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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 1 Business Rule Check Note: sample code and result code can be supplied on request Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 1 Business Rule Check Note: sample code and result code can be supplied on request ErrorType ErrorCode ErrorDescription Variable VariableValue NumberRecordFailing W WR30A Please check result evaluation, the MRL changed in 2011 resEvaluation$resVal$EU MRL J003A$0.016$0.02 1 W WR30A Please check result evaluation, the MRL changed in 2011 resEvaluation$resVal$EU MRL J003A$0.018$0.02 1

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Page 1: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 1Business Rule Check

Note: sample code and result code can be supplied on request

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 1Business Rule Check

Note: sample code and result code can be supplied on request

ErrorType ErrorCode ErrorDescription Variable VariableValue NumberRecordFailing

W WR30A Please check result evaluation, the MRL changed in 2011 resEvaluation$resVal$EU MRL J003A$0.016$0.02 1

W WR30A Please check result evaluation, the MRL changed in 2011 resEvaluation$resVal$EU MRL J003A$0.018$0.02 1

Page 2: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Totals for Cereals, Sum (fruit, vegetables, other plant origin) and Animal products are for unprocessed commodities

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 2Table A0: Summary of samples taken in 2011 by product class

Totals for Cereals, Sum (fruit, vegetables, other plant origin) and Animal products are for unprocessed commodities

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 2Table A0: Summary of samples taken in 2011 by product class

Samples TotalWithout

Residues %

Withresidues

belowMRL %

ExceedingMRL %

NonCompliant %

Animal products 42 42 100% 0 0.0% 0 0.0% 0 0.0%

Baby food 21 19 90% 0 0.0% 2 9.5% 2 9.5%

Cereals 16 10 63% 6 38% 0 0.0% 0 0.0%

Processed products 37 36 97% 1 2.7% 0 0.0% 0 0.0%

Sum of fruits and nuts, vegetables, other plant products 4400 4056 92% 238 5.4% 106 2.4% 106 2.4%

4516 4163 92% 245 5.4% 108 2.4% 108 2.4%

Page 3: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

EEA = EU Member States, and Iceland and Norway - TC = Other Countries not part of EEA - UNK = Unknown

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 3Table A0: Summary of samples taken in 2011 by region of origin

EEA = EU Member States, and Iceland and Norway - TC = Other Countries not part of EEA - UNK = Unknown

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 3Table A0: Summary of samples taken in 2011 by region of origin

Strategy=Enforcement

Origin Samples Samples % Exceeding MRL Exceeding MRL % Non Compliant Non Compliant %

TC 4055 90% 97 2.4% 97 2.4%

Strategy=Surveillance

Origin Samples Samples % Exceeding MRL Exceeding MRL % Non Compliant Non Compliant %

Domestic 303 6.7% 9 3.0% 9 3.0%

EEA 85 1.9% 0 .00% 0 .00%

TC 68 1.5% 2 2.9% 2 2.9%

UNK 5 .11% 0 .00% 0 .00%

Page 4: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 4Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 4Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Strategy=Enforcement

ProductClass Product Total Ex % Domestic Ex % EEA Ex %

ThirdCountry Ex %

Vegetables Courgettes 240 0 100 0 0 . 0 0 . 240 0 100

Peppers 2900 90 96.9 0 0 . 0 0 . 2900 90 96.9

Tomatoes 915 7 99.2 0 0 . 0 0 . 915 7 99.2

Vegetables 4055 97 97.6 0 0 . 0 0 . 4055 97 97.6

4055 97 97.6 0 0 . 0 0 . 4055 97 97.6

Page 5: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 5Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 5Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Strategy=Enforcement

ProductClass Product Organic Ex %

NonOrganic Ex % Raw Ex % Process Ex %

Vegetables Courgettes 0 0 . 240 0 100 240 0 100 0 0 .

Peppers 0 0 . 2900 90 96.9 2900 90 96.9 0 0 .

Tomatoes 0 0 . 915 7 99.2 915 7 99.2 0 0 .

Vegetables 0 0 . 4055 97 97.6 4055 97 97.6 0 0 .

0 0 . 4055 97 97.6 4055 97 97.6 0 0 .

Page 6: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 6Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 6Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Strategy=Surveillance

Product Class Product Total Ex % Domestic Ex % EEA Ex %Third

Country Ex %

Animal products Bovine Liver 5 0 100 5 0 100 0 0 . 0 0 .

Poultry liver 11 0 100 10 0 100 0 0 . 1 0 100

Poultry meat 17 0 100 17 0 100 0 0 . 0 0 .

Swine Liver 9 0 100 9 0 100 0 0 . 0 0 .

Animal products 42 0 100 41 0 100 0 0 . 1 0 100

Baby food Baby food for infants and young childern 9 0 100 6 0 100 3 0 100 0 0 .

Processed cereal-based baby foods 12 2 83.3 11 2 81.8 1 0 100 0 0 .

Baby food 21 2 90.5 17 2 88.2 4 0 100 0 0 .

Cereals Rice 30 0 100 20 0 100 6 0 100 3 0 100

Wheat 23 0 100 23 0 100 0 0 . 0 0 .

Cereals 53 0 100 43 0 100 6 0 100 3 0 100

Fruits and nuts Apples 23 1 95.7 17 1 94.1 6 0 100 0 0 .

Bananas 25 0 100 1 0 100 2 0 100 20 0 100

Cranberries 1 0 100 1 0 100 0 0 . 0 0 .

Grapefruit 5 0 100 1 0 100 1 0 100 2 0 100

Lemons 16 0 100 0 0 . 2 0 100 14 0 100

Mandarins 20 0 100 0 0 . 16 0 100 4 0 100

Oranges 18 1 94.4 0 0 . 15 0 100 3 1 66.7

Peaches 7 1 85.7 6 1 83.3 1 0 100 0 0 .

Pears 26 1 96.2 10 0 100 14 0 100 2 1 50

Table grapes 9 0 100 4 0 100 4 0 100 0 0 .

Wine grapes 2 0 100 2 0 100 0 0 . 0 0 .

Fruits and nuts 152 4 97.4 42 2 95.2 61 0 100 45 2 95.6

Vegetables Aubergines (egg plants) 6 0 100 4 0 100 0 0 . 2 0 100

Beans (with pods) 27 1 96.3 24 1 95.8 1 0 100 2 0 100

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Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 7Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Strategy=Surveillance

Product Class Product Total Ex % Domestic Ex % EEA Ex %Third

Country Ex %

Beans (without pods) 1 0 100 1 0 100 0 0 . 0 0 .

Carrots 21 1 95.2 13 1 92.3 3 0 100 5 0 100

Chinese cabbage 3 0 100 3 0 100 0 0 . 0 0 .

Courgettes 2 0 100 0 0 . 0 0 . 2 0 100

Cucumbers 18 0 100 15 0 100 1 0 100 2 0 100

Head cabbage 19 0 100 18 0 100 0 0 . 1 0 100

Leek 11 0 100 10 0 100 0 0 . 1 0 100

Lettuce 12 0 100 12 0 100 0 0 . 0 0 .

Peas (with pods) 2 0 100 1 0 100 0 0 . 1 0 100

Peas (without pods) 8 0 100 5 0 100 3 0 100 0 0 .

Peppers 15 0 100 9 0 100 3 0 100 3 0 100

Potatoes 22 1 95.5 21 1 95.2 1 0 100 0 0 .

Spinach 16 1 93.8 15 1 93.3 1 0 100 0 0 .

Tomatoes 10 1 90 9 1 88.9 1 0 100 0 0 .

Vegetables 193 5 97.4 160 5 96.9 14 0 100 19 0 100

461 11 97.6 303 9 97 85 0 100 68 2 97.1

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Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 8Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 8Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Strategy=Surveillance

Product Class Product Organic Ex %Non

Organic Ex % Raw Ex % Process Ex %

Animal products Bovine Liver 0 0 . 5 0 100 5 0 100 0 0 .

Poultry liver 0 0 . 11 0 100 11 0 100 0 0 .

Poultry meat 0 0 . 17 0 100 17 0 100 0 0 .

Swine Liver 0 0 . 9 0 100 9 0 100 0 0 .

Animal products 0 0 . 42 0 100 42 0 100 0 0 .

Baby food Baby food for infants and young childern 0 0 . 9 0 100 0 0 . 9 0 100

Processed cereal-based baby foods 0 0 . 12 2 83.3 0 0 . 12 2 83.3

Baby food 0 0 . 21 2 90.5 0 0 . 21 2 90.5

Cereals Rice 0 0 . 30 0 100 15 0 100 15 0 100

Wheat 0 0 . 23 0 100 1 0 100 22 0 100

Cereals 0 0 . 53 0 100 16 0 100 37 0 100

Fruits and nuts Apples 0 0 . 23 1 95.7 23 1 95.7 0 0 .

Bananas 0 0 . 25 0 100 25 0 100 0 0 .

Cranberries 0 0 . 1 0 100 1 0 100 0 0 .

Grapefruit 0 0 . 5 0 100 5 0 100 0 0 .

Lemons 0 0 . 16 0 100 16 0 100 0 0 .

Mandarins 0 0 . 20 0 100 20 0 100 0 0 .

Oranges 0 0 . 18 1 94.4 18 1 94.4 0 0 .

Peaches 0 0 . 7 1 85.7 7 1 85.7 0 0 .

Pears 0 0 . 26 1 96.2 26 1 96.2 0 0 .

Table grapes 0 0 . 9 0 100 9 0 100 0 0 .

Wine grapes 0 0 . 2 0 100 2 0 100 0 0 .

Fruits and nuts 0 0 . 152 4 97.4 152 4 97.4 0 0 .

Vegetables Aubergines (egg plants) 0 0 . 6 0 100 6 0 100 0 0 .

Beans (with pods) 0 0 . 27 1 96.3 27 1 96.3 0 0 .

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Figures in bold are subtotals and totals for product groupsEx = number of samples above MRL; % = percentage of samples below MRL

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 9Table A1: Exceedence of MRL, number of samples exceeding MRL and percentage of samples below the MRL

Strategy=Surveillance

Product Class Product Organic Ex %Non

Organic Ex % Raw Ex % Process Ex %

Beans (without pods) 0 0 . 1 0 100 1 0 100 0 0 .

Carrots 0 0 . 21 1 95.2 21 1 95.2 0 0 .

Chinese cabbage 0 0 . 3 0 100 3 0 100 0 0 .

Courgettes 0 0 . 2 0 100 2 0 100 0 0 .

Cucumbers 0 0 . 18 0 100 18 0 100 0 0 .

Head cabbage 0 0 . 19 0 100 19 0 100 0 0 .

Leek 0 0 . 11 0 100 11 0 100 0 0 .

Lettuce 0 0 . 12 0 100 12 0 100 0 0 .

Peas (with pods) 0 0 . 2 0 100 2 0 100 0 0 .

Peas (without pods) 0 0 . 8 0 100 8 0 100 0 0 .

Peppers 0 0 . 15 0 100 15 0 100 0 0 .

Potatoes 0 0 . 22 1 95.5 22 1 95.5 0 0 .

Spinach 0 0 . 16 1 93.8 16 1 93.8 0 0 .

Tomatoes 0 0 . 10 1 90 10 1 90 0 0 .

Vegetables 0 0 . 193 5 97.4 193 5 97.4 0 0 .

0 0 . 461 11 97.6 403 9 97.8 58 2 96.6

Page 10: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 10Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 10Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Strategy=Enforcement

ProductClass Product Total ND % Domestic ND % EEA ND %

ThirdCountry ND %

Vegetables Courgettes 240 3 98.8 0 0 . 0 0 . 240 3 98.8

Peppers 2900 195 93.3 0 0 . 0 0 . 2900 195 93.3

Tomatoes 915 12 98.7 0 0 . 0 0 . 915 12 98.7

Vegetables 4055 210 94.8 0 0 . 0 0 . 4055 210 94.8

4055 210 94.8 0 0 . 0 0 . 4055 210 94.8

Page 11: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 11Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 11Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Strategy=Enforcement

ProductClass Product Organic ND %

NonOrganic ND % Raw ND % Process ND %

Vegetables Courgettes 0 0 . 240 3 98.8 240 3 98.8 0 0 .

Peppers 0 0 . 2900 195 93.3 2900 195 93.3 0 0 .

Tomatoes 0 0 . 915 12 98.7 915 12 98.7 0 0 .

Vegetables 0 0 . 4055 210 94.8 4055 210 94.8 0 0 .

0 0 . 4055 210 94.8 4055 210 94.8 0 0 .

Page 12: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 12Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 12Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Strategy=Surveillance

Product Class Product Total ND % Domestic ND % EEA ND %Third

Country ND %

Animal products Bovine Liver 5 0 100 5 0 100 0 0 . 0 0 .

Poultry liver 11 0 100 10 0 100 0 0 . 1 0 100

Poultry meat 17 0 100 17 0 100 0 0 . 0 0 .

Swine Liver 9 0 100 9 0 100 0 0 . 0 0 .

Animal products 42 0 100 41 0 100 0 0 . 1 0 100

Baby food Baby food for infants and young childern 9 0 100 6 0 100 3 0 100 0 0 .

Processed cereal-based baby foods 12 2 83.3 11 2 81.8 1 0 100 0 0 .

Baby food 21 2 90.5 17 2 88.2 4 0 100 0 0 .

Cereals Rice 30 6 80 20 4 80 6 2 66.7 3 0 100

Wheat 23 1 95.7 23 1 95.7 0 0 . 0 0 .

Cereals 53 7 86.8 43 5 88.4 6 2 66.7 3 0 100

Fruits and nuts Apples 23 11 52.2 17 11 35.3 6 0 100 0 0 .

Bananas 25 3 88 1 0 100 2 1 50 20 1 95

Cranberries 1 1 0 1 1 0 0 0 . 0 0 .

Grapefruit 5 4 20 1 1 0 1 0 100 2 2 0

Lemons 16 9 43.8 0 0 . 2 2 0 14 7 50

Mandarins 20 12 40 0 0 . 16 8 50 4 4 0

Oranges 18 8 55.6 0 0 . 15 7 53.3 3 1 66.7

Peaches 7 3 57.1 6 3 50 1 0 100 0 0 .

Pears 26 8 69.2 10 2 80 14 5 64.3 2 1 50

Table grapes 9 6 33.3 4 3 25 4 2 50 0 0 .

Wine grapes 2 2 0 2 2 0 0 0 . 0 0 .

Fruits and nuts 152 67 55.9 42 23 45.2 61 25 59 45 16 64.4

Vegetables Aubergines (egg plants) 6 0 100 4 0 100 0 0 . 2 0 100

Beans (with pods) 27 8 70.4 24 7 70.8 1 0 100 2 1 50

Page 13: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 13Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Strategy=Surveillance

Product Class Product Total ND % Domestic ND % EEA ND %Third

Country ND %

Beans (without pods) 1 1 0 1 1 0 0 0 . 0 0 .

Carrots 21 9 57.1 13 5 61.5 3 1 66.7 5 3 40

Chinese cabbage 3 2 33.3 3 2 33.3 0 0 . 0 0 .

Courgettes 2 0 100 0 0 . 0 0 . 2 0 100

Cucumbers 18 8 55.6 15 5 66.7 1 1 0 2 2 0

Head cabbage 19 6 68.4 18 5 72.2 0 0 . 1 1 0

Leek 11 5 54.5 10 4 60 0 0 . 1 1 0

Lettuce 12 4 66.7 12 4 66.7 0 0 . 0 0 .

Peas (with pods) 2 0 100 1 0 100 0 0 . 1 0 100

Peas (without pods) 8 2 75 5 2 60 3 0 100 0 0 .

Peppers 15 3 80 9 3 66.7 3 0 100 3 0 100

Potatoes 22 9 59.1 21 9 57.1 1 0 100 0 0 .

Spinach 16 5 68.8 15 5 66.7 1 0 100 0 0 .

Tomatoes 10 5 50 9 5 44.4 1 0 100 0 0 .

Vegetables 193 67 65.3 160 57 64.4 14 2 85.7 19 8 57.9

461 143 69 303 87 71.3 85 29 65.9 68 24 64.7

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Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 14Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 14Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Strategy=Surveillance

Product Class Product Organic ND %Non

Organic ND % Raw ND % Process ND %

Animal products Bovine Liver 0 0 . 5 0 100 5 0 100 0 0 .

Poultry liver 0 0 . 11 0 100 11 0 100 0 0 .

Poultry meat 0 0 . 17 0 100 17 0 100 0 0 .

Swine Liver 0 0 . 9 0 100 9 0 100 0 0 .

Animal products 0 0 . 42 0 100 42 0 100 0 0 .

Baby food Baby food for infants and young childern 0 0 . 9 0 100 0 0 . 9 0 100

Processed cereal-based baby foods 0 0 . 12 2 83.3 0 0 . 12 2 83.3

Baby food 0 0 . 21 2 90.5 0 0 . 21 2 90.5

Cereals Rice 0 0 . 30 6 80 15 6 60 15 0 100

Wheat 0 0 . 23 1 95.7 1 0 100 22 1 95.5

Cereals 0 0 . 53 7 86.8 16 6 62.5 37 1 97.3

Fruits and nuts Apples 0 0 . 23 11 52.2 23 11 52.2 0 0 .

Bananas 0 0 . 25 3 88 25 3 88 0 0 .

Cranberries 0 0 . 1 1 0 1 1 0 0 0 .

Grapefruit 0 0 . 5 4 20 5 4 20 0 0 .

Lemons 0 0 . 16 9 43.8 16 9 43.8 0 0 .

Mandarins 0 0 . 20 12 40 20 12 40 0 0 .

Oranges 0 0 . 18 8 55.6 18 8 55.6 0 0 .

Peaches 0 0 . 7 3 57.1 7 3 57.1 0 0 .

Pears 0 0 . 26 8 69.2 26 8 69.2 0 0 .

Table grapes 0 0 . 9 6 33.3 9 6 33.3 0 0 .

Wine grapes 0 0 . 2 2 0 2 2 0 0 0 .

Fruits and nuts 0 0 . 152 67 55.9 152 67 55.9 0 0 .

Vegetables Aubergines (egg plants) 0 0 . 6 0 100 6 0 100 0 0 .

Beans (with pods) 0 0 . 27 8 70.4 27 8 70.4 0 0 .

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Figures in bold are subtotals and totals for product groupsND = number of samples with residues above the reporting level (LOQ) % = percentage samples below reporting level (LOQ)

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 15Table A2: Samples above reporting level, number of samples above reporting level and percentage of samples below the reporting level

Strategy=Surveillance

Product Class Product Organic ND %Non

Organic ND % Raw ND % Process ND %

Beans (without pods) 0 0 . 1 1 0 1 1 0 0 0 .

Carrots 0 0 . 21 9 57.1 21 9 57.1 0 0 .

Chinese cabbage 0 0 . 3 2 33.3 3 2 33.3 0 0 .

Courgettes 0 0 . 2 0 100 2 0 100 0 0 .

Cucumbers 0 0 . 18 8 55.6 18 8 55.6 0 0 .

Head cabbage 0 0 . 19 6 68.4 19 6 68.4 0 0 .

Leek 0 0 . 11 5 54.5 11 5 54.5 0 0 .

Lettuce 0 0 . 12 4 66.7 12 4 66.7 0 0 .

Peas (with pods) 0 0 . 2 0 100 2 0 100 0 0 .

Peas (without pods) 0 0 . 8 2 75 8 2 75 0 0 .

Peppers 0 0 . 15 3 80 15 3 80 0 0 .

Potatoes 0 0 . 22 9 59.1 22 9 59.1 0 0 .

Spinach 0 0 . 16 5 68.8 16 5 68.8 0 0 .

Tomatoes 0 0 . 10 5 50 10 5 50 0 0 .

Vegetables 0 0 . 193 67 65.3 193 67 65.3 0 0 .

0 0 . 461 143 69 403 140 65.3 58 3 94.8

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 16Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 0 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 17Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 0 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 18Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 0 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 19Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 20Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 21Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 22Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalFeed

NrFound

MRLEx

168 tau-Fluvalinate 0 0 0

0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 23Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 42 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 24Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 42 0 0

37 DDE, p,p- 42 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 42 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 25Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 42 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 42 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 42 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 26Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 42 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 27Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 28Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 29Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

AnimalProducts

NrFound

MRLEx

168 tau-Fluvalinate 0 0 0

336 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 30Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 4 0 0

3 Aldicarb 4 0 0

4 Aldrin 12 0 0

5 Aldrin and Dieldrin 4 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 16 0 0

8 Azoxystrobin 15 0 0

9 Benomyl 5 0 0

10 Bifenthrin 21 0 0

11 Bitertanol 4 0 0

12 Boscalid 9 0 0

13 Bromopropylate 21 0 0

14 Bupirimate 21 0 0

15 Buprofezin 21 0 0

16 Captan 12 0 0

17 Carbaryl 4 0 0

18 Carbendazim and benomyl 9 0 0

19 Carbofuran 4 0 0

20 Chlordane 5 0 0

21 Chlorfenapyr 3 0 0

22 Chlorfenvinphos 11 0 0

23 Chlorobenzilate 5 0 0

24 Chlorothalonil 14 0 0

25 Chlorpropham 13 0 0

26 Chlorpropham (sum) 3 0 0

27 Chlorpyrifos 21 0 0

28 Chlorpyrifos-methyl 21 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 31Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

29 Clofentezine 4 0 0

30 Cyfluthrin 6 0 0

31 Cyfluthrin (sum) 9 0 0

32 Cypermethrin 7 0 0

33 Cypermethrin (sum) 9 0 0

34 Cyproconazole 5 0 0

35 Cyprodinil 21 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 14 0 0

39 DDT, p,p- 2 0 0

40 Deltamethrin 16 0 0

41 Demeton-S-Methyl 5 0 0

42 Diafenthiuron 0 0 0

43 Diallate 1 0 0

44 Diazinon 20 0 0

45 Dichlofluanid 7 0 0

46 Dichlorvos 21 0 0

47 Dicloran 5 0 0

48 Dicofol (sum) 15 0 0

49 Dicofol p, p' 6 0 0

50 Dieldrin 12 0 0

51 Difenoconazole 11 0 0

52 Dimethoate 8 0 0

53 Dimethoate (sum) 7 0 0

54 Dimethomorph 10 0 0

55 Dinocap (sum) 6 0 0

56 Diphenylamine 16 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 32Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 5 0 0

59 Endosulfan (sum) 20 0 0

60 Endrin 16 0 0

61 Epoxiconazole 4 0 0

62 Ethion 21 0 0

63 Fenarimol 16 0 0

64 Fenazaquin 4 0 0

65 Fenhexamid 12 0 0

66 Fenitrothion 21 0 0

67 Fenoxycarb 4 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 3 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 3 0 0

72 Fipronil 9 0 0

73 Fludioxonil 8 0 0

74 Flufenoxuron 4 0 0

75 Flusilazole 8 0 0

76 Folpet 10 0 0

77 Formetanate 4 0 0

78 Heptachlor 5 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 1 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 10 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 5 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 5 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 5 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 33Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

85 Hexaconazole 11 0 0

86 Hexythiazox 9 0 0

87 Imazalil 4 0 0

88 Imidacloprid 4 0 0

89 Indoxacarb as sum of the isomers S and R 4 0 0

90 Iprobenfos 1 0 0

91 Iprodione 9 0 0

92 Iprovalicarb 4 0 0

93 Kresoxim-methyl 21 0 0

94 Lambda-Cyhalothrin 16 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 11 0 0

96 Linuron 4 0 0

97 Malathion 14 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 7 0 0

99 Mepanipyrim 5 0 0

100 Metalaxyl 9 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 12 0 0

102 Metconazole 0 0 0

103 Methamidophos 4 0 0

104 Methidathion 11 0 0

105 Methiocarb 11 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 3 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 4 0 0

108 Methoxyfenozide 4 0 0

109 Monocrotophos 4 0 0

110 Myclobutanil 16 0 0

111 Oxadixyl 4 0 0

112 Oxamyl 9 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 34Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 4 0 0

114 Parathion 16 0 0

115 Parathion-methyl 13 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 8 0 0

117 Penconazole 16 0 0

118 Pencycuron 4 0 0

119 Permethrin (sum of isomers) 5 0 0

120 Phosalone 16 0 0

121 Phosmet 6 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 5 0 0

123 Pirimicarb 11 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 10 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 21 2 2

127 Prochloraz 6 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 4 0 0

129 Procymidone 16 0 0

130 Profenofos 16 0 0

131 Propamocarb 4 0 0

132 Propargite 16 0 0

133 Propiconazole 4 0 0

134 Propyzamide 4 0 0

135 Prothioconazole 4 0 0

136 Pyraclostrobin 4 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 4 0 0

140 Pyrimethanil 16 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 35Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

