rst-02-f-01841 transmittal memo

ADC2.2709

Weston Solutions, Inc. Federal Programs Division Suite 20 i 1090 King Georges Posi Road

^S&JSnHSEM, " i 5 ° n ' N e w Jerse>- ™337-3703 ' 732-225-6116 • Fax 732-225-7037

REMOVAL SUPPORT TEAM www.westonsolutions.com EPA CONTFtACT 68-W-00-113

2 0 1 0 4 6

RST-02-F-01841

TRANSMITTAL MEMO

To:

From:

Subject:

Date:

Louis DiGuardia, OSC

Removal Action Branch, U.S. EPA Region II

Smita Sumbaly, Data Reviewer RST Region II

- American ©rive-Ih Cleaners She Data Validation Assessment

May 09, 2005

The purpose ofthis memo is to transmit the following information:

Data validation results for the following parameters:

VOA- SUMMA Canisters VOA- Charcoal Tubes

09 samples 15 samples

Matrices and Number of Samples

A i r 24 samples

Sampling dates: April 13 and 14,2005

The final data assessment narrative and original analytical data package are attached.

G c : RST PM: Terry Kish

RST SITE FILE TDD #: 02-04-08-0026 ANALYTICAL TDD #: 02-05-04-0006

PCS//: 5303

an employem-owned company

In Association with Scientific and Environmental Associates Inc

Innovative Technological Solutions. Inc.. and TerranearPMC '

ADC2.2710

DATE:

TO:

FROM:

SUBJECT:

U.S. ENVIRONMENTAL PROTECTION AGENCY

MEMORANDUM

May 06. 2005

Louis DiCuardia. OSr USEPA Repinn II

Smita Surnbalv RST Data Review Team

QA/QC Compliance Review Summary

Asrequestedqualitycontjolandperforrnancemeasuresform^ u . ,

Data Completeness Spectra Matching Quality Surrogate Spikes Matrix Spikes/Duplicates Calibration

Blanks DFTPP and BFB Tuning Chromatography Holding Times Compound ID (HSL, TIC)

Summary of Results

Acceptable as Submitted

Acceptable with Comments

Unacceptable, Action Pending

Unacceptable

VOA

X

Data Reviewed by:

Approved By:

Area Code/Phone No.

Smita Surnbalv

g _fr/ —X (732) 225-6116

Date: 05/06/2005

Date: OSflo/cST

ADC2.2711

NARRATIVE

RFP No. 5303

SITE NAME: American Drive-ln Cleaners Site

3801 Hempstead Turnpike. Levittown. New York

Laboratory Name: Datachem Laboratories. 960 West LeVov Drive. Salt 1 ake Citv. UT

INTRODUCTION:

ThelaboratorVsrxrtiono^ A p r j ] ] 3 a n d u ? ( m

The laboratory reported_no_ problem(s) with the receipt of these sample les.

The laboratory reported no. problems with the analyses of volatile organic compounds

Theevaluator has commented o n m e ^ ^ All criteria have been assessed, but no discussion is given where the evaluator has determined that criteria were adequately performed or require no comment. Details relevant to these comments are given on the following forms.

Appropriate Forms I and Chain of Custody have been copied from the original data package and appended to the data assessment narrative for reference.

Volatile fVOAs)

_V_ Holding Time _Y_ Laboratory Control Sample _Y_ GC/MS Tuning _Y_ Compound ID (HSL, TIC) _V_ Calibration, Initial _y_ Spectra Quality _Y_ Calibration, Continuing ' _Y_ Standards

- ^ B , a n k _JL Chromatography _Y_ Surrogate Recovery Data Completeness

Comments:

Refer to Data Assessment Narrative.

ADC2.2712

ATTACHMENT 1 SOP NO. HW-6

PAGE 1

Functional Guidelines for Evaluating Organic Analysis

RFP No.: 5303 SDG No.: 05C-0058-01 and 05C-0058-n?

LABORATORY: DataChem Laboratories. Inc.

SITE: American Drive-In Cleaners Site

DATA ASSESSMENT

The current USEPA Region II Data Validation SOP for the Volatile Organic Analysis of Ambient Air in Canister (Revision 0, April 1994) was used for data review.

For samples collected by charcoal tubes, the data were reviewed by using principles outlined in USEPA Region II Data Validation SOP for Validating Volatile Compounds by SW-846 Method 8260 (Revision 0, April 1995).

All data are valid and acceptable except those analytes rejected "R"(unusable). Due to the detection of QC problems, some analytes may have the "J" (estimated), "N"(presumptive evidence for the presence of the material, "U" (non-detect) or "JN" (presumptive evidence for the presence of the material at an estimated value) flag. AH action is detailed on the attached sheets.

Reviewer's Signature: Smita Surnbalv Date: 05/06/2005

Verified By: Date:

ADC2.2713

ATTACHMENT 1 SOP NO. HW-6

PAGE 2

On April 13 and 14,2005, USEPA Region II Removal Support Team (RST) personnel collected 09 air samples following EPA Method TO-15 and 15 air samples following NIOSH Method 1003 for volatile organic compound analysis, from the American Drive-ln Cleaners Site, 3801 Hempstead Turnpike, Levittown, New York. Within 24 hours of collection, these samples were shipped to Data Chem Laboratories, 960 West LeVoy Drive, Salt Lake City, Utah. The laboratory verified that samples were received intact and no problems were noted.

Field sample identification (ID) and laboratory ID numbers:

Field Sample ID No. Laboratory ID No. Matrix Analysis

DCL Report Group: 05C-0058-01

AD1-AA-EXT1 ADI-AA-EXT2 ADI-IA-US ADI-IA-CHRIS AD1-IA-CHRIS2 AD1-1A-BARB ADI-IA-BLIMP AD1-IA-THRIFT ADI-IA-TB

05C00444 05C00445 05C00446 05C00447 05C00448 05C00449 05C00450 05C00451 05C00452

Air Air Air Air Air Air Air Air Air

VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by

TO-15 TO-15 TO-15 TO-15 TO-15 TO-15 TO-15 TO-15 TO-15

Sampling Date

04/13-04/13-04/13-04/13-04/13-04/13-04/13-04/13-04/13-

14/05 14/05 14/05 14/05 14/05 14/05 14/05 14/05 14/05

DCL Report Group: 05C-0058-02

ADI-SVW-5 05C00453 Air ADI-SVW-4 05C00454 Air ADI-SVW-3 05C00455 Air AD1-SVW-1 05C00456 Air ADI-SVW-2 05C00457 Air ADI-SS-1 05C00458 Air ADI-SS-2 05C00459 Air ADI-SS-3 05C00460 Air ADI-SS-4 05C00461 Air AD1-INF 05C00462 Air ADI-SS-5 O5C00463 Air AD1-SS-6 05C00464 Air ADI-SS-7 2 05C00465 Air AD1-FB 05C00466 Air ADI-LB 05C00467 Air

VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by VOC by

NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003 NIOSH 1003

04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05 04/13/05

'> Air sample ADI-IA-CHRIS2 is a field duplicate of ADI-IA-CHRIS.

2 ) Air sample ADI-SS-7 is a field duplicate of ADI-SS-6.

ADC2.2714

-.IMENT 1 SOP NO. HW-6 P A G E 3

L HOLDING TIME: ~

The amount of an analyte in a sample can change with time due to chemical instabilitv degradation, volatilization, etc. If the specified holding time is exceeded, the data may not be valid Those analytes detected in the samples whose holding time has been exceeded will be qualified as estimated, "J" . The non-detects (sample quantitation limits) will be flagged as estimated, " J " , or unusable, "R", if the holding times are grossly exceeded.

The following action was taken in the samples and analytes shown due to excessive holding time. 6

None

2. SURROGATES

All samples are spiked with surrogate compounds prior to sample preparation to evaluate overall laboratory performance and efficiency ofthe analytical technique. If the measured surrogate concentrations were outside contract specifications, qualifications were applied to the samples and analytes as shown below.

TO-15:None required qualification.

Not applicable for data generated by NIOSH method 1003.

3. MATRIX SPIKE/SPIKE DUPLICATE, MS/MSD:

The MS/MSD data are generated to determine the long term precision and accuracy ofthe analytical method in various matrices. The MS/MSD may be used in conjunction with other QC criteria for additional qualification of data.

All recoveries were within the control limits for LCS and LCSD.

4. BLANK CONTAMINATION:

Quality assurance (QA) blanks, i.e., method, trip, field, or rinse blanks are prepared to identify any contamination which may have been introduced into the samples during sample preparation or field activity. Method blanks measure laboratory contamination. Trip blanks measure cross-contamination of samples during shipment. Field and rinse blanks measure cross-contamination of samples during field operations. If the concentration ofthe analyte is less than 5 times the blank contaminant level (10 times for common contaminants) the analytes are qualified as non-detects, "U". The following analytes in the sample shown were qualified with "U" for these reasons:

A) Method blank contamination:

None

B) Trip blank contamination:

None

ADC2.2715

ATTACHMENT 1 PAGE 4 SOP NO. HW-6

Q Storage Blank ~ ~

Not Applicable

D) TICs "R" rejected

None required qualifications.

5. MASS SPECTROMETER TUNING:

Tuning and performance criteria are established to ensure adequate mass resolution, proper identification of compounds and to some degree, sufficient instrument sensitivity. These criteria are not sample specific. Instrument performance is determined using standard materials. Therefore, these criteria should be met in all circumstances. The tuning standard for volatile organics is Bromofluorobenzene(BFB) and for semi-volatiles DecafluorotriDhenvl-phosphine (DFTPP). F y

If the mass calibration is in error, all associated data will be classified as unusable "R".


6. CALIBRATION:

Satisfactory instrument calibration is established to ensure that the instrument is capable of producing acceptable quantitative data. An initial calibration demonstrates that the instrument is capable of giving acceptable performance at the beginning of an experimental sequence. The continuing calibration checks document that the instrument is civine satisfactory daily performance.

A) Response Factor GC/MS:

The response factor measures the instrument's response to specific chemical compounds The response factor for the Target Compound List (TCL) must be > 0.05 in both initial and continuing calibrations. A value < 0.05 indicates a serious detection and quantitation problem (poor sensitivity). Analytes detected in the sample will be qualified as estimated " J " All non-detects for that compound will be rejected "R". '


B) Percent Relative Standard Deviation (%RSD) and Percent Difference (%D):

Percent RSD is calculated from the initial calibration and is used to indicate the stability of the specific compound response factor over increasing concentration. Percent D compares the response factor of the continuing calibration check to the mean response factor (RRF) from the initial calibration. Percent D is a measure of the instrument's daily performance Percent RSD must be < 30% and %D must be < 25%. A value outside of these limits indicates potential detection and quantitation errors. For these reasons, all positive results are flagged as estimated, "J" and non-detects are flagged "UJ". If %RSD and %D erosslv exceed QC criteria, non-detects data may be qualified "R".

ADC2.2716

ME NT 1 SOP NO. HW-6 PAGE 5

For the PEST/PCB fraction, if %RSD exceeds 20% for all analytes except for the hvn m U S t C X C e e d 3 0 % R S D ) ' a » --ciated^sitWêsut " J " S

The following analytes in the sample shown were qualified for %RSD and %D:

As per method TO-15, following criteria were used for data evaluation: %RSD <30; %D <30.


