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Welcome Address

Dear Friends and Colleagues, Welcome to Cracow and the 9 th ESEAC/SEAC Conference on Electroanalysis. The Conference this year is one of the major interna-tional meetings in the field with about 70 oral and 160 poster presenta-tions from 30 countries and all Continents except Antarctica. The Organizers have applied strict quality criteria and we hope that the presented papers are really worthy of your attention.The five plenary lectures will be given by the renowned speakers who together with the other presenters will cover a wide range of current electroa-nalysis. This field is experiencing rapid growth in diverse areas. These include environmental protection, bio- and medical analysis, DNA analysis, new electrochemical sensors, modified electrode mate-rials, new voltammetric and amperometric methods, electroanalysis in the absence of supporting electrolytes, and the others. In addition to the scientific programme we hope you will enjoy social events that have been arranged. The unique in global scale Wieliczka Salt Mine will host us for a Banquet which we believe will be a spectacular event. Also the City of Cracow, its historical Old Town and Royal Castle should add unforgetable impressions to your scientific experiences. Cracow is the former capital of Poland, a more than ten-century old city where West and East, past and future meet each other. The Conference will take place at the campus of the University of Mining and Metallurgy which is ranked among the two best Polish technical universities. Thank you for attending the Conference; we are confident that you will find it as a very important scientific event.

With best regards

Professors and Chairmen Janusz Gołaś Andrzej Lewenstam Zbigniew Stojek

Welcome addresses during the get- together party will be given by:

TheCity Mayor of CracowProf. Andrzej Gołas

,

The Rector of the University of Mining and MetallurgyProf. Ryszard Tadeusiewicz

The Secretary of ESEAC

Prof. Ari Ivaska

The Chairman of the ESEAC 2002 ConferenceProf. Janusz Gołas

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Committees

International Scientific Committee

Andrzej Lewenstam (Turku, Finland and Cracow, Poland), Co-chairman,Zbigniew Stojek (Warsaw, Poland), Co-chairman, Phil N. Bartlett (Southampton, UK), Salvatore Daniele (Venice, Italy), Hendrik Emons (Julich, Germany), Ari Ivaska (Turku, Finland), Konstantin N. Mikhelson (St. Petersburg, Russia), Malcolm Smyth (Dublin, Ireland), Paulino Tunon-Blanco (Oviedo, Spain), Joseph Wang (Las Cruces, USA),

Contents

Committees 4

Sponsors 5

Poster Presentations 5

Conference Venue 5

Local Transport 6

Social Activities 7

Scientific Programme

Plenary Lectures and Oral Presentations 8

Poster Sessions 14

Map of Cracow 22-23

Local Organizing Committee

Janusz Gołaś, (Cracow), ChairmanJacek Maria Banaś (Cracow)Andrzej Bobrowski (Cracow)Zbigniew Brzózka (Warsaw)Jerzy Górecki (Cracow)Marian Jaskuła (Cracow)Paweł Kościelniak (Cracow)Andrzej Kowal (Cracow)Władysław W. Kubiak (Cracow)Zenon Łukaszewski (Poznan)Mariusz Macherzyński (Cracow)Andrzej Parczewski (Cracow) Conference OfficeMs. Gra yna Siemińska Sponsors

The Kościuszko Foundation, Inc. An American Center for Polish CultureUniversity of Mining and Metallurgy, CracowPolish Academy of Sciences

Poster Presentations

Two poster sessions will be organised : first on Monday 10.06.2002 16:40 - 18:00 (posters numbered P1- P80) and the second on Thursday 13.06.2002, 13:30 - 15:00 (the posters with numbers higher than 80). Please, pay attention that certain changes to the general schedule have been introduced according to the authors’ whishes.

Conference Venue

Cracow is a unique city of more than a thousand years history, a former capital of Poland, and the second largest, after Warsaw, academic centre.Cracow consists of an inner town and several suburbs. The city contains a large number of historic buildings. The most notable is the Royal Castle on the Wawel Hill. Other notable buildings are the Church of Saint Mary, the Gothic edifice dating from 1223, Collegium Maius, the oldest building of Jagiellonian University (1364), ancient city walls and many others. Cracow’s old centre was included by the UNESCO World Heritage Committee on the list of the world most precious cultural monuments, covers an area of 72 hectares and has 55 pieces of architecture of the highest class. Our town has a unique atmosphere as a significant scientific and artistic centre.

Place of the Conference The Conference sessions and poster presentations will take place in :The University of Mining and Metallurgy Conference Centre: Al. Mickiewicza 30, Building B-2.

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In Cracow you can reach the University of Mining and Metallurgy by public transport bus lines. Please get off the bus at the stops on Czarnowiejska or Mickiewicza streets as pointed below.

103 KROWODRZA GÓRKA - Krowoderskich Zuchów - Makowskiego - Stachiewicza

- Kijowska - Czarnowiejska - Al.Mickiewicza - Straszewskiego - Stradomska -

Dietla - Konopnickiej - Kamieńskiego - Wielicka - Jakubowskiego - Kostaneckiego -

PROKOCIM UJ - INSTYTUT FARMACJI UJ

139 CAHTS - Al.Solidarności - Al.Przyjaźni - Al.Ró - eromskiego - Obrońców

Krzy a - Mikołajczyka - Srebrnych Orłów - Wiślicka - gen. Okulickiego-

Dobrego Pasterza - Al.29-Listopada - Al.Słowackiego - Al. Mickiewicza - Czarno-

wiejska - Nawojki - Armii Krajowej - Balicka - BRONOWICE NOWE - Balicka -

BRONOWICE MLECZARNIA

159 CICHY KĄCIK - Piastowska - Nawojki - Czarnowiejska - Al.Mickiewicza -

Al.Słowackiego - Al.29-Listopada - Wileńska - Brogi - Miechowity - Młyńska -

Bora-Komorowskiego - gen.Okulickiego - Wiślicka - Srebnych Orłów - Kruszwicka

- Popielidów - Perkuna - Piasta Kołodzieja - OS. PIASTÓW

173 AZORY - Conrada - Armii Krajowej - Nawojki - Czarnowiejska - Al.Mickiewicza

- Al.Krasińskiego - Konopnickiej - Kamieńskiego - Wielicka - Teligi - Aleksandry

- BIE ANÓW NOWY

179 DWORZEC GŁÓWNY - Pawia - Ogrodowa - Warszawska - Al.Słowackiego -

Al.Mickiewicza - Al. Krasińskiego - Konopnickiej - Kamieńskiego - Sławka -

Klonowica - Halszki - Stojałowskiego - OS. KURDWANÓW

Social activities

Sunday 9.06.2002 Get-together party

Get-together party will commence the Conference at 7.00 p.m. in the Main Building (A-0) of the University of Mining and Metallurgy, Al. Mickiewicza 30