141 Pyriproxyfen 16 0 0

142 Quinoxyfen 5 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 4 0 0

144 Spiroxamine 9 0 0

145 Tebuconazole 11 0 0

146 Tebufenozide 9 0 0

147 Tebufenpyrad 16 0 0

148 Teflubenzuron 4 0 0

149 Terbacil 0 0 0

150 Tetraconazole 4 0 0

151 Tetradifon 21 0 0

152 Thiabendazole 4 0 0

153 Thiacloprid 4 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 4 0 0

155 Thiophanate-methyl 4 0 0

156 Tolclofos-methyl 21 0 0

157 Tolylfluanid 10 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 2 0 0

159 Triadimefon 8 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 8 0 0

161 Triazophos 16 0 0

162 Trifloxystrobin 4 0 0

163 Trifluralin 3 0 0

164 Vernolate 1 0 0

165 Vinclozolin 20 0 0

166 alpha-Endosulfan 1 0 0

167 beta-Endosulfan 1 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 36Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Baby/InfantFood

NrFound

MRLEx

168 tau-Fluvalinate 3 0 0

1389 2 2

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 37Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

1 Acephate 30 0 0

2 Acetamiprid 37 0 0

3 Aldicarb 37 0 0

4 Aldrin 39 0 0

5 Aldrin and Dieldrin 5 0 0

6 Atrazine 30 0 0

7 Azinphos-methyl 53 0 0

8 Azoxystrobin 53 0 0

9 Benomyl 6 0 0

10 Bifenthrin 53 1 0

11 Bitertanol 7 0 0

12 Boscalid 37 0 0

13 Bromopropylate 53 0 0

14 Bupirimate 53 0 0

15 Buprofezin 53 0 0

16 Captan 46 0 0

17 Carbaryl 37 0 0

18 Carbendazim and benomyl 37 0 0

19 Carbofuran 37 0 0

20 Chlordane 6 0 0

21 Chlorfenapyr 5 0 0

22 Chlorfenvinphos 17 0 0

23 Chlorobenzilate 6 0 0

24 Chlorothalonil 50 0 0

25 Chlorpropham 48 0 0

26 Chlorpropham (sum) 5 0 0

27 Chlorpyrifos 53 1 0

28 Chlorpyrifos-methyl 53 1 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 38Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

29 Clofentezine 7 0 0

30 Cyfluthrin 6 0 0

31 Cyfluthrin (sum) 45 0 0

32 Cypermethrin 8 5 0

33 Cypermethrin (sum) 45 0 0

34 Cyproconazole 30 0 0

35 Cyprodinil 53 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 41 0 0

39 DDT, p,p- 3 0 0

40 Deltamethrin 53 0 0

41 Demeton-S-Methyl 30 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 53 0 0

45 Dichlofluanid 38 0 0

46 Dichlorvos 53 0 0

47 Dicloran 6 0 0

48 Dicofol (sum) 21 0 0

49 Dicofol p, p' 32 0 0

50 Dieldrin 39 0 0

51 Difenoconazole 47 0 0

52 Dimethoate 39 0 0

53 Dimethoate (sum) 12 0 0

54 Dimethomorph 17 0 0

55 Dinocap (sum) 10 0 0

56 Diphenylamine 23 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 39Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

57 Dithiocarbamates 30 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 53 0 0

60 Endrin 44 0 0

61 Epoxiconazole 37 0 0

62 Ethion 53 0 0

63 Fenarimol 53 0 0

64 Fenazaquin 7 0 0

65 Fenhexamid 48 0 0

66 Fenitrothion 53 0 0

67 Fenoxycarb 37 0 0

68 Fenpropathrin 30 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 30 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 5 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 5 0 0

72 Fipronil 37 0 0

73 Fludioxonil 14 0 0

74 Flufenoxuron 7 0 0

75 Flusilazole 14 0 0

76 Folpet 43 0 0

77 Formetanate 7 0 0

78 Heptachlor 6 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 38 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 30 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 30 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 30 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 40Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

85 Hexaconazole 47 0 0

86 Hexythiazox 13 0 0

87 Imazalil 37 0 0

88 Imidacloprid 37 0 0

89 Indoxacarb as sum of the isomers S and R 37 0 0

90 Iprobenfos 2 0 0

91 Iprodione 41 0 0

92 Iprovalicarb 37 0 0

93 Kresoxim-methyl 53 0 0

94 Lambda-Cyhalothrin 53 2 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 38 0 0

96 Linuron 7 0 0

97 Malathion 11 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 42 0 0

99 Mepanipyrim 30 0 0

100 Metalaxyl 11 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 42 0 0

102 Metconazole 30 0 0

103 Methamidophos 37 0 0

104 Methidathion 47 0 0

105 Methiocarb 46 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 5 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 37 0 0

108 Methoxyfenozide 7 0 0

109 Monocrotophos 37 0 0

110 Myclobutanil 47 0 0

111 Oxadixyl 7 0 0

112 Oxamyl 45 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 41Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 7 0 0

114 Parathion 47 0 0

115 Parathion-methyl 18 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 35 0 0

117 Penconazole 53 0 0

118 Pencycuron 7 0 0

119 Permethrin (sum of isomers) 30 0 0

120 Phosalone 53 0 0

121 Phosmet 10 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 7 0 0

123 Pirimicarb 16 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 37 0 0

125 Pirimiphos-Ethyl 30 0 0

126 Pirimiphos-methyl 53 1 0

127 Prochloraz 40 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 5 0 0

129 Procymidone 53 0 0

130 Profenofos 53 0 0

131 Propamocarb 7 0 0

132 Propargite 23 0 0

133 Propiconazole 7 0 0

134 Propyzamide 7 0 0

135 Prothioconazole 7 0 0

136 Pyraclostrobin 7 0 0

137 Pyrazophos 30 0 0

138 Pyrethrins 30 0 0

139 Pyridaben 37 0 0

140 Pyrimethanil 23 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 42Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

141 Pyriproxyfen 23 0 0

142 Quinoxyfen 30 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 7 0 0

144 Spiroxamine 13 0 0

145 Tebuconazole 47 0 0

146 Tebufenozide 43 0 0

147 Tebufenpyrad 23 0 0

148 Teflubenzuron 7 0 0

149 Terbacil 30 0 0

150 Tetraconazole 7 0 0

151 Tetradifon 53 0 0

152 Thiabendazole 37 0 0

153 Thiacloprid 37 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 7 0 0

155 Thiophanate-methyl 7 0 0

156 Tolclofos-methyl 53 0 0

157 Tolylfluanid 46 2 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 2 0 0

159 Triadimefon 9 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 44 1 0

161 Triazophos 47 0 0

162 Trifloxystrobin 37 0 0

163 Trifluralin 5 0 0

164 Vernolate 2 0 0

165 Vinclozolin 51 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 43Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Cereals

NrFound

MRLEx

168 tau-Fluvalinate 5 0 0

4685 14 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 44Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

1 Acephate 38 0 0

2 Acetamiprid 59 1 1

3 Aldicarb 59 0 0

4 Aldrin 80 0 0

5 Aldrin and Dieldrin 39 0 0

6 Atrazine 38 0 0

7 Azinphos-methyl 152 2 0

8 Azoxystrobin 146 1 0

9 Benomyl 26 0 0

10 Bifenthrin 152 9 0

11 Bitertanol 21 0 0

12 Boscalid 59 1 0

13 Bromopropylate 152 1 0

14 Bupirimate 152 0 0

15 Buprofezin 152 5 0

16 Captan 131 0 0

17 Carbaryl 59 0 0

18 Carbendazim and benomyl 59 8 1

19 Carbofuran 59 0 0

20 Chlordane 26 0 0

21 Chlorfenapyr 24 0 0

22 Chlorfenvinphos 88 0 0

23 Chlorobenzilate 26 0 0

24 Chlorothalonil 136 0 0

25 Chlorpropham 128 0 0

26 Chlorpropham (sum) 24 0 0

27 Chlorpyrifos 152 9 0

28 Chlorpyrifos-methyl 152 4 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 45Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

29 Clofentezine 21 0 0

30 Cyfluthrin 41 2 0

31 Cyfluthrin (sum) 99 1 0

32 Cypermethrin 53 12 0

33 Cypermethrin (sum) 99 1 0

34 Cyproconazole 38 0 0

35 Cyprodinil 152 4 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 103 0 0

39 DDT, p,p- 16 0 0

40 Deltamethrin 152 0 0

41 Demeton-S-Methyl 38 0 0

42 Diafenthiuron 0 0 0

43 Diallate 15 0 0

44 Diazinon 137 0 0

45 Dichlofluanid 91 0 0

46 Dichlorvos 152 0 0

47 Dicloran 26 0 0

48 Dicofol (sum) 102 1 0

49 Dicofol p, p' 50 0 0

50 Dieldrin 80 0 0

51 Difenoconazole 126 0 0

52 Dimethoate 95 1 1

53 Dimethoate (sum) 45 0 0

54 Dimethomorph 82 1 0

55 Dinocap (sum) 52 0 0

56 Diphenylamine 114 1 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 46Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

57 Dithiocarbamates 38 4 0

58 EPN 0 0 0

59 Endosulfan (sum) 137 0 0

60 Endrin 119 0 0

61 Epoxiconazole 59 0 0

62 Ethion 152 0 0

63 Fenarimol 152 2 0

64 Fenazaquin 21 0 0

65 Fenhexamid 109 1 0

66 Fenitrothion 152 0 0

67 Fenoxycarb 59 0 0

68 Fenpropathrin 38 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 38 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 24 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 24 0 0

72 Fipronil 59 0 0

73 Fludioxonil 57 0 0

74 Flufenoxuron 21 0 0

75 Flusilazole 57 0 0

76 Folpet 115 0 0

77 Formetanate 21 0 0

78 Heptachlor 26 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 15 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 78 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 38 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 38 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 38 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 47Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

85 Hexaconazole 126 0 0

86 Hexythiazox 47 0 0

87 Imazalil 59 13 1

88 Imidacloprid 59 2 0

89 Indoxacarb as sum of the isomers S and R 59 1 0

90 Iprobenfos 12 0 0

91 Iprodione 103 0 0

92 Iprovalicarb 59 0 0

93 Kresoxim-methyl 152 3 0

94 Lambda-Cyhalothrin 152 8 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 93 0 0

96 Linuron 21 0 0

97 Malathion 69 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 83 0 0

99 Mepanipyrim 38 0 0

100 Metalaxyl 69 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 83 0 0

102 Metconazole 38 0 0

103 Methamidophos 59 0 0

104 Methidathion 126 0 0

105 Methiocarb 101 1 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 24 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 59 0 0

108 Methoxyfenozide 21 0 0

109 Monocrotophos 59 0 0

110 Myclobutanil 126 2 0

111 Oxadixyl 21 0 0

112 Oxamyl 99 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 48Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 21 0 0

114 Parathion 126 0 0

115 Parathion-methyl 90 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 62 0 0

117 Penconazole 152 5 0

118 Pencycuron 21 0 0

119 Permethrin (sum of isomers) 38 0 0

120 Phosalone 152 0 0

121 Phosmet 37 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 51 0 0

123 Pirimicarb 63 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 89 0 0

125 Pirimiphos-Ethyl 38 0 0

126 Pirimiphos-methyl 152 0 0

127 Prochloraz 75 2 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 39 0 0

129 Procymidone 152 0 0

130 Profenofos 152 0 0

131 Propamocarb 21 0 0

132 Propargite 114 0 0

133 Propiconazole 21 0 0

134 Propyzamide 21 0 0

135 Prothioconazole 21 0 0

136 Pyraclostrobin 21 0 0

137 Pyrazophos 38 0 0

138 Pyrethrins 38 0 0

139 Pyridaben 59 0 0

140 Pyrimethanil 114 1 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 49Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

141 Pyriproxyfen 114 1 0

142 Quinoxyfen 38 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 21 0 0

144 Spiroxamine 47 0 0

145 Tebuconazole 126 1 0

146 Tebufenozide 85 0 0

147 Tebufenpyrad 114 0 0

148 Teflubenzuron 21 0 0

149 Terbacil 38 0 0

150 Tetraconazole 21 0 0

151 Tetradifon 152 0 0

152 Thiabendazole 59 1 0

153 Thiacloprid 59 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 21 0 0

155 Thiophanate-methyl 21 0 0

156 Tolclofos-methyl 152 1 0

157 Tolylfluanid 95 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 27 0 0

159 Triadimefon 57 2 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 95 0 0

161 Triazophos 126 0 0

162 Trifloxystrobin 59 0 0

163 Trifluralin 24 0 0

164 Vernolate 12 0 0

165 Vinclozolin 140 1 0

166 alpha-Endosulfan 15 0 0

167 beta-Endosulfan 15 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 50Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Fruitand

NutsNr

FoundMRL

Ex

168 tau-Fluvalinate 24 0 0

11826 117 4

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 51Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 0 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 52Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 0 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 53Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 0 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 54Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 55Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 56Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 57Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Infusions

NrFound

MRLEx

168 tau-Fluvalinate 0 0 0

0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 58Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 0 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 59Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 0 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 60Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 0 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 61Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 62Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 63Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 64Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

Oilplants

NrFound

MRLExc

168 tau-Fluvalinate 0 0 0

0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 65Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 0 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 66Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 0 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 67Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 0 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 68Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 69Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 70Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 71Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Pulses

NrFound

MRLEx

168 tau-Fluvalinate 0 0 0

0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 72Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 0 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 73Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 0 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 74Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 0 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 75Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 76Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 77Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 78Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Spices

NrFound

MRLEx

168 tau-Fluvalinate 0 0 0

0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 79Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

1 Acephate 0 0 0

2 Acetamiprid 0 0 0

3 Aldicarb 0 0 0

4 Aldrin 0 0 0

5 Aldrin and Dieldrin 0 0 0

6 Atrazine 0 0 0

7 Azinphos-methyl 0 0 0

8 Azoxystrobin 0 0 0

9 Benomyl 0 0 0

10 Bifenthrin 0 0 0

11 Bitertanol 0 0 0

12 Boscalid 0 0 0

13 Bromopropylate 0 0 0

14 Bupirimate 0 0 0

15 Buprofezin 0 0 0

16 Captan 0 0 0

17 Carbaryl 0 0 0

18 Carbendazim and benomyl 0 0 0

19 Carbofuran 0 0 0

20 Chlordane 0 0 0

21 Chlorfenapyr 0 0 0

22 Chlorfenvinphos 0 0 0

23 Chlorobenzilate 0 0 0

24 Chlorothalonil 0 0 0

25 Chlorpropham 0 0 0

26 Chlorpropham (sum) 0 0 0

27 Chlorpyrifos 0 0 0

28 Chlorpyrifos-methyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 80Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

29 Clofentezine 0 0 0

30 Cyfluthrin 0 0 0

31 Cyfluthrin (sum) 0 0 0

32 Cypermethrin 0 0 0

33 Cypermethrin (sum) 0 0 0

34 Cyproconazole 0 0 0

35 Cyprodinil 0 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 0 0 0

39 DDT, p,p- 0 0 0

40 Deltamethrin 0 0 0

41 Demeton-S-Methyl 0 0 0

42 Diafenthiuron 0 0 0

43 Diallate 0 0 0

44 Diazinon 0 0 0

45 Dichlofluanid 0 0 0

46 Dichlorvos 0 0 0

47 Dicloran 0 0 0

48 Dicofol (sum) 0 0 0

49 Dicofol p, p' 0 0 0

50 Dieldrin 0 0 0

51 Difenoconazole 0 0 0

52 Dimethoate 0 0 0

53 Dimethoate (sum) 0 0 0

54 Dimethomorph 0 0 0

55 Dinocap (sum) 0 0 0

56 Diphenylamine 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 81Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

57 Dithiocarbamates 0 0 0

58 EPN 0 0 0

59 Endosulfan (sum) 0 0 0

60 Endrin 0 0 0

61 Epoxiconazole 0 0 0

62 Ethion 0 0 0

63 Fenarimol 0 0 0

64 Fenazaquin 0 0 0

65 Fenhexamid 0 0 0

66 Fenitrothion 0 0 0

67 Fenoxycarb 0 0 0

68 Fenpropathrin 0 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 0 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 0 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 0 0 0

72 Fipronil 0 0 0

73 Fludioxonil 0 0 0

74 Flufenoxuron 0 0 0

75 Flusilazole 0 0 0

76 Folpet 0 0 0

77 Formetanate 0 0 0

78 Heptachlor 0 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 0 0 0

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 0 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 0 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 82Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

85 Hexaconazole 0 0 0

86 Hexythiazox 0 0 0

87 Imazalil 0 0 0

88 Imidacloprid 0 0 0

89 Indoxacarb as sum of the isomers S and R 0 0 0

90 Iprobenfos 0 0 0

91 Iprodione 0 0 0

92 Iprovalicarb 0 0 0

93 Kresoxim-methyl 0 0 0

94 Lambda-Cyhalothrin 0 0 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0 0 0

96 Linuron 0 0 0

97 Malathion 0 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 0 0 0

99 Mepanipyrim 0 0 0

100 Metalaxyl 0 0 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 0 0 0

102 Metconazole 0 0 0

103 Methamidophos 0 0 0

104 Methidathion 0 0 0

105 Methiocarb 0 0 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 0 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 0 0 0

108 Methoxyfenozide 0 0 0

109 Monocrotophos 0 0 0

110 Myclobutanil 0 0 0

111 Oxadixyl 0 0 0

112 Oxamyl 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 83Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 0 0 0

114 Parathion 0 0 0

115 Parathion-methyl 0 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 0 0 0

117 Penconazole 0 0 0

118 Pencycuron 0 0 0

119 Permethrin (sum of isomers) 0 0 0

120 Phosalone 0 0 0

121 Phosmet 0 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 0 0 0

123 Pirimicarb 0 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0 0 0

125 Pirimiphos-Ethyl 0 0 0

126 Pirimiphos-methyl 0 0 0

127 Prochloraz 0 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 0 0 0

129 Procymidone 0 0 0

130 Profenofos 0 0 0

131 Propamocarb 0 0 0

132 Propargite 0 0 0

133 Propiconazole 0 0 0

134 Propyzamide 0 0 0

135 Prothioconazole 0 0 0

136 Pyraclostrobin 0 0 0

137 Pyrazophos 0 0 0

138 Pyrethrins 0 0 0

139 Pyridaben 0 0 0

140 Pyrimethanil 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 84Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

141 Pyriproxyfen 0 0 0

142 Quinoxyfen 0 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0 0 0

144 Spiroxamine 0 0 0

145 Tebuconazole 0 0 0

146 Tebufenozide 0 0 0

147 Tebufenpyrad 0 0 0

148 Teflubenzuron 0 0 0

149 Terbacil 0 0 0

150 Tetraconazole 0 0 0

151 Tetradifon 0 0 0

152 Thiabendazole 0 0 0

153 Thiacloprid 0 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0 0 0

155 Thiophanate-methyl 0 0 0

156 Tolclofos-methyl 0 0 0

157 Tolylfluanid 0 0 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 0 0 0

159 Triadimefon 0 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 0 0 0

161 Triazophos 0 0 0

162 Trifloxystrobin 0 0 0

163 Trifluralin 0 0 0

164 Vernolate 0 0 0

165 Vinclozolin 0 0 0

166 alpha-Endosulfan 0 0 0

167 beta-Endosulfan 0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 85Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound

SugarPlants

NrFound

MRLEx

168 tau-Fluvalinate 0 0 0

0 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 86Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

1 Acephate 88 0 0

2 Acetamiprid 115 0 0

3 Aldicarb 115 0 0

4 Aldrin 128 0 0

5 Aldrin and Dieldrin 33 0 0

6 Atrazine 88 0 0

7 Azinphos-methyl 193 0 0

8 Azoxystrobin 184 0 0

9 Benomyl 27 0 0

10 Bifenthrin 193 5 0

11 Bitertanol 27 0 0

12 Boscalid 115 2 0

13 Bromopropylate 193 0 0

14 Bupirimate 193 0 0

15 Buprofezin 193 0 0

16 Captan 166 0 0

17 Carbaryl 115 0 0

18 Carbendazim and benomyl 2666 27 0

19 Carbofuran 115 0 0

20 Chlordane 27 0 0

21 Chlorfenapyr 25 0 0

22 Chlorfenvinphos 78 0 0

23 Chlorobenzilate 27 0 0

24 Chlorothalonil 180 0 0

25 Chlorpropham 168 1 0

26 Chlorpropham (sum) 25 0 0

27 Chlorpyrifos 193 6 1

28 Chlorpyrifos-methyl 193 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 87Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

29 Clofentezine 2578 3 3

30 Cyfluthrin 35 3 0

31 Cyfluthrin (sum) 153 0 0

32 Cypermethrin 40 15 0

33 Cypermethrin (sum) 153 4 0

34 Cyproconazole 88 0 0

35 Cyprodinil 193 0 0

36 DDD, p,p- 0 0 0

37 DDE, p,p- 0 0 0

38 DDT (sum) 148 0 0

39 DDT, p,p- 13 0 0

40 Deltamethrin 193 0 0

41 Demeton-S-Methyl 88 0 0

42 Diafenthiuron 2551 0 0

43 Diallate 8 0 0

44 Diazinon 185 0 0

45 Dichlofluanid 128 0 0

46 Dichlorvos 193 0 0

47 Dicloran 27 0 0

48 Dicofol (sum) 100 0 0

49 Dicofol p, p' 93 0 0

50 Dieldrin 128 0 0

51 Difenoconazole 166 0 0

52 Dimethoate 136 1 1

53 Dimethoate (sum) 2603 3 2

54 Dimethomorph 69 0 0

55 Dinocap (sum) 43 0 0

56 Diphenylamine 105 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 88Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

57 Dithiocarbamates 88 11 1

58 EPN 0 0 0

59 Endosulfan (sum) 185 0 0

60 Endrin 161 0 0

61 Epoxiconazole 115 0 0

62 Ethion 193 0 0

63 Fenarimol 193 0 0

64 Fenazaquin 27 0 0

65 Fenhexamid 167 1 0

66 Fenitrothion 193 0 0

67 Fenoxycarb 115 0 0

68 Fenpropathrin 88 0 0

69 Fenvalerate (sum of RR, SS, RS and SR isomers) 88 0 0

70 Fenvalerate and Esfenvalerate (Sum of RR and SS isomers) 25 0 0

71 Fenvalerate and Esfenvalerate (Sum of RS and SR isomers) 25 0 0

72 Fipronil 115 0 0

73 Fludioxonil 57 0 0

74 Flufenoxuron 27 0 0

75 Flusilazole 57 0 0

76 Folpet 153 0 0

77 Formetanate 2578 68 17

78 Heptachlor 27 0 0

79 Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 8 0 0

80 Heptachlor (sum of heptachlor and the cis and trans isomers of heptachlor epoxide) 126 1 1

81 Heptachlor endo-epoxide 0 0 0

82 Hexachlorobenzene 88 0 0

83 Hexachlorocyclohexane (HCH), alpha-isomer 88 0 0

84 Hexachlorocyclohexane (HCH), beta-isomer 88 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 89Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

85 Hexaconazole 166 0 0

86 Hexythiazox 54 0 0

87 Imazalil 115 0 0

88 Imidacloprid 115 1 0

89 Indoxacarb as sum of the isomers S and R 115 0 0

90 Iprobenfos 5 0 0

91 Iprodione 148 0 0

92 Iprovalicarb 115 0 0

93 Kresoxim-methyl 193 1 0

94 Lambda-Cyhalothrin 193 8 0

95 Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 134 0 0

96 Linuron 27 0 0

97 Malathion 53 0 0

98 Malathion (sum of malathion and malaoxon expressed as malathion) 2691 37 11

99 Mepanipyrim 88 0 0

100 Metalaxyl 53 2 0

101 Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M (sum of isomers)) 140 1 0

102 Metconazole 88 0 0

103 Methamidophos 115 0 0

104 Methidathion 166 0 0

105 Methiocarb 155 5 0

106 Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressed as methiocarb) 25 0 0

107 Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed as methomyl) 4170 26 12

108 Methoxyfenozide 27 0 0

109 Monocrotophos 115 0 0

110 Myclobutanil 166 0 0

111 Oxadixyl 27 0 0

112 Oxamyl 4208 29 23

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 90Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

113 Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfone expressed as oxydemeton-methyl) 27 0 0

114 Parathion 166 0 0

115 Parathion-methyl 80 0 0

116 Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed as Parathion-methyl) 113 0 0