For NIOSH 1003 method, a quadratic model was used to calibrate the instrument The correlation coefficients for all analytes were greater than 0.995. correlation


8. INTERNAL STANDARDS PERFORMANCE GC/MS:

I

a ^ e c ? K | S t . a i , d a r d S ( I S ) P e r f o r m a n c e c r i t e r i a e n s«re that the GC/MS sensitivity and response are stable during every experimental run. The internal standard area count musôâ™bv more than a fac or of 2 (-50% to +100%) from the associated continuing calibrato™ andlrd I t j i t

e T ° n T * o f t h e . " , , e r n a I s t a n d a r d mart not vary more than ±30 seconTfr?mThe associatedI continuing calibration standard. If the area count is outside the (-50% to +100%) range of the associated standard, all ofthe positive results for compounds quanVitatedusine that IS are qualified as estimated, "J", and all non-detects as "UJ", or »R»" if tJiVre is I severe loss of sensitivity. ' mere is a

I f an internal standard retention time varies by more than 30 seconds, the reviewer will use

Lmp^ to determine either partiai °r totai r*cti™ °f srz:rftZ None required qualifications.

9. COMPOUND IDENTIFICATION:

A) Volatile and Semi-Volatile Fractions:

? R C p L ^ 0 m r h

U n d S i . d e n t i f i e d °.n t h e G C / M S by using the analyte's relative retention time RRT) and by comparison to the ion spectra obtained from know£ standards. For theresuTts

to be a Positive hit, the sample peak must be within ± 0.06 RRT units of the standard compound and have an ion spectra which has a ratio of the primary and seconda™ m/e intensities whhin 20% of that in the standard compound. For the^tentativeT-deZiitl compounds (TIC) the ,on spectra must match accurately. In the cases where there is not an adequate ion spectrum match, the laboratory may have provided false positive identifications.

No problems were observed. Qualifier N was applied to all TICs reported for all samples.

ADC2.2717

ATTACHMENT 1 PAGE 6 SOP NO. HW-6

B)" OTHER QC DATA OUT OF SPECIFICATION: ~~ ~ ~

VOA - The following compounds were qualified as estimated "J" in the associated air field duplicate samples because the Relative Percent Difference (RPD) between the sample and field duplicate sample is >50% for air samples:

Compound Matrix % RPD Associated Field Duplicate Samples

No problems were observed.

VOA - The following compounds were qualified as estimated "J" in the indicated samples because the on-column amount of these compounds exceeded the instrument's analytical range as defined by the highest concentration level of the Initial Calibration Sequence:

Fraction Compound(s') Sample(s')

No problems were observed.

10. CONTRACT PROBLEMS NON-COMPLIANCE:

Method TO-15 required using average RRF to calculate the final concentration of a compound detected in the sample analysis. The laboratory used the RRF from continuing calibration standard for sample quantitation. The impact is insignificant because die percent differences between the initial and continuing calibrations were within the control limit. The laboratory results can be used.

11. FIELD DOCUMENTATION:

None

12. OTHER PROBLEMS

As per DataChem, a batch of six canisters will be cleaned on a train. Based on the analytical results of samples collected with these canisters, the dirty one was subjected to analysis to verify the effectiveness of cleaning. The canister analyses showed various analytes were detected at concentrations of less than 1 ppbv and none of those canisters were used for sampling conducted for this site.

13. This package contains re-extractions, reanalyses or dilutions. Upon reviewing the QA results, the following Form l(s) are identified to be used.

None

ADC2.2718 'e-ln Cleaners Site

il 13-14, 2005 Sample #/Concentration [ug/m3]

Matrix: Air Air Air Air Volatiles Client ID#: ADI-AA-EXTI ADI-AA-EXT2 ADI-IA-US ADI-IA-CHRIS Low Concentration Lab ID#: (I5C00444 05C00445 05C00446 05CWI447

Dilution Factor PQL 1.0 1.0 1,0 1.0 Benzene 1.6 0.92 J 0.77 J 0.78 J 1.2 Trichloroethene 2.7 U U U U Toluene 1.9 1.6 J 1.3 J 7.2 11 Tetrachloroethene 3.4 1.2 J U 2.5 J . 2.8

• Ethylbenzene 2.2 U U U U LXylene (para & meta) 4.3 U U U U ; Xylene (Ortho) 2.2 u U • u U

- -, Matrix: Air Air Air Air

• Volatiles i Client ID#: ADI-IA-BARB ADI-IA-BLIMP ADJ-IATHRIFT AD1-IA-TB • Low Concentration j Lab 1D#: 05C00449 O5C0O450 05C0O451 05C00452

\ Dilution Factor PQL 1 1 1 1 ;Benzene • ... 1-6 ' 1.1 J 1.4 J 3.3 U ^Trichloroethene _/ 2.7 ] U U .... ...Y. U : Toluene - -1- -l^.I-i _13_ 27___ 5.9 U Tetrachloroethene : 3.4 j J 1.6 J _ U

j Ethylbenzene •j 2.2 i _ u _ U _ U U j Xylene (para & meta)

L _ 4.3 _ ± u ^2.0 j J _ _ U ^^.(PlJho). 1 ; 2.2 _ [ u 0.55 _ J i 0.76 J U

Air

ADI-IA-CHRIS2i

05C(HM48

1.0

1.2

U

11

2.6

U

U

U

PQL - Practical Quantitation Limit U - non-detected compound B - compound detected in the associated Method or Trip Blank J - estimated value

Project: American Drive-ln Cleaners Site ADC2.2719

Sampling Date: April 13, 2005 Matrix AIR AIR AIR AIR AIR

Field Sample ID ADI-SVW-5 ADI-SVW-4 ADI-SVW-3 ADI-SVW-1 ADI-SVW-2 Lab Sample ID 05C00453 05C00454 05C00455 05C00456 05CO0457

Sample Volume (Liter) 132.24 155.81 120.43 131.52 127.80 Sample Concentration ug/m3 ug/m3 ug/m3 ug/m3 ug/m3

VOLATILES ug/m3

1,1,1-Trichloroethane <76 <64 <83 <76 <78 1,1,2-Tricriloroethane <76 <64 <83 <76 <78 1,1-Dichloroethane <76 <64 <83 <76 <78 1,2,3-Trichloropropane <76 <64 <83 <76 <78 Benzyl chloride <76 <64 <83 <76 <78

: Bromoform "<76 <64 <83 <76 <78 Carbon tetrachloride <76 <64 <83 <76 <78 Chlorobenzene <76 <64 <83 <76 <78 Chlorobromoethane <76 <64 <83 <76 <78

; Chloroform <76 <64 <83 <76 <78 : Ethylene dichloride <76 "<64 <83 <76 <78 ' Hexachloroethane <76 ; " " ' <64 <83 <76 ' <78 ; Tetrachloroethene "<76' 1100 3100 1300 (160) : Trichloroethene <76 : < 6 4 (170) (130) <78 |ds-i,2-Dichiorothene "<76" <64 <83 ^ <76 <78 : o-Dichlorobenzene <76 f < 6 4 " <83 <76 <78 p-Dichlorobenzene <76 ; <64 <83 <76 <78

; trans-1,2-Dichloroethene <76 : < 6 4 " <83 <76 <78 : 1,4-Dioxane <76 ! < 6 4 <83 <76 <78

Matrix: A I R v AIR AIR AIR AIR Field Sample ID ; ADI-SS-1 ADI-SS-2 ADI-SS-3- ADI-SS-4 ADI-INF Lab Sample ID: 05C00458 05C00459 05C00460 05C00461 05C00462

i. Sample Volume (Liter) j 128.70 129.66 128.46 132.54 129.54 Sample Concentration i ug/m3 ug/m3 ug/m3 ug/m3 ug/m3

yOLATILES ug/m3

; 1,1,1-Trichloroethane ! ;i,1,2-Trich|oroethane |

" " <78"" <77 . <78 <75 • <77 ; 1,1,1-Trichloroethane ! ;i,1,2-Trich|oroethane | <78 <77 "<78 <75 <77 [1,1 -Dichloroethane : ' " ~ ' < 7 8 ' " r ' < 7 7 ' ' <78" <75 1 < 7 7 ! 1,2,3-trichloropropane ; <7B " 1 " < 7 7 " " <78 <75 " " < 7 7 (Benzyl chloride ; " < 7 8 " " j ' "<77 <78 " < 7 5 <77" i Bromoform j <78 ; <77 < 7 8 " " <75 <77 [carbon tetrachloride j <78 ' <77 " ' <78 : " < 7 5 ; < 7 7 " ! Chlorobenzene iChiorobromoethane I

<78 <77 <78 ' " " < 7 5 ...... - -! Chlorobenzene iChiorobromoethane I ' " "<78"" " " <77 <78 <75 <77' ' iChloroform "<78 ~: <77 <78 <75 <77 Ethylene dichloride <78 ' <77 <78 <75 <77

: Hexachloroethane " <78 <77 <78 <75 <77 • Tetrachloroethene <78 <77 <78 <75 5300 • Trichloroethene <78 <77 <78 <75 (120) cis-1,2-Dichlorothene < 7 8 " <77 <78 <75 <77

\ o-Dichlorobenzene <78 <77 <78 <75 <77 • p-Dichiorobenzehe <78 "<77 <78 <75 <77 trans-1,2-Dichloroethene "<78 <77 <78 <75 <77 1,4-Dioxane <78 <77 <78 <75 <77

ND - Parameter not detected above LOD ( ) - Parameter between Limit of Detection (LOD) and Limit of Quantitation (LOQ) n/a - denotes not applicable. ** - Result cannot be calculated for samples in ug/m3, air volume missing J - denotes estimated concentration.

irive-ln Cleaners Site

ADC2.2720 , .il 13, 2005

Matrix AIR AIR AIR AIR AIR Field Sample ID ADI-SS-5 ADI-SS-6 ADI-SS-7 ADI-FB ADI-LB Lab Sample ID 05C00463 05C00464 05C00465 05C00466 05C00467

Sample Volume (Liter) 170.19 127.14 129.36 0.00 0.00 Sample Concentration ug/m3 ug/m3 . ug/m3 ug/m 3 ug/m3

VOLATILES 1,1,1-Trichloroethane <59 <79 <77 •* -1,1,2-Trichloroethane <59 <79 <77 1,1-Dichloroethane <59 <79 <77 " •* .. 1,2,3-Trichloropropane <59 <79 <77 ••

: Benzyl chloride <59 <79 <77 : Bromoform <59 <79 <77 Carbon tetrachloride <59 <79 <77 ••

; Chlorobenzene <59 <79 <77 ** ; Chlorobromoethane <59 ; <79 . <77 -\ Chloroform <59 <79" <77 ' ** ** ; Ethylene dichloride "<59" '•" 7 ' <79 " ' "1 <77 «* ; Hexachloroethane < 5 9 " 7 <79 <77""" ; Tetrachloroethene <59~ (170) (170) ** ** ': Trichloroethene <59 <79 <77 ** ] cis-1,2-Dichlorothene < 5 9 ~ " < 7 9 " " t " " " ~ '~ <77 " - ' " " " •• o-DichlorObenzene " ' " < 5 9 . " ! " ' ~<79 T " <7>" : p-Dichlorobenzene <59 <79 f <77 '•• ; trans-i ,2-Dichloroethene <59 <79 : " <77 •* * " " 1,4-Dioxane ' < 5 9 " r < 7 9 \ " <77" **

• ** . ND - Parameter not detected above LOD ( ) - Parameter between Limit of Detection (LOD) and Limit of Quantitation (LOQ) n/a - denotes not applicable. ** - Result cannot be calculated for samples in ug/m3, air volume missing J - denotes estimated concentration.

DATA CHEM LABORATORIES, INC.

ADC2.272]

/•DP o

Case Narrative

Method:

Analysis:

Preparation SOP#:

DCL Set DD #(s):

T015

VOA

m-AN-014

05C-0058-01

Client:

Account #:

Matrix:

CASE#:

Weston Solutions, Inc.