Tuesday 11.06.2002 Wawel Royal Castle and Old Town sightseeing

Participants and accompanying persons are invited to a guided tour of Wawel Hill, which is also called the Polish Acropolis. At the Wawel Hill you will visit the Wawel Cathedral. The Cathedral used to be the place where the coronation of Polish kings was held. Then you will tour Kanonicza and Grodzka Streets that lead you to the Market Square. At the Market Square you can see several monuments like the Renessaince Cloth Hall, the Town Hall and the beautiful St.Mary

,s Church. After that you will

visit Kazimierz - the former Jewish City.

Wednesday 12.06.2002 Wieliczka Salt Mine sightseeing

Participants and accompanying persons are invited to a guided tour of the Wieliczka Salt Mine. The Salt Mine situated in the picturesque town of Wielicz-ka is an object of the UNESCO World Heritage Committee unique in the world range. The mine counts near 1000 years and contains many unique works of miner’s art of past time. In the museum a part of the route leads through three working floors and goes down to a depth of 140 meters.

Wednesday 12.06.2002 Banquet at Wieliczka Salt Mine

Banquet at Wieliczka Salt Mine will be held in a chamber about 140 meters under ground level.

Local Transport

Tickets must be punched on boarding the bus or tram. They are available in kiosks and Municipal Transport Company stands. (MPK; corner of Basztowa and Westerplatte Streets, and corner of Szewska and Podwale Streets). Available from drivers are only single trip tickets, offered for a surcharge.

Prices of bus/tram tickets in Cracow PLN

single trip ticket 2.20 one-hour ticket 2.80day ticket 9.00single trip night ticket 4.40weekly ticket 22.00

114 KAMPUS UJ - Bobrzyńskiego - Grota Roweckiego - Kapelanka - Monte Cassino

- Konopnickiej - Al.Krasińskiego - Al.Mickiewicza - Al.Słowackiego - Al.29-Listopada -

Opolska - Mackiewicza - Siewna - Górnickiego - Opolska - Wyki - PRĄDNIK

BIAŁY ZACHÓD

103 KROWODRZA GÓRKA - Krowoderskich Zuchów - Makowskiego - Stachiewicza -

Kijowska - Czarnowiejska - Al.Mickiewicza - Straszewskiego - Stradomska -

Dietla - Konopnickiej - Kamieńskiego - Wielicka - Jakubowskiego - Kosta-

neckiego - PROKOCIM UJ - INSTYTUT FARMACJI UJ

Scientific Programme

Sunday 9.06.2002 UMM Al. Mickiewicza 30, Building A-0 18:00 Registration

19:00 Get-Together Party

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Plenary Lectures and Oral Presentations

Monday 10.06.2002 University of Mining and Metallurgy Conference Centre, Building B-2, first floor, Auditorium Hall

Session Chairmen: Janusz Gołaś, Joseph Wang

09:00 - 09:20 Zygmunt Kowalski - Honorary Chairman’s special talk Polarography and voltammetry at the mercury drop growing in a step by step mode.

09:20 - 09:55 Richard G. Compton Plenary lecture: Ultrasonic enhancement of electroanalytical processes.

09:55 - 10:10 R. M. Town and H. P. van Leeuwen Metal ion speciation analysis by SCP (stripping chronopotentiometry).

10:10 - 10:25 K. N. Mikhelson Multi-species approach: a tool for improvement of the ion-selective electrode theory.

10:25 - 10:40 N.Serrano, J.Manuel Díaz-Cruz, C.Arino and M.Esteban Potentiometric stripping analysis as a tool for heavy metal speciation.

10:40 - 11:05 Coffee Break

Session Chairmen: Ari Ivaska, Paweł Kulesza

11:05 - 11:20 A.Michalska, S.Walkiewicz and K.Maksymiuk Amperometric ion sensing with poly(pyrrole) membranes.

11:20 - 11:35 A.A.Karyakin and E.E.Karyakina Transition metal hexacyanoferates in electroanalysis.

11:35 - 11:50 L.J.Nagels, G.Bazylak and D.Zielińska Designing potentiometric sensor materials for the determination of organic ionizable substances in HPLC and CE.

11:50 - 12:15 W.Kutner, K.Noworyta, R.Marczak, K.Winkler, A. de Bettencourt-Dias Electrochemical properties of thin films of fullerenes and their selected polymers. A.L.Balch, G.R.Deviprasad and F.D’Souza

12:15 - 12:40 C.M.A.Brett, S.Kresak , T.Hianik and A.M.Oliveira Brett Studies on self-assembled alkanethiol monolayers formed at applied potential on polycrystalline gold electrodes.

12:40 - 12:55 E.Ferapontova and L.Gorton Effect of the electrode material nature on direct electron transfer between the electrode and the heme active site of native and recombinant horseradish peroxidases.

13:00 - 14:00 Lunch

Session Chairmen: Salvadore Daniele, Andrzej Bobrowski

14:00 - 14:20 J.Barek and J.Zima Eighty years of polarography - history and future.

14:20 - 14:35 M.Josowicz Design of advanced materials for electrochemical gas sensors.

14:35 - 14:50 A.Walcarius New crystalline and organically modified silicates in electroanalysis: application to the detection of mercury(II) speciation.

14:50 - 15:05 P.Zuman Contributions to reductions of some azomethine bonds.

15:05 - 15:20 K.Aoki Increase in heterogeneous rate constants of Fe(CN)6 at nanometer-sized electrodes.

15:20 - 15:35 S. Pusztai, T.Dankházi and G. Farsang The role of halogen substituents in the electrodimerisation of halogeno-anilines in MeCN.

15:35 - 15:55 Coffee Break

Session Chairmen: Lo Gorton, György Farsang

15:55 - 16:10 W.Zhang, I.Gaberman and M.Ciszkowska Diffusion and concentration of molecular probes in thermoresponsive poly(n-isopropy- lacrylamide) hydrogels: effect of the volume phase transition.

