shivajiakola.ac.inshivajiakola.ac.in/pdf/sgb report.pdfi{indly find herewith final project report,...

NAAC Re-accredited with 'A' Grade (CGPA 3 11)

UGC Status'College with Potential for Excellence'

Near Shivaji Fark, Akola 444 0A1

Late Dr. Paniabrao Deshmukhiounde. iieslaent

Ref No.,M5g4'--+:=-To,

The Director,B. C, U, D,Sant Gadge Baba Amravati University,AMRAVATI,

Sir,

X ant enclosing herewith Final Project Report, Statement of Expenditure and Audited

Utilization Certificate of Minor Project in chemistry UGC File No'47-159/1-zWR))

Dated :- 15 April-2013 entitled "studies on Incidence and Extent of Pesticide Residues in

Natural Water Reservorirs in Akola Distt. of vidarbha Region (Maharashtra)" sanctioned

by U.G.C. to Dr. S. G. Bhadenge, Department of Chemistry of our college in prescribed format

of UGC.

'1ou are tierefore requested to forward the same to the Joint Secretary, UGC Western

Regional hffice, Ganeshkhind Pune for further necessary action.

Kindly do the needful.

Thanking you in anticiPation.

PA$}KSA4LS h $ffiffi i7 f g'S gtdb gf'At-t s,

^'effi.*d%m,Hr,Trtftffi

1. Final Project RePort2. Statement of Expenditure.3. Audited lltilization C ertificate.

a-: a,

,. r".r 'i : rt--t^ f,t^!-. nfrAntOA1?A

Pune with -vour recommendations

Yours FaithfullY,

Shri Shivaji Education Society' Amravati's

sF{Rg 6pgcvn.$fi CSLS.EGE SF Ail{TS, C&&$E4EffiCE AN& SCEEruCF KSEANAAC Re-accredited with 'A' Grade (CGPA 3.11)

UGC Status'College with Potential for Excellence'

Near Shivaji Park, Akola 444 001

The Joint Secretary,U niv e r sity Gr qnts C o mmi s sion,Western Regional Office'Ganeshkhind,PUNE - 477007, (M.S).

Through:- Director, B.C,U.D., Sant Gadge Baba Amravati UniversiQ, Amravati.

Subject :- Submission of Final Project Report, Statement of Expenditure and

Aud ited U til izatio n C ertificate'

Sir,

I{indly find herewith Final Project Report, Statement of Expenditure and Audited

(.ltilization Certificate of Minor Project in chemistry UGC Fite No.47-15g/12(WR0)

Doted :- 15 Aprit-Zl13. entitled "Stud,ies on Incidence and Extent of Pesticide Residues

in Nqturq.I Water Reservorirs in Akola Distt. Of Vidarbha Region (Maharashtra)"

sanctioned by U,G.C, to Dr. S. G. Bhadenge, Department of Chemistry of our college in

prescribed format of UGC.

Kindly do the needful.

Thanking you in anticiPation,

W Yours Faithfully,

Encl:-

1. Final Project Repor,.2. Statement of Expenditure.3. Auditeci Utrlization Certificate

6gp'""xffi;"{2.6';: i'(@r

UGC MINOR RESEARCH PROJECT

FINAL PROGRESS REPORT

Statement of Expenditure and Audited Utilization Certificate'

Title :

,,Studies on tncidence and Extent of Pesticide Residues in

Natural Water Reservorirs in Akola.

Distt. Of Vidarbha Region (Maharashtral"

For the Year- 2013 -15No.F.47-159112 (WRO) Dated -15 April 2013

Date of implementation- 01 July 2013

Name of Principal lnvestigator

Dr. S. G.BhadangeDepartment of ChemistrY

SHRI SHIVAJI COLLEGE OF ARTS, COMMERCE ANDsclENcE, AKQLA. (M. S.)

- JulY 2015

www.s hivaj iakola.ac. i n

The JointSecretary,U.G.C. Pune University CamPus

Gnnesh Khind,PUNE

Ref :- F.47-759/12 Dated -75 April2073

Sub :- Release of Rs. 30.669/- towards the expenditure incurred under MRP'

Through :- Proper Channel

Respected Sir,

Vide subject cited above you are requested to release the amount of Rs.30,669/- towards the

expenditure incurred under M,RP. The total amount sanctioned for the M.R.P. was L,20,000/-, 0ut of

this the amount of Rs.90,000/- was only released as a first installment.

Till the completion of the study the total expenditure incurred was Rs.1,20,669/-.

The amount of Rs.669/- was spent more that of Sanction of Rs.1,20,000/-.