8001

Air

5303

Analysis / Method: Method T015 is an EPA method used in the analysis of air samples for volatile organics by GC/MS, which have been sampled in a silonized canister.

General Set Information: DataChem Laboratories received nine silonized canisters for VOA analysis, the samples were analyzed within fourteen days of sampling. Recoveries of target analytes are reported on the Sample Analysis Data Sheet in units of ppb v/v and ug/m3.

Sample Preparation: This method has no extraction procedure for air samples. The sample preparation date is the same as the date of analysis. Two hundred milliliters of air sample and 100 milliliters of Internal Standard were trapped using an Entech 7100 microscale purge and trap concentrator.

Instrument Calibration: The GC/MS was hardware tuned to meet the criteria for 50 ng of 4-Bromofluorobenzene as specified in the method. This tune check is valid for 24 hours.

Initial and Continuing Calibration Verification: The initial calibration curve, which was analyzed prior to sample analysis, met the specified criteria ofthe method. For the initial calibration curve, the %RSD of the response factors for the TO-15 analytes were checked.

A continuing calibration standard (CCS), which is used for the quantitation of each target compound, was also analyzed prior to sample analysis. The CCS met the criteria as specified in the method. The response factors of the TO-15 analytes were acceptable when compared to the average response from the initial calibration curve.

Method Blank Analysis: A laboratory method blank (BL-230738-1) was prepared using 200 milliliters of humidified ultra high purity nitrogen and 100 milliliters of Internal Standards and analyzed prior to sample analysis. The blank was free of volatile organic contaminants.

960 West LeVoy Drive Salt Lake City, UT 84123 800-356-9135 801-266-7700 Fax:801-268-9992 www.datachem com

1

ADC2.2722 DATA CHEM LABORATORIES, INC.

Data Qualifier Codes: A "J" qualifier indicates that the result is greater than the MDL but less than the PQL. Analytes found in field samples, which also appear in the method blanks are reported with a "B" qualifier in the flag column. The "E" qualifier indicates a reported value above the analytical linear range.

LCS/LCSD: An LCS and LCSD pair (QC-230738-1 & QD-230738-1) was analyzed for the analytical batch. Compounds benzene, trichloroethene, toluene, tetrachloroethene, ethylbenzene, m,p-xylene and o-xylene were analyzed at a concentration of 10 ppb v/v.

Dilutions: None.

NC/CAR:

Miscellaneous Comments: Instrument designation is HP5972-0. Field samples were analyzed using auto sampler positions that were free from volatile contaminants

Sample Calculations: Target Compounds

A x Cfa

Relative Response Factor: RRF = [— 1 [ ] Ab Cx

Where A* is the area of the characteristic ion for the compound to be measured, Ab is the area ofthe characteristic ion for the internal standard , Cb is the concentration ofthe internal standard, and Cx is the concentration of the compound to be measured.

(AxKLJfDf) Concentration in ppb v/v: C= [ ]

(Ab) (RRF) „

Concentration in ug/m3: C = ppb v/v (MW/24.45)

Where I s is the amount of internal standard spiked in ppb, Df is a dilution factor (1 if no dilutions are made), RRF is the relative response factor (assumed to be 1 for non target analytes) and MW is the molecular weight of the compound of interest.

April 22, 2005 Date

960 West LeVoy Drive Salt Lake City, UT 84123 800-356-9135 801-266-7700 Fax:801-268-9992 www.datachem.com

DATA1

CHEM L A B O R A T O R I E S

A Sorenson Company

COVER PAGE

ANALYTICAL REPORT FOR Weston S o l u t i o n s , I n c .

Phone(732) 225-6116 Fax(732) 225-7037 E-mai1 : S . [email protected] . COM

ADC2.2723

04220507533492 Page 1

fflfflliii. G053G01V

DCL Report Group..: 05C-0058-01

Date Printed : 22-APR-05 07:53

Weston Solutions, Inc. At tent ion: Smita Sumbaly 1090 King Georges Post Road, Suite 201 Edison, NJ 08837-3703

Project Protocol #: P996F001 Client Ref Number.: RFP # 5303 PO: 004 Release Number....: 5303

Analysis Method(s): TO-15

C l i e n t Sample Name

Method Blank LCS LCS Dup ADI-AA-EXT1j1 ADI-AA-EXT2 j 1 ADJ-IA-US|108 ADI-IA-CHRISI ADI-IACHRIS2 | ADI-IA-BARB 11 ADI-IA-BLIMPl ADI-IATHRIFT| A D I - I A - T B | 1 0 8

08673- ' / 0 8 8 9 8 / 0 1 0 , / 1 0 8 7 3 0 / 108011 08683-^ .

108869y 698 /

L a b o r a t o r y Date Date Sample Name Sampled Received

BL-230738-1 NA NA QC-230738-1 NA NA QD-230738-1 NA NA 05C00444' 13-APR-05 15-APR-05 05C00445 13-APR-05 15-APR-05 05C00446 13-APR-05 15-APR-05 05C00447 13-APR-05 15-APR-05 05C00448 13-APR-05 15-APR-05 05C00449 13-APR-05 15-APR-05 05C00450 13-APR-05 , 15-APR-Q5 05C00451 13-APR-05 "' 15-APR-05 05C00452 13-APR-05 15-APR-05

I^rb-^up^ervis6t^_Clxpi 's topher Q. Coleman — Date

960 West LeVoy Drive /.Salt Lake City, Utah 84123-2547 Phone (801) 266-7700 Web Page: www.datachem.com FAX (801) 268-9992 E-mail: [email protected] 6

:- 7,: FORM H (TYPE I ) ADC2.2724. = = = SINGLE METHOD ANALYSES Form RLIMS63H-V1.4

04220507533492

CHEM SAMPLE GROUP COMMENTS

l A B O R A T O R I ES A Sorenson Company G053G01V DCL Report Group..: 05C-0058-01

Date P r i n t e d : 22-APR-05 07:53 C l i e n t Name...:Weston S o l u t i o n s , , I n c .

Release Number. . . . : 5303

Sample Group Comments

A n a l y z e d by GC/MS a c c o r d i n g t o method T015.

PQL - P r a c t i c a l Q u a n t i t a t i o n L i m i t - Lowest s t a n d a r d t h a t i s d e t e c t a b l e MDL - Method D e t e c t i o n L i m i t - S t a t i s t i c a l y d e r i v e d v a l u e u s i n g 40 CFR methods.

ug/m> f o r m u l a : ( R e s u l t * MW) / 24.45

G e n e r a l I n f o r m a t i o n

The DCL QC Database m a i n t a i n s a l l n u m e r i c a l f i g u r e s which a r e I n p u t from t h e p e r t i n e n t data s o u r c e . These data have n o t been rounded t o s i g n i f i c a n t f i g u r e s n o r have t h e y been m o i s t u r e c o r r e c t e d R e p o r t s generated f r o m t h e system, however, l i s t data which have been rounded t o t h e number ^ s i g n i f i c a n t f i g u r e s r e q u e s t e d by t h e c l i e n t o r deemed a p p r o p r i a t e f o r t h e method. T h i s mav c r e a t e n u n o r d i s c r e p a n c i e s between data which appear on t h e QC Summary Forms (Forms B-G) and those t h a t would be c a l c u l a t e d from rounded a n a l y t i c a l r e s u l t s . A d d i t i o n a l l y , i f a m o i s t u r e c o r r e c t i o n i s performed d i f f e r e n c e s w i l l be observed between t he QC data and the s u r r o g a t e data r e p o r t e d on Form A (or o t h e r r e p o r t forms) and c o r r e s p o n d i n g data r e p o r t e d on QC Summary Forms. I n these cases, t h e Form A w i l l i n d i c a t e t h e -Report Basis" as w e l l as t h e m o i s t u r e v a l u e used f o r making t h e c o r r e c t i o n R e p o r t g e n e r a t i o n o p t i o n s : IBOX

R e s u l t Svmbol D e f i n i t i o n s

ND - Not Detected above t h e MDL (LLD o r MDC f o r r a d i o c h e m i s t r y ) . ** - No r e s u l t c o u l d be r e p o r t e d , see sample comments f o r d e t a i i s .

Q u a l i f i e r Symbol D e f i n i t i o n s

U B

Not Detected above t h e MDL (LLD o r MDC f o r r a d i o c h e m i s t r y ) For o r g a n i c analyses t h e q u a l i f i e r i n d i c a t e s t h a t t h i s a n a i y t e was fou n d i n t h e method b l a n k For i n o r g a n i c analyses t h e q u a l i f i e r s i g n i f i e s t h e v a l u e i s between t h e MDL and PQL D l a n x -For o r g a n i c analyses t h e q u a l i f i e r i n d i c a t e s t h a t t h e v a l u e i s between t h e MDL and t h e POL I t i s a l s o used f o r i n d i c a t i n g an e s t i m a t e d v a l u e f o r t e n t a t i v e l y i d e n t i f i e d compounds m mass s p e c t r o m e t r y where a 1:1 response i s assumed.

QC F l a g Symbol D e f i n i t i o n s

* - Parameter o u t s i d e o f s p e c i f i e d QC l i m i t s .

960 West LeVoy Drive /'Salt Lake City, Utah 84123-2547' Phone (801) 266-7700 Web Page: www:datachem.com FAX (801) 268-9992 E-mail: [email protected]

DATAip CHEM L ABORATORI ES

A Sorenson Company

FORM A (TYPE I ) SINGLE METHOD ANALYSES

SAMPLE ANALYSIS DATA SHEET

ADC2.2725

form RLIMS63A-V1.4 04220507533492

Page 6

Date Frinted : 22-APR-05 07:53

C l i e n t Name : Weston Solutions, Inc. Cli e n t Ref Number....: RFP # 5303 PO: 0048535 Sampling Site : RFPtf 5303 PO-.0048535 Release Number : 5303

Date Received : 15-APR-05 00:00

DCL Preparation Group: Not Applicable Date Prepared : Not Applicable Preparation Method...: Not Applicable A l i q u o t Weight/Volume: 200 mL Net Weight/Volume. .. . : Not Required

Analytical Results

Client Sample Name DCL Sample Name. . . DCL Report Group..

S053G094

ADI-AA-EXT1|108673 05C00444 05C-0058-01

Matrix : AIR Date Sampled : 13-APR-05 00:00 Reporting Units. . . .- PPB V/V Report Basis : fSAs Received • Dried

DCL Analysis Group Analysis Method. . . Instrument Type. . . Instrument ID. . . .-. Column Type

G053L0OW TO-15 GC/MS VO 5972-0 DB-1 E Primary • Confirmation

A n a l y t e Date

Analyzed MDL Result U n i t s Qual. D i l u t i o n PQL Benzene 18-APR-05 20: 17 0.0939 0.29 PPB V/V J 0.5 Benzene 18-APR-05 20 17 0.30 0.92 ua/m' J 1.6 T r i c h l o r o e t h e n e 18-APR-05 20. 17 0.109 ND PPB V/V 0.5 T r i c h l o r o e t h e n e 18-APR-05 20 17 0. 59 ND ua/m' 2.7 Toluene 18-APR-05 20. 17 0.120 0.43 PPB V/V J 0.5 Toluene 18-APR-05 20 17 0.45 1.6 ua/m' J 1.9 T e t r a c h l o r o e t h e n e 18-APR-05 20. 17 0.117 0.18 PPB V/v J 0.5 i T e t r a c h l o r o e t h e n e 18-APR-05 20- 17 0.79 1.2 ua/mJ J 3.4 Ethylbenzene 18-APR-05 20 17 0.0872 ND PPB V/v 0.5 Ethylbenzene m,p-Xvlene m,p-Xvlene o-Xvlene o-Xylene

18-APR-05 20 18-APR-05 20: 18-APR-05 20 18-APR-05 20: 18-APR-OS 20:

17 17 17 17 17

0.38 0.215 0.93

0.103 0.45

ND ND ND ND ND

ua/m> PPB V/V ua/m' PPB V/V uq/m>

1

2.2 1.0 4.3 0:5 2.2

960 West LeVoy Drive / Salt Phone (801) 266-7700 FAX (801) 268-9992

Lake City, Utah 84123-2547 Web Page: www.datachem.com E-mail: [email protected]

ADC2.2726

CHEM L A B O R A T O R I ES

A Sorenson Company

FORM A (TYPE I )

SINGLE METHOD ANALYSES


Form RLIMS63A-V1.4 04220507533492

Page . 7

Date P r i n t e d : 22-APR-OS 07:53

C l i e n t Name : Weston S o l u t i o n s , I n c .

