o'donnell, david (deq) [mailto:[email protected] ... · fw 413 hall street tables and...
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![Page 1: O'Donnell, David (DEQ) [mailto:ODONNELLD@michigan.gov ... · FW 413 Hall Street Tables and Figures- - GR VI MDEQ DATA 2.htm[6/13/2016 12:08:53 PM]-800-424-8802, or-. From: Bandlow,](https://reader034.vdocuments.mx/reader034/viewer/2022050111/5f486cf2440cc03d8b73e370/html5/thumbnails/1.jpg)
FW 413 Hall Street Tables and Figures- - GR VI MDEQ DATA 2.htm[6/13/2016 12:08:53 PM]
From: O'Donnell, David (DEQ) [mailto:[email protected]] Sent: Thursday, June 09, 2016 8:44 AMTo: Bandlow, David (DEQ) <[email protected]>Cc: Hendershott, Abigail (DEQ) <[email protected]>; Nightingale, Elizabeth <[email protected]>Subject: RE: 413 Hall Street, Tables and Figures
From: Bandlow, David (DEQ) Sent: Thursday, June 09, 2016 8:12 AMTo: O'Donnell, David (DEQ)Cc: Hendershott, Abigail (DEQ); Nightingale, Elizabeth; Schram, Tammy (DEQ)Subject: Fw: 413 Hall Street, Tables and FiguresImportance: High
David, Please see note below from Betsy. Can we provide her with all of the raw lab data that we have in the 413 Hall Street file today? Thanks, Dave
From: Nightingale, Elizabeth <[email protected]>Sent: Wednesday, June 8, 2016 11:47:40 PMTo: Bandlow, David (DEQ)Subject: RE: 413 Hall Street, Tables and Figures Hi guys – I need to write an action memo ASAP to get more funding for this response, and I need to include your raw lab data in my record for the action memo. Could I possibly request the raw lab data associated with these figures ASAP? Thanks, Betsy Betsy NightingaleFederal On-Scene CoordinatorUnited States Environmental Protection Agency, Region 59311 Groh RoadGrosse Ile, MI 48138 office: 734-692-7665cell: 734-770-8402fax: 734-692-7677email: [email protected]
Report spills to the National Response Center at:
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FW 413 Hall Street Tables and Figures- - GR VI MDEQ DATA 2.htm[6/13/2016 12:08:53 PM]
-800-424-8802, or-www.nrc.uscg.mil.
From: Bandlow, David (DEQ) [mailto:[email protected]] Sent: Tuesday, June 07, 2016 9:38 AMTo: Nightingale, Elizabeth <[email protected]>Cc: [email protected]: Fw: 413 Hall Street, Tables and Figures
From: Trevor Painter (Global) <[email protected]>Sent: Friday, May 27, 2016 1:11:07 PMTo: Bandlow, David (DEQ)Cc: Hendershott, Abigail (DEQ); Jill Auger; Andy GirardSubject: 413 Hall Street, Tables and Figures Dear Mr. Bandlow,
Global has compiled the requested tables and figures for the 413 Hall Street Site in Grand Rapids, MI. If you have any questions, don't not hesitate to contact me. Sincerely,
Trevor Painter
Trevor D. Painter
Staff Engineer
Global Environmental Engineering
O: (231) 264-3000; 302
M: (231) 631-3472
363 W. South Airport Road
Traverse City, MI 49686
www.globaleei.com
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
MDEQ-RRD-GRAND RAPIDS
RE: HALL STREET
Grand Rapids, MI 49503-2341
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods
approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .
Sincerely,
14 January 2016 Work Order: 1601031
Price: $690.00
George Krisztian
Laboratory Director
Lab Work Order # 1601031
Page 1 of 9Page 1 of 10
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
Project:
Project Manager:
Reported:
MDEQ-RRD-GRAND RAPIDS
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
HALL STREET
Grand Rapids MI, 49503-2341
Site Code: 4100112101/14/2016
Sample ID Laboratory ID Date SampledMatrix Date Received
Analytical Report for Samples
Qualifier
1601031-01 Water 01/11/2016GP 11 @25' 01/11/2016
1601031-02 Water 01/11/2016GP 11 @30' 01/11/2016
1601031-03 Water 01/11/2016GP 11 @35' 01/11/2016
Notes and Definitions
X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene
have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.
A03 Result(s) and reporting limit(s) are estimated due to low matrix spike recovery.