117 Penconazole 193 2 0

118 Pencycuron 27 0 0

119 Permethrin (sum of isomers) 88 2 0

120 Phosalone 193 0 0

121 Phosmet 40 0 0

122 Phosmet (phosmet and phosmet oxon expressed as phosmet) 38 0 0

123 Pirimicarb 67 0 0

124 Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 126 0 0

125 Pirimiphos-Ethyl 88 0 0

126 Pirimiphos-methyl 193 0 0

127 Prochloraz 128 0 0

128 Prochloraz (sum of prochloraz and its metabolites containing the 2,4,6-Trichlorophenol moiety expressed as prochloraz) 33 0 0

129 Procymidone 2744 14 13

130 Profenofos 193 0 0

131 Propamocarb 27 0 0

132 Propargite 105 0 0

133 Propiconazole 27 0 0

134 Propyzamide 27 0 0

135 Prothioconazole 27 0 0

136 Pyraclostrobin 27 0 0

137 Pyrazophos 88 0 0

138 Pyrethrins 88 0 0

139 Pyridaben 115 0 0

140 Pyrimethanil 105 2 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 91Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

141 Pyriproxyfen 105 1 0

142 Quinoxyfen 88 0 0

143 Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 27 0 0

144 Spiroxamine 54 0 0

145 Tebuconazole 166 0 0

146 Tebufenozide 142 0 0

147 Tebufenpyrad 105 0 0

148 Teflubenzuron 27 0 0

149 Terbacil 88 0 0

150 Tetraconazole 27 0 0

151 Tetradifon 2744 26 23

152 Thiabendazole 115 0 0

153 Thiacloprid 115 0 0

154 Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 27 0 0

155 Thiophanate-methyl 2578 0 0

156 Tolclofos-methyl 193 0 0

157 Tolylfluanid 146 1 0

158 Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed as tolylfluanid) 13 0 0

159 Triadimefon 48 0 0

160 Triadimefon (sum of Triadimefon and Triadimenol) 145 0 0

161 Triazophos 166 0 0

162 Trifloxystrobin 115 0 0

163 Trifluralin 25 1 0

164 Vernolate 5 0 0

165 Vinclozolin 188 1 0

166 alpha-Endosulfan 8 0 0

167 beta-Endosulfan 8 0 0

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 92Table A3: Scope of analytical methods, number of samples analysed for each residue by matrix

Rownumber Compound Vegetables

NrFound

MRLEx

168 tau-Fluvalinate 25 0 0

47488 311 108

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 93Table A4: Overview of samples taken in National and EU co-ordinated programmes

EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 93Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Enforcement Origin=TC Country=Turkey

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Vegetables Courgettes Unprocessed Production method unknown 240 3 0 0 0 0

Vegetables Peppers Unprocessed Production method unknown 2900 195 90 0 0 0

Vegetables Tomatoes Unprocessed Production method unknown 915 12 7 0 0 0

Origin 4055 210 97 0 0 0

Region 4055 210 97 0 0 0

Strategy 4055 210 97 0 0 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 94Table A4: Overview of samples taken in National and EU co-ordinated programmes

EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 94Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=Domestic Country=Bulgaria

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Animal products Bovine Liver Freezing Production method unknown 5 0 0 5 0 0

Animal products Poultry liver Freezing Production method unknown 10 0 0 10 0 0

Animal products Poultry meat Freezing Production method unknown 17 0 0 17 0 0

Animal products Swine Liver Freezing Production method unknown 9 0 0 9 0 0

Baby food Baby food for infants and young childern Processed Production method unknown 6 0 0 0 0 0

Baby food Processed cereal-based baby foods Milling Other production method 4 2 2 0 0 0

Baby food Processed cereal-based baby foods Processed Production method unknown 7 0 0 7 0 0

Cereals Rice Polishing Production method unknown 9 0 0 0 0 0

Cereals Rice Unprocessed Production method unknown 11 4 0 11 3 0

Cereals Wheat Milling Production method unknown 22 1 0 22 1 0

Cereals Wheat Unprocessed Production method unknown 1 0 0 0 0 0

Fruits and nuts Apples Unprocessed Integrated Pest Management 5 3 1 0 0 0

Fruits and nuts Apples Unprocessed Production method unknown 12 8 0 0 0 0

Fruits and nuts Bananas Unprocessed Production method unknown 1 0 0 0 0 0

Fruits and nuts Cranberries Unprocessed Production method unknown 1 1 0 0 0 0

Fruits and nuts Grapefruit Unprocessed Production method unknown 1 1 0 0 0 0

Fruits and nuts Peaches Unprocessed Traditional production 6 3 1 0 0 0

Fruits and nuts Pears Unprocessed Production method unknown 4 2 0 4 2 0

Fruits and nuts Pears Unprocessed Traditional production 6 0 0 6 0 0

Fruits and nuts Table grapes Unprocessed Production method unknown 4 3 0 0 0 0

Fruits and nuts Wine grapes Unprocessed Production method unknown 2 2 0 0 0 0

Vegetables Aubergines (egg plants) Unprocessed Production method unknown 4 0 0 0 0 0

Vegetables Beans (with pods) Freezing Production method unknown 11 5 1 11 2 1

Vegetables Beans (with pods) Unprocessed Production method unknown 12 2 0 12 1 0

Vegetables Beans (with pods) Unprocessed Traditional production 1 0 0 1 0 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 95Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=Domestic Country=Bulgaria

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Vegetables Beans (without pods) Unprocessed Production method unknown 1 1 0 0 0 0

Vegetables Carrots Unprocessed Production method unknown 7 4 0 7 2 0

Vegetables Carrots Unprocessed Traditional production 6 1 1 6 1 1

Vegetables Chinese cabbage Unprocessed Production method unknown 3 2 0 0 0 0

Vegetables Cucumbers Unprocessed Production method unknown 1 1 0 1 1 0

Vegetables Cucumbers Unprocessed Under glass / protected growing condition 14 4 0 14 3 0

Vegetables Head cabbage Unprocessed Production method unknown 18 5 0 0 0 0

Vegetables Leek Unprocessed Production method unknown 10 4 0 0 0 0

Vegetables Lettuce Unprocessed Production method unknown 2 2 0 0 0 0

Vegetables Lettuce Unprocessed Traditional production 3 0 0 0 0 0

Vegetables Lettuce Unprocessed Under glass / protected growing condition 7 2 0 0 0 0

Vegetables Peas (with pods) Freezing Production method unknown 1 0 0 0 0 0

Vegetables Peas (without pods) Freezing Production method unknown 3 0 0 0 0 0

Vegetables Peas (without pods) Unprocessed Production method unknown 2 2 0 0 0 0

Vegetables Peppers Unprocessed Production method unknown 9 3 0 0 0 0

Vegetables Potatoes Unprocessed Production method unknown 5 0 0 5 0 0

Vegetables Potatoes Unprocessed Traditional production 16 9 1 16 8 0

Vegetables Spinach Freezing Production method unknown 1 0 0 1 0 0

Vegetables Spinach Freezing Traditional production 2 0 0 2 0 0

Vegetables Spinach Unprocessed Production method unknown 2 2 0 2 2 0

Vegetables Spinach Unprocessed Traditional production 9 3 1 9 3 1

Vegetables Spinach Unprocessed Under glass / protected growing condition 1 0 0 1 0 0

Vegetables Tomatoes Unprocessed Production method unknown 2 1 0 0 0 0

Vegetables Tomatoes Unprocessed Traditional production 6 3 0 0 0 0

Vegetables Tomatoes Unprocessed Under glass / protected growing condition 1 1 1 0 0 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 96Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=Domestic Country=Bulgaria

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Origin 303 87 9 179 29 3

Region 303 87 9 179 29 3

Strategy=Surveillance Origin=EEA Country=Belgium

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Pears Unprocessed Production method unknown 2 2 0 2 2 0

Vegetables Beans (with pods) Freezing Production method unknown 1 0 0 1 0 0

Vegetables Peas (without pods) Freezing Production method unknown 1 0 0 0 0 0

Vegetables Spinach Freezing Production method unknown 1 0 0 1 0 0

Origin 5 2 0 4 2 0

Strategy=Surveillance Origin=EEA Country=European Union

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Cereals Rice Polishing Production method unknown 2 0 0 0 0 0

Strategy=Surveillance Origin=EEA Country=France

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Pears Unprocessed Production method unknown 1 1 0 1 1 0

Vegetables Potatoes Unprocessed Production method unknown 1 0 0 1 0 0

Origin 2 1 0 2 1 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 97Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=EEA Country=Germany

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Baby food Processed cereal-based baby foods Milling Other production method 1 0 0 0 0 0

Vegetables Carrots Unprocessed Production method unknown 1 1 0 1 1 0

Origin 2 1 0 1 1 0

Strategy=Surveillance Origin=EEA Country=Greece

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Baby food Baby food for infants and young childern Processed Production method unknown 1 0 0 0 0 0

Cereals Rice Unprocessed Production method unknown 1 1 0 1 1 0

Fruits and nuts Apples Unprocessed Production method unknown 1 0 0 0 0 0

Fruits and nuts Bananas Unprocessed Production method unknown 2 1 0 0 0 0

Fruits and nuts Grapefruit Unprocessed Production method unknown 1 0 0 0 0 0

Fruits and nuts Lemons Unprocessed Production method unknown 2 2 0 0 0 0

Fruits and nuts Mandarins Unprocessed Production method unknown 16 8 0 16 6 0

Fruits and nuts Oranges Unprocessed Production method unknown 15 7 0 15 6 0

Fruits and nuts Peaches Unprocessed Production method unknown 1 0 0 0 0 0

Fruits and nuts Pears Unprocessed Production method unknown 8 1 0 8 1 0

Fruits and nuts Table grapes Unprocessed Production method unknown 4 2 0 0 0 0

Vegetables Carrots Unprocessed Production method unknown 1 0 0 1 0 0

Vegetables Peppers Unprocessed Production method unknown 1 0 0 0 0 0

Origin 54 22 0 41 14 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 98Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=EEA Country=Hungary

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Baby food Baby food for infants and young childern Processed Production method unknown 1 0 0 0 0 0

Vegetables Peas (without pods) Freezing Production method unknown 1 0 0 0 0 0

Origin 2 0 0 0 0 0

Strategy=Surveillance Origin=EEA Country=Italy

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Pears Unprocessed Production method unknown 2 1 0 2 1 0

Vegetables Tomatoes Unprocessed Production method unknown 1 0 0 0 0 0

Origin 3 1 0 2 1 0

Strategy=Surveillance Origin=EEA Country=Poland

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Apples Unprocessed Production method unknown 5 0 0 0 0 0

Vegetables Peas (without pods) Freezing Production method unknown 1 0 0 0 0 0

Origin 6 0 0 0 0 0

Strategy=Surveillance Origin=EEA Country=Romania

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Cereals Rice Polishing Production method unknown 2 0 0 0 0 0

Vegetables Carrots Unprocessed Production method unknown 1 0 0 1 0 0

Origin 3 0 0 1 0 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 99Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=EEA Country=Slovakia

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Baby food Baby food for infants and young childern Processed Production method unknown 1 0 0 0 0 0

Strategy=Surveillance Origin=EEA Country=Spain

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Cereals Rice Unprocessed Production method unknown 1 1 0 1 1 0

Fruits and nuts Pears Unprocessed Production method unknown 1 0 0 1 0 0

Vegetables Cucumbers Unprocessed Production method unknown 1 1 0 1 1 0

Vegetables Peppers Unprocessed Production method unknown 2 0 0 0 0 0

Origin 5 2 0 3 2 0

Region 85 29 0 54 21 0

Strategy=Surveillance Origin=TC Country=Albania

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Vegetables Cucumbers Unprocessed Production method unknown 1 1 0 1 1 0

Strategy=Surveillance Origin=TC Country=Argentina

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Bananas Unprocessed Production method unknown 1 0 0 0 0 0

Strategy=Surveillance Origin=TC Country=Brazil

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Animal products Poultry liver Freezing Production method unknown 1 0 0 1 0 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 100Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=TC Country=Burundi

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Vegetables Beans (with pods) Freezing Production method unknown 2 1 0 2 1 0

Vegetables Peas (with pods) Freezing Production method unknown 1 0 0 0 0 0

Origin 3 1 0 2 1 0

Strategy=Surveillance Origin=TC Country=Colombia

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Bananas Unprocessed Production method unknown 1 0 0 0 0 0

Strategy=Surveillance Origin=TC Country=Costa Rica

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Bananas Unprocessed Production method unknown 1 0 0 0 0 0

Strategy=Surveillance Origin=TC Country=Ecuador

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Bananas Unprocessed Production method unknown 17 1 0 0 0 0

Strategy=Surveillance Origin=TC Country=Egypt

ProductClass Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Cereals Rice Polishing Production method unknown 2 0 0 0 0 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 101Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=TC Country=Macedonia, The Former Yugoslav Republic of

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Cereals Rice Unprocessed Production method unknown 1 0 0 1 0 0

Fruits and nuts Grapefruit Unprocessed Production method unknown 1 1 0 0 0 0

Vegetables Head cabbage Unprocessed Production method unknown 1 1 0 0 0 0

Vegetables Leek Unprocessed Production method unknown 1 1 0 0 0 0

Vegetables Peppers Unprocessed Production method unknown 3 0 0 0 0 0

Origin 7 3 0 1 0 0

Strategy=Surveillance Origin=TC Country=South Africa

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Oranges Unprocessed Production method unknown 1 0 0 1 0 0

Fruits and nuts Pears Unprocessed Production method unknown 2 1 1 2 1 1

Origin 3 1 1 3 1 1

Strategy=Surveillance Origin=TC Country=Tokelau

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Lemons Unprocessed Production method unknown 1 1 0 0 0 0

Strategy=Surveillance Origin=TC Country=Turkey

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Grapefruit Unprocessed Production method unknown 1 1 0 0 0 0

Fruits and nuts Lemons Unprocessed Production method unknown 13 6 0 0 0 0

Fruits and nuts Mandarins Unprocessed Production method unknown 4 4 0 4 4 0

Fruits and nuts Oranges Unprocessed Production method unknown 2 1 1 2 1 1

Vegetables Aubergines (egg plants) Unprocessed Production method unknown 2 0 0 0 0 0

Vegetables Carrots Unprocessed Production method unknown 5 3 0 5 3 0

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EUTotal = number of samples in EU programme, EUND = number of detections in EU programme, EUEx = number of exceedences in EU programme

Total = total samples in national and EU programe, ND= number of detections in national and EU programme, Ex number of MRL exceedences in national and EUprogramme

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 102Table A4: Overview of samples taken in National and EU co-ordinated programmes

Strategy=Surveillance Origin=TC Country=Turkey

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Vegetables Courgettes Unprocessed Production method unknown 2 0 0 0 0 0

Vegetables Cucumbers Unprocessed Production method unknown 1 1 0 1 0 0

Origin 30 16 1 12 8 1

Region 68 24 2 20 11 2

Strategy=Surveillance Origin=UNK Country=Non domestic, import

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Fruits and nuts Bananas Unprocessed Production method unknown 1 0 0 0 0 0

Fruits and nuts Table grapes Unprocessed Production method unknown 1 1 0 0 0 0

Origin 2 1 0 0 0 0

Strategy=Surveillance Origin=UNK Country=Unknown

Product Class Product Treatment Production Method Total ND Ex EUTotal EUND EUEx

Cereals Rice Unprocessed Production method unknown 1 0 0 1 0 0

Fruits and nuts Bananas Unprocessed Production method unknown 1 1 0 0 0 0

Fruits and nuts Grapefruit Unprocessed Production method unknown 1 1 0 0 0 0

Origin 3 2 0 1 0 0

Region 5 3 0 1 0 0

Strategy 461 143 11 254 61 5

4516 353 108 254 61 5

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Figures in bold totals for all countries

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 103Table A5: Overview of country of origin for samples taken in National and EU co-ordinated programmes

Figures in bold totals for all countries

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 103Table A5: Overview of country of origin for samples taken in National and EU co-ordinated programmes

ProductType=Animal products

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Brazil 1 1 0 0 0

Bulgaria 41 41 0 0 0

ProductType 42 42 0 0 0

ProductType=Baby food

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Bulgaria 17 15 0 2 2

Germany 1 1 0 0 0

Greece 1 1 0 0 0

Hungary 1 1 0 0 0

Slovakia 1 1 0 0 0

ProductType 21 19 0 2 2

ProductType=Cereals

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Bulgaria 43 38 5 0 0

Egypt 2 2 0 0 0

European Union 2 2 0 0 0

Greece 1 0 1 0 0

Macedonia, The Former Yugoslav Republic of 1 1 0 0 0

Romania 2 2 0 0 0

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Figures in bold totals for all countries

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 104Table A5: Overview of country of origin for samples taken in National and EU co-ordinated programmes

ProductType=Cereals

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Spain 1 0 1 0 0

Unknown 1 1 0 0 0

ProductType 53 46 7 0 0

ProductType=Fruits and nuts

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Argentina 1 1 0 0 0

Belgium 2 0 2 0 0

Bulgaria 42 19 21 2 2

Colombia 1 1 0 0 0

Costa Rica 1 1 0 0 0

Ecuador 17 16 1 0 0

France 1 0 1 0 0

Greece 50 29 21 0 0

Italy 2 1 1 0 0

Macedonia, The Former Yugoslav Republic of 1 0 1 0 0

Non domestic, import 2 1 1 0 0

Poland 5 5 0 0 0

South Africa 3 2 0 1 1

Spain 1 1 0 0 0

Tokelau 1 0 1 0 0

Turkey 20 8 11 1 1

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Figures in bold totals for all countries

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 105Table A5: Overview of country of origin for samples taken in National and EU co-ordinated programmes

ProductType=Fruits and nuts

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Unknown 2 0 2 0 0

ProductType 152 85 63 4 4

ProductType=Vegetables

Country TotalBelowLOQ

BetweenLOQand

MRLExceeding

MRLNon

Compliant

Albania 1 0 1 0 0

Belgium 3 3 0 0 0

Bulgaria 160 103 52 5 5

Burundi 3 2 1 0 0

France 1 1 0 0 0

Germany 1 0 1 0 0

Greece 2 2 0 0 0

Hungary 1 1 0 0 0

Italy 1 1 0 0 0

Macedonia, The Former Yugoslav Republic of 5 3 2 0 0

Poland 1 1 0 0 0

Romania 1 1 0 0 0

Spain 3 2 1 0 0

Turkey 4065 3851 117 97 97

ProductType 4248 3971 175 102 102

4516 4163 245 108 108

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 106Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 2 2 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 5 5 0 0 0.025 0.013 0.005 0.01 0

Aldicarb 0.010 0.050 5 5 0 0 0.025 0.013 0.005 . 0

Azinphos-methyl 0.010 0.020 14 14 0 0 0.010 0.006 0.005 0.05 0

Azoxystrobin 0.005 0.010 14 14 0 0 0.005 0.005 0.005 . 0

Benomyl 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.5 0

Bitertanol 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 5 5 0 0 0.005 0.005 0.005 2 0

Bromopropylate 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.01 0

Bupirimate 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.005 0.010 14 14 0 0 0.005 0.005 0.005 1 0

Carbaryl 0.010 0.050 5 5 0 0 0.025 0.013 0.005 0.05 0

Carbendazim and benomyl 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.2 0

Carbofuran 0.010 0.050 5 5 0 0 0.025 0.013 0.005 . 0

Chlorfenapyr 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 7 7 0 0 0.005 0.005 0.005 0.02 0

Chlorothalonil 0.005 0.020 14 14 0 0 0.010 0.006 0.005 5 0

Chlorpropham (sum) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.05 0

Clofentezine 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.02 0

Cyfluthrin (sum) 0.010 0.020 7 7 0 0 0.010 0.009 0.010 . 0

Cypermethrin (sum) 0.010 0.020 7 7 0 0 0.010 0.009 0.010 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 107Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyproconazole 0.020 0.020 2 2 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.005 0.010 14 14 0 0 0.005 0.005 0.005 2 0

Deltamethrin 0.005 0.020 14 14 0 0 0.010 0.006 0.005 0.2 0

Diazinon 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.005 0.020 9 9 0 0 0.010 0.006 0.005 . 0

Dichlorvos 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 5 5 0 0 0.005 0.005 0.005 2 0

Dicofol (sum) 0.010 0.010 11 11 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.005 0.030 9 9 0 0 0.015 0.007 0.005 1 0

Dimethoate 0.010 0.020 7 7 0 0 0.010 0.006 0.005 . 0

0.020 0.020 1 0 0 1 0.040 0.040 0.040 0.02 1

Dimethoate (sum) 0.010 0.010 5 4 1 0 0.018 0.008 0.005 0.02 0

Dimethomorph 0.010 0.010 7 7 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.010 0.050 3 3 0 0 0.025 0.018 0.025 0.05 0

Diphenylamine 0.005 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 2 2 0 0 0.025 0.025 0.025 1 0

Endosulfan (sum) 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 5 5 0 0 0.010 0.007 0.005 0.05 0

Ethion 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 14 14 0 0 0.010 0.006 0.005 0.02 0

Fenazaquin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Fenhexamid 0.010 0.020 12 12 0 0 0.010 0.006 0.005 2 0

Fenitrothion 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 108Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenoxycarb 0.010 0.020 5 5 0 0 0.010 0.007 0.005 0.05 0

Fenpropathrin 0.020 0.020 2 2 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 2 2 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 5 5 0 0 0.005 0.004 0.005 . 0

Fludioxonil 0.010 0.010 6 6 0 0 0.005 0.005 0.005 1 0

Flufenoxuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.5 0

Flusilazole 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.02 0

Hexaconazole 0.005 0.020 9 9 0 0 0.010 0.006 0.005 0.02 0

Hexythiazox 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.010 0.020 5 5 0 0 0.010 0.007 0.005 . 0

Imidacloprid 0.010 0.050 5 5 0 0 0.025 0.013 0.005 2 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 5 5 0 0 0.010 0.007 0.005 0.02 0

Iprodione 0.010 0.020 10 10 0 0 0.010 0.006 0.005 5 0

Iprovalicarb 0.010 0.020 5 5 0 0 0.010 0.007 0.005 0.05 0

Kresoxim-methyl 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.020 14 14 0 0 0.010 0.006 0.005 0.2 0

Linuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 7 7 0 0 0.010 0.006 0.005 0.02 0

Mepanipyrim 0.020 0.020 2 2 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 7 7 0 0 0.010 0.006 0.005 0.05 0

Metconazole 0.020 0.020 2 2 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.010 0.020 5 5 0 0 0.010 0.007 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 109Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methidathion 0.005 0.020 9 9 0 0 0.010 0.006 0.005 0.02 0

Methiocarb 0.010 0.050 10 10 0 0 0.025 0.009 0.005 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.2 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 5 5 0 0 0.025 0.013 0.005 . 0

Methoxyfenozide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.2 0

Monocrotophos 0.010 0.020 5 5 0 0 0.010 0.007 0.005 0 0

Myclobutanil 0.005 0.010 9 9 0 0 0.005 0.005 0.005 0.3 0

Oxadixyl 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.010 0.050 7 7 0 0 0.025 0.011 0.005 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Parathion 0.005 0.010 9 9 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.005 0.010 10 10 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.010 0.020 14 14 0 0 0.010 0.006 0.005 0.05 0

Pencycuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.010 0.020 14 14 0 0 0.010 0.006 0.005 0.05 0

Phosmet 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.010 0.010 8 8 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.005 0.010 6 6 0 0 0.005 0.005 0.005 1 0

Pirimiphos-methyl 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.05 0

Prochloraz 0.010 0.050 5 5 0 0 0.025 0.013 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 110Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.005 0.020 14 14 0 0 0.010 0.006 0.005 . 0

Profenofos 0.005 0.020 14 14 0 0 0.010 0.006 0.005 0.05 0

Propargite 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.01 0

Propiconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Pyrethrins 0.050 0.050 2 2 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 5 5 0 0 0.025 0.013 0.005 0.5 0

Pyrimethanil 0.005 0.010 12 12 0 0 0.005 0.005 0.005 2 0

Pyriproxyfen 0.005 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Quinoxyfen 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.5 0

Spiroxamine 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.010 0.020 9 9 0 0 0.010 0.006 0.005 2 0

Tebufenozide 0.010 0.050 10 10 0 0 0.025 0.009 0.005 0.05 0

Tebufenpyrad 0.005 0.010 12 12 0 0 0.005 0.005 0.005 1 0

Teflubenzuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Tetraconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Tetradifon 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.050 5 5 0 0 0.025 0.013 0.005 0.05 0

Thiacloprid 0.010 0.050 5 5 0 0 0.025 0.013 0.005 1 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 111Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Tolclofos-methyl 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.1 0

Tolylfluanid 0.010 0.020 9 9 0 0 0.010 0.006 0.005 . 0

0.010 0.010 1 0 1 0 0.020 0.020 0.020 3 0

Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed astolylfluanid)