C l i e n t Ref Number. . . . : RFP # 5303 PO: 0048535

Sampling S i t e . . . : RFP# 5303 PO:0048535 Release Number : 5303

Date Received... : 15-APR-05 00:00

DCL P r e p a r a t i o n Group: Not A p p l i c a b l e

Date Prepared : Not A p p l i c a b l e P r e p a r a t i o n Method. . . : Not A p p l i c a b l e A l i q u o t Weight/Volume: 200 mL Net Weight/Volume... . : Not Required

Analytical Results

C l i e n t Sample Name DCL Sample Name... DCL Report Group..

S053G095

ADI-AA-EXT2|108898 05C00445 05C-0058-01

•L M a t r i x . . : AIR

Date Sampled : 13-APR-05 00:00 R e p o r t i n g U n i t s . . . : PPB V/V

Report Basis : 0 A s Received • D r i e d

DCL A n a l y s i s Group: G053LOOW A n a l y s i s Method... I n s t r u m e n t Type...

I n s t r u m e n t ID Column Type

TO-15 GC/MS VO 5972-0 DB-1 H Primary

• C o n f i r m a t i o n

A n a l y t e Date

Analyzed MDL R e s u l t U n i t s Qual. D i l u t i o n POL Benzene 18-APR-05 21- 39 0.0939 0.24 PPB V/V . J 1 0 5 Benzene 18-APR-05 21: 39 0.30 0.77 uq/m5 J 1 1 6 T r i c h l o r o e t h e n e 18-APR-05 21: 39 0.109 ND PPB V/V 1. 0 5 T r i c h l o r o e t h e n e 18-APR-05 21: 39 0.59 ND ua/m» 1 2 7 Toluene 18-APR-05 21: 39 0.120 0.34 PPB V/V J 1 0 5 Toluene 18-APR-05 21: 39 0.45 1.3 ua/m' J 1 1 q T e t r a c h l o r o e t h e n e 18-APR-05 21: 39 0.117 ND PPB V/V 1 n >; T e t r a c h l o r o e t h e n e 18-APR-05 21: 39 0.79 ND ua/m' ... ,,• * 1 3 4 Ethvlbenzene 18-APR-05 21: 39 0.0872 ND PPB V/V 1 n c Ethvlbenzene 18-APR-05 21: 39 0.38 ND ua/m' 1 •} 9 m.p-Xvlene 18-APR-05 21: 39 0.215 ND PPB V/V 1 1 o m,p-Xylene 18-APR-05 21: 39 0.93 ND ua/m' 1 4 3 o-Xvlene 18-APR-05 21: 39 0.103 ND PPB V/V 1 n o-Xylene 18-APR-05 21: 39 0.45 ND ua/m' 1 2.2

960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 Phone (801) 266-7700 Web Page: www.datachem.com FAX (801) 268-9992 E-mail: [email protected]

ADC2.2727

DATA^P CHEM L A B O R A T O R I E S

A Sorenson Company



form RLIMS63A-V1.4 04220507533492

Page 8

Date Printed .- 22-APR-05 07:53

C l i e n t Name : Weston Solutions, Inc. Cli e n t Ref Number....: RFP # 5303 PO: 0048535 Sampling S i t e : RFP# 5303 PO:0048535 Release Number.......: 5303


DCL Preparation Group: Not Applicable Date Prepared : Not Applicable Preparation Method...: Not Applicable A l i q u o t Weight/Volume: 200 mL Net Weight/Volume....: Not Required

Analytical Results

C l i e n t Sample Name DCL Sample Name... DCL Report Group..

S053G096

ADI-IA-US|108010 05C00446 05C-0058-01

Matrix : AIR Date Sampled : 13-APR-05 00:00 Reporting Units. . . : PPB V/V Report Basis : E)As Received • Dried

DCL Analysis Group: G053L00W Analysis Method... Instrument Type... Instrument ID Column Type

TO-15 GC/MS VO 5972-0 DB-1 E) Primary •• Confirmation

A n a l y t e Date

Analyzed MDL Result U n i t s Qual. D i l u t i o n PQL Benzene 18-APR-05 23:03 0.0939 0.24 PPB V/V J 0.5 Benzene 18-APR-05 23:03 0.30 0.78 uo/m3 J 1.6 T r i c h l o r o e t h e n e 18-APR-05 23:03 0.109 ND PPB v/v 0.5 T r i c h l o r o e t h e n e 18-APR-05 23:03 0.59 ND ua/m' 2.7 Toluene 18-APR-05 23:03 0 .120 1.9 PPB V/V . i 0.5 Toluene 18-APR-05 23:03 0.45 7.2 ua/m' 1.9 PTetrachloroethene 18-APR-05 23:03 0.117 0.37 PPB V/V J 0.5 T e t r a c h l o r o e t h e n e 18-APR-05 23:03 0.79 2.5 Ua/m' J 3.4 Ethvlbenzene 18-APR-05 23:03 0.0872 ND PPB V/V I 0.5 Ethylbenzene 18-APR-05 23:03 0.38 ND ua/m' I 2.2 m.p-Xylene 18-APRr-OS 23:03 0.215 ND PPB V/V 1.0 m.p-Xylene 18-APR-05 23:03 0.93 ND ua/m' 4.3 o-Xvlene 18-APR-05 23:03 0 .103 ND PPB V/V j 0.5 o-Xylene 18-APR-05 23:03 0.45 ND ua/m' 1 2.2

960 West LeVoy Drive / .Salt Lake City, Utah 84123-2547 Phone (801) 266-7700 Web Page: www.datachem.com FAX (801) 268-9992 E-mail: [email protected] u

ADC2.2728


A Sorenson Company



Form RLIMS63A-V1.4 04220507533492

Page 9

Date Printed : 22-APR-05 07:53

C l i e n t Name : Weston Solutions, Inc. C l i e n t Ref Number. . . : RFP # 5303 PO: 0048535 Sampling Site : RFP# 5303 PO:0048535 Release Number : 5303

Date Received : 15-APR-05 00:00 • C l i e n t Sample Name DCL Sample Name... DCL Report Group..

S053G097

ADI-IA-CHRIS|108730 05C00447 05C-0058-01

Matrix : AIR Date Sampled : 13-APR-05 00:00 Reporting Units...: PPB V/V Report Basis. .....: @As Received • Dried

DCL Preparation Group Date Prepared Preparation Method... . Aliq u o t Weight/Volume Net Weight/Volume....

Not Applicable Not Applicable Not Applicable 200 mL Not Required

Analytical Results

DCL Analysis Group Analysis Method... Instrument Type... Instrument ID.. .. Column Type

GO53L0OW TO-15 GC/MS VO 5972-0 DB-1 IS Primary • Confirmation

A n a l y t e Date

Analyzed MDL Res u l t U n i t s Qual. D i l u t i o n . PQL Benzene 19-APR-05 00:27 0.0939 0.37 PPB V/V J 1 0.5 Benzene 19-APR-05 00:27 0.30 1.2 ua/m3 J 1 . 1.6 T r i c h l o r o e t h e n e 19-APR-05 00:27 0.109 ND PPB V/V 1 0.5 T r i c h l o r o e t h e n e 19-APR-05 00:27 0.59 ND ua/m3 1 2 .7 Toluene 19-APR-05 00:27 0.120 3.0 PPB V/V 1 0.5 Toluene 19-APR-05 00:27 0.45 11. ua/m 3 1 1.9 T e t r a c h l o r o e t h e n e 19-APR-05 00:27 0.117 0.41 PPB- V/V J 1 0.5 T e t r a c h l o r o e t h e n e 19-APR-05 00:27 0.79 2.8 ua/m3 J .. - 1- . •.. 3.4 Ethylbenzene 19-APR-05 00:27 0.0872 ND PPB V/V 1 0.5 E t h y l b e n z ene 19-APR-05 00:27 0.38 ND ua/m3 1 2.2 m,p-Xylene 19-APR-05 00:27 0.215 ND PPB V/v 1 1.0 m,p-Xylene 19-APR-05 00:27 0. 93 ND ua/m3 1 ' 4.3 o-Xylene 19-APR-05 00:27 0.103 ND PPB V/V 1 0.5 o-Xylene 19-APR-05 00:27 0.45 ND ua/m3 • 1 2.2

960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 Phone (801) 266-7700 Web Page: www.datachem.com FAX (801) 268-9992 E-mail: [email protected] 29

DATA^P CHEM L ABORATORI ES

A Sorenson Company



ADC2.2729

r u n u K J j l M b b J A - V l . 4 04220507533492

Page 10

S053G098

Date P r i n t e d . : 22-APR-OS 07:53

C l i e n t Name : Weston S o l u t i o n s , I n c .

C l i e n t Ref Number....: RFP « 5303 PO: 0048535 Sampling S i t e : RFPtt 5303 PO:0048535

Release Number : 5303

Date Received :..: 15-APR-05 00:00

DCL P r e p a r a t i o n Group: Not A p p l i c a b l e Date Prepared : Not A p p l i c a b l e P r e p a r a t i o n Method. . . : Not A p p l i c a b l e

A l i q u o t Weight/Volume: 200 mL Net Weight/Volume.. . . : Not Required

Analytical Results

C l i e n t Sample Name: ADI-IACHRIS2|108011

DCL Sample Name...: 05C00448

DCL Report Group..: 05C-0058-01

M a t r i x : AIR

Date Sampled : 13-APR-05 00:00

R e p o r t i n g U n i t s . . . : PPB V/V

Report Basis : E A s Received • D r i e d

DCL A n a l y s i s Group: G053L00W A n a l y s i s Method. .. Ins t r u m e n t Type...

Ins t r u m e n t ID Column Type

TO-15 GC/MS VO 5972-0 DB-1

H Primary


A n a l y t e Date

Analyzed MDL Result U n i t s Qual. : D i l u t i o n PQL Benzene 19-APR-05 01:50 0.0939 0.36 PPB V/V J 1 0.5 Benzene 19-APR-05 01:50 0.30 1.2 uq/m' J 1 1.6 T r i c h l o r o e thene 19-APR-05 01:50 0.109 ND PPB V/V •1'. 0.5 T r i c h l o r o e t h e n e 19-APR-05 01:50 0.59 ND Uq/m' 1 2.7 Toluene 19-APR-05 01:50 0.120 2.8 PPB V/V 1 0.5 Toluene 19-APR-05 01:50 0.45 11. uq/m' 1 1.9 T e t r a c h l o r o e t h e n e 19-APR-05 01:50 0.117 0.38 PPB V/V J 1 0.5 Te t r a c h 1 o r o e thene 19-APR-05 01:50 0.79 2.6 uq/m' J 1 3.4 Ethvlbenzene 19-APR-05 01:50 0.0872 ND PPB V/V 1 0.5 Ethvlbenzene 19-APR-05 01:50 0.38 ND uq/m' 1 2.2 m,p-Xvlene 19-APR-05 01:50 0.21S ND PPB V/V 1 1.0 m,p-Xylene 19-APR-05 01:50 0.93 ND UQ/m' 1 4.3 o-XVlene 19-APR-05 01:50 0.103 ND PPB V/V : 1 0.5 o-Xvlene 19-APR-05 01:SO 0.45 ND Uq/m' 1 2.2


ADC2.2730


A Sorenson Company

FORM A (TYPE I )

SINGLE METHOD ANALYSES


Date P r i n t e d : 22-APR-OS 07:53

C l i e n t Name : Weston S o l u t i o n s , I n c . C l i e n t Ref Number....: RFP # 5303 PO: 0048535

Sampling S i t e : RFP# 5303 PO:0048535 Release Number : 5303

Date Received. . : 15-APR-05 00:00

C l i e n t Sample Name

DCL Sample Name...