Reporting LimitRL
Indicates compound analyzed for but not detectedND
Not ApplicableNA
Lab Work Order # 1601031
Page 2 of 9Page 2 of 10
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601031-01
RLCAS #
Client ID: GP 11 @25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/11/16ND B6A1106
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/11/16ND B6A1106
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/11/16ND B6A1106
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/11/16ND B6A1106
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/11/16ND B6A1106
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/11/16ND B6A1106
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/11/16ND B6A1106
5.0 ug/L 1 82602-Hexanone591-78-6 01/11/16ND B6A1106
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/11/16ND B6A1106
20 A03ug/L 1 82602-Propanone (acetone)67-64-1 01/11/1625 B6A1106
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/11/16ND B6A1106
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Benzene71-43-2 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromobenzene108-86-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromoform75-25-2 01/11/16ND B6A1106
5.0 ug/L 1 8260Bromomethane74-83-9 01/11/16ND B6A1106
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/11/16ND B6A1106
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/11/16ND B6A1106
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/11/16ND B6A1106
5.0 ug/L 1 8260Chloroethane75-00-3 01/11/16ND B6A1106
1.0 ug/L 1 8260Chloroform67-66-3 01/11/161.4 B6A1106
5.0 ug/L 1 8260Chloromethane74-87-3 01/11/16ND B6A1106
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/11/16ND B6A1106
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/11/16ND B6A1106
5.0 ug/L 1 8260Cyclohexane110-82-7 01/11/16ND B6A1106
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/11/16ND B6A1106
Lab Work Order # 1601031
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601031-01
RLCAS #
Client ID: GP 11 @25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/11/16ND B6A1106
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/11/16ND B6A1106
5.0 ug/L 1 8260Diethyl ether60-29-7 01/11/16ND B6A1106
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/11/16ND B6A1106
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/11/16ND B6A1106
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/11/16ND B6A1106
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/11/16ND B6A1106
1.0 ug/L 1 8260Methyl iodide74-88-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Methylene chloride75-09-2 01/11/16ND B6A1106
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/11/16ND B6A1106
5.0 Xug/L 1 8260Naphthalene91-20-3 01/11/16ND B6A1106
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/11/16ND B6A1106
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/11/16ND B6A1106
1.0 ug/L 1 8260o-Xylene95-47-6 01/11/16ND B6A1106
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/11/16ND B6A1106
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/11/16ND B6A1106
1.0 ug/L 1 8260Styrene100-42-5 01/11/16ND B6A1106
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/11/16ND B6A1106
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/11/16ND B6A1106
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/11/16ND B6A1106
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/11/16ND B6A1106
1.0 ug/L 1 8260Toluene108-88-3 01/11/16ND B6A1106
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/11/16ND B6A1106
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/11/16ND B6A1106
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/11/16ND B6A1106
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/11/16ND B6A1106
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/11/16ND B6A1106
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/11/16ND B6A1106
85-115101 %Surrogate: Bromofluorobenzene 826001/11/16 B6A1106
82.7-115101 %Surrogate: Dibromofluoromethane 826001/11/16 B6A1106
85-11599.9 %Surrogate: Toluene-d8 826001/11/16 B6A1106
Lab Work Order # 1601031
Page 4 of 9Page 4 of 10
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601031-02
RLCAS #
Client ID: GP 11 @30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/11/16ND B6A1106
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/11/16ND B6A1106
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/11/16ND B6A1106
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/11/16ND B6A1106
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/11/16ND B6A1106
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/11/16ND B6A1106
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/11/16ND B6A1106
5.0 ug/L 1 82602-Hexanone591-78-6 01/11/16ND B6A1106
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/11/16ND B6A1106
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/11/16ND B6A1106
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/11/16ND B6A1106
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Benzene71-43-2 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromobenzene108-86-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromoform75-25-2 01/11/16ND B6A1106
5.0 ug/L 1 8260Bromomethane74-83-9 01/11/16ND B6A1106
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/11/16ND B6A1106
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/11/16ND B6A1106
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/11/16ND B6A1106
5.0 ug/L 1 8260Chloroethane75-00-3 01/11/16ND B6A1106
1.0 ug/L 1 8260Chloroform67-66-3 01/11/161.6 B6A1106
5.0 ug/L 1 8260Chloromethane74-87-3 01/11/16ND B6A1106
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/11/16ND B6A1106
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/11/16ND B6A1106
5.0 ug/L 1 8260Cyclohexane110-82-7 01/11/16ND B6A1106
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/11/16ND B6A1106
Lab Work Order # 1601031
Page 5 of 9Page 5 of 10
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601031-02
RLCAS #
Client ID: GP 11 @30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/11/16ND B6A1106
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/11/16ND B6A1106
5.0 ug/L 1 8260Diethyl ether60-29-7 01/11/16ND B6A1106
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/11/16ND B6A1106
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/11/16ND B6A1106
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/11/16ND B6A1106
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/11/16ND B6A1106
1.0 ug/L 1 8260Methyl iodide74-88-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Methylene chloride75-09-2 01/11/16ND B6A1106
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/11/16ND B6A1106
5.0 Xug/L 1 8260Naphthalene91-20-3 01/11/16ND B6A1106
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/11/16ND B6A1106
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/11/16ND B6A1106
1.0 ug/L 1 8260o-Xylene95-47-6 01/11/16ND B6A1106
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/11/16ND B6A1106
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/11/16ND B6A1106
1.0 ug/L 1 8260Styrene100-42-5 01/11/16ND B6A1106
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/11/16ND B6A1106
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/11/16ND B6A1106
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/11/16ND B6A1106
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/11/16ND B6A1106
1.0 ug/L 1 8260Toluene108-88-3 01/11/16ND B6A1106
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/11/16ND B6A1106
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/11/16ND B6A1106
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/11/16ND B6A1106
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/11/16ND B6A1106
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/11/16ND B6A1106
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/11/16ND B6A1106
85-115103 %Surrogate: Bromofluorobenzene 826001/11/16 B6A1106
82.7-11599.9 %Surrogate: Dibromofluoromethane 826001/11/16 B6A1106
85-115101 %Surrogate: Toluene-d8 826001/11/16 B6A1106
Lab Work Order # 1601031
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601031-03
RLCAS #
Client ID: GP 11 @35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/11/16ND B6A1106
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/11/16ND B6A1106
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/11/16ND B6A1106
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/11/16ND B6A1106
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/11/16ND B6A1106
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/11/16ND B6A1106
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/11/16ND B6A1106
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/11/16ND B6A1106
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/11/16ND B6A1106
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/11/16ND B6A1106
5.0 ug/L 1 82602-Hexanone591-78-6 01/11/16ND B6A1106
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/11/16ND B6A1106
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/11/16ND B6A1106
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/11/16ND B6A1106
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Benzene71-43-2 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromobenzene108-86-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/11/16ND B6A1106
1.0 ug/L 1 8260Bromoform75-25-2 01/11/16ND B6A1106
5.0 ug/L 1 8260Bromomethane74-83-9 01/11/16ND B6A1106
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/11/16ND B6A1106
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/11/16ND B6A1106
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/11/16ND B6A1106
5.0 ug/L 1 8260Chloroethane75-00-3 01/11/16ND B6A1106
1.0 ug/L 1 8260Chloroform67-66-3 01/11/161.8 B6A1106
5.0 ug/L 1 8260Chloromethane74-87-3 01/11/16ND B6A1106
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/11/16ND B6A1106
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/11/16ND B6A1106
5.0 ug/L 1 8260Cyclohexane110-82-7 01/11/16ND B6A1106
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/11/16ND B6A1106
Lab Work Order # 1601031
Page 7 of 9Page 7 of 10
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601031-03
RLCAS #
Client ID: GP 11 @35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/11/16ND B6A1106
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/11/16ND B6A1106
5.0 ug/L 1 8260Diethyl ether60-29-7 01/11/16ND B6A1106
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/11/16ND B6A1106
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/11/16ND B6A1106
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/11/16ND B6A1106
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/11/16ND B6A1106
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/11/16ND B6A1106
1.0 ug/L 1 8260Methyl iodide74-88-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Methylene chloride75-09-2 01/11/16ND B6A1106
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/11/16ND B6A1106
5.0 Xug/L 1 8260Naphthalene91-20-3 01/11/16ND B6A1106
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/11/16ND B6A1106
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/11/16ND B6A1106
1.0 ug/L 1 8260o-Xylene95-47-6 01/11/16ND B6A1106
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/11/16ND B6A1106
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/11/16ND B6A1106
1.0 ug/L 1 8260Styrene100-42-5 01/11/16ND B6A1106
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/11/16ND B6A1106
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/11/16ND B6A1106
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/11/16ND B6A1106
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/11/16ND B6A1106
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/11/16ND B6A1106
1.0 ug/L 1 8260Toluene108-88-3 01/11/16ND B6A1106
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/11/16ND B6A1106
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/11/16ND B6A1106
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/11/16ND B6A1106
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/11/16ND B6A1106
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/11/16ND B6A1106
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/11/16ND B6A1106
85-115104 %Surrogate: Bromofluorobenzene 826001/11/16 B6A1106
82.7-115100 %Surrogate: Dibromofluoromethane 826001/11/16 B6A1106
85-115100 %Surrogate: Toluene-d8 826001/11/16 B6A1106
Lab Work Order # 1601031
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Page 9 of 10
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Page 10 of 10
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
MDEQ-RRD-GRAND RAPIDS
RE: HALL STREET
Grand Rapids, MI 49503-2341
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods
approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .
Sincerely,
15 January 2016 Work Order: 1601052
Price: $920.00
George Krisztian
Laboratory Director
Lab Work Order # 1601052
Page 1 of 19Page 1 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
Project:
Project Manager:
Reported:
MDEQ-RRD-GRAND RAPIDS
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
HALL STREET
Grand Rapids MI, 49503-2341
Site Code: 4100112101/15/2016
Sample ID Laboratory ID Date SampledMatrix Date Received
Analytical Report for Samples
Qualifier
1601052-01 Water 01/13/2016GP13@25' 01/12/2016
1601052-02 Water 01/13/2016GP13@30' 01/12/2016
1601052-03 Water 01/13/2016GP13@35' 01/12/2016
1601052-04 Water 01/13/2016GP13@40' 01/12/2016
1601052-05 Water 01/13/2016GP14@25' 01/13/2016
1601052-06 Water 01/13/2016GP14@30' 01/13/2016
1601052-07 Water 01/13/2016GP14@35' 01/13/2016
1601052-08 Water 01/13/2016GP14@40' 01/13/2016
Notes and Definitions
X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene
have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.
A11 Result is estimated due to high initial verification standard criteria failure.
A09 Result is estimated due to high recovery of batch quality control.
A06 Result is estimated due to high continuing calibration standard criteria failure.
Reporting LimitRL
Indicates compound analyzed for but not detectedND
Not ApplicableNA
Lab Work Order # 1601052
Page 2 of 19Page 2 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-01
RLCAS #
Client ID: GP13@25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/161.0 B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/1621 B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 3 of 19Page 3 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-01
RLCAS #
Client ID: GP13@25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
10 ug/L 10 8260Tetrachloroethylene127-18-4 01/14/16560 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/1610 B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11595.7 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115102 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115104 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
Page 4 of 19Page 4 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-02
RLCAS #
Client ID: GP13@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/168.6 B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 5 of 19Page 5 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-02
RLCAS #
Client ID: GP13@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/16140 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/163.0 B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11595.3 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
Page 6 of 19Page 6 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-03
RLCAS #
Client ID: GP13@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/163.4 B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 7 of 19Page 7 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-03
RLCAS #
Client ID: GP13@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/16100 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/161.4 B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11594.8 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
Page 8 of 19Page 8 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-04
RLCAS #
Client ID: GP13@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 9 of 19Page 9 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-04
RLCAS #
Client ID: GP13@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/1646 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/161.1 B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11598.5 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115103 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-11599.7 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
Page 10 of 19Page 10 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-05
RLCAS #
Client ID: GP14@25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 11 of 19Page 11 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-05
RLCAS #
Client ID: GP14@25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/1662 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11597.1 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115103 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
Page 12 of 19Page 12 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-06
RLCAS #
Client ID: GP14@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 13 of 19Page 13 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-06
RLCAS #
Client ID: GP14@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/163.3 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11598.4 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115101 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
Page 14 of 19Page 14 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-07
RLCAS #
Client ID: GP14@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
Page 15 of 19Page 15 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-07
RLCAS #
Client ID: GP14@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/164.7 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11598.3 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115103 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-08
RLCAS #
Client ID: GP14@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1304
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1304
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1304
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1304
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1304
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1304
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1304
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1304
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1304
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1304
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1304
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1304
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1304
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1304
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1304
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1304
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1304
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1304
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1304
Lab Work Order # 1601052
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601052-08
RLCAS #
Client ID: GP14@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1304
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1304
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1304
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1304
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1304
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1304
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1304
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1304
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1304
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1304
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1304
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1304
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1304
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1304
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1304
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1304
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/164.4 B6A1304
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1304
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1304
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1304
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1304
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1304
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1304
85-11596.3 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1304
82.7-115105 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1304
85-115102 %Surrogate: Toluene-d8 826001/13/16 B6A1304
Lab Work Order # 1601052
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
MDEQ-RRD-GRAND RAPIDS
RE: HALL STREET
Grand Rapids, MI 49503-2341
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods
approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .
Sincerely,
20 January 2016 Work Order: 1601033
Price: $1,840.00
George Krisztian
Laboratory Director
Lab Work Order # 1601033
Page 1 of 19Page 1 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
Project:
Project Manager:
Reported:
MDEQ-RRD-GRAND RAPIDS
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
HALL STREET
Grand Rapids MI, 49503-2341
Site Code: 4100112101/20/2016
Sample ID Laboratory ID Date SampledMatrix Date Received
Analytical Report for Samples
Qualifier
1601033-01 Water 01/12/2016GP11@40' 01/11/2016
1601033-02 Water 01/12/2016GP11@45' 01/11/2016
1601033-03 Water 01/12/2016GP11@50' 01/11/2016
1601033-04 Water 01/12/2016GP11@55' 01/11/2016
1601033-05 Water 01/12/2016GP12@25' 01/12/2016
1601033-06 Water 01/12/2016GP12@30' 01/12/2016
1601033-07 Water 01/12/2016GP12@35' 01/12/2016
1601033-08 Water 01/12/2016GP12@40' 01/12/2016
Notes and Definitions
X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene
have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.
T Reported value is less than the reporting limit (RL). Result is estimated.
A07 Result(s) and reporting limit(s) are estimated due to poor precision.
A06 Result is estimated due to high continuing calibration standard criteria failure.
A04 Result is estimated due to high matrix spike recovery.
Reporting LimitRL
Indicates compound analyzed for but not detectedND
Not ApplicableNA
Case Narrative
Priority Samples
Lab Work Order # 1601033
Page 2 of 19Page 2 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-01
RLCAS #
Client ID: GP11@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205
5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205
5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Chloroform67-66-3 01/12/162.0 B6A1205
5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205
5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205
Lab Work Order # 1601033
Page 3 of 19Page 3 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-01
RLCAS #
Client ID: GP11@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205
5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205
5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205
1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205
85-115102 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205
82.7-115101 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205
85-115101 %Surrogate: Toluene-d8 826001/12/16 B6A1205
Lab Work Order # 1601033
Page 4 of 19Page 4 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-02
RLCAS #
Client ID: GP11@45'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205
5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205
5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Chloroform67-66-3 01/12/161.8 B6A1205
5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205
5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205
Lab Work Order # 1601033
Page 5 of 19Page 5 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-02
RLCAS #
Client ID: GP11@45'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205
5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205
5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205
1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205
85-11599.4 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205
82.7-115102 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205
85-115100 %Surrogate: Toluene-d8 826001/12/16 B6A1205
Lab Work Order # 1601033
Page 6 of 19Page 6 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-03
RLCAS #
Client ID: GP11@50'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205
5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205
5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Chloroform67-66-3 01/12/162.0 B6A1205
5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205
5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205
Lab Work Order # 1601033
Page 7 of 19Page 7 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-03
RLCAS #
Client ID: GP11@50'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205
5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205
5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205
1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205
85-115103 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205
82.7-11599.2 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205
85-115101 %Surrogate: Toluene-d8 826001/12/16 B6A1205
Lab Work Order # 1601033
Page 8 of 19Page 8 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-04
RLCAS #
Client ID: GP11@55'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/12/16ND B6A1205
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/12/16ND B6A1205
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/12/16ND B6A1205
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/12/16ND B6A1205
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/12/16ND B6A1205
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/12/16ND B6A1205
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/12/16ND B6A1205
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/12/16ND B6A1205
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/12/16ND B6A1205
5.0 ug/L 1 82602-Hexanone591-78-6 01/12/16ND B6A1205
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/12/16ND B6A1205
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/12/16ND B6A1205
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/12/16ND B6A1205
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Benzene71-43-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromobenzene108-86-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Bromoform75-25-2 01/12/16ND B6A1205
5.0 ug/L 1 8260Bromomethane74-83-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/12/16ND B6A1205
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/12/16ND B6A1205
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Chloroethane75-00-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Chloroform67-66-3 01/12/161.2 B6A1205
5.0 ug/L 1 8260Chloromethane74-87-3 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/12/16ND B6A1205
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/12/16ND B6A1205
5.0 ug/L 1 8260Cyclohexane110-82-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/12/16ND B6A1205
Lab Work Order # 1601033
Page 9 of 19Page 9 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-04
RLCAS #
Client ID: GP11@55'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/12/16ND B6A1205
5.0 ug/L 1 8260Diethyl ether60-29-7 01/12/16ND B6A1205
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/12/16ND B6A1205
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/12/16ND B6A1205
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/12/16ND B6A1205
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyl iodide74-88-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Methylene chloride75-09-2 01/12/16ND B6A1205
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/12/16ND B6A1205
5.0 Xug/L 1 8260Naphthalene91-20-3 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/12/16ND B6A1205
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/12/16ND B6A1205
1.0 ug/L 1 8260o-Xylene95-47-6 01/12/16ND B6A1205
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/12/16ND B6A1205
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Styrene100-42-5 01/12/16ND B6A1205
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/12/16ND B6A1205
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/12/16ND B6A1205
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/12/16ND B6A1205