16:10 - 16:25 Y.Bonfil, M.Brand and E.Kirowa-Eisner Silver, gold and silver-gold alloys in subtractive anodic stripping voltammetry.

16:25 - 16:40 F.Berbel, E.Kapoya, J.M. Díaz-Cruz, C.Arino and M.Esteban Voltammetric detection in HPLC assisted by multivariate curve resolution.

16:40 - 18:00 Poster session

Tuesday 11.06.2002 University of Mining and Metallurgy Conference Centre, Building B-2, first floor, Auditorium Hall

Session Chairmen: Andrzej Lewenstam, Kurt Kalcher

09:00 - 09:35 Ernoe Pretsch Plenary lecture: Ion fluxes in potentiometry: how to reduce their effects and how to make use of them.

09:35 - 09:55 J.Gołaś Recent trends in Polish electroanalytical chemistry.

09:55 - 10:15 H.Emons, B.Huellenkremer and M.J.Schoening Development of electrochemical flow-through detection by voltohmmetry and voltammetry.

10:15 - 10:30 N.S.Lawrence, E.H.Seymour, E.L.Beckett, J.Davis and R.G.Compton Voltammetric sensing of amines and sulfhydryl species.

10:30 - 10:45 J.D.Wadhawan, P.J.Welford, H.B.McPeak, C.E.W.Hahn and R.G.Compton Is it possible to determine simultaneously oxygen and carbon dioxide via voltammetric techniques?

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10:45 - 11:10 Coffee Break

Session Chairmen: Hendrik Emonds, Andrzej Barański

11:10 - 11:25 J.Puy, M.Torrent, J.Galceran, J.Salvador, E.Companys, J.Cecilia, Binding curve from normalised limiting currents of heterogeneous J.L.Garcés and F.Mas metal-macromolecular systems. The case of Cd/humic acid.

11:25 - 11:40 S.Daniele, A.Gambirasi, M.A.Baldo and C.Bragato Nanostructured platinum microelectrodes for the detection of hydrogen peroxide.

11:40 - 11:55 E.A.Hutton, R.Pauliukaite, B.Ogorevc and M.R.Smyth An electrochemical microsensor for the selective determination of ascorbic acid in gastric juice.

11:55 - 12:10 S.B.Hocevar, R.Pauliukaite, B.Ogorevc and J.Wang Characterization and applicability of a bismuth bulk electrode.

12:10 - 12:25 M.C. Blanco López, M.J. Lobo Castanón, A.J. Miranda Ordieres Biomimetic voltammetric sensor for vanillylmandelic acid. and P.T. Tunón-Blanco

12:25 - 12:40 A.Zon, T.Ossowski, M.Pałys and Z.Stojek Supramolecular derivatives of 9,10-anthraquinone. Electrochemistry at low ionic strength and complexing properties.

12:40 - 12:55 K. Wagner, J.W. Strojek and K. Kozieł Electrochemical and microgravimetric investigations of lead and copper deposition and stripping at solid electrodes.

13:00 - 14:00 Lunch

Session Chairmen: Pauline T. Tunón-Blanco, Renata Bilewicz

14:00 - 14:20 J.Janata, T.Kikas and H.Ishida Amperometric arrays for chemical plume tracking.

14:20 - 14:40 H.B.Mark, Jr. Electrochemically aided control of solid phase micro-extraction (ESAPME) using conducting polymer coated fibers.

14:40 - 14:55 D.O’Hare, J.V.Macpherson and A.Willows Behaviour of graphite-epoxy composite electrodes.

14:55 - 15:10 G. Lassanes-Shustak, I. Turyan, R. Shacham, M. Sheffer and D. Mandler Application of sol-gel technology for structuring the electrode-electrolyte interface.

15:10 - 15:25 M.Opallo and M.Saczek-Maj Carbon ceramic electrode modified with redox liquid.

15:25 - 15:40 F.-M. Matysik, D. Marggraf and J. A. C. Broekaert Development and characterization of indirect electrochemical detection for nonaqueous capillary electrophoresis.

15:40 - 15:55 M.T. Neshkova, V.D. Nikolova and V. Petrov New real-time electroanalytical approaches based on the principle of the electro- chemical quartz-crystal microbalance (EQCM). In situ stoichiometry and phase composition monitoring of electrodeposited chalcogenide thin films under hydrodynamic control.

16:30 WAWEL Royal Castle and Old Town sightseeing

Wednesday 12.06.2002 University of Mining and Metallurgy Conference Centre, Building B-2, first floor, Auditorium Hall

Session Chairmen: Zbigniew Stojek, Konstantin Mikhelson

09:00 - 09:35 Andrzej Więckowski Plenary lecture: Modern surface analysis: new approaches to study electrode sur- faces for electrochemistry and electrocatalysis.

09:35 - 10:00 A.S.Barański and L.J.Nelson Electrochemical detection at hot-disk ultramicroelectrodes under flow injection and capillary electrophoresis conditions.

10:00 - 10:15 S.Nilsson, M.Svedberg, J.Pettersson, F.Björefors, K.Markides and L.Nyholm Electrochemistry as a versatile tool to study processes in electrospray ionisation mass spectrometry.

10:15 - 10:30 A.Jaworski, D.Hazebrouck and K.Wikiel An automatic voltammetric analyzer for monitoring electrochemical deposition processes.

10:30 - 10:45 M.Pałys and Z.Stojek Relation between diffusion coefficients of the reactant and the product and steady-state currents measured under low ionic strength conditions.

10:45 - 11:00 Ch.Amatore, C.Sella, L.Thouin and J.-S.Warkocz Diffusion at double microband electrodes operated within a thin film coating. Theory and experimental illustration.

11:00 - 11:20 P.J.Kulesza Inorganic templates as design elements in nanocomposite materials on electrodes: fabrication, charge transport and possibility of sensor applications.

11:20 - 11:45 Coffee Break

Session Chairmen: Chris Brett, Jiri Janata

11:45 - 12:05 K.Slowinska, S.W.Feldberg and M.Majda Electrochemical proton time-of-flight, a microelectrode generator-sensor method with potentiometric detection.

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12:05 - 12:30 J.Wang, D.Xu, R.Polsky, N.Kawde and A.Erdem Particle-based electrochemical assays of DNA hybridization.