DCL Report. Group. .

Form RLIMS63A-V1.4 04220507533492

Page 11

M a t r i x

Date Sampled....

R e p o r t i n g U n i t s .

Report B a s i s . . . .

ADI-IA-BARB|108683 05C00449

05C-0058-01

AIR

13-APR-05 00:00 PPB V/V

IS As Received • D r i e d

DCL P r e p a r a t i o n Group: Not A p p l i c a b l e Date Prepared : Not A p p l i c a b l e P r e p a r a t i o n Method...: Not A p p l i c a b l e A l i q u o t Weight/Volume: 200 mL Net Weight/Volume....: Not Required

Analytical Results

DCL A n a l y s i s Group A n a l y s i s Method... I n s t r u m e n t Type...

I n s t r u m e n t ID Column Type

G053L00W TO-15 GC/MS VO 5972-0 DB-1 (3 P r i m a r y


A n a l y t e Benzene

Date Analyzed MDL

0.0939 R e s u l t U n i t s Qual. D i l u t i o n PQL

0.5 Benzene T r i c h l o r o e t h e n e T r i c h l o r o e t h e n e Toluene

19-APR-05 03:13 19-APR-OS 03:13

0.35 0.30

19-APR-05 03:13 1.1

PPB V/V

0.109 19-APR-05 19-APR-05

ND uq/m'

03:13 03:13 03 :13

0.59 0.120

PPB V/V ND 3.5

uq/m' PPB V/V

1.6 0.5

0.5 1.9 T e t r a c h l o r o e t h e n e

T e t r a c h l o r o e t h e n e

19-APR-05 0.45 19-APR-05 19-APR-05

03 :13 03 :13

13. 0.117 0.17 0.79

0.0872 1.1

PPB V/V uq/m3

0.5

Ethvlbenzene Ethylbenzene

19-APR-05 19-APR-OS

03:13 03:13

ND PPB V/V 3.4 0.5

m.p-Xvlene m,p-Xvlene o-Xvlene

0. 38 19-APR-OS 03:13 19-APR-05 03:13

ND 0.215 ND

Uq/m'

0.93 0.103

PPB V/V ND Uq/m'

2.2 1.0

o-Xylene 19-APR-05 19-APR-05

03.13 ND 03:13 0.4S

PPB V/V ND uq/m'

4.3 0.5

960 West LeVoy Drive" / Salt Lake City, Utah 84123-2547

l ^ ^ n ^ l ^ L l l 0 0 W e b P a 9 e : www.datachem.com FAX (801) 268-9992 E-mail: [email protected]

39

ADC2.2731

DATA^P CHEM L A BORATORI ES

A Sorenson Company



Form RLIMS63A-V1.4 04220507533492

Page. 12

Date Printed : 22-APR-OS 07:53

C l i e n t Name : Weston Solutions, Inc. Cl i e n t Ref Number. . . . •. RFP # 5303 PO: 0048535 Sampling Site : RFP# 5303 PO:0.048535 Release Number.......: 5303


DCL Preparation Group: Not Applicable Date Prepared : Not Applicable Preparation Method. . . -. Not Applicable Aliquot Weight/Volume: 200 mL Net Weight/Volume....: Not Required

Analytical Results

Client Sample Name DCL Sample Name... DCL Report Group. .

S053G09B

ADI-IA-BLIMP110 8 671 05C00450 OSC-0058-01

Matrix : AIR Date Sampled : 13-APR-05 00:00 Reporting Units. . . : PPB V/V Report Basis : OAs Received • Dried

DCL Analysis Group: G053L00W Analysis Method. . . Instrument Type. . . Instrument ID Column Type

TO-15 GC/MS VO 5972-0 DB-1 0 Primary • Confirmation

Analyte Date

Analyzed MDL R e s u l t Units Qual. D i l u t i o n PQL Benzene 19-APR-05 04:36 0.0939 0.42 PPB V/V J 1 ' 0.5 Benzene 19-APR-05 04:36 0.30 1.4 ua/m3 J 1 1.6 Trichloroethene 19-APR-05 04:36 0.109 ND PPB V/V 1 0.5 Trichloroethene 19-APR-05 04:36 0.59 ND uq/m3 1 2.7 Toluene 19-APR-OS 04:36 0.120 7.2 PPB V/V 1 O.S [Toluene 19-APR-05 04:36 0.45 27. uq/m3 • .•• 1 1.9 [Tetrachloroethene 19-APR-05 04:36 0.117 0.24 PPB V/V J 1 0.5 Tetrachloroethene 19-APR-05 04:36 0.79 1.6 uq/m3 J 1 3.4 Ethvlbenzene 19-.APR-05 04:36 0.0872 ND PPB V/V 1 0.5 Ethvlbenzene 19-APR-OS 04:36 0.38 ND uq/m> 1 2.2 m,p-Xvlene 19-APR-05 04:36 0.215 0.47 PPB V/V J 1 1.0 m,p-Xylene 19-APR-05 04:36 0.93 2.0 uq/m3 J 1 4.3 o-Xvlene 19-APR-OS 04:36 0.103 0.13 PPB V/V J 1 0.5 o-Xylene 19-APR-05 04:36 0.45 0.55 pg/m3 J 1 2.2

960 West LeVoy Drive /Salt Lake City, Utah 84123-2547 Phone (801) 266-7700 Web Page: www.datachem.com FAX (801) 268-9992 E-mail: [email protected]

ADC2.2732 .

CHEM L A 8 0 R A T 0 R I E S

A Sorenson Company



Form RLIMS63A-V1.4 04220507533492

Page 13

Date Printed : 22-APR-05 07:53 .

Cl i e n t Name : Weston Solutions, Inc. C l i e n t Ref Number....: RFP * 5303 PO: 0048535 Sampling Si t e : RFP# 5303 PO: 0048535 Release Number : 5303

Date Received . : 15-APR-05 00:00

DCL Preparation Group: Not Applicable Date Prepared : Not Applicable Preparation Method.. . : Not Applicable A l i q u o t Weight/Volume: 200 mL Net Weight/Volume....: Not Required

Client Sample Name DCL Sample Name. . . DCL Report Group..

S053G09C

ADI-IATHRIFT|108869 05C00451 05C-0058-01

Matrix .....: AIR Date Sampled : 13-APR-0.5 00:00 Reporting Units. . . : PPB V/V Report Basis : E)As Received • Dried

DCL Analysis Group: G053L00W Analysis Method. Instrument Type. Instrument ID... Column Type

Analytical Results

TO-15 GC/MS VO 5972-0 DB-1 HPrimary • Confirmation

Analyte Date

Analyzed MDL Result Units Qual. D i l u t i o n PQL Benzene 19-APR-OS 06:04 0.0939 1.0 PPB V/V 1 0.5 Benzene 19-APR-05 06:04 0.30 3.3 ua/m' 1 1.6 Trichloroethene 19-APR-05 06:04 0.109 • ND PPB. V/V 1 0.5 Trichloroethene 19-APR-05 06:04 0.59 ND ua/m' 1 2.7 Toluene 19-APR-05 06:04 0.120 1.6 PPB V/V 1 0.5 Toluene 19-APR-05 06:04 0.45 5.9 ua/m' 1 1.9 Tetrachloroethene 19-APR-05 06:04 0.117 .ND PPB V/V .. 1 0.5 Tetrachloroethene 19-APR-05 06:04 0.79 ND ua/m' 1 3.4 Ethvlbenzene 19-APR-05 06:04 0.0872 ND PPB V/V 1 0.5 Ethvlbenzene 19-APR-05 06:04 0.38 ND ua/m' 1 2.2 m.p-Xvlene 19-APR-05 06:04 0.215 0.38 PPB V/v J 1 .1.0 m,p-Xylene 19-APR-05 06:04 0.93 1.7 ua/m' J 1 4.3 o-Xvlene 19-APR-OS 06:04 0.103 0.17 PPB V/V J 1 0.5 o-Xvlene 19-APR-05 06:04 0.45 0.76 ua/m' J 1 2.2


ADC2.2733

DATA1

CHEM - A B O R A T O R I ES

A Sorenson Company



Form RLIMS63A-V1.4 04220507533492

Page 14

Date P r i n t e d : 22-APR-05 07:53

C l i e n t Name : Weston S o l u t i o n s , I n c . C l i e n t Ref N u m b e r . . . . : RFP # 5303 PO: 0048535 S a m p l i n g S i t e . : RFPtt 5303 PO:004853S Release Number : 5303

Date Rece ived : 15-APR-OS 00:00

C l i e n t Sample Name DCL Sample Name. . . DCL Report G r o u p . .

S053G09D

ADI-IA-TB|108698 05C00452

05C-0058-01

M a t r i x : AIR

Date Sampled : 13-APR-05 00:00 Reporting U n i t s . . . : PPB V/V

Report Basis : |XjAs Received • Dri e d

DCL P r e p a r a t i o n Group: Not A p p l i c a b l e Date Prepared : Not A p p l i c a b l e

P r e p a r a t i o n Method...: Not A p p l i c a b l e A l i q u o t Weight/Volume: 200 mL Net Weight/Volume. . . . : Not Required

Analytical Results

DCL A n a l y s i s Group: G053LOOW An a l y s i s Method.. Instrument Type.. Instrument ID. Column Type...