The amount of Rs.669/- was necessary to spent for the completion of the study or

otherwise it was not possible to completes the study under the M.R'P'

The Detatls of the expenditure are given below

Kindly Send the Remaining amount of Rs. 30,669/-

Thanking You

P rincipal I nvestig oto rShri Shivaji College, Akola

(DRS.G.Bhadange)

5 h r i * li l'**dt? S.ti f t€rH 6VO fA rt s.c r.,S r!s, co ni$tgff€,{gKR €n_A:

A Grae.ie t. &{QM,1 1,by NAAC

Sanction AmountRs.

L,20,000/-

Rs.1,20,000/-

Rs.90,000/-

A 30,000=00 il,d lnstallment

B Excess Expenditure incurredfor the

completion for the Completlon of the study

Rs, 1,20,669-90,000= 30,669 /-Total amount to be released

B=Rs. 669 = 00/-

Total Ri.30,669 = oo/-

Total Expendituretrncurred Rs.

Amount to be leased Rs.

ffi

UNIVERSITY GRANT COMMISSION

WESTERN REGIONAL OFFICE GANESHKIND,

PUNE _ 44TLOO7

U T I LISATI O N CERT IF I CAT E

It is certified that the grant of Rs. 1,20,0001- Sanctioned by the University Grant

Commission for U.G.C. Sponsored Minor Research Project in Chemistry Department to Dr. S. G.

Bhadange has been utilized as per details given in the attached, statement in accordance with the

terms and conditions laid down by the University Grant Commission wide letter

No. F.47-1 59 /7}(WROJ Dated :- 15rh April 2013. [Full allotted amountJ and. as these terms and

conditions have been fulfilled by the college/ University and the grant has been utilized for the

purpose for which it was sanctioned'

It is further certified that inventories of permanent of semi permanent assets created

/acquired wholly or mainly out of the grants given by the university Grant Commission as

indicated above are being maintained in the prescribed form and are being kept up to date and

these assets have not been disposed of encumbered of utilized for any purpose'

*.iffirfniffiffid-*/- Af tS;€ o:Frf .?fi e r e &,S? phg$

Akola

CHARTERED A C gO'UNTANTS

PrincipdllnvestigatorlDr. S. G. Bhadangel

M. No. 32803

Annexure - V

UNIVER.SITY GRANTS COMMISSIONBAHADUR SHAH ZAFAR MARG

NEW DETHI - 110 002.

STATEMENT' OF EXPENDITI"IRE IN

1. Name of Principal Investigator :-

2. Department of University/College :-

3. UGC approval No. and Date

4. Title of the Research Project

5. Effective date ofstarting the project : -

6. [a) Period of Expenditure :-

7. Details of Expenditure

RESPECT CF MINOR RESEARCH PROJECT

Dr. S. G. Bhadange

Shri Shivaji College of Arts. Commerce & Science,

Akola.

No.F.47-159112 [WRO) Dated -15 April 2013

"Studies on Incidence and Extent of Pesticide

Residues in Natural Water Reservorirs in AkolaDistt. Of Vidarbha Region [Maharashtra)"

01 July 2013

From July 2013 to fuly 2015

4. It is certified that the grant of Rs. 12,0000/- [Rupees. One Lack Twenty.thousand onlyJ received from the

University Grants Commission under the scheme of support fqr Minor Research Proiect entitled " Studies on

Incidence and Extent of Pesticide Residues in Natural Water Reservorirs in Akola Dist. Of Vidarbha

Region (Maharashtra)" vide UGC letter No. F.47-15g/12 Dated -15 April-2013 has been fully utilized for

the purpose for which it was sanctioned and in accordance with the terms and conditiotii t"ia down by the

University Grants Cornmission

Principal InvestigatorDr. S. G. Bhadangel

SrNo

Item Amount Approved Rs. Expenditure Incurred Rs.

Books & Journals 10000/- 1003s/-

u Contingency 10000/- 10117 /-

Iii Field Work/Travel (Give details in theproforma at Annexure- VIIJ,

10000/- 10200/-

IV Equipment 50000/- 50000/-

V Chemicals & Glassware 40000/- 403L7 /-

VI Other head I Special Need] Nil Nil

vllTotal= [Firstyear Rs 90000/- +

Second Year grant Rs.30000/-lr,20,000/- I,20,669 /-

--l

SHRI SHIVAJI COLLEGE OF ARTS, COMMERCE AND SCIENCE, AKOLA.

