petroleum standards

5/25/2018 Petroleum Standards

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AccuStandard

Certified

Reference

Standards4th Edition

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ET

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OvASTMM

Member


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M

New Products in this Catalog

Low Sulfur and Nitrogen Standards (see pages 6-11)

LUFT/LUST Standards (see pages 81-98) TPH Standards (see pages 81, 92-93, 96-97)

No Haz Fee ICP & AA Standards (see pages 67-75)

Additional New ASTM Standards

Involvement in the Petrochemical Industry Participation in regular ASTM meetings

Active in D-02 and D-16 subcommittees

Provides support to several Petrochemical Instrument Manufacturers

Resources Low Sulfur Analyzers (such as XOS) for Measurements to ppb Levels

Instrumention for Analyzing Standards for ICP, ICP-MS, AA, GC/MS,

GC/FID, GC/EC, GC/NPD, Karl Fischer Titrator, and others

NIST/NVLAP Accredited (Lab Code 200389-0) as a PT Provider

ISO 9001:2000 Certified (ISO 9001 for the last 10 years)

Extensive Inventory of ASTM and Related Standards

Experience in Petrochemical Requirements Years of Round Robin Studies with ASTM

Ampulled over 300 gallons of ASTM fuel sets including

over 35 gasoline and hydrocarbon blends

Standards for over 100 ASTM Methods

17 years of Manufacturing, Organic & Inorganic Standards Synthesizes rare Hydrocarbons not otherwise available

Notice the Difference with AccuStandard

PRINTED ONRECYCLED PAP

AccuStandard, Inc. 2003


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Table of Contents

Wear Metals GroupSulfur Standards Group

Quality System is Certified to comply with the International ISO 9001:2000 Quality Standard

Q

ASTM # Method Description paD-5441 MtBE Analysis by GCD-5442 Petroleum Waxes by GCD-5443 PNA Analysis by Multidimensional GCD-5453 Sulfur by Ultra Violet FluorescenceD-5480 Engine Oil Volatility by GCD-5482 Vapor Pressure Standards 29D-5501 Ethanol Analysis by GCD-5580 Aromatics by GC 32D-5599 Oxygenates by OFID 34D-5600 Trace Metals by ICP

D-5622 Oxygenates by Reductive PyrolysisD-5623 Sulfur Compounds by Sulfur Selective DetectionD-5708 Trace Metals by ICP 39D-5762 Nitrogen by ChemiluminescenceD-5769 Aromatics by GC/MS 42D-5771 Cloud Point of Petro ProductsD-5772 Cloud Point of Petro Products (Linear Cooling Rate)D-5773 Cloud Point of Petro Products (Constant Cooling Rate)D-5863 Trace Metals by AAD-5901 Freezing Point Aviation Fuels (Auto Optical Method)D-5972 Freezing Point Aviation FuelsD-5986 Oxygenates and Aromatics by GC/FTIRD-6160 PCBs by GCD-6258 Solvent Red 164 Dye Concentration in Diesel FuelsD-6277 Benzene in Spark Ignition FuelsD-6293 Oxygenates (O-PONA) in Engine Fuels by GCD-6296 Total Olefins in Spark Ignition Engine Fuels by GCD-6304 Water in Liquid Petro Products

D-6334 Sulfur in Gasoline by Wavelength WD-XRF 10D-6352 Boiling Range Distribution of PetroleumD-6378 Vapor PressureD-6379 Aromatic Hydrocarbon by HPLCD-6417 Engine Oil by GCD-6428 Sulfur by ECDD-6443 Metals in Oil 58D-6445 Sulfur in Gasoline by ED-XRF 10D-6481 Lube Oils by ED-XRF 58, 63D-6550 Olefin Content of Gasoline by SFCD-6591 Aromatic Hydrocarbon by HPLC(IP 391)E-1064 Water in PetroleumISO/CD V & Ni with Mn

Organometallic (Wear Metals) Analysis by AA, ICP, DCP, XRF 26, 28, 59Plasma Emission Spectroscopy (ICP) 67ICP (No Haz Fee) New 67

Atomic Absorption Spectroscopy (AA) 67, 73AA (No Haz Fee) New 67, 73Plasma Emission / Mass Spectroscopy (ICP/MS)Trace Metals, Chlorine in Lube Oil, and Organo Tin NewIon Chrom 76

LUFT/LUST and TPH (New Section) 81

IndexQuote Form bOrder Information b

D-3605 Trace Metals in Gas Turbine Fuel by AAD-4628 Wear Metals in Lube OilD-4927 Wear Metals and Additives by WDXRF 25, 63D-4951 Wear Metals and Additives by ICPD-5185 Wear Metals and Additives by ICPD-5708 Trace Metals by ICP 39,D-5863 Trace Metals by AAD-6443 Metals in Oil 58,D-6481 Lube Oils by ED-XRF 58, 63

ASTM # Method Description pageCross Reference Tables (ASTM,IP,ISO,DIN,JIS,AFNOR) IIAnalytical Capabilities IIIOn-Line Ordering IVQuality Control 1-2

D-56 Flash Point Standards 3D-86 Synthetic Distillation Standard 3D-92 Flash Point Standards (COC) 3D-93 Flash Point Standards (PMCC) 3D-445 Viscosity Calibration Standard 3D-611 Aniline Point Standard 4

D-1015 Freezing Point Standards 4D-1319 Olefin Analysis by FIA 4D-1744 Water in Liquid Petroleum Products 5D-2386 Freezing Point Calibration Standards 5D-2500 Cloud Point Calibration Standards 5D-2622 Sulfur by XRF 10D-2789 Hydrocarbon Analysis in Gasoline by GC/MS 11

PIANO, PONA, PNA by GC 12-13Proposed Method for Detailed Hydrocarbon Analysis 14Detailed Hydrocarbon Analysis PONA VI 14

D-2887 Boiling Range by GC 14Simulated Distillation (SIM DIS) by GC 15

D-3120 Sulfur by Oxidative Microcoulometry 16D-3230 Salts in Crude Oil 16D-3231 Phosphorus in Gasoline 16D-3237 Lead in Gasoline by AA 16D-3246 Sulfur in Petroleum Gas by Oxidative Microcoulometry 17D-3340 Li & Na in Lubricating Greases by Flame Photometer 17

D-3524 Diesel Fuel Analysis by GC 17D-3605 Trace Metal in Gas Turbine Fuels by AA 17D-3606 Aromatics in Gasoline by GC 18D-3610 Total Co Analysis by Potentiometric Titration 18D-3710 Boiling Range by GC 20D-3798 p-Xylene Analysis by GC 20D-3831 Manganese in Gasoline by AA 20D-4059 PCB Analysis by GC 21D-4110 Ion Chrom 76D-4291 Ethylene Glycol by GC 21D-4294 Sulfur by ED-XRF 7-11, 21D-4377 Water in Liquid Petroleum Products 5, 21D-4420 Aromatics in Gasoline by GC 22D-4628 Wear Metals in Lube Oil 22D-4629 Nitrogen by Chemiluminescence 23D-4815 Oxygenates in Gasoline by GC 24D-4927 Wear Metals and Additives by WD-XRF 25,63D-4928 Water in Liquid Petroleum Products 6, 25

D-4929 Chlorine in Crude Oil by Microcoulometry 25D-4951 Wear Metals and Additives by ICP 26D-5056 Trace Metals in Petroleum Coke by AA 26D-5059 Lead in Gasoline by X-Ray Spectroscopy 27D-5134 Petroleum Naphthas through n-Nonane by GC 27D-5184 Al and Si by ICP-AES & AA 28D-5185 Wear Metals and Additives by ICP 28D-5186 Aromatics by SFC 28D-5188 Vapor - Liquid Ratio Temperature 29D-5191 Vapor Pressure Standards 29D-5307 Boiling Range Distribution of Crude Petroleum by GC 29

D-2622 Sulfur by XRF 10D-3120 Sulfur by Oxidative Microcoulometry 10, 17D-3246 Sulfur in Petro Gas by Oxidative Microcoulometry 6-11D-4294 Sulfur by ED-XRF 10D-5453 Sulfur by Ultra Violet Fluorescence 6-11, 31D-5623 Sulfur Compounds by Sulfur Selective Detection 38D-6334 Sulfur in Gasoline by Wavelength WD-XRF 6-11D-6445 Sulfur in Gasoline by ED-XRF 6-11


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Use the AccuStandard Cross

Reference Tables to Match

various International

Methods for known

Petrochemical analysis.

Tables Generated from(a) R.A. Nadkarni, Guide to ASTM Test Methods for the Analysis of Petroleum Products and Lubricants, Manual 44(200), ASTM West Conshohocken, PA(b) Annual Book of ASTM Standards 2000, Volumes 05.01 to 05.05

ANALYSIS ASTM IP ISO DIN JIS AFNOR PAGE

Tag Flash Point D-56 51411 K 2580 M07-003 3

Distillation D-86 123 3405 51751 K 2254 M07-002 3

COC Flash Point D-92 36 2592 51376 K 2265 T60-118 3

PMCC Flash Point D-93 34 2719 51758 K 2265 M07-019 3

Kinematic Viscosity D-445 71-1 3104 51562 K 2283 T60-100 3

Aniline Point D-611 2 2977 51775 M07-021 4

Hydrocarbon Types by FID D-1319 156 3837 51791 K 2536 M07-024 4

Water (Karl Fischer) D-1744 6296 T60-154 5

Freezing Point D-2386 16 3013 51421 K 2276 M07-048 5

Cloud Point D-2500 219 3015 51597 K 2269 T60-105 5

Sulfur by XRF D-2622 51400T6 K 2541 10

Boiling Range By GC D-2887 3924 14

Sulfur by Oxidative Microcoulometry D-3120 16591 16

Lead by AAS D-3237 428 16

Sulfur by Oxidative Microcoulometry D-3246 373 M07-052 10

Metals by AA D-3605 413 8691 51790T3 17

Benzene by GC D-3606 425 18

Sulfur by ED-XRF D-4294 336 8754 M07-053 21

Water (Karl Fischer) D-4377 356 10336 5

Metals by AA D-4628 308 51391T1 22

Nitrogen by Chemiluminescence Detection D-4629 379 M07-058 23

Metals by WD-XRF D-4927 407 51391T2 25, 63

Water (Karl Fischer) D-4928 386 10337 5, 25

Lead in Gas By X-Ray D-5059 228 27

Vapor Pressure D-5191 394 M07-079 29, 32

Oxygenates D-5599 408 34-36

Cloud Point D-5771 444 52



Freezing Point D-5901 434 53

Auto-Freeze Point D-5972 435 53

Hydrocarbons Automatic D-6379 436 57

Hydrocarbons Automatic NEW D-6591 391 57

Metals 14597 62

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and a NIST/NVLAP

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Cross Reference Table Sorted by ASTM Method

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This is a partial list of Standards available for ASTM Methods

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Milligram to Kilogram Scale Glassware

Equipment to work under N2/Ar

Flash and Liquid Solid Phase Chrom. (mg to 2 kg)

Preparative TLCBuchi Rotary Evaporator

Vacuum Drying Oven

Parr Pressure Reactor (high pressure reaction, hydrogenation)

Distillation Equipment - High Vacuum Distillation, Molecular

Distillation (Kugelrohr), Spinning Band Columns,

Packed and Vigreaux columns

Melting Point Apparatus

pH meter

Viscometer

Centrifuge

Lab Resources

Analytical Capabilities

Inorganic (ICP)PE Optima 3000

Spectro FMD-07

Organics

GCs: (6) HP 5890 Series II, FID, NPD, ECD all withauto injectors

GC/MS: (3) HP 5971A

HP 5971A with OI Analytical Purge & Trap

PE Q-Mass 910

HPLC: Varian 5000 with Applied Bioscience Fluoresce

detector and HP auto injector

Sulfur (low level)XOS (XRF) with monochromatic wavelength disperser

Antek 9000 Series (UVF)

MiscellaneousIon Chromatograph, Waters 600E with

Conductivity detector 431, Alltech 335 Ion

Suppressor

Automatic Polarimeter, Zuzi W22

Karl Fischer Titrator

Analytical Instruments


6/116

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AccuStandard offers over 30,000 different standards, and if you can't find the specific standard you need, we will prepare a cus

formulation. Our custom organic and inorganic standards are a fast, economical way to address your unique requirements. To

make an inquiry for Custom Quotes visit our website.

