ordering information - labtech s.r.o. · introduction 2 introduction. configuration guide ea-irms...

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Phone: +44 (0)1837 54446

Fax: +44 (0)1837 54544

E-mail: [email protected]

Mail: Elemental Microanalysis Ltd1 Hameldown RoadOkehampton Business ParkOkehamptonDevon EX20 1UBUnited Kingdom

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1

Contents

ContentsElemental

Microanalysis

2

4

5

6

7

9

10

11

12

Introduction

Configuration Guide

Eurovector EA-3028HT/EuroPyr

Hekatech HT-O

ThermoFinnigan TC/EA

ThermoFinnigan TC/EA Modified Lower Fitting

Consumables and Kits

Europa

Europa Glassware and O-rings

GC Combustion/Pyrolysis

Equilibration Reagents and Sundries

Isotope Reference Materials

Nafion Dryers®

Preparation System Vials and Seals

Faxback form

This additional brochure contains extra configurations and products that arespecific to CF and EA-IRMS applications.

All other consumables and products such as reagents, capsules, glassware etc that can be used in both EA and EA-IRMS applications can be found in our mainOrganic Elemental CHN/O/S catalogue.

Other literature availablefrom Elemental MicroanalysisIn addition to this catalogue a range of other catalogues and product sheets are available:

Catalogues

We publish catalogues covering the following areas of elemental analysis:

• Organic Elemental (CHN/O/S)

• Nitrogen/Protein

• Inorganic

• Carbon/Sulphur

• IRMS

Product sheets

Product sheets are available for every instrument we support. These cover all the common day-to-day items required to run your instrument. These sheets are laminated to help them survive in the lab environment.

Contract analysis service

We also offer a contract analysis service for a variety of (mainly) organic compounds. Full details are in this brochure.

All literature is available using the ‘fax-back’form on the rear cover of this catalogue orcan be downloaded from our website.

ElementalMicroanalysis

About the CompanyElemental Microanalysis grew from small beginnings almost 30 years ago as a micro-analytical laboratory to its current form as a leading manufacturer and supplier of consumables, supplies and other products for Elemental Analysers. We operate from our purpose-built factory and laboratory complex in Devon UK.

You learn a lot in 30 years - a lot about yourproducts - how to make them and how to usethem, a lot about your customers and theirneeds. We have been developing, refining andusing products for elemental analysis since 1976 and have a unique in-depth knowledge of instruments from all manufacturers.

These days we offer the world’s largest range of products for elemental analysers sending our products to customers across the globe.

We take great care with the quality of our products. The vast majority are manufactured in-house by our trained technicians within ourISO 9001:2000 accredited quality system. Butwe don’t just make the products - we use themevery day in our own analytical laboratory giving

us constant feedback on their performance. We do not compromise on quality and don’texpect you to either. Our total satisfaction guarantee backs up our commitment to our product quality.

‘Price is what you pay, value is what you get’. As the leading independent supplier of elementalanalysis consumables you can achieve substantialsavings in comparison to the prices charged bythe original supplier of your instrument. But weknow that you need more from a supplier thansimply low prices. You need to buy with the confidence that your analysis will not becompromised by poor quality consumablesand the knowledge that your supplier has all the resources to provide the full range of supportthat you expect.

We will always treat our customers with honestyand integrity. If we do make a mistake we don’ttry to hide it - we recognise it and put it right. We won’t sell you short measure and we won’tmislead you in any way. Our business is built on long-term relationships as our customers willtestify - many have been with us for more than20 years.

