report no d3110-13 - apps2.staffordshire.gov.uk
TRANSCRIPT
Report No D3110-13 GNOSALL ST LAWRENCE PRIMARY SCHOOL, GNOSALL, STAFFORD FACTUAL REPORT ON GROUND INVESTIGATION Carried out for: Education Funding Agency Engineer: Mott MacDonald Ltd November 2013
www.esg.co.uk Environmental Scientifics Group Limited
Reg office: ESG House, Bretby Business Park, Ashby Road, Burton upon Trent, DE15 0YZ Incorporated in England: 02880501
Issue No Date Details 1.0 November 2013 Draft Report 2.0 November 2013 Final Report
The title to this report is vested in the Employer named but title to copyright is retained. The Contracts (Rights of Third Parties) Act 1999 does not apply to the contract with the Employer and the provisions of the said Act are hereby excluded.
GNOSALL ST LAWRENCE PRIMARY SCHOOL, GNOSALL, STAFFORD FACTUAL REPORT ON GROUND INVESTIGATION
Unit 4, Gainsborough Trading Estate, Leamington Road, Southam, Warwickshire, CV47 1RA, UK
Tel: +44 (0) 1926 819300 Fax: +44 (0) 1926 815030 email: [email protected]
Report No: D3110-13
Date: November 2013
Employer: Education Funding Agency 33 Greycoat Street London SW1P 2QF
Engineer: Mott MacDonald Ltd 35 Newhall Street Birmingham B3 3PU
November 2013 Report No D3110-13 Issue 2.0 Page 1 of 6
C O N T E N T S
Page 1 INTRODUCTION 2 2 THE SITE AND GEOLOGY 2 2.1 The Site 2.2 Published Geology 3 FIELDWORK 3 3.1 General 3.2 Exploratory Holes 3.3 Instrumentation and Monitoring 4 LABORATORY TESTING 4 4.1 Geotechnical Testing 4.2 Geoenvironmental Testing REFERENCES 6 ENCLOSURES A EXPLORATORY HOLE RECORDS B INSTRUMENTATION AND MONITORING C GEOTECHNICAL LABORATORY TEST RESULTS D GEOENVIRONMENTAL LABORATORY TEST RESULTS E DRAWINGS
November 2013 Report No D3110-13 Issue 2.0 Page 2 of 6
1 INTRODUCTION
In July 2013 Environmental Scientifics Group (ESG) was commissioned by Mott MacDonald Ltd,
on behalf of the Education Funding Authority, to carry out a ground investigation at Gnosall St
Lawrence Primary School, Lowfield Lane, Gnosall, Stafford. The investigation was required to
obtain preliminary geotechnical and geoenvironmental information to assist in the planning and
design of new development at the school as part of the Priority Schools Building Programme.
The scope of the investigation, which was specified by Mott MacDonald Ltd, comprised cable
percussion boreholes, windowless sampler boreholes and laboratory testing. The investigation
was carried out in accordance with the contract specification, Eurocode 7 and relevant related
standards identified below (see also References). The fieldwork was carried out between the 5th
and 7th August 2013.
This report presents the factual records of the fieldwork and laboratory testing undertaken. The
data is also presented separately in digital format following AGS (2005).
2 THE SITE AND GEOLOGY
2.1 The Site
Gnosall St Lawrence Primary School lies on the southern edge of Gnosall , see Site Location Plan
in Enclosure E, about 9km south east of Stafford. The site is at National Grid reference SJ 831
205.
The school grounds are roughly triangular in shape, bounded by Lowfield Lane on the north
eastern side. The A518 Stafford Road lies just to the north west together with an existing garage
and open land. A small wooded area lies at the south western boundary with a disused and
dismantled railway line on its southern side and open agricultural land beyond.
The existing school buildings lie at the northern end of the grounds, fronting onto Lowfield Lane,
with grassed playing fields to the south.
November 2013 Report No D3110-13 Issue 2.0 Page 3 of 6
2.2 Published Geology
Published geological information covering the area, Geological Survey (GS) Sheet 139 'Stafford'
and the British Geological Survey (BGS) website, show superficial Glaciofluvial Sheet Deposits
underlying much of the site with Alluvium indicated along the south western side and Glacial Till to
the north east. Triassic age strata are the underlying bedrock with the Mercia Mudstone Group
shown beneath the north and east with the Bromsgrove Sandstone to the south west.
3 FIELDWORK
3.1 General
The fieldwork was carried out in general accordance with BS 5930+A2 (2010), BS EN 1997-2
(2007) and BS EN ISO 22475-1 (2006).
The exploratory hole locations were selected by Mott MacDonald Ltd and set out from local
features. The co-ordinates and reduced levels were surveyed by ESG to National Grid and
Ordnance Datum. The exploratory hole locations are shown on the Site Plan in Enclosure E.
3.2 Exploratory Holes
The exploratory holes are listed in the following table.
SUMMARY OF EXPLORATORY HOLES
TYPE QUANTITY MAXIMUM DEPTH (m) REMARKS
Cable Percussion Boring 5 6.40 BH1, BH2, BH3, BH4 and BH5
Windowless Sampler Boreholes 5 5.45 WS1, WS2, WS3, WS4 and WS5
The exploratory hole records are presented in Enclosure A and should be read in conjunction with
the Key which is included in that enclosure. The records provide descriptions of the materials
encountered in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003), for soils and
rocks respectively, as amplified by BS 5930+A2 (2010). The records also give details of the
samples taken together with observations made during boring, windowless sampling and pitting.
Standard penetration tests (SPT) were carried out in accordance with BS EN ISO 22476-
3:2005+A1 (2011) in the boreholes and windowless sampler holes and the results are included on
November 2013 Report No D3110-13 Issue 2.0 Page 4 of 6
the exploratory hole records. The SPT hammer energy ratio calibration certificates are also
included in Enclosure A.
On completion of the fieldwork geotechnical samples were transported to the Southam office of
ESG for temporary retention, with those required for testing being transferred to the in-house
Doncaster laboratory. Geoenvironmental samples were taken and stored in accordance with Mott
MacDonald Ltd requirements and BS EN ISO/IEC 17025 (2005) prior to and during transport to the
ESG Scientifics' Burton-on Trent laboratory.
3.3 Instrumentation and Monitoring
The instruments installed in the exploratory holes are shown on the logs and detailed in
Enclosure B. Records of groundwater and gas monitoring carried out by ESG after the fieldwork
period are presented in Enclosure B.
4 LABORATORY TESTING
4.1 Geotechnical Testing
The testing was scheduled by Mott MacDonald Ltd and was carried out in accordance with
BS 1377 (1990) unless otherwise stated. The testing is summarised below and the results are
presented in Enclosure C.
SUMMARY OF GEOTECHNICAL LABORATORY TESTING
TYPE REMARKS
Moisture Content Determination
Atterberg Limit Determination
Particle Size Distribution Analysis
Total Sulphate Content, Water Soluble Sulphate Content, Total Sulphur Content and pH Value of Soils
Testing by ESG Scientifics; test methods are BS 1377 or others recognised in BRE Special Digest 1 (2005); they are indicated on the results report sheets in Enclosure C
Organic Matter Content
Dry Density/Moisture Content Relationship (Light 2.5g compaction)
Moisture Condition Value/Moisture Content Relationship
California Bearing Ratio
November 2013 Report No D3110-13 Issue 2.0 Page 6 of 6
REFERENCES
AGS : 2005 : Electronic transfer of geotechnical and geoenvironmental data (Edition 3.1 including addendum May 2005). Association of Geotechnical and Geoenvironmental Specialists.
Baldwin M, Gosling R C and Brownlie N : 2007 : Soil and rock descriptions - a practical guide to the implementation of BS EN ISO 14688 and 14689. Ground Engineering, July.
BRE Special Digest 1 : 2005 : Concrete in aggressive ground. Building Research Establishment.
BS 1377 : 1990 : Methods of test for soils for civil engineering purposes. British Standards Institution.
BS 5930+A2 : 2010 : Code of practice for site investigations (Amendment 2). British Standards Institution.
BS EN 1997-2 : 2007 : Eurocode 7 - Geotechnical design - Part 2 Ground investigation and testing. British Standards Institution.
BS EN ISO 14688-1 : 2002 : Geotechnical investigation and testing - Identification and classification of soil - Part 1 Identification and description. British Standards Institution.
BS EN ISO 14689-1 : 2003 : Geotechnical investigation and testing - Identification and classification of rock - Part 1 Identification and description. British Standards Institution.
BS EN ISO 22475-1 : 2006 : Geotechnical investigation and testing – Sampling methods and groundwater measurements - Part 1 Technical principles for execution. British Standards Institution.
BS EN ISO 22476-3:2005+A1 : 2011 : Geotechnical investigation and testing - Field testing - Part 3 Standard penetration test. British Standards Institution.
BS EN ISO/IEC 17025 : 2005 : General requirements for the competence of testing and calibration laboratories. British Standards Institution.
GIFA10 : 2010 : Ground Investigation Services Framework Agreement. Mott Macdonald Ltd.
GS England and Wales Sheet 139 : 1950 : Stafford. 1:633600 geological map (solid and drift). Geological Survey of England and Wales
November 2013 Report No D3110-13 Issue 2.0 Enclosure A
ENCLOSURE A
EXPLORATORY HOLE RECORDS
Key to Exploratory Hole Records Key
Hammer Energy Ratio Report Calibration certificates for JH1 and 120 38BH
Borehole Logs BH1, BH2, BH3, BH4 and BH5
Windowless Sampler Logs WS1, WS2, WS3, WS4 and WS5
Notes: See report text for full references of standards
Project
Project No. Carried out for
GNOSALL ST LAWRENCE PRIMARY SCHOOL
D3110-13 Education Funding Agency
Key Sheet 1 of 2
Key to Exploratory Hole Records
SAMPLES Undisturbed U UT TW P L CBR BLK CS AMAL
Driven tube sample Driven thin wall tube sample nominally 100 mm diameter and full recovery unless otherwise stated Pushed thin wall tube sample Pushed piston sample Liner sample (from Windowless or similar sampler), full recovery unless otherwise stated CBR mould sample Block sample Core sample (from rotary core) taken for laboratory testing Amalgamated sample
Disturbed D B
Small sample Bulk sample
Other W G ES EW
Water sample Gas sample Environmental chemistry samples (in more than one container where appropriate) Soil sample Water sample
Comments Sample reference numbers are assigned to every sample taken. A sample reference of 'NR' indicates that attempt was made to take a tube sample, however, there was no recovery. Monitoring samples taken after completion of hole construction are not shown on the exploratory hole logs.
TESTS SPT S or SPT C IV HV PP KFH, KRH, KPI
Standard Penetration Test, open shoe (S) or solid cone (C) The Standard Penetration Test is defined in BS EN ISO 22476-3 (2005). The incremental blow counts are given in the Field Records column; each increment is 75 mm unless stated otherwise and any penetration under self weight in mm (SW) is noted. Where the full 300 mm test drive is achieved the total number of blows for the test drive is presented as N = ** in the Test column. Where the test drive blows reach 50 the total blow count beyond the seating drive is given (without the N = prefix). in situ Vane shear strength, peak (p) and remoulded (r) Hand vane shear strength, peak (p) and remoulded (r) Pocket penetrometer test, converted to shear strength Permeability tests (KFH = falling head, KRH = rising head; KPI = packer inflow); results provided in Field Records column (one value per stage for packer tests)
DRILLING RECORDS The mechanical indices (TCR/SCR/RQD & If) are defined in BS 5930+A2 (2010)
TCR SCR RQD If
Total Core Recovery, % Solid Core Recovery, % Rock Quality Designation, % Fracture spacing, mm. Minimum, typical and maximum spacings are presented. The term non-intact (NI) is used where the core is fragmented.
Flush returns, estimated percentage with colour where relevant, are given in the Records column CRF AZCL NR
Core recovered (length in m) in the following run Assessed zone of core loss Not recovered
GROUNDWATER
Groundwater strike Groundwater level after standing period
Notes: See report text for full references of standards
Project
Project No. Carried out for
GNOSALL ST LAWRENCE PRIMARY SCHOOL
D3110-13 Education Funding Agency
Key Sheet 2 of 2
Key to Exploratory Hole Records
INSTALLATION Standpipe/ piezometer SP SPIE PPIE EPIE Inclinometer or Slip Indicator ICE ICM SLIP Settlement Points or Pressure Cells ESET ETM EPCE PPCE
Details of standpipe/piezometer installations are given on the Record. Legend column shows installed instrument depths including slotted pipe section or tip depth, response zone filter material type and layers of backfill. The type of instrument installed is indicated by a code in the Legend column at the depth of the response zone: Standpipe Standpipe piezometer Pneumatic piezometer Electronic piezometer The installation of vertical profiling instruments is indicated on the Record. The base of tubing is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column at the base of the tubing: Biaxial inclinometer Inclinometer tubing for use with probe Slip indicator The installation of single point instruments is indicated on the Record. The location of the measuring device is shown in the Legend column. The type of instrument installed is indicated by a code in the Legend column: Electronic settlement cell/gauge Magnetic extensometer settlement point Electronic embedment pressure cell Electronic push in pressure cell
INSTALLATION LEGENDS
A legend describing the installation is shown in the rightmost column. Legends additional to BS5930 are used to describe the backfill materials as indicated below.
Arisings
Concrete
Grout
Bentonite
Sand
Gravel
Macadam
NOTES 1 2 3 4 5 6 7 8
Soils and rocks are described in accordance with BS EN ISO 14688-1 (2002) and 14689-1 (2003) respectively as amplified by BS 5930+A2 (2010). For fine soils, consistency determined during description is reported for those strata where undisturbed samples are available. Where the logger considers that the sample may not be representative of the condition in situ, for whatever reason, the reported consistency is given in brackets. The reliability of the sample is indicated by Probably or Possibly as appropriate. Hence (Probably firm) indicates the logger is reasonably confident of the assessment, but (Possibly firm) means less certainty. Where the samples available are too disturbed to allow a reasonable assessment of the in situ condition, no consistency is given. Evidence of the occurrence of very coarse particles (cobbles and boulders) is presented on the logs, however, because of their size in relation to the exploratory hole these records may not be fully representative of their size and frequency in the ground mass. The declination of bedding and joints is given with respect to the normal to the core axis. Thus in a vertical borehole this will be the dip. The assessment of SCR, RQD and Fracture Spacing excludes artificial fractures Strata legends are in accordance with BS 5930+A2 (2010). Water level observations of discernible entries during the advancing of the exploratory hole are given at the foot of the log and in the Legend column. The term "none observed" is used where no discrete entries are identified although this does not necessarily indicate that the hole has not been advanced below groundwater level. Under certain conditions groundwater cannot be observed, for instance, drilling with water flush or overwater, or boring at a rate much faster than water can make its way into the borehole (ref BS5930+A2:2010, Clause 47.2.7). In addition, where appropriate, water levels in the hole at the time of recovering individual samples or carrying out in situ tests and at shift changes are given in the Records column. The borehole logs present the results of Standard Penetration Tests recorded in the field without correction or interpretation. However, in certain ground conditions (eg high hydraulic head or where very coarse particles are present) some judgement may be necessary in considering whether the results are representative of in situ mass conditions.
Updated March 2012
SPT Hammer Energy Test Reportin accordance with BSEN ISO 22476-3:2005
JHl.spt
TPTest Operator:
SPT Hammer Ref: JH1
Test Date: 26/07/2012
Report Date:
File Name:
Dynamic sampling uk ltdunit 2 new zealand courtkingsway park dosekingsway ind parkderbyDE223FP
Instrumented Rod DataDiameter dr (mm):
Wall Thickness tr (mm):
Assumed Modulus Ea (GPa):
Accelerometer NO.1:
Accelerometer NO.2:
54
6.9200
6455
6457
SPT Hammer InformationHammer Mass m (kg): 63.5
Falling Height h (mm): 750
SPT String Length L (m): 15.0
Comments I LocationHammer tested at Dynamic sampling yard.
Velocity
Displacement
2 3 4 5 6 7 8 9 10Time (ms)
2 3 4 5 6 7 8 9 10Time (ms)
Force5
4
u3CD.!!2E
1
0
2 3 4 5 6 7 8 9 10 0
Time (ms)
Acceleration
0
-2
EE-4
-6
-82 3 4 5 6 7 8 9 10 0
Time (ms)o
20,000
15,000
~ 10,000
~ 5,000o
-5,000
250
200
150
~ 100
50o
-soo
CalculationsArea of Rod A (mm2): 1021
Theoretical Energy ~heor (J): 473
Measured Energy Emeas (J): 413
Energy Ratio Er (%): ~,[ _87 IT.parker
operations manager
SPTMAN ver.1.92 All rights reserved, Testconsult@2010
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
JHGMJRL
07/08/2013
07/08/2013
Type & No
Type & No
Pilcon 1500Service inspection pit hand excavated to 1.20mCable percussion to 5.00m
Records
Records
426.4818/11/2013 10:58:10(c) ESG www.esg.co.uk
GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
BH1Sheet 1 of 1
+104.25 mODE 383110.63N 320661.83
1.20 4.70 SPT hammer ID JH1
5.00m0.00m 150mm 4.50m
4.40 -4.70 60 mins
*
4.00-4.40 mDense to very
dense
0.100.10-0.50
0.30
0.600.60
0.80-1.20
1.101.20-1.651.20-1.65
1.902.00-2.45
2.002.00-2.45
2.60
3.00-3.453.00
3.00-3.45
3.904.00-4.454.00-4.454.00-4.50
4.70-4.984.70-4.97
D 1B 3
ES 2
D 4ES 5B 6
ES 7SPT C
B 8
ES 9SPT CD 10B 11
D 12
SPT CES 13B 14
D 15SPT SD 16B 17
SPT SD 18
N=8 (1,1/2,1,2,3)
N=11 (1,2/2,2,3,4)
N=9 (1,2/3,2,2,2)
N=50 (2,3/7,9,15,19)
50 (9,12/21,29 for 50mm)
1.20
1.50
3.00
4.00
4.50
dry
dry
dry
dry
dry
0.05
0.50
2.50
4.40
5.00
(0.45)
(2.00)
(1.90)
(0.60)
+104.20
+103.75
+101.75
+99.85
+99.25SP
MADE GROUND: macadam.
MADE GROUND: black sandy GRAVEL with lowcobble content. Gravel is angular fine tocoarse macadam, sandstone and clinker.Cobbles are sandstone and brick.
MADE GROUND: loose to medium dense brownclayey very gravelly fine to coarse SANDwith low cobble content. Gravel isrounded to angular fine to coarsequartzite, slag, sandstone and rare brick.Cobbles are brick.
Loose to medium dense, becoming dense tovery dense, light brown gravelly fine tomedium SAND with rare soft reddish brownsandy clay pockets. Gravel is angular torounded sandstone, quartzite and raremudstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Extremely weak light reddish brown finegrained SANDSTONE. Recovered as sand andgravel.(BROMSGROVE SANDSTONE FORMATION)
EXPLORATORY HOLE ENDS AT 5.00 m
sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Stiff brown slightly sandy slightlygravelly CLAY with rare silt pockets.Gravel is angular to rounded fine tomedium quartzite and sandstone.(Possible GLACIAL TILL)
Extremely weak to very weak light greyishbrown fine grained SANDSTONE.(BROMSGROVE SANDSTONE FORMATION)
EXPLORATORY HOLE ENDS AT 5.50 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
JHGMJRL
07/08/2013
07/08/2013
Type & No
Type & No
Pilcon 1500Service inspection pit hand excavated to 1.20mCable percussion to 5.50m
Records
Records
426.4818/11/2013 10:58:16(c) ESG www.esg.co.uk
GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
BH2Sheet 1 of 1
+102.14 mODE 383082.68N 320603.89
1.20 5.40 SPT hammer ID JH1
5.50m0.00m 150mm 5.00m
5.30 -5.43 60 mins
*
0.100.15
0.20-0.700.300.50
0.90-1.201.00
1.20-1.651.20
1.20-1.65
2.002.10-2.552.10-2.55
2.903.00-3.453.00-3.45
3.90
4.10-4.554.10-4.55
4.905.00-5.385.00-5.355.00-5.305.40-5.50
5.405.40-5.49
D 1ES 2B 5D 3
ES 4
B 8D 6
SPT CES 7B 9
D 10SPT CB 11
D 12SPT CB 13
D 14
SPT CB 15
D 16SPT SD 17B 18
SPT CD 19B 20
N=18 (2,3/3,4,5,6)
N=19 (2,3/5,5,4,5)
N=13 (1,2/2,3,4,4)
N=20 (8,7/5,4,5,6)
50 (4,5/8,9,33)
50 (25 for 50mm/50 for 45mm)
1.20
1.70
3.00
4.00
5.00
5.00
dry
dry
dry
dry
dry
dry
0.050.20
0.90
1.40
4.80
5.30
5.50
(0.70)
(0.50)
(3.40)
(0.50)
+102.09+101.94
+101.24
+100.74
+97.34
+96.84
+96.64SP
MADE GROUND: macadam.
MADE GROUND: black sandy GRAVEL of ashand macadam.
Brown SAND and GRAVEL with low cobblecontent and rare reddish brown sandy claypockets. Sand is medium to coarse. Gravelis subangular to rounded fine to coarsesandstone and quartzite. Cobbles arequartzite.(GLACIOFLUVIAL SHEET DEPOSITS)
Brown silty gravelly fine to coarse SAND.Gravel is subangular to rounded fine tomedium sandstone and quartzite.(GLACIOFLUVIAL SHEET DEPOSITS)
Medium dense brown very sandy GRAVEL withlow cobble content and rare firm reddishbrown sandy clay pockets. Gravel issubangular to rounded fine to coarsequartzite and sandstone. Cobbles are
TOPSOIL.
Brown slightly silty gravelly fine tomedium SAND. Gravel is subangular torounded fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Firm, becoming soft to firm, reddish brownslightly sandy slightly gravelly CLAYwith rare light grey very sandy clay andblack silt pockets. Gravel is rounded tosubrounded fine to medium sandstone andquartzite.(GLACIOFLUVIAL SHEET DEPOSITS)
Loose brown slightly clayey slightlygravelly medium SAND. Gravel is subangularto rounded fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Firm brown slightly gravelly sandy CLAY.Gravel is angular to subangular finequartzite, sandstone and mudstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Medium dense brown silty very sandy GRAVELwith low cobble content. Gravel isrounded fine to coarse quartzite andsandstone. Cobbles are sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Extremely weak to very weak reddish brownsilty fine to medium grained SANDSTONE.Recovered as subangular fine to coarsegravel.(BROMSGROVE SANDSTONE FORMATION)
EXPLORATORY HOLE ENDS AT 6.40 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole LogJHGMJRL
06/08/2013
06/08/2013
Type & No
Type & No
Pilcon 1500Service inspection pit hand excavated to 1.20mCable percussion to 6.40m
Records
Records
426.4818/11/2013 10:58:20(c) ESG www.esg.co.uk
GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
BH3Sheet 1 of 1
+98.17 mODE 383046.90N 320562.72
0.601 Seepage -1.702 Rose to 1.40 m after 20 minutes. Slow -
1.20 6.20 SPT hammer ID JH1
6.40m0.00m 150mm 5.80m
5.80 -6.20 60 mins
*1.30-1.60 m
Becoming soft tofirm.
4.10-4.50 m Sandis fine to medium.
0.000.000.200.300.30
0.70
0.90
1.20-1.651.201.20
1.70
2.00-2.452.00
2.80
3.00-3.453.003.00
4.004.10-4.55
4.104.10
4.80
5.00-5.455.00
5.80-6.125.80
6.20-6.40
EW 19EW 20
B 3D 1
ES 2
ES 4
D 5
SPT SES 6D 7
D 8
SPT CB 9
D 10
SPT SD 11B 12
D 13SPT SD 14B 15
D 16
SPT CB 17
SPT CD 18
SPT C
N=11 (1,2/3,2,3,3)
N=9 (1,1/2,2,3,2)
N=12 (1,2/2,3,4,3)
N=16 (3,4/4,5,3,4)
N=17 (2,3/3,4,5,5)
50 (10,12/18,23,9 for 20mm)
50 (9,16 for 35mm/40,10 for 15mm)
1.20
2.00
3.00
4.00
4.50
5.80
5.80
damp
1.80
damp
damp
dry
dry
dry
0.20
0.80
1.60
2.70
4.50
5.70
6.40
(0.60)
(0.80)
(1.10)
(1.80)
(1.20)
(0.70)
+97.97
+97.37
+96.57
+95.47
+93.67
+92.47
+91.77
1
2
2
SP
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
JHGMJRL
05/08/2013
05/08/2013
Type & No
Type & No
Pilcon 1500Service inspection pit hand excavated to 1.20mCable percussion to 4.00m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
BH4Sheet 1 of 1
+99.66 mODE 383189.91N 320505.55
1.20 3.90 SPT hammer ID JH1
4.00m0.00m 150mm 3.80m
3.60 -3.90 60 mins
*
0.000.200.20
0.20-0.600.500.70
0.80-1.20
1.00
1.20-1.651.20-1.65
1.902.00-2.45
2.002.00-2.40
2.70
3.00-3.453.00
3.00-3.453.00-3.50
3.60-3.743.60
3.60-3.733.90-4.00
3.90
EW 19D 1
ES 2B 3
ES 4D 5B 6
ES 7
SPT CB 8
ES 9SPT CD 10B 11
D 12
SPT SES 13D 14B 15
SPT SD 16D 17
SPT CD 18
N=6 (1,1/1,1,2,2)
N=7 (1,1/1,1,2,3)
N=21 (2,3/3,5,6,7)
50 (19,6 for 10mm/50 for 50mm)
50 (25 for 60mm/50 for 40mm)
1.20
2.00
3.00
3.80
3.80
dry
dry
damp
damp
damp
0.15
0.60
2.20
3.50
4.00
(0.45)
(1.60)
(1.30)
(0.50)
+99.51
+99.06
+97.46
+96.16
+95.66
SP
TOPSOIL.
MADE GROUND: brown and black gravelly fineto coarse SAND. Gravel is angular torounded fine to coarse clinker, slag,quartzite and sandstone.
MADE GROUND: loose light brown slightlysilty very gravelly fine to medium SAND.Gravel is subangular to rounded fine tocoarse predominantly quartzite andsandstone with rare clinker, slag andbrick.
Medium dense brown clayey gravelly fine tomedium SAND with low cobble content.Gravel is subrounded to rounded fine tomedium sandstone and rare quartzite.Cobbles are sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Extremely weak to very weak brown finegrained SANDSTONE.(BROMSGROVE SANDSTONE FORMATION)
EXPLORATORY HOLE ENDS AT 4.00 m
1:50
Firm to stiff brown slightly gravellysandy CLAY. Gravel is subangular torounded fine to medium sandstone.(Possible GLACIAL TILL)
Dense to very dense brown gravellypredominantly fine to medium SAND withfrequent clay pockets. Gravel issubangular fine to coarse sandstone.(Possible BROMSGROVE SANDSTONEFORMATION)
Extremely weak brown fine grainedSANDSTONE. Recovered as angular tosubangular fine to coarse gravel.(BROMSGROVE SANDSTONE FORMATION)
EXPLORATORY HOLE ENDS AT 6.20 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Borehole Log
None observed (see Key Sheet)
JHGMJRL
06/08/2013
06/08/2013
Type & No
Type & No
Pilcon 1500Service inspection pit hand excavated to 1.20mCable percusson to 6.20m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
BH5Sheet 1 of 1
+99.18 mODE 383248.49N 320428.97
1.20 6.00 SPT hammer ID JH1
6.20m0.00m 150mm 6.00m
5.50 -6.05 60 mins
*
0.200.20
0.20-0.600.50
0.90
1.101.20-1.651.20-1.651.20-1.70
2.00
2.20-2.652.20-2.65
3.00-3.453.00
3.00-3.45
3.70
4.00-4.454.00-4.454.00-4.50
4.80
5.00-5.455.00-5.455.00-5.50
6.00-6.226.00
D 1ES 2B 3
ES 4
D 5
ES 6SPT S
D 7B 8
D 9
SPT CB 10
SPT CD 11B 12
D 13
SPT SD 14B 15
D 16
SPT SD 17B 18
SPT CD 19
N=19 (2,4/4,5,6,4)
N=9 (1,1/1,2,2,4)
N=15 (1,2/2,4,4,5)
N=16 (2,2/3,4,4,5)
N=50 (3,4/6,10,13,21)
50 (9,16 for 55mm/39,11 for 15mm)
1.20
1.50
3.00
4.00
4.50
6.00
dry
damp
damp
dry
dry
dry
0.15
0.80
1.20
3.30
4.70
5.40
6.22
(0.65)
(0.40)
(2.10)
(1.40)
(0.70)
(0.82)
+99.03
+98.38
+97.98
+95.88
+94.48
+93.78
+92.96 SP
TOPSOIL.
MADE GROUND: brown slightly gravelly sandyCLAY with low cobble content. Gravel isangular to rounded fine to coarsesandstone and quartzite. Cobbles arelimestone.
MADE GROUND: firm brown mottled greyishbrown slightly gravelly sandy CLAY. Sandis fine. Gravel is subangular fine tomedium quartzite and rare slag. Rare blacksilt pockets.