MINOR RESEARCH PROJECT - DEPARTMENT OF CHEMISTRY

Investigator- Dr. S. G. Bhadange

F.47-159 /I2 Dated -15 APril 2013Details of "the Expenditures for the year - 2013 -15

Audited Statement of ExpendituresFor the year - 2OL3- 14 and 20L4 - Ls

SrNo

Non recurringsrant

AmountExnenditure

AmountSanctioned

Recurringsrant

AmountExnenditure

AmountSanctioned

I Books & journal 10,035/- 10,000/- Contingency

Chemicals

Travels

ta,tL7 /-

40,3L7 /-

10,200/-

10,000/-

40,000/-

10,000/-

2 Equipments 50,000/- 50,000/-Total 60,035 /- 60,000/- Total 60.634/- 6o,0oo/-

Grant Total Recurring & onrecurrlng 1,20,669 /- Sanctioned L,20,000/-


MrNOR RESEARCH PROJECT OF DR.S.G.BHADANGE -2013-15.

DEPARTMENT OF CHEMISTRY

Investigator - Dr.S.G.Bhadange

F.47-I5g/L2(WRO) Dated -15 April2013 Date of Implementation- 01|uly 2013

BOOKS.


SrNo.

GrantsVoucher

NoPurchased

From whomBill No. &

DateParticulars /DescriPtion

Amountin Rs

IBooks &fournals 1

BooksEmporium

Akola

571.4&

27 /0e/2013

Elements of PhysicalChemistrv Bv Puri

3Bs/-

Principals of PhysicalChemistrv Bv Puri

s3s/-

Natural Products Vol. II BY

O.P.Asrawal3so/-

Organic Chemistry of NaturalProducts Vol. I By Chatwal

3so/-

0rganic Chemistry of NaturalProducts Vol.ll By Chatwal

3so/-

Advance 0rganic ChemistrYVol. I and Vol. II Bv S.K. Ghosh

Bs}/-

0rganic Chemistry ByMorrison

B7s/-

StereochemistrY BY P.S. Kalsi zesl-0rsanic Svnthesis By J. Sing 455 /-Ad.0reanic Chemistrv 425/-Concise Inorganic ChemistrYBv Lee

700/-

Physical Chemistry By Bhalf2 coniesl

L,590/-

Ad.0rganic Chemistryf2 copies')

2,390/-

Ad. Inorganic ChemistrY Vol. I

Bv Madan '6so/-

Ad. Inorganic Chemistry Vol.II Bv Madan

4s0/-

SDectroscoDv Bv Y.R. Sharma 500/-

Rs. Ten thousand Thirty five onlY Total Rs.10,035/-

SHRI SHIVAJI COLLEGE OF ART'S, COMMERCE & SCIEI.ICE AKOLALIBRARY DEPARTMENT

Date- 22-8-2015

ACCESSION CERTIFICATE

It is certified that the Books purchased from MRP grant are handed over to the

college central library. Their Accession number is from 49757-49775

aA@lnvestigator

(Dr. S.G. Bhadange)LI$RARIAN

Strri Shivaii {arltge rf Artr-i'dtnt.t.* +: sclence-

AKOLA

sh,i si. f$lWldbJ, o, o.,,,Cornnrerce ft Science.AKOLA^

A chaHrry.adimp.l bpi,A$qhAa

Librarian

To,The PrinciPal,Shri Shivaii College of Arts,Commerce and Science,Akola.

Ref :- MRP of Dr. S. G. Bhadange F. No.47-159/12 (WRO), Dated L5'04'20t3'

Respected Sir,

I am submitting herewith actual expenses incurred against MRP

for 201.3-2014 and 20L4-201.5 vide its letter F. No. 47-1,59/t2 IWROJ,

Following is the summary of actual expenditure'

sanctioned by UGC

Dated 15.04.2013.

sh ri Sbrudhtloff4qJogAa5,ComAres@ftfo tensqffOhAe,

A Grade C. GP&$ttl,by NAAC

e4)pp1ffiffi[Bal

Advance against my name is 30,000/- [Rs. Thirty thousand only) for which I am submitting

the actual expenditure of the same, hence it should be nullified against my name'


SrNo

Type ofGrant

ParticularsAmount

SanctionedAdvance Expenditure

Sanctionedexpenditure

Actual Totalexnenditure

1

Non-Recurringqrant

Books 10,000/- 1o,000/- 1o,035/- 10,000/- 10,035/-

Equipment 5o,ooo/- 5o,ooo/- 50,000/- 50,000/- 50,000/-

2Recurringgrant

Contingency 1"0,000/- 05,000/- 5,499 /- 10,000/- r0,r17 /-Soecial Needs NiI Nil NiI NiI Nil

Travel/Fieldwork

10,0o0/- 5,000/- 491.0/- 1o,oo0/- L0,200/-

Chemicals 40,000/- 20,000/- 20,007 /- 40,000/- 40,s1,7 /-

ExtensionActivities

Nil Nil Nil Nil Nil

Tota t,20,000/- 90,000/- 90,4sr/- L,20,000/- L,20,669/-

I innod 1,7.0,000/-

Total expenditure t,20,669/-L,20,000/-D ,t; ha cenctinned

Q- -^fi nn orl ovnon ditt trP t,20,000/-

Adrrance paid to me for MRP expenditulg 90,000/-D A I +^ IInC I Itilizetinn Cprtificate Nil

30,669 /-Balance amount to be paid to me as per Utilization Ce

MrNOR RESEARCH PROIECT OF DR.S.G.BHADANGE -2013-15'


F.47 -1.se l12wRo)


Dated -15 April2013 Date of Implementation- 01luly 2013

CHARTERED ACCOUNTANTSj M. No. 3?805

SrNo.