Intr

oduc

tion

2

Introduction

Configuration GuideEA-IRMS Analysis

Note: See CHNOS catalogue for other EA configurations


Pro

duct

Qty

Eur

ovec

tor

noC

at n

o

O-r

ing

for c

eram

ic re

acto

rE

1353

8E

1506

Cer

amic

Out

er, 1

7mm

E12

507

C11

02G

lass

y C

arbo

n Tu

beE

1252

9C

7004

Nic

kelis

ed C

arbo

n20

mm

E10

145

B11

82G

lass

y C

arbo

n C

hips

120m

mE

1052

1C

7003

Qua

rtz W

ool

20m

mE

1051

4B

1017

Qua

rtz W

ool

20m

mE

1051

4B

1017

O-r

ing,

17m

m,

botto

m q

uick

fit

E13

539

E15

07

1 2 3 4 5 6 7 8

Key

1 82 3 4 5 6 7

1 72 3 4 5 6

Pro

duct

Qty

Eur

ovec

tor

noC

at n

o

O-r

ing

for c

eram

ic re

acto

rE

1353

8E

1506

Cer

amic

Out

er, 1

7mm

E12

507

C11

02G

lass

y C

arbo

n Tu

beE

1252

9C

7004

Gla

ssy

Car

bon

Chi

ps14

0mm

E10

521

C70

03Q

uartz

Woo

l20

mm

E10

514

B10

17Q

uartz

Woo

l20

mm

E10

514

B10

17O

-rin

g, 1

7mm

, bo

ttom

qui

ck fi

tE

1353

9E

1507

1 2 3 4 5 6 7

Key

Pro

duct

Qty

Eur

ovec

tor

noC

at n

o

O-r

ing,

18m

mE

1353

6E

1504

Mod

ified

Qua

rtz R

eact

orE

1251

2C

1056

Chr

ome

Cat

alys

t (M

ax-C

hrom

e)90

mm

E10

103

B14

50Q

uartz

Woo

l10

mm

E10

514

B10

17O

-rin

g, 6

mm

botto

m q

uick

fit

E13

540

E15

08

1 2 3 4 5

Key

1

2 3 4

5

GC

COLU

MN

S

Pro

duct

Eur

ovec

tor

noC

at n

o

GC

Col

umn,

1m

Sta

inle

ss S

teel

E11

520

E30

01G

CC

olum

n, 1

.5m

Sta

inle

ss S

teel

E11

521

E30

09

HY

DRO

GEN

OXY

GEN

Hig

h Te

mpe

ratu

re

Pyr

olys

isH

igh

Tem

pera

ture

P

yrol

ysis

Euro

vect

or E

A-30

28HT

/Eur

oPyr

4

H IN

LIQ

UIDS

USI

NG

CHRO

ME

CATA

LYST

Pro

duct

Qty

Ther

moF

. no

Cat

no

O-r

ing,

Vito

n11

2112

0E

6053

Gra

phite

Tub

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2135

1C

7010

Cer

amic

Tub

e11

2132

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1101

Gla

ssy

Car

bon

Rea

ctor

1121

310

C70

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raph

ite C

ruci

ble

1117

332

C70

12G

lass

y C

arbo

n C

hips

1117

400

C70

02S

ilver

Woo

l5m

m11

1743

0B

1119

Gla

ssy

Car

bon

Chi

ps11

1740

0C

7002

Qua

rtz W

ool

20m

m10

8777

0B

1017

GC

Col

umn

0.6m

1/4

Sta

inle

ss S

teel

1121

030

E30

35

1 2 3 4 5 6 7 8 9 10

Key

Pro

duct

Qty

Ther

moF

. no

Cat

no

O-r

ing,

Vito

n11

2112

0E

6053

Gra

phite

Tub

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3208

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7011

Cer

amic

Tub

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2132

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1101

Gla

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Car

bon

Rea

ctor

1121

310

C70

01G

lass

y C

arbo

n C

hips

1117

400

C70

02G

lass

y C

arbo

n C

hips

1117

400

C70

02Q

uartz

Woo

l20

mm

1087

770

B10

17G

CC

olum

n 0.