You can also Email your requirements to [email protected] or Fax us at 203-786-5287. Please include the follow

information: List of analytes and concentrations, Solvent or matrix, Quantity required (milliliters), Packaging unit size (millilit

per ampule, bottle, or vial).

Quality Control Options1. Gravimetric/Volumetric Certification: Each standard is measured gravimetrically and then QCed instrumentally (where

available). Every component in the standard is guaranteed to be within 0.5% of the requested value unless otherwise stated.

solutions are made up to volume using class A glassware. A certificate comes with each standard and documents the gravimetr

values used.

2. Quantitative Validation: Full QA/QC method includes extended GC analysis using both internal and calibration standards pl

statistical analysis. A data package is provided containing analytical and gravimetric data (Organic customs only).

Also available: OEM Standards - Privately labeled standards manufactured and tested to your specifications.

Custom Formulations


7/116

AccuPetroCheck Consensus Value QC Standards

AccuPetroTest Gasoline

AccuPetroTest Gasoline

AccuPetroTest

Fax 203-786-5287 Toll Free 800-442-5290 / 203-786-5290 Website www.accustandard.com

QC

Technical Note

Low Sulfur QC SampleSBPT-LSGAS $ 25 / 2 x 15 mL

Parameter Method Approx. RangeSulfur D-5453 0 - 50 g/g

Olefin QC SampleSBPT-OLEFINSFC $ 25 / 2 x 15 mL

Parameter Method Approx. RangeTotal Olefins D-6550 1 - 40 Vol.%

AccuPetroCheck QC StandardsTwo of the fuels are available asAccuPetroCheck Consensus Value QC

Standards. The AccuPetroCheck CARB a

Conventional gasoline reference materials ha

all parameters listed on the certificate with t

Consensus Values and the regression equatio

for reproducability. Use of these Reference

Materials improve the quality of laboratory

results. The Consensus Values listed reflect

initial statistical treatment of the data at the

the catalog was published. The actual certif

provided with the AccuPetroCheck QC stan

will have the accepted Consensus Value base

statistical treatment of the data.

Sulfur Single Blind AccuPetroTestAlternative Matrices StandardsAccuStandard has manufactured a number o

Diesel and White Mineral Oil QC products

containing a gravimetrically prepared amou

Sulfur. Use of these alternative matrix mate

can provide further evaluation of the QA/QC

process in the laboratory. Two samples will

sent for the test parameter and a separate sea

envelope containing the gravimetrically prep

sulfur values is also provided. The secondsample is for repeatability testing or for use

future QA/QC reference.

Sulfur in White Mineral Oil QCStandardSBPT-SWMO $ 25 / 2 x 15 mL

Parameter Approx. RangeSulfur 20 - 11000 g/g

See ASTM Methods D-2622, D-3120,D-3246-92, D-4294, D-5453 for SulfurCalibration Standards

Sulfur in Diesel Fuel QC StandardSBPT-SDF $ 25 / 2 x 15 mL

Parameter Approx. RangeSulfur 20 - 11000 g/g

See ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration Standards

Conventional Gasoline QCStandardASTM-FUEL-QCS-02-PAK $ 60 / 5 x 15 mL

Parameter Method Value Conc.Total Aromatics D-1319 34.6 Vol.%Total Olefins D-1319 12.4 Vol.%Total Saturates D-1319 62.8 Vol.%Sulfur D-2622 0.0338 Wt.%Sulfur D-4294 0.0368 Wt.%Sulfur D-5453 317.36 g/gSulfur D-6344 338.78 g/gBenzene D-5769 0.55 Vol.%Toluene D-5769 5.53 Vol.%Total Aromatics D-5769 32.51 Vol.%

Benzene D-6277 0.52 Vol.%Total Olefins D-6550 12.4 Vol.%

CARB Low Sulfur RFG QCStandardASTM-FUEL-QCS-01-PAK $ 60 / 5 x 15 mL

Parameter Method Value Conc.Total Aromatics D-1319 24.5 Vol.%Total Olefins D-1319 5.3 Vol.%Total Saturates D-1319 58.3 Vol.%Sulfur D-2622 0.0057 Wt.%Sulfur D-4294 0.0078 Wt.%Sulfur D-5453 55.76 g/gSulfur D-6344 59.31 g/gBenzene D-5769 0.80 Vol.%Toluene D-5769 4.92 Vol.%Total Aromatics D-5769 23.42 Vol.%

Benzene D-6277 0.78 Vol.%Total Olefins D-6550 5.3 Vol.%

AccuPetroCheck and AccuPetroTest Real World Gasoline QC StandardsIn cooperation with ASTM D-02 subcommittee 3 and 4, AccuStandard ampulled 21 Real World gasoline reference fuels. Consensus Values

been determined for these reference fuels by various ASTM Round Robins to provide Petrochemical Laboratories with a source of well

characterized gasoline standards for use in QA/QC applications and as Single Blind test samples over an extended period of time. As new A

D-02.03 and D-02.04 Test methods are promulgated they require mandatory Quality Control testing of real world samples. AccuStandard

PetroTest & PetroCheck standards are being successfully used to achieve these new Quality Control requirements.

Quality Control Standards

Quality Control Standardscontinue on next page

Real

This comprehensivesingle blind gasoline QCsample tests for moreparameters from a singlesample. The actualgasoline sample will haveconsensus values listedon the datasheet that fallwithin the range listed foreach parameter.

Comprehensive Single Blind Gasoline QC SampleSBPT-COMP $ 50 / 2 x 15 mL

Parameter Method Approx. Range Conc.Total Aromatics D-1319 8 - 60 Vol.%Total Olefins D-1319 1 - 40 Vol.%Total Saturates D-1319 30 - 80 Vol.%Sulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%Sulfur D-5453 0.5 -500 g/gSulfur D-6344 1.0 - 1000 g/gBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%Total Aromatics D-5769 8 - 60 Vol.%Benzene D-6277 0.1 - 2.0 Vol.%Total Olefins D-6550 1 - 40 Vol.%


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2 Quality System is Certified to comply with the International ISO 9001 Quality Standard

QC

QC

Quality Control Standards

Conducting a Petrochemical Round Robin for a new ASTM method?

Select AccuStandard to prepare the necessary samples for the Round Robin studyAccuStandard has packaged for ASTM committee D-02 various select groups of gasoline fuels and hydrocarbon products for use in various

Round Robin studies.

Large Sample OfferingAccuStandard was selected by ASTM committee D-02 to fill, seal and package an initial set of 21 different types of Round Robin Gasolines.

Each gasoline was selected due to its unique properties. These unique properties will be determined by various ASTM methods under evalua

through ASTM subcommittees. AccuStandard has expanded this offering with additional materials blended for other ASTM Round Robins.

FlexibilityUse the original 21 gasoline samples to conduct a Round Robin and we can label the samples appropriately to protect the integrity of the Rou

Robin. In addition, we can easily add additional samples to your specific Round Robin study to expand the scope of the method for differen

matrices, concentrations or instrument types.

AccuPetroTest Gasoline QCAccuPetroTest Single BlindStandardsPetrochemical laboratories looking to

the performance of the laboratory for

specific parameter can order the Sing

Blind AccuPetroTest sample for the

parameter of interest. Two real worl

gasoline samples will be sent for the parameter requested and a separate s

envelope containing the determined

Consensus Value is also provided. T

second sample is for repeatability tes

or as a future QA/QC reference.

Petro PT Samples

Oxygenate PT SampleWith MtBE contamination problems in drinking water, numerous states arenow requiring certification for Oxygenate monitoring. Join AccuStandardsnext study for Oxygenate analysis. Our timely PT schedule easily allowsyour lab to be proactive in new regulatory requirements. The analytes inthe standard and the PT sample have been drawn from the California listof known prevalent oxygenates in gasoline. These new Oxygenate PTsamples and standards allow your Lab to:

Expand testing capabilities Generate new testing revenue

Eliminate standard preparation Easily combine with otherAccuStandard Volatile standards

***

WP-PT Oil, Grease & TPHIPE-OILG-001-AS $ 32 / 5 mLIPE-OILG-001-AT $ 32 / 5 mLIPE-OILG-001-AV $ 32 / 5 mLSample conc. after prepContains 2 analytes listed below

Analyte List Sample rangeTotal Oi l & Grease 5-100 mg/LTPH 5-100 mg/L

Oil and GreaseWC-OILG-10X-1 $ 45 / 100 mL1000 g/mL Total Oil and Grease in n-Propanol

Contains 500 g/mL vegetable oil and 500 g/mL of petroleum oil.Shake well before use.

Suggested Calibration Standard

Olefins QC SampleSBPT-OLEFIN $ 25 / 2 x 15 mL

Parameter Method Approx. RangeTotal Aromatics D-1319 8-60 Vol.%Total Olefins D-1319 1 - 40 Vol.%

Total Saturates D-1319 30-80 Vol. %See ASTM Method D-1319 for Sulfur CalibrationStandards

Sulfur QC SampleSBPT-SGAS $ 25 / 2 x 15 mL

Parameter Method Approx. RangeSulfur D-2622 0.0001 - 0.0930 Wt.%Sulfur D-4294 0.0016 - 0.0930 Wt.%

Sulfur D-5453 4.0 - 500 g/gSulfur D-6344 1.0 - 1000 g/g

See ASTM Methods D-2622, D-3120, D-3246-92,D-4294, D-5453 for Sulfur Calibration Standards

Benzene/Toluene QC SampleSBPT-BENZ $ 25 / 2 x 15 mL

Parameter Method Approx. RangeBenzene D-5769 0.1 - 2.0 Vol.%Toluene D-5769 1.0 - 15 Vol.%

See ASTM Methods, D-3606, D-5580-95, D-5769-95for Benzene Calibration Standards

Aromatics QC SampleSBPT-AROM $ 25 / 2 x 15 mL

Parameter Method Approx. RangeTotal Aromatics D-5769 8 - 60 Vol.%

See ASTM Methods, D-3606, D-5580-95, D-5769-95for Benzene Calibration Standards

SUFFIX KEY"AS" = Formal PT Study"AT" = Pre-Test"AV" = Values Included

This PT sample can be used by gravimetric oil and greasemethods. In addition, it can also be used for TPH analysis bgravimetric methods including the EPA method 1664. Thesample contains real world material commonly found at

petroleum containment sites.

Technical Note

MTBETAME

ETBEDiisopropylether

WS-PT OxygenatesOPE-OXY-001-AS $ 47 / 2 mLOPE-OXY-001-AT $ 47 / 2 mL

OPE-OXY-001-AV $ 47 / 2 mLSample conc. after prep 5.0-50 g/LContains 4 analytes listed below

NEW

TAME (2000 g/mL)t-Butanol (10000 g/mL)

Oxygenate Gasoline Additive StandardOGAD-001 $ 30 / 1 x 1 mLOGAD-001-PAK SAVE 20% $ 120 / 5 x 1 mLAt stated conc. in MeOH 5 comps.

MtBE (2000 g/mL)ETBE (2000 g/mL)Isopropyl ether (2000 g/mL)

Suggested Calibration Standard

ASTM Round Robin

&

PT

Samples

Lab Code 200389-0

* Designed for NELAC/CA Indicates that theses analyteincluded in the NVLAP Scope oAccreditation, Lab Code 20038

NEW

**

*


9/116

ASTM D-56, D-92, D-93 Flash Point Standards


Memb

Certified Flash Point StandardsThe reference material is a stable, pure hydrocarbon with a method specific flash pointdetermined by an inter-laboratory study using the ASTM Method # referenced.

Cat. No. ASTM # Nominal Flash Point Price / Unit

ASTM-P-133-01 PMCC D93 65C $ 175 / 250 mLASTM-P-133-02 PMCC D93 134C 130 /250 mLASTM-P-133-03 COC D92 138C 130 /250 mLASTM-P-133-04 TCC D56 67C 175 /250 mL

Physical Properties

Cat. No. ASTM # Nominal Flash Point Price / Unit

ASTM-P-132-01 PMCC D93 65C $ 110 /250 mLASTM-P-132-02 PMCC D93 93C 110 / 250 mLASTM-P-132-03 COC D92 200C 110 / 250 mLASTM-P-132-04 COC D92 230C 110 / 250 mL

ASTM D-86 Synthetic Distillation Standard

The automatic distillation apparatus duplicates the distillation conditions of the manual method. Theincreased reliance on electronic control requires an independent standard to verify that the apparatus isperforming correctly. This synthetic blend of hydrocarbons boil in the temperature range specified inASTM D-86 distillation groups 1 and 2, and a fuel oil that meets the group 4 criteria.