Loose to medium dense brown slightly siltygravelly fine to medium SAND with raresandy clay pockets. Gravel is subangularto subrounded fine to coarse predominantlyquartzite with rare sandstone andmudstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MPGMJRL
05/08/2013
05/08/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 3.80mRefusal at 3.80m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
WS1Sheet 1 of 1
+103.89 mODE 383097.88N 320646.63
1.20 3.80 SPT hammer ID 120 38BH
*
3.80 m Verydense, possible
bedrock
0.100.20-0.50
0.30
0.50-1.000.60
1.20-1.651.20-2.00
1.50
2.00-2.452.00-3.00
2.50
3.00-3.453.00-3.80
3.80-3.81
ES 1B 3
ES 2
B 5ES 4
SPT SB 7
D 6
SPT SB 9
D 8
SPT SB 10
SPT S
N=8 (2,2/2,2,2,2)
N=14 (3,4/4,3,3,4)
N=20 (4,4/5,5,5,5)
(50 for 10mm)
0.080.20
2.00
3.80
(1.80)
(1.80)
+103.81+103.69
+101.89
+100.09
MADE GROUND: macadam.
MADE GROUND: black and brown sandyGRAVEL. Sand is fine to coarse. Gravel isangular fine to coarse sandstone, macadam andrare slag.
Loose brown silty very gravelly fine tocoarse SAND with rare firm sandy claypockets. Gravel is subangular to roundedfine to coarse sandstone, quartzite andrare mudstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Medium dense brown slightly silty gravellyfine to medium SAND. Gravel is subangularto rounded medium to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
EXPLORATORY HOLE ENDS AT 3.80 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MPGMJRL
05/08/2013
05/08/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 3.60mRefusal at 3.60m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
WS2Sheet 1 of 1
+104.20 mODE 383120.43N 320614.13
1.20 3.60 SPT hammer ID 120 38BH
*
3.30-3.38 mReddish brown
mottled lightgreenish grey
slightly gravellysandy clay
band/pocket
0.100.20-0.60
0.30
0.60-1.000.70
1.20-1.651.20
1.70
2.00-2.452.00-3.00
2.50
3.00-3.45
3.30
3.503.60-4.00
ES 1B 3
ES 2
B 5ES 4
SPT SES 6
D 7
SPT SB 9
D 8
SPT S
D 10
D 11SPT S
N=8 (2,2/2,2,2,2)
N=18 (3,3/4,4,5,5)
N=12 (2,2/2,2,3,5)
50 (8,8/13,13,14,10 for 20mm)
0.080.20
3.60
(3.40)
+104.12+104.00
+100.60
MADE GROUND: macadam.
MADE GROUND: dark brown and black slightlysandy GRAVEL of angular fine to coarsemacadam and sandstone.
Loose becoming medium dense brown slightlysilty very gravelly fine to coarse SANDwith occasional slightly sandy gravellyclay bands/pockets and rare black siltpockets. Gravel is subangular tosubrounded fine to coarse quartzite,sandstone and rare mudstone.(GLACIOFLUVIAL SHEET DEPOSITS)
EXPLORATORY HOLE ENDS AT 3.60 m
1:50
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole LogMPGMJRL
05/08/2013
05/08/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
WS3Sheet 1 of 1
+101.17 mODE 383046.73N 320587.04
3.001 Rose to 2.60 m after 20 minutes. -1.20 5.00 SPT hammer ID 120 38BH
*
0.200.20-0.70
0.300.50
0.800.901.00
1.20-1.65
1.50
1.80
2.00-2.45
2.50
3.00-3.45
3.20
3.50
4.00-4.45
4.20
4.80
5.00-5.45
ES 1B 4D 2
ES 3
ES 5D 6
ES 7
SPT S
D 8
D 9
SPT S
ES 10
SPT S
D 11
D 12
SPT S
D 13
D 14
SPT S
N=9 (1,2/2,3,2,2)
N=7 (1,1/1,1,2,3)
N=11 (2,2/2,2,3,4)
N=19 (1,1/4,5,5,5)
N=20 (5,5/5,5,5,5)
0.12
0.75
1.85
2.20
3.45
4.00
5.00
(0.63)
(1.10)
(0.35)
(1.25)
(0.55)
(1.00)
+101.05
+100.42
+99.32
+98.97
+97.72
+97.17
+96.17
1
1
Soft dark brown slightly sandy silty CLAY.Frequent rootlets. (TOPSOIL)
MADE GROUND: soft dark brown slightlysandy gravelly CLAY with medium cobblecontent. Sand is fine to coarse. Gravel isangular to rounded fine to coarsequartzite, brick, concrete, slag, slateand asbestos corrugated roof fragments.Cobbles are angular concrete and brick.
MADE GROUND: loose light brown gravellymedium to coarse SAND with low cobblecontent. Gravel is fine to coarsequartzite and rare brick, concrete andcoal. Cobble is brick.
Firm greyish brown slightly gravelly sandyCLAY. Gravel is fine to coarse subangularto rounded quartzite.(GLACIOFLUVIAL SHEET DEPOSITS)
Loose to medium dense brown slightly siltyslightly gravelly medium SAND. Gravel isangular to rounded fine to coarsequartzite and sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Firm brown slightly sandy slightlygravelly to gravelly CLAY. Sand is fine tomedium. Gravel is subangular to roundedfine to coarse quartzite and sandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Medium dense brown slightly clayeygravelly medium SAND. Gravel is roundedfine to medium quartzite. (GLACIOFLUVIALSHEET DEPOSITS)
EXPLORATORY HOLE ENDS AT 5.00 m
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole LogMPGMJRL
05/08/2013
05/08/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 5.00m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
WS4Sheet 1 of 1
+101.58 mODE 383075.06N 320571.21
4.501 - -1.20 5.00 SPT hammer ID 120 38BH
*
3.40-3.48 m Firmreddish brown
slightly gravellysandy clay
0.100.20
0.400.50
0.50-1.00
1.20-1.65
1.50
2.00-2.452.00-3.00
2.50
3.00-3.453.00-4.00
3.403.50
4.00-4.45
4.50
5.00-5.45
D 1ES 2
D 3ES 4B 5
SPT S
ES 6
SPT SB 8
D 7
SPT SB 10
D 12D 9
SPT S
D 11
SPT S
N=6 (1,2/1,2,1,2)
N=10 (1,2/3,2,3,2)
N=17 (4,4/5,4,4,4)
N=6 (3,2/2,2,1,1)
N=8 (2,1/2,2,2,2)
0.30
5.00
(0.30)
(4.70)
+101.28
+96.58
1
Soft dark brown slightly gravelly sandyCLAY. Sand is predominantly fine tomedium. Gravel is subangular to roundedfine to medium quartzite. Frequentrootlets. (TOPSOIL)
Loose to medium dense brown silty verygravelly fine to coarse SAND withoccasional slightly gravelly sandy claypockets/bands. Gravel is angular torounded fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
EXPLORATORY HOLE ENDS AT 5.00 m
1:50
Time Tools usedFrom to (m)
Checked
Equipment, Methods and Remarks
Backfill/
Coordinates
ChisellingDepths (m)
Samples and Tests
Project
to
No. Post strike behaviour Depth sealed
Project No.Carried out for
Diameter Casing Depth
StrataDepth Date Time Depth,Level Legend
Start
End
(Thickness)Casing Water
Groundwater EntriesStruck
Notes: For explanation of symbols and
Instruments
(m)
abbreviations see key sheet. All depths and reducedlevels in metres. Stratum thickness given in bracketsin depth column.
Description
Depth from
Borehole
Scale
Depth Related Remarks *
Drilled
Depth DateCasing
Time
(m)
Ground Level
Water
Logged
Window Sampler Hole Log
None observed (see Key Sheet)
MPGMJRL
05/08/2013
05/08/2013
Type & No
Type & No
Service inspection pit hand excavated to 1.20mWindowless sampler to 3.50m
Records
Records
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GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13Education Funding Agency
National Grid
Chainage
WS5Sheet 1 of 1
+104.22 mODE 383162.73N 320576.99
1.20 3.50 SPT hammer ID 120 38BH
*
3.50 m Refusal,possible bedrock
0.00-0.080.08-0.22
0.40
0.600.60-1.00
1.20-1.651.20
1.902.00-2.45
2.50
2.903.00-3.45
3.50-3.513.50
B 1B 2
D 3
ES 4B 5
SPT SES 6
D 7SPT S
ES 8
D 9SPT S
SPT SD 10
N=6 (1,1/2,2,1,1)
N=19 (3,4/4,5,5,5)
N=9 (3,3/3,2,2,2)
(50 for 10mm)
0.080.22
0.60
1.80
3.20
3.50
(0.38)
(1.20)
(1.40)
(0.30)
+104.14+104.00
+103.62
+102.42
+101.02
+100.72
MADE GROUND: macadam.
MADE GROUND: black slightly sandy GRAVELof angular fine to medium sandstone,concrete and macadam.
MADE GROUND: brown very clayey slightlygravelly fine to medium SAND with highcobble content. Gravel is angular fine tocoarse brick fragments and roundedquartzite. Cobbles are brick and concrete.
MADE GROUND: loose brown slightly gravellyfine to medium SAND with rare firmreddish brown clay pockets. Gravel isrounded fine to coarse sandstone andquartzite with rare brick and concrete.
Medium dense light brown slightly gravellyto gravelly predominantly medium SAND.Gravel is fine to coarse quartzite andsandstone.(GLACIOFLUVIAL SHEET DEPOSITS)
Stiff reddish brown slightly sandyslightly gravelly CLAY. Gravel is roundedfine to coarse quartzite and sandstone.(Possible GLACIAL TILL)
EXPLORATORY HOLE ENDS AT 3.50 m
1:50
November 2013 Report No D3110-13 Issue 2.0 Enclosure B
ENCLOSURE B
INSTRUMENTATION AND MONITORING
Installation Details B1
Groundwater Monitoring B2
Gas Monitoring
Hol
e N
o
Inst
rum
ent I
D
Inst
alla
tion
Typ
e
Dat
e of
Inst
alla
tion
Ref
eren
ce d
epth
(m
BG
L)
Pie
zom
eter
D
iam
eter
(m
m)
Top
of r
espo
nse
zone
(m
BG
L)
Bas
e of
res
pons
e zo
ne (
mB
GL)
Tub
ing
Com
plet
ion
Det
ails
Hea
dwor
ks Remarks
BH1 SP 7 Aug 2013 0.00 50 2.50 5.00 Gas tap Stop cock cover
BH2 SP 7 Aug 2013 0.00 50 0.50 5.50 Gas tap Stop cock cover
BH3 SP 6 Aug 2013 0.00 50 0.50 1.70 Gas tap Stop cock cover
BH4 SP 5 Aug 2013 0.00 50 2.20 4.00 Gas tap Stop cock cover
BH5 SP 6 Aug 2013 0.00 50 1.00 6.20 Gas tap Stop cock cover
Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Electronic Piezometer Prepared: 04/11/2013 06:55
GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13 Education Funding Agency
Project
Project No.Carried out for
B1
Groundwater Installation Details
Sheet 1 of 1
DateTime
(hhmmss)Comments
BH1 SP 4.7 0.00 28 Aug 2013 Dry
BH1 SP 4.7 0.00 19 Sep 2013 Dry
BH1 SP 4.7 0.00 4 Oct 2013 Dry
BH1 SP 4.7 0.00 11 Oct 2013 Dry
BH1 SP 4.7 0.00 17 Oct 2013 Dry
BH1 SP 4.7 0.00 31 Oct 2013 Dry
BH2 SP 5.4 0.00 28 Aug 2013 Dry
BH2 SP 5.4 0.00 19 Sep 2013 Dry
BH2 SP 5.4 0.00 4 Oct 2013 Dry
BH2 SP 5.4 0.00 11 Oct 2013 Dry
BH2 SP 5.4 0.00 17 Oct 2013 Dry
BH2 SP 5.4 0.00 31 Oct 2013 Dry
BH3 SP 1.7 0.00 28 Aug 2013 1.01
BH3 SP 1.7 0.00 19 Sep 2013 0.98
BH3 SP 1.7 0.00 4 Oct 2013 0.86
BH3 SP 1.7 0.00 11 Oct 2013 1.05
BH3 SP 1.7 0.00 17 Oct 2013 0.87
BH3 SP 1.7 0.00 31 Oct 2013 0.78
BH4 SP 4 0.00 28 Aug 2013 Dry
BH4 SP 4 0.00 19 Sep 2013 Dry
BH4 SP 4 0.00 4 Oct 2013 Dry
BH4 SP 4 0.00 11 Oct 2013 3.45
BH4 SP 4 0.00 17 Oct 2013 3.45
BH4 SP 4 0.00 31 Oct 2013 3.20
BH5 SP 6 0.00 28 Aug 2013 Dry
BH5 SP 6 0.00 19 Sep 2013 Dry
BH5 SP 6 0.00 4 Oct 2013 Dry
BH5 SP 6 0.00 11 Oct 2013 Dry
BH5 SP 6 0.00 17 Oct 2013 Dry
BH5 SP 6 0.00 31 Oct 2013 Dry
Reading
Hole ID
Inst
rum
ent
Typ
e
Ref
eren
ce
Dep
th(m
BG
L)
Head(m above Tip)
* calculated
Water Level (mBGL)
* calculated
Inst
rum
ent I
D
Bas
e of
In
stru
men
t(m
BG
L)
Notes: Type: SP - Standpipe, SPIE - Standpipe Piezometer, HPIE - Hydraulic Piezometer, PPIE - Pneumatic Piezometer, EPIE - Vibrating Wire Piezometer, PWEL - Pumping Well
GNOSALL St LAWRENCE PRIMARY SCHOOL
D3110-13 Education Funding Agency
Project
Project No.Carried out for
B2
Groundwater Monitoring
Sheet 1 of 1
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH1Dry 0.0
5.8 0.00.0BH1 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
2.8
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
19.9
0.0
0.20 0.0
2.8
78.5
78.5
78.5
19.9 2.8 0.0
19.9 2.9
0.0 19.8
0.0
2.9 0.00.0 77.2BH3 0.00 00:03:00
77.2
77.2
0.0
0.0
77.2
77.2
77.10.0
0.0
0.0
0.0
78.5
15.6 5.8 0.0
15.6 5.8 0.0
0.0
0.0
DryCalm
CloudyNone
78.778.5
78.5
79.2
78.8
78.8
78.8
78.8
78.8
77.8
19.9
78.8
19.6 2.6 0.0
19.9 2.8 0.0
0.0
0.0
20.6 0.5 0.00.0
20.7 0.5 0.0
20.7 0.4 0.0
0.0
0.0
20.7 0.4 0.0
20.7 0.4 0.0
0.0
0.0
20.1 0.6 0.0
20.7 0.4 0.0
0.0
0.0
0.015.6 5.8 0.0
5.8 0.0
0.0
0.0
5.8 0.0
1003 21
BH1 0.00 00:01:30
0.00 00:00:30
BH1 0.00 00:01:00 0.200.0
0.0
0.0
0.100.0
0.10 0.00.0
BH1 0.00 00:02:00 0.000.0
00:02:30BH1 0.00
BH1 0.00 00:03:00
0.20
0.0
Dry 0.00.00.00 00:00:00
BH2 0.00
BH2 0.00 00:00:30
00:01:30
BH2
1003
0.00
0.10
0.00 00:01:00 0.600.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH2 0.00 00:03:00
0.00
0.00 00:01:30
BH3
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
BH2
BH3
BH3 0.00 00:02:00 0.0
00:00:00
BH2 0.00 00:02:00
00:02:30BH2 0.00
BH3
BH3 0.00 00:01:00
BH3 0.00 00:00:30
0.00
00:02:30
0.001.01
0.0
0.0
0.000.0
0.0
0.0
0.0
0.0
0.0
0.0 15.8
0.0
0.0
0.0
15.6
5.4
15.6
15.7
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
1003
22
19
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
28/08/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH4Dry 0.0
0.0 0.00.0BH4 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
78.4
78.4
78.4
78.4
21.5 0.0 0.0
21.5 0.0 0.0
0.0
0.0
DryCalm
CloudyNone
78.978.3
78.4
78.7
78.4
78.4
78.4
78.3
78.3
78.421.2 0.3 0.00.0
21.2 0.3 0.0
21.2 0.3 0.0
0.0
0.0
21.2 0.4 0.0
21.2 0.3 0.0
0.0
0.0
20.8 0.4 0.0
21.2 0.4 0.0
0.0
0.0
0.021.5 0.0 0.0
0.0 0.0
0.0
0.0
0.0 0.0
1001 18
BH4 0.00 00:01:30
0.00 00:00:30
BH4 0.00 00:01:00 0.000.0
0.0
0.0
0.000.0
0.00 0.00.0
BH4 0.00 00:02:00 0.000.0
00:02:30BH4 0.00
BH4 0.00 00:03:00
0.00
0.0
Dry 0.00.00.00 00:00:00
BH5 0.00
BH5 0.00 00:00:30
00:01:30
BH5
1002
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH5 0.00 00:03:00
BH5
BH5 0.00 00:02:00
00:02:30BH5 0.00 0.0
0.0
0.0
0.0
0.0 21.0
0.0
0.0
0.0
21.5
0.0
21.5
21.6
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
18
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
28/08/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH1Dry 0.0
3.4 0.00.0BH1 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
79.7
79.7
79.7
79.7
16.6 3.6 0.0
16.6 3.6 0.0
0.0
0.0
WetModerate
CloudyHeavy
79.779.7
79.7
78.8
78.8
78.7
78.8
78.7
78.7
78.820.7 0.4 0.00.0
20.7 0.4 0.0
20.7 0.4 0.0
0.0
0.0
20.6 0.6 0.0
20.7 0.5 0.0
0.0
0.0
20.3 0.8 0.0
20.5 0.7 0.0
0.0
0.0
0.016.6 3.6 0.0
3.5 0.0
0.0
0.0
3.5 0.0
997 13
BH1 0.00 00:01:30
0.00 00:00:30
BH1 0.00 00:01:00 0.000.0
0.0
0.0
0.000.0
0.00 0.00.0
BH1 0.00 00:02:00 0.000.0
00:02:30BH1 0.00
BH1 0.00 00:03:00
0.00
0.0
Dry 0.00.00.00 00:00:00
BH2 0.00
BH2 0.00 00:00:30
00:01:30
BH2
997
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH2 0.00 00:03:00
BH2
BH2 0.00 00:02:00
00:02:30BH2 0.00 0.0
0.0
0.0
0.0
0.0 16.9
0.0
0.0
0.0
16.7
3.3
16.7
16.8
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
12
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
19/09/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH4Dry 0.0
0.0 0.00.0BH4 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
2.7
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
19.8
0.0
0.00 0.0
2.7
78.4
78.4
78.4
19.7 2.6 0.0
19.8 2.7
0.0 19.9
0.0
2.7 0.00.0 77.3BH3 0.00 00:03:00
77.9
77.6
0.0
0.0
77.4
77.4
77.40.0
0.0
0.0
0.0
78.4
21.5 0.0 0.0
21.5 0.0 0.0
0.0
0.0
WetModerate
CloudyHeavy
78.778.6
78.4
78.5
78.5
78.6
78.5
78.5
78.6
78.2
19.8
78.6
19.5 2.2 0.0
19.6 2.4 0.0
0.0
0.0
21.1 0.2 0.00.0
21.1 0.3 0.0
21.1 0.3 0.0
0.0
0.0
21.0 0.3 0.0
21.0 0.3 0.0
0.0
0.0
20.9 0.5 0.0
20.9 0.5 0.0
0.0
0.0
0.021.5 0.0 0.0
0.0 0.0
0.0
0.0
0.0 0.0
998 16
BH4 0.00 00:01:30
0.00 00:00:30
BH4 0.00 00:01:00 0.000.0
0.0
0.0
0.000.0
0.00 0.00.0
BH4 0.00 00:02:00 0.000.0
00:02:30BH4 0.00
BH4 0.00 00:03:00
0.00
0.0
Dry 0.00.00.00 00:00:00
BH5 0.00
BH5 0.00 00:00:30
00:01:30
BH5
998
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH5 0.00 00:03:00
0.00
0.00 00:01:30
BH3
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
BH5
BH3
BH3 0.00 00:02:00 0.0
00:00:00
BH5 0.00 00:02:00
00:02:30BH5 0.00
BH3
BH3 0.00 00:01:00
BH3 0.00 00:00:30
0.00
00:02:30
0.000.98
0.0
0.0
0.000.0
0.0
0.0
0.0
0.0
0.0
0.0 21.2
0.0
0.0
0.0
21.5
0.0
21.5
21.3
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
998
15
15
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
19/09/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH4Dry 0.0
0.0 0.00.0BH4 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
3.2
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
19.2
0.0
0.00 0.0
3.3
78.4
78.3
78.2
19.0 3.5 0.0
19.4 3.2
0.0 19.5
0.0
3.1 0.00.0 77.4BH3 0.00 00:02:30
77.4
77.4
0.0
0.0
77.4
77.4
77.40.0
0.0
0.0
0.0
78.2
21.6 0.0 0.0
21.7 0.0 0.0
0.0
0.0
DampLight
CloudyNone
80.178.6
78.2
78.3
77.6
77.6
77.6
77.5
77.5
77.5
19.3
77.6
19.7 2.7 0.0
19.1 3.5 0.0
0.0
0.0
21.2 1.0 0.00.0
21.2 1.1 0.0
21.2 1.1 0.0
0.0
0.0
21.2 1.2 0.0
21.2 1.1 0.0
0.0
0.0
21.2 0.4 0.0
21.2 1.2 0.0
0.0
0.0
0.021.7 0.0 0.0
0.0 0.0
0.0
0.0
0.0 0.0
996
BH4 0.00 00:01:30
0.00 00:00:30
BH4 0.00 00:01:00 0.000.0
0.0
0.0
0.000.0
0.00 0.00.0
BH4 0.00 00:02:00 0.000.0
00:02:00BH4 0.00
BH4 0.00 00:02:30
0.00
0.0
Dry 0.00.00.00 00:00:00
BH5 0.00
BH5 0.00 00:00:30
00:01:30
BH5
996
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH5 0.00 00:02:30
0.00
0.00 00:01:30
BH3
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
BH5
BH3
BH3 0.00 00:02:00 0.0
00:00:00
BH5 0.00 00:02:00
00:02:00BH5 0.00
BH3
BH3 0.00 00:01:00
BH3 0.00 00:00:30
0.00
00:02:00
0.000.86
0.0
0.0
0.000.0
0.0
0.0
0.0
0.0
0.0
0.0 19.8
0.0
0.0
0.0
21.6
0.0
21.5
21.2
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.1
0.0
0.0
0.0
0.0
0.0
0.2
Equipment Used LMSxi 5429 + Dip
996
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
04/10/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH2Dry 0.0
0.3 0.00.0BH2 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
0.00 0.0
78.5
78.5
78.6
78.6
21.3 0.0 0.0
21.3 0.0 0.0
0.0
0.0
DryLight
CloudyNone
78.878.4
78.6
78.8
78.4
78.4
78.4
78.4
78.4
78.521.4 0.0 0.00.0
21.5 0.0 0.0
21.5 0.0 0.0
0.0
0.0
21.5 0.1 0.0
21.5 0.1 0.0
0.0
0.0
21.1 1.5 0.0
21.5 0.3 0.0
0.0
0.0
0.021.3 0.0 0.0
0.1 0.0
0.0
0.0
0.1 0.0
996
BH2 0.00 00:01:30
0.00 00:00:30
BH2 0.00 00:01:00 0.000.0
0.0
0.0
0.000.0
0.00 0.00.0
BH2 0.00 00:02:00 0.000.0
00:02:30BH2 0.00
BH2 0.00 00:03:00
0.00
0.0
Dry 0.00.00.00 00:00:00
BH1 0.00
BH1 0.00 00:00:30
00:01:30
BH1
996
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
BH1 0.00 00:03:00
BH1
BH1 0.00 00:02:00
00:02:30BH1 0.00 0.0
0.0
0.0
0.0
0.0 20.2
0.0
0.0
0.0
21.3
1.5
21.3
21.3
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 5429 + Dip
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
04/10/2013
MQ
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH1Dry 0.0
0.0 0.00.0BH1 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
3.8
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
18.0
0.0
0.00 0.0
3.8
78.5
78.5
78.4
18.0 3.8 0.0
17.9 3.8
0.0 17.9
0.0
3.9 0.00.0 78.2BH3 0.00 00:03:00 0.000.0
78.1
78.1
0.0
0.0
78.1
78.2
78.20.0
0.0
0.0
0.0
78.5
21.4 0.1 0.0
21.2 0.2 0.0
0.0
0.0
WetLight
CloudyNone
78.478.4
78.5
78.5
78.7
78.6
78.7
78.5
78.5
78.1
17.9
78.7
18.0 3.8 0.0
18.0 3.8 0.0
0.0
0.0
20.7 0.4 0.00.0
20.8 0.4 0.0
20.7 0.4 0.0
0.0
0.0
21.1 0.3 0.0
20.9 0.4 0.0
0.0
0.0
21.2 0.2 0.0
21.2 0.2 0.0
0.0
0.0
0.021.1 0.4 0.0
0.0 0.0
0.0
0.0
0.0 0.0
999 14
BH1 0.00 00:01:30
0.00 00:00:30
BH1 0.00 00:01:00 -0.200.0
0.0
0.0
0.000.0
-0.30 0.00.0
BH1 0.00 00:02:00 -0.701.0
00:02:30 -0.801.0BH1 0.00
BH1 0.00 00:03:00 -1.102.0
0.80
0.0
Dry 0.01.00.00 00:00:00
BH2 0.00
BH2 0.00 00:00:30
00:01:30
BH2
1000
0.20
0.00
0.00 00:01:00 1.503.0
0.0
0.0
0.0
0.0
0.0
0.0
0.300.0
1.0
BH2 0.00 00:03:00 0.0
0.00 0.0
0.00 00:01:30
BH3
0.0
0.0
0.00 0.0
0.000.0
0.0
0.00
BH2
BH3
BH3 0.00 00:02:00 0.0
00:00:00
BH2 0.00 00:02:00
00:02:30BH2 0.00
BH3
BH3 0.00 00:01:00
BH3 0.00 00:00:30
0.00
00:02:30 0.00
0.001.05
0.0
0.0
0.000.0
0.0
0.0
0.0
0.40
0.80
0.0
0.0
0.0 21.5
0.0
0.0
0.0
21.4
0.0
21.4
21.5
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
1001
14
14
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
11/10/2013
SB
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH43.45 3.0
2.1 0.00.0BH4 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
1.70 0.0
78.6
78.7
78.7
78.6
18.6 2.7 0.0
18.6 2.7 0.0
0.0
0.0
WetLight
CloudyNone
78.578.5
78.7
78.7
78.9
78.7
78.9
78.7
78.7
79.018.2 2.8 0.00.0
19.1 2.0 0.0
18.4 2.6 0.0
0.0
0.0
20.3 1.0 0.0
19.9 1.4 0.0
0.0
0.0
20.5 0.7 0.0
20.4 0.8 0.0
0.0
0.0
0.018.5 2.7 0.0
2.7 0.0
0.0
0.0
2.7 0.0
1001 14
BH4 0.00 00:01:30
0.00 00:00:30
BH4 0.00 00:01:00 1.102.0
0.0
0.0
1.603.0
0.90 0.01.0
BH4 0.00 00:02:00 0.300.0
00:02:30 1.102.0BH4 0.00
BH4 0.00 00:03:00 -0.300.0
0.00
0.0
Dry 0.00.00.00 00:00:00
BH5 0.00
BH5 0.00 00:00:30
00:01:30
BH5
1001
0.00
-0.20
0.00 00:01:00 0.000.0
0.0
0.0
0.0
0.0
0.0
0.0
0.901.0
0.0
BH5 0.00 00:03:00 0.0
BH5
BH5 0.00 00:02:00
00:02:30BH5 0.00 0.0
0.00.10
0.00
0.0
0.0
0.0 18.8
0.0
0.0
0.0
18.5
2.6
18.6
19.3
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
14
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
11/10/2013
SB
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
17/10/2013
SB
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
9
9
Equipment Used LMSxi 1904 + Dip
987
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.4
20.7
20.7
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 20.7
0.0
0.0
0.0
20.7
0.0
0.0
0.0
0.00
0.00
3.45
0.0
-3.0
-1.60-3.0
0.00
00:02:30 -1.60
-1.60
BH4 0.00 00:01:00
BH4 0.00 00:00:30
00:00:00
BH3 0.00 00:02:00
00:02:30BH3 0.00
BH4
BH3
BH4
BH4 0.00 00:02:00 -3.0
BH4
0.0
0.0
-1.60 0.0
-1.60-3.0
-3.0
-1.60
0.00 -3.0
0.00 00:01:30
0.0
BH3 0.00 00:03:00 0.0
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
0.00
0.00 00:01:00 0.000.0
0.0
0.00 00:00:00
BH3 0.00
BH3 0.00 00:00:30
00:01:30
BH3
989
0.0
0.87 0.00.0
00:03:00 0.000.0
-0.20
BH2 0.00
BH2 0.00
00:02:30 0.000.0
BH2 0.00 00:02:00 0.000.0
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH2 0.00 00:01:00
988 9
BH2 0.00 0.4 0.0
0.0
0.0
0.4 0.0
0.020.6 0.4 0.0
18.9 3.3 0.0
19.4 2.8 0.0
0.0
0.0
19.7 2.4 0.0
19.9 2.0 0.0
0.0
0.0
20.1 1.8 0.0
20.2 1.7 0.0
0.0
0.0
20.3 1.5 0.00.0
21.3 0.0 0.0
21.3 0.0 0.0
0.0
0.0
78.6
21.3
78.1
78.9
77.7
78.0
77.9
78.0
77.7
77.9
WetCalm
NoneNone
78.878.8
78.8
20.7 0.4 0.0
20.7 0.4 0.0
0.0
0.0
0.0
0.0
0.0
0.0
78.6
78.6
0.0
0.0
78.6
78.6
78.7
0.00 00:03:00 -1.60-3.0BH4 0.0 0.00.0 78.7
21.2 0.0
0.0 21.2
0.0
78.8
78.8
78.8
21.3 0.0 0.0
0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
21.3
0.0
-0.10 0.0
0.0
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH2Dry 0.0
0.4 0.00.0BH2 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
BH5Dry -3.0
0.5 0.00.0BH5 0.00 00:00:00
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
-1.60 0.0
78.5
78.5
78.5
78.5
20.9 0.5 0.0
20.9 0.5 0.0
0.0
0.0
Calm
SlightNone
78.478.5
78.5
78.6
78.7
78.6
78.6
78.6
78.6
78.716.6 4.6 0.00.0
16.7 4.6 0.0
16.6 4.6 0.0
0.0
0.0
16.9 4.4 0.0
16.8 4.5 0.0
0.0
0.0
17.0 4.3 0.0
16.9 4.3 0.0
0.0
0.0
0.020.9 0.5 0.0
0.5 0.0
0.0
0.0
0.5 0.0
988 9
BH5 0.00 00:01:30
0.00 00:00:30
BH5 0.00 00:01:00 -1.60-3.0
0.0
0.0
-1.60-3.0
-1.60 0.0-3.0
BH5 0.00 00:02:00 -1.60-3.0
00:02:30 -1.60-3.0BH5 0.00
BH5 0.00 00:03:00 -1.60-3.0
-0.20
0.0
Dry 0.00.00.00 00:00:00
BH1 0.00
BH1 0.00 00:00:30
00:01:30
BH1
987
-0.20
-0.20
0.00 00:01:00 -0.200.0
0.0
0.0
0.0
0.0
0.0
0.0
-0.200.0
0.0
BH1 0.00 00:03:00 0.0
BH1
BH1 0.00 00:02:00
00:02:30BH1 0.00 0.0
0.0-0.20
-0.20
0.0
0.0
0.0 21.0
0.0
0.0
0.0
20.9
0.5
20.9
20.9
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
Equipment Used LMSxi 1904 + Dip
10
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSALL St LAWRENCE PRIMARY SCHOOL
1.00 0.10
CO(ppm)
1.00
17/10/2013
SB
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 1Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
31/10/2013
GM
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSALL St LAWRENCE PRIMARY SCHOOL
1.00
CO(ppm)
1.00
Equipment Used LMSxI 1904 + Dip
990
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
1.0
20.1
20.1
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 20.3
0.0
0.0
0.0
20.0
0.0
0.0
0.0
0.00.0
0.00
0.00
0.00
0.0
0.00
BH5 0.00 00:03:00
BH5 0.00 00:02:30
00:02:00
BH5 0.00 00:00:00
00:00:30
00:01:30
BH5 0.00
BH5
BH4
BH5
0.0
0.00.00 00:03:30
0.0
BH5 0.00
BH5 0.00 00:01:00 0.0
0.0
0.0
Dry 0.00.0 0.00
0.00 00:05:00
0.00 00:04:00
BH4 0.00 00:04:30
BH4
0.0
0.0
0.00.0
0.0
0.20
00:03:00 0.501.0
0.40
00:03:30BH4 0.00
BH4 0.00
BH4 0.00
00:02:30 0.400.0
BH4 0.00 00:02:00 0.901.0
0.60 0.01.0
0.300.0
0.0
0.0
1.102.0
00:01:30
0.00 00:00:30
BH4 0.00 00:01:00
990
BH4 0.00 1.7 0.0
0.0
0.0
1.7 0.0
19.4 2.2 0.0
0.0
0.0
19.6 2.0 0.0
19.2 2.4 0.0
19.1 2.5 0.0
0.0
0.0
19.0 2.6 0.00.0
18.1 3.1 0.0
17.2 3.9 0.0
0.0
0.0
16.9 4.2 0.0
16.6 4.4 0.0
0.0
0.0
16.5 4.5 0.0
16.4 4.6 0.0
0.0
0.0
WetLight
CloudyNone
19.9 1.8 0.0
19.8 1.8 0.0
0.0
0.0
0.0
0.0
0.0
16.4 4.6 0.0
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
16.4
0.60 0.0
4.6
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH43.20 1.0
1.6 0.00.0BH4 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
Project No Project Sheet No
Date State of Ground 2Wind
Operator Wind Direction
Cloud CoverPrecipitation
Detection Limits
31/10/2013
GM
0.10
CO2(% vol)
H2S(ppm)
Nitrogen(%vol)
Remarks
D3110-13
CH4(% LEL)
0.10 0.100.10
GNOSALL St LAWRENCE PRIMARY SCHOOL
1.00
CO(ppm)
1.00
Equipment Used LMSxi 1904 + Dip
988
989
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
0.0
3.3
20.2
20.1
Reading Depth
(mBGL)
0.00.0
0.0
0.0
0.0
0.0 19.2
0.0
0.0
0.0
20.3
0.0
0.0
0.0Dry
0.0
2.0
1.202.0
0.00
00:02:30 0.90
1.00
BH1 0.00 00:01:00
BH1 0.00 00:00:30
00:00:00
BH2 0.00 00:01:30
00:02:00BH2 0.00
BH1
BH1
BH1 0.00 00:02:00 2.0
BH1
0.0
0.0
1.20 0.0
1.102.0
2.0
1.40
0.00 1.0
0.00 00:01:30
BH2 0.00 00:02:30
0.0
0.0
0.0
0.0
0.0
0.000.0
0.00
Dry
0.00
0.00 00:00:30 0.000.0
0.0BH2 0.00
BH2 0.00 00:00:00
00:01:00
BH2
0.000:03:00
BH3 0.00
BH3 0.00
00:02:30
BH3 0.00 00:02:00
0.00 0.00.0
0.000.0
0.0
0.0
0.000.0
00:01:30
0.00 00:00:30
BH3 0.00 00:01:00
989
BH3 0.00 2.9 0.0
0.0
0.0
3.1 0.0
0.020.6 2.3 0.0
21.1 0.9 0.00.0
20.7 0.6 0.0
20.6 0.6 0.0
0.0
0.0
20.6 0.6 0.0
20.6 0.6 0.0
0.0
0.0
20.6 0.6 0.00.0
19.0 3.1 0.0
17.2 4.7 0.0
0.0
0.0
17.1
WetLight
CloudyNone
instrument
Water rising into
20.4 2.7 0.0
20.5 2.5 0.0
0.0
0.0
0.0
0.0
0.0
0.0
1.0
0.0
0.0
0.00 00:03:00 0.901.0BH1 4.7 0.00.0
17.1 4.7
0.80
0.0 17.1
0.0
17.2 4.7 0.0
4.7
0.0
Depth to Groundwater
(m BGL)
CH4(% vol)
O2(% vol)
17.2
0.0
-0.30 0.0
4.7
Borehole IDDepth of
Installation(m BGL)
FlowRate(l/hr)
Differential Pressure
(Pa)
Time of Reading
hh:mm:ssInst
ID
Barometric Pressure(mbars)
Air temp
(oC)
BH30.78 0.0
3.2 0.00.0BH3 0.00 00:00:00
Environmental Services Group Limited Gas Monitoring Record
Form IMS-SOP-SI-260-F1, 07/03
November 2013 Report No D3110-13 Issue 2.0 Enclosure C
ENCLOSURE C
GEOTECHNICAL LABORATORY TEST RESULTS
Index Properties – Summary of Results INDX 1 and 2
Particle Size Distribution Analyses PSD 1 to 18
Soil Sample Analysis ESG Scientifics Report No EFS/135115
Chemical Tests – Summary of Results CHEM 1 Dry Density/Moisture Content Relationship (Light Compaction) COMPL 1 and 2
Moisture Condition Value/Moisture Content Relationship MCVREL 1 and 2
California Bearing Ratio CBR 1 and 2
Project No Project Name
p p d w < 425 WL WP IP p sµm
sieve
from to % % % % Mg/m3
10 2.00 DBrown slightly gravelly SAND.