6m 1

/4 S

tain

less

Ste

el11

2103

0E

3035

1 2 3 4 5 6 7 8

Key

1 2 3 4 5 6 7

8

1 2 3 4 5 6 7 9

10

8 7

SOLI

DSA

MPL

ESLI

QUID

SAM

PLES

270m

m27

0mm

20m

m

Hig

h Te

mpe

ratu

re

Pyr

olys

isH

igh

Tem

pera

ture

P

yrol

ysis

5

Ther

moF

inni

gan

TC/E

A

Pro

duct

Qty

Hek

atec

h no

Cat

no

Cer

amic

Rea

ctor

HE

468

110

C11

03G

lass

y C

arbo

n Tu

beH

E 4

6860

100

C70

04N

icke

lised

Car

bon

10m

mH

E 3

3823

800

B11

82G

lass

y C

arbo

n C

hips

135m

mH

E 3

3823

850

C70

03N

icke

l Woo

l5m

mH

E 3

3825

00B

1007

GC

Col

umn,

1m

Sta

inle

ss S

teel

HE

260

0790

0E

3001

1 2 3 4 5 6

Key

1 2 3 4 5

HEK

ATE

CHH

T-O

6

Hig

h Te

mpe

ratu

re

Pyr

olys

is

Heka

tech

HT-

O

ElementalMicroanalysis Consumables and Kits

Nickel Wool B1007

Product Pack Cat.no.

Glassy carbon tube 12 x 7 x 356 1 C7001

Glassy carbon tube 12 x 9 x 453 for use with E4405 1 C7007

Glassy carbon tube 12 x 7 x 450

(one end closed with 2mm central hole) 1 C7005

Glassy carbon tube 12 x 9 x 400 1 C7004

Glassy carbon chips (splinter powder) 3-4mm 25g C7002

Glassy carbon chips (splinter powder) 2-3mm 25g C7003

Graphite crucible 4.5 x 3.5 x 30mm 1 C7012

Quartz wool (very pure, very fine) 5g B1017



Nickel wool 2g B1007

Silver wool 10g B1119

Chrome catalyst (fine powder) 100g B1450

Chrome catalyst (fine powder) 25g B1451

Nickelised Carbon 30% Ni, granular 0.3-0.85mm 5g B1086






Spares Kits for IsoPrime™ ElementalAnalyser ModulesProduct OEM Cat.no.

EA-CN 1000 analysis kit 6063056 X3250

EA-O and/or H for solid samples

(High temperature) 1000 analyses 6062979 X3251

EA-Sulphur 1000 analysis kit 6062974 X3252

EA-Hydrogen kit for liquid samples

(low temperature) 6062977 X3253

EA-Oxygen kit for liquid samples 6062978 X3254

(High temperature)6

Cons

umab

les

and

Kits

Modified Lower Fitting for Improved Analysis of WatersThe adapter channels the helium flow up between the ceramic outer anddown through the centre of the glassy carbon tube ensuring all water vapour is swept down into the reactive zone. Use of this fitting requires a different length glassy carbon inner from standard (see below).

Product Part no.Adapter E4405O-ring E6054 (pack of 2)Glassy carbon tube 12 x 9 x 453 C7007

TC/EA SparesProduct Thermo No. Cat no.Replacement TC/EA Furnace Element 35450010 E4406Furnace Repair* E4407

*Furnace repair - a faulty furnace may be may sent to Elemental Microanalysis for examination with a new element and/or thermocouple fitted if required.

Ther

moF

inni

gan

TC/E

A

Modified Lower Fitting

Glassy Carbon ChipsC7003

Graphite Crucible C7012

Glassy Carbon Tube

Nickelised CarbonB1181

11 2 8 9 3

7

2 3 4 3 3 6 3 75

Key

Pro

duct

Qty

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opa

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-rin

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40Q

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1001

016

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on

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90m

m-

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82C

oppe

r Wire

s, h

igh

purit

y80

mm

C10

0104

2B

1035

Qua

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hips

10

mm

C10

0101

7B

1008

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ing,

low

erE

1005

550

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C10

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Cop

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1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 A B

10 11 12 13 12

11 2 8 9 3 7

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7

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10 11 12 13 12

11 12 1514 12

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N &

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SDE

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NDE

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AB

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boso

rb 6

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mes

hC

1001

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B10

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12-

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C10

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sep

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epar

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n co

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Pre

pack

ed R

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ion

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(inc

lude

s C

1050

line

r)Tr

ansp

aren

tX

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sluc

ent

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repa

cked

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n Tu

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1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 A B

Key

15

9 9

A

A

AB

EURO

PARO

BO

PREP

CN

HPY

ROLY

SIS

OPY

ROLY

SIS

8

6

C1063 C1032

C1030

C1041C1040C1039

C1094 C2030

C1050

Pre-packed tubes for this instrument are available -please see configuration guide for details.