The group 1 and 2 standards cover the boiling range 129 - 368 F (54 - 187 C) and are verified byconsensus analysis with twelve refinery laboratories. The group 4 standard covers the range from 410 -670 F (210 - 355 C). Products are packaged in convenient sizes to meet your laboratory sampleanalysis demands.

Verified by consensus analysis using ASTM Method # referenced

Meth

Cat. No. Group Description Price / Unit

ASTM-P-126-01 1, 2 Synthetic Distillation Standard $ 160 /500 mLASTM-P-126-SET 1, 2 Synthetic Distillation Standard 290 /2 x 500 mL

ASTM-P-127-01 4 Distillation Standard 160 /250 mLASTM-P-127-02 4 Distillation Standard 290 /500 mL

Oils are tested inaccordance withASTM D-445

Technical NoteAlso see Cloud PointStandards used for ASTMMethod D-2500 on page 5

Standards of Interest

ASTM D-445 Viscosity Calibration Standards

ASTM D-92 & Flash & Fire Points by Cleveland Open Cup (COC) &

ASTM D-93 Flash Point by Pensky Martin Closed Cup (PMCC)

See Method D-56 on this page for the comprehensive line of flash point standards

Cat. No. Viscosity @ 40 C Price / Unit

ASTM-P-128-01 4 Cst $ 60 /500 mLASTM-P-128-02 7 Cst 60 /500 mLASTM-P-128-03 19 Cst 60 /500 mLASTM-P-128-04 61 Cst 60 /500 mLASTM-P-128-05 180 Cst 60 /500 mL

ASTM-P-128-06 520 Cst 60 /500 mL

Originally designed forASTM D-56-98a,D-92-98a, D-93-99b

Originally designed forASTM D-86-99a

Originally designed forASTM D-445-97


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Member

ASTM

The following set of standardhave been prepared for thedetermination of Aromatics,Olefins, Oxygenates and

Saturates in petroleum fractioby Fluorescent IndicatorAdsorption (FIA) IP designat156/95.

The final certificate for the Fcalibration curve lists not onlthe volume percents for thehydrocarbon types, but also individual volume percents foeach analyte in the functionagroup.

To further assist thePetrochemist, the weight fracfor each hydrocarbon type aindividual analyte is listed on

final certificate. By providingindividual weights thePetrochemical chemist can uthe FIA standards for othertypes of instrumentationmeasuring these Petroleumfractions.

Technical Note

ASTM D-611 (Reapproved 1998) Aniline Point Standards

ASTM D-1015 Freezing Points of High Purity Hydrocarbons

See Method D-2386 page 5 for AccuStandards new line of Freezing Point Standards

Method 611

1015

1319

The accuracy of automated aniline point apparatus can be verified using a range of standards whoseaniline points are determined using ASTM D-611 (Method A) and ASTM D-611 (Method E). Standards arepackaged in 20 mL ampules in an inert atmosphere.

Physical Properties

Cat. No. Nominal Aniline Point Price / Unit

D-611-SET Set include 5 Standards listed below $ 90 / 5 x 20 mLAniline Point Verification SetMethod 611(A)

D-611-01 0C 20 mLD-611-02 30C 20 mLD-611-03 55C 20 mLD-611-04 68C 20 mLD-611-05 94C 20 mL

Cat. No. Nominal Aniline Point Price / Unit

D-611E-SET Set include 3 Standards listed below $ 90 / 3 x 20 mLAniline Point Verification SetMethod 611(E)

D-611E-01 43C 20 mLD-611E-02 62C 20 mLD-611E-03 77C 20 mL

Cat. No. Price / Unit

ASTM-P-134-PAK Pure Aniline $ 30 / 5 x 15 mL

Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7

Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %

Total Olefins 2.0 4.0 5.0 6.0 8.0 10.0 12.0Total Paraffins 57.0 55.0 52.0 51.0 45.0 45.0 40.0Total Aromatics 23.0 24.0 25.0 26.0 29.0 28.0 30.0Total Oxygenate 18.0 17.0 18.0 17.0 18.0 17.0 18.0

ASTM D-1319 Calibration Standards by Fluorescent Indicator Adsorption FIA

For routine purposes pureAniline is packaged in ampuunder dry nitrogen. Thisminimizes the risk of oxidatio

Technical Note

For the mandatory real world QC samplesstipulated in the Method, see page 1-2


Vol. %1-Heptene 33.3

Vol. %1-Pentene 33.32,3-Dimethyl-2-butene 33.3

FIA Olefin StandardFIA-OLE $ 40 / 1 x 1 mLFIA-OLE-5ML SAVE 40% $ 120 / 1 x 5 mL

3 comps.

mix ratiom-Xylene 161,2,4-Trimethylbenzene 81,3,5-Trimethylbenzene 81,2,4,5-Tetramethylbenzene 4Naphthalene 4

mix ratioBenzene 4Toluene 32Ethylbenzene 8p-Xylene 8o-Xylene 8

Vol. %2,3-Dimethylpentane 14Isooctane 16n-Octane 14n-Decane 7

Vol. %n-Pentane 8n-Hexane 9Cyclohexane 15n-Heptane 14

FIA Aromatic StandardFIA-ARO $ 30 / 1 x 1 mLFIA-ARO-5ML SAVE 33%$ 100 / 1 x 5 mL

10 comps.

FIA Paraffin StandardFIA-PAR $ 30 / 1 x 1 mLFIA-PAR-5ML SAVE 33% $ 100 / 1 x 5 mL

8 comps.

D-1319

Meets

EPAGuidelines

forRFG

Analysis

Olefin FIA Calibration CurveFIA-CAL-SET $ 300 / Set of 7 x 1 mL

Originally designed forD-611-82

Originallydesigned forD-1319-99


11/116

ASTM D-1744, E-1064, D-4377 Water in Liquid Petroleum Products by

D-4928, D-6304 Karl Fischer


Memb

Many ASTM Petrochemicalmethods and specificationsreference using QA/QCstandards for water contentmeasurements. AccuStandahas formulated a compreherange of water standardspackaged in convenient sizemeet the various referencedmethods.

Technical Note

ASTM D-2386 Freezing Point Calibration Standards

ASTM D-2500 Cloud Point Calibration Standards

Meth

Verified by consensus analysisASTM Method D-2386

Technical Note

Cat. No. Description Price / Unit

KF-0.6X-5ML-VAP Water content 60 g/g $ 65 /10 x 5 mLKF-1X-2ML-VAP Water content 100 g/g 40 /10 x 2 mLKF-1X-5ML-VAP Water content 100 g/g 45 /10 x 5 mLKF-1X-20ML-PAK Water content 100 g/g 50 /5 x 20 mL

KF-10X-2ML-VAP Water content 1000 g/g 40 /10 x 2 mLKF-10X-5ML-VAP Water content 1000 g/g 45 /10 x 5 mLKF-10X-20ML-PAK Water content 1000 g/g 50 /5 x 20 mL

KF-50X-2ML-VAP Water content 5000 g/g 40 /10 x 2 mLKF-50X-5ML-VAP Water content 5000 g/g 45 /10 x 5 mLKF-50X-20ML-PAK Water content 5000 g/g 50 /5 x 20 mL

Value Added Paks (Cat. No.sending in -VAP) providemultiple single units packagedtogether for both greaterstability and cost savings.

Physical Properties

Cat. No. Nominal Freezing Point Price / Unit

ASTM-P-129-01 - 50 C $ 110 /250 mL

ASTM-P-129-02 - 45 C 110 /250 mL

Cat. No. Cloud Point, Approx. Value Price / Unit

ASTM-P-131-01 + 5 C $ 110 /250 mLASTM-P-131-02 - 2 C 110 /250 mLASTM-P-131-03 - 10 C 110 /250 mLASTM-P-131-04 - 15 C 110 /250 mLASTM-P-131-05 - 20 C 110 /250 mL

Standards are available for coulometric Karl Fischer titrations and are packaged in 2 mL, 5 mL, and 20 mL ampules insets of 5 and 10. The following concentrations are available:

Originally designed for

D-2386-97

Verified by consensus analysis ASTM Method D-2500

Technical NoteOriginally designed forD-2500-00


12/116


ASTM

SULFUR

Low Sulfur Standards on following pages

Sulfur StandardsASTM Methods for

Sulfur

Analysis

D-2622-98, D-3120-96, D-3246-96, D-4294-98, D-5453-00, D-6334-98, D-6445-99 & Proposed ASTM Sulfur MethAccuStandard offers the Petroleum Industry the most complete line of calibration standards designed for todays Proposed &

Promulgated test methods for Sulfur analysis. These calibration standards are designed specifically for the analysis of Sulfur in

wide variety of matrices such as #2 diesel fuel, white mineral oil, kerosene, gasoline, crude oil & residual oil.

Traceability, Quality and Certification

All Sulfur standards are manufactured from the highest quality raw materials, including well characterized starting materials &lowest sulfur matrices available from the Petrochemical market. All standards are manufactured on a weight/weight basis usin

balances that are calibrated and verified daily against reference mass standards directly traceable to NIST under test No.

822/254480. The concentration of these working level Sulfur standards have established traceability links to NIST SRMs whe

available.

Convenient PackagingSince applicable concentration ranges will vary based on the instrumentation used & the nature of the sample the standards can

ordered as complete sets, individual bottles, or Ready-to-Aspirate AccuShots.

AccuShots... Packaged to improve analytical standard integrityAccuStandard is the first standard manufacturer to provide sulfur standards in convenient and Ready-to-Aspirate AccuShot 20

sealed ampules. Each 20 mLAccuShot provides the necessary material for calibration curve development or daily QA/QC. B

purchasing AccuShots the analytical chemist can open a fresh shot for each analysis which eliminates opening and pipettingrepeatedly from a stock bottle. This minimizes contamination and evaporation. These ship with no haz fee for additional savin

ASTM D-5453

Test to Low ppbSulfur

Contact us for a copy of theSouthwest Research Institute

D-5453 Fitness for Use Report


13/116

Limits of Detection < 1 ppm

Fast and easy sample preparation.

Typical measurement time: 300 sec

Dynamic range: 0-1000 ppm in one

calibration.

No sample conversion or reagents

required.

Exceptional signal-to-background

provides high sensitivity for

low-level sulfur fuels

Analytical Capabilities

X-Ray Optical Systems, Inc.15 Tech Valley DriveEast Greenbush, NY 12061Tel. 518-880-1500website: www.xos.com

Monochromatic WDXRF Technology

MWD XRF Sulfur Analyzerin Diesel and Gasoline Fuels

XOS SINDIE AnalyzerX-Ray optics enable detection capability well

beyond traditional XRF techniques. The

same Monochromatic WD XRF technology

of the SINDIE bench-top sulfur analyzer is

available in an on-line sulfur analyzer.

SULFURANALYSIS INULTRA LOW SULFUR FUELS

Repeatability:1 ppm 0.5 ppm

10 ppm 1.7 ppm

100 ppm 5.3 ppm

500 ppm 11.7 ppm


14/116


ASTM

SULFUR

Sulfur in

Mineral Oil

Diesel Fuel

Sulfur in Light Weight Mineral Oil (20 cSt)Sulfur in Heavy Weight Mineral Oil (75 cSt)

Individual Sulfur 1 -10 units 10 +unitsStandards 4 oz Bottle $ 55 ea $ 50 ea

Sulfur StandardsASTM Methods

AccuShots... Packaged to improve analyticalstandard integrity

AccuStandard is the first standard manufacturer toprovide sulfur standards in convenient and Ready-to-Aspirate AccuShot 20 mL sealed ampules. Each 20 mLAccuShot provides the necessary material for calibrationcurve development or daily QA/QC. By purchasingAccuShots the analytical chemist can open a fresh shotfor each analysis which eliminates opening and pipettingrepeatadly from a stock bottle. This minimizescontamination and evaporation. These ship with no hazfee for additional savings.