3.8 40 s 19 b NP
15 3.90 DBrown slightly gravelly SAND with rare clay pockets.
6.5 52 s 17 b NP
18 4.70 4.97 DBrown slightly gravelly SAND.
7.5
16 4.90 DBrown slightly sandy slightly gravelly CLAY.
12 90 s 33 a 14 19
17 5.00 5.35 DBrown slightly sandy slightly gravelly CLAY.
8.2 81 s 29 a 13 16
5 0.90 DBrown slightly sandy slightly gravelly CLAY.
17 89 s 34 a 14 20
7 1.20 DBrown slightly sandy slightly gravelly CLAY.
14 89 s 34 a 15 19
10 2.80 DBrown slightly sandy slightly gravelly CLAY.
18 84 s 28 a 12 16
11 3.00 DBrown slightly sandy slightly gravelly CLAY.
13 89 s 28 a 12 16
14 4.10 DBrown slightly sandy slightly gravelly CLAY.
11 75 s 26 a 12 14
18 5.80 DBrown slightly sandy slightly clayey GRAVEL.
5.0
14 3.00 3.45 DBrown clayey gravelly SAND.
12 72 s 28 b NP
17 3.60 3.73 DBrown gravelly SAND.
11
5 0.90 DBrown slightly sandy slightly gravelly silty CLAY.
14 77 s 26 a 15 11
7 1.20 1.65 DBrown slightly gravelly clayey SAND.
10 58 s 22 b NP
13 3.70 DBrown slightly sandy slightly gravelly CLAY.
12 86 s 31 a 13 18
14 4.00 4.45 DBrown slightly sandy slightly gravelly CLAY.
11 86 s 30 a 12 18
19 6.00 DBrown slightly sandy GRAVEL.
4.9
8 2.50 DBrown slightly gravelly SAND with rare clay pockets.
8.5 33 s 23 b NP
7 1.70 DBrown gravelly SAND.
6.5 28 s 20 b NP
8 2.50 DBrown gravelly silty SAND.
4.6 18 s 19 b NP
2 0.30 DBrown slightly gravelly clayey SAND.
15 56 s 31 a 21 10
9 1.80 DBrown slightly gravelly slightly clayey SAND.
16 72 s 22 b NP
11 3.20 DBrown gravelly SAND.
16
12 3.50 DBrown slightly sandy slightly gravelly CLAY.
11 62 s 30 a 12 18
14 4.80 DBrown gravelly SAND.
9.9
1 0.10 DBrown slightly sandy slightly gravelly CLAY with frequent rootlets and plant remains.
16 65 s 28 a 17 11
7 2.50 DOrangish brown gravelly SAND.
4.0
12 3.40 DBrown sandy slightly clayey GRAVEL.
9.0
11 4.50 DBrown gravelly SAND.
13
3 0.40 DBrown gravelly slightly clayey SAND.
12 43 s 26 b NP
7 1.90 DBrown gravelly SAND.
3.3
General notes: All above tests carried out to BS1377 : 1990 unless annotated otherwise. See individual test reports for further details.
Key : p bulk density, linear WL Liquid limit WP Plastic limit <425um preparation p s particle density
p d dry density a 4 point cone test NP non - plastic n from natural soil -g = gas jar
w moisture content b 1 point cone test IP s sieved specimen -p = small pyknometer
QA Ref
INDX 1
Plasticity Index
Printed:21/10/2013 16:09SLR 1Rev 91Mar 12
WS4
WS5
WS5
WS3
WS4
WS4
WS4
WS3
WS3
WS3
WS3
BH5
WS1
WS2
WS2
BH5
BH5
BH5
BH5
BH3
BH3
BH4
BH4
BH3
BH3
BH3
BH3
BH1
BH1
BH2
BH2
GNOSSALL St LAWRENCE PRIMARY SCHOOL
INDEX PROPERTIES - SUMMARY OF RESULTS
Soil Description
D3110-13
BH1
Hole No.
Mg/m3
Remarks
Sample
Depth (m)No. type
Table
Project No Project Name
p p d w < 425 WL WP IP p sµm
sieve
from to % % % % Mg/m3
GNOSSALL St LAWRENCE PRIMARY SCHOOL
INDEX PROPERTIES - SUMMARY OF RESULTS
Soil Description
D3110-13
Hole No.
Mg/m3
Remarks
Sample
Depth (m)No. type
10 3.50 DBrown sandy GRAVEL with frequent clay pockets.
5.6 36 s 27 a 13 14
General notes: All above tests carried out to BS1377 : 1990 unless annotated otherwise. See individual test reports for further details.
Key : p bulk density, linear WL Liquid limit WP Plastic limit <425um preparation p s particle density
p d dry density a 4 point cone test NP non - plastic n from natural soil -g = gas jar
w moisture content b 1 point cone test IP s sieved specimen -p = small pyknometer
QA Ref
WS5
SLR 1Rev 91Mar 12
Printed:21/10/2013 16:09INDX 2
Plasticity Index
Table
silt+clay =11
03752
11
Whole *<60mm1
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
6765
480.6001.18 60
8728
7370
81201410
7.90.063 110.150
340.425
2317
0.300
5.0
62
68
3.352.00
6.3
55
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
3751
Soil description%Passing
Brown very gravelly clayey SAND.
100969237.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 1
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
11 B
ESGD3110-13201308150000000011
QA Ref
SLR 2,9Rev 88Aug 11
2.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =7
0786
7
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
9494
750.6001.18 92
9728
9696
96201410
8.10.063 70.150
480.425
2412
0.300
5.0
93
95
3.352.00
6.3
88
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
786
Soil description%Passing
Orangish brown gravelly SAND with rare clay pockets.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
3
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 2
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
14 B
ESGD3110-13201308150000000014
QA Ref
SLR 2,9Rev 88Aug 11
3.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =7
0687
7
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
9595
730.6001.18 93
10028
9897
99201410
7.90.063 80.150
420.425
2414
0.300
5.0
94
96
3.352.00
6.3
88
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
687
Soil description%Passing
Brown gravelly SAND with rare clay pockets.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
4
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 3
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
17 B
ESGD3110-13201308150000000017
QA Ref
SLR 2,9Rev 88Aug 11
4.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =3
04849
3
Whole *<60mm4
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
5754
330.6001.18 47
9128
7566
85201410
9.70.063 30.150
200.425
116
0.300
5.0
50
60
3.352.00
6.3
40
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
4647
Soil description%Passing
Brown SAND AND SAND with rare clay pockets and one cobble.
96969537.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
32
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 4
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH2
5 B
ESGD3110-13201308150000000021
QA Ref
SLR 2,9Rev 88Aug 11
0.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =7
0984
7
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
9492
740.6001.18 88
10028
9996
100201410
5.00.063 70.150
520.425
2714
0.300
5.0
91
94
3.352.00
6.3
83
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
984
Soil description%Passing
Brown gravelly silty SAND
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
4
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 5
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH2
8 B
ESGD3110-13201308150000000024
QA Ref
SLR 2,9Rev 88Aug 11
0.90
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =9
05041
9
Whole *<60mm2
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
5653
320.6001.18 46
8528
6965
81201410
11.00.063 90.150
220.425
1614
0.300
5.0
49
59
3.352.00
6.3
39
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
4940
Soil description%Passing
Brown very sandy clayey GRAVEL.
100928837.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
92
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 6
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH2
13 B
ESGD3110-13201308150000000031
QA Ref
SLR 2,9Rev 88Aug 11
3.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =6
05242
6
Whole *<60mm4
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
5349
360.6001.18 43
8028
6963
74201410
14.30.063 60.150
280.425
1912
0.300
5.0
46
56
3.352.00
6.3
39
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
5040
Soil description%Passing
Brown very sandy GRAVEL with occasional clay pockets and one cobble.
97928737.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
73
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 7
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH3
17 B
ESGD3110-13201308150000000055
QA Ref
SLR 2,9Rev 88Aug 11
5.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =2
04454
2
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
6158
490.6001.18 54
9128
7670
83201410
5.80.063 20.150
350.425
178
0.300
5.0
56
63
3.352.00
6.3
52
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
4454
Soil description%Passing
Brown very gravelly SAND.
1001009437.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
27
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 8
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
6 B
ESGD3110-13201308150000000064
QA Ref
SLR 2,9Rev 88Aug 11
0.80
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
89
0137089
0.0049Whole *<60mm
00.0035
0.212
Particle Size mm
Particle Size mm
0.0374
%Passing
100756350
8888
0.0015
850.6001.18 87
10028
9591
100201410
6.1
2.65
0.063 180.150
810.425
7051
0.300
Particle density, Mg/m3
5.0
87
88
3.352.00
6.3
86
Clay
Sample Proportions
*<60mm values to aid description only
Sand
10
Silt
9 Cobbles / boulders
1211
Gravel
Remarks
1370
Soil description%Passing
Brown gravelly clayey SAND
14100100100
0.02660.01890.009837.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
50
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0526
1815
1312
PSD 9
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
15 B
ESGD3110-13201308150000000073
QA Ref
SLR 2,9Rev 88Aug 11
3.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
2713
021392713
0.0046Whole *<60mm
00.0035
0.212
Particle Size mm
Particle Size mm
0.0363
%Passing
100756350
8381
0.0015
740.6001.18 77
9528
8886
94201410
7.4
2.65
0.063 420.150
670.425
6054
0.300
Particle density, Mg/m3
5.0
79
84
3.352.00
6.3
77
Clay
Sample Proportions
*<60mm values to aid description only
Sand
18
Silt
12 Cobbles / boulders
2620
Gravel
Remarks
2139
Soil description%Passing
Brown slightly gravelly sandy silty CLAY.
3510010097
0.02590.01850.009737.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0510
4238
3330
PSD 10
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
3 B
ESGD3110-13201308150000000080
QA Ref
SLR 2,9Rev 88Aug 11
0.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
2822
07432822
0.0044Whole *<60mm
00.0032
0.212
Particle Size mm
Particle Size mm
0.0295
%Passing
100756350
9494
0.0015
860.6001.18 91
9928
9796
98201410
4.4
2.65
0.063 500.150
780.425
7062
0.300
Particle density, Mg/m3
5.0
93
95
3.352.00
6.3
89
Clay
Sample Proportions
*<60mm values to aid description only
Sand
25
Silt
20 Cobbles / boulders
3528
Gravel
Remarks
743
Soil description%Passing
Brown slightly gravelly sandy CLAY.
48100100100
0.02150.01550.008437.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0413
5049
4442
PSD 11
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
15 B
ESGD3110-13201308150000000092
QA Ref
SLR 2,9Rev 88Aug 11
4.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
119
01070119
0.0049Whole *<60mm
00.0035
0.212
Particle Size mm
Particle Size mm
0.0367
%Passing
100756350
9292
0.0016
740.6001.18 88
10028
9695
99201410
7.2
2.65
0.063 200.150
610.425
5036
0.300
Particle density, Mg/m3
5.0
90
93
3.352.00
6.3
82
Clay
Sample Proportions
*<60mm values to aid description only
Sand
10
Silt
9 Cobbles / boulders
1412
Gravel
Remarks
1070
Soil description%Passing
Brown gravelly SAND with frequent clay pockets.
18100100100
0.02600.01850.009737.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
96
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0516
2019
1816
PSD 12
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
18 B
ESGD3110-13201308150000000095
QA Ref
SLR 2,9Rev 88Aug 11
5.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =14
03056
14
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
7673
580.6001.18 68
9828
8681
95201410
6.50.063 150.150
440.425
2920
0.300
5.0
70
77
3.352.00
6.3
64
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
3056
Soil description%Passing
Brow slightly gravelly sandy CLAY.
1001009837.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
Not applicable
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 13
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS1
3 B
ESGD3110-13201308150000000099
QA Ref
SLR 2,9Rev 88Aug 11
0.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =2
01286
2
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
8989
780.6001.18 88
9628
9291
95201410
3.50.063 30.150
510.425
249
0.300
5.0
88
90
3.352.00
6.3
85
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
1286
Soil description%Passing
Orangish brown gravelly SAND.
1001009837.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
2
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 14
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS1
10 B
ESGD3110-13201308150000000107
QA Ref
SLR 2,9Rev 88Aug 11
3.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =4
03858
4
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
7066
400.6001.18 59
9728
8479
93201410
5.50.063 40.150
220.425
106
0.300
5.0
62
72
3.352.00
6.3
52
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
3858
Soil description%Passing
Brown very gravelly SAND.
1001009837.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
7
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 15
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS2
9 B
ESGD3110-13201308150000000115
QA Ref
SLR 2,9Rev 88Aug 11
2.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
124
04438134
0.0046Whole *<60mm
90.0035
0.212
Particle Size mm
Particle Size mm
0.0352
%Passing
95756350
5855
0.0016
420.6001.18 49
8128
7166
75201410
9.1
2.65
0.063 170.150
350.425
2722
0.300
Particle density, Mg/m3
5.0
51
60
3.352.00
6.3
46
Clay
Sample Proportions
*<60mm values to aid description only
Sand
6
Silt
4 Cobbles / boulders
108
Gravel
Remarks
4035
Soil description%Passing
Dark brown clayey very sandy GRAVEL with two cobbles.
15919183
0.02540.01810.009537.5
Sieving Sedimentation
9.5 hydrometer
BS 1377 : Part 2 : 1990
562
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
assumed
Dry mass of sample, kg
Sieve: natural material Hydro: as BS1377 Preparation / Pretreatment
0.06300.0492
1716
1311
PSD 16
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS3
4 B
ESGD3110-13201308150000000120
QA Ref
SLR 2,9Rev 88Aug 11
0.20
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =6
04549
6
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
6058
400.6001.18 53
9628
7668
92201410
4.40.063 60.150
240.425
1510
0.300
5.0
55
62
3.352.00
6.3
48
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
4549
Soil description%Passing
Brown very gravelly SAND with rare clay pockets.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
33
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: natural material Preparation / Pretreatment
PSD 17
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS4
8 B
ESGD3110-13201308150000000139
QA Ref
SLR 2,9Rev 88Aug 11
2.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
silt+clay =9
02269
9
Whole *<60mm0
0.212
Particle Size mm
Particle Size mm
%Passing
100756350
8381
540.6001.18 75
10028
9490
98201410
2.20.063 80.150
270.425
1712
0.300
5.0
78
84
3.352.00
6.3
68
Clay
Sample Proportions
*<60mm values to aid description only
SandSilt
Cobbles / bouldersGravel
Remarks
2269
Soil description%Passing
Brown very gravelly SAND.
10010010037.5
Sieving Sedimentation
none
BS 1377 : Part 2 : 1990
5
9.2 wet sieve
Uniformity Coefficient D60 / D10
SievingSedimentation
Test Method
12590
100100
Dry mass of sample, kg
Sieve: pre dried, Preparation / Pretreatment
PSD 18
0
10
20
30
40
50
60
70
80
90
100
0.001 0.01 0.1 1 10 100 1000Particle size mm
Per
cen
t P
assi
ng
Particle Size Distribution Analysis
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS4
10 B
ESGD3110-13201308150000000141
QA Ref
SLR 2,9Rev 88Aug 11
3.00
SILTFine Medium Coarse
SANDFine Medium Coarse
GRAVELFine Medium CoarseCLAY COBBLES
Spec Ref
Figure
BOULDERS
� Printed:21/10/2013 16:17
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnossall St Lawrence Primary School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 11-Sep-2013Declan Burns Operations Director
Laboratory and Analytical Business
11-Sep-2013
The 7 samples described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTSOIL SAMPLE ANALYSIS
Report No. EFS/135115 (Ver. 1)
Table 1 Main Analysis Results (Page 2)Analytical and Deviating Sample Overview (Page 3)Table of Method Descriptions (Page 4)Table of Report Notes (Page 5)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 5Where individual results are flagged see report notes for status.
EFS/135115 Ver. 1
Units : mg/kg mg/l % pH UnitsMethod Codes : ICPACIDS ICPWSS TSBRE1 WSLM50
Method Reporting Limits : 20 10 0.005UKAS Accredited : Yes Yes No No
LAB
ID N
umber C
L/
Client Sample Description
Sam
ple Date
SO
4-- (acid sol)
SO
4-- (H2O
sol) mg/l
Total S
ulphur.
pH (B
S1377)
1321688 BH1 B 6 0.80 07-Aug-13 886 275 0.060 7.3
1321689 BH3 B 9 2.00 06-Aug-13 98 28 0.012 7.8
1321690 BH4 B 3 0.20 05-Aug-13 608 41 0.200 6.8
1321691 BH4 B 11 2.00 05-Aug-13 256 27 0.049 7.9
1321692 BH5 B 12 3.00 06-Aug-13 168 <10 0.021 8.2
1321693 WS1 B 7 1.20 05-Aug-13 48 25 0.007 7.8
1321694 WS5 B 1 0.00 05-Aug-13 454 1110 0.159 7.7
Contact
Date Printed
Report Number EFS/135115
Table Number 1
Fax +44 (0) 1283 554422
Soil Sample Analysis
Mr J Litten
11-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 5Where individual results are flagged see report notes for status.
EFS/135115 Ver. 1
SOIL Analysis S135115
CustomerSiteReport No S135115
MethodID
BS
1377CL
CustS
erv
Dep.O
pt
ICP
AC
IDS
ICP
BR
E
ICP
WS
S
KO
NE
NS
.
TS
BR
E1
WS
LM50
ID Number Description Sampled
Chloride (A
) BS
1377
Report B
DO
Cl if pH
<5.5
DO
Mg if S
O4(W
)>3000
DO
NO
3 if pH<5.5
SO
4-- (acid sol)
Magnesium
(BR
E)
SO
4-- (H2O
sol) mg/l
Nitrite as N
:
Total S
ulphur.
pH (B
S1377)
���� ����
CL/1321688 BH1 0.80 07/08/13CL/1321689 BH3 2.00 06/08/13CL/1321690 BH4 0.20 05/08/13CL/1321691 BH4 2.00 05/08/13CL/1321692 BH5 3.00 06/08/13CL/1321693 WS1 1.20 05/08/13CL/1321694 WS5 0.00 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 3 of 5Where individual results are flagged see report notes for status.
EFS/135115 Ver. 1
Matrix MethodID Analysis Basis
Method Description
Soil ICPACIDS Air Dried Determination of Total Sulphate in soil samples by Hydrochloric Acid extraction followed by ICPOES detection
Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection
Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection
Soil WSLM50 Air Dried Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.
Report Number: EFS/135115
Method Descriptions
Page 4 of 5Where individual results are flagged see report notes for status.
EFS/135115 Ver. 1
Project No Project Name
LOI pH CO2 <2
2:1watersol.
groundwater
acidsol.
TSMgNO3
NH4
mg/Lmg/L
watersol.
acidsol.
mm
from to % g/L g/L % % % % % %
4 0.60 DDark brown gravelly slightly clayey SAND. 0.3 c 70
3 0.30 DBrown gravelly SAND.
0.5 c 51
8 1.70 DBrown gravelly SAND.
0.4 c 75
5 0.70 DBrown slightly gravelly SAND. 0.6 c 74
11 3.00 DBrown gravelly slightly clayey SAND. 0.8 c 60
6 1.50 DBrown gravelly SAND.
0.2 c 84
11 3.50 DBrown gravelly slightly silty SAND. 0.2 c 66
7 1.90 DBrown gravelly SAND.
0.1 c 60
BS 1377 : definitive method unless stated : * Sulphate tests preparation / test methods : BRE Special Digest SD1, dependent options :
Org1. BS 1377:Part 3:1990:clause 5.3 4. TRL447 - 1 water soluble sulphate TS Total Sulphur to BR279 / EN ISO15178
LOI Mass loss on ignition at 440oC 2. BS 1377:Part 3:1990:clause 5.4 5. TRL447 - 2 acid soluble sulphate Mg Soluble Magnesium to BR279, colorimetric
CO2 Carbonate content ( rapid titration ) 3. BS 1377:Part 3:1990:clause 5.5 6. BR279 - groundwater sulphate NO3 Soluble Nitrate to BR279, colorimetric
Cl Chloride content < 2mm material passing 2mm sieve NH4 qualitative
QA Ref
WS2
WS5
Sample
Depth (m)No. type
Hole No. Soil Description
Sulphate as SO4 SD1 options
Pre
para
tion/
test
*
Org
%
Chloride, Cl
Printed:21/10/2013 16:14
BH1
Remarks
Organic matter content ( s-sulphides, c-chlorides identified )
BH2
BH3
CHEMICAL TESTS - SUMMARY OF RESULTS
CHEM 1SLR 3Rev 95Aug 11
D3110-13 GNOSSALL St LAWRENCE PRIMARY SCHOOL
BH4
BH5
WS1
Table
Soil description Derived Parameters +
Test method BS 1377:part 4:1990: clause 3.4, 2.5 kg rammer in a CBR mould Maximum dry density, Mg/m3
Preparation Original material was natural, separate specimens tested
Material > 37.5mm %
Material < 37.5mm > 20mm % Optimum moisture content, %
Particle density, Mg/m3 assumed
Remarks
1.93
12
Brown gravelly slightly clayey SAND.
2.65
1
9
COMPL 1
DRY DENSITY / MOISTURE CONTENT RELATIONSHIPBS1377 : PART 4 : 1990 : LIGHT COMPACTION, 2.5 kg rammer
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
1.20
8 B
ESGD3110-13201308150000000008
QA Ref
SLD 4, 3.3/4Rev 66Aug 11
1.4
1.5
1.6
1.7
1.8
1.9
2.0
2.1
2.2
0 4 8 12 16 20 24 28 32
MOISTURE CONTENT %
DR
Y D
EN
SIT
Y M
g/m
3
----- zero, 5% and 10% air voids
Spec Ref
Figure
� Printed:21/10/2013 16:16
Soil description Derived Parameters +
Test method BS 1377:part 4:1990: clause 3.4, 2.5 kg rammer in a CBR mould Maximum dry density, Mg/m3
Preparation Original material was natural, single sample tested
Material > 37.5mm %
Material < 37.5mm > 20mm % Optimum moisture content, %
Particle density, Mg/m3 assumed
Remarks
2.00
10
Brown gravelly slightly clayey SAND.