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/12/16ND B6A1205
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/12/16ND B6A1205
1.0 ug/L 1 8260Toluene108-88-3 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/12/16ND B6A1205
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/12/16ND B6A1205
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/12/16ND B6A1205
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/12/16ND B6A1205
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/12/16ND B6A1205
85-115101 %Surrogate: Bromofluorobenzene 826001/12/16 B6A1205
82.7-115101 %Surrogate: Dibromofluoromethane 826001/12/16 B6A1205
85-115100 %Surrogate: Toluene-d8 826001/12/16 B6A1205
Lab Work Order # 1601033
Page 10 of 19Page 10 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-05
RLCAS #
Client ID: GP12@25'
QC Batch
Organics-Volatiles
20 ug/L 20 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302
20 ug/L 20 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302
20 ug/L 20 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302
20 ug/L 20 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302
20 ug/L 20 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302
20 ug/L 20 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302
100 ug/L 20 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302
20 ug/L 20 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302
20 ug/L 20 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302
100 ug/L 20 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302
20 ug/L 20 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302
100 ug/L 20 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302
20 ug/L 20 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302
20 ug/L 20 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302
20 ug/L 20 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302
20 ug/L 20 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302
20 ug/L 20 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302
20 ug/L 20 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302
20 ug/L 20 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302
100 ug/L 20 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302
100 ug/L 20 82602-Hexanone591-78-6 01/13/16ND B6A1302
100 A07, Xug/L 20 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302
400 ug/L 20 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302
100 ug/L 20 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302
100 ug/L 20 8260Acrylonitrile107-13-1 01/13/16ND B6A1302
20 ug/L 20 8260Benzene71-43-2 01/13/16ND B6A1302
20 ug/L 20 8260Bromobenzene108-86-1 01/13/16ND B6A1302
20 ug/L 20 8260Bromochloromethane74-97-5 01/13/16ND B6A1302
20 ug/L 20 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302
20 ug/L 20 8260Bromoform75-25-2 01/13/16ND B6A1302
100 ug/L 20 8260Bromomethane74-83-9 01/13/16ND B6A1302
20 ug/L 20 8260Carbon disulfide75-15-0 01/13/16ND B6A1302
20 ug/L 20 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302
20 ug/L 20 8260Chlorobenzene108-90-7 01/13/16ND B6A1302
100 ug/L 20 8260Chloroethane75-00-3 01/13/16ND B6A1302
20 ug/L 20 8260Chloroform67-66-3 01/13/16ND B6A1302
100 ug/L 20 8260Chloromethane74-87-3 01/13/16ND B6A1302
20 ug/L 20 8260cis-1,2-Dichloroethylene156-59-2 01/13/1661 B6A1302
20 ug/L 20 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302
100 ug/L 20 8260Cyclohexane110-82-7 01/13/16ND B6A1302
20 ug/L 20 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302
Lab Work Order # 1601033
Page 11 of 19Page 11 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-05
RLCAS #
Client ID: GP12@25'
QC Batch
Organics-Volatiles
20 ug/L 20 8260Dibromomethane74-95-3 01/13/16ND B6A1302
100 ug/L 20 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302
100 ug/L 20 8260Diethyl ether60-29-7 01/13/16ND B6A1302
100 ug/L 20 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302
20 ug/L 20 8260Ethylbenzene100-41-4 01/13/16ND B6A1302
100 ug/L 20 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302
100 ug/L 20 8260Hexachloroethane67-72-1 01/13/16ND B6A1302
20 ug/L 20 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302
40 ug/L 20 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302
20 ug/L 20 8260Methyl iodide74-88-4 01/13/16ND B6A1302
100 ug/L 20 8260Methylene chloride75-09-2 01/13/16ND B6A1302
20 ug/L 20 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302
100 Xug/L 20 8260Naphthalene91-20-3 01/13/16ND B6A1302
20 ug/L 20 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302
20 ug/L 20 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302
20 ug/L 20 8260o-Xylene95-47-6 01/13/16ND B6A1302
20 ug/L 20 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302
20 ug/L 20 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302
20 ug/L 20 8260Styrene100-42-5 01/13/16ND B6A1302
20 ug/L 20 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302
1000 ug/L 20 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302
100 ug/L 20 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302
20 ug/L 20 8260Tetrachloroethylene127-18-4 01/13/161400 B6A1302
100 ug/L 20 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302
20 ug/L 20 8260Toluene108-88-3 01/13/16ND B6A1302
20 ug/L 20 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302
20 ug/L 20 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302
100 ug/L 20 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302
20 ug/L 20 8260Trichloroethylene79-01-6 01/13/1626 B6A1302
20 ug/L 20 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302
20 ug/L 20 8260Vinyl chloride75-01-4 01/13/16ND B6A1302
85-115104 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302
82.7-115100 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302
85-115100 %Surrogate: Toluene-d8 826001/13/16 B6A1302
Lab Work Order # 1601033
Page 12 of 19Page 12 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-06
RLCAS #
Client ID: GP12@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1302
5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1302
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1302
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1302
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1302
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1302
1.0 ug/L 1 8260Chloroform67-66-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1302
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1302
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1302
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302
Lab Work Order # 1601033
Page 13 of 19Page 13 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-06
RLCAS #
Client ID: GP12@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1302
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1302
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1302
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1302
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1302
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1302
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1302
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/163.0 B6A1302
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1302
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1302
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1302
85-115105 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302
82.7-11599.9 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302
85-115100 %Surrogate: Toluene-d8 826001/13/16 B6A1302
Lab Work Order # 1601033