Ready-to-Use


8

ASTM Methods Sulfur in Mineral Oil

Sulfur conc. calculated from % sulfur in di-n-butyl sulfide

Technical Note

Sulfur in Ready-to-UseConcentration White Mineral Oil Sulfur AccuShots

g/g Wt. % Cat. No. Cat. No.Blank 0.000 SWMO-BL-4 SWMO-BL-SHOT

100 0.010 SWMO-1X-4 SWMO-1X-SHOT200 0.020 SWMO-2X-4 SWMO-2X-SHOT300 0.030 SWMO-3X-4 SWMO-3X-SHOT400 0.040 SWMO-4X-4 SWMO-4X-SHOT500 0.050 SWMO-5X-4 SWMO-5X-SHOT750 0.075 SWMO-7.5X-4 SWMO-7.5X-SHOT

1,000 0.10 SWMO-10X-4 SWMO-10X-SHOT1,500 0.15 SWMO-15X-4 SWMO-15X-SHOT2,000 0.20 -------------------- --------------------------3,000 0.30 SWMO-30X-4 SWMO-30X-SHOT4,000 0.40 -------------------- --------------------------5,000 0.50 SWMO-50X-4 SWMO-50X-SHOT7,000 0.70 SWMO-70X-4 SWMO-70X-SHOT

10,000 1.00 SWMO-100X-4 SWMO-100X-SHOT

15,000 1.50 SWMO-150X-4 SWMO-150X-SHOT20,000 2.00 SWMO-200X-4 SWMO-200X-SHOT30,000 3.00 SWMO-300X-4 SWMO-300X-SHOT40,000 4.00 SWMO-400X-4 SWMO-400X-SHOT50,000 5.00 SWMO-500X-4 SWMO-500X-SHOT60,000 6.00 SWMO-600X-4 SWMO-600X-SHOT

Set of above SWMO-CAL-SET-4 Each AccuShot productCat. No.s 19 x 4 oz. $ 850 contains 5 x 20 mL

ampules at the statedconc. for $ 60Individual Sulfur 1 -10 units 10 +units

Standards 4 oz Bottle $ 55 ea $ 50 ea

Sulfur in Ready-to-UseConcentration White Mineral Oil Sulfur AccuShots

g/g Wt. % Cat. No. Cat. No.Blank 0.000 SWMO-LT-BL-4 SWMO-LT-BL-SHOT

100 0.010 SWMO-LT-1X-4 SWMO-LT-1X-SHOT200 0.020 SWMO-LT-2X-4 SWMO-LT-2X-SHOT300 0.030 SWMO-LT-3X-4 SWMO-LT-3X-SHOT400 0.040 SWMO-LT-4X-4 SWMO-LT-4X-SHOT500 0.050 SWMO-LT-5X-4 SWMO-LT-5X-SHOT750 0.075 SWMO-LT-7.5X-4 SWMO-LT-7.5X-SHOT

1,000 0.10 SWMO-LT-10X-4 SWMO-LT-10X-SHOT1,500 0.15 SWMO-LT-15X-4 SWMO-LT-15X-SHOT2,000 0.20 -------------------- --------------------------3,000 0.30 SWMO-LT-30X-4 SWMO-LT-30X-SHOT4,000 0.40 -------------------- --------------------------5,000 0.50 SWMO-LT-50X-4 SWMO-LT-50X-SHOT7,000 0.70 SWMO-LT-70X-4 SWMO-LT-70X-SHOT

10,000 1.00 SWMO-LT-100X-4 SWMO-LT-100X-SHOT

15,000 1.50 SWMO-LT-150X-4 SWMO-LT-150X-SHOT20,000 2.00 SWMO-LT-200X-4 SWMO-LT-200X-SHOT30,000 3.00 SWMO-LT-300X-4 SWMO-LT-300X-SHOT40,000 4.00 SWMO-LT-400X-4 SWMO-LT-400X-SHOT50,000 5.00 SWMO-LT-500X-4 SWMO-LT-500X-SHOT60,000 6.00 SWMO-LT-600X-4 SWMO-LT-600X-SHOT

Set of above SWMO-LT-CAL-SET-4 Each AccuShot productCat. No.s 19 x 4 oz. $ 850 contains 5 x 20 mL

ampules at the statedconc. for $ 60

ASTM Methods Sulfur in #2 Diesel FuelSulfur in Ready-to-Use

Concentration #2 Diesel Fuel Sulfur AccuShots

g/g Wt. % Cat. No. Cat. No.Blank 0.000 SDF-BL-4 SDF-BL-SHOT

100 0.010 SDF-1X-4 SDF-1X-SHOT200 0.020 SDF-2X-4 SDF-2X-SHOT300 0.030 SDF-3X-4 SDF-3X-SHOT400 0.040 SDF-4X-4 SDF-4X-SHOT500 0.050 SDF-5X-4 SDF-5X-SHOT750 0.075 SDF-7.5X-4 SDF-7.5X-SHOT

1,000 0.10 SDF-10X-4 SDF-10X-SHOT1,500 0.15 SDF-15X-4 SDF-15X-SHOT2,000 0.20 ------------- -------------3,000 0.30 SDF-30X-4 SDF-30X-SHOT4,000 0.40 ------------- -------------5,000 0.50 SDF-50X-4 SDF-50X-SHOT7,000 0.70 SDF-70X-4 SDF-70X-SHOT

10,000 1.00 SDF-100X-4 SDF-100X-SHOT15,000 1.50 SDF-150X-4 SDF-150X-SHOT20,000 2.00 SDF-200X-4 SDF-200X-SHOT

30,000 3.00 SDF-300X-4 SDF-300X-SHOT40,000 4.00 SDF-400X-4 SDF-400X-SHOT50,000 5.00 SDF-500X-4 SDF-500X-SHOT60,000 6.00 SDF-600X-4 SDF-600X-SHOT

Set of above SDF-CAL-SET-4 Each AccuShot productCat. No.s 19 x 4 oz. $ 850 contains 5 x 20 mL


Cross Reference TableASTM IP ISO DIN JIS AFNOR sorted by

ASTM Method see beginning of Catalog

Sulfur Standards for ASTM D-2622, D-3120, D-3246, D-4294, D-5453, D-6334, D-6445 &Proposed ASTM Sulfur Methods


15/116

Method ASTM

For the mandatory reaworld QC samplesstipulated in the Methosee pages 1- 2.

Standards of Intere

Sulfur in Heavy Distillate Kerosene




ASTM Methods Sulfur in Kerosene

Sulfur concentration

calculated from % sulfin di-n-butyl sulfide.

Technical Note

Sulfur in Light Ready-to-UseConcentration Distillate Kerosene Sulfur AccuShots

g/g Wt. % Cat. No. Cat. No.Blank 0.000 SK-BL-4 SK-BL-SHOT

100 0.010 SK-1X-4 SK-1X-SHOT200 0.020 ---------------300 0.030 SK-3X-4 SK-3X-SHOT400 0.040 ---------------500 0.050 SK-5X-4 SK-5X-SHOT750 0.075 SK-7.5X-4 SK-7.5X-SHOT

1,000 0.10 SK-10X-4 SK-10X-SHOT1,500 0.15 ---------------2,000 0.20 SK-20X-4 SK-20X-SHOT3,000 0.30 SK-30X-4 SK-30X-SHOT4,000 0.40 SK-40X-4 SK-40X-SHOT5,000 0.50 SK-50X-4 SK-50X-SHOT7,000 0.70 ---------------

10,000 1.00 SK-100X-4 SK-100X-SHOT15,000 1.50 ---------------20,000 2.00 SK-200X-4 SK-200X-SHOT30,000 3.00 ---------------40,000 4.00 ---------------50,000 5.00 ---------------60,000 6.00 ---------------

Set of above SK-CAL-SET-4 Each AccuShot productCat. No.s 12 x 4 oz. $ 500 contains 5 x 20 mL


Sulfur in HeavyConcentration Distillate Kerosene

g/g Wt. % Cat. No.Blank 0.000 SK-HD-BL-4

100 0.010 SK-HD-1X-4200 0.020 SK-HD-2X-4300 0.030 SK-HD-3X-4400 0.040 SK-HD-4X-4500 0.050 SK-HD-5X-4750 0.075 SK-HD-7.5X-4

1,000 0.10 SK-HD-10X-41,500 0.15 SK-HD-15X-42,000 0.20 SK-HD-20X-43,000 0.30 SK-HD-30X-44,000 0.40 SK-HD-40X-45,000 0.50 SK-HD-50X-47,000 0.70 SK-HD-70X-4

10,000 1.00 SK-HD-100X-415,000 1.50 SK-HD-150X-420,000 2.00 SK-HD-200X-430,000 3.00 SK-HD-300X-440,000 4.00 SK-HD-400X-450,000 5.00 SK-HD-500X-460,000 6.00 SK-HD-600X-4

Set of above SK-HD-CAL-SET-4Cat. No.s 21 x 4 oz. $ 950



Sulfur in Light Distillate Kerosene

Sulfu



16/116

ASTM D-3120, D-3246 Sulfur Calibration Set

ASTM D-2622, D-4294 Sulfur Calibration Standards ASTM D-2622, D-6334, Low Level SulfurD-6445 Calibration Standards

ASTM D-2622, D-6334, Mid Level SulfurD-6445 Calibration Standards


ASTM

SULFUR

ASTM 2622-

6445


For the mandatory real world QC samples stipulated in manyASTM Sulfur Methods, see page 1-2


Cat. No. Sulfur Conc. Sulfur Wt. % UnitSTP-BL-4 Blank 0.0 4 oz.STP-1X-4 10 g/g 0.001 4 oz.STP-2X-4 20 g/g 0.002 4 oz.STP-3X-4 30 g/g 0.003 4 oz.STP-5X-4 50 g/g 0.005 4 oz.STP-10X-4 100 g/g 0.010 4 oz.STP-20X-4 200 g/g 0.020 4 oz.STP-30X-4 300 g/g 0.030 4 oz.STP-40X-4 400 g/g 0.040 4 oz.STP-60X-4 600 g/g 0.060 4 oz.STP-100X-4 1000 g/g 0.10 4 oz.STP-200X-4 2000 g/g 0.20 4 oz.STP-300X-4 3000 g/g 0.30 4 oz.

STP-CAL-SET $ 650 / set of 13 x 4 oz.In Isooctane Set contains the above 13 individual bottles

Standards can be mixed for quantity discounts

1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur Standard


1 to 4 units $ 60 each per Sulfur Standard

5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur Standard

Cat. No. Sulfur Conc. Sulfur Wt. % UnitD-2622-LL-200X-4 200 g/g 0.020 4 ozD-2622-LL-400X-4 400 g/g 0.040 4 ozD-2622-LL-600X-4 600 g/g 0.060 4 ozD-2622-LL-700X-4 700 g/g 0.070 4 ozD-2622-LL-800X-4 800 g/g 0.080 4 ozD-2622-LL-900X-4 900 g/g 0.090 4 ozD-2622-LL-1100X-4 1100 g/g 0.110 4 ozD-2622-LL-1200X-4 1200 g/g 0.120 4 oz

Well characterized Thiophene & 2-Methyl thiophene are usedin a low sulfur Isooctane/Toluene matrix for this calibration set.

Technical Note

Well characterized Thiophene & 2-Methyl thiophene are usedin a low sulfur Isooctane/Toluene matrix for this calibration set.

New Requested Additions for use on XRF Energy

Dispersive or Wavelength Instruments

Cat. No. Sulfur Conc. Sulfur Wt. % UnitD-2622-LL-BL-4 Blank 0.0 4 oz.D-2622-LL-5X-4 5 g/g 0.0005 4 oz.D-2622-LL-10X-4 10 g/g 0.0010 4 oz.D-2622-LL-30X-4 30 g/g 0.0030 4 oz.D-2622-LL-50X-4 50 g/g 0.0050 4 oz.D-2622-LL-75X-4 75 g/g 0.0075 4 oz.D-2622-LL-100X-4 100 g/g 0.010 4 oz.D-2622-LL-300X-4 300 g/g 0.030 4 oz.D-2622-LL-500X-4 500 g/g 0.050 4 oz.D-2622-LL-1000X-4 1000 g/g 0.100 4 oz.