2.65
0
11
COMPL 2
DRY DENSITY / MOISTURE CONTENT RELATIONSHIPBS1377 : PART 4 : 1990 : LIGHT COMPACTION, 2.5 kg rammer
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
2.00
11 B
ESGD3110-13201308150000000069
QA Ref
SLD 4, 3.3/4Rev 66Aug 11
1.4
1.5
1.6
1.7
1.8
1.9
2.0
2.1
2.2
0 2 4 6 8 10 12 14 16
MOISTURE CONTENT %
DR
Y D
EN
SIT
Y M
g/m
3
----- zero, 5% and 10% air voids
Spec Ref
Figure
� Printed:21/10/2013 16:16
The above characteristics are NOT covered by UKAS accreditation to BS1377
sheet 1 of 2
Method of interpretation of MCV
-0.99
Steepest straight line
Sensitivity ( Change in MCV per 1% moisture content )
Correlation ( proximity of test points to regression line )
Characteristics of calibration line (determined using linear regression)
17.5
-0.79
1.26
Intercept
Slope
MCVREL 1
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
1.20
8 B
ESGD3110-13201308150000000085
QA Ref
SLD 4, 5.5Rev 72Aug 11
MCV CALIBRATION
0
4
8
12
16
20
24
0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV
Moi
stur
e C
onte
nt %
valid points regression
ineffective/invalid extended regression
Spec Ref
Figure
� Printed:21/10/2013 16:16
Test No * ineffective / invalid point 1 * 2 3 4 5
%
sheet 2 of 2
Brown slightly gravelly sandy CLAY.
Remarks
%
Moisture Condition Value
Dry density after test
Moisture Content
Bulk density after test Mg/m³
Mg/m³
% #N/A
15.7
2.04
2.18 2.21
1.92 1.97
2.24
13.5 11.9 10.8
Material retained on 20mm sieve Steepest straight line
Procedure / Preparation
Initial moisture content <20mm Method of determining MCV
BS1377:Part 1 and Part 4, clause 5.5
3.7
Soil description
1.84
15.7
9.3
9.9
2.05
2.262.13
4.9 7.2 8.9
MCVREL 1
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH5
1.20
8 B
ESGD3110-13201308150000000085
QA Ref
SLD 4, 5.5Rev 72Aug 11
Number of Blows
644832241612864321
1816141210864200
5
10
15
20
25
30
Moisture Condition Value , MCV,
Cha
nge
in P
enet
ratio
n -
mm
test 1 2 3 4 5
Spec Ref
Figure
� Printed:21/10/2013 16:16
The above characteristics are NOT covered by UKAS accreditation to BS1377
sheet 1 of 2
Method of interpretation of MCV
#N/A
Steepest straight line
Sensitivity ( Change in MCV per 1% moisture content )
Correlation ( proximity of test points to regression line )
Characteristics of calibration line (determined using linear regression)
#N/A
#N/A
#N/A
Intercept
Slope
MCVREL 2
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS2
0.60
5 B
ESGD3110-13201308150000000111
QA Ref
SLD 4, 5.5Rev 72Aug 11
MCV CALIBRATION
0
2
3
5
7
8
10
0 2 4 6 8 10 12 14 16 18 20Moisture Condition Value MCV
Moi
stur
e C
onte
nt %
valid points regression
ineffective/invalid extended regression
Spec Ref
Figure
� Printed:21/10/2013 16:16
Test No * ineffective / invalid point 1 2 3 4 5
%
sheet 2 of 2
Brown gravelly SAND with occasional clay pockets.
Test Inconclusive. Material type not suitable. Remarks
%
Moisture Condition Value
Dry density after test
Moisture Content
Bulk density after test Mg/m³
Mg/m³
% #N/A
8.5
1.55
1.64 1.75
1.53 1.55
1.91
7.2 12.7 5.5
Material retained on 20mm sieve Steepest straight line
Procedure / Preparation
Initial moisture content <20mm Method of determining MCV
BS1377:Part 1 and Part 4, clause 5.5
4.3
Soil description
1.56
8.5
17.4
#N/A
1.63
1.631.69
#N/A #N/A #N/A
MCVREL 2
MOISTURE CONDITION VALUE ( MCV ) / MOISTURE CONTENT RELATIONSHIP BS1377:PART 4 : 1990 : CLAUSE 5.5
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
WS2
0.60
5 B
ESGD3110-13201308150000000111
QA Ref
SLD 4, 5.5Rev 72Aug 11
Number of Blows
644832241612864321
1816141210864200
5
10
15
20
25
30
Moisture Condition Value , MCV,
Cha
nge
in P
enet
ratio
n -
mm
test 1 2 3 4 5
Spec Ref
Figure
� Printed:21/10/2013 16:16
%
Notes :
Soil description
%
Mg/m³
11
2.15
12
12
Test Conditions
Sample Retained on 20 mm sieve
Sample Conditions
%
%
BASETOP
1.92Mg/m³
CBR Values %
Moisture Content - BASE
Bulk Density
Dry Density
mm
Method of Compaction
days 4Soaking PeriodPre
para
tion
11
Recompacted - Rammer compaction with specified effort ( 2.5kg )
Soaked test
2.41.5
5.0 1.9 3.40
0
1.9
Amount of Swell -0.41
Brown gravelly slightly clayey SAND.
Initial Moisture Content
Moisture Content - TOP
YES
Penetration mm
Accepted CBR % 3.4
kgSurcharge applied
2.5
kPa
CBR 1
0.00
0.20
0.40
0.60
0.80
1.00
1.20
1.40
1.60
1.80
2.00
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.5 7 7.5
Penetration - mm
For
ce o
n P
lung
er -
kN
TOPBASE
California Bearing Ratio ( BS1377:1990:Part 4 , section 7 )
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH1
1.20
8 B
ESGD3110-13201308150000000008
QA Ref
SLR 4.7Rev 89Aug 11
Spec Ref
Figure
� Printed:21/10/2013 16:15
%
Notes :
Soil description
%
Mg/m³
12
2.13
13
13
Test Conditions
Sample Retained on 20 mm sieve
Sample Conditions
%
%
BASETOP
1.90Mg/m³
CBR Values %
Moisture Content - BASE
Bulk Density
Dry Density
mm
Method of Compaction
days 4Soaking PeriodPre
para
tion
11
Recompacted - Rammer compaction with specified effort ( 2.5kg )
Soaked test
7.33.1
5.0 5.4 150
0
5.4
Amount of Swell -0.12
Brown gravelly slightly clayey SAND.
Initial Moisture Content
Moisture Content - TOP
YES
Penetration mm
Accepted CBR % 15
kgSurcharge applied
2.5
kPa
CBR 2
0.00
1.00
2.00
3.00
4.00
5.00
6.00
7.00
8.00
9.00
10.00
0 0.5 1 1.5 2 2.5 3 3.5 4 4.5 5 5.5 6 6.5 7 7.5
Penetration - mm
For
ce o
n P
lung
er -
kN
TOPBASE
California Bearing Ratio ( BS1377:1990:Part 4 , section 7 )
Project No
Project Name
D3110-13
GNOSSALL St LAWRENCE PRIMARY SCHOOL
Sample Details: Hole No
Depth (m BGL)
Samp No Type
ID
BH4
2.00
11 B
ESGD3110-13201308150000000069
QA Ref
SLR 4.7Rev 89Aug 11
Spec Ref
Figure
� Printed:21/10/2013 16:15
November 2013 Report No D3110-13 Issue 2.0 Enclosure D
ENCLOSURE D
GEOENVIRONMENTAL LABORATORY TEST RESULTS
ESG Scientifics Report EFS/135116M
ESG Scientifics Report EFS/135126M
ESG Scientifics Report EXR/162608
ESG Scientifics Report EXR/162639
ESG Scientifics Report EXR/162915
ESG Scientifics Report EXR/166207
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 5 of 5Where individual results are flagged see report notes for status.
EFS/135115 Ver. 1
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnossall St Lawrence Primary School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 12-Sep-2013Declan Burns Operations Director
Laboratory and Analytical Business
Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)
(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.
ESG accepts no responsibility for any sampling not carried out by our personnel.
12-Sep-2013
The 19 samples described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTSOIL SAMPLE ANALYSIS
Report No. EFS/135116M (Ver. 1)
Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Pages 4 to 22)Table of GRO Results (Page 23)Table of TPH (Si) banding (std) (Page 24)GC-FID Chromatograms (Pages 25 to 62)Table of VOC (HSA) Results (Pages 63 to 80)Table of Asbestos Screening Results (Page 81)Analytical and Deviating Sample Overview (Pages 82 to 85)Table of Additional Report Notes (Page 86)Table of Method Descriptions (Page 87)Table of Report Notes (Page 88)Table of Sample Descriptions (Appendix A Page 1 of 1)
Tests marked '^' have been subcontracted to another laboratory.
All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 1 of 88
Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL
Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 0.6 16 1 0.1Accreditation Code: UM U UM UM UM UM UM UM UM UM UM U UM UM UM
LAB
ID N
umber C
L/
Client Sample Description
Sam
ple Date
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
1321695 BH1 ES 2 0.30 07-Aug-13 Req 0.9 0.6 6.4 1.51 19.8 32.9 25.9 <0.5 1.4 68.0 1.1 69 125.5 2.39 <0.1
1321696 BH1 ES 5 0.60 07-Aug-13 Req 0.9 0.6 6.3 0.29 13.3 18.2 50.6 <0.51 0.7 15.8 <0.5 21.4 81.4 <1 <0.1
1321697 BH1 ES 9 1.90 07-Aug-13 Req <0.5 0.3 5 <0.2 12.6 11 13.2 <0.5 <0.5 11.2 <0.5 13.7 34.1 <1 <0.1
1321698 BH2 ES 2 0.15 07-Aug-13 Req <0.5 0.4 6.6 <0.20 13.6 25.2 10.7 <0.5 1.9 17.9 <0.5 30.8 27.2 1.44 <0.1
1321699 BH2 ES 4 0.50 07-Aug-13 Req <0.5 0.3 4.7 <0.2 12.7 9.8 6.4 <0.5 <0.5 12.2 <0.5 14.4 31.5 <1 <0.1
1321700 BH3 ES 2 0.30 06-Aug-13 Req <0.5 0.3 3.8 <0.2 12.7 8.8 12.4 <0.5 <0.5 10.7 <0.5 13.6 42.3 <1 <0.1
1321701 BH4 ES 2 0.20 05-Aug-13 Req <0.5 0.7 9.5 1.19 29.9 62.1 29.5 <0.5 2.5 35.6 <0.5 24.7 85.1 <1 <0.1
1321702 BH4 ES 9 1.90 05-Aug-13 Req <0.5 0.4 5 0.66 18.2 33.4 62.5 <0.5 0.7 17.4 <0.5 13.4 46.5 1.06 <0.1
1321703 BH5 ES 2 0.20 06-Aug-13 Req <0.5 0.6 6.3 <0.20 22.7 14.4 21.4 <0.5 <0.5 19.7 <0.5 32 60.4 <1 <0.1
1321704 WS1 ES 1 0.10 05-Aug-13 Req <0.5 0.2 4.9 0.34 14.7 22.9 11.7 <0.5 1.4 17.3 <0.5 41.9 76 <1 <0.1
1321705 WS1 ES 2 0.30 05-Aug-13 Req <0.5 0.3 4.2 <0.20 11.3 10.9 17.4 <0.5 <0.5 10.8 <0.5 14.5 44.1 <1 <0.1
1321706 WS2 ES 1 0.10 05-Aug-13 Req <0.5 0.2 5.2 0.47 38.8 15.2 9.1 <0.5 1.2 14.6 0.8 42.8 40.7 1.88 <0.1
1321707 WS2 ES 2 0.30 05-Aug-13 Req <0.5 0.3 5.3 <0.2 22.7 10.9 7.3 <0.5 0.6 13.0 <0.5 23.1 33.5 <1 <0.1
1321708 WS3 ES 1 0.20 05-Aug-13 Req <0.5 1.2 11.8 0.55 19 25.6 129.4 <0.52 1 17.0 0.7 26.0 164 2.34 <0.1
1321709 WS3 ES 7 1.00 05-Aug-13 Req <0.5 0.4 5.6 <0.21 13.9 11.7 20.9 <0.5 <0.5 12.6 <0.5 17 46.1 <1 <0.1
1321710 WS4 ES 2 0.20 05-Aug-13 Req <0.5 0.5 7.4 0.22 15.7 13.5 33.7 <0.5 <0.5 12.5 <0.5 19.5 64.5 <1 <0.1
1321711 WS5 ES 4 0.60 05-Aug-13 Req <0.5 0.4 4.6 0.23 12.0 10 25.5 <0.5 <0.5 8.6 <0.5 16.0 56.1 <1 <0.1
1321712 WS5 ES 6 1.20 05-Aug-13 Req <0.5 0.5 5.5 <0.20 14.5 17.0 19.5 <0.5 <0.5 17.4 <0.5 18.8 61.1 <1 <0.1
1321713 WS5 ES 8 2.50 05-Aug-13 Req <0.5 0.2 3.8 <0.20 7.9 7.4 3.6 <0.5 <0.5 8.2 <0.5 9.0 20 <1 <0.1
Contact
Date Printed
Report Number EFS/135116M
Table Number 1
Fax +44 (0) 1283 554422
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam Soil Sample Analysis
Mr J Litten
12-Sep-2013
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 2 of 88
Units : mg/kg mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : ICPSOIL ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 KONECR TSBRE1 WSLM59 PAHMSUS
Method Reporting Limits : 36 10 0.5 0.5 0.2 10 0.5 0.1 0.005 0.02Accreditation Code: UM UM UM UM U U U N N N N
LAB
ID N
umber C
L/
Client Sample Description
Sam
ple Date
Iron
SO
4-- (H2O
sol) mg/l
pH units (A
R)
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
VO
C H
SA
-GC
MS
Chrom
ium (III)
Chrom
ium vi:
Total S
ulphur.
Total O
rganic Carbon
PA
H (16) by G
CM
S
1321695 BH1 ES 2 0.30 07-Aug-13 211 142 8.2 <0.5 <0.5 NAIIS 6.0 Req Req <19.8 <0.1 0.362 2.61 Req
1321696 BH1 ES 5 0.60 07-Aug-13 150 158 7.6 <0.6 <0.6 NAIIS 9.8 Req Req <13.3 <0.1 0.041 0.93 Req
1321697 BH1 ES 9 1.90 07-Aug-13 129 336 6.9 <0.5 <0.5 NAIIS 4.4 Req Req <12.6 <0.1 0.028 0.29 Req
1321698 BH2 ES 2 0.15 07-Aug-13 170 100 8.1 <0.6 <0.6 NAIIS 16.7 Req Req <13.6 <0.1 0.213 20.56 Req
1321699 BH2 ES 4 0.50 07-Aug-13 141 38 7.5 <0.5 <0.5 NAIIS 4.5 Req Req <12.7 <0.1 0.023 0.40 Req
1321700 BH3 ES 2 0.30 06-Aug-13 122 34 7.2 <0.6 <0.6 NAIIS 12.5 Req Req <12.7 <0.1 0.015 0.41 Req
1321701 BH4 ES 2 0.20 05-Aug-13 242 106 6.9 <0.6 <0.6 NAIIS 13.6 Req Req <29.9 <0.1 0.235 9.06 Req
1321702 BH4 ES 9 1.90 05-Aug-13 129 56 7.8 <0.5 <0.5 NAIIS 7.4 Req Req <18.2 <0.1 0.055 2.12 Req
1321703 BH5 ES 2 0.20 06-Aug-13 233 22 7.6 <0.5 <0.5 NAIIS 8.3 Req Req <22.7 <0.1 0.022 0.67 Req
1321704 WS1 ES 1 0.10 05-Aug-13 157 72 7.8 <0.6 <0.6 NAIIS 11.0 Req Req <14.7 <0.1 0.305 >25 Req
1321705 WS1 ES 2 0.30 05-Aug-13 127 30 6.9 <0.6 <0.6 NAIIS 9.9 Req Req <11.3 <0.1 0.029 1.23 Req
1321706 WS2 ES 1 0.10 05-Aug-13 166 319 8.0 <0.5 <0.5 CH 8.2 Req Req <38.8 <0.1 0.401 11.62 Req
1321707 WS2 ES 2 0.30 05-Aug-13 165 127 8.1 <0.5 <0.5 NAIIS 5.7 Req Req <22.7 <0.1 0.078 0.81 Req
1321708 WS3 ES 1 0.20 05-Aug-13 138 128 7.6 <0.6 <0.6 NAIIS 15.4 Req Req <18.6 <0.1 0.085 2.27 Req
1321709 WS3 ES 7 1.00 05-Aug-13 140 94 7.7 <0.6 <0.6 NAIIS 10.8 Req Req <13.9 <0.1 0.029 0.56 Req
1321710 WS4 ES 2 0.20 05-Aug-13 153 37 6.2 <0.6 <0.6 NAIIS 13.4 Req Req <15.7 <0.1 0.026 0.92 Req
1321711 WS5 ES 4 0.60 05-Aug-13 138 41 6.4 <0.6 <0.6 NAIIS 10.3 Req Req <12.0 <0.1 0.033 0.95 Req
1321712 WS5 ES 6 1.20 05-Aug-13 168 133 8.1 <0.5 <0.5 NAIIS 6.5 Req Req <14.5 <0.1 0.031 0.54 Req
1321713 WS5 ES 8 2.50 05-Aug-13 87 30 7.8 <0.5 <0.5 NAIIS 5.5 Req Req <7.9 <0.1 0.011 0.07 Req
Contact
Date Printed
Report Number EFS/135116M
Table Number 1
Fax +44 (0) 1283 554422
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam Soil Sample Analysis
Mr J Litten
12-Sep-2013
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 3 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH1 ES 2 0.30 Job Number: S13_5116MLIMS ID Number: CL1321695 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.53 0.89 100 UAcenaphthene 83-32-9 4.66 0.41 98 UMFluorene 86-73-7 5.07 0.20 92 UMPhenanthrene 85-01-8 5.96 1.84 99 UMAnthracene 120-12-7 6.02 2.17 97 UFluoranthene 206-44-0 7.37 19.00 99 UMPyrene 129-00-0 7.67 22.40 96 UMBenzo[a]anthracene 56-55-3 9.40 13.40 96 UMChrysene 218-01-9 9.45 13.10 98 UMBenzo[b]fluoranthene 205-99-2 10.96 29.00 98 UMBenzo[k]fluoranthene 207-08-9 11.00 10.60 94 UMBenzo[a]pyrene 50-32-8 11.40 24.70 96 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 19.50 87 UMDibenzo[a,h]anthracene 53-70-3 12.85 3.88 91 UMBenzo[g,h,i]perylene 191-24-2 13.17 20.40 97 UMTotal (USEPA16) PAHs - - < 181.37 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 95 2-Fluorobiphenyl 98Acenaphthene-d10 94 Terphenyl-d14 77Phenanthrene-d10 93Chrysene-d12 98Perylene-d12 100
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 4 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH1 ES 5 0.60 Job Number: S13_5116MLIMS ID Number: CL1321696 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.54 0.10 98 UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 0.40 98 UMAnthracene 120-12-7 6.02 0.18 94 UFluoranthene 206-44-0 7.37 2.72 99 UMPyrene 129-00-0 7.67 2.75 95 UMBenzo[a]anthracene 56-55-3 9.40 1.80 93 UMChrysene 218-01-9 9.45 1.93 98 UMBenzo[b]fluoranthene 205-99-2 10.96 3.00 98 UMBenzo[k]fluoranthene 207-08-9 11.00 1.02 94 UMBenzo[a]pyrene 50-32-8 11.40 2.32 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 1.73 89 UMDibenzo[a,h]anthracene 53-70-3 12.84 0.34 98 UMBenzo[g,h,i]perylene 191-24-2 13.17 1.76 97 UMTotal (USEPA16) PAHs - - < 20.33 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 96 2-Fluorobiphenyl 98Acenaphthene-d10 95 Terphenyl-d14 78Phenanthrene-d10 93Chrysene-d12 95Perylene-d12 96
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 5 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH1 ES 9 1.90 Job Number: S13_5116MLIMS ID Number: CL1321697 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 - < 0.08 - UMFluorene 86-73-7 - < 0.08 - UMPhenanthrene 85-01-8 - < 0.08 - UMAnthracene 120-12-7 - < 0.08 - UFluoranthene 206-44-0 7.37 0.36 99 UMPyrene 129-00-0 7.67 0.39 95 UMBenzo[a]anthracene 56-55-3 9.40 0.24 91 UMChrysene 218-01-9 9.45 0.20 92 UMBenzo[b]fluoranthene 205-99-2 10.96 0.39 98 UMBenzo[k]fluoranthene 207-08-9 11.00 0.16 94 UMBenzo[a]pyrene 50-32-8 11.40 0.30 98 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 0.23 95 UMDibenzo[a,h]anthracene 53-70-3 - < 0.08 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.20 72 UMTotal (USEPA16) PAHs - - < 3.08 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 96Acenaphthene-d10 98 Terphenyl-d14 76Phenanthrene-d10 97Chrysene-d12 95Perylene-d12 94
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 6 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH2 ES 2 0.15 Job Number: S13_5116MLIMS ID Number: CL1321698 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.47 0.55 97 UMAcenaphthylene 208-96-8 4.53 0.52 86 UAcenaphthene 83-32-9 4.66 8.85 94 UMFluorene 86-73-7 5.06 9.29 93 UMPhenanthrene 85-01-8D 5.96 86.30 99 UMAnthracene 120-12-7 6.02 29.20 98 UFluoranthene 206-44-0D 7.38 142.00 97 UMPyrene 129-00-0D 7.68 109.40 94 UMBenzo[a]anthracene 56-55-3 9.41 49.70 97 UMChrysene 218-01-9 9.46 48.10 97 UMBenzo[b]fluoranthene 205-99-2 10.96 48.30 98 UMBenzo[k]fluoranthene 207-08-9 11.00 18.70 96 UMBenzo[a]pyrene 50-32-8 11.40 37.80 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 24.00 86 UMDibenzo[a,h]anthracene 53-70-3 12.85 5.32 94 UMBenzo[g,h,i]perylene 191-24-2 13.16 19.00 97 UMTotal (USEPA16) PAHs - - 636.89 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 94 2-Fluorobiphenyl 95Acenaphthene-d10 95 Terphenyl-d14 75Phenanthrene-d10 96Chrysene-d12 100Perylene-d12 99
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 7 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH2 ES 4 0.50 Job Number: S13_5116MLIMS ID Number: CL1321699 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 4.66 0.61 98 UMFluorene 86-73-7 5.07 0.38 90 UMPhenanthrene 85-01-8 5.96 4.50 99 UMAnthracene 120-12-7 6.02 1.91 94 UFluoranthene 206-44-0 7.37 14.10 98 UMPyrene 129-00-0 7.67 11.40 95 UMBenzo[a]anthracene 56-55-3 9.40 5.30 96 UMChrysene 218-01-9 9.45 5.05 99 UMBenzo[b]fluoranthene 205-99-2 10.96 5.29 97 UMBenzo[k]fluoranthene 207-08-9 10.99 1.93 97 UMBenzo[a]pyrene 50-32-8 11.40 4.16 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 2.44 99 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.51 92 UMBenzo[g,h,i]perylene 191-24-2 13.16 2.13 98 UMTotal (USEPA16) PAHs - - < 59.95 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 95Acenaphthene-d10 101 Terphenyl-d14 77Phenanthrene-d10 103Chrysene-d12 109Perylene-d12 109
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 8 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH3 ES 2 0.30 Job Number: S13_5116MLIMS ID Number: CL1321700 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.46 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 94 2-Fluorobiphenyl 98Acenaphthene-d10 92 Terphenyl-d14 78Phenanthrene-d10 90Chrysene-d12 89Perylene-d12 87
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 9 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH4 ES 2 0.20 Job Number: S13_5116MLIMS ID Number: CL1321701 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.47 0.42 97 UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 0.21 98 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.92 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 97 2-Fluorobiphenyl 98Acenaphthene-d10 95 Terphenyl-d14 76Phenanthrene-d10 95Chrysene-d12 93Perylene-d12 90
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 10 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH4 ES 9 1.90 Job Number: S13_5116MLIMS ID Number: CL1321702 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.38 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 71 2-Fluorobiphenyl 98Acenaphthene-d10 95 Terphenyl-d14 77Phenanthrene-d10 92Chrysene-d12 89Perylene-d12 86
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 11 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH5 ES 2 0.20 Job Number: S13_5116MLIMS ID Number: CL1321703 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.12 98 UMPyrene 129-00-0 7.67 0.12 98 UMBenzo[a]anthracene 56-55-3 9.40 0.10 94 UMChrysene 218-01-9 9.45 0.10 86 UMBenzo[b]fluoranthene 205-99-2 10.96 0.17 93 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.40 0.13 84 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.83 0.12 98 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.12 93 UMTotal (USEPA16) PAHs - - < 1.69 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 101 2-Fluorobiphenyl 97Acenaphthene-d10 99 Terphenyl-d14 77Phenanthrene-d10 100Chrysene-d12 98Perylene-d12 95
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 12 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS1 ES 1 0.10 Job Number: S13_5116MLIMS ID Number: CL1321704 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.47 0.25 95 UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 0.16 98 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.17 96 UMPyrene 129-00-0 7.67 0.27 96 UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 9.45 0.09 76 UMBenzo[b]fluoranthene 205-99-2 10.96 0.25 93 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.40 0.18 59 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 0.15 91 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.19 82 UMTotal (USEPA16) PAHs - - < 2.33 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 81 2-Fluorobiphenyl 96Acenaphthene-d10 95 Terphenyl-d14 77Phenanthrene-d10 92Chrysene-d12 94Perylene-d12 94
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 13 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS1 ES 2 0.30 Job Number: S13_5116MLIMS ID Number: CL1321705 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.42 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 94 2-Fluorobiphenyl 98Acenaphthene-d10 92 Terphenyl-d14 77Phenanthrene-d10 92Chrysene-d12 90Perylene-d12 90
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 14 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS2 ES 1 0.10 Job Number: S13_5116MLIMS ID Number: CL1321706 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 3.47 0.41 95 UMAcenaphthylene 208-96-8 4.53 0.90 86 UAcenaphthene 83-32-9 4.66 29.20 94 UMFluorene 86-73-7 5.06 32.80 94 UMPhenanthrene 85-01-8D 5.97 181.00 97 UMAnthracene 120-12-7D 6.02 70.40 98 UFluoranthene 206-44-0D 7.38 205.00 96 UMPyrene 129-00-0D 7.68 153.00 92 UMBenzo[a]anthracene 56-55-3D 9.41 66.80 97 UMChrysene 218-01-9D 9.46 60.50 97 UMBenzo[b]fluoranthene 205-99-2D 10.97 61.70 98 UMBenzo[k]fluoranthene 207-08-9 11.00 23.50 94 UMBenzo[a]pyrene 50-32-8 11.40 46.40 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 27.50 87 UMDibenzo[a,h]anthracene 53-70-3 12.85 6.62 93 UMBenzo[g,h,i]perylene 191-24-2 13.17 24.00 97 UMTotal (USEPA16) PAHs - - 988.66 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 99 2-Fluorobiphenyl 94Acenaphthene-d10 100 Terphenyl-d14 74Phenanthrene-d10 104Chrysene-d12 110Perylene-d12 107
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 15 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS2 ES 2 0.30 Job Number: S13_5116MLIMS ID Number: CL1321707 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 4.66 0.45 96 UMFluorene 86-73-7 5.06 0.46 90 UMPhenanthrene 85-01-8 5.96 3.01 99 UMAnthracene 120-12-7 6.02 1.95 98 UFluoranthene 206-44-0 7.37 5.58 98 UMPyrene 129-00-0 7.67 4.43 94 UMBenzo[a]anthracene 56-55-3 9.40 2.10 96 UMChrysene 218-01-9 9.45 2.11 95 UMBenzo[b]fluoranthene 205-99-2 10.96 2.16 98 UMBenzo[k]fluoranthene 207-08-9 11.00 0.80 93 UMBenzo[a]pyrene 50-32-8 11.40 1.70 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 1.10 88 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.20 77 UMBenzo[g,h,i]perylene 191-24-2 13.17 0.97 99 UMTotal (USEPA16) PAHs - - < 27.24 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 97 2-Fluorobiphenyl 97Acenaphthene-d10 97 Terphenyl-d14 79Phenanthrene-d10 98Chrysene-d12 105Perylene-d12 107
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 16 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS3 ES 1 0.20 Job Number: S13_5116MLIMS ID Number: CL1321708 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.54 0.13 100 UAcenaphthene 83-32-9 4.66 0.10 96 UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 1.26 99 UMAnthracene 120-12-7 6.02 0.44 98 UFluoranthene 206-44-0 7.37 3.32 99 UMPyrene 129-00-0 7.67 3.04 94 UMBenzo[a]anthracene 56-55-3 9.40 1.73 93 UMChrysene 218-01-9 9.45 1.80 93 UMBenzo[b]fluoranthene 205-99-2 10.96 2.79 98 UMBenzo[k]fluoranthene 207-08-9 11.00 0.92 94 UMBenzo[a]pyrene 50-32-8 11.40 2.26 99 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 1.73 84 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.31 47 UMBenzo[g,h,i]perylene 191-24-2 13.17 1.62 97 UMTotal (USEPA16) PAHs - - < 21.62 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 78 2-Fluorobiphenyl 96Acenaphthene-d10 96 Terphenyl-d14 77Phenanthrene-d10 96Chrysene-d12 100Perylene-d12 102
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 17 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS3 ES 7 1.00 Job Number: S13_5116MLIMS ID Number: CL1321709 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.10 99 UMPyrene 129-00-0 7.67 0.10 97 UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 10.96 0.10 79 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.48 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 95 2-Fluorobiphenyl 95Acenaphthene-d10 95 Terphenyl-d14 77Phenanthrene-d10 96Chrysene-d12 97Perylene-d12 98
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 18 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS4 ES 2 0.20 Job Number: S13_5116MLIMS ID Number: CL1321710 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.48 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 69 2-Fluorobiphenyl 96Acenaphthene-d10 94 Terphenyl-d14 76Phenanthrene-d10 95Chrysene-d12 96Perylene-d12 96
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 19 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS5 ES 4 0.60 Job Number: S13_5116MLIMS ID Number: CL1321711 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.97 0.20 98 UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 7.37 0.35 99 UMPyrene 129-00-0 7.67 0.28 96 UMBenzo[a]anthracene 56-55-3 9.40 0.14 94 UMChrysene 218-01-9 9.45 0.12 98 UMBenzo[b]fluoranthene 205-99-2 10.96 0.18 95 UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 11.40 0.12 84 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.83 0.09 90 UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 13.17 0.09 72 UMTotal (USEPA16) PAHs - - < 2.20 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 98 2-Fluorobiphenyl 97Acenaphthene-d10 98 Terphenyl-d14 79Phenanthrene-d10 98Chrysene-d12 101Perylene-d12 99
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 20 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS5 ES 6 1.20 Job Number: S13_5116MLIMS ID Number: CL1321712 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 4.54 0.10 98 UAcenaphthene 83-32-9 4.66 0.24 98 UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 5.96 1.25 99 UMAnthracene 120-12-7 6.02 0.76 97 UFluoranthene 206-44-0 7.37 7.87 98 UMPyrene 129-00-0 7.67 6.97 94 UMBenzo[a]anthracene 56-55-3 9.40 3.72 94 UMChrysene 218-01-9 9.45 3.72 99 UMBenzo[b]fluoranthene 205-99-2 10.96 5.04 98 UMBenzo[k]fluoranthene 207-08-9 11.00 1.86 94 UMBenzo[a]pyrene 50-32-8 11.40 4.01 97 UMIndeno[1,2,3-cd]pyrene 193-39-5 12.82 2.70 88 UMDibenzo[a,h]anthracene 53-70-3 12.85 0.52 97 UMBenzo[g,h,i]perylene 191-24-2 13.17 2.66 92 UMTotal (USEPA16) PAHs - - < 41.60 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 97 2-Fluorobiphenyl 97Acenaphthene-d10 96 Terphenyl-d14 77Phenanthrene-d10 96Chrysene-d12 100Perylene-d12 100
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 21 of 88
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: WS5 ES 8 2.50 Job Number: S13_5116MLIMS ID Number: CL1321713 Date Booked in: 30-Aug-13QC Batch Number: 130720 Date Extracted: 05-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 0513PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.08 - UMAcenaphthylene 208-96-8 - < 0.08 - UAcenaphthene 83-32-9 - < 0.08 - UMFluorene 86-73-7 - < 0.08 - UMPhenanthrene 85-01-8 - < 0.08 - UMAnthracene 120-12-7 - < 0.08 - UFluoranthene 206-44-0 - < 0.08 - UMPyrene 129-00-0 - < 0.08 - UMBenzo[a]anthracene 56-55-3 - < 0.08 - UMChrysene 218-01-9 - < 0.08 - UMBenzo[b]fluoranthene 205-99-2 - < 0.08 - UMBenzo[k]fluoranthene 207-08-9 - < 0.08 - UMBenzo[a]pyrene 50-32-8 - < 0.08 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.08 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.08 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.08 - UMTotal (USEPA16) PAHs - - < 1.35 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 96 2-Fluorobiphenyl 97Acenaphthene-d10 98 Terphenyl-d14 77Phenanthrene-d10 99Chrysene-d12 98Perylene-d12 96
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 22 of 88
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: Soil
Job Number: s13_5116 Date Booked in: 30-Aug-13
Directory: D:\TES\DATA\Y2013\0904HSA_GC12\090413 2013-09-04 14-26-43\127B2701.D Date extracted: 04-Sep-13
Method: Headspace GCFID Date Analysed: 04-Sep-13, 23:03:42Accreditation Code: UM
* Sample data with an asterisk are not UKAS accredi ted.
Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
CL1321695 BH1 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321696 BH1 ES 5 0.60 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321697 BH1 ES 9 1.90 <0.010 <0.010 <0.010 <0.010 <0.010 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321698 BH2 ES 2 0.15 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321699 BH2 ES 4 0.50 <0.010 <0.010 <0.010 <0.010 <0.010 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321700 BH3 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321701 BH4 ES 2 0.20 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321702 BH4 ES 9 1.90 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321703 BH5 ES 2 0.20 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321704 WS1 ES 1 0.10 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321705 WS1 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321706 WS2 ES 1 0.10 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321707 WS2 ES 2 0.30 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321708 WS3 ES 1 0.20 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321709 WS3 ES 7 1.00 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321710 WS4 ES 2 0.20 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321711 WS5 ES 4 0.60 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321712 WS5 ES 6 1.20 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
CL1321713 WS5 ES 8 2.50 <0.011 <0.011 <0.011 <0.011 <0.011 <0.2 <0.2 <0.2 <0.2 <0.2
Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 23 of 88
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: SoilJob Number: S13_5116 Separation: Silica gel Date Booked in: 30-Aug-13QC Batch Number: 130720 Eluents: Hexane, DCM Date Extracted: 05-Sep-13Directory: D:\TES\DATA\Y2013\02\0906TPH_GC3\059B6201.D Date Analysed: 06-Sep-13Method: Ultra Sonic
This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aro matics Aliphatics Aromatics Aliphatics Aromatics Aliphat ics Aromatics
CL1321695 BH1 ES 2 0.30 <4 6.85 <4 <4 6.67 <4 10 49.4 111 888 174 1150
CL1321696 BH1 ES 5 0.60 <4 10.9 <4 <4 <4 <4 <4 10.5 <9.71 112 <22 151
CL1321697 BH1 ES 9 1.90 <4 4.86 <4 <4 <4 <4 <4 <4 <9.16 13.5 <21 22.5
CL1321698 BH2 ES 2 0.15 <5 <5 <5 <5 5.9 42.3 11.3 485 146 1660 199 2350
CL1321699 BH2 ES 4 0.50 <4 <4 <4 <4 <4 <4 <4 30.6 <9.17 147 <21 190
CL1321700 BH3 ES 2 0.30 <5 20.7 <5 <5 <5 <5 <5 <5 <10.01 <10.01 <23 27.7
CL1321701 BH4 ES 2 0.20 <5 <5 <5 <5 <5 <5 <5 <5 <10.14 11.3 <23 <23
CL1321702 BH4 ES 9 1.90 <4 <4 <4 <4 <4 <4 <4 <4 <9.46 <9.46 <22 <22
CL1321703 BH5 ES 2 0.20 <4 7.39 <4 <4 <4 <4 <4 <4 <9.55 14.5 <22 26
CL1321704 WS1 ES 1 0.10 <4 16.6 <4 <4 <4 <4 9.2 12 384 662 572 1000
CL1321705 WS1 ES 2 0.30 <4 14.7 <4 <4 <4 <4 <4 <4 <9.72 31.7 <22 60.9
CL1321706 WS2 ES 1 0.10 <4 8.68 <4 <4 9.9 129 26.4 1030 388 2450 584 3940
CL1321707 WS2 ES 2 0.30 <4 <4 <4 <4 <4 <4 <4 13.6 <9.29 72.9 <21 95.1
CL1321708 WS3 ES 1 0.20 <5 <5 <5 <5 <5 <5 <5 16.8 29.3 174 35.9 226
CL1321709 WS3 ES 7 1.00 <4 30.2 <4 <4 <4 <4 <4 <4 <9.82 12.7 <22 47.6
CL1321710 WS4 ES 2 0.20 <5 34.4 <5 <5 <5 <5 <5 <5 <10.12 13 <23 52
CL1321711 WS5 ES 4 0.60 <4 <4 <4 <4 <4 <4 <4 <4 <9.77 14.9 <22 <22
CL1321712 WS5 ES 6 1.20 <4 <4 <4 <4 <4 6.27 5.6 34.3 21.8 213 29.6 272
CL1321713 WS5 ES 8 2.50 <4 <4 <4 <4 <4 <4 <4 <4 <9.27 <9.27 <21 <21
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 24 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321695ALI Job Number: S13_5116MMultiplier: 14.88 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\050F5801.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\050F5801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 25 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321695ARO Job Number: S13_5116MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\088B4401.D
min0 1 2 3 4 5
pA
0
200
400
600
800
1000
1200
1400
FID2 B, (0906TPH_GC3\088B4401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 26 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321696ALI Job Number: S13_5116MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 5 0.60Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\004F5901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\004F5901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 27 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321696ARO Job Number: S13_5116MMultiplier: 12 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 5 0.60Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\089B4501.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (0906TPH_GC3\089B4501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 28 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321697ALI Job Number: S13_5116MMultiplier: 14.56 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 9 1.90Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\005F6001.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\005F6001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 29 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321697ARO Job Number: S13_5116MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH1 ES 9 1.90Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\090B4601.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (0906TPH_GC3\090B4601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 30 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321698ALI Job Number: S13_5116MMultiplier: 14.88 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 2 0.15Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\006F6101.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\006F6101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 31 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321698ARO Job Number: S13_5116MMultiplier: 12 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 2 0.15Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\091B4701.D
min0 1 2 3 4 5
pA
0
500
1000
1500
2000
2500
3000
FID2 B, (0906TPH_GC3\091B4701.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 32 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321699ALI Job Number: S13_5116MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 4 0.50Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\007F6201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\007F6201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 33 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321699ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH2 ES 4 0.50Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\092B4801.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (0906TPH_GC3\092B4801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 34 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321700ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH3 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\008F6301.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\008F6301.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 35 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321700ARO Job Number: S13_5116MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH3 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\093B4901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (0906TPH_GC3\093B4901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 36 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321701ALI Job Number: S13_5116MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 2 0.20Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\009F6401.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\009F6401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 37 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321701ARO Job Number: S13_5116MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 2 0.20Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\094B5001.D
min0 1 2 3 4 5
pA
0
200
400
600
800
1000
FID2 B, (0906TPH_GC3\094B5001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 38 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321702ALI Job Number: S13_5116MMultiplier: 15.04 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 9 1.90Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\010F6501.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\010F6501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 39 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321702ARO Job Number: S13_5116MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH4 ES 9 1.90Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\095B5101.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (0906TPH_GC3\095B5101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 40 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321703ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 2 0.20Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\011F6601.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\011F6601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 41 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321703ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 ES 2 0.20Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\096B5201.D
min0 1 2 3 4 5
pA
0
200
400
600
800
1000
FID2 B, (0906TPH_GC3\096B5201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 42 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321704ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 1 0.10Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\012F6701.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\012F6701.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 43 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321704ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 1 0.10Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\097B5301.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (0906TPH_GC3\097B5301.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 44 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321705ALI Job Number: S13_5116MMultiplier: 14.88 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 2 0.30Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\013F6801.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\013F6801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 45 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321705ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS1 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\098B5401.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (0906TPH_GC3\098B5401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 46 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321706ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 1 0.10Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\014F6901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\014F6901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 47 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321706ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 1 0.10Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\099B5501.D
min0 1 2 3 4 5
pA
0
500
1000
1500
2000
2500
3000
3500
4000
4500
FID2 B, (0906TPH_GC3\099B5501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 48 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321707ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 2 0.30Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\015F7001.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\015F7001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 49 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321707ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS2 ES 2 0.30Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\100B5601.D
min0 1 2 3 4 5
pA
0
200
400
600
800
1000
1200
FID2 B, (0906TPH_GC3\100B5601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 50 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321708ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 1 0.20Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\016F7101.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\016F7101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 51 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321708ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 1 0.20Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\054B5701.D
min0 1 2 3 4 5
pA
0
200
400
600
800
1000
FID2 B, (0906TPH_GC3\054B5701.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 52 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321709ALI Job Number: S13_5116MMultiplier: 14.72 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 7 1.00Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\017F7201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\017F7201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 53 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321709ARO Job Number: S13_5116MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS3 ES 7 1.00Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\055B5801.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (0906TPH_GC3\055B5801.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 54 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321710ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 2 0.20Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\018F7301.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\018F7301.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 55 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321710ARO Job Number: S13_5116MMultiplier: 11.52 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS4 ES 2 0.20Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\056B5901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
FID2 B, (0906TPH_GC3\056B5901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 56 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321711ALI Job Number: S13_5116MMultiplier: 15.36 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 4 0.60Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\019F7401.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\019F7401.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 57 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321711ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 4 0.60Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\057B6001.D
min0 1 2 3 4 5
pA
0
200
400
600
800
1000
FID2 B, (0906TPH_GC3\057B6001.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 58 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321712ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 6 1.20Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\020F7501.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\020F7501.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 59 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321712ARO Job Number: S13_5116MMultiplier: 11.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 6 1.20Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\058B6101.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
600
700
800
900
FID2 B, (0906TPH_GC3\058B6101.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 60 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321713ALI Job Number: S13_5116MMultiplier: 15.2 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 8 2.50Acquisition Date/Time: 07-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\021F7601.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0906TPH_GC3\021F7601.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 61 of 88
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321713ARO Job Number: S13_5116MMultiplier: 11.36 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: WS5 ES 8 2.50Acquisition Date/Time: 06-Sep-13Datafile: D:\TES\DATA\Y2013\02\0906TPH_GC3\059B6201.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID2 B, (0906TPH_GC3\059B6201.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 62 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH1 ES 5 0.60 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321696 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 4
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 6 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 90 Dibromofluoromethane 1161,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 90 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 83Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 691,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 58m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 27Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 63 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH1 ES 9 1.90 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321697 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 5
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 2 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 93 Dibromofluoromethane 1141,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 93 Toluene-d8 99
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 91Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 791,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 76m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 49Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 64 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH2 ES 2 0.15 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321698 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 6
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 1 M UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 4 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 26 75 UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.27 14 M UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 5.07 8 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 80 Dibromofluoromethane 1221,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 76 Toluene-d8 96
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 59Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 421,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 34m and p-Xylene 108-38-3/106-42-3 5.64 6 M UM Naphthalene-d8 7.25 11Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 65 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH2 ES 4 0.50 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321699 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 7
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 4 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 88 Dibromofluoromethane 1151,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 88 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 84Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 721,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 67m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 42Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 66 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH3 ES 2 0.30 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321700 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 8
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 1 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 94 Dibromofluoromethane 1151,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 95 Toluene-d8 98
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 92Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 831,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 79m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 54Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 67 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH4 ES 2 0.20 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321701 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 9
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 23 68 UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 85 Dibromofluoromethane 1171,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 80 Toluene-d8 95
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 61Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 411,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 33m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 8Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 68 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH4 ES 9 1.90 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321702 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 10
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 5 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 93 Dibromofluoromethane 1101,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 91 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 86Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 731,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 66m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 37Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 69 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 ES 2 0.20 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321703 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 11
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 2 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 94 Dibromofluoromethane 1141,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 92 Toluene-d8 98
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 88Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 781,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 69m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 41Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 70 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS1 ES 1 0.10 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321704 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 12
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 2 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 29 71 UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 5.07 8 M UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 66 Dibromofluoromethane 1351,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 63 Toluene-d8 89
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 40Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 241,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 18m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.26 4Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 71 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS1 ES 2 0.30 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321705 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 13
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 6 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 90 Dibromofluoromethane 1181,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 90 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 85Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 711,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 65m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 31Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 72 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS2 ES 1 0.10 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321706 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 14
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 6.22 2 M UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 4.31 2 M UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 11 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 7.26 31 M UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 84 Dibromofluoromethane 1101,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 81 Toluene-d8 93
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 66Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 501,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.38 42m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 15Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 73 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS2 ES 2 0.30 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321707 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 15
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 2 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 90 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 91 Toluene-d8 98
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 88Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 801,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 76m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 60Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 74 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS3 ES 1 0.20 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321708 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 16
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 4 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 9 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 4 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 4 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 4 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 83 Dibromofluoromethane 1171,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 83 Toluene-d8 94
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 69Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 491,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 40m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 14Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 75 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS3 ES 7 1.00 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321709 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 17
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 4 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 88 Dibromofluoromethane 1171,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 89 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 84Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 711,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 65m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 37Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 76 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS4 ES 2 0.20 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321710 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 18
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 6 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 84 Dibromofluoromethane 1211,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 85 Toluene-d8 96
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 78Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 631,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 52m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 23Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 77 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 4 0.60 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321711 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 19
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 4 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 89 Dibromofluoromethane 1141,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 89 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 81Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 681,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 58m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 31Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 78 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 6 1.20 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321712 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 20
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 5 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 89 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 89 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 81Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 681,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 59m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.25 34Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 79 of 88
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: WS5 ES 8 2.50 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321713 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5116M Operator: TP Position: 21
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 5 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 - < 1 - UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 5 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 5 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 91 Dibromofluoromethane 1121,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 92 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 92Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 841,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 81m and p-Xylene 108-38-3/106-42-3 - < 4 - UM Naphthalene-d8 7.24 75Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 80 of 88
Page 1 of 1
Report No:
Report Date: 06/09/2013Project Number:
Sample Number
Sample Date
Sample Location Test DateTotal Sample Dry Weight
(g)
Weight of <2mm
Fraction (g)
Asbestos(g) in >8mm+>2mm
Asbestos(g) in <2mm
% Asbestos by weight of Total Dried Sample
CL/1321695 07/08/13 BH1 0.30 05/09/2013 Screen OnlyCL/1321696 07/08/13 BH1 0.60 05/09/2013 Screen OnlyCL/1321697 07/08/13 BH1 1.90 05/09/2013 Screen OnlyCL/1321698 07/08/13 BH2 0.15 05/09/2013 Screen OnlyCL/1321699 07/08/13 BH2 0.50 05/09/2013 Screen OnlyCL/1321700 06/08/13 BH3 0.30 05/09/2013 Screen OnlyCL/1321701 05/08/13 BH4 0.20 05/09/2013 Screen OnlyCL/1321702 05/08/13 BH4 1.90 05/09/2013 Screen OnlyCL/1321703 06/08/13 BH5 0.20 05/09/2013 Screen OnlyCL/1321704 05/08/13 WS1 0.10 05/09/2013 Screen OnlyCL/1321705 05/08/13 WS1 0.30 05/09/2013 Screen OnlyCL/1321706 05/08/13 WS2 0.10 05/09/2013 Screen & IDCL/1321707 05/08/13 WS2 0.30 05/09/2013 Screen OnlyCL/1321708 05/08/13 WS3 0.20 05/09/2013 Screen OnlyCL/1321709 05/08/13 WS3 1.00 05/09/2013 Screen OnlyCL/1321710 05/08/13 WS4 0.20 05/09/2013 Screen OnlyCL/1321711 05/08/13 WS5 0.60 05/09/2013 Screen OnlyCL/1321712 05/08/13 WS5 1.20 05/09/2013 Screen OnlyCL/1321713 05/08/13 WS5 2.50 05/09/2013 Screen Only
Name: Louise JamesAuthorised Signatory:
Position: Lab Project Manager
Sampling has been carried out by a third party
For the attention of:
Address:
ESG Environmental Chemistry
ANO-0488-06722Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent
Client:
Detection limit of Method SCI-ASB-020 is 0.001%
ESG Asbestos Limited Certificate of Analysis for As bestos in Soils
ESG Southam
Asbestos Fibre Types Identified
ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS
S135116Gnossall St Lawrence Primary School
NAIISNAIIS
Site Address:
NAIISNAIIS
NAIISNAIISNAIIS
NAIISNAIIS
NAIIS
Chrysotile(Free Fibres)NAIISNAIISNAIISNAIISNAIIS
NAIISNAIIS
The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.
NAACR = Not Analysed at Clients Request NAIIS = No A sbestos Identified in Sample (Screens Only)
NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys
NAIIS
1089
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 81 of 88
SOIL Analysis S135116
CustomerSiteReport No S135116
MethodID
CA
LC_C
R3
CE
N Leachate
CustS
erv
GR
OH
SA
ICP
BO
R
ICP
MS
S
ICP
SO
IL
ICP
WS
S
KO
NE
CR
MC
ertS
PA
HM
SU
S
PH
SO
IL
ID Number Description Sampled
Chrom
ium (III)
CE
N Leac(P
)1
Report B
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
SO
4-- (H2O
sol) mg/l
Chrom
ium vi:
MC
ertS A
nalysis
PA
H (16) by G
CM
S
pH units (A
R)
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
CL/1321695 BH1 0.30 07/08/13CL/1321696 BH1 0.60 07/08/13CL/1321697 BH1 1.90 07/08/13CL/1321698 BH2 0.15 07/08/13CL/1321699 BH2 0.50 07/08/13CL/1321700 BH3 0.30 06/08/13CL/1321701 BH4 0.20 05/08/13CL/1321702 BH4 1.90 05/08/13CL/1321703 BH5 0.20 06/08/13CL/1321704 WS1 0.10 05/08/13CL/1321705 WS1 0.30 05/08/13CL/1321706 WS2 0.10 05/08/13CL/1321707 WS2 0.30 05/08/13CL/1321708 WS3 0.20 05/08/13CL/1321709 WS3 1.00 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 82 of 88
SOIL Analysis S135116
CustomerSiteReport No S135116
MethodID
SF
AP
I
Sub002a
TM
SS
TP
HU
SS
I
TS
BR
E1
VO
CH
SA
S
WS
LM59
ID Number Description Sampled
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
Total S
ulphur.
VO
C H
SA
-GC
MS
Total O
rganic Carbon
���� ���� ���� ���� ���� ����
CL/1321695 BH1 0.30 07/08/13CL/1321696 BH1 0.60 07/08/13CL/1321697 BH1 1.90 07/08/13CL/1321698 BH2 0.15 07/08/13CL/1321699 BH2 0.50 07/08/13CL/1321700 BH3 0.30 06/08/13CL/1321701 BH4 0.20 05/08/13CL/1321702 BH4 1.90 05/08/13CL/1321703 BH5 0.20 06/08/13CL/1321704 WS1 0.10 05/08/13CL/1321705 WS1 0.30 05/08/13CL/1321706 WS2 0.10 05/08/13CL/1321707 WS2 0.30 05/08/13CL/1321708 WS3 0.20 05/08/13CL/1321709 WS3 1.00 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 83 of 88
SOIL Analysis S135116
CustomerSiteReport No S135116
MethodID
CA
LC_C
R3
CE
N Leachate
CustS
erv
GR
OH
SA
ICP
BO
R
ICP
MS
S
ICP
SO
IL
ICP
WS
S
KO
NE
CR
MC
ertS
PA
HM
SU
S
PH
SO
IL
ID Number Description Sampled
Chrom
ium (III)
CE
N Leac(P
)1
Report B
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
SO
4-- (H2O
sol) mg/l
Chrom
ium vi:
MC
ertS A
nalysis
PA
H (16) by G
CM
S
pH units (A
R)
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
CL/1321710 WS4 0.20 05/08/13CL/1321711 WS5 0.60 05/08/13CL/1321712 WS5 1.20 05/08/13CL/1321713 WS5 2.50 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 84 of 88
SOIL Analysis S135116
CustomerSiteReport No S135116
MethodID
SF
AP
I
Sub002a
TM
SS
TP
HU
SS
I
TS
BR
E1
VO
CH
SA
S
WS
LM59
ID Number Description Sampled
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
Total S
ulphur.
VO
C H
SA
-GC
MS
Total O
rganic Carbon
���� ���� ���� ���� ���� ����
CL/1321710 WS4 0.20 05/08/13CL/1321711 WS5 0.60 05/08/13CL/1321712 WS5 1.20 05/08/13CL/1321713 WS5 2.50 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 85 of 88
Report Number : EFS/135116
Method Code
Sample IDThe following information should be taken into cons ideration when using the
data contained within this report
VOCHSAS CL/1321698
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1321701
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1321704
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1321706
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
VOCHSAS CL/1321708
Due to matrix interference, the Internal Standard recovery for this Test is below the required QMS specification. This has been confirmed by repeating the analysis. All other Laboratory Process Controls meet the requirements of the QMS. These circumstances should be taken into consideration when utilising the data
Additional Report Notes
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135116M Ver. 1Page 86 of 88
Matrix MethodID Analysis Basis
Method Description
Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium
Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID
Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection
Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS
Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection
Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection
Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection
Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection
Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.
Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on
oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil
with GCFID detection including quantitation of Aromatic and Aliphatic fractions.
Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection
Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS
Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection
Report Number: EFS/135116
Method Descriptions
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 87 of 88
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
Where individual results are flagged see report notes for status.EFS/135116M Ver. 1Page 88 of 88
Client : ESG Southam
Site : Gnossall St Lawrence Primary School
Report Number : S13_5116M
Note: major constituent in upper case
Lab ID Number Client ID
CL/1321695 BH1 ES 2 0.30CL/1321696 BH1 ES 5 0.60CL/1321697 BH1 ES 9 1.90CL/1321698 BH2 ES 2 0.15CL/1321699 BH2 ES 4 0.50CL/1321700 BH3 ES 2 0.30CL/1321701 BH4 ES 2 0.20CL/1321702 BH4 ES 9 1.90CL/1321703 BH5 ES 2 0.20CL/1321704 WS1 ES 1 0.10CL/1321705 WS1 ES 2 0.30CL/1321706 WS2 ES 1 0.10CL/1321707 WS2 ES 2 0.30CL/1321708 WS3 ES 1 0.20CL/1321709 WS3 ES 7 1.00CL/1321710 WS4 ES 2 0.20CL/1321711 WS5 ES 4 0.60CL/1321712 WS5 ES 6 1.20CL/1321713 WS5 ES 8 2.50
Sample Descriptions
Grey Stone SILT
Brown Stone SAND Brown MADE GROUND
Brown Stone SILT Brown Stone SILT
Brown Stone SAND Brown Stone SILT
Brown Stone SAND Grey Stone SILT
Grey Stone SAND
Grey Stone SILT Brown Stone SAND
Brown Stone SILT Brown Stone SAND Brown Stone SILT Brown Stone SILT
Brown Stone SAND
Description
Grey Stone SILT Brown Stone SILT
Appendix A Page 1 of 1 END OF REPORT
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnossall St Lawrence Primary School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS or MCERTS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 11-Sep-2013Declan Burns Operations Director
Laboratory and Analytical Business
11-Sep-2013
The 1 sample described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTSOIL SAMPLE ANALYSIS
Report No. EFS/135126M (Ver. 1)
ESG accepts no responsibility for any sampling not carried out by our personnel.
Table 1 Main Analysis Results (Pages 2 to 3)Table of PAH (MS-SIM) (80) Results (Page 4)Table of GRO Results (Page 5)Table of TPH (Si) banding (std) (Page 6)GC-FID Chromatograms (Pages 7 to 8)Table of VOC (HSA) Results (Page 9)Table of Asbestos Results (Page 10)Analytical and Deviating Sample Overview (Pages 11 to 12)Table of Method Descriptions (Page 13)Table of Report Notes (Page 14)Table of Sample Descriptions (Appendix A Page 1 of 1)
Tests marked '^' have been subcontracted to another laboratory.
All results are reported on a dry weight basis at 105oC unless otherwise stated. (except QC samples)
Accreditation Codes: N (Not Accredited), U (UKAS), UM (UKAS & MCERTS)
(NVM) - denotes the sample matrix is dissimilar to matrices upon which the MCERTS validation was based,and is therefore not accredited for MCERTS.
Where individual results are flagged see report notes for status.EFS/135126M Ver. 1Page 1 of 14
Units : mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kg mg/kgMethod Codes : GROHSA ICPBOR ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPMSS ICPSOIL ICPSOIL
Method Reporting Limits : 0.2 0.5 0.1 0.3 0.2 1.2 1.6 0.7 0.5 0.5 2 0.5 0.6 16 1 0.1Accreditation Code: UM U UM UM UM UM UM UM UM UM UM U UM UM UM
LAB
ID N
umber C
L/
Client Sample Description
Sam
ple Date
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
1321755 BH5 D 1.10 05-Aug-13 Req <0.5 0.4 4.9 <0.20 19.8 21 25.0 <0.5 0.5 16.1 <0.5 31.8 57.5 75.2 0.66
Contact
Date Printed
Report Number EFS/135126M
Table Number 1
Fax +44 (0) 1283 554422
Soil Sample Analysis
Mr J Litten
11-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 2 of 14
Units : mg/kg mg/kg pH Units mg/kg mg/kg % mg/kg µg/kg mg/kg mg/kg % % M/M mg/kgMethod Codes : ICPSOIL ICPWSS PHSOIL SFAPI SFAPI Sub002a TMSS TPHUSSI VOCHSAS CALC_CR3 KONECR TSBRE1 WSLM59 PAHMSUS
Method Reporting Limits : 36 10 0.5 0.5 0.2 10 0.5 0.1 0.005 0.02Accreditation Code: UM UM UM UM U U U N N N N
LAB
ID N
umber C
L/
Client Sample Description
Sam
ple Date
Iron
SO
4-- (H2O
sol) mg/l
pH units (A
R)
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
VO
C H
SA
-GC
MS
Chrom
ium (III)
Chrom
ium vi:
Total S
ulphur.