0.005 0.010 2 2 0 0 0.005 0.004 0.004 3 0

Triadimefon 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 8 8 0 0 0.010 0.008 0.010 0.1 0

Triazophos 0.005 0.010 9 9 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 5 5 0 0 0.010 0.007 0.005 0.5 0

Trifluralin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.5 0

Vinclozolin 0.010 0.010 13 13 0 0 0.005 0.005 0.005 . 0

alpha-Endosulfan 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

beta-Endosulfan 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 112Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.01 0

Aldicarb 0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Azinphos-methyl 0.009 0.020 13 13 0 0 0.010 0.009 0.010 0.05 0

Azoxystrobin 0.010 0.010 12 12 0 0 0.005 0.005 0.005 . 0

Benomyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.006 0.010 13 13 0 0 0.005 0.005 0.005 0.5 0

Boscalid 0.010 0.010 10 10 0 0 0.005 0.005 0.005 2 0

Bromopropylate 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Bupirimate 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.005 0.010 13 13 0 0 0.005 0.005 0.005 1 0

Carbaryl 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 10 10 0 0 0.005 0.005 0.005 0.2 0

Carbofuran 0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Chlorfenapyr 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 2 2 0 0 0.005 0.004 0.004 0.02 0

Chlorothalonil 0.010 0.020 12 12 0 0 0.010 0.009 0.010 5 0

Chlorpropham (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.006 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Cyfluthrin (sum) 0.009 0.020 12 12 0 0 0.010 0.009 0.010 . 0

Cypermethrin (sum) 0.006 0.020 11 11 0 0 0.010 0.009 0.010 . 0

0.020 0.020 1 0 1 0 0.030 0.030 0.030 0.7 0

Cyproconazole 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 113Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyprodinil 0.005 0.010 13 13 0 0 0.005 0.005 0.005 2 0

Deltamethrin 0.009 0.020 13 13 0 0 0.010 0.009 0.010 0.2 0

Diazinon 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

Dichlorvos 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 1 1 0 0 0.005 0.005 0.005 2 0

Dicofol (sum) 0.008 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 10 10 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.009 0.030 12 12 0 0 0.015 0.013 0.015 1 0

Dimethoate 0.005 0.020 12 12 0 0 0.010 0.009 0.010 . 0

Dimethoate (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.009 0.050 2 2 0 0 0.025 0.015 0.015 0.05 0

Diphenylamine 0.005 0.010 3 3 0 0 0.005 0.004 0.005 0.05 0

Dithiocarbamates 0.050 0.050 10 9 1 0 0.888 0.111 0.025 1 0

Endosulfan (sum) 0.006 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

Ethion 0.006 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 13 13 0 0 0.010 0.009 0.010 0.02 0

Fenhexamid 0.010 0.020 12 12 0 0 0.010 0.009 0.010 2 0

Fenitrothion 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Fenoxycarb 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

Fenpropathrin 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 114Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fipronil 0.005 0.005 10 10 0 0 0.003 0.003 0.003 . 0

Fludioxonil 0.010 0.010 1 1 0 0 0.005 0.005 0.005 1 0

Flusilazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Hexaconazole 0.007 0.020 12 12 0 0 0.010 0.009 0.010 0.02 0

Hexythiazox 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

Imidacloprid 0.050 0.050 10 10 0 0 0.025 0.025 0.025 2 0

Indoxacarb as sum of the isomers S and R 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.02 0

Iprodione 0.010 0.020 12 12 0 0 0.010 0.009 0.010 5 0

Iprovalicarb 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

Kresoxim-methyl 0.007 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.020 13 13 0 0 0.010 0.009 0.010 0.2 0

Malathion 0.006 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.02 0

Mepanipyrim 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.05 0

Metconazole 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

Methidathion 0.006 0.020 12 12 0 0 0.010 0.009 0.010 0.02 0

Methiocarb 0.005 0.050 12 12 0 0 0.025 0.021 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.2 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 115Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Monocrotophos 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0 0

Myclobutanil 0.006 0.010 12 12 0 0 0.005 0.005 0.005 0.3 0

Oxamyl 0.009 0.050 12 12 0 0 0.025 0.022 0.025 0.01 0

Parathion 0.005 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 11 11 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.005 0.020 13 13 0 0 0.010 0.009 0.010 0.05 0

Phosalone 0.006 0.020 13 13 0 0 0.010 0.009 0.010 0.05 0

Phosmet 0.005 0.005 1 1 0 0 0.003 0.003 0.003 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 11 11 0 0 0.005 0.005 0.005 1 0

Pirimiphos-methyl 0.006 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Prochloraz 0.008 0.050 11 11 0 0 0.025 0.023 0.025 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.005 0.020 13 13 0 0 0.010 0.009 0.010 . 0

Profenofos 0.005 0.020 13 13 0 0 0.010 0.009 0.010 0.05 0

Propargite 0.005 0.010 3 3 0 0 0.005 0.004 0.005 0.01 0

Pyrethrins 0.050 0.050 10 10 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.5 0

Pyrimethanil 0.005 0.010 3 3 0 0 0.005 0.004 0.005 2 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 116Table B: Results of the EU co-ordinated programme

Product=Beans (with pods) Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Pyriproxyfen 0.005 0.010 3 3 0 0 0.005 0.004 0.005 0.05 0

Quinoxyfen 0.010 0.010 10 10 0 0 0.005 0.005 0.005 0.02 0

Spiroxamine 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.009 0.020 12 12 0 0 0.010 0.009 0.010 2 0

Tebufenozide 0.010 0.050 11 11 0 0 0.025 0.023 0.025 0.05 0

Tebufenpyrad 0.006 0.010 3 3 0 0 0.005 0.004 0.005 1 0

Tetradifon 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.05 0

Thiacloprid 0.050 0.050 10 10 0 0 0.025 0.025 0.025 1 0

Tolclofos-methyl 0.005 0.010 13 13 0 0 0.005 0.005 0.005 0.1 0

Tolylfluanid 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

Triadimefon 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.1 0

Triazophos 0.006 0.010 12 12 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.5 0

Trifluralin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Vinclozolin 0.005 0.010 13 13 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 117Table B: Results of the EU co-ordinated programme

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 117Table B: Results of the EU co-ordinated programme

Product=Bovine Liver Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Aldrin 0.000 0.000 5 5 0 0 0.000 0.000 0.000 . 0

DDD, p,p- 0.001 0.001 5 5 0 0 0.000 0.000 0.000 . 0

DDE, p,p- 0.001 0.001 5 5 0 0 0.001 0.001 0.001 . 0

DDT, p,p- 0.001 0.001 5 5 0 0 0.001 0.001 0.001 . 0

Hexachlorocyclohexane (HCH), alpha-isomer 0.001 0.001 5 5 0 0 0.000 0.000 0.000 0.2 0

Hexachlorocyclohexane (HCH), beta-isomer 0.001 0.001 5 5 0 0 0.001 0.001 0.001 0.1 0

Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0.001 0.001 5 5 0 0 0.001 0.001 0.001 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 118Table B: Results of the EU co-ordinated programme

Product=Carrots Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 16 16 0 0 0.025 0.024 0.025 0.01 0

Aldicarb 0.010 0.050 16 16 0 0 0.025 0.024 0.025 . 0

Azinphos-methyl 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.05 0

Azoxystrobin 0.010 0.010 21 21 0 0 0.005 0.005 0.005 . 0

Benomyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.010 0.010 21 20 1 0 0.020 0.006 0.005 0.05 0

Bitertanol 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 15 15 0 0 0.005 0.005 0.005 1 0

0.010 0.010 1 0 1 0 0.015 0.015 0.015 2 0

Bromopropylate 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.05 0

Captan 0.010 0.050 20 20 0 0 0.025 0.020 0.025 0.1 0

Carbaryl 0.010 0.050 16 16 0 0 0.025 0.024 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 16 15 1 0 0.014 0.006 0.005 0.1 0

Carbofuran 0.010 0.050 16 16 0 0 0.025 0.024 0.025 . 0

Chlorfenapyr 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.5 0

Chlorothalonil 0.010 0.020 21 21 0 0 0.010 0.009 0.010 1 0

Chlorpropham (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.010 0.010 21 17 3 1 0.216 0.022 0.005 0.1 1

Chlorpyrifos-methyl 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.05 0

Clofentezine 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 119Table B: Results of the EU co-ordinated programme

Product=Carrots Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyfluthrin (sum) 0.010 0.020 17 17 0 0 0.010 0.010 0.010 0.02 0

Cypermethrin (sum) 0.010 0.020 17 17 0 0 0.010 0.010 0.010 0.05 0

Cyproconazole 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.010 0.010 21 21 0 0 0.005 0.005 0.005 2 0

Deltamethrin 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.05 0

Diazinon 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.010 0.020 19 19 0 0 0.010 0.009 0.010 . 0

Dichlorvos 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.1 0

Dicofol (sum) 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 15 15 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.010 0.030 17 17 0 0 0.015 0.014 0.015 0.3 0

Dimethoate 0.010 0.020 19 19 0 0 0.010 0.009 0.010 . 0

Dimethoate (sum) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.050 0.050 1 1 0 0 0.025 0.025 0.025 0.05 0

Diphenylamine 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 15 15 0 0 0.025 0.025 0.025 0.2 0

Endosulfan (sum) 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0.05 0

Ethion 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.02 0

Fenazaquin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

Fenhexamid 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 120Table B: Results of the EU co-ordinated programme

Product=Carrots Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenitrothion 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.01 0

Fenoxycarb 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0.05 0

Fenpropathrin 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 15 15 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 16 16 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 2 2 0 0 0.005 0.005 0.005 1 0

Flufenoxuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Flusilazole 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Folpet 0.010 0.050 20 20 0 0 0.025 0.020 0.025 0.02 0

Hexaconazole 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.02 0

Hexythiazox 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.010 0.020 16 16 0 0 0.010 0.010 0.010 . 0

Imidacloprid 0.010 0.050 16 16 0 0 0.025 0.024 0.025 . 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0.02 0

Iprodione 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.5 0

Iprovalicarb 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0.05 0

Kresoxim-methyl 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.02 0

Linuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.2 0

Malathion 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.02 0

Mepanipyrim 0.020 0.020 15 15 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 121Table B: Results of the EU co-ordinated programme

Product=Carrots Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Metconazole 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0.01 0

Methidathion 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.02 0

Methiocarb 0.010 0.050 20 20 0 0 0.025 0.020 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 16 16 0 0 0.025 0.024 0.025 . 0

Methoxyfenozide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Monocrotophos 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0 0

Myclobutanil 0.010 0.010 17 17 0 0 0.005 0.005 0.005 0.2 0

Oxadixyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Oxamyl 0.010 0.050 17 17 0 0 0.025 0.023 0.025 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Parathion 0.010 0.010 17 17 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 16 16 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.05 0

Pencycuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.05 0

Phosmet 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 16 16 0 0 0.005 0.005 0.005 0.5 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 122Table B: Results of the EU co-ordinated programme

Product=Carrots Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Pirimiphos-methyl 0.010 0.010 21 21 0 0 0.005 0.005 0.005 1 0

Prochloraz 0.010 0.050 16 16 0 0 0.025 0.024 0.025 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.02 0

Profenofos 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.05 0

Propargite 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.01 0

Propiconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Pyrethrins 0.050 0.050 15 15 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 16 16 0 0 0.025 0.024 0.025 0.05 0

Pyrimethanil 0.010 0.010 6 6 0 0 0.005 0.005 0.005 1 0

Pyriproxyfen 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.05 0

Quinoxyfen 0.010 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Spiroxamine 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.5 0

Tebufenozide 0.010 0.050 20 20 0 0 0.025 0.020 0.025 0.05 0

Tebufenpyrad 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.05 0

Teflubenzuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Tetraconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Tetradifon 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.050 16 16 0 0 0.025 0.024 0.025 0.05 0

Thiacloprid 0.010 0.050 16 16 0 0 0.025 0.024 0.025 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 123Table B: Results of the EU co-ordinated programme

Product=Carrots Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.1 0

Tolclofos-methyl 0.010 0.010 21 21 0 0 0.005 0.005 0.005 0.5 0

Tolylfluanid 0.010 0.020 20 20 0 0 0.010 0.009 0.010 . 0

Triadimefon 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.010 0.020 17 17 0 0 0.010 0.010 0.010 0.1 0

Triazophos 0.010 0.010 17 17 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 16 16 0 0 0.010 0.010 0.010 0.05 0

Trifluralin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 1 0

Vinclozolin 0.010 0.010 21 21 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 124Table B: Results of the EU co-ordinated programme

Product=Cucumbers Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 15 15 0 0 0.025 0.024 0.025 0.3 0

Aldicarb 0.010 0.050 15 15 0 0 0.025 0.024 0.025 . 0

Azinphos-methyl 0.009 0.020 18 18 0 0 0.010 0.009 0.010 0.2 0

Azoxystrobin 0.010 0.010 17 17 0 0 0.005 0.005 0.005 1 0

Benomyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.006 0.010 18 16 2 0 0.040 0.008 0.005 0.1 0

Bitertanol 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Boscalid 0.010 0.010 1 0 1 0 0.021 0.021 0.021 3 0

0.010 0.010 14 14 0 0 0.005 0.005 0.005 0.2 0

Bromopropylate 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.005 0.010 18 18 0 0 0.005 0.005 0.005 1 0

Buprofezin 0.005 0.010 18 18 0 0 0.005 0.005 0.005 1 0

Captan 0.005 0.050 17 17 0 0 0.025 0.021 0.025 0.02 0

Carbaryl 0.010 0.050 15 15 0 0 0.025 0.024 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 15 15 0 0 0.005 0.005 0.005 0.1 0

Carbofuran 0.010 0.050 15 15 0 0 0.025 0.024 0.025 . 0

Chlorfenapyr 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 3 3 0 0 0.005 0.004 0.005 0.02 0

Chlorothalonil 0.010 0.020 17 17 0 0 0.010 0.009 0.010 1 0

Chlorpropham (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.006 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Clofentezine 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 125Table B: Results of the EU co-ordinated programme

Product=Cucumbers Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyfluthrin (sum) 0.009 0.020 17 17 0 0 0.010 0.009 0.010 0.1 0

Cypermethrin (sum) 0.006 0.020 17 16 1 0 0.030 0.011 0.010 0.2 0

Cyproconazole 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.5 0

Deltamethrin 0.009 0.020 18 18 0 0 0.010 0.009 0.010 0.2 0

Diazinon 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.010 0.020 15 15 0 0 0.010 0.010 0.010 . 0

Dichlorvos 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.3 0

Dicofol (sum) 0.008 0.010 4 4 0 0 0.005 0.005 0.005 0.2 0

Dicofol p, p' 0.010 0.010 14 14 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.009 0.030 17 17 0 0 0.015 0.013 0.015 0.1 0

Dimethoate 0.005 0.020 16 16 0 0 0.010 0.009 0.010 . 0

Dimethoate (sum) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 2 2 0 0 0.005 0.005 0.005 1 0

Dinocap (sum) 0.009 0.050 2 2 0 0 0.025 0.015 0.015 0.05 0

Diphenylamine 0.005 0.010 4 4 0 0 0.005 0.004 0.005 0.05 0

Dithiocarbamates 0.050 0.050 14 13 1 0 0.064 0.028 0.025 2 0

Endosulfan (sum) 0.006 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.05 0

Ethion 0.006 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 18 18 0 0 0.010 0.009 0.010 0.2 0

Fenazaquin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.2 0

Fenhexamid 0.010 0.020 17 17 0 0 0.010 0.009 0.010 1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 126Table B: Results of the EU co-ordinated programme

Product=Cucumbers Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenitrothion 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Fenoxycarb 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.05 0

Fenpropathrin 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 14 14 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 15 15 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 2 2 0 0 0.005 0.005 0.005 1 0

Flufenoxuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.2 0

Flusilazole 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Folpet 0.010 0.050 16 16 0 0 0.025 0.023 0.025 0.02 0

Hexaconazole 0.007 0.020 17 17 0 0 0.010 0.009 0.010 0.02 0

Hexythiazox 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.2 0

Imidacloprid 0.010 0.050 15 14 1 0 0.130 0.032 0.025 1 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.2 0

Iprodione 0.010 0.020 16 16 0 0 0.010 0.009 0.010 2 0

Iprovalicarb 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.1 0

Kresoxim-methyl 0.007 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.020 18 18 0 0 0.010 0.009 0.010 0.1 0

Linuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.006 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 16 16 0 0 0.010 0.009 0.010 0.02 0

Mepanipyrim 0.020 0.020 14 14 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 15 15 0 0 0.010 0.009 0.010 0.5 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 127Table B: Results of the EU co-ordinated programme

Product=Cucumbers Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

0.020 0.020 1 0 1 0 0.025 0.025 0.025 0.05 0

Metconazole 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.01 0

Methidathion 0.006 0.020 17 17 0 0 0.010 0.009 0.010 0.05 0

Methiocarb 0.005 0.050 17 17 0 0 0.025 0.021 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.2 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 15 15 0 0 0.025 0.024 0.025 . 0

Methoxyfenozide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Monocrotophos 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0 0

Myclobutanil 0.006 0.010 17 17 0 0 0.005 0.005 0.005 0.1 0

Oxadixyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.009 0.050 17 17 0 0 0.025 0.021 0.025 0.02 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Parathion 0.005 0.010 17 17 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.005 0.010 3 3 0 0 0.005 0.004 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.005 0.020 18 18 0 0 0.010 0.009 0.010 0.1 0

Pencycuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.006 0.020 18 18 0 0 0.010 0.009 0.010 0.05 0

Phosmet 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.005 0.010 3 3 0 0 0.005 0.004 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 128Table B: Results of the EU co-ordinated programme

Product=Cucumbers Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 15 15 0 0 0.005 0.005 0.005 1 0

Pirimiphos-methyl 0.006 0.010 18 18 0 0 0.005 0.005 0.005 0.1 0

Prochloraz 0.008 0.050 16 16 0 0 0.025 0.022 0.025 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.005 0.020 18 18 0 0 0.010 0.009 0.010 . 0

Profenofos 0.005 0.020 18 18 0 0 0.010 0.009 0.010 0.05 0

Propargite 0.005 0.010 4 4 0 0 0.005 0.004 0.005 0.01 0

Propiconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Pyrethrins 0.050 0.050 14 14 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 15 15 0 0 0.025 0.024 0.025 0.1 0

Pyrimethanil 0.005 0.010 4 4 0 0 0.005 0.004 0.005 1 0

Pyriproxyfen 0.005 0.010 4 4 0 0 0.005 0.004 0.005 0.1 0

Quinoxyfen 0.010 0.010 14 14 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 1 0

Spiroxamine 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.009 0.020 17 17 0 0 0.010 0.009 0.010 0.5 0

Tebufenozide 0.010 0.050 16 16 0 0 0.025 0.023 0.025 0.05 0

Tebufenpyrad 0.006 0.010 4 4 0 0 0.005 0.005 0.005 0.1 0

Teflubenzuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Tetraconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.2 0

Tetradifon 0.005 0.010 18 18 0 0 0.005 0.005 0.005 2 0

Thiabendazole 0.010 0.050 15 15 0 0 0.025 0.024 0.025 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 129Table B: Results of the EU co-ordinated programme

Product=Cucumbers Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Thiacloprid 0.010 0.050 15 15 0 0 0.025 0.024 0.025 0.3 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.1 0

Tolclofos-methyl 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.010 0.020 16 16 0 0 0.010 0.009 0.010 . 0

Triadimefon 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.010 0.020 16 16 0 0 0.010 0.010 0.010 . 0

Triazophos 0.006 0.010 17 17 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 15 15 0 0 0.010 0.010 0.010 0.2 0

Trifluralin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Vinclozolin 0.005 0.010 18 18 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 130Table B: Results of the EU co-ordinated programme

Product=Mandarins Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 5 5 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 8 8 0 0 0.025 0.018 0.025 1 0

Aldicarb 0.010 0.050 8 8 0 0 0.025 0.018 0.025 . 0

Azinphos-methyl 0.007 0.020 20 20 0 0 0.010 0.006 0.005 0.05 0

Azoxystrobin 0.005 0.010 20 20 0 0 0.005 0.005 0.005 . 0

Benomyl 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.005 0.010 20 16 4 0 0.080 0.017 0.005 0.1 0

Bitertanol 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.05 0

Bromopropylate 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.01 0

Bupirimate 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.005 0.010 20 20 0 0 0.005 0.005 0.005 1 0

Captan 0.005 0.050 17 17 0 0 0.025 0.011 0.005 0.02 0

Carbaryl 0.010 0.050 8 8 0 0 0.025 0.018 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 8 8 0 0 0.005 0.005 0.005 . 0

Carbofuran 0.010 0.050 8 8 0 0 0.025 0.018 0.025 . 0

Chlorfenapyr 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 9 9 0 0 0.005 0.004 0.005 0.02 0

Chlorothalonil 0.005 0.020 18 18 0 0 0.010 0.006 0.005 0.01 0

Chlorpropham (sum) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.005 0.010 20 17 3 0 0.347 0.036 0.005 2 0

Chlorpyrifos-methyl 0.005 0.010 20 19 1 0 0.154 0.012 0.005 1 0

Clofentezine 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.5 0

Cyfluthrin (sum) 0.009 0.020 12 12 0 0 0.010 0.008 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 131Table B: Results of the EU co-ordinated programme

Product=Mandarins Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cypermethrin (sum) 0.006 0.020 12 12 0 0 0.010 0.008 0.010 2 0

Cyproconazole 0.020 0.020 5 5 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.05 0

Deltamethrin 0.005 0.020 20 20 0 0 0.010 0.006 0.005 0.05 0

Diazinon 0.005 0.010 19 19 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.005 0.020 13 13 0 0 0.010 0.007 0.005 . 0

Dichlorvos 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.1 0

Dicofol (sum) 0.005 0.010 14 14 0 0 0.005 0.005 0.005 2 0

Dicofol p, p' 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.005 0.030 14 14 0 0 0.015 0.008 0.005 0.1 0

Dimethoate 0.007 0.020 14 14 0 0 0.010 0.007 0.005 . 0

Dimethoate (sum) 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.008 0.010 9 9 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.009 0.050 5 5 0 0 0.025 0.013 0.005 0.05 0

Diphenylamine 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 5 5 0 0 0.025 0.025 0.025 5 0

Endosulfan (sum) 0.005 0.010 19 19 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 8 8 0 0 0.010 0.008 0.010 0.05 0

Ethion 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 20 20 0 0 0.010 0.006 0.005 0.02 0

Fenazaquin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.5 0

Fenhexamid 0.010 0.020 16 16 0 0 0.010 0.007 0.005 0.05 0

Fenitrothion 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 132Table B: Results of the EU co-ordinated programme

Product=Mandarins Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenoxycarb 0.010 0.020 8 8 0 0 0.010 0.008 0.010 2 0

Fenpropathrin 0.020 0.020 5 5 0 0 0.010 0.010 0.010 2 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 5 5 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 8 8 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 6 6 0 0 0.005 0.005 0.005 7 0

Flufenoxuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.3 0

Flusilazole 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.1 0

Folpet 0.010 0.050 15 15 0 0 0.025 0.012 0.005 0.02 0

Hexaconazole 0.005 0.020 14 14 0 0 0.010 0.006 0.005 0.02 0

Hexythiazox 0.010 0.010 9 9 0 0 0.005 0.005 0.005 1 0

Imazalil 0.010 0.020 8 4 4 0 1.410 0.469 0.015 5 0

Imidacloprid 0.010 0.050 8 8 0 0 0.025 0.018 0.025 1 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 8 8 0 0 0.010 0.008 0.010 0.02 0

Iprodione 0.010 0.020 14 14 0 0 0.010 0.007 0.005 1 0

Iprovalicarb 0.010 0.020 8 8 0 0 0.010 0.008 0.010 0.05 0

Kresoxim-methyl 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.020 20 18 2 0 0.025 0.007 0.005 0.2 0

Linuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.005 0.010 10 10 0 0 0.005 0.004 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 10 10 0 0 0.010 0.008 0.008 0.02 0

Mepanipyrim 0.020 0.020 5 5 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.010 10 10 0 0 0.005 0.004 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 10 10 0 0 0.010 0.008 0.008 0.5 0

Metconazole 0.020 0.020 5 5 0 0 0.010 0.010 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 133Table B: Results of the EU co-ordinated programme

Product=Mandarins Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methamidophos 0.010 0.020 8 8 0 0 0.010 0.008 0.010 0.01 0

Methidathion 0.005 0.020 14 14 0 0 0.010 0.006 0.005 5 0

Methiocarb 0.005 0.050 16 16 0 0 0.025 0.011 0.005 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.2 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 8 8 0 0 0.025 0.018 0.025 . 0