D-2622-LL-CAL-SET $ 450 / 10 x 4 oz.

In Isooctane : Toluene (3:1)Set contains the above 10 individual bottles


1 to 4 units $ 60 each per Sulfur Standard5 to 10 units $ 55 each per Sulfur Standardmore than 10 units $ 50 each per Sulfur Standard

Cat. No. Sulfur Conc. Sulfur Wt. %D-3120-92-BL Blank D-3120-92-1X 1 g/g 0.0001D-3120-92-3X 3 g/g 0.0003D-3120-92-10X 10 g/g 0.0010D-3120-92-30X 30 g/g 0.0030D-3120-92-50X 50 g/g 0.0050D-3120-92-75X 75 g/g 0.0075D-3120-92-100X 100 g/g 0.010

Well characterized di-n-butyl sulfide is used in a low sulfurIsooctane matrix for this calibration set.

Technical Note

Technical Note


A well characterized di-n-butyl sulfide starting matl is used with alow sulfur Isooctane matrix for RFG/gasoline sulfur standards.

Technical Note

Sulfur Calibration SetD-3120-92-CAL-SET $ 75 / set of 8 x 1 mLIn Isooctane

Sulfur Calibration Standards in Isooctane forGasoline & Reformulated Gasoline Analysis Low Level Sulfur Calibration Standards for use on

XRF Energy Dispersive or Wavelength InstrumentsOriginallydesigned for

D-2622-98D-4294-98

Originally

designed forD-2622-98D-6334-98D-6445-99

Originallydesigned forD-3120-96D-3246-96

Originallydesigned forD-2622-98D-6334-98D-6445-99

Member

AccuStandard is an active member in ASTM and

strives to keep abreast of ASTM method revisions.

If our listed formulation does not meet the most

recent method revision, please contact Technical

Support, ext. 117 for an updated product.


17/116

ASTM Methods Sulfur Standards

ASTM D-2789 Hydrocarbon Types in Low Olefinic Gas by MS


ASTM-SSTD-A/B-SET $ 100 / 10 x 2 mLThe set contains the following 10 standards in isooctane

(Vol. %)cis-1,2-Dimethylcyclohexane 15.5Benzene 7.7Toluene 10p-Xylene 16.5

(Vol. %)2-Methylpentane 7.22,4-Dimethy lpentane 9.4n-Octane 16.6Methylcyclopentane 7.1Methylcyclohexane 10

AccuStandard's Technical

Service Dept. can provideReady-to-Inject working levcalibration standards to meeunique laboratory applicationCall or fax us your standardrequirements.

Technical NoteSulfur in Residual Oil Standards




Trace Quantities of Sulfur in LiquidAromatic Hydrocarbons by OxidativeMicrocoulometryASTM-P-0020-PAK $ 75 / 5 x 1 mL1000 g/mL in Xylenes

Sulfur (as Dibenzothiophene)

Total Sulfur in Aromatic Compoundsby Hydrogenolysis & RateometricColorimetryASTM-P-0010-PAK $ 75 / 5 x 1 mL1000 g/mL in Toluene

Sulfur (as Thiophene)

Composition Test MixD-2789-CTM $ 40 / 1 x 1 mL

D-2789-CTM-PAK SAVE 20% $ 160 / 5 x 1 mL9 comps.

ASTM Methods Sulfur Calibration Standards

ASTM

Sulfur in Crude Oil Standards

Both the actual volume %ratio and the final weightfractions for each analyte wbe listed on the certificate.

Technical Note

Concentration Sulfur in Crude Oil

g/g Wt. % Cat. No.1,000 0.10 SCO-10X-42,500 0.25 SCO-25X-45,000 0.50 SCO-50X-4

10,000 1.00 SCO-100X-420,000 2.00 SCO-200X-430,000 3.00 SCO-300X-440,000 4.00 SCO-400X-450,000 5.00 SCO-500X-4

Set of above SCO-CAL-SET-4Cat. No.s 8 x 4 oz. $ 500

Concentration Sulfur in Crude Oil

g/g Wt. % Cat. No.3,500 0.35 SRO-35X-47,000 0.70 SRO-70X-4

10,000 1.00 SRO-100X-415,000 1.50 SRO-150X-420,000 2.00 SRO-200X-430,000 3.00 SRO-300X-440,000 4.00 SRO-400X-4

Set of above SRO-CAL-SET-4Cat. No.s 7 x 4 oz. $ 450

Cat. No. Description Unit

ASTM-SSTDA-BL Sulfur Blank 2 mL

ASTM-SSTDA-01 Sulfur @ 0.5 g/g in Isooctane 2 mLASTM-SSTDA-02 Sulfur @ 1.0 g/g in Isooctane 2 mLASTM-SSTDA-03 Sulfur @ 2.5 g/g in Isooctane 2 mLASTM-SSTDA-04 Sulfur @ 5.0 g/g in Isooctane 2 mL

ASTM-SSTDB-BL Sulfur Blank 2 mLASTM-SSTDB-04 Sulfur @ 5.0 g/g in Isooctane 2 mLASTM-SSTDB-05 Sulfur @ 10.0 g/g in Isooctane 2 mLASTM-SSTDB-06 Sulfur @ 25.0 g/g in Isooctane 2 mLASTM-SSTDB-07 Sulfur @ 50.0 g/g in Isooctane 2 mL

Originallydesigned for

D-2789-95



18/116


PIANO

PIANO, PONA, PNA Analysis

PIONA

PIANO, PONA, PNA

High Aromatic PIAN BlendASTM-P-0037 $ 120 / 100 L

110 comps.High Aromatic blend contains the PIAN componentsblended to resemble a reformate. The actual certificatewill have the exact weight % for each analyte accurateto four decimal places. Analyte list is drawn fromCat. No.s: ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034

Low Aromatic PIAN BlendASTM-P-0036 $ 120 / 100 L

110 comps.Low Aromatic blend contains the PIAN componentsblended to resemble a light naphtha. The actual certificatewill have the exact weight % for each analyte accurate tofour decimal places. Analyte list is drawn fromCat. No.s: ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034

AccuStandard has introduced the PIANO line of quantitative and qualitative Petrochemical Standards for class type analysis of petrochemica

samples or product streams. PIANO analysis involves the determination of the percentage of the following five fractions Paraffins, Isoparaf

Aromatics, Naphthenes, and Olefins.

PONA analysis involves analyzing the naphtha sample for Paraffins, Olefins, Naphthenes, and Aromatics. If the Isoparaffins and Olefins are

present, the analysis is just for PNA.

The PIANO line of standards is used to determine quantitative and qualitative retention times and indices as well as to monitor response fact

within the hydrocarbon blend. These complex mixes are prepared from materials of the highest available purity, accurate to four decimal plaand include a detailed data sheet on the formulation composition. The typical range for the analytes in each formulation has been provided f

each catalog item. The exact composition on a weight % basis for each analyte has been provided on the certificate, and a disk deliverable

spreadsheet is available on request.

Mini Inert Valves SealThe PIANO standards are supplied in convenient to use crimp top vials with Viton septa that resist

mineral oil, aliphatic, aromatics hydrocarbons, and higher temperatures. Mini inert valve seals are

available for an additional $ 25 vial. To order, add -MIV to any of the PIANO catalog numbers on

this page.

For individual PIANO descriptions see next page


PIANO

PONA

PNA

AccuStandard, Your Standards and Technical Information Source!

Total PetroleumHydrocarbon PatternRecognition Standards

BOOK-TPH $ 35

Analytical Standards andReference Material for all209 PCB Congeners

S-3571 $ 25

PIANO MixtureASTM-P-0030 $ 250 / 100 L

135 comps.The PIANO formulation contains the n-Paraffins,Isoparaffins,Aromatics, Naphthenes, and Olefins from thefive Cat. No.s: ASTM-P-0031, ASTM-P-0032,

ASTM-P-0033, ASTM-P-0034, ASTM-P-0035

Approximate weight percentages for the total: n-Paraffins18.5%, Isoparaffins 17.9%, Aromatics 23.6%, Naphthenes20.9%, Olefins 19.0%.The actual certificate will list the weight % for all analytesin the formulation.


19/116

PIANO, PONA, PNA Analysis


PIAN

AccuStandard may add and/or subtractPIANO Analytes and vary the weight %for each Analyte. The certificate willreflect the exact Analyte composition.

Production Note

PIANO, PONA, PNA

Typ. Wt. %3-Methyl-1-butene 1.93961-Pentene 4.13552-Methyl-1-butene 1.44402-Methyl-1,3-butadiene 2.3889trans-2-Pentene 1.8034cis-2-Pentene 1.9792

4-Methylpentene-1 3.43721-Hexene 7.0484trans-2-Hexene 1.73022-Methylpentene-2 3.3901cis-2-Hexene 3.87651-Heptene 7.6134trans-3-Heptene 3.3469cis-3-Heptene 5.8657trans-2-Heptene 3.7217cis-2-Heptene 5.76791-Octene 7.6901trans-2-Octene 1.9432cis-2-Octene 3.95021-Nonene 7.6425trans-3-Nonene 1.9972cis-3-Nonene 4.0042trans-2-Nonene 1.9848cis-2-Nonene 2.7952

1-Decene 8.2053

Typ. Wt. %Cyclopentane 4.9143Methylcyclopentane 3.2829Cyclohexane 5.32681,1-Dimethylcyclopentane 3.4612cis-1,3-Dimethylcyclopentane 0.5963trans-1,2-Dimethylcyclopentane 1.4715trans-1,3-Dimethylcyclopentane 2.7531

Methylcyclohexane 5.6091Ethylcyclopentane 3.5534ctc-1,2,3-Trimethylcyclopentane 1.5859cct-1,2,4-Trimethylcyclopentane 3.7208ctc-1,2,4-Trimethylcyclopentane 1.6467trans-1,4-Dimethylcyclohexane 3.64991-Ethyl-1-methylcyclopentane 1.0554trans-1,2-Dimethylcyclohexane 1.6537ccc-1,2,3-Trimethylcyclopentane 0.7971Isopropylcyclopentane 3.5042cis-1,2-Dimethylcyclohexane 3.7159n-Propylcyclopentane 3.6438ccc-1,3,5-Trimethylcyclohexane 3.52631,1,4-Trimethylcyclohexane 3.6791ctt-1,2,4-Trimethylcyclohexane 3.6107ctc-1,2,4-Trimethylcyclohexane 3.50691,1,2-Trimethylcyclohexane 3.3354Isobutylcyclopentane 3.7123Isopropylcyclohexane 5.7233n-Butylcyclopentane 3.6944Isobutylcyclohexane 5.6729t-1-Methyl-2-propylcyclohexane 3.8434t-1-Methyl-2-(4MP)cyclopentane 3.7534

PIANO Olefins MixASTM-P-0035 $ 120 / 100 L25 Olefins listed below at varying Wt. %typically in the range from 1.2 to 9.0 Wt. %.The actual certificate will have the exact Wt. %for each analyte.

PIANO Naphthenes MixASTM-P-0034 $ 120 / 100 L30 Napthenes listed below at varying Wt. %typically in the range from 0.5 to 8.0 Wt. %. Theactual certificate will have the exact Wt. % foreach analyte.