12:30 - 12:45 F.Turcu, M.Etienne, B.Ballesteros Katemann and W.Schuhmann Formation of chemically active nanostructures as a basis for novel miniaturised analytical devices.

12:45 - 13:00 L. Gorton, F.-D. Munteanu, L. T. Kubota, A. Malinauskas and A. Kuhn Electrocatalytic oxidation of NADH at electrodes modified with different dyes immobilised on transition metal phosphates.

13:00 - 13:15 N.Mano, S.Ben-Ali and A.Kuhn Electrode modification by molecular lego for sensor applications.

13:15 - 13:30 P.Ugo, N.Pepe and L.M.Moretto Direct electroanalysis of proteins at nanoelectrode ensembles: the cytochrome c case.

13:30 - 13:45 J.Barek, J.C.Moreira and J.Zima Voltammetric determination of biologically active organic substances using non-traditional electrode materials.

14:00 - 15:00 Lunch

16:00 Wieliczka Salt Mine Sightseeing

19:00 Banquet at Wieliczka Salt Mine

Thursday 13.06.2002 University of Mining and Metallurgy Conference Centre, Building B-2, first floor, Auditorium Hall

Session Chairman: Władysław W. Kubiak

09:00 - 09:35 Marek Trojanowicz Plenary lecture: Flow electrochemistry in chemical analysis - recent advences and perspectives.

09:35 - 10:10 Johann Bobacka Plenary lecture: Potentiometric ion sensors based on conducting polymers.

10:10 - 10:25 M.Fojta, L.Havran, F.Jelen, R.Kizek, S.Billova, A.Kourilova Sensors for DNA hybridization with electrochemical detection. M.Masarik and E.Palecek

10:25 - 10:40 R.Bilewicz, S.Sęk and P.Rowiński Molecularly ordered matrices for immobilization of biomolecules on electrodes.

10:40 - 11:05 Coffee Break

Session Chairmen: Jiri Barek, Koichi Aoki

11:10 - 11:25 G.-U.Flechsig, O.Korbut, P.Gründler, J.Wang and A.Erdem Hybridisation of nucleic acids at heated electrodes.

11:25 - 11:40 P.Mader Electroanalytical methods and certification of biological matrix reference materials.

11:40 - 11:55 L.Stoica, T.Ruzgas and L.Gorton Is pH a guarding parameter of cellobiose dehydrogenase?

11:55 - 12:10 D.Leech, S.Richer, N.LeGrand, F.Barriere, Y.Ferry, D.Rochefort, Laccase reduction of molecular oxygen: applications to sensing, paper bleaching R.Bourbonnais and M.Paice and fuel cells.

12:10 - 12:25 S.Szunerits, N.Sojic, L.Servant and D.R.Walt Optical tools as analytical devices for electrochemically initiated phenomena: application to corrosion studies and electrochemiluminescence.

12:30 - 13:30 Lunch

13:30 - 15:00 Poster Session

Session Chairmen: Małgorzata Ciszkowska, Karel Vytras

15:00 - 15:15 Z.Łukaszewski, B.Karbowska and W.Zembrzuski Determination of mobile thallium in soil by flow-injection differential pulse anodic stripping voltammetry.

15:15 - 15:30 P.J.Almeida, J.A.Rodrigues, L.F.Guido, J.R.Santos, A.A.Barros and A.G.Fogg Voltammetric determination of free and total sulphite in beer.

15:30 - 15:45 A.Bobrowski, B.Baś, J.Dominik, E.Niewiara, J.Zarębski, E. Szalińska Methodology for chromium speciation in water samples by catalytic adsorptive stripping voltammetry.

15:45 - 16:00 E.Ferapontova and E.Domínguez Elecrochemical detection of DNA damage induced by oxidative electrochemical damage of DNA and by UV-irradiation performed with DNA-modified gold electrodes.

16:00 - 16:15 Closing of the Conference

Friday 14.06.2002

Optional excursions: Auschwitz, rafting on the Dunajec River Breakthrough, Zakopane

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P1 Electroanalysis of autoantibodies and platinum-containing medicines with DNA-based amperometric biosensor. S.S.Babkina, N.A.Ulakhovich, E.N.Moiseeva

P2 The coated – wire ion selective electrode for determination of copper (II) based on new derivation thiosemicarbazid. M.Mazloum Ardekani , M.Salavaty Niassar ,S.Farhadi , M.Khayat Kashany

P3 Coated- wire ion selective electrode based on N,N′- Ethylene Bis (P-…) for measurement of copper ion. M. Mazloum Ardakani, M.Salavati- Niassar, P. Pourhakkak

P4 Development of an amperometric biosensor for ß- N-oxalyl-L-α, ß-diaminopropionic acid (ß-ODAP). N. W. Beyene, K. Kalcher

P5 Selective thiocyanate PVC-membrane based on a 1,8-dibezyl-1,3,6,8,10, 13-hexaaza cyclotetradecan nickel (II) perchlorate. M. Mazlum Ardakany, M. Salavati Niasari, A. A. Ensafi, M. Chahooki P6 Silver(I) coated-wire selective electrode based on Hydroxy Resorc[4]arene derivative. M. Mazloum Ardakani, M. Salavati Niasari, A. A. Ensafi, S.W. Mirhoseini

P7 The coated – wire electrode for determination of chromate and dichromate based on Bis(acetylacetonato) Copper(II). M.Mazloum Ardakani, M.Salavati – Niasari, A. Dastanpoor

P8 Selective redoxmetry for reductant’s analyses (COD, ascorbic acid, glucose ...). S.B.Sapogova, A.M.Pisarevsky, I.P.Polozova, A.V.Kaverin

P9 Selective redoxmetry for iodometric enzymatic analyses of biochemical objects. A.V.Kaverin, A.M.Pisarevsky, I.P.Polozova, S.B.Sapogova

P10 Potentiometric sensors prepared by chemical treatment of silver electrode surface. M. Kolar, D. Dobcnik

P11 Flow injection analysis of aziprotryne using an electrochemical sensor based on cobalt phthalocyanine modified carbon paste electrode. A. Zapardiel, M. Chicharro, E. Bermejo, E. Madrid, M. Moreno, A. Sánchez, C. Rodríguez.

