15) The accreditation status of subcontracted analysis is

displayed on the appended subcontracted analysis reports.Analytical and Deviating Sample Overview (Pages 16 to 17)Table of Method Descriptions (Page 18)Table of Report Notes (Page 19)Table of Sample Descriptions (Appendix A Page 1 of 1)

ESG accepts no responsibility for any sampling not carried out by our personnel.

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)Tests marked '^' have been subcontracted to another laboratory.

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/168759M Ver. 1Page 1 of 19

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Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg pH Units mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL ICPWSS PHSOIL SFAPI

Method Reporting Limits : 0.2 0.5 0.3 0.2 1.6 0.7 0.5 2 0.5 16 0.5 0.1 36 10 0.5Accreditation Code: UM UM UM UM UM UM UM UM UM UM UM UM UM UM UM

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

1635106 TP05 ES 2 0.50 18-Oct-16 Req <0.6 14.0 0.41 23.2 37.8 <0.6 31 1.0 106.6 259 1.018 55800 269 7.6 <0.6

1635144 TP03 ES 1 0.20 18-Oct-16 Req 1.0 19.8 0.54 37.8 112.6 <0.61 50.8 1.1 157.5 258 1.042 45200 719 6.7 <0.7

Contact

Date Printed

Report Number EFS/168759M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 2 of 19

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Units : mg/kg mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : SFAPI SFAPI SFAPI Sub020 TMSS TPHUSSI VOCHSAS ICPMSS KONECR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 0.5 0.5 2 0.1 20 0.6 0.1 0.005 0.04Accreditation Code: UM U UM U U N N N N

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Vanadium

(MS

)

Chrom

ium vi:

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1635106 TP05 ES 2 0.50 18-Oct-16 <0.6 <0.6 <0.3 NAIIS 22.3 Req Req 35.5 <0.1 0.046 1.74 Req

1635144 TP03 ES 1 0.20 18-Oct-16 <0.7 <0.7 <0.3 NAIIS 30.4 Req Req 43.6 <0.1 0.098 4.55 Req

Contact

Date Printed

Report Number EFS/168759M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 3 of 19

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Limited Bridgend: Velindre Cancer HospitalSample Details: TP05 ES 2 0.50 Job Number: S16_8759MLIMS ID Number: CL1635106 Date Booked in: 26-Oct-16QC Batch Number: 161229 Date Extracted: 27-Oct-16

Quantitation File: Initial Calibration Date Analysed: 29-Oct-16Directory: 6\102816GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.65 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 101Acenaphthene-d10 109 Terphenyl-d14 88Phenanthrene-d10 109Chrysene-d12 118Perylene-d12 119

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Limited Bridgend: Velindre Cancer HospitalSample Details: TP03 ES 1 0.20 Job Number: S16_8759MLIMS ID Number: CL1635144 Date Booked in: 26-Oct-16QC Batch Number: 161229 Date Extracted: 27-Oct-16

Quantitation File: Initial Calibration Date Analysed: 29-Oct-16Directory: 6\102816GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.11 - UMAcenaphthylene 208-96-8 3.85 0.13 94 UAcenaphthene 83-32-9 - < 0.11 - UMFluorene 86-73-7 - < 0.11 - UMPhenanthrene 85-01-8 5.03 0.17 98 UMAnthracene 120-12-7 5.07 0.16 98 UFluoranthene 206-44-0 6.24 0.82 93 UMPyrene 129-00-0 6.51 0.56 94 UMBenzo[a]anthracene 56-55-3 8.12 0.65 95 UMChrysene 218-01-9 8.17 0.70 97 UMBenzo[b]fluoranthene 205-99-2 9.62 0.78 93 UMBenzo[k]fluoranthene 207-08-9 9.66 0.27 93 UMBenzo[a]pyrene 50-32-8 10.04 0.45 92 UMIndeno[1,2,3-cd]pyrene 193-39-5 11.42 0.36 74 UMDibenzo[a,h]anthracene 53-70-3 - < 0.11 - UMBenzo[g,h,i]perylene 191-24-2 11.70 0.24 90 UMTotal (USEPA16) PAHs - - < 6.00 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 97 2-Fluorobiphenyl 104Acenaphthene-d10 109 Terphenyl-d14 91Phenanthrene-d10 110Chrysene-d12 121Perylene-d12 120

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 5 of 19

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Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: Soil

Job Number: S16_8759 Date Booked in: 26-Oct-16

Directory: E:\TES\DATA\2016\1027HSA_GC9\102716 2016-10-27 13-27-48\125B2501.D Date extracted: 27-Oct-16

Method: Headspace GCFID Date Analysed: 27-Oct-16, 20:36:43Accreditation Code: UM

y * Sample data with an asterisk are not UKAS accredited .