TO-15 GC/MS VO 5972-0 DB-1 H Primary

O C o n f i r m a t i o n

A n a l y t e

Benzene Benzene T r i c h l o r o e t h e n e T r i c h l o r o e t h e n e Toluene

T,

.Toluene e t r a c h l o r o e t h e n e

T e t r a c h l o r o e t h e n e

Date Analyzed-

19-APR-05 07:26 19-APR-OS 07:26 19-APR-05 07-. 26 19-APR-OS 07:26 19-APR-05 19-APR-05

07:26 07:26

19-APR-OS 19-APR-OS

07:26

MDL 0.0939 0.30

0 .109 0.59

0.120 0.45

0.117

Result ND ND ND ND ND ND ND

U n i t s

PPB V/V ug/m3. PPB V/V uq/m3

PPB V/V vq/" 3

PPB V/V

Qual. D i l u t i o n PQL 0.5 1.6 0.5 2.7 0.5 1.9

07:26 07:26

0.79. .ND uq/m' Ethvlbenzene Ethvlbenzene

19-APR-OS 19-APR-05

0.0872 ND PPB V/V 07:26 07:26

0. 38 ND Uq/m3

m,p-Xvlene m.p-Xylene o-Xvlene o-Xvlene

19-APR-OS 0.215 19-APR-05 07:26

ND

19-APR-05 07:26 0.93

PPB V/V ND

19-APR-05 07:26 0.103 ND

pq/m3

0.45 PPB V/V

ND Uq/m3

1.0 4.3 0.5 2.2

960 West LeVoy Drive / Salt Lake City, Utah 8*123-2547

ADC2.2734 CHAIN OF CUSTODY RECORD

RFP No.:

5303

PONo.:

0048535 Restoring Resource Efficiency

Removal Support Team EPA CONTRACT 68-W-00-113

Phone (732)225-6116 Fax: 732-225-7037

Matrix Box No.: Preservative Box No.:

1. Surface 2. Ground Waler 3.1 «trhatc A. Rinsate 5. Soil/Sediment 6 . Oil 7. Waste 8. Air

1. HCI 2. HN03 ^ 3. Na2S04 4. H2S04 ™ 5. Other (Specify) 6. Ice Only N. Not Preserved

Page 1 of3

Send verbal and written results to: Weston Solutions, Inc. Suite 201,1090 King Georges Post Road, Edison, New Jersey 08837-3703 Attention: Smita Sumbaly, RST Analytical Coordinator

SUMMA t t a l x r

QErferBoocI) 4/13/05-4/14/05 Tdal Orifx*

ID kAnl Cmima h a m

108673 ADI-AA-EXT 1 8 1012 -1012 24 hr 108932 >30/1.5 TO-15

108898 ADI-AA-EXT2 8 1014 - 1014 24 hr 108850 >30/6 TO-15

108010 ADI-IA-US 8 1018-1018 24.hr 108772 >30/10 TO-15

108730 ADI-IA-CHRIS 8 1024 -1024 24 hr 108878 29/0 TO-15

108011 ADI-IA-CHRIS2 8 1024 - 1024 24 hr 108616 30/1 TO-15

108683 ADI-IA-BARB 8 1031 - 1031 24 hr 108663 >30 / 0 TO-15 ^

108671 ADI-IA-BLIMP &> 8 1035 - 1035 24 hr 108935 >30/8 TO-15

108869 ADI-IA-THRIFT 'Cf\ 8 1040 - 1040 24 hr 108919 30/0 TO-15

108698 ADI-IA-TB o 8 NA NA NA NA TO-15

Comments: Report Only BTEX, PCE, TCE MDL < lug/m3 TAT= 1 week verbal, 2 weeks written

Person Assuming Responsibility for Samples: / \ ^ Time/Date

Sample Number Relinquished By: Time

lu<5

Date

H, Received By: Reason for Change of

Custody

Sample Number Relinquished By: Time Date

i f f . Recerved By: Reason for Change of

Custody

Sample Number Relinquished By: Time Date Received By: Reason for Change of Custody

Weston Solutions, Inc. FEDERAL PROGRAMS DIVISION In Association with Scientific and Environmental Associates, Inc., Resource Applications, Inc., and Innovative Technical Solutions, Inc.

2 CHEM 'LABORATORIES, INC

ADC2.2735

Case Narrative SDG* 5303 DCL RE: O5C-0OS8-02 Gas Chromatography

SUBMITTED TO:

SUBMITTED BY:

Analysis of:

Sample Type:

Sample(s): 15

Smita Sumbaly Weston Solutions Inc. 1090 King Georges Post Road, Suite 201 Edison, NJ 08837-3703

Young Hee Yoon

1,1,1-Trichloroethane, 1,1,2-Trichloroethane, 1,1-Dichloroethane, 1,2,3-Trichloropropane, Benzyl Chloride, Bromoform, Carbon t e t r a c h l o r i d e , Chlorobenzene, Chiorobromomethane, Chloroform, Ethylene D i c h l o r i d e , Hexachloroethane, Tetrachloroethene, Trichloroethene, cis-1,2-Dichloroethene, o-Dichlorobenzene, p-Dichlorobenzene, trans-1,2-Dichloroethene,

Charcoal Tube( coconut base, Lot# 11108, G i i l i a n Instrument Corp,. Cat # 10225)

Analyses: 270

DataChem Laboratory Nos.: 05C00453 through 05C00467

The above numbered charcoal tube sample was analyzed by gas chromatography according t o NMAM 4th e d i t i o n method 1003 with m o d i f i c a t i o n s i d e n t i f i e d with an a s t e r i s k (*).

Desorption Process;

Gas Chromatograph:

Column:*

Oven Condi t ion:*

30 minutes i n . 1 . 0 mL o f carbon d i s u l f i d e .

Hewlett-Packard Model 5890A equipped w i t h a flame i o n i z a t i o n d e t e c t o r .

30m x 0.32mm fused s i l i c a c a p i l l a r y coated i n t e r n a l l y w i t h 1.0 um of DB-5ms

4 0°C f o r 7 minutes, up t o 60°C f o r 8 minutes at a ra te of 5°C per minute , then up to 95°C f o r 1 minutes at a r a t e of 10°C per minute, and then up to 140°C f o r 1.5 minutes at a ra te of 25°C per minute.

Media standards were used f o r the ana lys i s .

960 West LeVoy Drive • Salt Lake City, UT 84123 • 800-356-9135 • 801-266-7700 • Fax:801-268-9992 • wvvw.datacl

ADC2.2736

The LOD i s 0.010 mg/sample and LOQ i s 0.030 mg/sample f o r each analyt<

The reported values have not been f i e l d blank corrected.

The r e s u l t s are tabulated on the f o l l o w i n g page(s).

Yourrg Hee Yoofi

110

DATAip CHEM L A B O R A T O R I ES

A Sorenson Company

ANALYTICAL REPORT

ADC2.2737 Form Page i ot 11 Part 1 of 5 O4220510250O05X

Date Laboratory Group Name 05C-005ft-o? Account No. 08001

Weston Solutions, Inc. Attention: Smita Sumbaly 1090 King Georges Post Road, Suite 201 Edison, NJ 08837-3703

FAX (737) 7^.70^7 Telephone (732)

E-mail S. SI 1MB A T. YPVJESTONSnn TT T ONS rnq

Sampling Collection and Shipment

Sampling Site RFPf 5303 PO;004fl'i3'. Date of Collection April 13, 9n0^

Analysis

Date Samples Received at Laboratory April 15, 7005

Method of Analysis NTOSH 1QQ3

Date(s) of Analysis Apri 1 71, ?no5

Analytical Results

F i e l d S a m p l e Number

L a b o r a t o r y Number

Sample Type

1,1

,1-T

ri

ch

loro

eth

an

e

mg

/sa

mp

le

1,1

,2-T

r ic

hlo

ro

eth

an

e

mg

/sam

ple

1,1

-D

ich

loro

eth

an

e

mg

/sa

mp

le

1,2

,3

-T

rl

ch

loro

pro

pa

ne

mg

/sa

mp

le

Be

nz

yl

Ch

lori

de

mg

/sa

mp

le

Bro

mo

form

m

g/s

am

ple

Ca

rbo

n

Te

tra

eh

lorid

a

Tig

/sam

ple

• c • M c • C H

Xt Ol O E M a O a H \ a o> t » (S A D I - S V W - 5 05C00453 TUBE ND ND ND ND ND ND ND ND

A D I - S V W - 4 0SC00454 TUBE ND KD ND ND ND ND ND ND A D I - S V W - 3 0SC0O455 TUBE ND ND ND ND ND ND ND ND A D I - S V W - 1 05C00456 TUBE ND ND ND ND ND ND ND ND A D I - S V W - 2 05C00457 TUBE ND ND ND ND ND HD ND ND A D I - S S - 1 0 5 0 0 0 4 5 6 TUBE ND ND ND ND ND ND ND ND ' & D I - S S - 2 0SC00459 TUBE ND ND ND ~vr

ND ND ND ND ND A D I - S S - 3 OSC00460 TUBE ND ND ND ND ND ND ND ND A D I - S S - 4 0 5 C 0 0 4 6 1 TUBE ND ND ND ND ND ND ND ND A D I — I N F 0SC004S2 TUBE ND ND ND ND ND ND ND ND A D I - S S - 5 0SC00463 TUBB ND ND ND ND ND ND ND ND A D I - S S - 6 05C00464 TUBE ND ND ND ND ND ND ND ND A D I - S S - 7 05C00465 TUBE

Daae .

ND ND * * c

ND ND ND ND ND ND

ND Parameter not detected above NR Parameter not requested. NA Parameter not applicable.

LOD. page. ( ) Parameter-between LOD and LOQ.

Analyst: x^ung Hee Toon "

Beviever: vicki Hoe-Lin Tsai

960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 ^ ( S O ? ? 1

6 86 OQQ7°° S e b ^ 'ww.daUohemtoom FAX (801) 268-9992 E-mail: [email protected] 111

ADC2.2738 ANALYTICAL REPORT

A Sorenson Company

Analyt ica l Results Laboratory Group Name OSC-POSR-p?

F i e l d Sample Number

ADI—FB

ADI—LB


05C00466

05C00467

Sampl Type

TUBE

TUBE

L i m i t o f D e t e c t i o n

L i m i t o f Q u a n t i t a t i o n

• B a

•H XS V

H • a I 0 E

H u n - o n -JB Ol

H O E

ND

ND

0.010

0 . 0 3 0

O u o

H XS O

- » c u H H ft I • E

«x B a - M B

H J S V . . - J J Oi

H U E

ND

ND

0.010

0 . 0 3 0

O M o

H e J B H 0 ft

• 6 D e e 1 « a

H J ! \ — JJ Oi

H O E

ND

ND

0.010

0 . 0 3 0

• B K a

~> o « U U H H ftft I O E

<n n o -O • N H S

-JS O I H O E

ND

ND

0.010

0 . 0 3 0

•o

JC • O H

ft H E S-i« N a c \ e tr>

w E

ND

ND

0.010

0 . 0 3 0

E c W H o ft « E O « E • 0 \ U Ol

W E

ND ND

0.010

0.030

JJ • O t l O H

•O O, E H E o u a .0 o • M H \ • JB Oi Q U E

ND

ND

0 .010

0 . 0 3 0

• N B « « H

j j a o E M « o «

H-v XS Oi

O E

ND

ND

0 .010

0 . 0 3 0

t See comment on l a s t page . ND Parameter no t d e t e c t e d above LOD. NR Parameter no t r e q u e s t e d . NA Parameter no t a p p l i c a b l e .

** See comment on l a s t page. ( ) Parameter between LOD. and LOQ.

960 West LeVoy Drive / S a l t Lake Ci ty , Utah 84123-2547 ™ Yf t t f ? 1 A« 6oooo 7 0 0 W e b Page: www.datachem.com FAX (801) 268-9992 E-mail: [email protected] 112

DATA» CHEM L A B O R A T O R I E S

A S o r e n s o n Company

ANALYTICAL REPORT

Date

Form i Page 3 Part 2 of O422O51025OO05X

ADC2.2739

of 11 5

Laboratory Group Name 05C-005B-09 Account No. 08001


Sampling Collection and Shipment Sampling Site RFP« 5303 PO:0048535

FAX (732) 225-7037 Telephone (73?,- 775-6116

E-mail s .siiMRAi.YPWF.STnN.snr.irTTONs cm

Date of Collection April 13, 7005


Analysis Method of Analysis NTOSH 1003

Date(s) of Analysis April 71, 7005

Analytical Results



Sample Type

« c a XS • ' •Urt e a

o E E u o a 0 E a H o \ XS H o> OJO E C

hlo

ro

for

m

mg

/sa

mp

le

Eth

yle

ne

Dlc

hlo

r i

de

mg

/sa

mp

le.