P12 Selective fluoride recognition and potentiometric properties of ion-selective electrodes based on Zr(IV)-porphyrins. Ł. Górski, E. Malinowska, M. E. Meyerhoff

P13 Electrocatalytic response of electrode modified by cobalt(II) phthalocyanine during oxidation of some organic compounds. L.G.Shaidarova, S.A.Ziganshina, A.V.Gedmina, H.K.Budnikov

P14 Iodine - iodide reference electrode for potentiometric titrations of bases in acetic acid. C. Maccà, L. Soldà P15 Use and misuse of selectivity coefficients in the characterisation of ion-selective electrodes. C. Maccà

P16 Novel modified potentiometric sensors for separate surfactant determination in homologous series. A.I.Kulapin, E.B.Nikol’skaya, E.G.Kulapina

P17 Binuclear phthalocyanates of nikel (II) as active components in anion-selective electrodes. Y. N. Blikova, N. V. Shvedene, K. N. Otkidach, I. V. Pletnev, L. G.Tomilova

P18 The properties of the indomethacin ion-selective electrode with polymeric membrane. J. Lenik, B. Marczewska

P19 The properties of the cadmium ion-selective electrode containing in the polymeric membrane chelating substance. C. Wardak , B. Marczewska

P20 Na+-selective miniaturised ise based on silicon back-side contact structure with self- plasticising ion-selective membrane. K. Wyglądacz, M. Durnas, Z. Brzózka, E. Malinowska

P21 The effekt of lipophilic compounds on the selectivity and sensitivity detection limits of ionselective electrodes based on phosphoryl containing podands. O.M. Petrukhin, S.N. Kouratchenkova, A.F. Zhukov, Yu.I. Urusov,V.Ye. Baulin

P22 Construction and characterization of solid contact calcium-selective microelectrodes. M. Södergård, J. Bobacka, A. Lewenstam and A. Ivaska

P23 Potentiometric study of equilibrium constants of quercetin. S.Micić, Nataša Pejić, V. Kuntić, M. Aleksić, D. Malešev

P25 Determination of nitrogen in lubricating oils and additives using an ammonia ion selective electrode. K.A.Kwakye, M.Obeng

P26 Determination of boron in lubricating oils using potentiometric titration. K. A. Kwakye

P27 Comparison of methyl isobutyl ketone (MIBK),toluene and chlorobenzene as solvents in the measurement of the total base number (TBN) of lubricating oils by potentiometric titration in perchloric acid. M.Obeng, K.A.Kwakye,

P28 Potentiometric sensors on the basis of semiconductor materials in ecoanalytical monitoring. V. A. Burakhta, L. I. Khasainova, Z. Kh. Kunasheva

P29 Salophene metallocomplexes as ionophores in polymeric membranes of anion-selective electrodes. W. Wróblewski, K. Wojciechowski, Z. Brzózka

P31 Electrode modification with cubic liquid-crystalline phases hosting biocatalysts. P Rowiński, R Bilewicz

P32 Simultaneous voltammetric determination of molybdenum and copper by adsorption cathodic differential pulse stripping method using a principal component artificial neural network. A A. Ensafi, T. Khayamian, M. Atabati

P33 A square-wave voltammetry of reversible redox reactions on the thin mercury film covered solid electrode. M. Lovrić

P34 Influence of the preparation method on the sensitivity of electrodes modified with organic-inorganic hybrids. S. Sayen, M. Etienne, A. Walcarius

P35 Electrochemical detection of copper(II) at an electrode modified by a carnosine–silica hybrid material. S. Sayen, C. Gérardin, L. Rodehuser, A. Walcarius

P36 Norflurazon and its voltametric behaviour at mercury electrode. M. Zimpl, M. Kotoucek, K. Lemr

P37 Application of an optimization procedure for the determination of rifampicin by differential pulse adsorptive stripping voltammetry using metal complexation. M. Asunción Alonso Lomillo, O. Domínguez Renedo, M. J. Arcos Martínez.

P38 Application of an optimization procedure in adsorptive stripping voltammetry for the determination of gallium. M. J. Gómez , O. Domínguez, J. Aguilar.

Poster SessionsUniversity of Mining and Metallurgy Conference Centre, Building B-2, second floor, Conference Hall

Poster Session I - Monday 10.06.2002 16:40 - 18:00

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P39 Simultaneous determination of aluminium and chromium by adsorptive stripping voltammetry with PCV. M. Cámara, O. Domínguez, M. J. Arcos.

P40 Application of an optimization procedure in adsorptive stripping voltammetry for the determination of indium with ammonium pyrrolidine dithiocarbamate. I. Paolicchi, O. Domínguez, M. Asunción Alonso, M. J. Arcos.

P41 Electrochemical detection of organic diamines based on the enhancement of anodic cobalt(II) oxidation. A. Vaskelis, A. Jagminiene

P42 Determination of tributyltin and dibutyltin compounds by differential pulse anodic stripping voltammetry at trace levels. H. M.V.M. Soares, A. A.N. Almeida

P43 Determination of Cr(VI) by adsorptive stripping voltammetry using 2,2’-Bipyridine. R. Jugade, A.P.Joshi

P44 Some applications of electrocatalysis in stripping voltammetry of sulfur compounds. F. G. Banica, A. Ion, N. Spataru, T. Spataru

P45 The effect of the type electrolyte on the analytical determination amount Cd in Pb-Cd alloys by ALSV method. R.M.Zejnilovic, N.Z.Blagojevic, V.R.Kastratovic

P46 Electrochemical study and flow-injection determination of tin at various carbon eletctrodes. L.K. Shpigun, V.K.Lunina

P47 Electrochemical solid phase microextraction of anions and cations using polypyrrole coatings and an integrated three-electrode device. G. Liljegren, J. Pettersson, K. Markides, L. Nyholm

P48 Square wave voltammetry of the molybdenum-1,10 phenanthroline-Fulvic acid complex. F. Quentel, C. Elleouet, C. L. Madec, A. Laouenan, V. Mirceski

P49 Cathodic stripping voltammetry of 5-phenyl-1,3,4-oxadiazole- 2-thiol and its cobalt(II) complex. S. Skrzypek, M. Kasprzak, W. Ciesielski

P50 Cathodic stripping voltammetry of 6-methyl-2-thiouracil. M. Kasprzak, S. Skrzypek, W. Ciesielski

P51 Cathodic electrochemical detection of nitrophenols at a bismuth film electrode. E. A. Hutton, B. Ogorevc, M. R. Smyth

P52 Electrochemical detection of hydrogen peroxide at carbon based electrodes modified. with selected polycyanometalates R. Pauliukaite, B. Ogorevc

P53 Assembly and characterization of nanoparticles based electrochemical probes. F. Valentini, S. Orlanducci, D. Compagnone, M. L. Terranova, S. Botti, G. Palleschi.