Total O
rganic Carbon
PA
H (16) by G
CM
S
1321755 BH5 D 1.10 05-Aug-13 19400 26 7.7 <0.6 <0.6 NAIIS 13.8 Req Req <19.8 <0.1 0.019 0.74 Req
Contact
Date Printed
Report Number EFS/135126M
Table Number 1
Fax +44 (0) 1283 554422
Soil Sample Analysis
Mr J Litten
11-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 3 of 14
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St Lawrence Primary SchoolSample Details: BH5 D 1.10 Job Number: S13_5126MLIMS ID Number: CL1321755 Date Booked in: 30-Aug-13QC Batch Number: 130716 Date Extracted: 04-Sep-13
Quantitation File: Initial Calibration Date Analysed: 05-Sep-13Directory: 0413PAH.GC5\ Matrix: SoilDilution: 1.0 Ext Method: Ultrasonic
Accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit Accr.
(min) mg/kg code
Naphthalene 91-20-3 - < 0.09 - UMAcenaphthylene 208-96-8 - < 0.09 - UAcenaphthene 83-32-9 - < 0.09 - UMFluorene 86-73-7 - < 0.09 - UMPhenanthrene 85-01-8 - < 0.09 - UMAnthracene 120-12-7 - < 0.09 - UFluoranthene 206-44-0 - < 0.09 - UMPyrene 129-00-0 - < 0.09 - UMBenzo[a]anthracene 56-55-3 - < 0.09 - UMChrysene 218-01-9 - < 0.09 - UMBenzo[b]fluoranthene 205-99-2 - < 0.09 - UMBenzo[k]fluoranthene 207-08-9 - < 0.09 - UMBenzo[a]pyrene 50-32-8 - < 0.09 - UMIndeno[1,2,3-cd]pyrene 193-39-5 - < 0.09 - UMDibenzo[a,h]anthracene 53-70-3 - < 0.09 - UMBenzo[g,h,i]perylene 191-24-2 - < 0.09 - UMTotal (USEPA16) PAHs - - < 1.48 - N
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 85 2-Fluorobiphenyl 99Acenaphthene-d10 88 Terphenyl-d14 80Phenanthrene-d10 85Chrysene-d12 83Perylene-d12 86
Concentrations are reported on a dry weight basis.
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 4 of 14
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: Soil
Job Number: S13_5126 Date Booked in: 30-Aug-13
Directory: D:\TES\DATA\Y2013\0905HSA_GC12\090513 2013-09-05 09-59-58\035F3701.D Date extracted: 05-Sep-13
Method: Headspace GCFID Date Analysed: 05-Sep-13, 21:49:27Accreditation Code: UM
* Sample data with an asterisk are not UKAS accredi ted.
Concentration, (mg/kg) - as dry weight. AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
CL1321755 BH5 D 1.10 <0.012 <0.012 <0.012 <0.012 <0.012 <0.2 <0.2 <0.2 <0.2 <0.2
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 5 of 14
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : Gnossall St Lawrence Primary School Matrix: SoilJob Number: S13_5126 Separation: Silica gel Date Booked in: 30-Aug-13QC Batch Number: 130716 Eluents: Hexane, DCM Date Extracted: 04-Sep-13Directory: D:\TES\DATA\Y2013\02\0905TPH_GC3\065B1901.D Date Analysed: 05-Sep-13Method: Ultra Sonic
This sample data is not MCERTS accredited. Concentration, (mg/kg) - as dry weight.* This sample data is not ISO17025 accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aro matics Aliphatics Aromatics Aliphatics Aromatics Aliphat ics Aromatics
CL1321755 BH5 D 1.10 <5 <5 <5 <5 <5 <5 <5 <5 <10.16 <10.16 <23 <23
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 6 of 14
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: CL1321755ALI Job Number: S13_5126MMultiplier: 14.88 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 D 1.10Acquisition Date/Time: 05-Sep-13Datafile: D:\TES\DATA\Y2013\02\0905TPH_GC3\015F1901.D
min0 1 2 3 4 5
pA
0
100
200
300
400
500
FID1 A, (0905TPH_GC3\015F1901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 7 of 14
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: CL1321755ARO Job Number: S13_5126MMultiplier: 11.84 Client: ESG SouthamDilution: 1 Site: Gnossall St Lawrence Primary SchoolAcquisition Method: 5UL_RUNF.M Client Sample Ref: BH5 D 1.10Acquisition Date/Time: 05-Sep-13Datafile: D:\TES\DATA\Y2013\02\0905TPH_GC3\065B1901.D
min0 1 2 3 4 5
pA
0
50
100
150
200
250
300
350
400
450
FID2 B, (0905TPH_GC3\065B1901.D)
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appr opriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 8 of 14
Volatile Organic Compounds by HSA-GCMS
Accredited?: YesCustomer and Site Details: ESG Southam: Gnossall St Lawrence Primary School Directory/Quant file: 903VOC_MS19\ Initial Calibration Matrix: SoilSample Details: BH5 D 1.10 Date Booked in: 30-Aug-13 Method: HeadspaceLIMS ID Number: CL1321755 Date Analysed: 03-Sep-13 Multiplier: 1Job Number: S13_5126M Operator: TP Position: 2
Target Compounds CAS # R.T. Concentration % Fit Accr. Target Compounds CAS # R.T. Concentration % Fit Accr.(min.) µg/kg code (min.) µg/kg code
Dichlorodifluoromethane 75-71-8 ** - < 1 - N o-Xylene 95-47-6 - < 2 - UM
Chloromethane 74-87-3 * - < 3 - N Styrene 100-42-5 - < 1 - UM
Vinyl Chloride 75-01-4 - < 1 - UM Bromoform 75-25-2 - < 1 - UM
Bromomethane 74-83-9 - < 1 - UM iso-Propylbenzene 98-82-8 - < 1 - UM
Chloroethane 75-00-3 - < 2 - UM 1,1,2,2-Tetrachloroethane 79-34-5 ** - < 1 - N
Trichlorofluoromethane 75-69-4 - < 1 - UM Propylbenzene 103-65-1 - < 1 - UM
1,1-Dichloroethene 75-35-48 * - < 1 - N Bromobenzene 108-86-1 - < 1 - UM
trans 1,2-Dichloroethene 156-60-5 - < 1 - UM 1,2,3-Trichloropropane 96-18-4 - < 1 - UM
1,1-Dichloroethane 75-34-3 - < 1 - UM 2-Chlorotoluene 95-49-8 - < 1 - UM
MTBE 1634-04-4 - < 1 - UM 1,3,5-Trimethylbenzene 108-67-8 - < 1 - UM
2,2-Dichloropropane 594-20-7 - < 1 - UM 4-Chlorotoluene 106-43-4 - < 1 - UM
cis 1,2-Dichloroethene 156-59-2 - < 6 - UM tert-Butylbenzene 98-06-6 - < 1 - UM
Bromochloromethane 74-97-5 - < 1 - UM 1,2,4-Trimethylbenzene 95-63-6 - < 1 - UM
Chloroform 67-66-3 - < 1 - UM sec-Butylbenzene 135-98-8 - < 1 - UM
1,1,1-Trichloroethane 71-55-6 - < 1 - UM p-Isopropyltoluene 99-87-6 - < 1 - UM
Carbon Tetrachloride 56-23-5 - < 1 - UM 1,3-Dichlorobenzene 541-73-1 - < 1 - UM
1,1-Dichloropropene 563-58-6 - < 1 - UM 1,4-Dichlorobenzene 106-46-7 - < 1 - UM
Benzene 71-43-2 - < 1 - UM n-Butylbenzene 104-51-8 * - < 1 - N
1,2-Dichloroethane 107-06-2 - < 1 - UM 1,2-Dichlorobenzene 95-50-1 - < 1 - UM
Trichloroethene 79-01-6 4.58 2 M UM 1,2-Dibromo-3-chloropropane 96-12-8 - < 1 - UM
1,2-Dichloropropane 78-87-5 - < 1 - UM 1,2,4-Trichlorobenzene 120-82-1 * - < 3 - N
Dibromomethane 74-95-3 - < 1 - UM Hexachlorobutadiene 87-68-3 ** - < 2 - N
Bromodichloromethane 75-27-4 - < 1 - UM Naphthalene 91-20-3 - < 6 - UM
cis 1,3-Dichloropropene 10061-01-5 - < 1 - UM 1,2,3-Trichlorobenzene 87-61-6 - < 3 - UM
Toluene 108-88-3 - < 6 - UM Concentrations are reported on a dry weight basistrans 1,3-Dichloropropene 10061-02-6 - < 1 - UM Compounds marked ** are not UKAS or Mcerts accredited1,1,2-Trichloroethane 79-00-5 - < 1 - UM "M" denotes that % fit has been manually interpretedTetrachloroethene 127-18-4 - < 3 - UM This analysis was conducted on an 'As Recieved' basis.1,3-Dichloropropane 142-28-9 - < 1 - UM Internal standards R.T. Area % Surrogates % RecDibromochloromethane 124-48-1 - < 1 - UM Pentafluorobenzene 4.13 95 Dibromofluoromethane 1171,2-Dibromoethane 106-93-4 - < 1 - UM 1,4-Difluorobenzene 4.47 95 Toluene-d8 97
Chlorobenzene 108-90-7 - < 1 - UM Chlorobenzene-d5 5.58 92Ethylbenzene 100-41-4 - < 2 - UM Bromofluorobenzene 5.97 791,1,1,2-Tetrachloroethane 630-20-6 - < 1 - UM 1,4-Dichlorobenzene-d4 6.37 73m and p-Xylene 108-38-3/106-42-3 - < 5 - UM Naphthalene-d8 7.25 41Note: Volatile compounds degrade with time, and this may affect the integrity of the data depending on the timescale between sampling and analysis. It is recommended that analysis takes place within 7 days of sampling.
Where individual results are flagged see report notes for status.Results corrected to dry weight at 105°C where appropriate, in accordance with the MCERTS standard.
EFS/135126M Ver. 1Page 9 of 14
Page 1 of 1
Report No:
Report Date: 03/09/2013Project Number:
Sample Number
Sample Date
Sample Location Test DateTotal Sample Dry Weight
(g)
Weight of <2mm
Fraction (g)
Asbestos(g) in >8mm+>2mm
Asbestos(g) in <2mm
% Asbestos by weight of Total Dried Sample
CL/1321755 05/08/13 BH5 1.10 03/09/2013 Screen Only
Name: Louise JamesAuthorised Signatory:
Position: Lab Project Manager
The sample analysis for the above results was carried out using the procedures detailed in ESG Asbestos Limited in house method (SCI-ASB-020) based on HSE document MDHS 90 - Asbestos Contaminated Land - Draft 5 - November 1997 (withdrawn). Fibre identification was carried out using ESG Asbestos Limited in house method of transmitted/polarised light microscopy and centre stop dispersion staining (SCI-ASB-007), based on HSE’s HSG 248. The analysis of fine fraction for asbestos content only includes fibres and does not discriminate non-asbestos fibres. All fibres are assumed, unless specified, to be amphiboles. All tests were carried out at ESG Asbestos Laboratory, Ashbourne House, Bretby Business Park, Ashby Road, Burton-upon-Trent, Staffordshire. DE15 0XD, UKAS Laboratory Number 1089.
NAACR = Not Analysed at Clients Request NAIIS = No A sbestos Identified in Sample (Screens Only)
NADIS = No Asbestos Detected in Sample (ID & Quant Only)Keys
Site Address:
NAIIS
ESG Southam
Asbestos Fibre Types Identified
ASBESTOS ANALYSIS RESULTS - SOIL ANALYSIS
S135126Gnossall St Lawrence Primary School
Client:
Detection limit of Method SCI-ASB-020 is 0.001%
ESG Asbestos Limited Certificate of Analysis for As bestos in Soils Sampling has been carried out by a third party
For the attention of:
Address:
ESG Environmental Chemistry
ANO-0488-06721Etwall House, Bretby Business Park, Ashby Road, Burton upon Trent
1089
Where individual results are flagged see report notes for status.EFS/135126M Ver. 1Page 10 of 14
SOIL Analysis S135126
CustomerSiteReport No S135126
MethodID
CA
LC_C
R3
CE
N Leachate
CustS
erv
GR
OH
SA
ICP
BO
R
ICP
MS
S
ICP
SO
IL
ICP
WS
S
KO
NE
CR
MC
ertS
PA
HM
SU
S
PH
SO
IL
ID Number Description Sampled
Chrom
ium (III)
CE
N Leac(P
)1
Report B
GR
O (A
A) by H
SA
GC
-FID
Boron (H
20 Soluble)
Antim
ony (MS
)
Arsenic (M
S)
Cadm
ium (M
S)
Chrom
ium (M
S)
Copper (M
S)
Lead (MS
)
Mercury (M
S)
Molybdenum
(MS
)
Nickel (M
S)
Selenium
(MS
)
Vanadium
(MS
)
Zinc (M
S)
Barium
.
Beryllium
.
Iron
SO
4-- (H2O
sol) mg/l
Chrom
ium vi:
MC
ertS A
nalysis
PA
H (16) by G
CM
S
pH units (A
R)
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
CL/1321755 BH5 1.10 05/08/13 E E
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Where individual results are flagged see report notes for status.EFS/135126M Ver. 1Page 11 of 14
SOIL Analysis S135126
CustomerSiteReport No S135126
MethodID
SF
AP
I
Sub002a
TM
SS
TP
HU
SS
I
TS
BR
E1
VO
CH
SA
S
WS
LM59
ID Number Description Sampled
Cyanide(F
ree) (AR
)
Phenol Index.(A
R)
^Asbestos S
creen
Tot.M
oisture @ 105C
TP
H by G
CF
ID (A
R/S
i)
Total S
ulphur.
VO
C H
SA
-GC
MS
Total O
rganic Carbon
���� ���� ���� ���� ���� ����
CL/1321755 BH5 1.10 05/08/13 E E
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Where individual results are flagged see report notes for status.EFS/135126M Ver. 1Page 12 of 14
Matrix MethodID Analysis Basis
Method Description
Soil CALC_CR3 Air Dried Calculated from the difference between Total Chromium and Hexavalent Chromium
Soil GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons (GRO) by Headspace GCFID
Soil ICPBOR Air Dried Determination of Boron in soil samples by hot water extraction followed by ICPOES detection
Soil ICPMSS Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPMS
Soil ICPSOIL Air Dried Determination of Metals in soil samples by aqua regia digestion followed by ICPOES detection
Soil ICPWSS Air Dried Determination of Water Soluble Sulphate in soil samples by water extraction followed by ICPOES detection
Soil KONECR Air Dried Determination of Chromium vi in soil samples by water extraction followed by colorimetric detection
Soil PAHMSUS As Received Determination of Polycyclic Aromatic Hydrocarbons (PAH) by hexane/acetone extraction followed by GCMS detection
Soil PHSOIL As Received Determination of pH of 2.5:1 deionised water to soil extracts using pH probe.
Soil SFAPI As Received Segmented flow analysis with colorimetric detectionSoil SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Soil TMSS As Received Determination of the Total Moisture content at 105ºC by loss on
oven drying gravimetric analysisSoil TPHUSSI As Received Determination of hexane/acetone extractable Hydrocarbons in soil
with GCFID detection including quantitation of Aromatic and Aliphatic fractions.
Soil TSBRE1 Air Dried Determination of Total Carbon and/or Total Sulphur in solid samples by high temperature combustion/infrared detection
Soil VOCHSAS As Received Determination of Volatile Organic Compounds (VOC) by Headspace GCMS
Soil WSLM59 Air Dried Determination of Organic Carbon in soil using sulphurous Acid digestion followed by high temperature combustion and IR detection
Report Number: EFS/135126
Method Descriptions
Where individual results are flagged see report notes for status.EFS/135126M Ver. 1Page 13 of 14
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
Where individual results are flagged see report notes for status.EFS/135126M Ver. 1Page 14 of 14
Client : ESG Southam
Site : Gnossall St Lawrence Primary School
Report Number : S13_5126M
Note: major constituent in upper case
Lab ID Number Client ID
CL/1321755 BH5 D 1.10
Sample Descriptions
Description
Brown Stone SILT
Appendix A Page 1 of 1 END OF REPORT
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnossall St Lawrence Primary School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 20-Sep-2013Declan Burns Operations Director
Laboratory and Analytical Business
20-Sep-2013
The 19 samples described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTCEN LEACHATE 2:1
Report No. EXR/162608 (Ver. 2)
Table 1 Main Analysis Results (Pages 2 to 4)Table of Cyanide (Free) Analysis Results (Pages 5 to 25)Analytical and Deviating Sample Overview (Pages 26 to 29)Table of Method Descriptions (Page 30)Table of Report Notes (Page 31)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 KONENS ICHALW ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPWATVAR
Method Reporting Limits : 0.01 1 0.1 3 1 1 0.01 0.001 0.001 0.0001 0.001 0.001 0.002 0.002 0.01UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
pH units w
Chrom
ium (III)
Chloride as C
l w
Fluoride as F
(IC) w
Total S
ulphur as SO
4 (Dissolved) a
Calcium
as Ca (D
issolved) a
Magnesium
as Mg (D
issolved) a
Barium
as Ba (D
issolved) a
Nickel as N
i (Dissolved)
Chrom
ium as C
r (Dissolved)
Cadm
ium as C
d (Dissolved)
Copper as C
u (Dissolved)
Lead as Pb (D
issolved)
Zinc as Z
n (Dissolved)
Manganese as M
n (Dissolved)
Iron as Fe (D
issolved) a
1418768 BH1 ES 2 0.30 07-Aug-13 7.8 <0.01 4 0.4 94 40 3 0.1 0.001 0.001 <0.0001 0.007 0.001 0.034 0.148 0.05
1418769 BH1 ES 5 0.60 07-Aug-13 8.5 <0.01 12 0.8 156 84 3 0.14 0.004 0.002 <0.0001 0.012 0.001 0.035 0.101 <0.01
1418770 BH1 ES 9 1.90 07-Aug-13 7.7 <0.01 20 0.2 202 99 4 0.17 0.002 0.002 <0.0001 0.007 0.002 0.089 0.112 <0.01
1418771 BH2 ES 2 0.15 07-Aug-13 8.1 <0.01 53 0.3 44 40 2 0.19 <0.001 0.003 <0.0001 0.004 <0.001 0.096 0.019 <0.01
1418772 BH2 ES 4 0.50 07-Aug-13 8.8 <0.01 6 0.5 100 63 <1 0.11 0.002 0.008 <0.0001 0.022 0.002 0.02 0.005 0.05
1418773 BH3 ES 2 0.30 06-Aug-13 8.0 <0.01 9 0.5 17 38 7 0.22 <0.001 0.003 <0.0001 0.007 <0.001 0.134 0.004 0.02
1418774 BH4 ES 2 0.20 05-Aug-13 7.9 <0.01 4 0.4 31 45 4 0.11 0.002 0.003 <0.0001 0.01 <0.001 0.043 0.012 0.28
1418775 BH4 ES 9 1.90 05-Aug-13 8.1 <0.01 5 0.4 16 38 4 0.11 0.001 0.002 <0.0001 0.008 0.002 0.039 0.022 0.13
1418776 BH5 ES 2 0.20 06-Aug-13 8.2 <0.01 4 0.8 5 43 6 0.22 0.004 0.007 0.0001 0.013 0.004 0.087 0.125 3.44
1418777 WS1 ES 1 0.10 05-Aug-13 8.0 <0.01 4 0.3 31 55 3 0.11 <0.001 0.003 <0.0001 0.003 0.002 0.016 0.004 <0.01
1418778 WS1 ES 2 0.30 05-Aug-13 8.0 <0.01 3 0.3 9 54 3 0.13 0.002 0.003 <0.0001 0.009 0.002 0.049 0.016 0.14
1418779 WS2 ES 1 0.10 05-Aug-13 8.0 <0.01 8 0.2 128 73 9 0.14 0.003 0.002 <0.0001 0.009 0.001 0.065 0.11 0.13
1418780 WS2 ES 2 0.30 05-Aug-13 8.2 <0.01 2 2.7 15 28 2 0.18 <0.001 0.002 <0.0001 0.006 0.002 0.106 0.017 0.29
1418781 WS3 ES 1 0.20 05-Aug-13 8.2 <0.01 3 1.1 23 77 6 0.31 0.003 0.003 <0.0001 0.022 0.002 0.106 0.047 0.11
1418782 WS3 ES 7 1.00 05-Aug-13 8.2 <0.01 4 0.8 5 29 4 0.16 0.005 0.008 <0.0001 0.011 0.011 0.098 0.083 4.08
1418783 WS4 ES 2 0.20 05-Aug-13 7.9 <0.01 7 0.3 8 53 5 0.25 0.007 0.012 0.0002 0.016 0.02 0.122 0.148 5.51
1418784 WS5 ES 4 0.60 05-Aug-13 9.1 <0.01 7 0.4 15 31 4 0.5 0.008 0.009 0.0002 0.055 0.1 0.401 0.103 3.32
1418785 WS5 ES 6 1.20 05-Aug-13 8.0 <0.01 42 0.2 32 43 2 0.07 0.002 0.003 <0.0001 0.004 0.003 0.025 0.03 0.68
1418786 WS5 ES 8 2.50 05-Aug-13 8.1 <0.01 6 0.4 9 15 4 0.17 0.008 0.014 0.0003 0.013 0.008 0.071 0.247 8.25
Contact
Date Printed
Report Number EXR/162608
Table Number 1
Fax +44 (0) 1283 554422
CEN Leachate 2:1
Mr J Litten
20-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l ug/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS SFAPI SFAS Sub045 ICPWATVAR PHEHPLCVL PHEHPLCVL PHEHPLCVL
Method Reporting Limits : 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.01 0.02 0.05 5 0.01 0.0005 0.0005 0.0005UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Arsenic as A
s (Dissolved)
Boron as B
(Dissolved) a
Mercury as H
g (Dissolved)
Selenium
as Se (D
issolved)
Vanadium
as V (D
issolved)
Molybdenum
as Mo (D
issolved)
Antim
ony as Sb (D
issolved)
Am
moniacal N
itrogen as N
Chrom
ium V
I as Cr
Cyanide (T
otal) as CN
Sulphide as S
^Cyanide (F
ree) 5ug/l
Beryllium
as Be (D
issolved) a
Phenol
Cresols
Dim
ethylphenols
1418768 BH1 ES 2 0.30 07-Aug-13 0.001 0.17 <0.0001 0.002 0.005 0.005 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418769 BH1 ES 5 0.60 07-Aug-13 0.005 0.34 <0.0001 0.002 0.004 0.017 0.005 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418770 BH1 ES 9 1.90 07-Aug-13 0.002 0.23 <0.0001 0.001 0.002 0.005 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418771 BH2 ES 2 0.15 07-Aug-13 0.001 0.14 <0.0001 0.002 0.002 0.006 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418772 BH2 ES 4 0.50 07-Aug-13 0.014 0.1 <0.0001 0.003 0.022 0.006 0.003 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418773 BH3 ES 2 0.30 06-Aug-13 0.001 0.15 <0.0001 <0.001 0.002 0.003 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418774 BH4 ES 2 0.20 05-Aug-13 0.004 0.07 <0.0001 0.001 0.005 0.008 0.003 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418775 BH4 ES 9 1.90 05-Aug-13 0.007 0.07 <0.0001 <0.001 0.004 0.012 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418776 BH5 ES 2 0.20 06-Aug-13 0.003 0.1 <0.0001 <0.001 0.008 0.004 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418777 WS1 ES 1 0.10 05-Aug-13 0.001 0.05 <0.0001 0.002 0.002 0.008 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418778 WS1 ES 2 0.30 05-Aug-13 0.002 0.06 <0.0001 <0.001 0.002 0.005 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418779 WS2 ES 1 0.10 05-Aug-13 0.005 0.13 <0.0001 0.004 0.008 0.009 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 0.0193 0.0034 0.0075
1418780 WS2 ES 2 0.30 05-Aug-13 0.006 0.16 <0.0001 0.001 0.008 <0.001 0.001 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418781 WS3 ES 1 0.20 05-Aug-13 0.01 0.15 <0.0001 0.002 0.006 0.006 0.004 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418782 WS3 ES 7 1.00 05-Aug-13 0.011 0.13 <0.0001 0.001 0.016 0.007 0.004 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418783 WS4 ES 2 0.20 05-Aug-13 0.004 0.12 <0.0001 <0.001 0.015 0.001 0.002 0.01 <0.01 <0.02 <0.05 <5 <0.01 0.0013 0.0036 0.0088
1418784 WS5 ES 4 0.60 05-Aug-13 0.005 0.45 <0.0001 <0.001 0.013 0.002 0.004 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418785 WS5 ES 6 1.20 05-Aug-13 0.004 0.06 <0.0001 <0.001 0.004 0.002 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
1418786 WS5 ES 8 2.50 05-Aug-13 0.01 0.09 <0.0001 <0.001 0.018 0.003 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
Contact
Date Printed
Report Number EXR/162608
Table Number 1
Fax +44 (0) 1283 554422
CEN Leachate 2:1
Mr J Litten
20-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 3 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
Units : mg/lMethod Codes : PHEHPLCVL
Method Reporting Limits : 0.0005UKAS Accredited : No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Trim
ethylphenols
1418768 BH1 ES 2 0.30 07-Aug-13 <0.0005
1418769 BH1 ES 5 0.60 07-Aug-13 <0.0005
1418770 BH1 ES 9 1.90 07-Aug-13 <0.0005
1418771 BH2 ES 2 0.15 07-Aug-13 <0.0005
1418772 BH2 ES 4 0.50 07-Aug-13 <0.0005
1418773 BH3 ES 2 0.30 06-Aug-13 <0.0005
1418774 BH4 ES 2 0.20 05-Aug-13 <0.0005
1418775 BH4 ES 9 1.90 05-Aug-13 <0.0005
1418776 BH5 ES 2 0.20 06-Aug-13 <0.0005
1418777 WS1 ES 1 0.10 05-Aug-13 <0.0005
1418778 WS1 ES 2 0.30 05-Aug-13 <0.0005
1418779 WS2 ES 1 0.10 05-Aug-13 0.0052
1418780 WS2 ES 2 0.30 05-Aug-13 <0.0005
1418781 WS3 ES 1 0.20 05-Aug-13 <0.0005
1418782 WS3 ES 7 1.00 05-Aug-13 <0.0005
1418783 WS4 ES 2 0.20 05-Aug-13 <0.0005
1418784 WS5 ES 4 0.60 05-Aug-13 <0.0005
1418785 WS5 ES 6 1.20 05-Aug-13 <0.0005
1418786 WS5 ES 8 2.50 05-Aug-13 <0.0005
Contact
Date Printed
Report Number EXR/162608
Table Number 1
Fax +44 (0) 1283 554422
CEN Leachate 2:1
Mr J Litten
20-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 4 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Louise SmithEnvironmental Scientifics Group
ESG Environmental ChemistryEtwall House - Ashby RoadBretby Business ParkBurton upon TrentStaffordshireDE15 0YZ
Dear Louise
Please find attached the results for the batch of 19 samples described below.
Samples Registered on: 12-Sep-2013
Analysis Started on: 13-Sep-2013
Analysis Completed on: 20-Sep-2013
Results for Batch Number 20056966
Your Purchase Order Number: 56037 BEC
You will be invoiced shortly by our accounts department.
If we can be of further assistance then please do not hesitate to contact us.
Yours sincerely
Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation. Details of analytical procedures and
performance data are available on request. The date of sample analysis is available on request.
The Environment Agency carries out analytical work to high standards and within the scope of its UKAS accreditation, but has no
knowledge of whether the circumstances or the validity of the procedures used to obtain the samples provided to the laboratory were
representative of the need for which the information was required.
The Environment Agency and/or its staff does not therefore accept any liability for the consequences of any acts or omissions made on
the basis of the analysis or advice or interpretation provided.
William FardonCustomer Services Team Manager
Tel: (0113) 231 [email protected]
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 1 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554063 Sampled on: 7-Aug-13 @ (Time not supplied)
Comments: W1418768 BH1 0.30
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 2 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554064 Sampled on: 7-Aug-13 @ (Time not supplied)
Comments: W1418769 BH1 0.60
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 3 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554065 Sampled on: 7-Aug-13 @ (Time not supplied)
Comments: W1418770 BH1 1.90
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 4 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554066 Sampled on: 7-Aug-13 @ (Time not supplied)
Comments: W1418771 BH2 0.15
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 5 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554067 Sampled on: 6-Aug-13 @ (Time not supplied)
Comments: W1418772 BH2 0.50
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 6 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554068 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418773 BH3 0.30
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 7 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554069 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418774 BH4 0.20
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 8 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554070 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418775 BH4 1.90
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 9 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554071 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418776 BH5 0.20
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 10 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554072 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418777 WS1 0.10
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 11 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554073 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418778 WS1 0.30
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 12 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554074 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418779 WS2 0.10
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 13 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554075 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418780 WS2 0.30
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 14 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554076 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418781 WS3 0.20
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 15 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554077 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418782 WS3 1.00
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 16 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554078 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418783 WS4 0.20
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 17 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554079 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418784 WS5 0.60
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX0.00580 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 18 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554080 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418785 WS5 1.20
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 19 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002554081 Sampled on: 5-Aug-13 @ (Time not supplied)
Comments: W1418786 WS5 2.50
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005DBDC
Cyanide as CN SX<0.00500 mg/l 182UKAS0.005DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 20 of 21
Report ID - 20056966 - 1
Analytical Report
0754
Final Report
Batch description: W162608Reported on:
20-Sep-2013
Method Description Summary for all samples in batch Number 20056966 182 SX I Cyanide - (total) - UV digested; determined colorimetrically by CF analyser
183 SX I Cyanide - (free) - determined colorimetrically by CF analyser
Laboratory Site Manager
Simon Padley
All reporting limits quoted are those achievable for clean samples of the relevant matrix. No allowance is made for instances when dilutions are
necessary owing to the nature of the sample or insufficient volume of the sample being available. In these cases higher reporting limits may be
quoted and will be above the MRV.