Page 14 of 19Page 14 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-07
RLCAS #
Client ID: GP12@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1302
5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1302
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1302
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1302
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1302
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1302
1.0 Tug/L 1 8260Chloroform67-66-3 01/13/160.95 B6A1302
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1302
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1302
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1302
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302
Lab Work Order # 1601033
Page 15 of 19Page 15 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-07
RLCAS #
Client ID: GP12@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1302
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1302
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1302
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1302
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1302
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1302
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1302
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/162.2 B6A1302
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1302
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1302
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1302
85-115103 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302
82.7-115102 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302
85-11598.9 %Surrogate: Toluene-d8 826001/13/16 B6A1302
Lab Work Order # 1601033
Page 16 of 19Page 16 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-08
RLCAS #
Client ID: GP12@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/13/16ND B6A1302
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/13/16ND B6A1302
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/13/16ND B6A1302
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/13/16ND B6A1302
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/13/16ND B6A1302
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/13/16ND B6A1302
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/13/16ND B6A1302
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/13/16ND B6A1302
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/13/16ND B6A1302
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/13/16ND B6A1302
5.0 ug/L 1 82602-Hexanone591-78-6 01/13/16ND B6A1302
5.0 A07, Xug/L 1 82602-Methylnaphthalene91-57-6 01/13/16ND B6A1302
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/13/16ND B6A1302
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/13/16ND B6A1302
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Benzene71-43-2 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromobenzene108-86-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/13/16ND B6A1302
1.0 ug/L 1 8260Bromoform75-25-2 01/13/16ND B6A1302
5.0 ug/L 1 8260Bromomethane74-83-9 01/13/16ND B6A1302
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/13/16ND B6A1302
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/13/16ND B6A1302
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/13/16ND B6A1302
5.0 ug/L 1 8260Chloroethane75-00-3 01/13/16ND B6A1302
1.0 Tug/L 1 8260Chloroform67-66-3 01/13/160.94 B6A1302
5.0 ug/L 1 8260Chloromethane74-87-3 01/13/16ND B6A1302
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/13/16ND B6A1302
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/13/16ND B6A1302
5.0 ug/L 1 8260Cyclohexane110-82-7 01/13/16ND B6A1302
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/13/16ND B6A1302
Lab Work Order # 1601033
Page 17 of 19Page 17 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601033-08
RLCAS #
Client ID: GP12@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/13/16ND B6A1302
5.0 ug/L 1 8260Diethyl ether60-29-7 01/13/16ND B6A1302
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/13/16ND B6A1302
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/13/16ND B6A1302
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/13/16ND B6A1302
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/13/16ND B6A1302
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/13/16ND B6A1302
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/13/16ND B6A1302
1.0 ug/L 1 8260Methyl iodide74-88-4 01/13/16ND B6A1302
5.0 ug/L 1 8260Methylene chloride75-09-2 01/13/16ND B6A1302
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/13/16ND B6A1302
5.0 Xug/L 1 8260Naphthalene91-20-3 01/13/16ND B6A1302
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/13/16ND B6A1302
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/13/16ND B6A1302
1.0 ug/L 1 8260o-Xylene95-47-6 01/13/16ND B6A1302
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/13/16ND B6A1302
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/13/16ND B6A1302
1.0 ug/L 1 8260Styrene100-42-5 01/13/16ND B6A1302
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/13/16ND B6A1302
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/13/16ND B6A1302
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/13/16ND B6A1302
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/13/163.1 B6A1302
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/13/16ND B6A1302
1.0 ug/L 1 8260Toluene108-88-3 01/13/16ND B6A1302
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/13/16ND B6A1302
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/13/16ND B6A1302
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/13/16ND B6A1302
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/13/16ND B6A1302
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/13/16ND B6A1302
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/13/16ND B6A1302
85-115101 %Surrogate: Bromofluorobenzene 826001/13/16 B6A1302
82.7-115101 %Surrogate: Dibromofluoromethane 826001/13/16 B6A1302
85-115100 %Surrogate: Toluene-d8 826001/13/16 B6A1302
Lab Work Order # 1601033
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Page 19 of 20
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Page 20 of 20
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
MDEQ-RRD-GRAND RAPIDS
RE: HALL STREET
Grand Rapids, MI 49503-2341
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
I certify that the analyses performed by the MDEQ Environmental Laboratory were conducted by methods
approved by the U.S. Environmental Protection Agency and other appropriate regulatory agencies .
Sincerely,
20 January 2016 Work Order: 1601058
Price: $1,840.00
George Krisztian
Laboratory Director
Lab Work Order # 1601058
Page 1 of 19Page 1 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
Project:
Project Manager:
Reported:
MDEQ-RRD-GRAND RAPIDS
350 Ottawa Ave. NW, Unit 10
Abigail Hendershott
HALL STREET
Grand Rapids MI, 49503-2341
Site Code: 4100112101/20/2016
Sample ID Laboratory ID Date SampledMatrix Date Received
Analytical Report for Samples
Qualifier
1601058-01 Water 01/14/2016GP15@25' 01/13/2016
1601058-02 Water 01/14/2016GP15@30' 01/13/2016
1601058-03 Water 01/14/2016GP15@35' 01/13/2016
1601058-04 Water 01/14/2016GP15@40' 01/13/2016
1601058-05 Water 01/14/2016GP16@25' 01/14/2016
1601058-06 Water 01/14/2016GP16@30 01/14/2016
1601058-07 Water 01/14/2016GP16@35 01/14/2016
1601058-08 Water 01/14/2016GP16@40 01/14/2016
Notes and Definitions
X Methods 8260 & 624 are used to analyze volatile organics that have boiling points below 200 ºC. 2-Methylnaphthalene & naphthalene