P55 The brdicka polarographic catalytic hydrogen evolution and its utilization for determination of organic thiols. P. Mader, V. Veselá, I. Šestáková, V. Dorcák, P. Cížková

P57 Cyclic voltammetry and quartz crystal microbalance electrochemical studies of 1-isothiocyanato-4-(methylsulfinyl)butane. K. Sarna , T. Kasprzycka-Guttman , Z. Fijałek

P58 Functionalization of electrode surfaces with monolayers of thiophene derivatives. K. Stolarczyk, R. Bilewicz, A. Skwierawska, J. F. Biernat,

P59 Accessible potential windows of platinum and glassy carbon electrodes in glacial acetic acid and its mixtures with ethyl acetate. S. Michałkiewicz, M. Kaczor

P60 Determination of water in acetic acid with Pt microelectrodes. S. Michałkiewicz, E. Bzinkowska, J. Małyszko

P61 “Ecl - package” – software for electrochemiluminescence simulation at microelectrodes I. B. Svir, A. I. Oleinick, A. V. Klimenko.

P62 Developement of a new electrochemical device for low flow analytical systems and capilary electrophoresis. M. Chicharro, A. Zapardiel, E. Bermejo, A. Sánchez

P63 The study of silver cementation on copper by electrogravimetry. H. Cesiulis

P64 Tensammetric titration of potassium ion with tetraphenylborate. A. Ion, M. B. Costache, I. V. Grecu, F. G. Banica

P65 Permselective properties of electropolymerized guaiacol derivatives. G. Milczarek, A. Ciszewski

P66 The new methods of the determination of the stability and of the formation and dissociation kinetic of complexes in non-aqueous solutions. E. Gorodkiewicz, Z. Figaszewski

P67 Application of hybrid genetic-simplex algorithm for decomposition of electochemical responses in SDLSV method. M. Jaskuła, G. Kasprzyk

P68 The polyelectrolytic effect in metal macromolecular complexation. E.Companys, J.Puy, M.Torrent, J.Galceran, J.Salvador, J.Cecília, J.L.Garcés, F. Mas

P69 Preparation and characterisation of mercury microelectrodes with insulating thickness comparable to the electrode radius. Application to determination of heavy metals in real matrices. I. Ciani, S. Daniele, A. Baldo

P70 Charge transfers between two immiscible liquids: studies with a liquid|liquid microelectrode. S. Peulon, V. Guillou, M. L’Her

P71 Electrocatalytic properties of electropolymerized curcumin-Ni(II) complex. G. Milczarek, B. Lewandowska, K. Krutowski, A. Ciszewski

P72 Coulometric titration of cysteine, cystine and glutathione with anodic generated chlorine. W. Ciesielski, M. Skowron, S. Skrzypek

P73 The determination of electrochemically active cyanic complex of silver in borate- phosphate-carbonate electrolytes. O. Bersirova, V. Kublanovsky

P74 Chronopotentiometry as a method for determining stability constants of metal complexes. V. Kublanovsky, V. Nikitenko, K. Litovchenko

P75 Development of electrochemically based technique for hydrogen distribution analysis in metal. S.M. Beloglazov

P76 Voltammetric characterisation of alkanethiol self-assembled monolayers integrity on gold surface for SAW biosensor development. L. Rotariu, M. Schlensog, B. Schmid

P80 Development of a method for measurement of traces of chromium (VI) by electrochemical batch injection analysis. O. Filipe, C.S. Neves, C.M.A. Brett

P108 Electrocatalytic voltammetry for fludarabine determination in urine. N. de los Santos-Álvarez, M J. Lobo-Castañón, A. J. Miranda-Ordieres, P. Tunon-Blanco

P116 Electrocatalytic voltammetry for fludarabine determination in urine. N. de los Santos-Álvarez, M. J. Lobo-Castañón, A. J. Miranda-Ordieres, P. Tunon-Blanco

P117 Electrocatalytic detection of oligonucleotide hybridisation. P. Rodríguez Granda, P. de los Santos Álvarez, M. J. Lobo Castañón, A. J. Miranda Ordieres, P. Tunon-Blanco.

P118 Adsortive-stripping voltammetry of rifamycins at unmodified and surfactant hemically- modified carbon paste electrodes. S. Gutiérrez Fernández, M. J. Lobo Castañón, A. J. Miranda Ordieres, P. Tunon-Blanco

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P121 Development of a multiresidue liquid chromatography method with electrochemical detection (HPLC-ECD) for the determination of macrolide antibiotics. J. González de la Huebra, G. Bordin, A. R. Rodriguez

P130 A remote stripping sensor based on mercury microelectrodes for in situ monitoring of trace metal contaminants. M. A. Baldo, S. Daniele, G. A. Mazzocchin , J. Wang

P134 Electrochemical sensors and biosensors for polyphenolic compounds in olive oil and red wines. D. Compagnone, S.H. Alarcon, M. Del Carlo, A. Pepe, G. Palleschi

Poster Session I I - Thursday 13.06.2002, 13:30 - 15:00

P24 Influence of the electrode substrate on the polymer-modified-voltammetric-electrode analytical performance. M.Robótka, W.W.Kubiak

P30 Modulation of the cationic sensitivity of the poly(pyrrole) films doped with adenosine triphosphate. J. Migdalski, T. Błaż, B. Paczosa, A. Lewenstam

P56 Low-support chronoamperometry at microelectrodes as a promising tool for the determination of diffusion coefficients of substrate and product. W. Hyk, A. Nowicka, Z. Stojek

P77 High precision voltammetric current – potential calculations using infinite series solution. J. Mocak, A. Bobrowski

P78 The effect of chemical structure of alkyl oxybutylene-oxyethylene block copolymers on their analytical signals in the indirect tensammetric technique. Z. Łukaszewski, E. W. Nowak, A. Szymański

P79 Comparison of analytical signals in different tensammetric techniques. Z. Łukaszewski, E. W. Nowak, A. Szymański

P81 Small-volume radial flow cell for all-solid-state ion-selective electrodes. M. Vázquez, J. Bobacka, A. Ivaska, A. Lewenstam