Ha

xa

ch

lor

o

eth

an

e

mg

/sa

mp

le

Te

tra

ch

lor

o

eth

an

e

mg

/sa

mp

le

• c •

XS i t • o • O Oi rt E xs a 0 a M DI H E C

ls-l,2

-D

ic

hl

oro

eth

en

e

mg

/sa

mp

le o

M c 0 rt rt • ft xstsu u • a rt H a Q C \ 1 • e> OJ3 E

A D I - S V W - 5 OSC00453 TUBE ND ND ND ND ND ND ND ND A D I - S V W - 4 0SC00454 TUBE ND ND ND ND 0 . 1 7 ND ND ND A D I - S V W - 3 0SC0045S TUBE ND ND ND ND 0 . 3 7 ( 0 . 0 2 1 ) ND ND

A D I - S V W - 1 0SC004SS TUBE ND ND ND ND 0 . 1 7 ( 0 . 0 1 7 ) ND ND

A D I - S V W - 2 0SC004S7 TUBE ND ND ND ND ( 0 . 0 2 1 ) ND HD ND

A D I - S S - 1 0SC00458 TUBE ND ND ND ND ND ND ND ND A O I - S S - 2 OSC00459 TUBE ND ND ND ND ND ND ND ND A D I - S S - 3 OSC00460 TUBE ND ND ND ND ND ND ND ND A D I - S S - 4 05C00461 TUBE ND ND ND ND ND ND ND ND ADI—INF 05C00462 TUBE ND ND ND ND 0 . 6 9 ( 0 . 0 1 S ) ND ND

A D I - S S - 5 0SC00463 TUBB ND ND ND ND ND ND ND ND A D I - S S - 6 05C00464 TUBE ND ND ND ND ( 0 . 0 2 1 ) ND ND ND A D I - S S - 7

* 05C00465

— i - i _ _ .

TUBE ND ND ND ND ( 0 . 0 2 2 ) ND ND ND

ND Parameter not detected above LOD. NR Parameter not requested. NA Parameter not applicable.

( ) Parameter between LOD and LOQ.



CHEM I A B O R A T O R I E S

A Sorenson Company

Analytical Results

Form ARF-BL Page 4 of 11 Part 2 of 5 04220510250005X

Date Laboratory Group Name 05C-0058-n7



Sample Type

Ch

loro

br

om

om

eth

an

e m

g/s

am

ple

Ch

lor

ofo

rm

m

g/s

am

ple

Eth

yle

ne

Dic

hlo

rid

e

mg

/sa

mp

la

He

xa

ch

lor

o

eth

an

e

mg

/sa

mp

la

Te

tra

ch

lor

o

eth

an

e

mg

/sa

mp

le

• c a

JC V

. a o • UH o Oi w E jz a 0 a -<\ u ni H E

H JB U —< D M 1 C H

M e a, -JS E

H i l « I t> a a 0 \

H M Ot D O E

0 n a O H

H e o. JS c E o a a

H H a 0 c \ 1 • Ol O JD E ADI—FB 0 5 C 0 0 4 6 6 TUBE ND ND ND ND ND ND ND ND

ADI—LB 0 S C 0 0 4 6 7 TUBE ND ND ND ND ND ND ND ND L i m i t o f D e t e c t i o n 0 . 0 1 0 0 . 0 1 0 0 . 0 1 0 0 . 0 1 0 0 . 0 1 0 0 . 0 1 0 0 . 0 1 0 0 . 0 1 0 L i m i t o f Qua n t i t a t i o n 0 . 0 3 0 0 . 0 3 0 0 . 0 3 0 0 . 0 3 0 0 . 0 3 0 0 . 0 3 0 0 . 0 3 0 0 . 0 3 0

-




DATA^P CHEM L A B O R A T O R I ES


ANALYTICAL REPORT Form ADC2.2741 Page

Part 3 of 5 O422051O25O005X

(

Date : _ Laboratory Group Name 05C-005R-0? Account No. 08001


FAX (737) 775-7037 Telephone (737) 775-ftnf

E-mail S.SUMBAI.YPWF..NTON.NnT TfTTONft POM

Sampling Collection and Shipment Sampling Site RFP* 5303 PD:0048535 Date of Collection April 13, 7npc



Date(s) of Analysis Apri 1 71, 7005

Analytical Results



Sample T y p e

p—

Dic

hlo

ro

be

nz

en

e m

g/s

am

pla

tra

ns-1

,2-D

I ch

loro

eth

an

e

mg

/sa

mp

le

1,1

,1-T

ri

ch

lor

oe

tha

ne

ug

/m3

1,1

,2—

Tr

ich

loro

eth

an

e

ug

/m3

o u 0

- rt JC u rt O Q c m 1 « E

rt J S \ rt a a

1,2

,3-T

ri

ch

loro

pro

pa

ne

ug

/m3

Be

nz

yl

Ch

lorid

e

ug

/m 3

e u o >VI Om 6 E o \ H Ol n a A D I - S V W - 5 0SC004S3 TUBB ND ND <76. <76. <76 . < 7 6 . <76. <76.

A D I - S V W - 4 0SC004S4 TUBB ND ND <64. <64. <64 . < 6 4 . <64. <64. A D I - S V W - 3 0SCO04SS TUBB ND ND <83. <83 . < 8 3 . < 8 3 . <83 . <83 . A D I - S V W - 1 0SC004SS TUBB ND ND <76. <7fi . <76 . <76 . <76. <7S . A D I - S V W - 2 OSC00457 TUBE ND ND <76 . <78 . < 7 8 . < 7 8 . <78 . <78. A D I - S S - 1 05C00458 TUBB ND ND <76. <78 . < 7 8 . < 7 8 . <78 . <78. A D I - S S - 2 05C00459 TUBE ND ND <77. <77 . < 7 7 . < 7 7 . <77. <77. A D I - S S - 3 O5CO046O TUBB ND ND <78. <76. < 7 8 . < 7 8 . <78. <78. A D I - S S - 4 0SC00461 TUBE ND ND <7S . <7S . < 7 S . < 7 S . <7S. <7S. ADI—INF 05C00462 TUBB ND ND <77. <77 . < 7 7 . <77 . <77. <77. A D I - S S - 5 05C00463 TUBB ND ND <59 . <S9 . < 5 9 . < 5 9 . <S9. <S9 . A D I - S S - e 0SCOO464 TUBE ND ND <79 . <79 . < 7 9 . < 7 9 . <79. <79. A D I - S S - 7 0SC0046S TUBE ND ND <77 . <77 . < 7 7 . < 7 7 . <77. <77.

T s e e comment on l a s t p a g e . ND P a r a m e t e r n o t d e t e c t e d above LOD. NR P a r a m e t e r not r e q u e s t e d . NA P a r a m e t e r not a p p l i c a b l e .

* * See comment on l a s t p a g e . ( ) P a r a m e t e r between LOD and LOQ.

960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 ^ v n ? o i ? 0 1 L c ; 6 6 - 7 7 0 0 W e b P a e e : www.datachem.com FAX (801) 268-99.92 E-mail: [email protected] 115

ADC2.2742 -

CHEM ANALYTICAL REPORT

Form ARF-BL Page 6 of Part 3 of 04220510250005X

11 5

L A B O R A T O R I E S A S o r e n s o n Company

Analytical Results

Date ; Laboratory Group Name OSC-OOSR-O?

F i e l d Bample Number


Sample Type

O u • 0 rt rt • Oa JC B E U • • rt N a

a c \ 1 e tri (VD E

rt t> a B

i • OIJC C

- J J r t rt • a 1 O E • U ( B O B « H \ M JC Ol *> O E

1,1

,1-T

ri

ch

loro

eth

an

e

ug

/m3

0 u 0 rt XS u

• H

u 1 •

W 6<-l » • E rtJ3\

» JJ Oi rt C 9

O M O rt

U -< e a Cm 1 1 E

H J 3 \ »4J Ol

- l e g 1,2

,3

-T

rl

ch

loro

pro

pa

ne

ug

/m3

• •o M O rt XS

o rt

>*<•> N E B \ • Bi B) 3

E u O

VI o n E E 0 \ H oi |Q g

ADI—FB 0 S C 0 0 4 6 6 TUBE ND ND ** ** ** * * ** »* A D I - L B 0 5 C 0 0 4 6 7 TUBB ND ND * * • * ** *« ** ** L i m i t o f D e t e c t i o n 0 . 0 1 0 0 . 0 1 0

L i m i t o f Qua n t i t a t i o n 0 . 0 3 0 0 . 0 3 0

t See comment on l a s t page. ND Parameter not detected above LOD. NR Parameter not requested. NA Parameter not applicable.

** See comment on l a s t page. ( ) Parameter between LOD and LOQ.

960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 r ^ " ^ 8 0 1 ^ 6 6 - 7 7 0 0 W e b P a 6 e : www.datachem.com FAX (801) 268-9992 E-mail: [email protected] 116

DATA^P CHEM L A B O R A T O R I ES


ANALYTICAL REPORT

Date

ADC2.2743 Form Page 7 of 11 Part 4 of 5 O422O51025OO05X

Laboratory Group Name 05(1-0058-0? Account No. 08001 ;


FAX (73?) 775-7037 Telephone .73?,- 775-6116

E-mail S. SlIrffiALYPWESTONSOI .1 ITT ONS. COM

Sampling Collection and Shipment Sampling Site RFP* 5303 P0:0048535 Date of Collection April 13, 7005




Analytical Results



Sample T y p e

Ca

rbo

n

Te

tra

ch

lorid

e

ug

/m3

• c • N c c XI o u <n O E H S xs en O 3

• ss eg XS it «

O E M o<n o E E

H O N xs u en y JO 3

Ch

loro

form

u

g/m

3

Eth

yle

ne

Dic

hlo

rid

e

ug

/m3

Hex

ach

loro

e

tha

ne

ug

/m3

Ta

tra

ch

loro

e

the

ne

ug

/m3

Tric

hlo

ro

eth

en

e

ug

/m3

A D I - S V W - 5 05C004S3 TUBE < 7 6 . < 7 6 . < 7 6 . < 7 6 . < 7 6 . < 7 6 . < 7 « . < 7 6 .

A D I - S V W - 4 0SC00454 TUBE < 6 4 . < 6 4 . < 6 4 . < 6 4 . < 6 4 . < 6 4 . 1100 < 6 4 .

A D I - S V W - 3 05C004S5 TUBE < 8 3 . < 8 3 . < 8 3 . < 8 3 . < 8 3 . < 8 3 . 3100 ( 1 7 0 )

A D I - S V W - 1 0SC00456 TUBE < 7 6 . <76 . < 7 6 . < 7 6 . < 7 6 . < 7 6 . 1300 ( 1 3 0 )

A D I - S V W - 2 0SC00457 TUBE < 7 8 . < 7 8 . < 7 8 . <7 8 . < 7 8 . < 7 6 . ( I S O ) < 7 6 .

A O I - S S - 1 05C00458 TUBE < 7 8 . < 7 8 . < 7 6 . < 7 8 . < 7 8 . < 7 f l . < 7 8 . < 7 8 .

A D I - S S - 2 05C004S9 TUBE < 7 7 . < 7 7 . < 7 7 . <7f". < 7 7 . < 7 7 . < 7 7 . < 7 7 .

A D I - S S - 3 05C00460 TUBE < 7 8 . < 7 8 . < 7 8 . < 7 8 . < 7 8 . < 7 8 . < 7 8 . < 7 8 .

A D I - S S - 4 05C004S1 TUBE < 7 S . < 7 S . < 7 5 . < 7 S . < 7 S . < 7 S . < 7 5 . < 7 S .

ADI—INF 05C00462 TUBE < 7 7 . < 7 7 . < 7 7 . < 7 7 . < 7 7 . < 7 7 . 5300 ( 1 2 0 )

A D I - S S - S O5C00463 TUBE < 5 9 . < S 9 . < 5 9 . < 5 9 . < S 9 . < S 9 . < S 9 . < S 9 .