have boiling points above 200 ºC and are better suited to analysis by methods 8270 & 625 as semivolatile organics.
T Reported value is less than the reporting limit (RL). Result is estimated.
A05 Result and reporting limit are estimated due to low continuing calibration standard criteria failure.
Reporting LimitRL
Indicates compound analyzed for but not detectedND
Not ApplicableNA
Case Narrative
Priority Samples
Lab Work Order # 1601058
Page 2 of 19Page 2 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-01
RLCAS #
Client ID: GP15@25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403
5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403
5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Chloroform67-66-3 01/14/161.0 B6A1403
5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403
5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403
Lab Work Order # 1601058
Page 3 of 19Page 3 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-01
RLCAS #
Client ID: GP15@25'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403
5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403
5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403
1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/1699 B6A1403
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403
85-115103 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403
82.7-115101 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403
85-11598.8 %Surrogate: Toluene-d8 826001/14/16 B6A1403
Lab Work Order # 1601058
Page 4 of 19Page 4 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-02
RLCAS #
Client ID: GP15@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403
5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403
5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Chloroform67-66-3 01/14/161.0 B6A1403
5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403
5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403
Lab Work Order # 1601058
Page 5 of 19Page 5 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-02
RLCAS #
Client ID: GP15@30'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403
5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403
5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403
1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/1612 B6A1403
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403
85-115101 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403
82.7-115103 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403
85-11597.5 %Surrogate: Toluene-d8 826001/14/16 B6A1403
Lab Work Order # 1601058
Page 6 of 19Page 6 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-03
RLCAS #
Client ID: GP15@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403
5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403
5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Chloroform67-66-3 01/14/161.0 B6A1403
5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403
5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403
Lab Work Order # 1601058
Page 7 of 19Page 7 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-03
RLCAS #
Client ID: GP15@35'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403
5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403
5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403
1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/169.5 B6A1403
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403
85-115101 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403
82.7-115101 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403
85-11598.1 %Surrogate: Toluene-d8 826001/14/16 B6A1403
Lab Work Order # 1601058
Page 8 of 19Page 8 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-04
RLCAS #
Client ID: GP15@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403
5.0 ug/L 1 82602-Hexanone591-78-6 01/14/16ND B6A1403
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Benzene71-43-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromobenzene108-86-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Bromoform75-25-2 01/14/16ND B6A1403
5.0 ug/L 1 8260Bromomethane74-83-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/14/16ND B6A1403
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Chloroethane75-00-3 01/14/16ND B6A1403
1.0 Tug/L 1 8260Chloroform67-66-3 01/14/160.99 B6A1403
5.0 ug/L 1 8260Chloromethane74-87-3 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403
5.0 ug/L 1 8260Cyclohexane110-82-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403
Lab Work Order # 1601058
Page 9 of 19Page 9 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-04
RLCAS #
Client ID: GP15@40'
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403
5.0 ug/L 1 8260Diethyl ether60-29-7 01/14/16ND B6A1403
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/14/16ND B6A1403
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyl iodide74-88-4 01/14/16ND B6A1403
5.0 ug/L 1 8260Methylene chloride75-09-2 01/14/16ND B6A1403
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403
5.0 Xug/L 1 8260Naphthalene91-20-3 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403
1.0 ug/L 1 8260o-Xylene95-47-6 01/14/16ND B6A1403
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Styrene100-42-5 01/14/16ND B6A1403
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/14/169.5 B6A1403
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403
1.0 ug/L 1 8260Toluene108-88-3 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/14/16ND B6A1403
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/14/16ND B6A1403
85-115104 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403
82.7-11598.6 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403
85-11597.7 %Surrogate: Toluene-d8 826001/14/16 B6A1403
Lab Work Order # 1601058
Page 10 of 19Page 10 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-05
RLCAS #
Client ID: GP16@25'
QC Batch
Organics-Volatiles
20 ug/L 20 82601,1,1,2-Tetrachloroethane630-20-6 01/14/16ND B6A1403
20 ug/L 20 82601,1,1-Trichloroethane71-55-6 01/14/16ND B6A1403
20 ug/L 20 82601,1,2,2-Tetrachloroethane79-34-5 01/14/16ND B6A1403
20 ug/L 20 82601,1,2-Trichloroethane79-00-5 01/14/16ND B6A1403
20 ug/L 20 82601,1-Dichloroethane75-34-3 01/14/16ND B6A1403
20 ug/L 20 82601,1-Dichloroethylene75-35-4 01/14/16ND B6A1403
100 ug/L 20 82601,2,3-Trichlorobenzene87-61-6 01/14/16ND B6A1403
20 ug/L 20 82601,2,3-Trichloropropane96-18-4 01/14/16ND B6A1403
20 ug/L 20 82601,2,3-Trimethylbenzene526-73-8 01/14/16ND B6A1403
100 ug/L 20 82601,2,4-Trichlorobenzene120-82-1 01/14/16ND B6A1403
20 ug/L 20 82601,2,4-Trimethylbenzene95-63-6 01/14/16ND B6A1403
100 ug/L 20 82601,2-Dibromo-3-chloropropane96-12-8 01/14/16ND B6A1403
20 ug/L 20 82601,2-Dibromoethane106-93-4 01/14/16ND B6A1403
20 ug/L 20 82601,2-Dichlorobenzene95-50-1 01/14/16ND B6A1403
20 ug/L 20 82601,2-Dichloroethane107-06-2 01/14/16ND B6A1403
20 ug/L 20 82601,2-Dichloropropane78-87-5 01/14/16ND B6A1403
20 ug/L 20 82601,3,5-Trimethylbenzene108-67-8 01/14/16ND B6A1403
20 ug/L 20 82601,3-Dichlorobenzene541-73-1 01/14/16ND B6A1403
20 ug/L 20 82601,4-Dichlorobenzene106-46-7 01/14/16ND B6A1403
100 ug/L 20 82602-Butanone (MEK)78-93-3 01/14/16ND B6A1403
100 ug/L 20 82602-Hexanone591-78-6 01/14/16ND B6A1403
100 Xug/L 20 82602-Methylnaphthalene91-57-6 01/14/16ND B6A1403
400 ug/L 20 82602-Propanone (acetone)67-64-1 01/14/16ND B6A1403
100 ug/L 20 82604-Methyl-2-pentanone (MIBK)108-10-1 01/14/16ND B6A1403
100 ug/L 20 8260Acrylonitrile107-13-1 01/14/16ND B6A1403