P82 Determination of molybdenum after sorption on activated carbon. R. Zielińska, B. Rożańska, K. Kasiura

P83 Cyclic voltammetric studies on zinc monocrystals in organic solvents. J. Swiatowska-Mrowiecka, E. Temmerman, J. Banaś

P84 High precision voltammetric current – potential calculations using Infinite series solution. J. Mocak, A. Bobrowski P85 The orthogonal set of parameters for the evaluation of smoothing in voltammetry. M. Jakubowska, W. W. Kubiak

P86 Electrochemical determination of glue and thiourea in the process of copper refinery of the sarcheshmeh factory. B.Rezaei, E.Rezaei

P87 Development of absolute electroanalytical approaches to characterization of bulk redox conducting materials. A. Lewera, B. Dąbrowska, P. J. Kulesza, M. A. Malik, G. Żukowska, W. Wieczorek

P88 The novel voltammetric detection methods with mercury electrodes and electrochemical analyser EA9. B.Baś, E.Niewiara, M.Jakubowska, J.Migdalski, Z.Kowalsk, W.W.Kubiak

P89 Application of the fumed silica to enhance mineralization of botanic samples for voltammetric analysis. E.Niewiara, B.Baś, Z.Kowalski, W.W.Kubiak

P90 Application of linearly growing mercury drop surface in electroanalytical experiment. Z. Kowalski , B. Baś, E. Niewiara

P91 Electrostatic reaction control at nano-structured interfaces. F. Marken, K. J. McKenzie

P92 Liquid | liquid electroinsertion of chromates and dichromates. F. Marken, C. M. Hayman, P. C.B. Page

P93 Solid-state voltammetric probing of spin transition in cobalt hexacyanoferrate molecular magnet. K. Miecznikowski, M. Winiarek, P. J. Kulesza, M. A. Malik, G. Wittstock, S. Sauter

P94 Non-competitive immunosensor for prostatic specific antigen based on impedance measurement of enzyme-catalysed polymer degradation. C. Fernández-Sánchez, C. McNeil

P95 Voltammetric determination of micro particles of some local anaesthetics and ntithusics immobilised on the graphite electrode. S. Komorsky-Lovric, N. Vukašinovic, R. Penovski

P96 Electrochemical study of amitrole at glassy carbon electrode and its determination in environmental samples. M. Chicharro, A. Zapardiel, E. Bermejo, M. Moreno

P97 Carbon paste electrode modified with dibenzo-dithia-diazapentacene for electrocatalytic electro-oxidation of NADH. D. Dicu, F. Munteanu, I. C. Popescu, L. Gorton

P98 Combined use of voltammetry and multivariate curve resolution for the study of metallothioneins and related molecules. S.Díaz-Cruz, M. José López Martínez, J. Manuel Díaz-Cruz, C. Ariño, R.Tauler, M. Esteban

P99 Determination of platinum by adsorptive-catalytic stripping voltammetry in the presence of azometine complexing agents. Part 2 Application. J. Kowalska, M. Zbrzezna, M. Sawicki, S. Huszal, J. Golimowski

P100 Determination of platinum by adsorptive-catalytic stripping voltammetry in the presence of azometine complexing agents. Part 1 Theory. M. Sawicki, S. Huszal, J. Kowalska, M. Zbrzezna, J. Golimowski

P101 Electrochemical biosensor based on semiconductor structures: individual and simulta- neous determination of simazine and 2,4-D. N. F. Starodub, V. M. Starodub, V. E. Krivenchuk, V. F. Shapovalenko

P102 Trace determination of azathioprine and risperidone in pharmaceutical formulations by differential pulse polarography. C. Jeyaseelan, A. P. Joshi

P103 Amperometric cholesterol and glucose biosensors based on an electrocatalytic prussian-blue (PB) layer and electropolymerized films of polypyrrole. Influence of a self-assembled mono-layer on the PB layer lifetime and the biosensor s sensitivity. J. C. Vidal, J. Espuelas, E. García-Ruiz, J. R. Castillo

P104 Entrapment of cholesterol oxidase and cholesterol esterase inside electropolymerized films of polypyrrole and aminonaphthalene derivatives for the amperometric determination of total cholesterol in serum. J.C. Vidal, J. Espuelas, F. Pascual, E. García, J.R. Castillo

P105 Decouplerfree elimination of high voltage-field effects in electrochemical detection of neurotransmitters in on-chip capillary electrophoresis. O. Klett, I. Nischang, O. Larsson, L. Nyholm

P106 Determination of drugs by biosensors based on amine oxidase from squid liver. O. V. Yagodina, B. N. Kormilitsyn

P107 Factors influencing the immobilization of oligonucleotides at glassy carbon electrodes. M. L. Pedano, G. A. Rivas.

P109 Low-density lipoprotein gold modified electrode – electroanalytical tool for antioxidative behaviour evaluation. S. C. Litescu, G.L. Radu, C. Bala

P110 Enzymatic determination of fructose at a tetrathiafulvalene modified self-assembled monolayer gold disk electrode. S. Campuzano, R. Gálvez, M. Pedrero, F. J. Manuel de Villena, J. M. Pingarrón.

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P111 Analytical abilities of enzyme immunosensor for ribonuclease. E.V. Khaldeeva, E.P. Medyantseva, G.R. Safina, H.C.Budnikov

P112 Cholinesterase biosensors based on disposable screen-printed Pt-contained electrodes for analysis of atrazine and simazine. N.Y. Ilyicheva, E. P. Medyantseva, H.K. Budnikov

P113 Electrochemical behaviour of osmium-labelled dna on mercury and carbon electrodes. L. Havran, M. Fojta, R. Kizek, S. Billova, E. Palecek

P114 Analysis of bicarbonate in artificial kidney dialysis fluid by “electronic tongue” sensor system. A. Legin, S. Makarychev-Mikhailov, E. Suglobova, A. Rudnitskaya, P. Gavrilenkov, A. Smirnov, Y. Vlasov

P115 Electrochemical oxidation of hyperforin on glassy carbon electrode and its analytical applications. M. Wurglics, W. Likussar, M. Schubert-Zsilavecz, A. Ortner

P119 Rapid toxicity assessment. A new method based on quantifying mediated microbial respiration at a microelectrode. J. Webber, A.Tizzard, J. Hay, R.Gooneratne, R.John, N.F.Pasco

P120 Determination of impurities in paracetamol preparations by HPLC method with amperometric detection. E. Wyszecka-Kaszuba, M. Warowna-Grześkiewicz, Z. Fijałek

P122 Sequence specific electrochemical detection of Listeria monocytogenes by DNA biosensors. T. Oczkowski, M. Filipiak

P123 Development of biological sensor based on electrocatalytic detection of hydrogen peroxide at prussian blue/polymer composite film. K. Derwińska, Ł. Tymecki, R Koncki, K. Miecznikowski, S. Głąb, P. J. Kulesza

P124 The use coulometry and voltammetry for evaluation of antioxidant capacity of the plant extracts. I. F. Abdullin, H. C. Budnikov, E. N. Turova, N. N. Chernyshova

P125 Combination of differential pulse polarography and multivariate curve resolution for the study of phytochelatins and related molecules. B. H. Cruz, A. Alberich, J. M. Díaz-Cruz, C. Ariño, R. Tauler, M. Esteban.