GrantsVoucher

NoPurchased

From whomBill No &

DateParticulars

/DescriptionAmount

in Rs

II ContingencY

2

PrimeComputerServices,

Akola

t2/08/2073 Quick Heal Antivirus 1,500 /-

-J 21/03/2074HP Original TonerCartridee

3,999 /-

4 07106/201,4

Tone Refilling 300/-

OCR Drum 3s0l-PCR Roller 340/-

5 09 /L0 /2074 Pen Drive 16 GB 900 /-

6 1,4/12/2014 DVD Disk R/w f1B) 900/-

7 22/01./201,5 HP Printer Taflon Film 980 /-

oShri Shivaji

College,Consumer

Co-op. Stores,Akola

1080&

10/02/2075

Ex Bond Paper [1 rimJ 340/-Transparent TaPe 070 /-Gum Bottle 078/-

9

t079&

L0/02/2075

Paper 44 [1 rimJ t70l-

Paper Legal Size [1 rimJ teo /-

ffind One Hundred Seventeen only Total LO,LL7 /-

P ri n cip aY1 nvesti gato rDr. S. G. Bhadangel

MrNOR RESEARCH PROJECT OF DR.S.G.BHADANGE -2013-15.



F.47-15g/12[WRO) Dated -15 April20L3 Date of Implementation- 01luly 2013

SrNo

GrantsVoucher

NoTravel Rout

Bill No &Date

Particulars/Descriution

Amountin Rs

llt

Fieldwork

&Travels

10Akola-Akot

[Travel & otherChareesl

1.6108/2013To collect water samPle

for MRP L,L30/-

tlAkola-Patur


z0/L0/2013To collect water samPlefor MRP 860/-

L2

Akola-Murtizapur

fTravel & otherCharsesl

28/12/2ABto

2e lt2/2013

To collect water samPle

for MRP t,260/-

a3Akola-Balapur

fTravel & otherChareesl

70/03/2014to

11/03/2014

To collect water samPlefor MRP 1,660/-

L4Akola-Telhara[Travel & other

Chareesl

0s/07 /2014To collect water samPlefor MRP t,tB0/-

15Akola-Mhaisang


25/0e /2074To collect water samPle

for MRP 680/-

L6

Akola-Barshitakli

[Travel & otherCharsesl

12112/20L4

To collect water samPlefor MRP Bzo/-

t7Akola-Mana


16/07/201sto

77 /01/2015

To collect water samplefor MRP r,sgo/-

1B

Akola-Hiwarkhed


22/03/20Ls

To collect water samPlefor MRP ezo/-

Total amount of Rs. Ten thousand Two Hu44I94-941y L0,200/-

':;j;]:+N. ..1/ ,..- *'i*dr \ -F

tlEl-i,''i^ -',1$

A*\ \P';:'-?;*,"r

inwilg -'.,'."';

CCOUNTANTS

ShriShiir8liifafl@lddd,ccnspss6 ft fiElpaggAb$hte,

A Grade c. GPA.dhSfiby NMc

MINOR RESEARCH PROJECT OF DR.S.G.BHADANGE -2013-15.

DEPARTMEI{T OF CHEMISTRY


F.47-LSg/L2IWRO) Dated -15 April2013 Date of Implementation- 01fuly 2013

EQUIPMENTS.

0.,".,0rflffi*.Dr. S. G. Bhadangel

pftnLqFdL

c$[$l$F{'sffiRftfr:Afl 6FAt€ 8 ryffi.9 *ff,F9 $mc

Akola

SrNo

GrantsVoucher

No

PurchasedFromwhom

Bill No&

DateParticulars / Description

Rate inRs

Amountin Rs

lv Equipments

T9

ShreeGanesh

ScientificSyndicate,Amravati.