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1635106 TP05 ES 2 0.50 <0.013 <0.013 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3

CL1635144 TP03 ES 1 0.20 <0.014 <0.014 <0.014 <0.014 <0.014 <0.3 <0.3 <0.3 <0.3 <0.3

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 6 of 19

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ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: SoilJob Number: S16_8759M Separation: Silica gel Date Booked in: 26-Oct-16QC Batch Number: 161237 Eluents: Hexane, DCM Date Extracted: 31-Oct-16Directory: D:\TES\DATA\Y2016\103116TPH_GC3\103116 2016-10-31 13-17-44\070B2601.D Date Analysed: 31-Oct-16, 18:49:42Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

CL1635106 TP05 ES 2 0.50 <5.25 <5 <5.25 <5 <5.25 <5 <5.25 <5 <11.51 <11.27 <26.3 <26

CL1635144 TP03 ES 1 0.20 <5.86 <6 <5.86 <6 <5.86 <6 <5.86 <6 <12.84 14.9 <29.3 <29

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 7 of 19

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1635106ALI Job Number: S16_8759MMultiplier: 16.32 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP05 ES 2 0.50Acquisition Date/Time: 31-Oct-16, 20:59:07Datafile: D:\TES\DATA\Y2016\103116TPH_GC3\103116 2016-10-31 13-17-44\023F3601.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID1 A, (023F3601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 8 of 19

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1635106ARO Job Number: S16_8759MMultiplier: 12 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP05 ES 2 0.50Acquisition Date/Time: 31-Oct-16, 18:36:42Datafile: D:\TES\DATA\Y2016\103116TPH_GC3\103116 2016-10-31 13-17-44\069B2501.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

FID2 B, (069B2501.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 9 of 19

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1635144ALI Job Number: S16_8759MMultiplier: 16.32 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP03 ES 1 0.20Acquisition Date/Time: 31-Oct-16, 21:12:04Datafile: D:\TES\DATA\Y2016\103116TPH_GC3\103116 2016-10-31 13-17-44\024F3701.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (024F3701.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 10 of 19

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromatics Fraction.

Sample ID: CL1635144ARO Job Number: S16_8759MMultiplier: 12.32 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP03 ES 1 0.20Acquisition Date/Time: 31-Oct-16, 18:49:42Datafile: D:\TES\DATA\Y2016\103116TPH_GC3\103116 2016-10-31 13-17-44\070B2601.D

min0 1 2 3 4 5

pA

0

100

200

300

400

500

600

FID2 B, (070B2601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 11 of 19

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Limited Bridgend: Velindre Cancer Hospital Directory/Quant file: 027VOC.MS19\ Initial Calibration Matrix: SoilSample Details: TP05 ES 2 0.50 Date Booked in: 26-Oct-16 Method: HeadspaceLIMS ID Number: CL1635106 Date Analysed: 27-Oct-16 Multiplier: 1.06Job Number: S16_8759M Operator: PR Position: 12

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 * - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 - < 4 - U Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 * - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 - < 1 - U Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 - < 1 - U

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 * - < 1 - N 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 - < 4 - U

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 * - < 3 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked * are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Received' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.01 99 Dibromofluoromethane 1071,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.36 100 Toluene-d8 97

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.47 87Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.86 771,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.26 66m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.09 39

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 12 of 19

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Limited Bridgend: Velindre Cancer Hospital Directory/Quant file: 027VOC.MS19\ Initial Calibration Matrix: SoilSample Details: TP03 ES 1 0.20 Date Booked in: 26-Oct-16 Method: HeadspaceLIMS ID Number: CL1635144 Date Analysed: 27-Oct-16 Multiplier: 1.04Job Number: S16_8759M Operator: PR Position: 13

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 * - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 - < 4 - U Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 * - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 - < 1 - U Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 7 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 - < 1 - U

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 * - < 1 - N 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 - < 4 - U

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 * - < 3 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 7 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 - < 7 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked * are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Received' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.01 99 Dibromofluoromethane 1061,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.36 100 Toluene-d8 94

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.47 81Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.86 651,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.26 50m and p-Xylene 108-38-3/106-42-3 - < 6 - UM Naphthalene-d8 7.09 18

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 13 of 19

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Page 122: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations
Page 123: Sample Analysis S169096 ESG Environmental Chemistry ... · PDF fileWhere individual results are flagged see report notes for status. EFS/169096 Ver ... Opinions and interpretations

Sample Analysis S168759M

CustomerSiteReport No S168759M

MethodID

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL

SF

AP

I

Sub020

ID Number Description Sampled

RE

PO

RT

A

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

Cyanide(F

ree) (AR

)

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

� � � � � � � � � � � � � � � � � � � � �

CL/1635106 TP05 0.50 18/10/16CL/1635144 TP03 0.20 18/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60296

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168759M Ver. 1Page 16 of 19

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Sample Analysis S168759M

CustomerSiteReport No S168759M

MethodID

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59

ID Number Description Sampled

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

� � �

CL/1635106 TP05 0.50 18/10/16CL/1635144 TP03 0.20 18/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60296

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168759M Ver. 1Page 17 of 19

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Matrix MethodID Analysis Basis

Method Description

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Oven Dried @ < 35°C

Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Oven Dried @ < 35°C

Determination of Metals in Marine Sediments and Soil samples by aqua regia digestion followed by ICPMS detection

Soil ICPSOIL Oven Dried @ < 35°C

Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil KONECR Oven Dried @ < 35°C

Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysis (% based upon wet weight)Soil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/168759M

Method Descriptions

Where individual results are flagged see report notes for status.EFS/168759M Ver. 1Page 18 of 19

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table. All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168759M Ver. 1Page 19 of 19

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1635106 TP05 ES 2 0.50CL/1635144 TP03 ES 1 0.20 Brown Stone SILT

Sample Descriptions

ESG Limited Bridgend

Velindre Cancer Hospital

S16_8759

Description

Brown Stone SILT

EFS/168759M Ver. 1Appendix A Page 1 of 1

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Our Ref: EFS/168766M (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Mr A Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Mr A Putt

Dear Mr Putt

Sample Analysis - Velindre Cancer Hospital

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 07/12/16 when they will be discarded. Please call 01283 554547 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

J ColbourneProject Co-ordinator01283 554547

November 7, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Laboratory and Analytical) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501

EFS/168766M Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre Cancer Hospital

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accredited.Any opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 07-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

TEST REPORT

Report No. EFS/168766M (Ver. 1)

The 1 sample described in this report were registered for analysis by ESG on 26-Oct-2016. This report supersedes any versions previously issued by the laboratory.

07-Nov-2016

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Page 4)Table of GRO Results (Page 5)Table of TPH (Si) banding (std) (Page 6)GC-FID Chromatograms (Page 7)Table of VOC (HSA) Results (Page 8)Subcontracted Analysis Reports (Pages 9 to 10) The accreditation status of subcontracted analysis is displayed on the appended subcontracted analysis reports.Analytical and Deviating Sample Overview (Pages 11 to 12)Table of Method Descriptions (Page 13)Table of Report Notes (Page 14)Table of Sample Descriptions (Appendix A Page 1 of 1)

ESG accepts no responsibility for any sampling not carried out by our personnel.

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)Tests marked '^' have been subcontracted to another laboratory.

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/168766M Ver. 1Page 1 of 14

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Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg pH Units mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL ICPWSS PHSOIL SFAPI

Method Reporting Limits : 0.2 0.5 0.3 0.2 1.6 0.7 0.5 2 0.5 16 0.5 0.1 36 10 0.5Accreditation Code: UM UM UM UM UM UM UM UM UM UM UM UM UM UM UM

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

1635142 TP21 ES 2 0.50 20-Oct-16 Req 1 20.5 0.68 31.7 65.6 <0.58 32.2 1.0 139.9 220 1.125 53300 553 8.8 <0.7

Contact

Date Printed

Report Number EFS/168766M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 2 of 14

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Units : mg/kg mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : SFAPI SFAPI SFAPI Sub020 TMSS TPHUSSI VOCHSAS ICPMSS KONECR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 0.5 0.5 2 0.1 20 0.6 0.1 0.005 0.04Accreditation Code: UM U UM U U N N N N

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Vanadium

(MS

)

Chrom

ium vi:

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1635142 TP21 ES 2 0.50 20-Oct-16 <0.7 <0.7 <0.3 NAIIS 26.5 Req Req 41.1 <0.1 0.069 2.13 Req

Contact

Date Printed

Report Number EFS/168766M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 3 of 14

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Limited Bridgend: Velindre Cancer HospitalSample Details: TP21 ES 2 0.50 Job Number: S16_8766MLIMS ID Number: CL1635142 Date Booked in: 26-Oct-16QC Batch Number: 161230 Date Extracted: 27-Oct-16

Quantitation File: Initial Calibration Date Analysed: 27-Oct-16Directory: \102716MS14\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.11 - UMAcenaphthylene 208-96-8 - < 0.11 - UAcenaphthene 83-32-9 - < 0.11 - UMFluorene 86-73-7 - < 0.11 - UMPhenanthrene 85-01-8 - < 0.11 - UMAnthracene 120-12-7 - < 0.11 - UFluoranthene 206-44-0 - < 0.11 - UMPyrene 129-00-0 - < 0.11 - UMBenzo[a]anthracene 56-55-3 - < 0.11 - UMChrysene 218-01-9 - < 0.11 - UMBenzo[b]fluoranthene 205-99-2 - < 0.11 - UMBenzo[k]fluoranthene 207-08-9 - < 0.11 - UMBenzo[a]pyrene 50-32-8 - < 0.11 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.11 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.11 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.11 - UMTotal (USEPA16) PAHs - - < 1.74 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 150 2-Fluorobiphenyl 101Acenaphthene-d10 102 Terphenyl-d14 100Phenanthrene-d10 101Chrysene-d12 115Perylene-d12 107

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 4 of 14

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Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: Soil

Job Number: S16_8766 Date Booked in: 26-Oct-16

Directory: E:\TES\DATA\2016\1027HSA_GC9\102716 2016-10-27 13-27-48\016F1601.D Date extracted: 27-Oct-16

Method: Headspace GCFID Date Analysed: 27-Oct-16, 18:02:13Accreditation Code: UM

y * Sample data with an asterisk are not UKAS accredited .