P126 Voltammetric determination of Cd, Pb and Zn in ultrasound - assisted soil extract. B. Krasnodębska - Ostrega, M. Kowalska

P127 Voltammetric mercury determination in sediments sampled in a lagoon ecosystem (Ravenna, Italy). C. Locatelli, G. Torsi

P128 Experimental design methodologies to optimise the square-wave cathodic stripping. voltammetry determination of As(V) in water S. Sanllorente, O. Domínguez, M. J. Arcos

P129 Is any complexation isotherm valid to analyse macromolecular binding of trace metal ions in environmental samples? J. L. Garcés, F. Mas, J. C., E. Companys, J. Galceran, J. Salvador, J. Puy

P131 Voltammetric determination of oxytetracycline residues in food samples using carbon fibre microelectrodes. L. Agüí, A. Guzmán, M. Pedrero, P. Yáñez-Sedeño, J.M. Pingarrón

P132 Electronic tongue for the quality assessment of soft drinks. A. Legin, B. Seleznev, A. Rudnitskaya, G. Roy, Yu. Vlasov, P. Milne

P133 Galvanostatic study of phenolic compounds as inhibitors of srb-induced corrosion of aluminium. Yu.V. Goliak, S.M. Beloglazov

P135 Voltammetric monitoring of the content of iron in waters and effluents using a dental amalgam sensor electrode. Ø. Mikkelsen, K. H. Schrøder

P136 Determination of ions in wood pulp by all-solid-state Ion-selective electrodes (ISEs). F. Sundfors, J. Bobacka, A. Ivaska, A. Lewenstam

P137 Electrochemical sensor development for toxic heavy metals. R. O. Kadara, J. Newman, I. E. Tothill

P138 Carbon paste electrodes plated with metallic films in stripping potentiometry of some heavy metals and metalloids. I. Svancara, R. Metelka, R. Pazdera, J. Czaganova, G. Jansova, A. Królicka, A. Bobrowski, K. Vytras

P139 Cathodic stripping voltammetric determination of selenium(IV) in the flow system. M. Korolczuk, M. Grabarczyk

P140 A novel catalytic adsorptive stripping voltammetric method of iron determination as its 1,2-cyclohexane dionedioxime complex. A. Królicka, A. Bobrowski

P141 The extraction and voltammetric detection of poly(hexamethylenebiguanide) in environmen- tal water samples. M. J. Pickup, D. W. M. Arrigan, N. J.Truslove, D. Williams, L. Jayes

P142 Carbon paste electrodes in the analysis of organic substances. J. Zima and J. Barek

P143 Hybrid films composed of monolayers of polyoxometallates and two-dimensional conducting polymers: fabrication, reactivity and potential applications. M. Chojak, K. Miecznikowski, P. J. Kulesza, M. A. Malik, A. Kuhn

P144 Monitoring microspot enzyme activity with scanning electrochemical microscopy. C. A. Wijayawardhana, T. Wilhelm, G. Wittstock

P145 Effect of a plasticizer on the detection limit of calcium-selective electrodes. I. Bedlechowicz, M. Maj Żurawska, T. Sokalski, A. Hulanicki

P146 Hydrogen peroxide detection with iridium oxide electrode. H. Elzanowska, V.I. Birss

P147 Thick-film potentiometric silver-ion selective electrodes. Ł. Tymecki, E. Zwierkowska, S. Głąb, R. Koncki

P148 SEM and AFM studies of the porphyrinic large disc sensor for nitric oxide measurements. M. Macherzyński, A. Kowal, J. Gołaś

P149 Influence of polymer structure on properties of membrane coated potentiometric microsensors. J. Marstalerz, H. Müller, K. Edelmann A. Reiche, B. Sandner

P150 Capillary electrophoresis for the forensic analysis of ball-point pen inks extracted from paper. J. Mania, J. Bis, P. Kościelniak

P151 Application of capillary electrophoresis to the drug analysis of forensic interest. K. Madej, M. Woźniakiewicz

P152 Formation of chemically active microstructures as a basis for novel miniaturised analytical devices. F. Turcu, M. Etienne, B. B. Katemann, W. Schuhmann

P154 Enhancement of electrolytic ionization efficiency in electrospray (ES) with electrochemistry on-line with ESI/MS. T. Zhang, S.P. Palii, J.R. Eyler, A. Brajter-Toth

P155 Biosensor arrays based on enzymes immobilised on screen-printed electrodes. E. Dock, S. Sapelnikova, J. Emnéus, T. Ruzgas

P156 Voltammetric determination of traces of labile forms of chromium in on-line system. M. Grabarczyk, M. Korolczuk

P157 Estimation of usefullness of the mercury film electrode on the silver base [Hg(Ag)Fe]. B. Baś, E. Niewiara, Z. Kowalski

P158 Controlled growth mercury drop microelectrode (CGMDME). B. Baś, E. Niewiara, Z. Kowalski

P159 NH4+- sensitive electrode for determination of urease kinetics.

B. Krajewska, M. Chudy, M. Drozdek, Z. Brzózka

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Map of Cracow

ESEAC 2002

Railway Station

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Conference Office

Ms. Gra yna Siemińska International School of TechnologyUniversity of Mining and MetallurgyAl.Mickiewicza 30, 30-059 Kraków, Poland e-mail: eseac@uci.agh.edu.plphone/fax +48 12 617 25 34

Conference site at:http://www.agh.edu.pl/eseac

Notes

Notes

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