Methoxyfenozide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Monocrotophos 0.010 0.020 8 8 0 0 0.010 0.008 0.010 0 0

Myclobutanil 0.005 0.010 14 14 0 0 0.005 0.004 0.005 3 0

Oxadixyl 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.008 0.050 12 12 0 0 0.025 0.013 0.005 0.02 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Parathion 0.005 0.010 14 14 0 0 0.005 0.004 0.005 0.05 0

Parathion-methyl 0.005 0.010 13 13 0 0 0.005 0.004 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 7 7 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.005 0.020 20 20 0 0 0.010 0.006 0.005 0.05 0

Pencycuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.005 0.020 20 20 0 0 0.010 0.006 0.005 0.05 0

Phosmet 0.005 0.010 5 5 0 0 0.005 0.004 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.2 0

Pirimicarb 0.005 0.010 11 11 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.005 0.010 9 9 0 0 0.005 0.005 0.005 3 0

Pirimiphos-methyl 0.005 0.010 20 20 0 0 0.005 0.005 0.005 2 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 134Table B: Results of the EU co-ordinated programme

Product=Mandarins Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Prochloraz 0.008 0.050 10 10 0 0 0.025 0.015 0.015 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 10 0

Procymidone 0.005 0.020 20 20 0 0 0.010 0.006 0.005 0.02 0

Profenofos 0.005 0.020 20 20 0 0 0.010 0.006 0.005 0.05 0

Propargite 0.005 0.010 15 15 0 0 0.005 0.005 0.005 3 0

Propiconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Pyrethrins 0.050 0.050 5 5 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 8 8 0 0 0.025 0.018 0.025 0.5 0

Pyrimethanil 0.005 0.010 15 15 0 0 0.005 0.005 0.005 10 0

Pyriproxyfen 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.6 0

Quinoxyfen 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.3 0

Spiroxamine 0.010 0.010 9 9 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.009 0.020 14 14 0 0 0.010 0.007 0.005 . 0

Tebufenozide 0.010 0.050 14 14 0 0 0.025 0.012 0.005 2 0

Tebufenpyrad 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.5 0

Teflubenzuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Tetraconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Tetradifon 0.005 0.010 20 20 0 0 0.005 0.005 0.005 2 0

Thiabendazole 0.010 0.050 8 7 1 0 0.910 0.128 0.025 5 0

Thiacloprid 0.010 0.050 8 8 0 0 0.025 0.018 0.025 0.02 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 135Table B: Results of the EU co-ordinated programme

Product=Mandarins Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Thiophanate-methyl 0.020 0.020 3 3 0 0 0.010 0.010 0.010 . 0

Tolclofos-methyl 0.005 0.010 20 20 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.009 0.020 16 16 0 0 0.010 0.007 0.005 . 0

Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed astolylfluanid)

0.005 0.010 2 2 0 0 0.005 0.004 0.004 0.05 0

Triadimefon 0.005 0.010 9 9 0 0 0.005 0.004 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 11 11 0 0 0.010 0.008 0.010 0.1 0

Triazophos 0.005 0.010 14 14 0 0 0.005 0.004 0.005 0.01 0

Trifloxystrobin 0.010 0.020 8 8 0 0 0.010 0.008 0.010 0.3 0

Trifluralin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Vinclozolin 0.005 0.010 19 19 0 0 0.005 0.005 0.005 . 0

alpha-Endosulfan 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

beta-Endosulfan 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 136Table B: Results of the EU co-ordinated programme

Product=Oranges Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 6 6 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 8 8 0 0 0.025 0.020 0.025 1 0

Aldicarb 0.010 0.050 8 8 0 0 0.025 0.020 0.025 . 0

Azinphos-methyl 0.010 0.020 18 18 0 0 0.010 0.007 0.005 0.05 0

Azoxystrobin 0.005 0.010 18 18 0 0 0.005 0.005 0.005 . 0

Benomyl 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.005 0.010 18 17 1 0 0.040 0.007 0.005 0.1 0

Bitertanol 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.05 0

Bromopropylate 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Bupirimate 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.005 0.010 18 18 0 0 0.005 0.005 0.005 1 0

Captan 0.005 0.050 16 16 0 0 0.025 0.012 0.005 0.02 0

Carbaryl 0.010 0.050 8 8 0 0 0.025 0.020 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.5 0

Carbofuran 0.010 0.050 8 8 0 0 0.025 0.020 0.025 . 0

Chlorfenapyr 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 10 10 0 0 0.005 0.005 0.005 0.02 0

Chlorothalonil 0.005 0.020 18 18 0 0 0.010 0.007 0.005 0.01 0

Chlorpropham (sum) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.005 0.010 18 16 2 0 0.058 0.009 0.005 0.3 0

Chlorpyrifos-methyl 0.005 0.010 18 17 1 0 0.030 0.006 0.005 0.5 0

Clofentezine 0.020 0.020 2 2 0 0 0.010 0.010 0.010 0.5 0

Cyfluthrin (sum) 0.010 0.020 11 11 0 0 0.010 0.009 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 137Table B: Results of the EU co-ordinated programme

Product=Oranges Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cypermethrin (sum) 0.010 0.020 11 11 0 0 0.010 0.009 0.010 2 0

Cyproconazole 0.020 0.020 6 6 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Deltamethrin 0.005 0.020 18 18 0 0 0.010 0.007 0.005 0.05 0

Diazinon 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.005 0.020 13 13 0 0 0.010 0.007 0.005 . 0

Dichlorvos 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Dicofol (sum) 0.010 0.010 11 11 0 0 0.005 0.005 0.005 2 0

Dicofol p, p' 0.010 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.005 0.030 16 16 0 0 0.015 0.009 0.005 0.1 0

Dimethoate 0.010 0.020 12 12 0 0 0.010 0.008 0.008 . 0

Dimethoate (sum) 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 10 10 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.05 0

Diphenylamine 0.005 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 6 6 0 0 0.025 0.025 0.025 5 0

Endosulfan (sum) 0.005 0.010 14 14 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 8 8 0 0 0.010 0.009 0.010 0.05 0

Ethion 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 18 18 0 0 0.010 0.007 0.005 0.02 0

Fenazaquin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.5 0

Fenhexamid 0.010 0.020 13 13 0 0 0.010 0.007 0.005 0.05 0

Fenitrothion 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 138Table B: Results of the EU co-ordinated programme

Product=Oranges Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenoxycarb 0.010 0.020 8 8 0 0 0.010 0.009 0.010 2 0

Fenpropathrin 0.020 0.020 6 6 0 0 0.010 0.010 0.010 2 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 6 6 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 8 8 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 6 6 0 0 0.005 0.005 0.005 7 0

Flufenoxuron 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.3 0

Flusilazole 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.1 0

Folpet 0.010 0.050 16 16 0 0 0.025 0.013 0.010 0.02 0

Hexaconazole 0.005 0.020 16 16 0 0 0.010 0.007 0.005 0.02 0

Hexythiazox 0.010 0.010 4 4 0 0 0.005 0.005 0.005 1 0

Imazalil 0.010 0.020 8 4 3 1 11.550 1.926 0.415 5 1

Imidacloprid 0.010 0.050 8 8 0 0 0.025 0.020 0.025 1 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 8 8 0 0 0.010 0.009 0.010 0.02 0

Iprodione 0.010 0.020 15 15 0 0 0.010 0.007 0.005 0.02 0

Iprovalicarb 0.010 0.020 8 8 0 0 0.010 0.009 0.010 0.05 0

Kresoxim-methyl 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.020 18 18 0 0 0.010 0.007 0.005 . 0

Linuron 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 11 11 0 0 0.010 0.008 0.010 0.02 0

Mepanipyrim 0.020 0.020 6 6 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 11 11 0 0 0.010 0.008 0.010 0.5 0

Metconazole 0.020 0.020 6 6 0 0 0.010 0.010 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 139Table B: Results of the EU co-ordinated programme

Product=Oranges Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methamidophos 0.010 0.020 8 8 0 0 0.010 0.009 0.010 0.01 0

Methidathion 0.005 0.020 16 16 0 0 0.010 0.007 0.005 5 0

Methiocarb 0.010 0.050 10 10 0 0 0.025 0.017 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 8 8 0 0 0.025 0.020 0.025 . 0

Methoxyfenozide 0.010 0.010 2 2 0 0 0.005 0.005 0.005 1 0

Monocrotophos 0.010 0.020 8 8 0 0 0.010 0.009 0.010 0 0

Myclobutanil 0.005 0.010 16 16 0 0 0.005 0.005 0.005 3 0

Oxadixyl 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.010 0.050 11 11 0 0 0.025 0.016 0.025 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Parathion 0.005 0.010 16 16 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.005 0.010 9 9 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 9 9 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.010 0.020 18 17 1 0 0.040 0.009 0.005 0.05 0

Pencycuron 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.010 0.020 18 18 0 0 0.010 0.007 0.005 0.05 0

Phosmet 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.2 0

Pirimicarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.005 0.010 14 14 0 0 0.005 0.005 0.005 3 0

Pirimiphos-methyl 0.005 0.010 18 18 0 0 0.005 0.005 0.005 1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 140Table B: Results of the EU co-ordinated programme

Product=Oranges Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Prochloraz 0.010 0.050 7 7 0 0 0.025 0.019 0.025 . 0

0.050 0.050 1 0 1 0 0.274 0.274 0.274 10 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 7 7 0 0 0.005 0.005 0.005 10 0

Procymidone 0.005 0.020 18 18 0 0 0.010 0.007 0.005 0.02 0

Profenofos 0.005 0.020 18 18 0 0 0.010 0.007 0.005 0.05 0

Propargite 0.010 0.010 12 12 0 0 0.005 0.005 0.005 3 0

Propiconazole 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 1 0

Pyrethrins 0.050 0.050 6 6 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 8 8 0 0 0.025 0.020 0.025 0.5 0

Pyrimethanil 0.005 0.010 12 12 0 0 0.005 0.005 0.005 10 0

Pyriproxyfen 0.005 0.010 12 12 0 0 0.005 0.005 0.005 0.6 0

Quinoxyfen 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.3 0

Spiroxamine 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.010 0.020 16 16 0 0 0.010 0.007 0.005 0.05 0

Tebufenozide 0.010 0.050 10 10 0 0 0.025 0.017 0.025 2 0

Tebufenpyrad 0.005 0.010 12 12 0 0 0.005 0.005 0.005 0.5 0

Teflubenzuron 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Tetraconazole 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Tetradifon 0.005 0.010 18 18 0 0 0.005 0.005 0.005 2 0

Thiabendazole 0.010 0.050 8 8 0 0 0.025 0.020 0.025 5 0

Thiacloprid 0.010 0.050 8 8 0 0 0.025 0.020 0.025 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 141Table B: Results of the EU co-ordinated programme

Product=Oranges Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 2 2 0 0 0.010 0.010 0.010 . 0

Tolclofos-methyl 0.005 0.010 18 17 1 0 0.030 0.006 0.005 0.05 0

Tolylfluanid 0.010 0.020 10 10 0 0 0.010 0.008 0.010 . 0

Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed astolylfluanid)

0.005 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Triadimefon 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 12 12 0 0 0.010 0.008 0.010 0.1 0

Triazophos 0.005 0.010 16 16 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 8 8 0 0 0.010 0.009 0.010 0.3 0

Trifluralin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Vinclozolin 0.010 0.010 17 17 0 0 0.005 0.005 0.005 . 0

alpha-Endosulfan 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

beta-Endosulfan 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 142Table B: Results of the EU co-ordinated programme

Product=Pears Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 17 17 0 0 0.025 0.021 0.025 0.1 0

Aldicarb 0.010 0.050 17 17 0 0 0.025 0.021 0.025 . 0

Azinphos-methyl 0.009 0.020 26 26 0 0 0.010 0.008 0.010 0.05 0

Azoxystrobin 0.005 0.010 24 24 0 0 0.005 0.005 0.005 0.05 0

Benomyl 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.005 0.010 26 25 1 0 0.012 0.005 0.005 0.3 0

Bitertanol 0.010 0.010 3 3 0 0 0.005 0.005 0.005 2 0

Boscalid 0.010 0.010 17 17 0 0 0.005 0.005 0.005 2 0

Bromopropylate 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.01 0

Bupirimate 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.2 0

Buprofezin 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.5 0

Carbaryl 0.010 0.050 17 17 0 0 0.025 0.021 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 17 15 1 1 0.279 0.023 0.005 0.2 1

Carbofuran 0.010 0.050 17 17 0 0 0.025 0.021 0.025 . 0

Chlorfenapyr 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 10 10 0 0 0.005 0.004 0.005 0.02 0

Chlorothalonil 0.005 0.020 24 24 0 0 0.010 0.008 0.010 1 0

Chlorpropham (sum) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.5 0

Chlorpyrifos-methyl 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.5 0

Clofentezine 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.5 0

Cyfluthrin (sum) 0.009 0.020 22 22 0 0 0.010 0.009 0.010 0.2 0

Cypermethrin (sum) 0.006 0.020 22 22 0 0 0.010 0.009 0.010 1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 143Table B: Results of the EU co-ordinated programme

Product=Pears Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyproconazole 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.1 0

Cyprodinil 0.005 0.010 26 26 0 0 0.005 0.005 0.005 1 0

Deltamethrin 0.005 0.020 26 26 0 0 0.010 0.007 0.010 0.1 0

Diazinon 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.005 0.020 18 18 0 0 0.010 0.009 0.010 . 0

Dichlorvos 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Dicofol (sum) 0.008 0.010 10 10 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 16 16 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.005 0.030 24 24 0 0 0.015 0.011 0.015 0.5 0

Dimethoate 0.005 0.020 18 18 0 0 0.010 0.009 0.010 . 0

Dimethoate (sum) 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.009 0.050 7 7 0 0 0.025 0.013 0.005 0.05 0

Diphenylamine 0.005 0.010 12 12 0 0 0.005 0.004 0.005 10 0

Dithiocarbamates 0.050 0.050 14 13 1 0 0.150 0.034 0.025 5 0

Endosulfan (sum) 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.3 0

Epoxiconazole 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.05 0

Ethion 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 26 26 0 0 0.010 0.007 0.010 0.3 0

Fenazaquin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Fenhexamid 0.010 0.020 22 22 0 0 0.010 0.008 0.010 0.05 0

Fenitrothion 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.01 0

Fenoxycarb 0.010 0.020 17 17 0 0 0.010 0.009 0.010 1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 144Table B: Results of the EU co-ordinated programme

Product=Pears Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenpropathrin 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 14 14 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 17 17 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 8 8 0 0 0.005 0.005 0.005 5 0

Flufenoxuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.5 0

Flusilazole 0.010 0.010 8 8 0 0 0.005 0.005 0.005 0.02 0

Hexaconazole 0.005 0.020 24 24 0 0 0.010 0.008 0.010 0.1 0

Hexythiazox 0.010 0.010 5 5 0 0 0.005 0.005 0.005 1 0

Imazalil 0.010 0.020 17 16 1 0 0.439 0.034 0.010 2 0

Imidacloprid 0.010 0.050 17 16 1 0 0.110 0.028 0.025 0.5 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.3 0

Iprodione 0.010 0.020 19 19 0 0 0.010 0.009 0.010 5 0

Iprovalicarb 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.05 0

Kresoxim-methyl 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.2 0

Lambda-Cyhalothrin 0.005 0.020 26 26 0 0 0.010 0.007 0.010 0.1 0

Linuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.005 0.010 6 6 0 0 0.005 0.004 0.003 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.02 0

Mepanipyrim 0.020 0.020 14 14 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.010 6 6 0 0 0.005 0.003 0.003 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 20 20 0 0 0.010 0.009 0.010 1 0

Metconazole 0.020 0.020 14 14 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.01 0

Methidathion 0.005 0.020 24 24 0 0 0.010 0.008 0.010 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 145Table B: Results of the EU co-ordinated programme

Product=Pears Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methiocarb 0.005 0.050 20 20 0 0 0.025 0.019 0.025 . 0

0.005 0.005 1 0 1 0 0.081 0.081 0.081 0.1 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 17 17 0 0 0.025 0.021 0.025 . 0

Methoxyfenozide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 2 0

Monocrotophos 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0 0

Myclobutanil 0.005 0.010 24 24 0 0 0.005 0.005 0.005 0.5 0

Oxadixyl 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.009 0.050 22 22 0 0 0.025 0.018 0.025 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Parathion 0.005 0.010 24 24 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.005 0.010 9 9 0 0 0.005 0.004 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 17 17 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.005 0.020 26 26 0 0 0.010 0.008 0.010 0.2 0

Pencycuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.006 0.020 26 26 0 0 0.010 0.008 0.010 0.05 0

Phosmet 0.005 0.010 5 5 0 0 0.005 0.004 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.2 0

Pirimicarb 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.005 0.010 19 19 0 0 0.005 0.005 0.005 2 0

Pirimiphos-methyl 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.05 0

Prochloraz 0.008 0.050 19 19 0 0 0.025 0.020 0.025 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 146Table B: Results of the EU co-ordinated programme

Product=Pears Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.005 0.020 26 26 0 0 0.010 0.007 0.010 . 0

Profenofos 0.005 0.020 26 26 0 0 0.010 0.007 0.010 0.05 0

Propargite 0.005 0.010 12 12 0 0 0.005 0.005 0.005 3 0

Propiconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.3 0

Pyrethrins 0.050 0.050 14 14 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 17 17 0 0 0.025 0.021 0.025 0.5 0

Pyrimethanil 0.005 0.010 12 12 0 0 0.005 0.004 0.005 5 0

Pyriproxyfen 0.005 0.010 12 12 0 0 0.005 0.004 0.005 0.2 0

Quinoxyfen 0.010 0.010 14 14 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Spiroxamine 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.009 0.020 24 24 0 0 0.010 0.008 0.010 1 0

Tebufenozide 0.010 0.050 19 19 0 0 0.025 0.020 0.025 1 0

Tebufenpyrad 0.005 0.010 12 12 0 0 0.005 0.004 0.005 0.2 0

Teflubenzuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Tetraconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.3 0

Tetradifon 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.050 17 17 0 0 0.025 0.021 0.025 5 0

Thiacloprid 0.010 0.050 17 17 0 0 0.025 0.021 0.025 0.3 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.5 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 147Table B: Results of the EU co-ordinated programme

Product=Pears Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Tolclofos-methyl 0.005 0.010 26 26 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.010 0.020 19 19 0 0 0.010 0.009 0.010 . 0

Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed astolylfluanid)

0.005 0.005 2 2 0 0 0.003 0.003 0.003 3 0

Triadimefon 0.005 0.010 3 3 0 0 0.005 0.004 0.005 . 0

0.005 0.005 1 0 1 0 0.074 0.074 0.074 0.1 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 22 22 0 0 0.010 0.009 0.010 0.1 0

Triazophos 0.005 0.010 24 24 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.5 0

Trifluralin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Vinclozolin 0.005 0.010 23 23 0 0 0.005 0.005 0.005 . 0

0.005 0.005 1 0 1 0 0.035 0.035 0.035 0.05 0

tau-Fluvalinate 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 148Table B: Results of the EU co-ordinated programme

Product=Potatoes Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 17 17 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 18 18 0 0 0.025 0.024 0.025 0.01 0

Aldicarb 0.010 0.050 18 18 0 0 0.025 0.024 0.025 . 0

Azinphos-methyl 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.05 0

Azoxystrobin 0.010 0.010 22 22 0 0 0.005 0.005 0.005 . 0

Benomyl 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Bitertanol 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 18 18 0 0 0.005 0.005 0.005 0.5 0

Bromopropylate 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Captan 0.010 0.050 21 21 0 0 0.025 0.021 0.025 0.05 0

Carbaryl 0.010 0.050 18 18 0 0 0.025 0.024 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 18 16 2 0 0.023 0.007 0.005 0.1 0

Carbofuran 0.010 0.050 18 18 0 0 0.025 0.024 0.025 . 0

Chlorfenapyr 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Chlorothalonil 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.01 0

Chlorpropham 0.010 0.020 20 20 0 0 0.010 0.009 0.010 . 0

Chlorpyrifos 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Clofentezine 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.02 0

Cyfluthrin (sum) 0.010 0.020 20 20 0 0 0.010 0.010 0.010 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 149Table B: Results of the EU co-ordinated programme

Product=Potatoes Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cypermethrin (sum) 0.010 0.020 20 20 0 0 0.010 0.010 0.010 0.05 0

Cyproconazole 0.020 0.020 17 17 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Deltamethrin 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.05 0

Diazinon 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.010 0.020 19 19 0 0 0.010 0.009 0.010 . 0

Dichlorvos 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Dicofol (sum) 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 17 17 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.010 0.030 20 20 0 0 0.015 0.014 0.015 0.1 0

Dimethoate 0.010 0.020 19 19 0 0 0.010 0.009 0.010 . 0

Dimethoate (sum) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.5 0

Dinocap (sum) 0.050 0.050 2 2 0 0 0.025 0.025 0.025 0.05 0

Diphenylamine 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 17 11 6 0 0.264 0.079 0.025 0.3 0

Endosulfan (sum) 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0.05 0

Ethion 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.02 0

Fenazaquin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

Fenhexamid 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.05 0

Fenitrothion 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 150Table B: Results of the EU co-ordinated programme

Product=Potatoes Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenoxycarb 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0.05 0

Fenpropathrin 0.020 0.020 17 17 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 17 17 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 18 18 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Flufenoxuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Flusilazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Folpet 0.010 0.050 21 21 0 0 0.025 0.022 0.025 0.1 0

Hexaconazole 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.02 0

Hexythiazox 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Imazalil 0.010 0.020 18 18 0 0 0.010 0.010 0.010 3 0

Imidacloprid 0.010 0.050 18 18 0 0 0.025 0.024 0.025 0.5 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0.02 0

Iprodione 0.010 0.020 21 21 0 0 0.010 0.009 0.010 0.02 0

Iprovalicarb 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0.05 0

Kresoxim-methyl 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.02 0

Linuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.02 0

Mepanipyrim 0.020 0.020 17 17 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.05 0

Metconazole 0.020 0.020 17 17 0 0 0.010 0.010 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 151Table B: Results of the EU co-ordinated programme

Product=Potatoes Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methamidophos 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0.01 0

Methidathion 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.02 0

Methiocarb 0.010 0.050 20 20 0 0 0.025 0.022 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 18 18 0 0 0.025 0.024 0.025 . 0

Methoxyfenozide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Monocrotophos 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0 0

Myclobutanil 0.010 0.010 20 20 0 0 0.005 0.005 0.005 0.02 0

Oxadixyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Oxamyl 0.010 0.050 20 20 0 0 0.025 0.022 0.025 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Parathion 0.010 0.010 20 20 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 19 19 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.05 0

Pencycuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Phosalone 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.05 0

Phosmet 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 19 19 0 0 0.005 0.005 0.005 0.2 0

Pirimiphos-methyl 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 152Table B: Results of the EU co-ordinated programme

Product=Potatoes Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Prochloraz 0.010 0.050 18 18 0 0 0.025 0.024 0.025 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.02 0

Profenofos 0.010 0.020 22 22 0 0 0.010 0.009 0.010 0.05 0

Propargite 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.01 0

Propiconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Pyrethrins 0.050 0.050 17 17 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 18 18 0 0 0.025 0.024 0.025 0.05 0

Pyrimethanil 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Pyriproxyfen 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Quinoxyfen 0.010 0.010 17 17 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Spiroxamine 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.2 0

Tebufenozide 0.010 0.050 20 20 0 0 0.025 0.022 0.025 0.05 0

Tebufenpyrad 0.010 0.010 5 5 0 0 0.005 0.005 0.005 0.05 0

Teflubenzuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Tetraconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Tetradifon 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.050 18 18 0 0 0.025 0.024 0.025 15 0

Thiacloprid 0.010 0.050 18 18 0 0 0.025 0.024 0.025 0.02 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 153Table B: Results of the EU co-ordinated programme

Product=Potatoes Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Thiophanate-methyl 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.1 0

Tolclofos-methyl 0.010 0.010 22 22 0 0 0.005 0.005 0.005 0.2 0

Tolylfluanid 0.010 0.020 20 20 0 0 0.010 0.009 0.010 . 0

Triadimefon 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.010 0.020 20 20 0 0 0.010 0.010 0.010 0.1 0

Triazophos 0.010 0.010 20 20 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 18 18 0 0 0.010 0.010 0.010 0.02 0

Trifluralin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Vinclozolin 0.010 0.010 22 22 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 154Table B: Results of the EU co-ordinated programme

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 154Table B: Results of the EU co-ordinated programme

Product=Poultry liver Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Aldrin 0.000 0.000 11 11 0 0 0.000 0.000 0.000 . 0