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1635142 TP21 ES 2 0.50 <0.014 <0.014 <0.014 <0.014 <0.014 <0.3 <0.3 <0.3 <0.3 <0.3

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 5 of 14

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ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: SoilJob Number: S16_8766M Separation: Silica gel Date Booked in: 26-Oct-16QC Batch Number: 161230 Eluents: Hexane, DCM Date Extracted: 27-Oct-16Directory: D:\TES\DATA\Y2016\102716TPH_GC3\102716 2016-10-27 11-06-52\080B4001.D Date Analysed: 27-Oct-16, 19:44:25Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

CL1635142 TP21 ES 2 0.50 <5.50 <5 <5.50 <5 <5.50 <5 <5.50 6.84 <12.04 19.7 <27.5 35.5

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 6 of 14

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1635142ALI Job Number: S16_8766MMultiplier: 16.16 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP21 ES 2 0.50Acquisition Date/Time: 27-Oct-16, 18:38:41Datafile: D:\TES\DATA\Y2016\102716TPH_GC3\102716 2016-10-27 11-06-52\022F3501.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (022F3501.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 7 of 14

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Limited Bridgend: Velindre Cancer Hospital Directory/Quant file: 027VOC.MS19\ Initial Calibration Matrix: SoilSample Details: TP21 ES 2 0.50 Date Booked in: 26-Oct-16 Method: HeadspaceLIMS ID Number: CL1635142 Date Analysed: 27-Oct-16 Multiplier: 1.08Job Number: S16_8766M Operator: PR Position: 15

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 * - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 - < 4 - U Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 * - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 - < 1 - U Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 7 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 - < 1 - U

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 * - < 1 - N 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 - < 4 - U

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 * - < 3 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 7 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 - < 7 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked * are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Received' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.01 94 Dibromofluoromethane 1081,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.36 96 Toluene-d8 94

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.47 83Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.86 711,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.25 59m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.09 28

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 8 of 14

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Sample Analysis S168766M

CustomerSiteReport No S168766M

MethodID

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL

SF

AP

I

Sub020

ID Number Description Sampled

RE

PO

RT

A

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

Cyanide(F

ree) (AR

)

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

� � � � � � � � � � � � � � � � � � � � �

CL/1635142 TP21 0.50 20/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60296

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168766M Ver. 1Page 11 of 14

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Sample Analysis S168766M

CustomerSiteReport No S168766M

MethodID

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59

ID Number Description Sampled

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

� � �

CL/1635142 TP21 0.50 20/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60296

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168766M Ver. 1Page 12 of 14

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Matrix MethodID Analysis Basis

Method Description

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Oven Dried @ < 35°C

Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Oven Dried @ < 35°C

Determination of Metals in Marine Sediments and Soil samples by aqua regia digestion followed by ICPMS detection

Soil ICPSOIL Oven Dried @ < 35°C

Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil KONECR Oven Dried @ < 35°C

Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysis (% based upon wet weight)Soil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/168766M

Method Descriptions

Where individual results are flagged see report notes for status.EFS/168766M Ver. 1Page 13 of 14

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168766M Ver. 1Page 14 of 14

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1635142 TP21 ES 2 0.50

Sample Descriptions

ESG Limited Bridgend

Velindre Cancer Hospital

S16_8766

Description

Brown Stone SILT

EFS/168766M Ver. 1Appendix A Page 1 of 1

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Our Ref: EFS/168767M (Ver. 1)Your Ref: H6108-16

Environmental ChemistryESG

Bretby Business Park

Ashby Road

Burton-on-Trent

Mr A Putt Staffordshire

ESG Limited Bridgend DE15 0YZ

ESG BridgendUnit 15 Telephone: 01283 554400

Crosby Yard Facsimile: 01283 554422

WildmillBridgendMid GlamorganCF31 1JZ

For the attention of Mr A Putt

Dear Mr Putt

Sample Analysis - Velindre Cancer Hospital

Samples from the above site have been analysed in accordance with the schedule supplied.The sample details and the results of analyses for these samples are given in the appended report.

An invoice for this work will follow under a separate cover.

Where appropriate the samples will be kept until 07/12/16 when they will be discarded. Please call 01283 554547 foran extension of this date.Please be aware that our policy for the retention of paper based laboratory records and analysis reports is 6 years.

If I can be of any further assistance please do not hesitate to contact me.

Yours sincerely

for ESG

J ColbourneProject Co-ordinator01283 554547

November 7, 2016

The work was carried out in accordance with Environmental Scientifics Group Ltd (Laboratory and Analytical) Standard Terms and Conditions of Contract.

Environmental Chemistry, ESG, P.O. Box 100, Burton-upon-trent, DE15 0XD Tel: 01283 554400 Fax: 01283 554422Environmental Scientifics Group Limited.

Registered No: 2880501

EFS/168767M Ver. 1

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ESG Limited BridgendESG BridgendUnit 15Crosby Yard WildmillBridgendMid GlamorganCF31 1JZ

Site: Velindre Cancer Hospital

The analysis was completed by:

Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accredited.Any opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.

The following tables are contained in this report:

On behalf ofESG : Date of Issue: 07-Nov-2016Tim Barnes Operations Director

Energy & Waste Services

TEST REPORT

Report No. EFS/168767M (Ver. 1)

The 1 sample described in this report were registered for analysis by ESG on 26-Oct-2016. This report supersedes any versions previously issued by the laboratory.