E1042

E1420

E1421

E1001

E1004

O-rings shown actual size

Glassware and O-rings

Europa GlasswareDescription Pack OEM Cat no.

Reduction Tube 1 C1001014 C1030

Scrubber 1 C1001015 C1032

Reaction/Reduction Tube, transparent 1 C1001012 C1040

Reaction/Reduction Tube, translucent 1 C1001013 C1041

Reaction/Reduction Tube, transparent, heavy wall 1 - C1039

Sleeve insert 180mm (Open both ends) 1 C1001048 C1050

Scrubber 1 E1002687 C1063

Sleeve insert 220mm (Open both ends) 1 C1094

Sleeve insert 220mm (Closed one end) 1 C2030

Europa O-ringsProduct Pack OEM Cat no

O-ring Viton 10 E1001O-ring Nitrile 10 E1004Seal Viton Chamfered Square Profile 5 E1042O-ring 1 E1005669 E1420O-ring 1 E1002684 E1421


Glas

swar

e an

d O

-rin

gs -

Euro

pa

9

Equilibration Reagents and Sundries

Product Pack Cat no

Platinum Catalysts sticks for HD equilibration 50 sticks B1452

5% Pt on Alumina -325 mesh powder 10g B1453

Tapered glass inserts 1000 E2800

Ceramic Tube

ElementalMicroanalysis GC Combustion/Pyrolysis

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Furnace Reaction TubesCeramic

Length OD ID Cat no Application

630mm 6mm 0.7mm C1110 GVI

600mm 3mm 0.5mm C1111 Thermo/GVI

400mm 1.6mm 0.8mm C1112 Europa/PDZ

300mm 1.55mm 0.6mm C1077 Europa/Thermo

QuartzLength OD ID Cat no Application

630mm 6mm 0.7mm C1115 GVI

220mm 6mm 1.0mm C1075 Europa/PDZ

300mm 6mm 1.0mm C1076 Europa

Note: quartz and ceramic tubes can be supplied in different lengths. Please contact us with your requirements.

Packing MaterialsProduct Pack size Cat no

Copper Oxide Wires 1% Pt 1%NiO 5g B1149

Copper Oxide Wires 3% Pt 1%NiO 5g B1151

Copper Wire 0.125mm diameter 10m D9101

Platinum Wire 0.125mm diameter 1m D9100

Nickel Wire 0.125mm diameter 10m D9102

Copper Granules, fine 0.05-0.2mm 100g B1108

Prepacked GC Reaction TubesLength OD ID Material Packing Cat no

600mm 3mm 0.5mm Ceramic Cu and Pt wires X1500

400mm 1.6mm 0.8mm Ceramic Cu wires X1501

400mm 1.6mm 0.8mm Ceramic Cu and Pt wires X1502

400mm 1.6mm 0.8mm Ceramic Ni wires X1503

630mm 6mm 0.7mm Quartz Copper Oxide wires

1% Pt, 1% NiO X1504

Note: many combinations of wire types, numbers of strands etc. are possible.

Please contact us with your Prepacked GC Reaction Tube requirements.

Quartz TubeC1076

A A1/8"

1/8"

1/8"

14"

Nafion Dryers®

Isotope Reference MaterialsElemental

Microanalysis

Complete DryerProduct Cat no

Stainless steel body, 1/8” end fittings (A) E2810Stainless steel body, 1/16” end fittings (A) E2811Fluoropolymer body, 1/8” end fittings (A) E2812Polypropylene body, 1/8” end fittings (A) E2813

Replacement Inner ElementsProduct Cat no

Elements, 12” long, 0.05” OD tubing, flanged end piecesPolypropylene ends E2820Fluoropolymer ends E2821Stainless steel ends E2822

Nafion® water removal dryers can be supplied as complete units or replacement inner elements.

Dryers and elements are supplied with 0.05” OD, 0.04” ID Nafion® tubing.