DDD, p,p- 0.001 0.001 11 11 0 0 0.000 0.000 0.000 . 0

DDE, p,p- 0.001 0.001 11 11 0 0 0.001 0.001 0.001 . 0

DDT, p,p- 0.001 0.001 11 11 0 0 0.001 0.001 0.001 . 0

Hexachlorocyclohexane (HCH), alpha-isomer 0.001 0.001 11 11 0 0 0.000 0.000 0.000 0.2 0

Hexachlorocyclohexane (HCH), beta-isomer 0.001 0.001 11 11 0 0 0.001 0.001 0.001 0.1 0

Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0.001 0.001 11 11 0 0 0.001 0.001 0.001 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 155Table B: Results of the EU co-ordinated programme

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 155Table B: Results of the EU co-ordinated programme

Product=Poultry meat Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Aldrin 0.000 0.000 17 17 0 0 0.000 0.000 0.000 . 0

DDD, p,p- 0.001 0.001 17 17 0 0 0.000 0.000 0.000 . 0

DDE, p,p- 0.001 0.001 17 17 0 0 0.001 0.001 0.001 . 0

DDT, p,p- 0.001 0.001 17 17 0 0 0.001 0.001 0.001 . 0

Hexachlorocyclohexane (HCH), alpha-isomer 0.001 0.001 17 17 0 0 0.000 0.000 0.000 0.2 0

Hexachlorocyclohexane (HCH), beta-isomer 0.001 0.001 17 17 0 0 0.001 0.001 0.001 0.1 0

Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0.001 0.001 17 17 0 0 0.001 0.001 0.001 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 156Table B: Results of the EU co-ordinated programme

Product=Processed cereal-based baby foods Treatment=Processed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acetamiprid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Aldicarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Aldrin 0.007 0.007 1 1 0 0 0.004 0.004 0.004 . 0

Aldrin and Dieldrin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Azinphos-methyl 0.009 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Azoxystrobin 0.005 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Bitertanol 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Boscalid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Bromopropylate 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Bupirimate 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Buprofezin 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Captan 0.005 0.010 3 3 0 0 0.005 0.003 0.003 . 0

Carbaryl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Carbendazim and benomyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Carbofuran 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Chlorfenvinphos 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Chlorothalonil 0.005 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Chlorpyrifos 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Chlorpyrifos-methyl 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Clofentezine 0.020 0.020 4 4 0 0 0.010 0.010 0.010 . 0

Cyfluthrin (sum) 0.009 0.020 5 5 0 0 0.010 0.009 0.010 . 0

Cypermethrin (sum) 0.006 0.020 5 5 0 0 0.010 0.009 0.010 . 0

Cyprodinil 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 157Table B: Results of the EU co-ordinated programme

Product=Processed cereal-based baby foods Treatment=Processed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

DDT (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

DDT, p,p- 0.005 0.005 1 1 0 0 0.003 0.003 0.003 . 0

Deltamethrin 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Diazinon 0.005 0.010 6 6 0 0 0.005 0.004 0.005 . 0

Dichlofluanid 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Dichlorvos 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Dicofol (sum) 0.008 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Dicofol p, p' 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Dieldrin 0.005 0.005 1 1 0 0 0.003 0.003 0.003 . 0

Difenoconazole 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Dimethoate (sum) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Dimethomorph 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Dinocap (sum) 0.009 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Diphenylamine 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Endosulfan (sum) 0.005 0.010 6 6 0 0 0.005 0.004 0.005 . 0

Endrin 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Epoxiconazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Ethion 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Fenarimol 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Fenazaquin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Fenhexamid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Fenitrothion 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Fenoxycarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Fipronil 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 158Table B: Results of the EU co-ordinated programme

Product=Processed cereal-based baby foods Treatment=Processed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fludioxonil 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Flufenoxuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Flusilazole 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Folpet 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Heptachlor (sum of heptachlor and heptachlor epoxide expressed as heptachlor) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Hexaconazole 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Hexythiazox 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Imazalil 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Imidacloprid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Indoxacarb as sum of the isomers S and R 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Iprodione 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Iprovalicarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Kresoxim-methyl 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Lambda-Cyhalothrin 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Linuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Malathion 0.005 0.010 3 3 0 0 0.005 0.004 0.003 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Metalaxyl 0.005 0.010 3 3 0 0 0.005 0.003 0.003 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Methamidophos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Methidathion 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Methiocarb 0.005 0.010 5 5 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 159Table B: Results of the EU co-ordinated programme

Product=Processed cereal-based baby foods Treatment=Processed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Methoxyfenozide 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Monocrotophos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Myclobutanil 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Oxadixyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Oxamyl 0.009 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Parathion 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Parathion-methyl 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Penconazole 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Pencycuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Phosalone 0.006 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Phosmet 0.005 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

Pirimicarb 0.005 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Pirimiphos-methyl 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Prochloraz 0.008 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Procymidone 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Profenofos 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Propargite 0.005 0.010 7 7 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 160Table B: Results of the EU co-ordinated programme

Product=Processed cereal-based baby foods Treatment=Processed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Propiconazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Propyzamide 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Pyraclostrobin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Pyridaben 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Pyrimethanil 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Pyriproxyfen 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Spiroxamine 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Tebuconazole 0.009 0.010 7 7 0 0 0.005 0.005 0.005 . 0

Tebufenozide 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Tebufenpyrad 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Teflubenzuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Tetraconazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Tetradifon 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Thiabendazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Thiacloprid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 4 4 0 0 0.010 0.010 0.010 . 0

Tolclofos-methyl 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

Tolylfluanid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed astolylfluanid)

0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Triadimefon 0.005 0.010 2 2 0 0 0.005 0.004 0.004 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 5 5 0 0 0.010 0.009 0.010 . 0

Triazophos 0.005 0.010 7 7 0 0 0.005 0.004 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 161Table B: Results of the EU co-ordinated programme

Product=Processed cereal-based baby foods Treatment=Processed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Trifloxystrobin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Vinclozolin 0.005 0.010 6 6 0 0 0.005 0.005 0.005 . 0

alpha-Endosulfan 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

beta-Endosulfan 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Page 162: Pesticide monitoring 2011 Bulgaria on August 24, 2012 at …babh.government.bg/uploads/File/ENG/Aktualno/Laboratorni... · 2014. 11. 2. · Baby food Baby food for infants and young

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 162Table B: Results of the EU co-ordinated programme

Product=Rice Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acetamiprid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Aldicarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Azinphos-methyl 0.007 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Azoxystrobin 0.008 0.010 15 15 0 0 0.005 0.005 0.005 5 0

Benomyl 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.005 0.010 15 14 1 0 0.020 0.006 0.005 0.05 0

Bitertanol 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.5 0

Bromopropylate 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.5 0

Captan 0.008 0.010 11 11 0 0 0.005 0.005 0.005 0.02 0

Carbaryl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 1 0

Carbendazim and benomyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Carbofuran 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Chlorfenapyr 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 9 9 0 0 0.005 0.004 0.005 0.02 0

Chlorothalonil 0.010 0.010 13 13 0 0 0.005 0.005 0.005 0.01 0

Chlorpropham (sum) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Chlorpyrifos 0.005 0.010 15 14 1 0 0.020 0.006 0.005 0.05 0

Chlorpyrifos-methyl 0.005 0.010 15 15 0 0 0.005 0.005 0.005 3 0

Cyfluthrin (sum) 0.009 0.020 9 9 0 0 0.010 0.007 0.005 0.02 0

Cypermethrin (sum) 0.006 0.020 9 9 0 0 0.010 0.007 0.005 . 0

Cyprodinil 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 163Table B: Results of the EU co-ordinated programme

Product=Rice Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Deltamethrin 0.009 0.010 15 15 0 0 0.005 0.005 0.005 2 0

Diazinon 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Dichlofluanid 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Dichlorvos 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.01 0

Dicofol (sum) 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Difenoconazole 0.009 0.010 9 9 0 0 0.005 0.005 0.005 0.05 0

Dimethoate 0.007 0.010 8 8 0 0 0.005 0.005 0.005 . 0

Dimethoate (sum) 0.010 0.010 7 7 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.008 0.010 9 9 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.009 0.050 5 5 0 0 0.025 0.017 0.025 0.05 0

Diphenylamine 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Endosulfan (sum) 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.1 0

Ethion 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Fenazaquin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Fenhexamid 0.010 0.010 13 13 0 0 0.005 0.005 0.005 0.05 0

Fenitrothion 0.005 0.010 15 15 0 0 0.005 0.005 0.005 . 0

Fenoxycarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Fipronil 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Fludioxonil 0.010 0.010 7 7 0 0 0.005 0.005 0.005 0.05 0

Flufenoxuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Flusilazole 0.010 0.010 7 7 0 0 0.005 0.005 0.005 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 164Table B: Results of the EU co-ordinated programme

Product=Rice Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Folpet 0.010 0.020 9 9 0 0 0.010 0.007 0.005 0.02 0

Hexaconazole 0.007 0.010 9 9 0 0 0.005 0.005 0.005 0.02 0

Hexythiazox 0.010 0.010 10 10 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Imidacloprid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Indoxacarb as sum of the isomers S and R 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Iprodione 0.010 0.010 9 9 0 0 0.005 0.005 0.005 3 0

Iprovalicarb 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Kresoxim-methyl 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.010 13 13 0 0 0.005 0.005 0.005 . 0

0.010 0.010 2 0 2 0 0.500 0.400 0.400 1 0

Linuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.005 0.010 8 8 0 0 0.005 0.004 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.010 7 7 0 0 0.005 0.005 0.005 8 0

Metalaxyl 0.005 0.010 8 8 0 0 0.005 0.004 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.010 7 7 0 0 0.005 0.005 0.005 0.05 0

Methamidophos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Methidathion 0.005 0.010 9 9 0 0 0.005 0.004 0.005 0.02 0

Methiocarb 0.005 0.010 12 12 0 0 0.005 0.005 0.005 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Methoxyfenozide 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 165Table B: Results of the EU co-ordinated programme

Product=Rice Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Monocrotophos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0 0

Myclobutanil 0.005 0.010 9 9 0 0 0.005 0.004 0.005 0.02 0

Oxadixyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.008 0.010 9 9 0 0 0.005 0.005 0.005 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Parathion 0.005 0.010 9 9 0 0 0.005 0.004 0.005 0.05 0

Parathion-methyl 0.005 0.010 12 12 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Pencycuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Phosmet 0.005 0.010 6 6 0 0 0.005 0.004 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.005 0.010 12 12 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.2 0

Pirimiphos-methyl 0.005 0.010 15 14 1 0 0.030 0.006 0.005 5 0

Prochloraz 0.008 0.010 6 6 0 0 0.005 0.005 0.005 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Procymidone 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Profenofos 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Propargite 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.01 0

Propiconazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 166Table B: Results of the EU co-ordinated programme

Product=Rice Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Propyzamide 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Pyridaben 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Pyrimethanil 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Pyriproxyfen 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 1 0

Spiroxamine 0.010 0.010 10 10 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.009 0.010 9 9 0 0 0.005 0.005 0.005 2 0

Tebufenozide 0.010 0.010 10 10 0 0 0.005 0.005 0.005 . 0

Tebufenpyrad 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Teflubenzuron 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Tetraconazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Tetradifon 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Thiacloprid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 4 4 0 0 0.010 0.010 0.010 0.01 0

Tolclofos-methyl 0.005 0.010 15 15 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.009 0.010 10 10 0 0 0.005 0.005 0.005 . 0

0.010 0.010 2 0 2 0 0.020 0.020 0.020 0.05 0

Triadimefon 0.005 0.010 8 8 0 0 0.005 0.004 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.010 0.020 7 7 0 0 0.010 0.008 0.010 0.1 0

Triazophos 0.005 0.010 9 9 0 0 0.005 0.004 0.005 0.02 0

Trifloxystrobin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 167Table B: Results of the EU co-ordinated programme

Product=Rice Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Trifluralin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Vinclozolin 0.005 0.010 15 15 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 168Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 4 4 0 0 0.025 0.020 0.025 3 0

Aldicarb 0.010 0.050 4 4 0 0 0.025 0.020 0.025 . 0

Azinphos-methyl 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Azoxystrobin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Bifenthrin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Bitertanol 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 4 4 0 0 0.005 0.005 0.005 10 0

Bromopropylate 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Captan 0.050 0.050 3 3 0 0 0.025 0.025 0.025 0.1 0

Carbaryl 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.1 0

Carbofuran 0.010 0.050 4 4 0 0 0.025 0.020 0.025 . 0

Chlorfenvinphos 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Chlorothalonil 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.01 0

Chlorpyrifos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Clofentezine 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.02 0

Cyfluthrin (sum) 0.020 0.020 4 4 0 0 0.010 0.010 0.010 0.02 0

Cypermethrin (sum) 0.020 0.020 4 4 0 0 0.010 0.010 0.010 . 0

Cyproconazole 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.05 0

Cyprodinil 0.010 0.010 4 4 0 0 0.005 0.005 0.005 8 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 169Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Deltamethrin 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.5 0

Diazinon 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.020 0.020 3 3 0 0 0.010 0.010 0.010 . 0

Dichlorvos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Dicofol (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.010 0.030 4 4 0 0 0.015 0.013 0.015 2 0

Dimethoate 0.020 0.020 3 3 0 0 0.010 0.010 0.010 . 0

Dimethoate (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Diphenylamine 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 3 3 0 0 0.025 0.025 0.025 0.05 0

Endosulfan (sum) 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Ethion 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.02 0

Fenazaquin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

Fenhexamid 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Fenitrothion 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Fenoxycarb 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Fenpropathrin 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 3 3 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 4 4 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 1 1 0 0 0.005 0.005 0.005 7 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 170Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Flufenoxuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Flusilazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Folpet 0.050 0.050 3 3 0 0 0.025 0.025 0.025 10 0

Hexaconazole 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.02 0

Hexythiazox 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.010 0.020 4 4 0 0 0.010 0.009 0.010 . 0

Imidacloprid 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.05 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 4 4 0 0 0.010 0.009 0.010 2 0

Iprodione 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.02 0

Iprovalicarb 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Kresoxim-methyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.5 0

Linuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.02 0

Mepanipyrim 0.020 0.020 3 3 0 0 0.010 0.010 0.010 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Metconazole 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.01 0

Methidathion 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.02 0

Methiocarb 0.010 0.050 4 4 0 0 0.025 0.020 0.025 . 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 4 4 0 0 0.025 0.020 0.025 . 0

Methoxyfenozide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Monocrotophos 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 171Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Myclobutanil 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Oxadixyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Parathion 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Pencycuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Phosmet 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Pirimicarb 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 2 0

Pirimiphos-methyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Prochloraz 0.010 0.050 4 4 0 0 0.025 0.020 0.025 . 0

Procymidone 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.02 0

Profenofos 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Propargite 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

Propiconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Pyrethrins 0.050 0.050 3 3 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 172Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Pyrimethanil 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Pyriproxyfen 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Quinoxyfen 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 10 0

Spiroxamine 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.05 0

Tebufenozide 0.010 0.050 4 4 0 0 0.025 0.020 0.025 10 0

Tebufenpyrad 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Teflubenzuron 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Tetraconazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Tetradifon 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.05 0

Thiacloprid 0.010 0.050 4 4 0 0 0.025 0.020 0.025 0.02 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 1 1 0 0 0.010 0.010 0.010 0.1 0

Tolclofos-methyl 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.010 0.020 4 4 0 0 0.010 0.009 0.010 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.020 0.020 4 4 0 0 0.010 0.010 0.010 0.1 0

Triazophos 0.010 0.010 4 4 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.010 0.020 4 4 0 0 0.010 0.009 0.010 0.02 0

Vinclozolin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 173Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.050 0.050 10 10 0 0 0.025 0.025 0.025 3 0

Aldicarb 0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Azinphos-methyl 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.05 0

Azoxystrobin 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Benomyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Bifenthrin 0.010 0.010 12 11 1 0 0.020 0.006 0.005 0.05 0

Boscalid 0.010 0.010 10 10 0 0 0.005 0.005 0.005 10 0

Bromopropylate 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Captan 0.010 0.050 12 12 0 0 0.025 0.022 0.025 0.1 0

Carbaryl 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.05 0

Carbendazim and benomyl 0.010 0.010 10 8 2 0 0.013 0.007 0.005 0.1 0

Carbofuran 0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Chlorfenapyr 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Chlorothalonil 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.01 0

Chlorpropham (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Cyfluthrin (sum) 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.02 0

Cypermethrin (sum) 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

Cyproconazole 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 174Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyprodinil 0.010 0.010 12 12 0 0 0.005 0.005 0.005 8 0

Deltamethrin 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.5 0

Diazinon 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.01 0

Dichlofluanid 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

Dichlorvos 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.01 0

Dicloran 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Dicofol (sum) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 10 10 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.010 0.030 11 11 0 0 0.015 0.014 0.015 2 0

Dimethoate 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

Dimethoate (sum) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Dimethomorph 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

Dinocap (sum) 0.050 0.050 1 1 0 0 0.025 0.025 0.025 0.05 0

Diphenylamine 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Dithiocarbamates 0.050 0.050 10 9 0 1 0.630 0.086 0.025 0.05 1

Endosulfan (sum) 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

Ethion 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.02 0

Fenhexamid 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.05 0

Fenitrothion 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.01 0

Fenoxycarb 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

Fenpropathrin 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.01 0

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 175Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fipronil 0.005 0.005 10 10 0 0 0.003 0.003 0.003 . 0

Fludioxonil 0.010 0.010 1 1 0 0 0.005 0.005 0.005 7 0

Flusilazole 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.02 0

Folpet 0.010 0.050 12 12 0 0 0.025 0.022 0.025 10 0

Hexaconazole 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.02 0

Hexythiazox 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

Imidacloprid 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.05 0

Indoxacarb as sum of the isomers S and R 0.020 0.020 10 10 0 0 0.010 0.010 0.010 2 0

Iprodione 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.02 0

Iprovalicarb 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.05 0

Kresoxim-methyl 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.010 0.020 12 11 1 0 0.070 0.015 0.010 0.5 0

Malathion 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.02 0

Mepanipyrim 0.020 0.020 10 10 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.05 0

Metconazole 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.02 0

Methamidophos 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.01 0

Methidathion 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.02 0

Methiocarb 0.010 0.050 11 11 0 0 0.025 0.023 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 176Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Monocrotophos 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0 0

Myclobutanil 0.010 0.010 11 11 0 0 0.005 0.005 0.005 0.02 0

Oxamyl 0.010 0.050 11 11 0 0 0.025 0.023 0.025 0.01 0

Parathion 0.010 0.010 11 11 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 11 11 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.05 0

Phosalone 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.05 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.010 0.010 11 11 0 0 0.005 0.005 0.005 2 0

Pirimiphos-methyl 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Prochloraz 0.050 0.050 10 10 0 0 0.025 0.025 0.025 . 0

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.02 0

Profenofos 0.010 0.020 12 12 0 0 0.010 0.009 0.010 0.05 0

Propargite 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.01 0

Pyrethrins 0.050 0.050 10 10 0 0 0.025 0.025 0.025 1 0

Pyridaben 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.05 0

Pyrimethanil 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Pyriproxyfen 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 177Table B: Results of the EU co-ordinated programme

Product=Spinach Treatment=Unprocessed

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Quinoxyfen 0.010 0.010 10 10 0 0 0.005 0.005 0.005 0.02 0

Spiroxamine 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.05 0

Tebufenozide 0.010 0.050 11 11 0 0 0.025 0.023 0.025 10 0

Tebufenpyrad 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Tetradifon 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.05 0

Thiacloprid 0.050 0.050 10 10 0 0 0.025 0.025 0.025 0.02 0

Tolclofos-methyl 0.010 0.010 12 12 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

Triadimefon 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.010 0.020 11 11 0 0 0.010 0.010 0.010 0.1 0

Triazophos 0.010 0.010 11 11 0 0 0.005 0.005 0.005 0.01 0

Trifloxystrobin 0.020 0.020 10 10 0 0 0.010 0.010 0.010 0.02 0

Trifluralin 0.010 0.010 1 0 1 0 0.040 0.040 0.040 0.5 0

Vinclozolin 0.010 0.010 12 12 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 1 1 0 0 0.005 0.005 0.005 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 178Table B: Results of the EU co-ordinated programme

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 178Table B: Results of the EU co-ordinated programme

Product=Swine Liver Treatment=Freezing

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Aldrin 0.000 0.000 9 9 0 0 0.000 0.000 0.000 . 0

DDD, p,p- 0.001 0.001 9 9 0 0 0.000 0.000 0.000 . 0

DDE, p,p- 0.001 0.001 9 9 0 0 0.001 0.001 0.001 . 0

DDT, p,p- 0.001 0.001 9 9 0 0 0.001 0.001 0.001 . 0

Hexachlorocyclohexane (HCH), alpha-isomer 0.001 0.001 9 9 0 0 0.000 0.000 0.000 0.2 0

Hexachlorocyclohexane (HCH), beta-isomer 0.001 0.001 9 9 0 0 0.001 0.001 0.001 0.1 0

Lindane (Gamma-isomer of hexachlorociclohexane (HCH)) 0.001 0.001 9 9 0 0 0.001 0.001 0.001 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 179Table B: Results of the EU co-ordinated programme

Product=Wheat Treatment=Milling

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Acephate 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.02 0

Acetamiprid 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.01 0

Aldicarb 0.010 0.050 18 18 0 0 0.025 0.022 0.025 . 0

Azinphos-methyl 0.007 0.020 22 22 0 0 0.010 0.008 0.010 0.05 0

Azoxystrobin 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.3 0

Bifenthrin 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.5 0

Bitertanol 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Boscalid 0.010 0.010 18 18 0 0 0.005 0.005 0.005 0.5 0

Bromopropylate 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Bupirimate 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Buprofezin 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Captan 0.005 0.050 19 19 0 0 0.025 0.021 0.025 0.02 0

Carbaryl 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.5 0

Carbendazim and benomyl 0.010 0.010 18 18 0 0 0.005 0.005 0.005 0.1 0

Carbofuran 0.010 0.050 18 18 0 0 0.025 0.022 0.025 . 0

Chlorfenapyr 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

Chlorfenvinphos 0.005 0.010 7 7 0 0 0.005 0.004 0.005 0.02 0

Chlorothalonil 0.005 0.020 21 21 0 0 0.010 0.008 0.010 0.1 0

Chlorpropham (sum) 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.02 0

Chlorpyrifos 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Chlorpyrifos-methyl 0.005 0.010 21 21 0 0 0.005 0.005 0.005 3 0

0.010 0.010 1 0 1 0 0.017 0.017 0.017 0.05 0

Cyfluthrin (sum) 0.009 0.020 21 21 0 0 0.010 0.009 0.010 0.02 0

Cypermethrin (sum) 0.006 0.020 21 21 0 0 0.010 0.009 0.010 2 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 180Table B: Results of the EU co-ordinated programme

Product=Wheat Treatment=Milling

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cyproconazole 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.1 0

Cyprodinil 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.5 0

Deltamethrin 0.005 0.020 22 22 0 0 0.010 0.008 0.010 2 0

Diazinon 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.02 0

Dichlofluanid 0.005 0.020 16 16 0 0 0.010 0.010 0.010 . 0

Dichlorvos 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.01 0

Dicofol (sum) 0.005 0.010 6 6 0 0 0.005 0.005 0.005 0.02 0

Dicofol p, p' 0.010 0.010 16 16 0 0 0.005 0.005 0.005 . 0

Difenoconazole 0.005 0.030 22 22 0 0 0.015 0.012 0.015 0.1 0

Dimethoate 0.007 0.020 16 16 0 0 0.010 0.010 0.010 . 0

Dimethoate (sum) 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

Dimethomorph 0.008 0.010 7 7 0 0 0.005 0.005 0.005 0.05 0

Dinocap (sum) 0.009 0.050 4 4 0 0 0.025 0.015 0.015 0.05 0

Diphenylamine 0.005 0.010 7 7 0 0 0.005 0.004 0.005 0.05 0

Dithiocarbamates 0.050 0.050 15 15 0 0 0.025 0.025 0.025 1 0

Endosulfan (sum) 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Epoxiconazole 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0.2 0

Ethion 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.01 0

Fenarimol 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.02 0

Fenazaquin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.01 0

Fenhexamid 0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.05 0

Fenitrothion 0.005 0.010 22 22 0 0 0.005 0.005 0.005 . 0

Fenoxycarb 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0.05 0

Fenpropathrin 0.020 0.020 15 15 0 0 0.010 0.010 0.010 0.01 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 181Table B: Results of the EU co-ordinated programme