Typ. Wt. %n-Pentane 9.4375n-Hexane 9.5661n-Heptanea 9.8048n-Octane 9.5518n-Nonane 9.0482n-Decane 9.2517n-Undecane 9.3172n-Dodecane 9.1855n-Tridecane 8.9332

n-Tetradecane 8.7989n-Pentadecane 7.1057

Typ. Wt. %Benzene 7.1437Toluene 4.5738EthylBenzene 6.7670m-Xylene 2.2259p-Xylene 4.4815o-Xylene 2.2519

Isopropylbenzene 2.2248n-Propylbenzene 4.49791-Methyl-3-ethylbenzene 2.22431-Methyl-4-ethylbenzene 2.22061,3,5-Trimethylbenzene 1.10761-Methyl-2-ethylbenzene 2.26111,2,4-Trimethylbenzene 2.2535tert-Butylbenzene 4.5310Isobutylbenzene 4.4216sec-Butylbenzene 2.23681-Methyl-3-isopropylbenzene 1.10661-Methyl-4-isopropylbenzene 1.06681-Methyl-2-isopropylbenzene 1.12411-Methyl-3-n-propylbenzene 2.11351-Methyl-4-n-propylbenzene 2.2336n-Butylbenzene 2.20871,2-Diethylbenzene 1.09471-Methyl-2-n-propylbenzene 2.2641

1,4-Dimethyl-2-ethylbenzene 2.28031,3-Dimethyl-5-ethylbenzene 2.28581,2-Dimethyl-4-ethylbenzene 2.25581,3-Dimethyl-2-ethylbenzene 1.14161,2-Dimethyl-3-ethylbenzene 2.18641,2,4,5-Tetramethylbenzene 0.23602-Methylbutylbenzene 1.1453trans-1-Butyl-2-methylbenzene 0.7641n-Pentylbenzene 4.4828t-1-Butyl,3,5-dimethylbenzene 2.1641t-1-butyl-ethylbenzene 2.23221,3,5-Triethylbenzene 4.56711,2,4-Triethylbenzene 1.1087n-Hexylbenzene 4.5029

Typ. Wt. %2,3-Dimethylheptane 1.48703,4-Dimethylheptane 3.74502-Methyloctane 3.75763-Methyloctane 5.60203,3-Diethylpentane 1.57552,2-Dimethyloctane 3.41353,3-Dimethyloctane 3.25822,3-Dimethyloctane 3.88423-Ethyloctane 3.74822-Methylnonane 3.7144

3-Methylnonane 5.7687

Typ. Wt. %2,2-Dimethylhexane 1.30612,5-Dimethyl hexane 3.69752,2,3-Trimethylpentane 1.73712,4-Dimethylhexane 1.62522,3-Dimethylhexane 1.62122-Methylheptane 4.40734-Methylheptane 3.20153-Methylheptane 5.51863-Ethylhexane 0.69993,3-Dimethylheptane 1.7011

2,5-Dimethylheptane 5.67313,5-Dimethylheptane 0.7565

Typ. Wt. %Isopentane 2.19282,3-Dimethylbutane 0.44662-Methylpentane 3.28153-Methylpentane 5.38652,2-Dimethylpentane 1.77472,4-Dimethylpentane 3.69932,2,3-Trimethylbutane 3.92913,3-Dimethylpentane 1.18482-Methylhexane 2.23842,3-Dimethylpentane 1.7883

3-Methylhexane 1.67083-Ethylpentane 0.5080

PIANO Aromatics MixASTM-P-0033 $ 120 / 100 L38 Aromatics listed below at varying Wt. %typically in the range from 0.2 to 7.0 Wt. %.The actual certificate will have the exactWt. % for each analyte.

PIANO n-Paraffins MixASTM-P-0031 $ 80 / 100 L11 paraffins listed below at varying Wt. %typically in the range from 7.0 to 11.0 Wt. %.The actual certificate will have the exact Wt.% for each analyte.

PIANO Mix SetASTM-PIANO-SET $ 700 / 6 x 100 LSet includes the following Cat. No.:ASTM-P-0030, ASTM-P-0031, ASTM-P-0032,ASTM-P-0033, ASTM-P-0034, ASTM-P-0035

Special PackagingMini inert valve seals are available for an additional $ 25 / vial.To order, add -MIV to any of the PIANO cat.# on this page.

PIANO Isoparaffins MixASTM-P-0032 $ 120 / 100 L35 Isoparaffins listed below at varying Wt. % typically in the range from 0.5 to 6.0 Wt. %. The actualcertificate will have the exact Wt. % for each analyte.

PIANO MixtureASTM-P-0030 $ 250 / 100 L (135 comps.)The PIANO formulation contains the n-Paraffins, Isoparaffins,Aromatics, Naphthenes, and Olefins from

the Five Cat. No.s: ASTM-P-0031, ASTM-P-0032, ASTM-P-0033, ASTM-P-0034, ASTM-P-0035

Approximate weight %s for the total: n-Paraffins 18.5%, Isoparaffins 17.9%, Aromatics 23.6%,Naphthenes 20.9%, Olefins 19.0%. The certificate lists the weight % for all analytes in the formulation.


20/116


Member

ASTM

ASTM D-2887 Boiling Range Distribution of Petroleum Fractions by GC

Detailed Hydrocarbon Analysis

AccuStandard offers a hydrocarbon window defining standard with the C8 to C40 odd and

even Alkanes. As an added benefit, AccuStandard included pristane and phytane in theformulation. Use of this one standard measuring the C17/ pristane and C18/ phytane ratio

can be used to estimate degradation of fuel oil.

If you prefer, AccuStandard has also developed a fuel oil degradation mixture containingjust the four required analytes to determine the C17/pristane and C8/ phytane ratio

Catalog Numbers DRH-005S-10X.

Technical Note

This sample is a petroleum fractionhaving a boiling range from 250F to850F, evaluated in round robinstudies by the ASTM D-02committee. Use of this sample andthe supplied ASTM boiling rangeconsensus values helps to evaluatesystem performance

Technical NoteTriacontanen-HentriacontaneDotriacontaneTritriacontaneTetratriacontanePentatriacontaneHexatriacontaneHeptatriacontaneOctatriacontaneNonatriacontane

Tetracontane

Wt. %n-Octadecane 5n-Eicosane 2n-Tetracosane 2n-Octacosane 1n-Dotriacontane 1n-Hexatriacontane 1n-Tetracontane 1n-Tetratetracontane 1

Wt. %n-Hexane 6n-Heptane 6n-Octane 8n-Nonane 8n-Decane 12n-Undecane 12n-Dodecane 12n-Tetradecane 12n-Hexadecane 10

Column Test MixtureASTM-D2887 $ 10 / 1 x 1 mL1% v/v in n-Octane 2 comps.

n-Hexadecane n-Octadecane

HeptadecaneOctadecanePhytane (2,6,10,14-Tetramethylhexadecane)Pristane (2,6,10,14-Tetramethylpentadecane)

NonadecanePhytaneEicosaneHeneicosaneDocosaneTricosaneTetracosanePentacosaneHexacosaneHeptacosane

OctacosaneNonacosane

OctaneNonaneDecaneUndecaneDodecaneTridecaneTetradecanePentadecaneHexadecaneHeptadecane

OctadecanePristane

Detailed Hydrocarbon Analysis

Fuel Oil Degradation/RetentionTime Mix for Quantification ofC17/Pristane & C18/Phytane ratiosDRH-005S-10X $ 20 / 1 x 1 mL

2.0 mg/mL each in CH2Cl2 : CS2 (1:1) 4 comps.

Calibration MixDRH-002N $ 10 / 100 mgDRH-002N-10X $ 40 / 1 gm

17 comps.

Complete Hydrocarbon Analysis

Hydrocarbon WindowDefining Standard*DRH-008S-R2 $ 65 / 1 x 1 mLDRH-008S-R2-PAK SAVE 20% $ 260 / 5 x 1 mL500 g/mL each in Chloroform 35 comps.

Method 2887

DHA

Proposed ASTM Method for Detailed Hydrocarbon Analysis (DHA)Determination of Individual Components and Groups of Components in Spark Ignition Engine fuels byHigh Efficiency Open Tubular Column Gas Chromatography (Detailed Hydrocarbon Analysis)

Detailed Hydrocarbon Analysis (includes oxygenates)

ASTM-P-0038 $ 120 / 100 L30 Analytes listed below at varying targeted weight %. The actual certificate will has the exact Wt. % for each analyte.

p-XyleneEthylbenzeneOctane2,3-DimethylheptaneNonane5-Methylnonane1-Ethyl-2-methylbenzene

BenzeneCyclohexane3-Ethylpentanet-1,2-DimethylcyclopentaneHeptane2,2,3-Trimethylpentane2,3,3-TrimethylpentaneToluene

EthanolPentane2-Methyl-2-propanol2-Methylbutene2,3-DimethylbutaneMethyl-t-butyl etherHexaneMethylcyclopentene

DecaneUndecane1,2,3,5-TetramethylbenzeneNaphthaleneDodecane1-MethylnaphthaleneTridecane

DHA - PONA-VI (PONA 6) is aqualitative mixture of variousgasoline and refinery materialsprepared to provide nearly everycomponent that may be encounte

in feedstock and finished gasolineSome oxygenates have been addto allow this blend to be used forDHA method setup. This blendcontains approximately 450components (peaks).

ASTM-P-0139 $ 120 / 100 L

Calibration Solution *

DRH-002S-R1 $ 50 / 1 x 1 mLDRH-002S-R1-PAK SAVE 20% $ 200 / 5 x 1 mLAt stated conc. in Chloroform 17 comps.

Calibration Solution *

DRH-002S-R2 $ 50 / 1 x 1 gmDRH-002S-R2-PAK SAVE 20% $ 200 / 5 x 1 gm1 % Wt./Wt. each in Chloroform 20 comps.

NEW

g/mLn-Hexane 600n-Heptane 600n-Octane 800n-Nonane 800n-Decane 1200n-Undecane 1200n-Dodecane 1200n-Tetradecane 1200n-Hexadecane 1000

g/mLn-Octadecane 500n-Eicosane 200n-Tetracosane 200n-Octacosane 100n-Dotriacontane 100n-Hexatriacontane 100n-Tetracontane 100n-Tetratetracontane 100

n-Tetratetracontanen-Tetracontanen-Hexatriacontanen-Dotriacontanen-Octacosanen-Tetracosanen-Eicosane

n-Octadecanen-Hexadecanen-Tetradecanen-Dodecanen-Undecanen-Decane

NEW

n-Nonanen-Octanen-Heptanen-Hexanen-Pentanen-Pentadecanen-Heptadecane

* Can be shipped by Air and Sea

ASTM D-2887 Reference GasOil Sample Lot #2D-2887-REFOIL $ 35 / 1 x 1

Originally designed for D-2887-99


21/116

SIM DIS Standards Simulated Distillation


Memb

Meth

See ASTM Methods D-3710D-5307, D-5442, D-6352 foadditional calibrationstandards for hydrocarbonanalysis.


AccuStandard designed thefollowing formulations for aProposed ASTM Method undevelopment for Motor OilVolatility analysis & SIM DISapplications.

Technical Note

Polywax 1000

ASTM-P-0138N-2G $ 20 / 2 grams

Polywax 1000

Polywax 850


Polywax 850

Simulated Distillation (SIM DIS) and Proposed Motor Oil Volatility MethodAccuStandard has developed an extensive line of SIM DIS standards for normal and high temperature analytical requirements when generati

boiling point versus retention time calibration curves. Since normal paraffins above Alkane C60 are not readily available, Polywax 500, Poly

655, Polywax 850 and Polywax 1000 standards have been incorporated to perform SIM DIS analysis of heavy petroleum fractions with boili

points up to 1350 F. If you require additional analytes added to the formulations for extended SIM DIS work, use our custom quotation req

form located in the back of the catalog.

Wt. %n-Tetradecane 0.0333n-Pentadecane 0.0333n-Hexadecane 0.0333n-Heptadecane 0.0333n-Octadecane 0.0333n-Eicosane 0.0333Polywax 500 0.5

Wt. %n-Pentane 0.0333n-Hexane 0.0333n-Heptane 0.0333n-Octane 0.0333n-Nonane 0.0333n-Decane 0.0333n-Undecane 0.0333n-Dodecane 0.0666

Polywax 655


Polywax 655

Polywax 500


Polywax 500

Working Level SIM DIS Paraffin Solutionwith Polywax 500ASTM-P-0052 $ 40 / 1 x 1 mLASTM-P-0052-PAK SAVE 20% $ 160 / 5 x 1 mLAt stated conc. in Carbon disulfide 15 comps.

Petrochemical Standards

Wt. %n-Dodecane 13.33n-Tetradecane 6.66n-Pentadecane 6.66n-Hexadecane 6.66n-Heptadecane 6.66n-Octadecane 6.66n-Eicosane 6.66

Wt. %n-Pentane 6.66n-Hexane 6.66n-Heptane 6.66n-Octane 6.66n-Nonane 6.66n-Decane 6.66n-Undecane 6.66

Stock SIM DIS Paraffin SolutionASTM-P-0050 $ 85 / 1 x 5 mL

14 comps.