Solid sample results are determined on a "dried" sample fraction except for parameters where the method description identifies that "as received"
sample was used.
Key to Results Flags:
Samples received outside analysis holding times. It is possible that the results may be compromised.DB
Analysis started outside of specified holding time. It is possible that the results may be compromised.DC
Please note all samples will be retained for 10 working days for aqueous samples and 30 working days for solid samples after reporting unless
otherwise agreed with Customer Services
Key to Lab ID: LE = Leeds, NM = Nottingham, SX = Starcross, SC = Sub-Contracted outside NLS, FI = Field Data - outside NLS, NLS = Calculated
Key to Accreditation: UKAS = Methodology accredited to ISO/IEC 17025:2005, MCertS = Methodology accredited to MCertS Performance Standard
for testing of soils, none = Methodology not accredited
Any subsequent version of this report denoted with a higher version number will supersede this and any previous versions
END OF TEST REPORT
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 21 of 21
WATER Analysis W162608
CustomerSiteReport No W162608
MethodID
Calc_C
R3
CU
ST
SE
RV
ICH
ALW
ICP
MS
W
ICP
WA
TV
AR
KO
NE
NS
ID Number Description Sampled
Chrom
ium (III) (C
ALC
)
Report B
(CE
N1)
Fluoride as F
(IC)
Nickel as N
i MS
(Dissolved)
Chrom
ium as C
r MS
(Dissolved)
Cadm
ium as C
d MS
(Dissolved)
Copper as C
u MS
(Dissolved)
Lead as Pb M
S (D
issolved)
Zinc as Z
n MS
(Dissolved)
Manganese as M
n MS
(Dissolved)
Arsenic as A
s MS
(Dissolved)
Mercury as H
g MS
(Dissolved)
Selenium
as Se M
S (D
issolved)
Vanadium
as V M
S (D
issolved)
Molybdenum
as Mo M
S (D
issolved)
Antim
ony as Sb M
S (D
issolved)
Total S
ulphur as SO
4 (Diss) V
AR
Calcium
as Ca (D
issolved) VA
R
Magnesium
as Mg (D
issolved) VA
R
Barium
as Ba (D
issolved) VA
R
Iron as Fe (D
issolved) VA
R
Boron as B
(Dissolved) V
AR
Beryllium
as Be (D
issolved) VA
R
Chloride as C
l (Kone)
Am
moniacal N
itrogen (Kone)
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1418768 BH1 0.30 07/08/13EX/1418769 BH1 0.60 07/08/13EX/1418770 BH1 1.90 07/08/13EX/1418771 BH2 0.15 07/08/13EX/1418772 BH2 0.50 07/08/13EX/1418773 BH3 0.30 06/08/13EX/1418774 BH4 0.20 05/08/13EX/1418775 BH4 1.90 05/08/13EX/1418776 BH5 0.20 06/08/13EX/1418777 WS1 0.10 05/08/13EX/1418778 WS1 0.30 05/08/13EX/1418779 WS2 0.10 05/08/13EX/1418780 WS2 0.30 05/08/13EX/1418781 WS3 0.20 05/08/13EX/1418782 WS3 1.00 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 26 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
WATER Analysis W162608
CustomerSiteReport No W162608
MethodID
KO
NE
NS
LeachPrep
PH
EH
PLC
VL
SF
AP
I
SF
AS
Sub045
WS
LM3
ID Number Description Sampled
Chrom
ium V
I. as Cr (K
one)
Leachate Prep
Phenols by H
PLC
(Low Level)
Cyanide (T
otal) as CN
SF
A
Sulphide as S
SF
A
^Cyanide (F
ree) 5ug/l
pH units
���� ���� ���� ����
EX/1418768 BH1 0.30 07/08/13EX/1418769 BH1 0.60 07/08/13EX/1418770 BH1 1.90 07/08/13EX/1418771 BH2 0.15 07/08/13EX/1418772 BH2 0.50 07/08/13EX/1418773 BH3 0.30 06/08/13EX/1418774 BH4 0.20 05/08/13EX/1418775 BH4 1.90 05/08/13EX/1418776 BH5 0.20 06/08/13EX/1418777 WS1 0.10 05/08/13EX/1418778 WS1 0.30 05/08/13EX/1418779 WS2 0.10 05/08/13EX/1418780 WS2 0.30 05/08/13EX/1418781 WS3 0.20 05/08/13EX/1418782 WS3 1.00 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 27 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
WATER Analysis W162608
CustomerSiteReport No W162608
MethodID
Calc_C
R3
CU
ST
SE
RV
ICH
ALW
ICP
MS
W
ICP
WA
TV
AR
KO
NE
NS
ID Number Description Sampled
Chrom
ium (III) (C
ALC
)
Report B
(CE
N1)
Fluoride as F
(IC)
Nickel as N
i MS
(Dissolved)
Chrom
ium as C
r MS
(Dissolved)
Cadm
ium as C
d MS
(Dissolved)
Copper as C
u MS
(Dissolved)
Lead as Pb M
S (D
issolved)
Zinc as Z
n MS
(Dissolved)
Manganese as M
n MS
(Dissolved)
Arsenic as A
s MS
(Dissolved)
Mercury as H
g MS
(Dissolved)
Selenium
as Se M
S (D
issolved)
Vanadium
as V M
S (D
issolved)
Molybdenum
as Mo M
S (D
issolved)
Antim
ony as Sb M
S (D
issolved)
Total S
ulphur as SO
4 (Diss) V
AR
Calcium
as Ca (D
issolved) VA
R
Magnesium
as Mg (D
issolved) VA
R
Barium
as Ba (D
issolved) VA
R
Iron as Fe (D
issolved) VA
R
Boron as B
(Dissolved) V
AR
Beryllium
as Be (D
issolved) VA
R
Chloride as C
l (Kone)
Am
moniacal N
itrogen (Kone)
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1418783 WS4 0.20 05/08/13EX/1418784 WS5 0.60 05/08/13EX/1418785 WS5 1.20 05/08/13EX/1418786 WS5 2.50 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 28 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
WATER Analysis W162608
CustomerSiteReport No W162608
MethodID
KO
NE
NS
LeachPrep
PH
EH
PLC
VL
SF
AP
I
SF
AS
Sub045
WS
LM3
ID Number Description Sampled
Chrom
ium V
I. as Cr (K
one)
Leachate Prep
Phenols by H
PLC
(Low Level)
Cyanide (T
otal) as CN
SF
A
Sulphide as S
SF
A
^Cyanide (F
ree) 5ug/l
pH units
���� ���� ���� ����
EX/1418783 WS4 0.20 05/08/13EX/1418784 WS5 0.60 05/08/13EX/1418785 WS5 1.20 05/08/13EX/1418786 WS5 2.50 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 29 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
Matrix MethodID Analysis Basis
Method Description
Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI
Water ICHALW As Received Analysis of halide ions in water using ion-chromatography with conductivity detector
Water ICPMSW As Received Direct quantitative determination of Metals in water samples using ICPMS
Water ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using ICPOES
Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with
colorimetric detectionWater SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Water WSLM3 As Received Determination of the pH of water samples by pH probe
Report Number: W/EXR/162608
Method Descriptions
Page 30 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 31 of 31Where individual results are flagged see report notes for status.
EXR/162608 Ver. 2
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnossall St Lawrence Primary School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 11-Sep-2013Declan Burns Operations Director
Laboratory and Analytical Business
11-Sep-2013
The 1 sample described in this report were registered for analysis by ESG on 30-Aug-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTCEN LEACHATE 2:1
Report No. EXR/162639 (Ver. 1)
Table 1 Main Analysis Results (Pages 2 to 4)Sub Contracted Analysis Results (Pages 5 to 7)Analytical and Deviating Sample Overview (Pages 8 to 9)Table of Method Descriptions (Page 10)Table of Report Notes (Page 11)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 KONENS ICHALW ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW ICPWATVAR
Method Reporting Limits : 0.01 1 0.1 3 1 1 0.01 0.001 0.001 0.0001 0.001 0.001 0.002 0.002 0.01UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
pH units w
Chrom
ium (III)
Chloride as C
l w
Fluoride as F
(IC) w
Total S
ulphur as SO
4 (Dissolved) a
Calcium
as Ca (D
issolved) a
Magnesium
as Mg (D
issolved) a
Barium
as Ba (D
issolved) a
Nickel as N
i (Dissolved)
Chrom
ium as C
r (Dissolved)
Cadm
ium as C
d (Dissolved)
Copper as C
u (Dissolved)
Lead as Pb (D
issolved)
Zinc as Z
n (Dissolved)
Manganese as M
n (Dissolved)
Iron as Fe (D
issolved) a
1418932 BH5 D 1.10 05-Aug-13 8.1 <0.02 2 0.8 8 56 5 0.34 0.076 0.023 0.0002 0.07 0.016 0.507 0.03 1.78
Contact
Date Printed
Report Number EXR/162639
Table Number 1
Fax +44 (0) 1283 554422
CEN Leachate 2:1
Mr J Litten
11-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l ug/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS SFAPI SFAS Sub045 ICPWATVAR PHEHPLCVL PHEHPLCVL PHEHPLCVL
Method Reporting Limits : 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.01 0.02 0.05 5 0.01 0.0005 0.0005 0.0005UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Arsenic as A
s (Dissolved)
Boron as B
(Dissolved) a
Mercury as H
g (Dissolved)
Selenium
as Se (D
issolved)
Vanadium
as V (D
issolved)
Molybdenum
as Mo (D
issolved)
Antim
ony as Sb (D
issolved)
Am
moniacal N
itrogen as N
Chrom
ium V
I as Cr
Cyanide (T
otal) as CN
Sulphide as S
^Cyanide (F
ree) 5ug/l
Beryllium
as Be (D
issolved) a
Phenol
Cresols
Dim
ethylphenols
1418932 BH5 D 1.10 05-Aug-13 0.002 0.16 <0.0001 <0.001 0.003 0.004 0.002 <0.01 <0.01 <0.02 <0.05 <5 <0.01 <0.0005 <0.0005 <0.0005
Contact
Date Printed
Report Number EXR/162639
Table Number 1
Fax +44 (0) 1283 554422
CEN Leachate 2:1
Mr J Litten
11-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 3 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
Units : mg/lMethod Codes : PHEHPLCVL
Method Reporting Limits : 0.0005UKAS Accredited : No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Trim
ethylphenols
1418932 BH5 D 1.10 05-Aug-13 <0.0005
Contact
Date Printed
Report Number EXR/162639
Table Number 1
Fax +44 (0) 1283 554422
CEN Leachate 2:1
Mr J Litten
11-Sep-2013
Gnossall St Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 4 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
Report ID - 20056793 - 1
Analytical Report
0754
Final Report
Batch description: W162639Reported on:
11-Sep-2013
Louise SmithEnvironmental Scientifics Group
ESG Environmental ChemistryEtwall House - Ashby RoadBretby Business ParkBurton upon TrentStaffordshireDE15 0YZ
Dear Louise
Please find attached the results for the batch of 1 samples described below.
Samples Registered on: 06-Sep-2013
Analysis Started on: 10-Sep-2013
Analysis Completed on: 10-Sep-2013
Results for Batch Number 20056793
Your Purchase Order Number: 56037 BEC
You will be invoiced shortly by our accounts department.
If we can be of further assistance then please do not hesitate to contact us.
Yours sincerely
Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation. Details of analytical procedures and
performance data are available on request. The date of sample analysis is available on request.
The Environment Agency carries out analytical work to high standards and within the scope of its UKAS accreditation, but has no
knowledge of whether the circumstances or the validity of the procedures used to obtain the samples provided to the laboratory were
representative of the need for which the information was required.
The Environment Agency and/or its staff does not therefore accept any liability for the consequences of any acts or omissions made on
the basis of the analysis or advice or interpretation provided.
William FardonCustomer Services Team Manager
Tel: (0113) 231 [email protected]
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 1 of 3
Report ID - 20056793 - 1
Analytical Report
0754
Final Report
Batch description: W162639Reported on:
11-Sep-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002549751 Sampled on: 5-Sep-13 @ (Time not supplied)
Comments: W1418932 - BH5 1.10
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.005 mg/l 183UKAS0.005
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 2 of 3
Report ID - 20056793 - 1
Analytical Report
0754
Final Report
Batch description: W162639Reported on:
11-Sep-2013
Method Description Summary for all samples in batch Number 20056793 183 SX I Cyanide - (free) - determined colorimetrically by CF analyser
Laboratory Site Manager
Simon Padley
All reporting limits quoted are those achievable for clean samples of the relevant matrix. No allowance is made for instances when dilutions are
necessary owing to the nature of the sample or insufficient volume of the sample being available. In these cases higher reporting limits may be
quoted and will be above the MRV.
Solid sample results are determined on a "dried" sample fraction except for parameters where the method description identifies that "as received"
sample was used.
Please note all samples will be retained for 10 working days for aqueous samples and 30 working days for solid samples after reporting unless
otherwise agreed with Customer Services
Key to Lab ID: LE = Leeds, NM = Nottingham, SX = Starcross, SC = Sub-Contracted outside NLS, FI = Field Data - outside NLS, NLS = Calculated
Key to Accreditation: UKAS = Methodology accredited to ISO/IEC 17025:2005, MCertS = Methodology accredited to MCertS Performance Standard
for testing of soils, none = Methodology not accredited
Any subsequent version of this report denoted with a higher version number will supersede this and any previous versions
END OF TEST REPORT
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 3 of 3
WATER Analysis W162639
CustomerSiteReport No W162639
MethodID
Calc_C
R3
CU
ST
SE
RV
ICH
ALW
ICP
MS
W
ICP
WA
TV
AR
KO
NE
NS
ID Number Description Sampled
Chrom
ium (III) (C
ALC
)
Report B
(CE
N1)
Fluoride as F
(IC)
Nickel as N
i MS
(Dissolved)
Chrom
ium as C
r MS
(Dissolved)
Cadm
ium as C
d MS
(Dissolved)
Copper as C
u MS
(Dissolved)
Lead as Pb M
S (D
issolved)
Zinc as Z
n MS
(Dissolved)
Manganese as M
n MS
(Dissolved)
Arsenic as A
s MS
(Dissolved)
Mercury as H
g MS
(Dissolved)
Selenium
as Se M
S (D
issolved)
Vanadium
as V M
S (D
issolved)
Molybdenum
as Mo M
S (D
issolved)
Antim
ony as Sb M
S (D
issolved)
Total S
ulphur as SO
4 (Diss) V
AR
Calcium
as Ca (D
issolved) VA
R
Magnesium
as Mg (D
issolved) VA
R
Barium
as Ba (D
issolved) VA
R
Iron as Fe (D
issolved) VA
R
Boron as B
(Dissolved) V
AR
Beryllium
as Be (D
issolved) VA
R
Chloride as C
l (Kone)
Am
moniacal N
itrogen (Kone)
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1418932 BH5 1.10 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 8 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
WATER Analysis W162639
CustomerSiteReport No W162639
MethodID
KO
NE
NS
LeachPrep
PH
EH
PLC
VL
SF
AP
I
SF
AS
Sub045
WS
LM3
ID Number Description Sampled
Chrom
ium V
I. as Cr (K
one)
Leachate Prep
Phenols by H
PLC
(Low Level)
Cyanide (T
otal) as CN
SF
A
Sulphide as S
SF
A
^Cyanide (F
ree) 5ug/l
pH units
���� ���� ���� ����
EX/1418932 BH5 1.10 05/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No S36992
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St Lawrence Primary School Date Logged 30-Aug-2013
Report Due 11-Sep-2013
Page 9 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
Matrix MethodID Analysis Basis
Method Description
Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI
Water ICHALW As Received Analysis of halide ions in water using ion-chromatography with conductivity detector
Water ICPMSW As Received Direct quantitative determination of Metals in water samples using ICPMS
Water ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using ICPOES
Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with
colorimetric detectionWater SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Water WSLM3 As Received Determination of the pH of water samples by pH probe
Report Number: W/EXR/162639
Method Descriptions
Page 10 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 11 of 11Where individual results are flagged see report notes for status.
EXR/162639 Ver. 1
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnossall St. Lawrence Primary School
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 12-Sep-2013Declan Burns Operations Director
Laboratory and Analytical Business
12-Sep-2013
The 1 sample described in this report were registered for analysis by ESG on 05-Sep-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTWATER SAMPLE ANALYSIS
Report No. EXR/162915 (Ver. 1)
Table 1 Main Analysis Results (Pages 2 to 4)Table of PAH (MS-SIM) (10) Results (Page 5)Table of GRO Results (Page 6)Table of TPH (Si) banding (0.01) (Page 7)GC-FID Chromatograms (Pages 8 to 9)Analytical and Deviating Sample Overview (Pages 10 to 11)Table of Method Descriptions (Page 12)Table of Report Notes (Page 13)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l µg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 Calc_HD KONENS ISEF ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW PAHMSW ICPMSW ICPMSW
Method Reporting Limits : 0.01 7 1 0.1 3 1 1 0.01 1 0.001 0.001 0.0001 0.001 0.001UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
pH units w
Chrom
ium (III)
Total H
ardness as CaC
O3
Chloride as C
l w
Fluoride as F
a
Total S
ulphur as SO
4 (Dissolved) a
Calcium
as Ca (D
issolved) a
Magnesium
as Mg (D
issolved) a
Barium
as Ba (D
issolved) a
Sodium
as Na (D
issolved) a
Nickel as N
i (Dissolved)
Chrom
ium as C
r (Dissolved)
Cadm
ium as C
d (Dissolved)
PA
H G
C-M
S (16) o
Copper as C
u (Dissolved)
Lead as Pb (D
issolved)
1420399 BH3 EW 19 0.00 28-Aug-13 7.2 <0.01 387 46 0.3 50 117 23 0.1 14 0.001 0.006 <0.0001 Req 0.004 <0.001
Contact
Date Printed
Report Number EXR/162915
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
12-Sep-2013
Gnossall St. Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPMSW ICPWATVAR ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS KONENS SFAPI SFAPI SFAS
Method Reporting Limits : 0.002 0.002 0.01 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.2 0.01 0.02 0.02 0.05UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Zinc as Z
n (Dissolved)
Manganese as M
n (Dissolved)
Iron as Fe (D
issolved) a
Arsenic as A
s (Dissolved)
Boron as B
(Dissolved) a
Mercury as H
g (Dissolved)
Selenium
as Se (D
issolved)
Vanadium
as V (D
issolved)
Molybdenum
as Mo (D
issolved)
Antim
ony as Sb (D
issolved)
Am
moniacal N
itrogen as N
Nitrate as N
Chrom
ium V
I as Cr
Cyanide (F
ree) as CN
Cyanide (T
otal) as CN
Sulphide as S
1420399 BH3 EW 19 0.00 28-Aug-13 <0.002 0.052 <0.01 <0.001 <0.01 <0.0001 0.001 0.002 <0.001 <0.001 0.01 2.6 <0.01 <0.02 <0.02 <0.05
Contact
Date Printed
Report Number EXR/162915
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
12-Sep-2013
Gnossall St. Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 3 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Units : mg/l mg/l mg/l µg/l µg/l µg/l µg/l µg/l µg/l mg/l mg/l mg/l mg/lMethod Codes : TPHFID-Si ICPWATVAR GROHSA VOCHSAW VOCHSAW VOCHSAW VOCHSAW VOCHSAW VOCHSAW PHEHPLCVL PHEHPLCVL PHEHPLCVL PHEHPLCVL
Method Reporting Limits : 0.01 0.01 0.1 1 1 1 2 1 1 0.0005 0.0005 0.0005 0.0005UKAS Accredited : Yes No No Yes Yes Yes Yes Yes Yes No No No No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
TP
H by G
C(S
i) o
Beryllium
as Be (D
issolved) a
GR
O-H
SA
(AA
)
Benzene
Toluene
Ethyl B
enzene
Xylenes
m/p X
ylenes
o Xylene
Phenol
Cresols
Dim
ethylphenols
Trim
ethylphenols
1420399 BH3 EW 19 0.00 28-Aug-13 Req <0.01 Req <1 <1 <1 <2 <1 <1 <0.0005 <0.0005 <0.0005 <0.0005
Contact
Date Printed
Report Number EXR/162915
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
12-Sep-2013
Gnossall St. Lawrence Primary School
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 4 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnossall St. Lawrence Primary SchoolSample Details: BH3 EW 19 0.00 Job Number: W16_2915LIMS ID Number: EX1420399 Date Booked in: 05-Sep-13QC Batch Number: 130639 Date Extracted: 06-Sep-13
Quantitation File: Initial Calibration Date Analysed: 06-Sep-13Directory: 906MS10.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle
UKAS accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit(min) ug/l
Naphthalene 91-20-3 - < 0.020 -Acenaphthylene 208-96-8 - < 0.010 -Acenaphthene 83-32-9 - < 0.010 -Fluorene 86-73-7 - < 0.010 -Phenanthrene 85-01-8 - < 0.010 -Anthracene 120-12-7 - < 0.010 -Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 - < 0.010 -Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3 - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.170 -
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 97 2-Fluorobiphenyl 69Acenaphthene-d10 92 Terphenyl-d14 64Phenanthrene-d10 90Chrysene-d12 81Perylene-d12 81
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Page 5 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : Gnossall St. Lawrence Primary School Matrix: Water
Job Number: W16_2915 Date Booked in: 05-Sep-13
Directory: D:\TES\DATA\Y2013\0909HSA_GC12\090913 2013-09-09 14-07-59\117B1701.D Date extracted: 09-Sep-13
Method: Headspace GCFID Date Analysed: 09-Sep-13, 19:31:56
y * Sample data with an asterisk are not UKAS accredi ted.
Concentration, (mg/l) AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
* EX1420399 BH3 EW 19 0.00 <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1
Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.
Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions
Page 6 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : Gnossall St. Lawrence Primary School Matrix: WaterJob Number: W16_2915 Separation: Silica gel Date Booked in: 05-Sep-13QC Batch Number: 130639 Eluents: Hexane, DCM Date Extracted: 06-Sep-13Directory: D:\TES\DATA\Y2013\090913TPH_GC16\090913 2013-09-09 08-18-23\087B4301.D Date Analysed: 09-Sep-13, 19:59:28Method: Bottle
Concentration, (mg/l)* This sample data is not UKAS accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aro matics Aliphatics Aromatics Aliphatics Aromatics Aliphat ics Aromatics
EX1420399 BH3 EW 19 0.00 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 0.012
Page 7 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: EX1420399ALI Job Number: W16_2915Multiplier: 0.019 Client: ESG SouthamDilution: 1 Site: Gnossall St. Lawrence Primary SchoolAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 EW 19 0.00Acquisition Date/Time: 09-Sep-13, 19:59:28Datafile: D:\TES\DATA\Y2013\090913TPH_GC16\090913 2013-09-09 08-18-23\031F4301.D
min0 2 4 6 8
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, Front Signal (031F4301.D)
Page 8 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: EX1420399ARO Job Number: W16_2915Multiplier: 0.0154 Client: ESG SouthamDilution: 1 Site: Gnossall St. Lawrence Primary SchoolAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 EW 19 0.00Acquisition Date/Time: 09-Sep-13, 19:59:28Datafile: D:\TES\DATA\Y2013\090913TPH_GC16\090913 2013-09-09 08-18-23\087B4301.D
min0 2 4 6 8
pA
0
100
200
300
400
FID2 B, Back Signal (087B4301.D)
Page 9 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
WATER Analysis W162915
CustomerSiteReport No W162915
MethodID
Calc_C
R3
Calc_H
D
CU
ST
SE
RV
GR
OH
SA
ICP
MS
W
ICP
WA
TV
AR
ID Number Description Sampled
Chrom
ium (III) (C
ALC
)
Total H
ardness as CaC
O3 (C
ALC
)
Report A
GR
O-H
SA
GC
FID
(AA
)
Nickel as N
i MS
(Dissolved)
Chrom
ium as C
r MS
(Dissolved)
Cadm
ium as C
d MS
(Dissolved)
Copper as C
u MS
(Dissolved)
Lead as Pb M
S (D
issolved)
Zinc as Z
n MS
(Dissolved)
Manganese as M
n MS
(Dissolved)
Arsenic as A
s MS
(Dissolved)
Mercury as H
g MS
(Dissolved)
Selenium
as Se M
S (D
issolved)
Vanadium
as V M
S (D
issolved)
Molybdenum
as Mo M
S (D
issolved)
Antim
ony as Sb M
S (D
issolved)
Total S
ulphur as SO
4 (Diss) V
AR
Calcium
as Ca (D
issolved) VA
R
Magnesium
as Mg (D
issolved) VA
R
Barium
as Ba (D
issolved) VA
R
Sodium
as Na (D
issolved) VA
R
Iron as Fe (D
issolved) VA
R
Boron as B
(Dissolved) V
AR
Beryllium
as Be (D
issolved) VA
R
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1420399 BH3 0.00 28/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No W58720
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St. Lawrence Primary School Date Logged 05-Sep-2013
Report Due 12-Sep-2013
Page 10 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
WATER Analysis W162915
CustomerSiteReport No W162915
MethodID
ISE
F
KO
NE
NS
PA
HM
SW
PH
EH
PLC
VL
SF
AP
I
SF
AS
TP
HF
ID-S
i
VO
CH
SA
W
WS
LM3
ID Number Description Sampled
Fluoride as F
Chloride as C
l (Kone)
Am
moniacal N
itrogen (Kone)
Nitrate as N
(Kone calc)
Chrom
ium V
I. as Cr (K
one)
PA
H G
C-M
S (16)
Phenols by H
PLC
(Low Level)
Cyanide (F
ree) as CN
SF
A
Cyanide (T
otal) as CN
SF
A
Sulphide as S
SF
A
TP
H by G
C(S
i)
BT
EX
Analysis H
SA
GC
-MS
Benzene (µg/l)
Toluene (µg/l)
Ethyl B
enzene (µg/l)
Xylenes (µg/l)
m/p X
ylenes (µg/l)
o Xylene (µg/l)
pH units
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1420399 BH3 0.00 28/08/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No W58720
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnossall St. Lawrence Primary School Date Logged 05-Sep-2013
Report Due 12-Sep-2013
Page 11 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Matrix MethodID Analysis Basis
Method Description
Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI
Water Calc_HD As Received Calculation based on Dissolved metals analysis by ICPOESWater GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons
(GRO) by Headspace FIDWater ICPMSW As Received Direct quantitative determination of Metals in water samples using
ICPMSWater ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using
ICPOESWater ISEF As Received Determination of Fluoride in water samples by Ion Selective
Electrode (ISE)Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PAHMSW As Received Determination of PolyAromatic Hydrocarbons in water by pentane
extraction GCMS quantitationWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with
colorimetric detectionWater TPHFID-Si As Received Determination of speciated pentane extractable hydrocarbons in
water by GCFIDWater VOCHSAW As Received Determination of Volatile Organics Compounds by Headspace
GCMSWater WSLM3 As Received Determination of the pH of water samples by pH probe
Report Number: W/EXR/162915
Method Descriptions
Page 12 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 13 of 13Where individual results are flagged see report notes for status.
EXR/162915 Ver. 1
ESG SouthamUnit 4Gainsborough Trading EstateLeamington RoadSouthamWarwickshireCV47 1RA
Site: Gnosall St Lawrence
The analysis was completed by:
Tests where the accreditation is set to N or No, and any individual data items marked with a * are not UKAS accreditedAny opinions or interpretations expressed herein are outside the scope of any UKAS accreditation held by ESG.
The following tables are contained in this report:
On behalf ofESG : Date of Issue: 12-Nov-2013Declan Burns Operations Director
Laboratory and Analytical Business
12-Nov-2013
The 2 samples described in this report were registered for analysis by ESG on 02-Nov-2013. This report supersedes any versions previously issued by the laboratory.
TEST REPORTWATER SAMPLE ANALYSIS
Report No. EXR/166207 (Ver. 2)
Table 1 Main Analysis Results (Pages 2 to 4)Table of PAH (MS-SIM) (10) Results (Pages 5 to 6)Table of GRO Results (Page 7)Table of TPH (Si) banding (0.01) (Page 8)GC-FID Chromatograms (Pages 9 to 12)Table of Subcontracted Analysis Results (Pages 13 to 18)Analytical and Deviating Sample Overview (Pages 19 to 20)Table of Method Descriptions (Page 21)Table of Report Notes (Page 22)
Tests marked '^' have been subcontracted to another laboratory.
ESG accepts no responsibility for any sampling not carried out by our personnel.