Product=Wheat Treatment=Milling

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Fenvalerate (sum of RR, SS, RS and SR isomers) 0.020 0.020 15 15 0 0 0.010 0.010 0.010 . 0

Fipronil 0.005 0.010 18 18 0 0 0.005 0.003 0.003 . 0

Fludioxonil 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.2 0

Flufenoxuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Flusilazole 0.010 0.010 6 6 0 0 0.005 0.005 0.005 0.1 0

Folpet 0.010 0.050 18 18 0 0 0.025 0.022 0.025 2 0

Hexaconazole 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.1 0

Hexythiazox 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.5 0

Imazalil 0.010 0.020 18 18 0 0 0.010 0.009 0.010 . 0

Imidacloprid 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.1 0

Indoxacarb as sum of the isomers S and R 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0.02 0

Iprodione 0.010 0.020 17 17 0 0 0.010 0.009 0.010 0.5 0

Iprovalicarb 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0.05 0

Kresoxim-methyl 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.020 22 22 0 0 0.010 0.008 0.010 . 0

Linuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Malathion 0.005 0.005 2 2 0 0 0.003 0.003 0.003 . 0

Malathion (sum of malathion and malaoxon expressed as malathion) 0.010 0.020 20 20 0 0 0.010 0.009 0.010 8 0

Mepanipyrim 0.020 0.020 15 15 0 0 0.010 0.010 0.010 . 0

Metalaxyl 0.005 0.005 2 2 0 0 0.003 0.003 0.003 . 0

Metalaxyl (Metalaxyl including other mixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 20 20 0 0 0.010 0.009 0.010 0.05 0

Metconazole 0.020 0.020 15 15 0 0 0.010 0.010 0.010 . 0

Methamidophos 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0.01 0

Methidathion 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.02 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 182Table B: Results of the EU co-ordinated programme

Product=Wheat Treatment=Milling

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Methiocarb 0.005 0.050 19 19 0 0 0.025 0.021 0.025 . 0

Methiocarb (sum of methiocarb and methiocarb sulfoxide and sulfone, expressedas methiocarb)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Methomyl and thiodicarb (sum of methomyl and thiodicarb expressed asmethomyl)

0.010 0.050 18 18 0 0 0.025 0.022 0.025 . 0

Methoxyfenozide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Monocrotophos 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0 0

Myclobutanil 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.02 0

Oxadixyl 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.01 0

Oxamyl 0.008 0.050 21 21 0 0 0.025 0.019 0.025 0.01 0

Oxydemeton-methyl (sum of oxydemeton-methyl and demeton-S-methylsulfoneexpressed as oxydemeton-methyl)

0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Parathion 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Parathion-methyl 0.005 0.010 5 5 0 0 0.005 0.004 0.005 . 0

Parathion-methyl (sum of Parathion-methyl and paraoxon-methyl expressed asParathion-methyl)

0.010 0.010 17 17 0 0 0.005 0.005 0.005 0.02 0

Penconazole 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.05 0

Pencycuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Phosalone 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.05 0

Phosmet 0.005 0.010 4 4 0 0 0.005 0.004 0.005 . 0

Phosmet (phosmet and phosmet oxon expressed as phosmet) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Pirimicarb 0.005 0.010 4 4 0 0 0.005 0.004 0.005 . 0

Pirimicarb (sum of Pirimicarb and desmethyl pirimicarb expressed as Pirimicarb) 0.005 0.010 18 18 0 0 0.005 0.005 0.005 0.5 0

Pirimiphos-methyl 0.005 0.010 22 22 0 0 0.005 0.005 0.005 5 0

Prochloraz 0.008 0.050 19 19 0 0 0.025 0.021 0.025 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 183Table B: Results of the EU co-ordinated programme

Product=Wheat Treatment=Milling

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Prochloraz (sum of prochloraz and its metabolites containing the2,4,6-Trichlorophenol moiety expressed as prochloraz)

0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.5 0

Procymidone 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.02 0

Profenofos 0.005 0.020 22 22 0 0 0.010 0.008 0.010 0.05 0

Propargite 0.005 0.010 7 7 0 0 0.005 0.005 0.005 0.01 0

Propiconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Propyzamide 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.02 0

Pyraclostrobin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Pyrethrins 0.050 0.050 15 15 0 0 0.025 0.025 0.025 3 0

Pyridaben 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.05 0

Pyrimethanil 0.005 0.010 7 7 0 0 0.005 0.004 0.005 0.05 0

Pyriproxyfen 0.005 0.010 7 7 0 0 0.005 0.004 0.005 0.05 0

Quinoxyfen 0.010 0.010 15 15 0 0 0.005 0.005 0.005 0.02 0

Spinosad (sum of Spinosyn A and Spinosyn D, expressed as Spinosad) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 1 0

Spiroxamine 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.05 0

Tebuconazole 0.009 0.020 22 22 0 0 0.010 0.008 0.010 0.2 0

Tebufenozide 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.05 0

Tebufenpyrad 0.005 0.010 7 7 0 0 0.005 0.004 0.005 0.05 0

Teflubenzuron 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Tetraconazole 0.010 0.010 3 3 0 0 0.005 0.005 0.005 0.1 0

Tetradifon 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.02 0

Thiabendazole 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.05 0

Thiacloprid 0.010 0.050 18 18 0 0 0.025 0.022 0.025 0.1 0

Thiametoxam (sum of thiametoxam and clothianidin expressed as thiametoxam) 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

Thiophanate-methyl 0.020 0.020 3 3 0 0 0.010 0.010 0.010 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 184Table B: Results of the EU co-ordinated programme

Product=Wheat Treatment=Milling

CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Tolclofos-methyl 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.05 0

Tolylfluanid 0.009 0.020 19 19 0 0 0.010 0.009 0.010 . 0

Tolylfluanid (Sum of tolylfluanid and dimethylaminosulfotoluidide expressed astolylfluanid)

0.005 0.005 1 1 0 0 0.003 0.003 0.003 0.05 0

Triadimefon 0.005 0.005 1 1 0 0 0.003 0.003 0.003 . 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 21 20 1 0 0.030 0.010 0.010 0.2 0

Triazophos 0.005 0.010 22 22 0 0 0.005 0.005 0.005 0.02 0

Trifloxystrobin 0.010 0.020 18 18 0 0 0.010 0.009 0.010 0.05 0

Trifluralin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.1 0

Vinclozolin 0.005 0.010 21 21 0 0 0.005 0.005 0.005 . 0

tau-Fluvalinate 0.010 0.010 2 2 0 0 0.005 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 185Table C1: Results of national programme for unprocessed conventional products where residues were detected

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 185Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Cereals

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Cereals Rice Bifenthrin 0.005 0.010 15 14 1 0 0.020 0.006 0.005 0.05 0

Chlorpyrifos 0.005 0.010 15 14 1 0 0.020 0.006 0.005 0.05 0

Cypermethrin 0.010 0.010 1 1 0 0 0.005 0.005 0.005 . 0

0.010 0.010 5 0 5 0 0.700 0.246 0.200 2 0

Lambda-Cyhalothrin 0.005 0.010 13 13 0 0 0.005 0.005 0.005 . 0

0.010 0.010 2 0 2 0 0.500 0.400 0.400 1 0

Pirimiphos-methyl 0.005 0.010 15 14 1 0 0.030 0.006 0.005 5 0

Tolylfluanid 0.009 0.010 10 10 0 0 0.005 0.005 0.005 . 0

0.010 0.010 2 0 2 0 0.020 0.020 0.020 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 186Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Brassica vegetables Chinesecabbage

Methiocarb 0.005 0.005 2 2 0 0 0.003 0.003 0.003 . 0

0.005 0.005 1 0 1 0 0.056 0.056 0.056 0.1 0

Vinclozolin 0.005 0.005 2 2 0 0 0.003 0.003 0.003 . 0

0.005 0.005 1 0 1 0 0.017 0.017 0.017 0.05 0

Headcabbage

Cyfluthrin 0.010 0.010 7 7 0 0 0.005 0.005 0.005 . 0

0.010 0.010 1 0 1 0 0.060 0.060 0.060 0.3 0

Cypermethrin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

0.010 0.010 5 0 5 0 0.300 0.154 0.200 1 0

Kresoxim-methyl 0.005 0.010 19 18 1 0 0.030 0.006 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.010 19 16 3 0 0.030 0.008 0.005 0.2 0

Cane fruit, small fruitand berries

Cranberries Cyfluthrin 0.010 0.010 1 0 1 0 0.015 0.015 0.015 0.02 0

Lambda-Cyhalothrin 0.010 0.010 1 0 1 0 0.030 0.030 0.030 0.2 0

Citrus fruit Grapefruit Azoxystrobin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

0.008 0.008 1 0 1 0 0.036 0.036 0.036 1 0

Bifenthrin 0.005 0.010 5 4 1 0 0.040 0.012 0.005 0.1 0

Chlorpyrifos 0.005 0.010 5 4 1 0 0.077 0.019 0.005 0.3 0

Cyfluthrin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

0.010 0.010 1 0 1 0 0.015 0.015 0.015 0.02 0

Cyprodinil 0.005 0.010 5 4 1 0 0.034 0.011 0.005 0.05 0

Dimethomorph 0.008 0.010 2 1 1 0 0.035 0.020 0.020 0.05 0

Imazalil 0.020 0.020 1 0 1 0 0.581 0.581 0.581 5 0

Lambda-Cyhalothrin 0.005 0.020 4 4 0 0 0.010 0.006 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 187Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

0.010 0.010 1 0 1 0 0.090 0.090 0.090 0.2 0

Lemons Azinphos-methyl 0.007 0.010 16 14 2 0 0.042 0.009 0.005 0.05 0

Bifenthrin 0.005 0.010 16 15 1 0 0.060 0.008 0.005 0.1 0

Buprofezin 0.005 0.010 16 15 1 0 0.020 0.005 0.005 1 0

Cypermethrin 0.010 0.010 4 4 0 0 0.005 0.005 0.005 . 0

0.010 0.010 3 0 3 0 0.600 0.467 0.400 2 0

Dicofol (sum) 0.005 0.010 14 13 1 0 0.110 0.012 0.005 2 0

Imazalil 0.010 0.010 3 0 3 0 0.840 0.537 0.580 5 0

Kresoxim-methyl 0.005 0.010 16 14 2 0 0.039 0.008 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.010 16 14 2 0 0.080 0.011 0.005 0.2 0

Prochloraz 0.008 0.010 5 5 0 0 0.005 0.004 0.004 . 0

0.010 0.010 1 0 1 0 0.440 0.440 0.440 10 0

Mandarins Bifenthrin 0.005 0.010 20 16 4 0 0.080 0.017 0.005 0.1 0

Chlorpyrifos 0.005 0.010 20 17 3 0 0.347 0.036 0.005 2 0

Chlorpyrifos-methyl 0.005 0.010 20 19 1 0 0.154 0.012 0.005 1 0

Cypermethrin 0.010 0.010 3 3 0 0 0.005 0.005 0.005 . 0

0.010 0.010 5 0 5 0 0.900 0.356 0.300 2 0

Imazalil 0.010 0.020 8 4 4 0 1.410 0.469 0.015 5 0

Lambda-Cyhalothrin 0.005 0.020 20 18 2 0 0.025 0.007 0.005 0.2 0

Thiabendazole 0.010 0.050 8 7 1 0 0.910 0.128 0.025 5 0

Oranges Bifenthrin 0.005 0.010 18 17 1 0 0.040 0.007 0.005 0.1 0

Chlorpyrifos 0.005 0.010 18 16 2 0 0.058 0.009 0.005 0.3 0

Chlorpyrifos-methyl 0.005 0.010 18 17 1 0 0.030 0.006 0.005 0.5 0

Cypermethrin 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 188Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

0.010 0.010 2 0 2 0 0.200 0.200 0.200 2 0

Imazalil 0.010 0.020 8 4 3 1 11.550 1.926 0.415 5 1

Penconazole 0.010 0.020 18 17 1 0 0.040 0.009 0.005 0.05 0

Prochloraz 0.010 0.050 7 7 0 0 0.025 0.019 0.025 . 0

0.050 0.050 1 0 1 0 0.274 0.274 0.274 10 0

Tolclofos-methyl 0.005 0.010 18 17 1 0 0.030 0.006 0.005 0.05 0

Cucurbits Cucumbers Bifenthrin 0.006 0.010 18 16 2 0 0.040 0.008 0.005 0.1 0

Boscalid 0.010 0.010 1 0 1 0 0.021 0.021 0.021 3 0

0.010 0.010 14 14 0 0 0.005 0.005 0.005 0.2 0

Chlorpropham 0.010 0.020 16 16 0 0 0.010 0.009 0.010 . 0

0.005 0.005 1 0 1 0 0.010 0.010 0.010 0.05 0

Cypermethrin 0.010 0.010 1 0 1 0 0.070 0.070 0.070 0.2 0

Cypermethrin (sum) 0.006 0.020 17 16 1 0 0.030 0.011 0.010 0.2 0

Dithiocarbamates 0.050 0.050 14 13 1 0 0.064 0.028 0.025 2 0

Imidacloprid 0.010 0.050 15 14 1 0 0.130 0.032 0.025 1 0

Metalaxyl (Metalaxyl including othermixtures of constituent isomers includingMetalaxyl-M (sum of isomers))

0.010 0.020 15 15 0 0 0.010 0.009 0.010 0.5 0

0.020 0.020 1 0 1 0 0.025 0.025 0.025 0.05 0

Permethrin (sum of isomers) 0.020 0.020 14 13 1 0 0.026 0.011 0.010 0.05 0

Leafyvegetables & freshherbs

Lettuce Carbendazim and benomyl 0.010 0.010 10 9 1 0 0.014 0.006 0.005 0.1 0

Cypermethrin 0.010 0.010 1 0 1 0 0.200 0.200 0.200 2 0

Dithiocarbamates 0.050 0.050 10 9 1 0 0.723 0.095 0.025 5 0

Fenhexamid 0.010 0.020 11 11 0 0 0.010 0.010 0.010 . 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 189Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

0.010 0.010 1 0 1 0 0.080 0.080 0.080 40 0

Spinach Bifenthrin 0.010 0.010 16 15 1 0 0.020 0.006 0.005 0.05 0

Carbendazim and benomyl 0.010 0.010 14 12 2 0 0.013 0.006 0.005 0.1 0

Cypermethrin 0.010 0.010 1 0 1 0 0.020 0.020 0.020 0.7 0

Dithiocarbamates 0.050 0.050 13 12 0 1 0.630 0.072 0.025 0.05 1

Lambda-Cyhalothrin 0.010 0.020 16 15 1 0 0.070 0.013 0.010 0.5 0

Trifluralin 0.010 0.010 1 0 1 0 0.040 0.040 0.040 0.5 0

Legume vegetables(fresh)

Beans (withpods)

Cyfluthrin 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

0.010 0.010 1 0 1 0 0.040 0.040 0.040 0.1 0

0.010 0.010 1 0 1 0 0.040 0.040 0.040 0.7 0

Cypermethrin 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

0.010 0.010 3 0 3 0 0.400 0.250 0.300 0.7 0

Cypermethrin (sum) 0.006 0.020 18 18 0 0 0.010 0.009 0.010 . 0

0.020 0.020 1 0 1 0 0.030 0.030 0.030 0.7 0

Dimethoate 0.005 0.020 19 19 0 0 0.010 0.008 0.010 . 0

0.020 0.020 1 0 0 1 0.040 0.040 0.040 0.02 1

Dimethoate (sum) 0.010 0.010 6 5 1 0 0.018 0.007 0.005 0.02 0

Dithiocarbamates 0.050 0.050 12 11 1 0 0.888 0.097 0.025 1 0

Tolylfluanid 0.010 0.020 20 20 0 0 0.010 0.008 0.010 . 0

0.010 0.010 1 0 1 0 0.020 0.020 0.020 3 0

Beans(withoutpods)

Penconazole 0.005 0.005 1 0 1 0 0.020 0.020 0.020 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 190Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Peas(withoutpods)

Bifenthrin 0.005 0.010 8 7 1 0 0.035 0.008 0.005 0.05 0

Penconazole 0.005 0.005 1 0 1 0 0.014 0.014 0.014 0.2 0

0.005 0.010 7 7 0 0 0.005 0.005 0.005 0.05 0

Procymidone 0.005 0.010 7 7 0 0 0.005 0.004 0.005 0.3 0

0.005 0.005 1 0 1 0 0.014 0.014 0.014 0.02 0

Pome fruit Apples Buprofezin 0.005 0.005 1 0 1 0 0.185 0.185 0.185 3 0

0.005 0.010 22 19 3 0 0.300 0.029 0.005 0.5 0

Carbendazim and benomyl 0.010 0.010 9 7 2 0 0.030 0.010 0.005 0.2 0

Chlorpyrifos 0.005 0.010 23 20 3 0 0.440 0.043 0.005 0.5 0

Chlorpyrifos-methyl 0.005 0.010 23 22 1 0 0.020 0.005 0.005 0.5 0

Cypermethrin 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

0.010 0.010 2 0 2 0 0.400 0.400 0.400 1 0

Dimethoate 0.005 0.020 11 11 0 0 0.010 0.006 0.005 . 0

0.020 0.020 1 0 0 1 0.087 0.087 0.087 0.02 1

Dithiocarbamates 0.050 0.050 5 4 1 0 0.073 0.035 0.025 5 0

Fenarimol 0.005 0.020 23 22 1 0 0.113 0.010 0.005 0.3 0

Imidacloprid 0.010 0.050 9 8 1 0 0.180 0.036 0.025 0.5 0

Lambda-Cyhalothrin 0.005 0.020 23 22 1 0 0.030 0.007 0.005 0.1 0

Myclobutanil 0.005 0.010 21 19 2 0 0.177 0.019 0.005 0.5 0

Tebuconazole 0.009 0.020 21 20 1 0 0.039 0.008 0.005 1 0

Triadimefon 0.005 0.010 6 6 0 0 0.005 0.005 0.005 . 0

0.005 0.005 1 0 1 0 0.108 0.108 0.108 0.2 0

Pears Bifenthrin 0.005 0.010 26 25 1 0 0.012 0.005 0.005 0.3 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 191Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Carbendazim and benomyl 0.010 0.010 17 15 1 1 0.279 0.023 0.005 0.2 1

Dithiocarbamates 0.050 0.050 14 13 1 0 0.150 0.034 0.025 5 0

Imazalil 0.010 0.020 17 16 1 0 0.439 0.034 0.010 2 0

Imidacloprid 0.010 0.050 17 16 1 0 0.110 0.028 0.025 0.5 0

Methiocarb 0.005 0.050 20 20 0 0 0.025 0.019 0.025 . 0

0.005 0.005 1 0 1 0 0.081 0.081 0.081 0.1 0

Triadimefon 0.005 0.010 3 3 0 0 0.005 0.004 0.005 . 0

0.005 0.005 1 0 1 0 0.074 0.074 0.074 0.1 0

Vinclozolin 0.005 0.010 23 23 0 0 0.005 0.005 0.005 . 0

0.005 0.005 1 0 1 0 0.035 0.035 0.035 0.05 0

Potatoes Potatoes Carbendazim and benomyl 0.010 0.010 18 16 2 0 0.023 0.007 0.005 0.1 0

Dithiocarbamates 0.050 0.050 17 11 6 0 0.264 0.079 0.025 0.3 0

Heptachlor (sum of heptachlor and the cisand trans isomers of heptachlor epoxide)

0.010 0.010 18 18 0 0 0.005 0.005 0.005 . 0

0.010 0.010 1 0 0 1 0.024 0.024 0.024 0.01 1

Root and tubervegetables (excepttropical)

Carrots Bifenthrin 0.010 0.010 21 20 1 0 0.020 0.006 0.005 0.05 0

Boscalid 0.010 0.010 15 15 0 0 0.005 0.005 0.005 1 0

0.010 0.010 1 0 1 0 0.015 0.015 0.015 2 0

Carbendazim and benomyl 0.010 0.010 16 15 1 0 0.014 0.006 0.005 0.1 0

Chlorpyrifos 0.010 0.010 21 17 3 1 0.216 0.022 0.005 0.1 1

Cypermethrin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

0.010 0.010 2 0 2 0 0.020 0.020 0.020 0.05 0

Solanacea (e.g.tomatoes, peppers)

Peppers Lambda-Cyhalothrin 0.005 0.010 15 14 1 0 0.050 0.008 0.005 0.1 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 192Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Metalaxyl 0.005 0.010 5 5 0 0 0.005 0.005 0.005 . 0

0.005 0.005 2 0 2 0 0.212 0.202 0.202 0.5 0

Methiocarb 0.010 0.010 6 6 0 0 0.005 0.005 0.005 . 0

0.005 0.005 2 0 2 0 0.047 0.036 0.036 0.2 0

Pyrimethanil 0.005 0.010 15 13 2 0 0.422 0.034 0.005 2 0

Pyriproxyfen 0.005 0.010 15 14 1 0 0.348 0.028 0.005 1 0

Tomatoes Chlorpyrifos 0.010 0.010 10 9 1 0 0.016 0.006 0.005 0.5 0

Cypermethrin 0.010 0.010 1 0 1 0 0.020 0.020 0.020 0.5 0

Cypermethrin (sum) 0.010 0.020 9 7 2 0 0.064 0.018 0.010 0.5 0

Dithiocarbamates 0.050 0.050 7 6 1 0 0.080 0.033 0.025 3 0

Lambda-Cyhalothrin 0.010 0.020 10 9 1 0 0.050 0.013 0.010 0.1 0

Permethrin (sum of isomers) 0.020 0.020 7 6 1 0 0.029 0.013 0.010 0.05 0

Procymidone 0.010 0.020 9 9 0 0 0.010 0.008 0.010 . 0

0.020 0.020 1 0 0 1 0.058 0.058 0.058 0.02 1

Stem vegetables Leek Chlorpyrifos 0.006 0.010 11 10 1 0 0.440 0.044 0.005 0.5 0

Cypermethrin 0.010 0.010 2 2 0 0 0.005 0.005 0.005 . 0

0.010 0.010 1 0 1 0 0.300 0.300 0.300 0.5 0

Lambda-Cyhalothrin 0.005 0.010 11 9 2 0 0.200 0.025 0.005 0.3 0

Methiocarb 0.010 0.010 5 5 0 0 0.005 0.005 0.005 . 0

0.005 0.005 2 0 2 0 0.106 0.088 0.088 0.2 0

Stone fruit Peaches Acetamiprid 0.050 0.050 7 6 0 1 0.173 0.046 0.025 0.1 1

Carbendazim and benomyl 0.010 0.010 7 4 3 0 0.038 0.014 0.005 0.2 0

Dithiocarbamates 0.050 0.050 7 5 2 0 0.165 0.049 0.025 2 0

Table and wine grapes Tablegrapes

Boscalid 0.010 0.010 3 2 1 0 1.100 0.370 0.005 5 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 193Table C1: Results of national programme for unprocessed conventional products where residues were detected

ProductClass=Sum of fruits and nuts, vegetables, other plant products

ProductGroup Product CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

Level MRLNon

Compliant

Carbendazim and benomyl 0.010 0.010 3 2 1 0 0.020 0.010 0.005 0.3 0

Chlorpyrifos-methyl 0.005 0.010 9 8 1 0 0.060 0.011 0.005 0.2 0

Cypermethrin (sum) 0.010 0.020 6 5 1 0 0.050 0.015 0.010 0.5 0

Cyprodinil 0.005 0.010 9 6 3 0 1.500 0.192 0.005 5 0

Fenhexamid 0.010 0.010 6 5 1 0 2.030 0.343 0.005 5 0

Indoxacarb as sum of the isomers S and R 0.010 0.010 3 2 1 0 0.210 0.073 0.005 2 0

Penconazole 0.010 0.010 9 7 2 0 0.130 0.029 0.005 0.2 0

Pyrimethanil 0.005 0.010 9 8 1 0 0.120 0.018 0.005 5 0

Winegrapes

Bromopropylate 0.005 0.005 2 1 1 0 0.007 0.005 0.005 0.01 0

Cyfluthrin (sum) 0.009 0.009 2 1 1 0 0.155 0.080 0.080 0.3 0

Fenarimol 0.005 0.005 2 1 1 0 0.169 0.086 0.086 0.3 0

Kresoxim-methyl 0.007 0.007 2 1 1 0 0.067 0.035 0.035 1 0

Penconazole 0.005 0.005 2 1 1 0 0.125 0.064 0.064 0.2 0

Pyriproxyfen 0.005 0.005 2 1 1 0 0.020 0.011 0.011 0.05 0

Tropical andsubtropical fruit

Bananas Bifenthrin 0.005 0.010 25 24 1 0 0.060 0.007 0.005 0.1 0

Diphenylamine 0.005 0.010 25 24 1 0 0.012 0.005 0.005 0.05 0

Lambda-Cyhalothrin 0.005 0.010 25 24 1 0 0.020 0.005 0.005 0.1 0

Penconazole 0.005 0.010 25 24 1 0 0.013 0.005 0.005 0.05 0

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 194Table C3: Results of national programme processed conventional products where residues were detected