For our complete line ofOrganic Standards,request a copy of ourOrganic Catalog

For our complete line ofInorganic Standards,request a copy of ourInorganics Catalog


22/116

ASTM D-3230 Salts in Crude Oil

ASTM D-3237 Lead in Gasoline by AA Spectroscopy

ASTM D-3231 Phosphorus in Gasoline

ASTM D-3120 & D-3246 Trace Quantities of Sulfur in Light Liquid Petroleum Hydrocarbons by Oxidative Microcoulom


Method

,ASTM Standards

Sodium chloride 70 g/mLCalcium chloride 10 g/mLMagnesium chloride 20 g/mL

See page 1 for AccuStandacomprehensive line of Certif

Sulfur calibration standardsAccuPetroCheck, andAccuPetroTest quality controproducts.

Standards of Interests

Well characterized di-n-butyl sulfide is usedin a low sulfur Isooctane matrix for thiscalibration set.

Technical NoteCat. No. Sulfur Conc. Sulfur Wt.%

D-3120-BL Blank BlankD-3120-92-1X 1 g/g 0.0001D-3120-92-3X 3 g/g 0.0003D-3120-92-10X 10 g/g 0.0010D-3120-92-30X 30 g/g 0.0030D-3120-92-50X 50 g/g 0.0050D-3120-92-75X 75 g/g 0.0075D-3120-92-100X 100 g/g 0.010

Method 3120

3230

3231

3237

D-3231

Meets

EPAGuidelines

forRFG

Analysis

D-3237

Meets

EPAGuidelines

forRFG

Analysis

Element Quantity Cat. No. PriceMatrix Conc.

Phosphorus 100 mL ICP-41W-1 $ 34H2O 1000 g/mL

Phosphorus 500 mL ICP-41W-5 $ 67H2O 1000 g/mL

Mixed Salt SolutionD-3230-89-1 $ 75 / 100 mLD-3230-89-5 $ 150 / 500 mLAt stated conc. in Alcohol Solution (1-butanol : MeOH) (ratio 63:37) tr. H2O 3 comps.

Sulfur Calibration SetD-3120-92-CAL-SET $ 75 / set of 8 x 1 mLIn Isooctane

Lead Standard Calibration CurveD-3237-CAL-SET $ 210 / 4 x 100 mLSet includes the following Catalog Numbers:

Cat. No. Description Price / UnitD-3237-01 Blank 1% Aliquot 336/MIBK $ 20 /100 mLD-3237-02 0.02 g Pb / gal ( 5 .3 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 /100 mLD-3237-03 0.05 g Pb / gal ( 13.2 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mLD-3237-04 0.10 g Pb / gal ( 26.4 mg Pb/ L) in 1% Aliquat 336 / MIBK $ 80 / 100 mL

Working Level Standards &

Continuing Calibration Check (CCC)

Ready-to-Inject Petrochemical Standards and Calibration Curves

Reduce Costs

Increase Time Spent for Sample Analysis

Are Validated Against Independent Lots

Include Internal Standards or Surrogates

Follow ASTM Method Guidelines

Allow Direct Transfer to Autosampler Vials

Ready-to-Inject

Member

ASTM

Originally designed forD-3120-96D-3246-96


Originally designed for D-3231-99



23/116

ASTM D-3605 Trace Metals in Gas Turbine Fuels by AA &(Reapproved 1995) Flame Emission Spectroscopy

ASTM D-3524 (Reapproved 1999) Diesel Fuel Diluent in Used Diesel Engine Oils by GC


Technical Note

ASTM Standards

Column Resolution MixD-3524-CR $ 10 / 1 x 1 mLD-3524-CR-PAK SAVE 20% $ 40 / 5 x 1 mLAt stated conc. in n-Heptane 2 comps.

Wt. / Wt. %n-Hexadecane 1.0n-Octadecane 1.0

Internal Standard SolutionD-3524-IS-10ML $ 25 / 1 x 10 mL

D-3524-IS-10ML-PAK SAVE 20% $ 100 / 5 x 10 mLAt stated conc. in n-Heptane 2 comps.

Wt. / Wt. %n-Decane 1.0n-Octadecane 0.2

Meth

ASTM D-3246 Sulfur in Petroleum Gas by Oxidative Microcoulometry

ASTM D-3340 Lithium & Na in Lubricating Greases by Flame Photometer

* For your convenience these elements arealso available in HNO3. To order HNO3change the H to N at the end of the Cat. No.

Test to

Low ppb

Sulfur

Mid Level Daily QC SolutionD-3524-QC-10ML $ 30 / 1 x 10 mL

2 comps.Wt. / Wt. %

# 2 Diesel 5.030 W Motor oil 95

See pages 6 - 11 for AccuStandards comprehensive line of certified sulfur calibration standards

AccuStandard AccuTrace brand AA standards are produced under our rigorous ISO 9001 quality system toexacting specifications. Each standard is prepared from high purity starting materials; deionized water andhigh purity acids. Every standard is instrumentally assayed to verify 1000 ppm concentration of specifiedelement; Actual Lot Analysis is provided on the label and a Certificate of Analysis is included for ease ofrecord keeping and availability at audits.

D-3524 Calibration CurveD-3524-CAL-SET-5ML $ 150 / set of 6 x 5 mLD-3524-CAL-SET-10ML $ 250 / set of 6 x 10 mL

Analyte Standard 1 Standard 2 Standard 3 Standard 4 Standard 5 Standard 6Target Wt. % Target Wt. % Target Wt. % Target Wt. % Target Wt. % Target Wt. %

# 2 Diesel 10 7.5 5 2.5 1 030 W Motor oil 90 92.5 95 97.5 99 100

Element Unit Cat. No. Price

Matrix 1,000 g/mL

Lithium * 100 mL AA30H-1 $ 12HCl 500 mL AA30H-5 30

Sodium * 100 mL AA54H-1 13HCl 500 mL AA54H-5 33

Ca (Calcium) (250 g/mL)V (Vanadium) (250 g/mL)

Na (Sodium) (250 g/mL)Pb (Lead) (250 g/mL)

See Table of Contents for thWear Metals Group pages

Standards of InterestsD-3605-91 Trace Metals StandardD-3605-91-1 $ 165 / 1 x 100 mLAt stated conc. in 1,2,3,4-Tetrahydronaphthalene 4 comps.

Memb

See Pages 6-11





24/116


ASTM

D-3606

Meets

EPAGuidelines

forRFG

Analysis

ASTM Standards

ASTM D-3606 Benzene & Toluene in Finished Motor & Aviation Gasoline by GC

Aromatics Quantitative Calibration Standard (with Internal Standard: MEK)D-3606/IS-SET $ 115 / set of 7 x 1 mLD-3606/IS-SET-2ML $ 190 / set of 7 x 2 mLD-3606/IS-SET-2ML-PAK $ 760 / 5 x (7 x 2) mL

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7Calibr. range Target Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %

Benzene 0.06 - 5.0 4.8 2.4 1.2 0.6432 0.3168 0.1152 0.0576Toluene 0.5 - 20 19.2 14.4 9.6 4.8000 2.4000 0.9600 0.4800Isooctane 72.0 79.2 85.2 90.5568 93.2832 94.9248 95.4624Methyl ethyl ketone (Internal Std.) 4.0 4.0 4.0 4.0 4.0 4.0 4.0

Due to changes in the poss

use of other oxygenates likeethanol added to gasoline,AccuStandard formulated anew calibration curve usingsec-butanol as an InternalStandard. The use of this nISTD minimizes coelutioncaused by the oxygenate(sand pre column - standardcolumn configuration in the system.

Technical Note

Daily Quality Control Standard(without Internal Standard)D-3606-QC-25ML $ 125 / 1 x 25 mLD-3606-QC-25ML-PAK $ 600 / 5 x 25 mLEach at stated quantities 3 comps.

Compound Target Vol. %Benzene 0.67Toluene 5.00Isooctane 94.33

100

Gasoline Refinery Quality Control Standards

Daily Quality Control Standard(with Internal Standard: sec Butanol)D-3606-QC-IS2-25ML $ 125 / 1 x 25 mLD-3606-QC-IS2-25ML-PAK $ 600 / 5 x 25 mLEach at stated quantities 4 comps.

Compound Target Vol. %Benzene 0.6432Toluene 4.8000Isooctane 90.5568sec-Butanol (ISTD) 4.0

100

Aromatics Quantitative Calibration Standard (w/ Internal Standard: sec Butanol)D-3606/IS2-SET $ 115 / set of 7 x 1 mL

D-3606/IS2-SET-PAK $ 500 / 5 x (7 x 1) mL


Benzene 0.06 - 5.0 4.8 2.4 1.2 0.6432 0.3168 0.1152 0.0576Toluene 0.5 - 20 19.2 14.4 9.6 4.8000 2.4000 0.9600 0.4800Isooctane 72.0 79.2 85.2 90.5568 93.2832 94.9248 95.4624sec Butanol (Internal Standard) 4.0 4.0 4.0 4.0 4.0 4.0 4.0

Daily Quality Control Standard(with Internal Standard: MEK)D-3606-QC/IS-10ML $ 75 / 1 x 10 mLD-3606-QC/IS-10ML-PAK $ 300 / 5 x 10 mLEach at stated quantities 4 comps.

Compound Target Vol. %Benzene 0.6432Toluene 4.8000Isooctane 90.5568Methyl ethyl ketone (ISTD) 4.0

100

Daily Quality Control Standard(without Internal Standard)D-3606-QC-25ML $ 125 / 1 x 25 mLD-3606-QC-25ML-PAK $ 600 / 5 x 25 mLEach at stated quantities 3 comps.

Compound Target Vol. %Benzene 0.67Toluene 5.00Isooctane 94.33

100

Gasoline Refinery Quality Control Standards

Aromatics Quantitative Calibration Standard (without Internal Standards)D-3606-SET-25ML $ 800 / set of 7 x 25 mL


Benzene 0.06 - 5.0 5.00 2.50 1.25 0.67 0.33 0.12 0.06

Toluene 0.5 - 20 20.00 15.00 10.00 5.00 2.50 1.00 0.50Isooctane 75.00 82.50 88.75 94.33 97.17 98.88 99.44

ASTM D-3610 Total Cobalt in Alumina-Base Cobalt-Molybdenum Catalyst by Potentiometric Titration

Cobalt Oxide StandardD-3610-93-1 $ 50 / 1 x 100 mL

Cobalt oxide @ 1500 g/mL in Water

Method 3606

3610

,

Member


Originally designed forD-3610-88 (Re-Approved 1993)


25/116


Test to

Low ppb

SulfurSee Pages 6-11



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specific standard you need, we can prepare Custom Formulationsand Custom Packaging for both Organic and Inorganic needs.

See our Website for more info.


26/116

ASTM D-3831 Manganese in Gasoline by AA Spectroscopy

ASTM D-3710 (Reapproved 1999) Boiling Range Distribution of Gasoline & Gasoline Fractions by GC


Method 3710

3798

, 3831

See page 3 for AccuStandanew D-86 QA/QC Standards


ASTM Standards

Technical Note

Bulk Packaged p-Xylenewithout Internal StandardOther suggested internalstandards can be used inconjunction with the bulkpackaged D-3789 1 x 10 mLampule to meet your compaapplication. If you prefer toeliminate making standards,contact AccuStandardsTechnical Department with yunique formulation for a cusquotation. The customquotation request form islocated in the back of this

catalog.

Manganese Stock SolutionD-3831 $ 65 / 1 x 100 mL

Manganese @ 1.0 g Mn / gal (264.2 mg Mn / L) in Methyl isobutyl ketone

n-Octane 5.8n-Pentadecane 2.3n-Pentane 8.1n-Propylbenzene 4.7n-Tetradecane 2.3Toluene 11.6n-Tridecane 2.3p-Xylene 14.0

Vol./Vol. %n-Butylbenzene 3.5n-Decane 3.52,4-Dimethylpentane 5.8n-Dodecane 3.5n-Heptane 10.5n-Hexane 5.82-Methylbutane 10.52-Methylpentane 5.8

Vol./Vol. %

Approx.Wt./ Wt. %

n-Octane 5.4n-Pentadecane 2.2n-Pentane 7.6n-Propane 1.5n-Propylbenzene 4.3n-Tetradecane 2.2Toluene 10.8n-Tridecane 2.2p-Xylene 13

Approx.Wt./ Wt. %

n-Butane 4.5n-Butylbenzene 3.2n-Decane 3.22,4-Dimethylpentane 5.4n-Dodecane 3.2n-Heptane 9.7n-Hexane 5.42-Methylbutane 9.72-Methylpentane 5.42-Methylpropane 1.5

Quantitative Calibration StandardASTM-D3710 $ 25 / 1 x 1 mLASTM-D3710-PAK SAVE 36% $ 80 / 5 x 1 mL

16 comps.