Dimensions

Reference Materials (RM)Cat no Standard Pack %C ∂C13 %N ∂N15 %S ∂S34

B2151 Sediment 5g 6.5 -26 0.5 +4 0.9 +4B2153 Soil 5g 1.5 -27 0.15 +7 0.03 +5B2155 Protein (Casein) 5g 47 -27 14 +6 0.9 +6B2157 Wheat Flour 5g 40 -27 1.5 +3 0.1 -1B2159 Sorghum Flour 5g 42 -14 1.5 +2 0.1 +10

Uncertified Working Reference MaterialsCat no Standard Pack ∂C13 ∂N15

B2172 Olive Oil 5g -28.5 -B2174 Urea 5g -45 -0.8

Isotope Reference Materials from Elemental Microanalysis aretraceable to primary standards issued by IAEA Vienna.

These materials are supplied with Certificates of Analysis.

Values shown are indicative and may vary slightly from batch to batch.

Actual values shown on certificate.

11

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Nafion® is a registered trademark of E.I. DuPont

ElementalMicroanalysis Preparation System Vials and Seals

12

Prep

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Syst

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ials

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Sea

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Description Part No

4.5ml Borosilicate Vial - round bottomed, 46 x 15.5mm Pack of 1000

Non-evacuated, unlabelled, seal + white cap E2830Evacuated, unlabelled, seal + white cap E2831Non-evacuated, labelled, seal + white cap E2832Evacuated, labelled, seal + white cap E2833

5.9ml Soda Glass Vial - flat bottomed, 55 x 15.5mmPack of 1000


12ml Soda Glass Vial - flat bottomed, 101 x 15.5mmPack of 1000


12ml Borosilicate Vial - round bottomed, 101 x 15.5mmPack of 1000


12ml Soda Glass Vial - flat bottomed, 101 x 15.5mmSilicone coated for C13 Breath Testing, Pack of 1000


12ml Borosilicate Vial - round bottomed, 104 x 15.5mmPack of 1000The new thread profile on this Exetainer® gives a very tight screw fit, and is designed to avoid any cap movement when samples are heated - eg. on a GasBench.


Caps are available in a variety of colours, also replacement caps and seals - please enquire for details.

Exetainer® is a registered trademark of Labco Ltd.

LITERATURE REQUEST FAXBACK FORM

Elemental Microanalysis Ltd • Hameldown Road • Okehampton Business Park • Exeter Road • Okehampton • Devon EX20 1UB • United KingdomTel: +44 (0)1837 54446 • Fax: +44 (0)1837 54544 • E-mail: [email protected] • Website: www.microanalysis.co.uk

Company Registration No: 1281028 • VAT No: 217 5194 65

“the centre of excellence in elemental analysis”

Micro/CHN(OS) InstrumentsThermoFinnigan Flash EA™1112 CHNOSThermoFinnigan Flash EA™1112 NC/SThermoFinnigan (Carlo Erba/Fison) EA1110ThermoFinnigan (Carlo Erba/Fison) EA1108ThermoFinnigan (Carlo Erba/Fison) EA1106ThermoFinnigan (Carlo Erba/Fison) EA1102/1104ThermoFinnigan (Carlo Erba/Fison) NA2500 N/NC/NCSThermoFinnigan (Carlo Erba/Fison) NA1500 (Series 1&2)

Perkin Elmer 2400Perkin Elmer 240 Series ABCPerkin Elmer 440Perkin Elmer 2410

Exeter Analytical (CEC) CE440Exeter Analytical (CEC) 240

Europa RoboprepEuropa AncaEuropa Integra

Elementar (Foss Heraeus) Vario ELElementar (Foss Heraeus) CHN Rapid

EuroVector EA3000

Leco® CHN-900Leco® CHN-932Leco® CHN-1000Leco® CHN-2000Leco® CHN-600Leco® CHN-800Leco® Truspec CHN/CN

Costech ECS 4010

Name

Organisation

Address

Tel

Fax

E-mail

CataloguesCHNOSInorganicCarbon/SulphurNitrogen/Protein

Contract Analysis Service

Please tick to request the relevant literature.

For full details of all the products we supply for your instrument please copy this page and fax it back to us.

+44 (0)1837 54544 or your local dealer:

Elemental Microanalysis LtdHameldown Road

Okehampton Business ParkExeter RoadOkehampton

Devon EX20 1UBUnited Kingdom

Tel: +44 (0)1837 54446Fax: +44 (0)1837 54544

E-mail: [email protected]

www.microanalysis.co.uk

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