A D I - S S - 6 05C00464 TUBE < 7 9 . < 7 9 . < 7 9 . < 7 9 . < 7 9 . < 7 9 . ( 1 7 0 ) < 7 9 .

A D I - S S - 7 05C00465 TUBE < 7 7 . < 7 7 . < 7 7 . < 7 7 . < 7 7 . < 7 7 . ( 1 7 0 ) < 7 7 .

ND Parameter not detected above NR Parameter not requested. NA Parameter not applicable.

LOD. ** ( )

See comment on l a s t page, Parameter betyeen LOD and LOQ.





Analytical Results

Form ARF-BL Page 8 of 11 Part 4 of 5 O422051O25OO05X

Date Laboratory Group Name OSC-OOSfi-n?

F i e l d S a m p l e Number


Sample Type

Ca

rb

on

T

etr

a

ch

lorid

e

ug

/m3

C C • N C «

A O Men o E rt-s. X cn O 3

• c a

X XI

• 0 E u O n 0 E E rt O N X U Oi U A 3

Ch

lor

ofo

rm

u

g/m

3

Eth

yle

ne

Dlc

nlo

r i

de

ug

/m3

He

xa

ch

lor

o

ath

an

e ix

g/m

3

0 u o rt X 0 • m e n u • E x> J = \ • XI Ol H V 3 :r

ich

lor

oe

the

ne

ig/m

3

A D I — F B 0SCOO4S6 T U B B 4 * ** ** ** ** *» n 9

** A D I — L B 0 5 C 0 0 4 6 7 T U B E ** ** *» **

• ** • * ** **

L i m i t o f D e t e c t i o n

L i m i t o f Qua n t i t a t i o n



960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 K ? 1 ? ^ ? ? ^ J 6 S ; S ° ° W e b P a g e : www.datachem.com FAX (801) 268-9992 E-mail: [email protected] 118

DATA^P GHEM L A B O R A T O R I ES

A Sorenson Company

ANALYTICAL REPORT

Date

Form ADC2.2745 Page Part 5 of 5 04220510250005X

Laboratory Group Name 05C-0058-07 Account No. 08001


Sampling Collection and Shipment Sampling Site RFPt 5303 P0r0048535

FAX (732) 775-7037 Telephone (737) 775-fii^fi

E-mail S.SIMBAI.YPWRSTONSni.TITTQMS < W

Date of Collection April 13, 7005


Analysis Method of Analysis NIOSH 1003


Analytical Results



Sample T y p e

«H JS V

«H O * 1 c

M O -JS

*4 *>tn 1 c e « o \

u cn U O 9 o

-Dic

hlo

ro

be

nz

en

e

ug

/m.3

0 u 0 rt O j B C

cm rt N e 0 C N 1 • cn PtJQ 9 tr

an

s-1

,2—

Dl

ch

loro

eth

en

e u

g/m

3

Air

V

olu

me

Lit

ers

A D I - S V W - 5 OSC00453 TUBE < 7 6 . < 7 6 . < 7 6 . < 7 6 . 1 3 2 . 2 4

A D I - S V W - 4 05C004S4 TUBE < 6 4 . < 6 4 . < 6 4 . < 6 4 . 1 5 5 . 8 1

A D I - S V W - 3 0SC0045S TUBE < B 3 . < B 3 . < 8 3 . < 8 3 . 1 2 0 . 4 3

A D I - S V W - 1 05C00456 TUBE < 7 6 . < 7 6 . < 7 6 . < 7 6 . 1 3 1 . 5 2

A D I - S V W - 2 05C004S7 TUBE < 7 8 . < 7 8 . < 7 8 . < 7 8 . 1 2 7 . 8 0

A D I - S S - 1 OSC00458 TUBE < 7 8 . < 7 8 . < 7 « . < 7 8 . 1 2 8 . 7 0

ADX-SS-2 05C0Q4S9 TUBE < 7 7 . < 7 7 . < 7 7 . < 7 T . 1 2 9 . 6 6

A D I - S S - 3 05C00460 TUBE < 7 8 . < 7 8 . < 7 8 . < 7 8 . 1 2 8 . 4 6

A D I - S S - 4 0 5 C 0 0 4 6 1 TUBE < 7 S . < 7 5 . < 7 S . < 7 S . 1 3 2 . 5 4

ADI—INF 05C004S2 TUBE < 7 7 . < 7 7 . < 7 7 . < 7 7 . 1 2 9 . 5 4

A D I - S S - 5 05C00463 TUBE < 5 9 . < 5 9 . < S 9 . < S 9 . 1 7 0 . 1 9

A D I - S S - 6 05C00464 TUBE < 7 9 . < 7 9 . < 7 9 . < 7 9 . 1 2 7 . 1 4

A D I - S S - 7 05C00465 TUBE < 7 7 . < 7 7 . < 7 7 . < 7 7 . 1 2 9 . 3 6






Analytical Results

ANALYTICAL REPORT

Date

Form ARF-BL Page 10 of Part 5 of O422051025O005X

11 5

Laboratory Group Name 05C-0058-07


Laboratory Number

Sample Type

«-4 JS

u 0 • 1 c

<N C -J:

H i i n 1 • E » O S

^ M Pi U 0 9

O u o H • JC C 0 e m

- < n E Q c s 1 • o> OJS 9

o o JS c

. o en —1 N E Q B \ 1 C 01 C L O 9

D C 1 c

<N £ ••Jl

H • 1 0 • Mn C 0 E

• rt— M JS Oi J> 0 9

Air

V

olu

me

Lite

rs

ADI—FB 05C004S6 TUBE ** ** * * ** 0.0

ADI-LB 0SCOO467 TUBE ** ** *« ** 0.0

L i m i t of D e t e c t i o n

L i m i t of Q u a n t i t a t i o n

t See comment on l a s t page. ND Parameter not detected above LOD. NR Parameter not requested. NA Parameter not applicable.


960 West LeVoy Drive / Salt Lake City, Utah 84123-2547 Phone (801) 266-7700 Web Page: www.datachera.com FAX (801) 268-9992 E-mail: [email protected] 120

Form Page 04220510250005X

ADC2.2747

DATA^P CHEM

ANALYTICAL REPORT

l A B O R A T O R I ES A S o r e n s o n Company

Date Laboratory Group Name QSC-OoqR-o?

General Set Conanents

** Result cannot be calculated for samples missing air volume. ug/m5 formula: ((Result * 1000) / Volume) * 1000

General Lab Conments

The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted in the General Set Comments above. Samples have not been field blank corrected unless otherwise noted in the General Set Comments above. This test report shall not be reproduced, except in f u l l , without written approval of DataChem Laboratories, Inc. This page is the concluding page of the report.


ADC2.2748 CHAIN OF CUSTODY RECORD

RFP Ho.:

5303

PONo.:

0048535 Restoring Resource Efficiency

Removal Support Team EPA Contract 68-W-OO-113

Phone: (732) 225-6116 Fax: (732) 225-7037

PresetvafiveeoxNo.:

1. Surface 1. HCL

2. Ground water Z HNO,

3. Leachate 3. Na,SO. M

4. Rinsate 4. HjSO, ™

5. Soil/Sediment 5 Other (specify)

6. Oil 6. Ice Only

7 Waste N. Not preserved

8. Ail *See Comments

(Specify)


Page 2 of 3

SmptoMMf *&*WBe>1J M M )

ADI^SWv-5 S V E W E L L # 5 , # M l 8 4/13/05 600 0.2204 132.24 1 N NJOSH 1003 w/ TCE

ADI-SVW-4 SVE WELL #4 8 4/1305 797 0.1955 155.81 1 N NIOSH 1003v*/ TCE ADI-SVW-3 SVE WELL #3 < 8 4/13/DS 556 0.2166 120.43 1 N NIOSH 1003 vrf TCE

ADI-SVW-1 SVE WELL #1 ' U 8 4/13/05 600 0.2192 13152 1 N NIOSH 1003 nl TCE

ADI-SVW-2 SVE WELL #2 i 8 4/13/05 600 0.2130 127.80 1 N NIOSH 1003 w/ TCE

ADI-SS-1 SUB-SLAB VENT 1 c 6 8 4/13/05 600 0.2145 128.70 1 N NIOSH 1003 v* TCE

ADI-SS-2 SUB-SLAB VENT 2 <? 8 4/13/05 600 0.2161 129.66 1 N NIOSH 1003 w/ TCE

ADI-SS-3 SUB-SLAB VENT 3 I '0 8 4/13/05 600 0.2141 128.46 1 N NIOSH 1003 w/ T C n

ADI-SS-4 SUB-SLAB VENT 4 ( 8 4/13/05 600 02209 13Z54 1 N NIOSH 1003 v*/ TCE

ADMNF SVE SYSTEM INFLUENT ( a 8 4/13/05 600 0.2159 129.54 1 N NIOSH 1003 W TCE

ADI-SS-5 SUB-SLAB VENT 5 { >b 8 4/13/05 789 0.2157 170.19 1 N NIOSH 1003 w/ TCE

Comments: Detection Level for TCE < 0.01 mg/sample TAT = 1 week verbal, 2 weeks written

Person Assuming Responsibility for Samples: Time/Date

Sample Number Time

\o\6

Date Received By:

fgjP€~ x

Reason for Change of Custody

pe«-iuiraj TD LAG,

Sample Number Relinquished By: Time Received B Reason for Change of Custody

Sample Number Refinquished By: Tune Date Received By. Reason for Change of Custody

Weston Solutions, Inc. FEDERAL PROGRAMS DIVISION In Association with Scientific and Environmental Associates, Inc., Resource Applications, Inc., and Innovative Technical Solutions, Inc.

4

CHAIN OF CUSTODY RECORD ADC2.2749

RFP No.:

5303

j ^ K T N o j ;

0048535 SOLUTIONS Restoring Resource Efficiency

Removal Support Team EPA Contract 68-W-00-113

Phone: (732) 225-6116 Fax: (732) 225-7037

Matrix Box No_ Preservative Box No.;

1. Surface 1. HCL

2 Ground water 2. HNO,

3. Leachate 3. NaJSO.

4. Rinsate 4. HJ50,

5. Soil/Sediment 5 Other (specify)

6. Oil 6. Ice Only

7. Waste N. Not preserved

8. Air 'See Comments

(Specify)


Page 3 of 3

( E f e W f t H ) 0 * t C 4 f » M R . T H

ADI-SS-6 Sub Slab Vent 6 [fcCM AW 8 4/13/05 600 02119 127.14 1 N NOSH 1003 w/TCE

ADI-SS-7 Sub Slab Vent 6 <r< 8 4/13/05 600 0.2156 129.36 1 N NOSH 1003 W/TCE

ADI-FB Field Blank Uff 8 4/13/05 NA NA NA 1 N NOSH 1003 w/TCE

ADI-LB Lot Blank A ,

ft 8 4/13/05 NA NA NA 1 N NOSH 1003 w/TCE

1_

comments: Detection Level for TCE < 0.01 mg/sample TAT = 1 week verbal, 2 weeks written

Person Assuming Responsibility for Samples: . Time/Date

Sample Number ReJiDe^fia By: / Time Date Received By: Reason tor Change of Custody

&£<-i UfcTiTy TO LA>3> Sample Number Relinquished By: Time Date Received B Y Reason for Change of Custody

Sample Number

Weston Solutions. Inc.

Relinquished By. Time Date Received By: Reason for Change of Custody

In Association with Scientific and Environmental Associates, Inc.. Resource Applications, Inc., and Innovative Technical Solutions. Inc.

ADC2.2750

This page intentionally left blank

rst-02-f-01841 transmittal memo

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