Page 1 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Units : pH units mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l µg/l mg/l mg/lMethod Codes : WSLM3 Calc_CR3 Calc_HD KONENS ISEF ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPWATVAR ICPMSW ICPMSW ICPMSW PAHMSW ICPMSW ICPMSW
Method Reporting Limits : 0.01 7 1 0.1 3 1 1 0.01 1 0.001 0.001 0.0001 0.001 0.001UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
pH units w
Chrom
ium (III)
Total H
ardness as CaC
O3
Chloride as C
l w
Fluoride as F
a
Total S
ulphur as SO
4 (Dissolved) a
Calcium
as Ca (D
issolved) a
Magnesium
as Mg (D
issolved) a
Barium
as Ba (D
issolved) a
Sodium
as Na (D
issolved) a
Nickel as N
i (Dissolved)
Chrom
ium as C
r (Dissolved)
Cadm
ium as C
d (Dissolved)
PA
H G
C-M
S (16) o
Copper as C
u (Dissolved)
Lead as Pb (D
issolved)
1436683 BH3 W 31-Oct-13 7.2 <0.01 354 27 0.2 34 104 23 0.09 15 0.001 0.004 0.0004 Req 0.005 <0.001
1436684 BH4 W 31-Oct-13 7.4 <0.01 323 5 0.2 7 113 10 0.19 7 0.002 0.004 <0.0001 Req 0.006 <0.001
Contact
Date Printed
Report Number EXR/166207
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
12-Nov-2013
Gnosall St Lawrence
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 2 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Units : mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/l mg/lMethod Codes : ICPMSW ICPMSW ICPWATVAR ICPMSW ICPWATVAR ICPMSW ICPMSW ICPMSW ICPMSW ICPMSW KONENS KONENS KONENS SFAPI SFAS TPHFID-Si
Method Reporting Limits : 0.002 0.002 0.01 0.001 0.01 0.0001 0.001 0.001 0.001 0.001 0.01 0.2 0.01 0.02 0.05 0.01UKAS Accredited : Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
Zinc as Z
n (Dissolved)
Manganese as M
n (Dissolved)
Iron as Fe (D
issolved) a
Arsenic as A
s (Dissolved)
Boron as B
(Dissolved) a
Mercury as H
g (Dissolved)
Selenium
as Se (D
issolved)
Vanadium
as V (D
issolved)
Molybdenum
as Mo (D
issolved)
Antim
ony as Sb (D
issolved)
Am
moniacal N
itrogen as N
Nitrate as N
Chrom
ium V
I as Cr
Cyanide (T
otal) as CN
Sulphide as S
TP
H by G
C(S
i) o
1436683 BH3 W 31-Oct-13 0.005 <0.002 <0.01 <0.001 0.05 <0.0001 0.002 0.002 <0.001 <0.001 0.19 4.5 <0.01 <0.02 <0.05 Req
1436684 BH4 W 31-Oct-13 <0.002 <0.002 <0.01 0.001 0.05 <0.0001 <0.001 0.002 <0.001 <0.001 0.19 3.4 <0.01 <0.02 <0.05 Req
Contact
Date Printed
Report Number EXR/166207
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
12-Nov-2013
Gnosall St Lawrence
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 3 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Units : ug/l mg/l µg/l mg/l µg/l µg/l µg/l µg/l µg/l µg/l mg/l mg/l mg/l mg/lMethod Codes : Sub045 ICPWATVAR Sub045 GROHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA BTEXHSA PHEHPLCVL PHEHPLCVL PHEHPLCVL PHEHPLCVL
Method Reporting Limits : 5 0.01 0.1 5 5 5 15 10 5 0.0005 0.0005 0.0005 0.0005UKAS Accredited : No No No No Yes Yes Yes Yes Yes Yes No No No No
LAB
ID N
umber E
X/
Client Sample Description
Sam
ple Date
^Cyanide (F
ree) 5ug/l
Beryllium
as Be (D
issolved) a
^VO
C Low
Level
GR
O-H
SA
(AA
)
Ethyl B
enzene
Benzene
Toluene
Xylenes
m/p X
ylenes
o Xylene
Phenol
Cresols
Dim
ethylphenols
Trim
ethylphenols
1436683 BH3 W 31-Oct-13 <5 <0.01 Req Req <5 <5 <5 <15 <10 <5 <0.0005 <0.0005 <0.0005 <0.0005
1436684 BH4 W 31-Oct-13 <5 <0.01 Req Req <5 <5 <5 <15 <10 <5 <0.0005 <0.0005 <0.0005 <0.0005
Contact
Date Printed
Report Number EXR/166207
Table Number 1
Fax +44 (0) 1283 554422
Water Sample Analysis
Mr J Litten
12-Nov-2013
Gnosall St Lawrence
Bretby Business Park, Ashby Road
Burton-on-Trent, Staffordshire, DE15 0YZ
Tel +44 (0) 1283 554400
Client Name ESG Southam
Page 4 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnosall St LawrenceSample Details: BH3 W Job Number: W16_6207LIMS ID Number: EX1436683 Date Booked in: 02-Nov-13QC Batch Number: 130801 Date Extracted: 05-Nov-13
Quantitation File: Initial Calibration Date Analysed: 07-Nov-13Directory: 107MS17.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle
UKAS accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit(min) ug/l
Naphthalene 91-20-3 - < 0.020 -Acenaphthylene 208-96-8 - < 0.010 -Acenaphthene 83-32-9 - < 0.010 -Fluorene 86-73-7 - < 0.010 -Phenanthrene 85-01-8 - < 0.010 -Anthracene 120-12-7 - < 0.010 -Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 - < 0.010 -Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3* - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.170 -
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 112 2-Fluorobiphenyl 93Acenaphthene-d10 110 Terphenyl-d14 86Phenanthrene-d10 118Chrysene-d12 129Perylene-d12 144
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Page 5 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
1
Polycyclic Aromatic HydrocarbonsGC/MS (SIM)
Customer and Site Details: ESG Southam: Gnosall St LawrenceSample Details: BH4 W Job Number: W16_6207LIMS ID Number: EX1436684 Date Booked in: 02-Nov-13QC Batch Number: 130801 Date Extracted: 05-Nov-13
Quantitation File: Initial Calibration Date Analysed: 07-Nov-13Directory: 107MS17.PAH\ Matrix: WaterDilution: 1.0 Ext Method: Bottle
UKAS accredited?: Yes
Target Compounds CAS # R.T. Concentration % Fit(min) ug/l
Naphthalene 91-20-3 - < 0.020 -Acenaphthylene 208-96-8 - < 0.010 -Acenaphthene 83-32-9 - < 0.010 -Fluorene 86-73-7 - < 0.010 -Phenanthrene 85-01-8 - < 0.010 -Anthracene 120-12-7 - < 0.010 -Fluoranthene 206-44-0 - < 0.010 -Pyrene 129-00-0 7.43 0.012 91Benzo[a]anthracene 56-55-3 - < 0.010 -Chrysene 218-01-9 - < 0.010 -Benzo[b]fluoranthene 205-99-2 - < 0.010 -Benzo[k]fluoranthene 207-08-9 - < 0.010 -Benzo[a]pyrene 50-32-8 - < 0.010 -Indeno[1,2,3-cd]pyrene 193-39-5 - < 0.010 -Dibenzo[a,h]anthracene 53-70-3* - < 0.010 -Benzo[g,h,i]perylene 191-24-2 - < 0.010 -Total (USEPA16) PAHs - - < 0.172 -
"M" denotes that % fit has been manually interpreted
Internal Standards % Area Surrogates % Rec1,4-Dichlorobenzene-d4 NA Nitrobenzene-d5 NANaphthalene-d8 98 2-Fluorobiphenyl 95Acenaphthene-d10 95 Terphenyl-d14 82Phenanthrene-d10 99Chrysene-d12 96Perylene-d12 98
The Total PAH result is the sum of non-rounded individual PAH results and therefore may differ to the sum of the rounded individual PAH results printed above. By convention, whereany one or more result is a "less than", the total is expressed as a "less than" and includes the "less than" concentration within the total.
Page 6 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Gasoline Range Organics(BTEX and Aliphatic Carbon Ranges)
Customer and Site Details: ESG Southam : Gnosall St Lawrence Matrix: Water
Job Number: W16_6207 Date Booked in: 02-Nov-13
Directory: D:\TES\DATA\Y2013\1106HSA_GC12\110613 2013-11-06 16-46-52\110B1001.D Date extracted: 06-Nov-13
Method: Headspace GCFID Date Analysed: 06-Nov-13, 19:54:44
y * Sample data with an asterisk are not UKAS accredi ted.
Concentration, (mg/l) AliphaticsSample ID Client ID Benzene Toluene Ethyl benzene m/p-Xylene o-Xylene C5 - C 6 >C6 - C7 >C7 - C8 >C8 - C10 Total GRO
* EX1436683 BH3 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1
* EX1436684 BH4 W <0.005 <0.005 <0.005 <0.005 <0.005 <0.1 <0.1 <0.1 <0.1 <0.1
Note: Benzene elutes between C6 and C7, toluene elutes between C7 and C8, ethyl benzene and the xylenes elute between C8 and C9.Each BTEX compound is deducted from the appropriate band to give the aliphatic fractions, however aromatic compounds may still be contributing to these fractions
Page 7 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
ALIPHATIC / AROMATIC FRACTION BY GC/FID
Customer and Site Details: ESG Southam : Gnosall St Lawrence Matrix: WaterJob Number: W16_6207 Separation: Silica gel Date Booked in: 02-Nov-13QC Batch Number: 130801 Eluents: Hexane, DCM Date Extracted: 05-Nov-13Directory: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\081B3701.D Date Analysed: 06-Nov-13, 21:08:13Method: Bottle
Concentration, (mg/l)* This sample data is not UKAS accredited. >C8 - C10 >C10 - C12 >C12 - C16 >C16 - C21 >C21 - C35 >C8 - C40
Sample ID Client ID Aliphatics Aromatics Aliphatics Aromatics Aliphatics Aro matics Aliphatics Aromatics Aliphatics Aromatics Aliphat ics Aromatics
EX1436683 BH3 W <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01
EX1436684 BH4 W <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01 <0.01
Page 8 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: EX1436683ALI Job Number: W16_6207Multiplier: 0.0188 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 WAcquisition Date/Time: 06-Nov-13, 20:51:41Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\030F3601.D
min0 2 4 6 8
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, Front Signal (030F3601.D)
Page 9 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: EX1436683ARO Job Number: W16_6207Multiplier: 0.0144 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH3 WAcquisition Date/Time: 06-Nov-13, 20:51:41Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\080B3601.D
min0 2 4 6 8
pA
0
100
200
300
400
FID2 B, Back Signal (080B3601.D)
Page 10 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Petroleum Hydrocarbons (C8 to C40) by GC/FID Alipha tics Fraction.
Sample ID: EX1436684ALI Job Number: W16_6207Multiplier: 0.0188 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH4 WAcquisition Date/Time: 06-Nov-13, 21:08:13Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\031F3701.D
min0 2 4 6 8
pA
0
50
100
150
200
250
300
350
400
450
FID1 A, Front Signal (031F3701.D)
Page 11 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Petroleum Hydrocarbons (C8 to C40) by GC/FID Aromat ics Fraction.
Sample ID: EX1436684ARO Job Number: W16_6207Multiplier: 0.0142 Client: ESG SouthamDilution: 1 Site: Gnosall St LawrenceAcquisition Method: TPH_RUNF.M Client Sample Ref: BH4 WAcquisition Date/Time: 06-Nov-13, 21:08:13Datafile: D:\TES\DATA\Y2013\110613TPH_GC16\110613 2013-11-06 11-00-05\081B3701.D
min0 2 4 6 8
pA
0
100
200
300
400
FID2 B, Back Signal (081B3701.D)
Page 12 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Report ID - 20058864 - 1
Analytical Report
0754
Final Report
Batch description: W166207Reported on:
08-Nov-2013
Louise SmithEnvironmental Scientifics Group
ESG Environmental ChemistryEtwall House - Ashby RoadBretby Business ParkBurton upon TrentStaffordshireDE15 0YZ
Dear Louise
Please find attached the results for the batch of 2 samples described below.
Samples Registered on: 06-Nov-2013
Analysis Started on: 07-Nov-2013
Analysis Completed on: 08-Nov-2013
Results for Batch Number 20058864
Your Purchase Order Number: 56037 BEC
You will be invoiced shortly by our accounts department.
If we can be of further assistance then please do not hesitate to contact us.
Yours sincerely
Opinions and interpretations expressed herein are outside the scope of UKAS Accreditation. Details of analytical procedures and
performance data are available on request. The date of sample analysis is available on request.
The Environment Agency carries out analytical work to high standards and within the scope of its UKAS accreditation, but has no
knowledge of whether the circumstances or the validity of the procedures used to obtain the samples provided to the laboratory were
representative of the need for which the information was required.
The Environment Agency and/or its staff does not therefore accept any liability for the consequences of any acts or omissions made on
the basis of the analysis or advice or interpretation provided.
William FardonCustomer Services Team Manager
Tel: (0113) 231 [email protected]
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 1 of 6
Report ID - 20058864 - 1
Analytical Report
0754
Final Report
Batch description: W166207Reported on:
08-Nov-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002632748 Sampled on: 31-Oct-13 @ (Time not supplied)
Comments: W1436683 - BH3
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005
1,1,1,2-Tetrachloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1,1-Trichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1,2,2-Tetrachloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1,2-Trichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1-Dichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,2,3-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC
1,2,3-Trichloropropane SX<0.5 ug/l 1296UKAS0.5DBDC
1,2,3-Trimethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
1,2,4-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC
1,2,4-Trimethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dibromo-3-chloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dibromoethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dichlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dimethylbenzene :- {o-Xylene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,3,5-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC
1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,3-Dichlorobenzene SX<0.5 ug/l 1296UKAS0.5DBDC
1,3-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
1,4-Dichlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
2,2-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
Benzene SX<0.1 ug/l 1296UKAS0.1DBDC
Bromobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
Bromochloromethane SX<0.1 ug/l 1296UKAS0.1DBDC
Bromodichloromethane SX<0.1 ug/l 1296UKAS0.1DBDC
Bromoform :- {Tribromomethane} SX<0.1 ug/l 1296UKAS0.1DBDC
Carbon Disulphide SX<0.1 ug/l 1296None0.1DBDC
Carbon tetrachloride :- {Tetrachloromethane} SX<0.1 ug/l 1296UKAS0.1DBDC
Chlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
Chlorodibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC
Chloroform :- {Trichloromethane} SX0.152 ug/l 1296UKAS0.1DBDC
Chloromethane :- {Methyl Chloride} SX<0.5 ug/l 1296None0.5DBDC
cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 2 of 6
Report ID - 20058864 - 1
Analytical Report
0754
Final Report
Batch description: W166207Reported on:
08-Nov-2013
Dibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC
Dichloromethane :- {Methylene Dichloride} SX<0.5 ug/l 1296UKAS0.5DBDC
Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<0.2 ug/l 1296UKAS0.2DBDC
Ethyl tert-butyl ether :- {ETBE} SX<0.1 ug/l 1296UKAS0.1DBDC
Ethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
Hexachlorobutadiene SX<0.5 ug/l 1296None0.5DBDC
Hexachloroethane SX<0.5 ug/l 1296None0.5DBDC
Isopropylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
MTBE :- {Methyl tert-butyl ether} SX<0.1 ug/l 1296UKAS0.1DBDC
Naphthalene SX<0.5 ug/l 1296None0.5DBDC
n-ButylBenzene :- {1-Phenylbutane} SX<0.1 ug/l 1296UKAS0.1DBDC
n-Propylbenzene :- {1-phenylpropane} SX<0.1 ug/l 1296UKAS0.1DBDC
sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
Styrene :- {Vinylbenzene} SX<0.5 ug/l 1296UKAS0.5DBDC
tert-Amyl methyl ether :- {TAME} SX<0.1 ug/l 1296UKAS0.1DBDC
tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.1 ug/l 1296UKAS0.1DBDC
Tetrachloroethylene :- {Perchloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC
Toluene :- {Methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<0.5 ug/l 1296UKAS0.5DBDC
Trichloroethylene :- {Trichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
Trichlorofluoromethane SX<0.1 ug/l 1296UKAS0.1DBDC
Vinyl Chloride :- {Chloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 3 of 6
Report ID - 20058864 - 1
Analytical Report
0754
Final Report
Batch description: W166207Reported on:
08-Nov-2013
Environmental Scientifics Group Cyanide AnalysisClient: Project:
1
CC Environmental Scientifics GroupSample Point Name:
Folder No: 002632749 Sampled on: 31-Oct-13 @ (Time not supplied)
Comments: W1436684 - BH4
Quote No: 10242 Matrix: Freshwater
Lab ID Result Units TestcodeAnalyte MRV AccredFlag
Cyanide : Free as CN SX<0.00500 mg/l 183UKAS0.005
1,1,1,2-Tetrachloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1,1-Trichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1,2,2-Tetrachloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1,2-Trichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1-Dichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,1-Dichloroethylene :- {1,1-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,1-Dichloropropylene :- {1,1-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,2,3-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC
1,2,3-Trichloropropane SX<0.5 ug/l 1296UKAS0.5DBDC
1,2,3-Trimethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
1,2,4-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC
1,2,4-Trimethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dibromo-3-chloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dibromoethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dichlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dichloroethane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
1,2-Dimethylbenzene :- {o-Xylene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,3,5-Trichlorobenzene SX<0.5 ug/l 1296None0.5DBDC
1,3,5-Trimethylbenzene :- {Mesitylene} SX<0.1 ug/l 1296UKAS0.1DBDC
1,3-Dichlorobenzene SX<0.5 ug/l 1296UKAS0.5DBDC
1,3-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
1,4-Dichlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
2,2-Dichloropropane SX<0.1 ug/l 1296UKAS0.1DBDC
2-Chlorotoluene :- {1-Chloro-2-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
3-Chlorotoluene :- {1-Chloro-3-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
4-Chlorotoluene :- {1-Chloro-4-methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
4-Isopropyltoluene :- {4-methyl-Isopropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
Benzene SX<0.1 ug/l 1296UKAS0.1DBDC
Bromobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
Bromochloromethane SX<0.1 ug/l 1296UKAS0.1DBDC
Bromodichloromethane SX<0.1 ug/l 1296UKAS0.1DBDC
Bromoform :- {Tribromomethane} SX<0.1 ug/l 1296UKAS0.1DBDC
Carbon Disulphide SX<0.1 ug/l 1296None0.1DBDC
Carbon tetrachloride :- {Tetrachloromethane} SX<0.1 ug/l 1296UKAS0.1DBDC
Chlorobenzene SX<0.1 ug/l 1296UKAS0.1DBDC
Chlorodibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC
Chloroform :- {Trichloromethane} SX<0.1 ug/l 1296UKAS0.1DBDC
Chloromethane :- {Methyl Chloride} SX<0.5 ug/l 1296None0.5DBDC
cis-1,2-Dichloroethylene :- {cis-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
cis-1,3-Dichloropropylene :- {cis-1,3-Dichloropropene} SX<0.1 ug/l 1296UKAS0.1DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 4 of 6
Report ID - 20058864 - 1
Analytical Report
0754
Final Report
Batch description: W166207Reported on:
08-Nov-2013
Dibromomethane SX<0.1 ug/l 1296UKAS0.1DBDC
Dichloromethane :- {Methylene Dichloride} SX<0.5 ug/l 1296UKAS0.5DBDC
Dimethylbenzene : Sum of isomers (1,3- 1,4-) : {m+p xylene} SX<0.2 ug/l 1296UKAS0.2DBDC
Ethyl tert-butyl ether :- {ETBE} SX<0.1 ug/l 1296UKAS0.1DBDC
Ethylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
Hexachlorobutadiene SX<0.5 ug/l 1296None0.5DBDC
Hexachloroethane SX<0.5 ug/l 1296None0.5DBDC
Isopropylbenzene SX<0.1 ug/l 1296UKAS0.1DBDC
MTBE :- {Methyl tert-butyl ether} SX<0.1 ug/l 1296UKAS0.1DBDC
Naphthalene SX<0.5 ug/l 1296None0.5DBDC
n-ButylBenzene :- {1-Phenylbutane} SX<0.1 ug/l 1296UKAS0.1DBDC
n-Propylbenzene :- {1-phenylpropane} SX<0.1 ug/l 1296UKAS0.1DBDC
sec-Butylbenzene :- {1-Methylpropylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
Styrene :- {Vinylbenzene} SX<0.5 ug/l 1296UKAS0.5DBDC
tert-Amyl methyl ether :- {TAME} SX<0.1 ug/l 1296UKAS0.1DBDC
tert-Butylbenzene :- {(1,1-Dimethylethyl)benzene} SX<0.1 ug/l 1296UKAS0.1DBDC
Tetrachloroethylene :- {Perchloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC
Toluene :- {Methylbenzene} SX<0.1 ug/l 1296UKAS0.1DBDC
trans-1,2-Dichloroethylene :- {trans-1,2-Dichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
trans-1,3-Dichloropropylene :- {trans-1,3-Dichloropropene} SX<0.5 ug/l 1296UKAS0.5DBDC
Trichloroethylene :- {Trichloroethene} SX<0.1 ug/l 1296UKAS0.1DBDC
Trichlorofluoromethane SX<0.1 ug/l 1296UKAS0.1DBDC
Vinyl Chloride :- {Chloroethylene} SX<0.1 ug/l 1296UKAS0.1DBDC
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 5 of 6
Report ID - 20058864 - 1
Analytical Report
0754
Final Report
Batch description: W166207Reported on:
08-Nov-2013
Method Description Summary for all samples in batch Number 20058864 183 SX I Cyanide - (free) - determined colorimetrically by CF analyser
1296 SX O Volatiles - direct aqueous injected; determined by P and T GCMS
Laboratory Site Manager
Simon Padley
All reporting limits quoted are those achievable for clean samples of the relevant matrix. No allowance is made for instances when dilutions are
necessary owing to the nature of the sample or insufficient volume of the sample being available. In these cases higher reporting limits may be
quoted and will be above the MRV.
Solid sample results are determined on a "dried" sample fraction except for parameters where the method description identifies that "as received"
sample was used.
Key to Results Flags:
Samples received outside analysis holding times. It is possible that the results may be compromised.DB
Analysis started outside of specified holding time. It is possible that the results may be compromised.DC
The analysis start date specified is the date of the first test, dates for other analysis are available on request.
Please note all samples will be retained for 10 working days for aqueous samples and 30 working days for solid samples after reporting unless
otherwise agreed with Customer Services
Key to Lab ID: LE = Leeds, NM = Nottingham, SX = Starcross, SC = Sub-Contracted outside NLS, FI = Field Data - outside NLS, NLS = Calculated
Key to Accreditation: UKAS = Methodology accredited to ISO/IEC 17025:2005, MCertS = Methodology accredited to MCertS Performance Standard
for testing of soils, none = Methodology not accredited
Any subsequent version of this report denoted with a higher version number will supersede this and any previous versions
END OF TEST REPORT
NLS Starcross
Staplake Mount
Starcross
Exeter
EX6 8FD
NLS Nottingham
Meadow Lane
Nottingham
NG2 3HN
NLS Leeds
Olympia House
Gelderd Lane
Gelderd Road
Leeds LS12 6DD
Page 6 of 6
WATER Analysis W166207
CustomerSiteReport No W166207
MethodID
BT
EX
HS
A
Calc_C
R3
Calc_H
D
CU
ST
SE
RV
GR
OH
SA
ICP
MS
W
ICP
WA
TV
AR
ID Number Description Sampled
BT
EX
-HS
A A
nalysis
Chrom
ium (III) (C
ALC
)
Total H
ardness as CaC
O3 (C
ALC
)
Report A
GR
O-H
SA
GC
FID
(AA
)
Nickel as N
i MS
(Dissolved)
Chrom
ium as C
r MS
(Dissolved)
Cadm
ium as C
d MS
(Dissolved)
Copper as C
u MS
(Dissolved)
Lead as Pb M
S (D
issolved)
Zinc as Z
n MS
(Dissolved)
Manganese as M
n MS
(Dissolved)
Arsenic as A
s MS
(Dissolved)
Mercury as H
g MS
(Dissolved)
Selenium
as Se M
S (D
issolved)
Vanadium
as V M
S (D
issolved)
Molybdenum
as Mo M
S (D
issolved)
Antim
ony as Sb M
S (D
issolved)
Total S
ulphur as SO
4 (Diss) V
AR
Calcium
as Ca (D
issolved) VA
R
Magnesium
as Mg (D
issolved) VA
R
Barium
as Ba (D
issolved) VA
R
Sodium
as Na (D
issolved) VA
R
Iron as Fe (D
issolved) VA
R
Boron as B
(Dissolved) V
AR
���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1436683 BH3 31/10/13EX/1436684 BH4 31/10/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No W61453
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnosall St Lawrence Date Logged 02-Nov-2013
Report Due 08-Nov-2013
Page 19 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
WATER Analysis W166207
CustomerSiteReport No W166207
MethodID
ICP
WA
TV
AR
ISE
F
KO
NE
NS
PA
HM
SW
PH
EH
PLC
VL
SF
AP
I
SF
AS
Sub045
TP
HF
ID-S
i
WS
LM3
ID Number Description Sampled
Beryllium
as Be (D
issolved) VA
R
Fluoride as F
Chloride as C
l (Kone)
Am
moniacal N
itrogen (Kone)
Nitrate as N
(Kone calc)
Chrom
ium V
I. as Cr (K
one)
PA
H G
C-M
S (16)
Phenols by H
PLC
(Low Level)
Cyanide (T
otal) as CN
SF
A
Sulphide as S
SF
A
^Cyanide (F
ree) 5ug/l
^VO
C Low
Level
TP
H by G
C(S
i)
pH units
���� ���� ���� ���� ���� ���� ���� ���� ���� ����
EX/1436683 BH3 31/10/13EX/1436684 BH4 31/10/13
Deviating Sample KeyA The sample was received in an inappropriate container for this analysisB The sample was received without the correct preservation for this analysisC Headspace present in the sample containerD The sampling date was not supplied so holding time may be compromised - applicable to all analysisE Sample processing did not commence within the appropriate holding timeRequested Analysis Key
Analysis RequiredAnalysis dependant upon trigger result - Note: due date may be affected if triggeredNo analysis scheduled
^ Analysis Subcontracted - Note: due date may vary
The integrity of data for samples/analysis that have been categorised as Deviating may be compromised. Data may not be representative of the sample at the time of sampling.
ESG Environmental ChemistryAnalytical and Deviating Sample Overview
ESG Southam Consignment No W61453
Accredited to ISO17025
Note: For analysis where the scheduled turnaround i s greater than the holding time we will do our utmost to prioritis e these samples. However, it is possible that samples could become d eviant whilst being processed in the laboratory.
In this instance please contact the laboratory imme diately should you wish to discuss how you would like us to procee d. If you do not respond within 24 hours, we will proceed as ori ginally requested.
Gnosall St Lawrence Date Logged 02-Nov-2013
Report Due 08-Nov-2013
Page 20 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Matrix MethodID Analysis Basis
Method Description
Water BTEXHSA As Received Benzene, Toluene, Ethylbenzene, & Xylenes by headspace extraction GCFID quantitation
Water Calc_CR3 As Received Calculation of Chromium III from Total Chromium and Chromium VI
Water Calc_HD As Received Calculation based on Dissolved metals analysis by ICPOESWater GROHSA As Received Determination of Total Gasoline Range Organics Hydrocarbons
(GRO) by Headspace FIDWater ICPMSW As Received Direct quantitative determination of Metals in water samples using
ICPMSWater ICPWATVAR As Received Direct determination of Metals and Sulphate in water samples using
ICPOESWater ISEF As Received Determination of Fluoride in water samples by Ion Selective
Electrode (ISE)Water KONENS As Received Direct analysis using discrete colorimetric analysisWater PAHMSW As Received Determination of PolyAromatic Hydrocarbons in water by pentane
extraction GCMS quantitationWater PHEHPLCVL As Received Determination of Phenols by HPLCWater SFAPI As Received Segmented flow analysis with colorimetric detectionWater SFAS As Received Determination of Sulphide by segmented flow analysis with
colorimetric detectionWater SubCon* * Contact Laboratory for details of the methodology used by the sub-
contractor.Water TPHFID-Si As Received Determination of speciated pentane extractable hydrocarbons in
water by GCFIDWater WSLM3 As Received Determination of the pH of water samples by pH probe
Report Number: W/EXR/166207
Method Descriptions
Page 21 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
Report Notes
Generic Notes
Soil/Solid Analysis
Unless stated otherwise,- Results expressed as mg/kg have been calculated on the basis indicated in the Method Description table.
All results on MCERTS reports are reported on a 105ºC dry weight basis with the exception of pH and conductivity.- Sulphate analysis not conducted in accordance with BS1377- Water Soluble Sulphate is on a 2:1 water:soil extract
Waters AnalysisUnless stated otherwise results are expressed as mg/lNil : Where "Nil" has been entered against Total Alkalinity or Total Acidity this indicates that a measurementwas not required due to the inherent pH of the sample.
Oil analysis specific
Unless stated otherwise,- Results are expressed as mg/kg- SG is expressed as g/cm3@ 15oC
Gas (Tedlar bag) Analysis
Unless stated otherwise, results are expressed as ug/l
Asbestos Analysis
CH Denotes ChrysotileCR Denotes CrocidoliteAM Denotes AmositeNAIIS No Asbestos Identified in SampleNADIS No Asbestos Detected In Sample
Symbol Reference
^ Sub-contracted analysis.$$ Unable to analyse due to the nature of the sample¶ Samples submitted for this analyte were not preserved on site in accordance with laboratory protocols.
This may have resulted in deterioration of the sample(s) during transit to the laboratory.Consequently the reported data may not represent the concentration of the target analyte present in the sample at the time of sampling
¥ Results for guidance only due to possible interference& Blank corrected resultI.S Insufficient sample to complete requested analysisI.S(g) Insufficient sample to re-analyse, results for guidance onlyIntf Unable to analyse due to interferencesN.D Not determined N.Det Not detectedNS Information Not SuppliedReq Analysis requested, see attached sheets for resultsÞ Raised detection limit due to nature of the sample* All accreditation has been removed by the laboratory for this result‡ MCERTS accreditation has been removed for this result
Note: The Laboratory may only claim that data is accredited when all of the requirements of our QualitySystem have been met. Where these requirements have not been met the laboratory may elect to include the data in its final report and remove the accreditation from individual data items if it believes that the validity of thedata has not been affected. If further details are required of the circumstances which have led to the removal of accreditation then please do not hesitate to contact the laboratory.
END OF REPORT
Page 22 of 22Where individual results are flagged see report notes for status.
EXR/166207 Ver. 2
November 2013 Report No D3110-13 Issue 2.0 Enclosure E
ENCLOSURE E
DRAWINGS
Site Location Plan 1
Site Plan 2