07-Nov-2016

Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Page 4)Table of GRO Results (Page 5)Table of TPH (Si) banding (std) (Page 6)GC-FID Chromatograms (Page 7)Table of VOC (HSA) Results (Page 8)Subcontracted Analysis Reports (Pages 9 to 10) The accreditation status of subcontracted analysis is displayed on the appended subcontracted analysis reports.Analytical and Deviating Sample Overview (Pages 11 to 12)Table of Method Descriptions (Page 13)Table of Report Notes (Page 14)Table of Sample Descriptions (Appendix A Page 1 of 1)

ESG accepts no responsibility for any sampling not carried out by our personnel.

Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)Tests marked '^' have been subcontracted to another laboratory.

(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.

All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)

Where individual results are flagged see report notes for status.EFS/168767M Ver. 1Page 1 of 14

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Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg pH Units mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL ICPSOIL ICPWSS PHSOIL SFAPI

Method Reporting Limits : 0.2 0.5 0.3 0.2 1.6 0.7 0.5 2 0.5 16 0.5 0.1 36 10 0.5Accreditation Code: UM UM UM UM UM UM UM UM UM UM UM UM UM UM UM

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

pH units (A

R)

Cyanide(F

ree) (AR

)

1635143 TP18 ES 2 0.50 14-Oct-16 Req 0.9 14.8 0.43 21.8 35 <0.6 27.0 1 109.6 223 0.997 47900 253 6.8 <0.6

Contact

Date Printed

Report Number EFS/168767M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 2 of 14

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Units : mg/kg mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : SFAPI SFAPI SFAPI Sub020 TMSS TPHUSSI VOCHSAS ICPMSS KONECR TSBRE1 WSLM59 PAHMSUS

Method Reporting Limits : 0.5 0.5 2 0.1 20 0.6 0.1 0.005 0.04Accreditation Code: UM U UM U U N N N N

LAB

ID N

umber C

L/

Client Sample Description

Sam

ple Date

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

VO

C H

SA

-GC

MS

Vanadium

(MS

)

Chrom

ium vi:

Total S

ulphur.

Total O

rganic Carbon

PA

H (16) by G

CM

S

1635143 TP18 ES 2 0.50 14-Oct-16 <0.6 <0.6 <0.3 NAIIS 20.7 Req Req 32.9 <0.1 0.053 1.29 Req

Contact

Date Printed

Report Number EFS/168767M

Table Number 1

Fax +44 (0) 1283 554422

Bretby Business Park, Ashby Road

Burton-on-Trent, Staffordshire, DE15 0YZ

Tel +44 (0) 1283 554400

Client Name Sample Analysis

Mr A Putt

07-Nov-2016

Velindre Cancer Hospital

ESG Limited Bridgend

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 3 of 14

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1

Polycyclic Aromatic HydrocarbonsGC/MS (SIM)

Customer and Site Details: ESG Limited Bridgend: Velindre Cancer HospitalSample Details: TP18 ES 2 0.50 Job Number: S16_8767MLIMS ID Number: CL1635143 Date Booked in: 26-Oct-16QC Batch Number: 161230 Date Extracted: 27-Oct-16

Quantitation File: Initial Calibration Date Analysed: 27-Oct-16Directory: \102716MS14\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic

Accredited?: Yes

Target Compounds CAS # R.T. Concentration % Fit Accr.

(min) mg/kg code

Naphthalene 91-20-3 - < 0.10 - UMAcenaphthylene 208-96-8 - < 0.10 - UAcenaphthene 83-32-9 - < 0.10 - UMFluorene 86-73-7 - < 0.10 - UMPhenanthrene 85-01-8 - < 0.10 - UMAnthracene 120-12-7 - < 0.10 - UFluoranthene 206-44-0 - < 0.10 - UMPyrene 129-00-0 - < 0.10 - UMBenzo[a]anthracene 56-55-3 - < 0.10 - UMChrysene 218-01-9 - < 0.10 - UMBenzo[b]fluoranthene 205-99-2 - < 0.10 - UMBenzo[k]fluoranthene 207-08-9 - < 0.10 - UMBenzo[a]pyrene 50-32-8 - < 0.10 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.10 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.10 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.10 - UMTotal (USEPA16) PAHs - - < 1.61 - N

"M" denotes that % fit has been manually interpreted

Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 151 2-Fluorobiphenyl 118Acenaphthene-d10 102 Terphenyl-d14 101Phenanthrene-d10 103Chrysene-d12 118Perylene-d12 108

Concentrations are reported on a dry weight basis.

The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 4 of 14

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Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: Soil

Job Number: S16_8767 Date Booked in: 26-Oct-16

Directory: E:\TES\DATA\2016\1027HSA_GC9\102716 2016-10-27 13-27-48\017F1701.D Date extracted: 27-Oct-16

Method: Headspace GCFID Date Analysed: 27-Oct-16, 18:19:23Accreditation Code: UM

y * Sample data with an asterisk are not UKAS accredite d.

Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO

CL1635143 TP18 ES 2 0.50 <0.013 <0.013 <0.013 <0.013 <0.013 <0.3 <0.3 <0.3 <0.3 <0.3

Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

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ALIPHATIC / AROMATIC FRACTION BY GC/FID

Customer and Site Details: ESG Limited Bridgend : Velindre Cancer Hospital Matrix: SoilJob Number: S16_8767M Separation: Silica gel Date Booked in: 26-Oct-16QC Batch Number: 161230 Eluents: Hexane, DCM Date Extracted: 27-Oct-16Directory: D:\TES\DATA\Y2016\102716TPH_GC3\102716 2016-10-27 11-06-52\081B4101.D Date Analysed: 27-Oct-16, 19:57:42Method: Ultra Sonic

This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40

Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aromatics

CL1635143 TP18 ES 2 0.50 <5.09 <5 <5.09 <5 <5.09 8.6 <5.09 18.7 <11.16 29.5 <25.5 59.6

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 6 of 14

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Petroleum Hydrocarbons (C8 to C40) by GC/FID Aliphatics Fraction.

Sample ID: CL1635143ALI Job Number: S16_8767MMultiplier: 16.16 Client: ESG Limited BridgendDilution: 1 Site: Velindre Cancer HospitalAcquisition Method: 5UL_RUNF.M Client Sample Ref: TP18 ES 2 0.50Acquisition Date/Time: 27-Oct-16, 18:51:50Datafile: D:\TES\DATA\Y2016\102716TPH_GC3\102716 2016-10-27 11-06-52\023F3601.D

min0 1 2 3 4 5

pA

0

50

100

150

200

250

300

350

400

450

FID1 A, (023F3601.D)

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 7 of 14

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Volatile Organic Compounds by HSA-GCMS

Accredited?: YesCustomer and Site Details: ESG Limited Bridgend: Velindre Cancer Hospital Directory/Quant file: 027VOC.MS19\ Initial Calibration Matrix: SoilSample Details: TP18 ES 2 0.50 Date Booked in: 26-Oct-16 Method: HeadspaceLIMS ID Number: CL1635143 Date Analysed: 27-Oct-16 Multiplier: 1.06Job Number: S16_8767M Operator: PR Position: 16

Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code

Dichlorodifluoromethane 75-71-8 * - < 1 - N o-Xylene 95-47-6 - < 3 - UM

Chloromethane 74-87-3 - < 4 - U Styrene 100-42-5 - < 1 - UM

Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM

Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM

Chloroethane 75-00-3 - < 3 - UM 1,1,2,2-Tetrachloroethane 79-34-5 * - < 1 - N

Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM

1,1-Dichloroethene 75-35-48 - < 1 - U Bromobenzene 108-86-1 - < 1 - UM

trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM

1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM

MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM

2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM

cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM

Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM

Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM

1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM

Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM

1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM

Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 - < 1 - U

1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM

Trichloroethene 79-01-6 * - < 1 - N 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM

1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 - < 4 - U

Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 * - < 3 - N

Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM

cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM

Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked * are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Received' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.01 93 Dibromofluoromethane 1101,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.36 93 Toluene-d8 94

Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.47 78Ethylbenzene 100-41-4 - < 3 - UM Bromofluorobenzene 5.86 681,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.26 58m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.09 32

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 8 of 14

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Sample Analysis S168767M

CustomerSiteReport No S168767M

MethodID

CustS

erv

GR

OH

SA

ICP

BO

R

ICP

MS

S

ICP

SO

IL

ICP

WS

S

KO

NE

CR

MC

ertS

PA

HM

SU

S

PH

SO

IL

SF

AP

I

Sub020

ID Number Description Sampled

RE

PO

RT

A

GR

O (A

A) by H

SA

GC

-FID

Boron (H

20 Soluble)

Arsenic (M

S)

Cadm

ium (M

S)

Copper (M

S)

Lead (MS

)

Mercury (M

S)

Nickel (M

S)

Selenium

(MS

)

Vanadium

(MS

)

Zinc (M

S)

Barium

.

Beryllium

.

Iron

SO

4-- (H2O

sol) mg/l

Chrom

ium vi:

MC

ertS A

nalysis

PA

H (16) by G

CM

S

pH units (A

R)

Cyanide(F

ree) (AR

)

Cyanide(T

otal) (AR

)

Phenol Index.(A

R)

Thiocyanate(S

CN

)(AR

)

^Asbestos (screen).

� � � � � � � � � � � � � � � � � � � � �

CL/1635143 TP18 0.50 14/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60321

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168767M Ver. 1Page 11 of 14

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Sample Analysis S168767M

CustomerSiteReport No S168767M

MethodID

TM

SS

TP

HU

SS

I

TS

BR

E1

VO

CH

SA

S

WS

LM59

ID Number Description Sampled

Tot.M

oisture @ 105C

TP

H by G

CF

ID (A

R/S

i)

Total S

ulphur.

VO

C H

SA

-GC

MS

Total O

rganic Carbon

� � �

CL/1635143 TP18 0.50 14/10/16

Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeF Sample processing did not commence within the appropriate handling timeRequested Analysis Key

Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled

^ Analysis Subcontracted - Note: due date may vary

The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.