r4B/13-14&

301t1.113

Digital Potentiometer, EQ-

601/ Ecuiotronics [1pic.l5,400/- 5,400/-

Glass Electrode/Eouintronics 12 Nos.l

s7s/- 1.,1.50 /-

Silver Electrode /Equintronics [2 Nos.l

6so/- \,300/-

Total Rs.7,850/-

20

ShreeGanesh


162/13-14&

30/11"/13

Digital Conductivity Meter,EO-660A/ Equiptronics

8,100/- 8,1.00/-

Digital PhotoelectricColorimeter, EQ-650/Eouintronics

8,272/- 8,272/-

Total Rs.L6,372/-

21

ShreeGanesh


17B/L3-7430/17/r3

Digital Polarimeter, EQ-801Equiptronics

25,778/-25,7_7Bl

Total :- Rs. Fifty housand on ly Total Rs. 50,000/-

MINOR RESEARCH PROIECT OF DR.S.G.BHADANGE -2013-15'



F.47-Llg/L2(WRO) Dated -15 April2013 Date of Implementation- 01fuly 2013

CHEMTCALS.

SrNo

Grants VoucherNo

PurchasedFromwhom

Bill No. &Date

Particulars/ D escriPtionRate in

Rs

Amountin Rs

v Chemical

22

ShreeGanesh


1,68/13-74.&

261r1/2013

Diethvl Ether [500m1x 5l 260/- 1,300/-

Dimethyl Formamide150Oml x 2l

201/- +02/-

Dimethyl Glyoxime [10Ogm ] 3291- 32e /-Ethvl Acetate [500m1 x 3l L72/- 516/-

Ethvl Bromoacetate [250mI] 1704/- r,704/-

Glvcerol [500m1x 3l 229 /- 687 /-Guanadine Nitrate 1250eml 225/- 225/-

Hvdrazine Hydrate [5 00mll 706/- 706/-

Hydrazine Hydrochloride1100eml

1.es/- 79s/-

Hvdrochloric Acid 15lit. x Bl 494/- 3,952/-

Total Rs.10 0L6/-

,a

ShreeGanesh


2L4/14-15.&

11,102/2015

Acetone I2.5 lit. x 4l 820/- 3,280/-

Aniline 1500ml x 5l 35s /- L,775/-

Bromine[5x5x20mll 783 /- 3,915/-

Benzene [2.5 lit. x 2] r23s/- 2,470/-

Total Rs.11,440l-

24

ShreeGanesh


217 /14-75&

71/02/207s

Chloroform[2.5lit x 4l Bse/- 3,436/-

Petrolium Ether,60-80t2.5 lit. x 3l

738/- 2,21,4/-

Pvridine 1500ml x 4l 620/- 2,480/-

Maltose [500em x 1l 740/- 740/-'Iotal Rs.8,870/-

GlassWares

25

ShreeGanesh


167 /73-1,4&

26117/2013

Basirl Porcelin,3" 17 /- 1.24t/-Beaker,5Oml 30/- 750/-

Beaker,100ml 37/- 1,240/-

Beaker,500ml 77/- 5,680/-

Beaker,2000ml 270/- 1,080/-Total Rs.9,991/-

Fofi thousand Threr Hundred Severrlgen only,.- Total Rs.40,i L7=00/-

PrinciDr. S.

j;l!t:

ACCESSION CERTIFICATE.

It is certified that the Books purchased from MRP grant are handed over to the college

central / departmental Library. Their Accession number is from...... To .........'.....'..

Librarian Principal Investigator

llege

tt

MINOR RESEARCH PROIECT OF DR. S.G.BHADANGE -2013-014.


INVESTIGATOR - DR. S.G.BHADANGE.

File No.47-159/12[WRO]. Dated:- 13'd April-2013. Date of Implementation- 1.t |ul/ 201,3

ASSETS CERTIFICATE

It is certified that the following Equipment have been handed over to the college


\}$>/ r/" *LK|ntrItry;3ili:i$:i""Cl'jrigalt v"'

Shtt' "'

Seal of the college

Sr.No. Equipment Quantiry

01 Digital Potentiometer. EQ-601 [Equiptronics] 01.Pic

02 Glass Electrode, (Equiptronics) 02.Pic

03 Silver Electrode, (Equiptronics) 01.Pic

04 D igital Conductivity Meter, EQ-6 60A, [EquiptronicsJ 0L.Pic

05 Digital Photoelectric Colorimeter, EQ-65 0, (Equiptronics) 01.Pic

06 Digital Polarimeter, EQ-801, [Equiptronics] 01.Pic

a

FINAL REPORT OF THE WORK DONE ON THE MINOR RESEARCH PROJECT.

1. Project report Fihal

2. UGC Reference No.F.47-1 59 I 12 WRO), Dated -1sth April 2013.

3. Period of report. from -2013 to 2015

4. Title of research project "Studies on lncidence and Extent of Pesticide Residues in Natural WaterReservorirs in Akola Dist. Of Vidarbha Region {Maharashtra)"

5. (a) Name of the Principal lnvestigator - Dr. S. G. Bhadange.

