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revizuit de profesor universitarTRANSCRIPT
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La coloanele cu talere, fazarichidase gaseste in miscare turbulenta,p"":fT.ltistemul in care vitezatransferuluile masa este determinata de rezistentarazel llchlde.
Eficacitatea:La coloanele cu umplutura, dar si la cele cu
limite largi.talere, valorile eficacitatii sunt in
Functionarea discontinua:Coloanele cu umplutura cu diameter mari au masa foarte mare si prezinta
probleme deosebite larcalizarea unei distributii uniforme a celor doua faze. Ladiameter mai mici de 400 mm coloanele cu talere sunt mai ieftine decat celeechivalente cu umplutura.
c) Caracteristicile fazelor participante
Sisteme corozive:Este mai usor si mai ieftin sa se construiasca o coloana cu umplutura din
material rezistent la coroziune, decat o coloana cu talere care presupune un costfoarte ridicat.
Sisteme care contin solid sau slamuri:Coloanele cu umplutura sunt sisteme care nu contin solide sau slamuri, iar
coloanele cu talere sunt sisteme care contin solide sau slamuri in concentratie mare.
Sisteme care spumeaza:La coloanele cu umplutura pentru sistemele care spume aza datorjtabarbotarii
in lichid se formeaza pe talere o emulsie fina G - L formata din picaturi de lichid sispuma' cate va determina o uniformizare a concentratiei in coloana si prin urrnare oscadere a eficientei.
Sisteme termostabile:Coloanele cu umplutura sunt sisteme stabile din punct de vedere termic, iar
coloanele cu talere sunt sisteme care nu prezinta stabilitate din punct de vederetermic.
Sisteme vascoase:Coloanele cu umplutura sunt sisteme cu vascozitate mare, iar coloanele cu
talere sunt sisteme cu vascozitate mica.
Sisteme cu degajari de caldura:Daca efectul termic al procesului este mare la coloanele cu umplutura se
monteaza dispositive pentru colectare si redistribuire. In cazul coloan.lor.u talere semonteaza serpentine de racire pe talere care favorizeaza absorbtia. Exista sisteme cudegajari mari de caldura la absorbtie, iar coloanele cu umplutura sunt sisteme cudegajari neinsemnate de caldura la absorbtie.
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Umpluturi pentru coloane:
Umpluturile utilizate pentru coloane se pot imparti in 3 categorii:- corpuri de umplere de forma neregulata;- corpuri de umplere de forma definita;- agatare.
Pentru a fi eficiente, umpluturile trebuie sa indeplineasca urmatoareleconditii:
- sa prezinte o suprafata catmai uniforma raportata la unitatea de volum;- sa prezinte o rezistenta mica la curgerea fluidelor;- sa realizeze o amestecare buna a celor 2 faze;- sa fie ieftina;- sa prezinte o rezistenta mecanica si chimica corespunzatoare.
Corpurile de umplere de forma neregulata sunt in general foarte rarutilizate.
Corpurile de umplere pot fi asezate in mod regulat in coloana sau pot fiturnate. La umpluturile asezate in vrac distributia lichidului depinde de forma simarimea corpurilor de umplere, diamtrul coloanelor, inaltimea straturilor sidistributia initiala.
Umpluturile mici duc la formarea unor purje de lichid datorita efectelorcapilare ce apar la punctele de contact intre corpuri, ceea ce determina micsorareasuprafetei udate a umpluturii si prin urrnare scaderea eficacitatii coloanei.
In scopul realizarii unei bune distributii a lichidului in coloana, in sectiuneatransversal a straturilor de umplutura, se recomanda ca diametrul nominal alcorpurilor de umplere sa fie de cel putin 8 ori mai mic decat diametrul coloanei.
Evitarea formarii canalelor se face prin turnarea uniforma a umpluturii instrat, distributia uniforma a fazei lichide, impartirea umpluturii in mai multe straturiin care se interpun dispositive interioare pentru redistribuirea lichidului.
Gratarele se construiesc din lemne, material ceramic, metalice, plastic, informa simpla de bare paralele sau forme complexe, care permit dirijarea celor douafluide. In timp ce gratarele simple se demonteazansot, se rcalizeaza o scadere depresiune si nu se infunda cand lichidul contine particule solide in suspensie.Gratarele complexe asigura o umezire aproape complete a umpluturii, preintampinaaparitia unor curgeri partiale si a pungilor cu lichid.
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