Report Due 02-Nov-2016

Note: For analysis where the scheduled turnaround is greater than the holding time we will do our utmost to prioritise these samples. However, it is possible that samples could become deviant whilst being processed in the laboratory.

In this instance please contact the laboratory immediately should you wish to discuss how you would like us to proceed. If you do not respond within 24 hours, we will proceed as originally requested.

ESG Environmental ChemistryAnalytical and Deviating Sample Overview

ESG Limited Bridgend Consignment No S60321

Velindre Cancer Hospital Date Logged 26-Oct-2016

Where individual results are flagged see report notes for status.EFS/168767M Ver. 1Page 12 of 14

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Matrix MethodID Analysis Basis

Method Description

Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID

Soil ICPBOR Oven Dried @ < 35°C

Determination of Boron in soil samples by hot water extraction followed by ICPOES detection

Soil ICPMSS Oven Dried @ < 35°C

Determination of Metals in Marine Sediments and Soil samples by aqua regia digestion followed by ICPMS detection

Soil ICPSOIL Oven Dried @ < 35°C

Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection

Soil ICPWSS Oven Dried @ < 35°C

Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection

Soil KONECR Oven Dried @ < 35°C

Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection

Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection

Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.

Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-

contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on

oven drying gravimetric analysis (% based upon wet weight)Soil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil

with GCFID detection including quantitation of Aromatic and Aliphatic fractions.

Soil TSBRE1 Oven Dried @ < 35°C

Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection

Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS

Soil WSLM59 Oven Dried @ < 35°C

Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection

Report Number: EFS/168767M

Method Descriptions

Where individual results are flagged see report notes for status.EFS/168767M Ver. 1Page 13 of 14

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Report Notes

Generic Notes

Soil/Solid Analysis

Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.

All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract

Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.

Oil analysis specific

Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC

Gas (Tedlar bag) Analysis

Unless stated otherwise, results are expressed as ug/l

Asbestos Analysis

CH Denotes Chrysotile TR Denotes TremoliteCR Denotes Crocidolite AC Denotes ActinoliteAM Denotes Amosite AN Denotes AnthophyliteNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample

Symbol Reference

^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.

This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling

¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedN.F No FlowNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result§ accreditation has been removed for this result as it is a non-accredited matrix

Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.

Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.

EFS/168767M Ver. 1Page 14 of 14

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Client :

Site :

Report Number :

Note: major constituent in upper case

Lab ID Number Client ID

CL/1635143 TP18 ES 2 0.50

Sample Descriptions

ESG Limited Bridgend

Velindre Cancer Hospital

S16_8767

Description

Brown Stone SILT

EFS/168767M Ver. 1Appendix A Page 1 of 1

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January 2017 Report No H6108-16 Issue 1 Appendix G

APPENDIX G

PHOTOGRAPHS

Trial Pits Plate 1 to 69 Soakaway Pits Plate 70 to 95 Sonic Core Plate 96 to 119

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

Figure

Plate 1 and 2

Velindre Cancer Hospital, Cardiff

Plate 1: TP03 Face A

Plate 2: TP03 Face B

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

Plate 3: TP03 Spoil

Plate 4: TP04 Face A

FigureVelindre Cancer Hospital, Cardiff

Plate 3 and 4

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

Plate 5: TP04 Face B

Plate 6: TP04 Spoil

FigureVelindre Cancer Hospital, Cardiff

Plate 5 and 6

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

Plate 7: TP05 Face A

Plate 8: TP05 Face B

FigureVelindre Cancer Hospital, Cardiff

Plate 7 and 8

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

Plate 9: TP05 Spoil

Plate 10: TP06 Face A

FigureVelindre Cancer Hospital, Cardiff

Plate 9 and 10

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

Plate 12: TP06 Spoil

FigureVelindre Cancer Hospital, Cardiff

Plate 11 and 12

Plate 11: TP06 Face B

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 13 and 14

Plate 13: TP07 Face A

Plate 14: TP07 Face B

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 15 and 16

Plate 15: TP07 Spoil

Plate 16: TP08 Face A

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 17 and 18

Plate 17: TP08 Face B

Plate 18: TP08 Spoil

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 19 and 20

Plate 19: TP09 Face A

Plate 20: TP09 Face B

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 21 and 22

Plate 21: TP09 Spoil

Plate 22: TP10 Face A

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 23 and 24

Plate 23: TP10 Face B

Plate 24: TP10 Spoil

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 25 and 26

Plate 25: TP11 Face A

Plate 26: TP11 Face B

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 27 and 28

Plate 27: TP11 Spoil

Plate 28: TP12 Face A

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 29 and 30

Plate 29: TP12 Face B

Plate 30: TP12 Spoil

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 31 and 32

Plate 31: TP13 Face A

Plate 32: TP13 Face B

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Trial Pit Photographs

Notes:

Project

Project No. H6108-16

Carried out for Velindre NHS Trust

FigureVelindre Cancer Hospital, Cardiff

Plate 33 and 34

Plate 33: TP13 Spoil

Plate 34: TP14 Face A

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust

Plate 35: TP14 Face B

Figure

35 and 36

Velindre Cancer Hospital, Cardiff

Plate 36: TP14 Spoil

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 37 and 38

Plate 37: TP15 Face A

Plate 38: TP15 Face B

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 39 and 40

Plate 40: TP16 Face A

Plate 39: TP15 Spoil

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 41 and 42

Plate 41: TP16 Face B

Plate 42: TP16 Spoil

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 43 and 44

Plate 43: TP17 Face A

Plate 44: TP17 Face B

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 45 and 46

Plate 45: TP17 Spoil

Plate 46: TP18 Face A

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 47 and 48

Plate 47: TP18 Face B

Plate 48: TP18 Spoil

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 49 and 50

Plate 49: TP19 Face A

Plate 50: TP19 Face B

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 51 and 52

Plate 51: TP19 Spoil

Plate 52: TP20 Face A

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 53 and 54

Plate 53: TP20 Face B

Plate 54: TP20 Soil

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 55 and 56

Plate 55: TP21 Face A

Plate 56: TP21 Face B

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 57 and 58

Plate 57: TP21 Soil

Plate 58: TP22 Face A

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 59 and 60

Plate 59: TP22 Face B

Plate 60: TP22 Spoil

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 61 and 62

Plate 61: TP23 Face A

Plate 62: TP23 Face B

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 63 and 64

Plate 63: TP23 Spoil

Plate 64: TP24 Face A

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 65 and 66

Plate 65: TP24 Face B

Plate 66: TP24 Spoil

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 67 and 68

Plate 67: TP25 Face A

Plate 68: TP25 Face B

FigureVelindre Cancer Hospital, Cardiff

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Trial Pit Photographs

Notes:

Project

Project No. H-6108-16

Carried out for Velindre NHS Trust 69

Plate 69: TP25 Spoil

FigureVelindre Cancer Hospital, Cardiff

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Figure

Plate 70 and 71

Plate 70: SA01 Face A

Plate 71: SA01 Face B

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 72: SA01 Spoil

Plate 73: SA02 Face A

Figure

Plate 72 and 73

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 74: SA02 Face B

Plate 75: SA02 Spoil

Figure

Plate 74 and 75

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 76: SA03 Face A

Plate 77: SA03 Face B

Figure

Plate 76 and 77

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 78: SA03 Spoil

Plate 79: SA04 Face A

Figure

Plate 78 and 79

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 80: SA04 Face B

Plate 81: SA04 Spoil

Figure

Plate 80 and 81

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 82: SA05 Face A

Plate 83: SA05 Face B

Figure

Plate 82 and 83

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 84: SA05 Spoil

Plate 85: SA06 Face A

Figure

Plate 84 and 85

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 86: SA06 Face B

Plate 87: SA06 Spoil

Figure

Plate 86 and 87

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 88: SA07 Face A

Plate 89: SA07 Spoil

Figure

Plate 88 and 89

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 90: SA08 Face A

Plate 91: SA08 Face B

Figure

Plate 90 and 91

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 92: SA08 Spoil

Plate 93: SA09 Face A

Figure

Plate 92 and 93

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Soakaway Pit Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H-6108-16

Velindre NHS Trust

Plate 94: SA09 Face B

Plate 95: SA09 Spoil

Figure

Plate 94 and 95

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Figure

Plate 96 and 97

Plate 96: BH02S 11.50-13.00m

Plate 97: BH02S 13.00-14.50m

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 98: BH02S 14.50-16.00m

Plate 99: BH02S 16.00-17.50m

Figure

Plate 98 and 99

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 100: BH02S 17.50-19.00m

Plate 101: BH02S 19.00-20.00m

Figure

Plate 100 and 101

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 102: BH04S 0.00-3.00m

Plate 103: BH04S 3.00-6.00m

Figure

Plate 102 and 103

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 104: BH04S 6.00-9.00m

Plate 105: BH04S 9.00-11.70m

Figure

Plate 104 and 105

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 106: BH04S 11.70-13.90m

Plate 107: BH04S 13.90-15.90m

Figure

Plate 106 and 107

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 108: BH04S 15.90-17.30m

Plate 109: BH04S 17.30-18.50m

Figure

Plate 108 and 109

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 110: BH04S 18.50-20.00m

Plate 111: BH08S 0.00-3.00m

Figure

Plate 110 and 111

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 112: BH08S 3.00-6.00m

Plate 113: BH08S 6.00-9.00m

Figure

Plate 112 and 113

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 114: BH08S 9.00-10.00m

Plate 115: BH08S 10.00-13.00m

Figure

Plate 114 and 115

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 116: BH08S 13.00-15.90m

Plate 117: BH08S 15.90-18.00m

Figure

Plate 116 and 117

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Sonic Photographs

Notes:

Project

Project No.

Carried out for

Velindre Cancer Hospital

H6108-16

Velindre NHS Trust

Plate 118: BH08S 18.00-19.00m

Plate 119: BH08S 19.00-22.30m

Figure

Plate 118 and 119

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Mott MacDonald | Velindre Cancer Centre 8 Preliminary Contaminated Land Risk Assessment

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