(b) Department and University / College where work has progressed - Department Of Chemistry, Shri

Shivaji College of Arts, Commerce & Science, Akola.

6. Effective date of starling of the project- 01't July 2013.

7. Grant approved and expenditure incurred during the period of the report.

(a) Total amodnt approved Rs. 1,20,0001 Sanctioned for first lnstallment Rs.90,000 /-

(b) Total expenditure Rs. 1,20,669/-

REPORT OF THE WORK DONE : PLEASE SEE APPENDIX- A.

(i) Brief objective of the project: - Studies on lncidence and Extent of Pesticide Residues in Natural

Water Reservoirs in Akola Dist. Of Vidarbha Region (Maharashtra)

ii: Work done so far and results achieved and publications, if any, resulting from the work (Give details of

the papers and names of the journals in which it has been published or accepted for publication):

Nit

(iii) Has the progress been according to original plan of work and towards achieving the Objective? lf

not, state reasons. - Yes.

(iv) Please indicate the difficulties, if any, experienced in implementing the Project - Nil

(v) lf project has not been completed, please indicate the approximate time by which it is likely to be

completed. A summary of the work done for the period (Annual basis) may please be sent to the

Commission on a separate sheet: - [Please see Appendix-A]

vi. lf the project has been completed, please enclose a summary of the findings of the Study. Two

bound copies of the final report of work done may also be sent'to the Commission [Please see

Appendix-AI

vii. Any other information which would help in evaluation of work done on the project. At the completion

of the project, the first report should indicate the output, such as

(a) Manpower trained

(b) Ph. D. awarded

(c) Publication of results (d) other impact, if any NIL

SIGNATURE OF THE PRINCIPALINVESTIGATOR

[Dr.S.G.Bhadange] ffi PRINCIPAL[Dr.S.G.Bhadange]

UGC MINOR RESEARCH PROJECT

FINAL PROGRESS REPORT

Title :

,,Studies on lncidence and Extent of Pesticide Residues in Natural

Water Reservorirs in Akola.

Distt. Of Vidarbha Region (Maharashtra)"

For the Year- 2013 -15

No.F.47 -159112 (WRO) Dated -1sth April 2013

Date of implementation- 01't July 2013

Name of PrinciPal lnvestigator

Dr. S. G.Bhadange

Department of ChemistrY.

SHRI SHIVAJI COLLEGE OF ARTS, COMMERCE AND SGIENCE,

AKOLA. (M.S.)

JulY 2015

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Tiirt Pll.iNCiP./r;-,SIIRI SHIVA.II CC)L,I,}IGt' OF AI].T'S

COMM ERCI' & SCIE,NCE,,NI'AIT SHIVA.II

PARK, . ,----AKOI,A,.Ar<o[,A - 444 001.

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Suh.ject: Reieuse,J'grunt through D D. l'lo. / IITG,9 Confirmntion IYo-/ IYFiI;T-/ T'ransf'er No'

Srri Madarn,

picase find enclosed D.D.No./ Itl'CiS (lonflrnration Nc/ NIlI"[i'fransl'er No. peltaining

to release of'grant-in-aici to youri ctlllege as per' lollowing details:

I I).1.: - I)r'. Elhadarrge S. (1,

o SanctftT'i;iffi=?F1il"n..' - 41 -l 59/1 2(WRO), l)ated 20.02.13

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llnc I : A cknttw lecl gern en t

AC]KNOWI,EDG!]MIiNT F()Ir'TIIE GRANl'S RF](]F],IVtiD ITROM TJGC (WRO), PIJNF]

(to be returnccl inrnrccliately on rccciJrt of (l)l) No./R1'(JS (lottfirtrtation No./NIit..'t-/"Dsrulsfcr Nt$-

t_Appendix - A

Minor Research PROJECT

COMPLETION REPORT

From 0110712013 to 021A712015

Principal Investigator: - Dr. S. G. Bhadange

UGC File No.F.47-l59ll2 Dated - 15 April20L3

TitIC:. "STUDIES ON INCIDENCE AND EXTENT OF PESTICIDE RECIDUES IN

NATURAL WATER RESERVIORS IN AKOLA DISTRICT ON VIDARBHA REGION(MAHARASHTRA)"