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 194Table C3: Results of national programme processed conventional products where residues were detected

ProductClass=Baby food

ProductGroup Product Treatment CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

LevelNon

Compliant

Foodgroup notrelevant

Processed cereal-based babyfoods

Milling Pirimiphos-methyl 0.010 0.010 5 3 0 2 0.056 0.020 0.005 2

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All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 195Table C3: Results of national programme processed conventional products where residues were detected

All results expressed in mg/kgFor mean and median residue level calculations when results were below limit of detection LOQ/2 was substituted

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 195Table C3: Results of national programme processed conventional products where residues were detected

ProductClass=Cereals

ProductGroup Product Treatment CompoundMinLOQ

MaxLOQ Total

BelowLOQ

BetweenLOQandMRL

AboveMRL

MaxResidue

Level

MeanResidue

Level

MedianResidue

LevelNon

Compliant

Cereals Wheat Milling Chlorpyrifos-methyl 0.005 0.010 22 21 1 0 0.017 0.005 0.005 0

Triadimefon (sum of Triadimefon and Triadimenol) 0.005 0.020 21 20 1 0 0.030 0.010 0.010 0

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 196Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z- 22018 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.038 mg/kg 0.02 Non compliant

Z- 22129 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.160 mg/kg 0.05 Non compliant

Z- 22229 TR Peppers Importactivities

Unprocessed Clofentezine 0.020 0.024 mg/kg 0.02 Non compliant

Z- 22275 TR Peppers Importactivities

Unprocessed Clofentezine 0.020 0.026 mg/kg 0.02 Non compliant

Z- 24102 TR Peppers Importactivities

Unprocessed Dimethoate (sum) 0.010 0.066 mg/kg 0.02 Non compliant

Z- 25144 TR Peppers Importactivities

Unprocessed Dimethoate (sum) 0.010 0.054 mg/kg 0.02 Non compliant

Z- 26388 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.063 mg/kg 0.02 Non compliant

Z- 26507 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.016 mg/kg 0.01 Non compliant

Z- 27291 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.190 mg/kg 0.02 Non compliant

Z- 27546 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.880 mg/kg 0.02 Non compliant

Z- 27675 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 1.380 mg/kg 0.02 Non compliant

Z- 27679 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.040 mg/kg 0.02 Non compliant

Z- 28118 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.160 mg/kg 0.02 Non compliant

Z- 28481 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.040 mg/kg 0.02 Non compliant

Z- 28614 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.092 mg/kg 0.01 Non compliant

Z- 28955 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.018 mg/kg 0.01 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 197Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z- 28986 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.190 mg/kg 0.02 Non compliant

Z- 29253 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.021 mg/kg 0.02 Non compliant

Z- 29253 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.170 mg/kg 0.02 Non compliant

Z- 29860 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.190 mg/kg 0.02 Non compliant

Z- 30399 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.181 mg/kg 0.02 Non compliant

Z- 30749 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.050 mg/kg 0.02 Non compliant

Z- 30772 TR Peppers Importactivities

Unprocessed Clofentezine 0.020 0.050 mg/kg 0.02 Non compliant

Z- 31194 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.075 mg/kg 0.02 Non compliant

Z-11188 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.760 mg/kg 0.02 Non compliant

Z-12837 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.862 mg/kg 0.02 Non compliant

Z-1481 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.069 mg/kg 0.02 Non compliant

Z-15451 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.160 mg/kg 0.05 Non compliant

Z-15490 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.180 mg/kg 0.05 Non compliant

Z-15606 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.276 mg/kg 0.05 Non compliant

Z-15665 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.127 mg/kg 0.02 Non compliant

Z-15673 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.075 mg/kg 0.05 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 198Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z-15673 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.149 mg/kg 0.02 Non compliant

Z-15673 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.139 mg/kg 0.02 Non compliant

Z-15789 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.076 mg/kg 0.02 Non compliant

Z-15821 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.145 mg/kg 0.02 Non compliant

Z-15879 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.030 mg/kg 0.02 Non compliant

Z-16003 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.080 mg/kg 0.05 Non compliant

Z-16041 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.130 mg/kg 0.05 Non compliant

Z-16082 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.051 mg/kg 0.02 Non compliant

Z-16082 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.026 mg/kg 0.02 Non compliant

Z-16199 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.060 mg/kg 0.02 Non compliant

Z-16219 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.032 mg/kg 0.02 Non compliant

Z-16448 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.130 mg/kg 0.02 Non compliant

Z-16478 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.180 mg/kg 0.05 Non compliant

Z-16488 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.110 mg/kg 0.05 Non compliant

Z-16629 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.290 mg/kg 0.10 Non compliant

Z-16629 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.025 mg/kg 0.02 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 199Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z-16633 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.130 mg/kg 0.05 Non compliant

Z-16713 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.035 mg/kg 0.02 Non compliant

Z-16723 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.044 mg/kg 0.02 Non compliant

Z-16777 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.100 mg/kg 0.02 Non compliant

Z-16783 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.031 mg/kg 0.02 Non compliant

Z-16896 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.130 mg/kg 0.05 Non compliant

Z-16960 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.053 mg/kg 0.02 Non compliant

Z-17044 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.060 mg/kg 0.02 Non compliant

Z-17053 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.030 mg/kg 0.02 Non compliant

Z-17131 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.029 mg/kg 0.02 Non compliant

Z-17283 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.033 mg/kg 0.02 Non compliant

Z-17283 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.052 mg/kg 0.02 Non compliant

Z-17287 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.032 mg/kg 0.02 Non compliant

Z-17316 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.033 mg/kg 0.02 Non compliant

Z-17534 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.116 mg/kg 0.02 Non compliant

Z-17576 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.066 mg/kg 0.02 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 200Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z-17740 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.067 mg/kg 0.02 Non compliant

Z-17921 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.527 mg/kg 0.02 Non compliant

Z-18235 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.140 mg/kg 0.05 Non compliant

Z-18257 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 1.150 mg/kg 0.02 Non compliant

Z-18657 TR Peppers Importactivities

Unprocessed Procymidone 0.020 0.051 mg/kg 0.02 Non compliant

Z-18878 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.066 mg/kg 0.02 Non compliant

Z-19281 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.150 mg/kg 0.02 Non compliant

Z-19644 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.024 mg/kg 0.02 Non compliant

Z-19710 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.023 mg/kg 0.02 Non compliant

Z-20148 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.072 mg/kg 0.05 Non compliant

Z-20204 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.078 mg/kg 0.05 Non compliant

Z-20206 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.032 mg/kg 0.02 Non compliant

Z-20262 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.175 mg/kg 0.05 Non compliant

Z-20616 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.034 mg/kg 0.02 Non compliant

Z-20669 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.048 mg/kg 0.02 Non compliant

Z-20683 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.320 mg/kg 0.05 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 201Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z-20694 TR Peppers Importactivities

Unprocessed Tetradifon 0.010 0.026 mg/kg 0.02 Non compliant

Z-20946 TR Peppers Importactivities

Unprocessed Formetanate 0.010 0.081 mg/kg 0.05 Non compliant

Z-21404 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.042 mg/kg 0.02 Non compliant

Z-21626 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.045 mg/kg 0.02 Non compliant

Z-21701 TR Peppers Importactivities

Unprocessed Malathion (sum of malathion and malaoxonexpressed as malathion)

0.010 0.022 mg/kg 0.02 Non compliant

Z-2495 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.045 mg/kg 0.02 Non compliant

Z-339 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.180 mg/kg 0.02 Non compliant

Z-3781 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.070 mg/kg 0.02 Non compliant

Z-4007 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.730 mg/kg 0.02 Non compliant

Z-4605 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.900 mg/kg 0.02 Non compliant

Z-5188 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.060 mg/kg 0.02 Non compliant

Z-5209 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.110 mg/kg 0.02 Non compliant

Z-5400 TR Peppers Importactivities

Unprocessed Oxamyl 0.010 0.070 mg/kg 0.02 Non compliant

Z-8053 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.054 mg/kg 0.02 Non compliant

Z-8312 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.250 mg/kg 0.02 Non compliant

Z-8557 TR Peppers Importactivities

Unprocessed Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)

0.010 0.095 mg/kg 0.02 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 202Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Enforcement

SampleCode ORIGCOUNTRY Product

Samplingpoint Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

Z- 29996 TR Tomatoes Importactivities

Unprocessed Procymidone 0.020 0.073 mg/kg 0.02 Non compliant

Z-15654 TR Tomatoes Importactivities

Unprocessed Procymidone 0.020 0.080 mg/kg 0.02 Non compliant

Z-16092 TR Tomatoes Importactivities

Unprocessed Oxamyl 0.010 0.080 mg/kg 0.02 Non compliant

Z-16870 TR Tomatoes Importactivities

Unprocessed Oxamyl 0.010 0.079 mg/kg 0.02 Non compliant

Z-17727 TR Tomatoes Importactivities

Unprocessed Tetradifon 0.010 0.031 mg/kg 0.02 Non compliant

Z-3053 TR Tomatoes Importactivities

Unprocessed Oxamyl 0.010 0.150 mg/kg 0.02 Non compliant

Z-3857 TR Tomatoes Importactivities

Unprocessed Oxamyl 0.010 0.059 mg/kg 0.02 Non compliant

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Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 203Table D: Reported exceedences of MRL for surveillance and enforcement samples

Non compliant samples represent samples above MRL when measurement uncertainty has been taken into consideration. Numerical exceedences represent samplesabove MRL that are deemed to be compliant when measurement uncertainty has been taken into consideration

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 203Table D: Reported exceedences of MRL for surveillance and enforcement samples

Strategy=Surveillance

SampleCode ORIGCOUNTRY Product Sampling point Treatment Organic Residue LOQ Level Unit MRL Result Evaluation

M b.foods 04

BG Processedcereal-basedbaby foods

Mobile retailer,market/streetvendor

Milling Pirimiphos-methyl 0.010 0.056 mg/kg 0.01 Non compliant

M b.foods 05

BG Processedcereal-basedbaby foods

Mobile retailer,market/streetvendor

Milling Pirimiphos-methyl 0.010 0.028 mg/kg 0.01 Non compliant

Mapp02

BG Apples Storage Unprocessed Dimethoate 0.020 0.087 mg/kg 0.02 Non compliant

Mbeen12

BG Beans (withpods)

Mobile retailer,market/streetvendor

Freezing Dimethoate 0.020 0.040 mg/kg 0.02 Non compliant

M car14

BG Carrots Mobile retailer,market/streetvendor

Unprocessed Chlorpyrifos 0.010 0.216 mg/kg 0.10 Non compliant

Moran02

TR Oranges Mobile retailer,market/streetvendor

Unprocessed Imazalil 0.020 11.550 mg/kg 5.00 Non compliant

M peach05

BG Peaches Primaryproduction

Unprocessed Acetamiprid 0.050 0.173 mg/kg 0.10 Non compliant

M pear02

ZA Pears Mobile retailer,market/streetvendor

Unprocessed Carbendazim and benomyl 0.010 0.279 mg/kg 0.20 Non compliant

M pot04

BG Potatoes Storage Unprocessed Heptachlor (sum of heptachlor andthe cis and trans isomers ofheptachlor epoxide)

0.010 0.024 mg/kg 0.01 Non compliant

M spin07

BG Spinach Mobile retailer,market/streetvendor

Unprocessed Dithiocarbamates 0.050 0.630 mg/kg 0.05 Non compliant

M tom01

BG Tomatoes Primaryproduction

Unprocessed Procymidone 0.020 0.058 mg/kg 0.02 Non compliant

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To avoid duplicates residues marked as part of sum are excludedColumn nX indicates number of residues detected in product.

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 204Table E1: Number of residues detected by product

To avoid duplicates residues marked as part of sum are excludedColumn nX indicates number of residues detected in product.

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 204Table E1: Number of residues detected by product

Product Class Product Processed n0 n1 n2 n3 n4

Animal products Bovine Liver 5 . . . .

Animal products Poultry liver 11 . . . .

Animal products Poultry meat 17 . . . .

Animal products Swine Liver 9 . . . .

Baby food Baby food for infants and young childern Y 9 . . . .

Baby food Processed cereal-based baby foods Y 10 2 . . .

Cereals Rice 9 1 4 1 .

Cereals Rice Y 15 . . . .

Cereals Wheat 1 . . . .

Cereals Wheat Y 21 . 1 . .

Fruits and nuts Apples 12 4 5 1 1

Fruits and nuts Bananas 22 2 1 . .

Fruits and nuts Cranberries . . 1 . .

Fruits and nuts Grapefruit 1 1 2 1 .

Fruits and nuts Lemons 7 4 4 . 1

Fruits and nuts Mandarins 8 6 4 2 .

Fruits and nuts Oranges 10 5 2 . 1

Fruits and nuts Peaches 4 . 3 . .

Fruits and nuts Pears 18 7 1 . .

Fruits and nuts Table grapes 3 3 1 1 1

Fruits and nuts Wine grapes . . 1 . 1

Vegetables Aubergines (egg plants) 6 . . . .

Vegetables Beans (with pods) 19 6 2 . .

Vegetables Beans (without pods) . 1 . . .

Vegetables Carrots 12 9 . . .

Vegetables Chinese cabbage 1 2 . . .

Vegetables Courgettes 239 3 . . .

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To avoid duplicates residues marked as part of sum are excludedColumn nX indicates number of residues detected in product.

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 205Table E1: Number of residues detected by product

Product Class Product Processed n0 n1 n2 n3 n4

Vegetables Cucumbers 10 6 2 . .

Vegetables Head cabbage 13 3 2 1 .

Vegetables Leek 6 4 1 . .

Vegetables Lettuce 8 4 . . .

Vegetables Peas (with pods) 2 . . . .

Vegetables Peas (without pods) 6 1 1 . .

Vegetables Peppers 2717 185 9 3 1

Vegetables Potatoes 13 9 . . .

Vegetables Spinach 11 4 . 1 .

Vegetables Tomatoes 908 13 4 . .

4163 285 51 11 6

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To avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 206Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

To avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 206Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

Product=Apples

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

M app02 BG 2 Dimethoate(0.087) Carbendazim and benomyl(0.025)

M app03 BG 2 Tebuconazole(0.039) Dithiocarbamates(0.073)

M app04 BG 3 Carbendazim and benomyl(0.03) Chlorpyrifos-methyl(0.02) Chlorpyrifos(0.024)

ZK 1332 BG 2 Imidacloprid(0.18) Chlorpyrifos(0.44)

ZK 1334 BG 2 Buprofezin(0.13) Chlorpyrifos(0.44)

ZK-4627 BG 4 Fenarimol(0.113) Buprofezin(0.185) Myclobutanil(0.177) Triadimefon(0.108)

ZK-X-371 BG 2 Cypermethrin(0.4) Lambda-Cyhalothrin(0.03)

Product=Bananas

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-3832 XX 2 Diphenylamine(0.012) Penconazole(0.013)

Product=Beans (with pods)

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

M been05 BG 2 Dithiocarbamates(0.888) Cypermethrin (sum)(0.03)

ZK-X-376 BG 2 Cypermethrin(0.4) Cyfluthrin(0.04)

Product=Cranberries

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-X-188 BG 2 Cyfluthrin(0.015) Lambda-Cyhalothrin(0.03)

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To avoid duplicates residues marked as part of sum are excludedTo avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 207Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

Product=Cucumbers

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

M cuc 13 BG 2 Dithiocarbamates(0.064) Metalaxyl (Metalaxyl including other mixtures of constituent isomers including Metalaxyl-M(sum of isomers))(0.025)

ZK-X-154 BG 2 Bifenthrin(0.04) Cypermethrin(0.07)

Product=Grapefruit

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

Moran 06 TR 2 Imazalil(0.581) Chlorpyrifos(0.077)

ZK-284 XX 3 Dimethomorph(0.035) Cyprodinil(0.034) Azoxystrobin(0.036)

ZK-X-189 BG 2 Lambda-Cyhalothrin(0.09) Cyfluthrin(0.015)

Product=Head cabbage

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-X-11 MK 2 Lambda-Cyhalothrin(0.02) Cypermethrin(0.04)

ZK-X-12 BG 2 Lambda-Cyhalothrin(0.03) Cypermethrin(0.03)

ZK-X-375 BG 3 Cypermethrin(0.3) Cyfluthrin(0.06) Lambda-Cyhalothrin(0.03)

Product=Leek

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-X-121 BG 2 Lambda-Cyhalothrin(0.2) Cypermethrin(0.3)

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To avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 208Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

Product=Lemons

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK 1538 TR 4 Prochloraz(0.44) Lambda-Cyhalothrin(0.04) Imazalil(0.84) Buprofezin(0.02)

ZK-4324 TR 2 Kresoxim-methyl(0.031) Azinphos-methyl(0.03)

ZK-4628 TR 2 Kresoxim-methyl(0.039) Dicofol (sum)(0.11)

ZK-X-186 GR 2 Lambda-Cyhalothrin(0.08) Cypermethrin(0.6)

ZK-X-258 TK 2 Bifenthrin(0.06) Cypermethrin(0.4)

Product=Mandarins

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

Moran 03 TR 2 Imazalil(1.41) Chlorpyrifos(0.347)

Moran 05 TR 3 Lambda-Cyhalothrin(0.025) Imazalil(1.38) Chlorpyrifos(0.151)

Moran 07 TR 2 Imazalil(0.915) Thiabendazole(0.91)

ZK-X-256 GR 2 Cypermethrin(0.2) Bifenthrin(0.08)

ZK-X-257 GR 2 Cypermethrin(0.3) Bifenthrin(0.06)

ZK-X-260 GR 3 Lambda-Cyhalothrin(0.02) Cypermethrin(0.3) Bifenthrin(0.06)

Product=Oranges

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

Moran 10 GR 2 Imazalil(0.82) Chlorpyrifos(0.058)

Moran 11 GR 2 Imazalil(2.12) Chlorpyrifos(0.026)

ZK-X-87 GR 4 Cypermethrin(0.2) Tolclofos-methyl(0.03) Chlorpyrifos-methyl(0.03) Bifenthrin(0.04)

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To avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 209Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

Product=Peaches

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

M peach 03 BG 2 Dithiocarbamates(0.055) Carbendazim and benomyl(0.038)

M peach 04 BG 2 Dithiocarbamates(0.165) Carbendazim and benomyl(0.02)

M peach 05 BG 2 Carbendazim and benomyl(0.02) Acetamiprid(0.173)

Product=Pears

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-4327 GR 2 Triadimefon(0.074) Methiocarb(0.081)

Product=Peas (without pods)

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-4168 BG 2 Procymidone(0.014) Penconazole(0.014)

Product=Peppers

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

Z-21996

TR 2 Malathion (sum of malathion and malaoxonexpressed as malathion)(0.014)

Formetanate(0.043)

Z-22018

TR 3 Tetradifon(0.038) Malathion (sum of malathion and malaoxonexpressed as malathion)(0.015)

Carbendazim andbenomyl(0.013)

Z-24224

TR 2 Malathion (sum of malathion and malaoxonexpressed as malathion)(0.01)

Carbendazim and benomyl(0.01)

Z-26216

TR 2 Malathion (sum of malathion and malaoxonexpressed as malathion)(0.012)

Formetanate(0.024)

Z-29253

TR 2 Oxamyl(0.17) Malathion (sum of malathion and malaoxonexpressed as malathion)(0.021)

Z-12837 TR 2 Oxamyl(0.862) Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)(0.012)

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To avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 210Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

Product=Peppers

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

Z-15673 TR 3 Procymidone(0.139) Oxamyl(0.149) Formetanate(0.075)

Z-16082 TR 2 Tetradifon(0.026) Procymidone(0.051)

Z-16629 TR 2 Methomyl and thiodicarb (sum of methomyl andthiodicarb expressed as methomyl)(0.025)

Malathion (sum of malathion and malaoxonexpressed as malathion)(0.29)

Z-17283 TR 2 Procymidone(0.033) Tetradifon(0.052)

Z-17740 TR 2 Procymidone(0.067) Formetanate(0.041)

ZK-3831 BG 3 Pyrimethanil(0.422) Methiocarb(0.047) Metalaxyl(0.191)

ZK-4164 BG 4 Pyriproxyfen(0.348) Methiocarb(0.024) Metalaxyl(0.212) Pyrimethanil(0.032)

Product=Rice

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

VT884 BG 2 Pirimiphos-methyl(0.03) Chlorpyrifos(0.02)

ZK-X-191 GR 2 Lambda-Cyhalothrin(0.3) Cypermethrin(0.7)

ZK-X-263 BG 2 Cypermethrin(0.2) Bifenthrin(0.02)

ZK-X-9-1 BG 3 Cypermethrin(0.2) Tolylfluanid(0.02) Lambda-Cyhalothrin(0.5)

ZK-X-9-2 ES 2 Tolylfluanid(0.02) Cypermethrin(0.03)

Product=Spinach

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-X-187 BG 3 Lambda-Cyhalothrin(0.07) Cypermethrin(0.02) Bifenthrin(0.02)

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To avoid duplicates residues marked as part of sum are excluded

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 211Table E2: Full listing of samples containing more than one residue by productAll samples from National and EU programmes, surveillance and enforcement

Product=Table grapes

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

VT1153 BG 2 Pyrimethanil(0.12) Cyprodinil(0.09)

VT1211 GR 3 Penconazole(0.1) Fenhexamid(2.03) Chlorpyrifos-methyl(0.06)

ZK 1284 BG 4 Indoxacarb as sum of the isomers S and R(0.21) Penconazole(0.13) Cyprodinil(1.5) Boscalid(1.1)

Product=Tomatoes

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

M tom 05 BG 2 Cypermethrin (sum)(0.031) Chlorpyrifos(0.016)

M tom 07 BG 2 Dithiocarbamates(0.08) Cypermethrin (sum)(0.064)

Z-15604 TR 2 Malathion (sum of malathion and malaoxon expressed as malathion)(0.013) Formetanate(0.035)

ZK-X-156 BG 2 Lambda-Cyhalothrin(0.05) Cypermethrin(0.02)

Product=Wheat

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

M flour 12 BG 2 Triadimefon (sum of Triadimefon and Triadimenol)(0.03) Chlorpyrifos-methyl(0.017)

Product=Wine grapes

Code CountryNo

Residues Compound1 Compound2 Compound3 Compound4

ZK-3830 BG 2 Pyriproxyfen(0.02) Bromopropylate(0.007)

ZK-4331 BG 4 Penconazole(0.125) Kresoxim-methyl(0.067) Fenarimol(0.169) Cyfluthrin (sum)(0.155)

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Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 212Table G: Summary of transmissions included in report by laboratory

Pesticide monitoring 2011 Bulgaria on August 24, 2012 at 01:24:35 PM 212Table G: Summary of transmissions included in report by laboratory

ReportingCountry Laboratory Transmission File

LaboratoryAccreditation Method Status Determinations Received

BG CLCTC 12492 AnalyticalMeasure1CLCTC.xml Accredited ISO/IEC17025 15503 23AUG12:12:47:43

BG CLVCE 11994 AnalyticalMeasure1CLVSEE.xml Accredited ISO/IEC17025 336 10AUG12:15:58:41

BG MZ02 12465 AnalyticalMeasure1 Burgas.xml Accredited ISO/IEC17025 2094 23AUG12:10:26:06

BG MZ03 12217 AnalyticalMeasure1 Varna.xml Accredited ISO/IEC17025 1160 16AUG12:15:58:49

BG MZ04 11776 AnalyticalMeasure1 VTarnovo.xml Accredited ISO/IEC17025 4104 03AUG12:13:40:31

BG MZ15 11773 AnalyticalMeasure1 Pleven.xml Accredited ISO/IEC17025 6018 03AUG12:13:22:40

BG MZ15_CLCTC 12469 AnalyticalMeasure1_669_1.xml Accredited ISO/IEC17025 13942 23AUG12:10:41:33

BG MZ15_CLCTC 12484 AnalyticalMeasure2_669_2.xml Accredited ISO/IEC17025 17127 23AUG12:11:55:33

BG MZ16 11775 AnalyticalMeasure1 Plovdiv.xml Accredited ISO/IEC17025 3904 03AUG12:13:37:23

BG MZ22 11940 AnalyticalMeasure1 SRZI.xml Accredited ISO/IEC17025 1536 09AUG12:10:06:11