Qualitative Calibration StandardD-3710-QUAL $ 30 / 1 x 1 mLD-3710-QUAL-PAK SAVE 20% $ 120 / 5 x 1 mL

19 comps.

ASTM D-3798 Analysis of p-Xylene by GC

This SIM DIS (Simulated Distillation or GCD) Method is used to determine the boiling range distribution ofgasoline and gasoline components. ASTM Method D-3710 is used for petroleum products and fractionswith a final boiling point of 500F (260C) or lower. By having an insight into the composition of thegasoline blend, essential data for the calculation of vapor pressure and a prediction of the D-86 distillationcurve can be made.

p-Xylene Impurity Standardwithout ISTDD-3798-10ML $ 65 / 1 x 10 mLD-3798-10ML-PAK SAVE 20% $ 260 / 5 x 10 mLAt stated conc. by weight 10 comps.

p-Xylene Impurity Standardwith ISTDD-3798-IS $ 30 / 1 x 1 mLD-3798-IS-PAK SAVE 33% $ 100 / 5 x 1 mL

At stated conc. by weight 11 comps.

AccuStandards R & D team has developed a special highly purified p-Xylene designed for ASTM MethodD-3798 specifications. The incorporation of this p-Xylene into the formulation allows the analytical chemistto qualitatively and quantitatively measure the impurities in the p-Xylene feedstock streams.

Wt./Wt. %n-Pentane 0.15n-Octane 0.15Benzene 0.15Toluene 0.15Ethylbenzene 0.15

p-Xylene 98.65m-Xylene 0.15

Wt./Wt. %o-Xylene 0.15Cumene 0.15Propylbenzene 0.15

Total Analytes 100plus n-Undecane* (ISTD) 0.500grams

Wt./Wt. %n-Pentane 0.15n-Octane 0.15Benzene 0.15Toluene 0.15Ethylbenzene 0.15

Wt./Wt. %p-Xylene 98.65m-Xylene 0.15o-Xylene 0.15Cumene 0.15Propylbenzene 0.15

ASTM D-2887-99 Boiling Range Distribution of Petroleum Fractions by GCCalibration Solution *DRH-002S-R1 $ 50 / 1 x 1 mLDRH-002S-R1-PAK SAVE 20% $ 200 / 5 x 1 mLAt stated conc. in Chloroform 17 comps.

g/mLn-Hexane 600n-Heptane 600n-Octane 800n-Nonane 800n-Decane 1200

g/mLn-Undecane 1200n-Dodecane 1200n-Tetradecane 1200n-Hexadecane 1000

NEW

g/mLn-Octadecane 500n-Eicosane 200n-Tetracosane 200n-Octacosane 100

g/mLn-Dotriacontane 100n-Hexatriacontane 100n-Tetracontane 100n-Tetratetracontane100

* Can be shipped by Air and Sea

ASTM

Member




27/116

ASTM D-4291 (Reapproved 1998) Trace Ethylene Glycol in Used Engine Oil

ASTM D-4059 Polychlorinated Biphenyls in Insulating Liquids by GC


Memb

Meth

Additional Aroclors an

PCB Congener Standaavailable in our OrganCatalog

Ethylene Glycol Stock StandardD-4291-93 $ 20 / 1 x 1 mLD-4291-93-PAK SAVE 20% $ 80 / 5 x 1 mL

Ethylene glycol @ 2000 g/mL in water

PAK Cat. No.

Aroclor 1016 C-216N $ 25 / 100 mg 100 mg

Aroclor 1221 C-221N 25 / 100 mg 100 mg

Aroclor 1232 C-232N 25 / 10 mg 10 mg

Aroclor 1242 C-242N 25 / 100 mg 100 mg

Aroclor 1248 C-248N 25 / 10 mg 10 mg

Aroclor 1254 C-254N 25 / 100 mg 100 mg

Aroclor 1260 C-260N 25 / 100 mg 10 mg

Aroclor 1262 C-262N 25 / 100 mg 10 mg

Aroclor 1268 C-268N 25 / 10 mg 10 mgKit of above 9 Aroclors Z-008 $ 125 / 9 vials

Z-008

Aroclor # Cat. No. Price / Unit (Kit)

Neat Individual Aroclors

5 x 1 mLPrice

Aroclor 1016 50 C-216-ST-1 $ 25 C-216-ST-1-PAK $ 90

Aroclor 1016 500 C-216-ST-2 30 C-216-ST-2-PAK 120Aroclor 1221 50 C-221-ST-1 25 C-221-ST-1-PAK 90Aroclor 1221 500 C-221-ST-2 30 C-221-ST-2-PAK 120

Aroclor 1232 50 C-232-ST-1 25 C-232-ST-1-PAK 90Aroclor 1232 500 C-232-ST-2 30 C-232-ST-2-PAK 120






Aroclor 1268 50 C-268-ST-1 25 C-268-ST-1-PAK 90

Aroclor 1268 500 C-268-ST-2 30 C-268-ST-2-PAK 120

Cat. No.

1 x 1 mLPrice

Conc.(ppm w/w)

Aroclor #

ASTM Standards

ASTM D-4294 Sulfur in Petroleum Products by ED-XRF Spectroscopy

ASTM D-4377 Water in Crude oils by Potentiometric Karl Fischer Titration

D-4294Meets

EPAGuidelines

forRFG

Analysis

Aroclor-free transformer oil

also available as:

T-W130 $ 5 / 1 x 1 mL

See page 8-11 for AccuStandards comprehensive line of Certified Sulfur Calibration Standardsdesigned for matrix specific applications as described in Method D-4294 in section 9.0(Calibration & Standardization).

See page 5 for AccuStandards comprehensive line of Certified Karl Fischer Water Standards.

Aroclors in PCB-Free Transformer Oil (At 2 concentrations in Transcrest W130)




28/116

ASTM D-4628 Barium, Calcium, Magnesium & Zinc in Unused Lubricating Oil

ASTM D-4420 Aromatics in Finished Gasolines by GC


Method 4420

4628

,

Ready-to-Inject Petrochemical Standardsand Calibration Curves

Reduce Costs

Increase Time Spent for Sample AnalysisAre Validated Against Independent Lots

Include Internal Standards or Surrogates

Follow ASTM Method Guidelines

Allow Direct Transfer to Autosampler Vials

See Table of Contents for thWear Metals Group pages.


Vol. %n-Butylbenzene(C9 + aromatics) 15.00

Isooctane 57.00

Vol. %Benzene 3.00Toluene 10.00Total Xylenes (C8 aromatics) 15.00

Aromatics in Gasoline by GC/TCD-4420-CAL-SET $ 105 / set of 7 x 1 mL

Analyte Std. 1 Std. 2 Std. 3 Std. 4 Std. 5 Std. 6 Std. 7Target Target Target Target Target Target Target

Vol. % Vol. % Vol. % Vol. % Vol. % Vol. % Vol. %Benzene 0.05 0.10 0.25 0.75 1.25 2.50 5.00Toluene 0.5 1.00 2.50 5.00 10.00 15.00 25.00Total Xylenes (C8 aromatics) 5 10.00 15.00 20.00 25.00 1.00 3.00

n-Butylbenzene (C9 + aromatics) 30.00 25.00 20.00 10.00 5.00 15.00 2.50

Isooctane 64.45 63.90 62.25 64.25 58.75 66.50 64.50

Aromatics in Gasoline by GC/TXD-4420-94 $ 20 / 1 x 1 mLD-4420-94-PAK $ 80 / 5 x 1 mL

5 comps.

ASTM Standards



Lubricating Oil, Elements (Nominal Value) Wt.% listed belowASTM-P-0113-SET $ 2850 / 17 x 100 mL

Ba Ca Mg P S ZnCat. No. (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%) (Wt.%)

ASTM-P-0113-01 0.025 0.600 0.100 0.005 0.175 0.060ASTM-P-0113-02 0.000 0.500 0.150 0.200 0.050 0.080ASTM-P-0113-03 0.100 0.400 0.350 0.150 0.300 0.180ASTM-P-0113-04 0.175 0.260 0.225 0.250 0.150 0.120ASTM-P-0113-05 0.150 0.005 0.450 0.005 0.450 0.070ASTM-P-0113-06 0.000 0.400 0.500 0.025 0.350 0.100ASTM-P-0113-07 0.100 0.300 0.325 0.060 0.250 0.120ASTM-P-0113-08 0.200 0.200 0.250 0.100 0.450 0.100ASTM-P-0113-09 0.050 0.060 0.100 0.080 0.300 0.130ASTM-P-0113-10 0.075 0.060 0.400 0.050 0.200 0.050ASTM-P-0113-11 0.010 0.050 0.300 0.120 0.100 0.075ASTM-P-0113-12 0.000 0.025 0.200 0.150 0.200 0.130ASTM-P-0113-13 0.175 0.005 0.375 0.200 0.400 0.150ASTM-P-0113-14 0.005 0.170 0.175 0.250 0.550 0.110ASTM-P-0113-15 0.000 0.100 0.425 0.100 0.200 0.200ASTM-P-0113-16 0.005 0.010 0.275 0.010 0.600 0.250ASTM-P-0113-17 0.000 0.000 0.000 0.000 0.000 0.000

ASTM

Member



WEARMETALS


29/116

ASTM D-4629 Trace Nitrogen in Liquid Petroleum Hydrocarbons by Syringe/Inlet OxidativeCombustion and Chemiluminescence Detection. IP Designation 379/88


Memb

Meth

Nitrogen introduced using Pyridine

Technical Note

Nitrogen Calibration Set-High Boiling SolventsD-4629-91-HB-CAL-SET $ 75 / set of 7 x 1 mL

Set includes the following Cat. No.s

Cat. No. Description Price / Unit

D-4629-91-HB-0.3X Nitrogen @ 0.3 g/mL in Toluene $ 20 /1 x 1 mLD-4629-91-HB-1X Nitrogen @ 1 g/mL in Toluene $ 20 /1 x 1 mLD-4629-91-HB-10X Nitrogen @ 10 g/mL in Toluene $ 20 /1 x 1 mLD-4629-91-HB-25X Nitrogen @ 25 g/mL in Toluene $ 20 /1 x 1 mLD-4629-91-HB-50X Nitrogen @ 50 g/mL in Toluene $ 20 /1 x 1 mLD-4629-91-HB-75X Nitrogen @ 75 g/mL in Toluene $ 20 / 1 x 1 mLD-4629-91-HB-100X Nitrogen @ 100 g/mL in Toluene $ 20 /1 x 1 mL

Nitrogen introduced using Carbazole

Technical Note

Nitrogen introduced using Aniline

Technical Note

The Nitrogen is introduced using Aniline and theSulfur is introduced using di-n-Butyl sulfide

Technical NoteLow level Nitrogen &Sulfur Calibration SetASTM-P-0071-SET $ 50 / 4 x 1 mL



ASTM-P-0071-BL Benzene Blank 1 x 1 mLASTM-P-0071-01 Nitrogen @ 0.25 g/g & Sulfur @ 0.25 g/g in Benzene 1 x 1 mLASTM-P-0071-02 Nitrogen @ 0.50 g/g & Sulfur @ 0.50 g/g in Benzene 1 x 1 mLASTM-P-0071-03 Nitrogen @ 1.00 g/g & Sulfur @ 1.00 g/g in Benzene 1 x 1 mL

Low level Nitrogen Calibration SetASTM-P-0070-SET $ 75 / 6 x 1 mL



ASTM-P-0070-BL Isooctane Blank 1 x 1 mLASTM-P-0070-1X Nitrogen @ 0.5 g/g in Isooctane 1 x 1 mL

ASTM-P-0070-2X Nitrogen @ 1.0 g/g in Isooctane

petroleum standards

Documents

nitrogen standards

luftlust standards

tph standards

haz fee icp aa standards

vapor pressure standards

multidimensional gcd

organic inorganic standards

sulfur compounds