Amount Sanction: - 1' 20' 000/-

Infroduction: -

Pesticide is a substance intended for preventing, destroying, repelling or migrating pests. A

substance intended for use as plant growth regulator, defoliant or desiccant is also classified as

pesticide. Pesticide is classified into insecticides, fungicides, herbicides or weedicides, acaricides,

nematicides based on the target pest. They are classified into five groups based on their structure

viz, Organochlorine, organophosphate, carbamate, pyrethoids and others. Organochlorine pesticides

are hydrocarbon that contain chlorine atoms and most of them are highly persistent, carcinogenic

and mutagenic. DDT, DDE, Endosulphone, Lindane, Heptachlore, Chlorodane belong to this

group. Recent reports of increased incidence of abnormaldevelopment of testis and reproductive in

capabilities related to exposure of environmental chemical have are used a great conceffl. The male

reproductive system may be affected via different mechanism. The pesticides adversely affect

spermatogenesis and cause testicular atrophy and fetotoxicity. Pesticides chemical like DDT,

dieldrin and polycyclic hydrocarbon have been reported to alter the level of testosterone and to

decrease the reproductive ability. Impotency in farm workers on exposure to pesticides has also

been reported. Epidermiological studies have confirmerd that women manied to men exposed to

DBCP and chloropyrene have higher rate of abortions. Due to these injurious effects', many of the

highly toxic chlorinated hydrocarbon pesticides have been banned in the United States, Still these

chemicals persists as environmental contaminants and are in wide spread use in developing

countries.

Akola is tribal, rural district of Vidharbha region of Maharashtra. Major agriculture produce

is Cotton, capsicum and Soybean. This district is a top grower of cotton and Soybean. Eventually,

the illiterate tribal farmers use huge amounts of pesticides in their cotton and Soybean fields. It

results into percolation of large quantities of these hazardous chemicals in natural water reservoirs

as well as milk producing animals like cow, buffalo etc.

IVlethod & Matcrial:-

a) Extraction of pesticide residues from natural lvater reservoirs:

One liter water will be taken from each of randomly selected natural water reservoirs from various

Tahelis of the district during two seasons of the year. Each of the sample water flasks will be added

with 10-15 gm of sodium chloride and the mixture will be stired gently. The solution will be

transfer in to a 2liter reparatory funnel followed by addition of 60ml methylene chloride. The

funnel will be stoppard and shaken for three minutes, the lower dichloromethane layer will be

separated from the upper rvater layer and the lower organic layer is drained through granular

sodium sulphate (abiut 20g) into a250ml conical flask. The extraction will be repeated twice more

and the extracts will be combined. The dichloromethane will be evaporator under vacuum and the

volume will be reduced to I rnl. The mixture will transferred into a graduated tube using acetone

(5ml) and the solvent will be evaporated just to dryness. The volume will be made up to 1 ml and

will be stored into an auto sampler vial. Internal standard will be added and stored at 50C in a

freezer until analyzed"

b) For HPLC -Fluorescence detection.

Result:-

Results from the study have been shown in table which is carried out in the seasons Rainy

2013, Summer & Rainy 2014 from the various dams and rivers of different tahasil of Akola district

viz. Akola, Akot, Telhara, Balapur, Murtizapur, Barshitakli and Patur. The results are related to

the concentration of OC residues in water. The associated figure for mean concentration for

pesticide DDT was in the range of 0.01-0.05 pgll-. The pesticides chlorodane, Lindane and

heptachlor was not detected in the water samples showing that the farmers around the reservoir do

not use them in their farming activities. Endosulfan, a broad spectrum contact insecticide and

acaricide, is another pesticide used by many farmdrs. The associated figure for mean concentration

of Endosulfan was in the range of 0.01-0.02 prgll-.

Results:

Area DamslRivers Season ;DDTIDDE:

Chlorodane r HePtachlor

ND

ND

ND

ND

ND

Endosulfan ;

ND

ND

0.01

ND

ND

0.01- - ''.--..",. :-- -'.

ND

ND

0.01

N;

ND'.'..'.-..*..'-''--*.'.

o:ol

ND

ND

ND

0.0 i

ND

0.01

Nr*0.01

0.01

o.or

*-o-ND"

0.01

- -;;;-

0.02-$-

0.01

0.04

0;0.04

0.03

0.;;

0.02

0.03

0.03

0.05

*i-0.03

0.02.'o:03

0.05

0.02

-- -ryr -0.02

0.01--^0.0t--

o:01

0.01

0.02

0.01

0.02

0.01

0.0'i

ND

0.01

o.o+

0.02

0.04

0.03

0.;;

0.02

0.03

0.03

0.05

0ri0.03

0.02

o:03

0.05

0.02

- -1t,0.02

0.01--^0.0t

Akola

Akot

Balapur

Murtizapur

o:01

ND

ND

ND

N;

ND

ND

0.0;

0.01

ND

N;

0.01

ND

i

o:ol

0.01

ND

ND

ND

ND:-'-.:NDI_-.^.'.-;NDI

*.-.-.-*'*'""0.01

0.01t - -'.------ .'-' --- ..

Rainy 2013 ' 0.02 : 0.05 ,

-'t-- -- -1- - lSummer o.o4 o.o42014 :--- : : -Ra]ny2014 i 0 03 0.02 ,

Rainy 2013 0.03 , 0.05

Summer o.o5 o.o42014 --- - i- --- --r - --'-Rainy 2014 0.02 0.03---, Rainy 2013 I 0 04

i 0.04

l

Summer o.o3 o.o22014

Rainy 2014' 0.05 0.02

Rainy 2013 , 0.09 0.03

t;il.' o.o3 o.o5--* 'i'.---"'-i**--":

Rainy 2Ol4 ' 0'02 i 0.01r'-----' --- ..- .--

: -- -- -i - - - -lRainy 2013 0.05 0.04

' '' : -

!;ff" o.os o.o3

l nuiny 2014 '0.03 I 0.02 '--; :

Rainy 2013 . 0.05 0:02

'!|ff* : o.o+ i o.or r

i..''--- ..--- ".- --i---^-- .. i - -i

J:'"v3oY+906-i o'9-1 l

Rainy2013:005 I 0_01 ,iilff* i o.o+ i o.o: .

..-i ----- --i-- --^-'

'Rainy2014,0.04:0.05I-jiI

Rainy 2013 0.02 . 0.OS1 ...... .. .... . *----- -..-.---- ------ : - ..- ----i

;;il'"' o:or,oo,

Rainy 2014 ' 0.02 0.01-;,

: Rainy 2013 t 0.03" i 0.03 i

---:*--'"---i--** -'-.---l

;;ff" o.or ,o.o+.'--: '.-...-' ----i"* -.- --**

Rainy2Ol4.005 i002

Rainy 2013 : 0.06 i 0.04

Borgaon l,ake '

( LocalNallah)

:

i Masa Darn

i ( Local Nallah)

i

i^--------'-1

i Sisaudegaon

: Dami (Local Naltah)

i

j Popatkhedi Dam

i iOatf'er ll.iver)l

l-- *- -- -

i Chinchpanii Dam

I @ocalNallah)I

t- ---- ---- ..------------

:

i nnirureO

i DamI tLocal Nallah)'i

i

I

i Balapur dam

r (Mun River)

IlI

II ShivankhurdI

i DarrI llocat Nallah)

i

I

I Uma Dam

i rutouRiver)!

I- -.i-------- --*----------i Kat"putnu

Dam Sumtner(Kateptrnta 2014

0.04i0.05. 0.03t1........i......-

ND

0.01

ND

NDRiver)'': - - -l-

Rainy 2014 , 0.02 i 0.02 1 0.02

Barshitakli

Patur

Telhara

Tuljapur Dam(Local Nallah)

I

I

Patur Dam(Local Nallah) .

Summer

.?*.0_t4 _*0.06i0.06l 0.02

,-i__.. -..

;."''.'-*.'_--.-.-*..i.:---..--*:-''*'Rainy 2013 | 0.05 i 0.05 : 0.01

Hatola Darn Summer , 0.03 : 0.02 0.03 ND 0.01(LocalNallah) 2014

,20r4i0.04i0_92, 903 091 , NDi,-.. -"**-+--**-- -.

Januna Dam ' Su.n*., . O.O: i O.OZ 0.03 ND i ND(LocatNallah) 2014

Rainy 2013 '0.05 i 0'05 , 0'04 , 0 01 1 0:01 :

ND 0.01

0.02 ND

Rainy 2014 : 0.04 i 0.07 I 0.07 , 0'01 , ND:l

Rainy 2013 , 0.05 i 0.04 i 0.05 , ND , ND

0.01 : 0.01

-..'.--'.'---.'iNDiNDNDlND

Summer ' o.oz , o.o5 o.o22014 . ,-:-Rainy 2014 | 0.04 i 0.07 1 0.05

'i

Rainy z0l3 ' 0.05 i 0.0s I 0.08

(Nirguna 2014o"' 1 0.02 i o.os : 0'05 o'ot i

0'02

River) :"'^'"-^/ Rainy 2014'0.06 I 0-02 't 0'06 ' 0'01 . ND

,

, Rainy 2013 10.05 i 0-02 i 0.05 i ND i ND

numan sagar 2014\rrs'r\rrY'l

Rainy 2014' 0.05 ; 0'05 0.02 ND i 0'01

Conclusion:

From the observed result we concluded that the water of all these areas of Akola district

contains less amount of pesticide so water is suitable'for domestic as well as agricultural purpose

and also for drinking purpose after some treatment. Along with this pesticide analysis we also

analyzed some physico-chemical parameters and this parameter in the limit of..drinking water

standards of BIS and WHO.

Dr. S. G. BhadangePrincipal Investigator

shivajiakola.ac.inshivajiakola.ac.in/pdf/sgb report.pdfi{indly find herewith final project report,...

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