20 ug/L 20 8260Benzene71-43-2 01/14/16ND B6A1403
20 ug/L 20 8260Bromobenzene108-86-1 01/14/16ND B6A1403
20 ug/L 20 8260Bromochloromethane74-97-5 01/14/16ND B6A1403
20 ug/L 20 8260Bromodichloromethane75-27-4 01/14/16ND B6A1403
20 ug/L 20 8260Bromoform75-25-2 01/14/16ND B6A1403
100 ug/L 20 8260Bromomethane74-83-9 01/14/16ND B6A1403
20 ug/L 20 8260Carbon disulfide75-15-0 01/14/16ND B6A1403
20 ug/L 20 8260Carbon tetrachloride56-23-5 01/14/16ND B6A1403
20 ug/L 20 8260Chlorobenzene108-90-7 01/14/16ND B6A1403
100 ug/L 20 8260Chloroethane75-00-3 01/14/16ND B6A1403
20 ug/L 20 8260Chloroform67-66-3 01/14/16ND B6A1403
100 ug/L 20 8260Chloromethane74-87-3 01/14/16ND B6A1403
20 ug/L 20 8260cis-1,2-Dichloroethylene156-59-2 01/14/16ND B6A1403
20 ug/L 20 8260cis-1,3-Dichloropropylene10061-01-5 01/14/16ND B6A1403
100 ug/L 20 8260Cyclohexane110-82-7 01/14/16ND B6A1403
20 ug/L 20 8260Dibromochloromethane124-48-1 01/14/16ND B6A1403
Lab Work Order # 1601058
Page 11 of 19Page 11 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-05
RLCAS #
Client ID: GP16@25'
QC Batch
Organics-Volatiles
20 ug/L 20 8260Dibromomethane74-95-3 01/14/16ND B6A1403
100 ug/L 20 8260Dichlorodifluoromethane75-71-8 01/14/16ND B6A1403
100 ug/L 20 8260Diethyl ether60-29-7 01/14/16ND B6A1403
100 ug/L 20 8260Diisopropyl Ether108-20-3 01/14/16ND B6A1403
20 ug/L 20 8260Ethylbenzene100-41-4 01/14/16ND B6A1403
100 ug/L 20 8260Ethyltertiarybutylether637-92-3 01/14/16ND B6A1403
100 ug/L 20 8260Hexachloroethane67-72-1 01/14/16ND B6A1403
20 ug/L 20 8260Isopropylbenzene98-82-8 01/14/16ND B6A1403
40 ug/L 20 8260m & p - Xylene1330-20-7 01/14/16ND B6A1403
20 ug/L 20 8260Methyl iodide74-88-4 01/14/16ND B6A1403
100 ug/L 20 8260Methylene chloride75-09-2 01/14/16ND B6A1403
20 ug/L 20 8260Methyltertiarybutylether1634-04-4 01/14/16ND B6A1403
100 Xug/L 20 8260Naphthalene91-20-3 01/14/16ND B6A1403
20 ug/L 20 8260n-Butylbenzene104-51-8 01/14/16ND B6A1403
20 ug/L 20 8260n-Propylbenzene103-65-1 01/14/16ND B6A1403
20 ug/L 20 8260o-Xylene95-47-6 01/14/16ND B6A1403
20 ug/L 20 8260p-Isopropyl toluene99-87-6 01/14/16ND B6A1403
20 ug/L 20 8260sec-Butylbenzene135-98-8 01/14/16ND B6A1403
20 ug/L 20 8260Styrene100-42-5 01/14/16ND B6A1403
20 ug/L 20 8260tert-Butylbenzene98-06-6 01/14/16ND B6A1403
1000 ug/L 20 8260tertiary Butyl Alcohol75-65-0 01/14/16ND B6A1403
100 ug/L 20 8260tertiaryAmylmethylether994-05-8 01/14/16ND B6A1403
20 ug/L 20 8260Tetrachloroethylene127-18-4 01/14/16820 B6A1403
100 ug/L 20 8260Tetrahydrofuran109-99-9 01/14/16ND B6A1403
20 ug/L 20 8260Toluene108-88-3 01/14/16ND B6A1403
20 ug/L 20 8260trans-1,2-Dichloroethylene156-60-5 01/14/16ND B6A1403
20 ug/L 20 8260trans-1,3-Dichloropropylene10061-02-6 01/14/16ND B6A1403
100 ug/L 20 8260trans-1,4-Dichloro-2-butene110-57-6 01/14/16ND B6A1403
20 ug/L 20 8260Trichloroethylene79-01-6 01/14/16ND B6A1403
20 ug/L 20 8260Trichlorofluoromethane75-69-4 01/14/16ND B6A1403
20 ug/L 20 8260Vinyl chloride75-01-4 01/14/16ND B6A1403
85-115102 %Surrogate: Bromofluorobenzene 826001/14/16 B6A1403
82.7-115101 %Surrogate: Dibromofluoromethane 826001/14/16 B6A1403
85-11599.8 %Surrogate: Toluene-d8 826001/14/16 B6A1403
Lab Work Order # 1601058
Page 12 of 19Page 12 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-06
RLCAS #
Client ID: GP16@30
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/15/16ND B6A1502
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/15/16ND B6A1502
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/15/16ND B6A1502
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/15/16ND B6A1502
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/15/16ND B6A1502
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/15/16ND B6A1502
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/15/16ND B6A1502
5.0 ug/L 1 82602-Hexanone591-78-6 01/15/16ND B6A1502
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/15/16ND B6A1502
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/15/16ND B6A1502
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/15/16ND B6A1502
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Benzene71-43-2 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromobenzene108-86-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromoform75-25-2 01/15/16ND B6A1502
5.0 ug/L 1 8260Bromomethane74-83-9 01/15/16ND B6A1502
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/15/16ND B6A1502
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/15/16ND B6A1502
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/15/16ND B6A1502
5.0 ug/L 1 8260Chloroethane75-00-3 01/15/16ND B6A1502
1.0 ug/L 1 8260Chloroform67-66-3 01/15/16ND B6A1502
5.0 ug/L 1 8260Chloromethane74-87-3 01/15/16ND B6A1502
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/15/16ND B6A1502
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/15/16ND B6A1502
5.0 ug/L 1 8260Cyclohexane110-82-7 01/15/16ND B6A1502
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/15/16ND B6A1502
Lab Work Order # 1601058
Page 13 of 19Page 13 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-06
RLCAS #
Client ID: GP16@30
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/15/16ND B6A1502
5.0 A05ug/L 1 8260Dichlorodifluoromethane75-71-8 01/15/16ND B6A1502
5.0 ug/L 1 8260Diethyl ether60-29-7 01/15/16ND B6A1502
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/15/16ND B6A1502
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/15/16ND B6A1502
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/15/16ND B6A1502
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/15/16ND B6A1502
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/15/16ND B6A1502
1.0 ug/L 1 8260Methyl iodide74-88-4 01/15/16ND B6A1502
5.0 ug/L 1 8260Methylene chloride75-09-2 01/15/16ND B6A1502
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/15/16ND B6A1502
5.0 Xug/L 1 8260Naphthalene91-20-3 01/15/16ND B6A1502
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/15/16ND B6A1502
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/15/16ND B6A1502
1.0 ug/L 1 8260o-Xylene95-47-6 01/15/16ND B6A1502
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/15/16ND B6A1502
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/15/16ND B6A1502
1.0 ug/L 1 8260Styrene100-42-5 01/15/16ND B6A1502
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/15/16ND B6A1502
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/15/16ND B6A1502
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/15/16ND B6A1502
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/15/1611 B6A1502
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/15/16ND B6A1502
1.0 ug/L 1 8260Toluene108-88-3 01/15/16ND B6A1502
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/15/16ND B6A1502
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/15/16ND B6A1502
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/15/16ND B6A1502
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/15/16ND B6A1502
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/15/16ND B6A1502
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/15/16ND B6A1502
85-115102 %Surrogate: Bromofluorobenzene 826001/15/16 B6A1502
82.7-115101 %Surrogate: Dibromofluoromethane 826001/15/16 B6A1502
85-115100 %Surrogate: Toluene-d8 826001/15/16 B6A1502
Lab Work Order # 1601058
Page 14 of 19Page 14 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-07
RLCAS #
Client ID: GP16@35
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/15/16ND B6A1502
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/15/16ND B6A1502
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/15/16ND B6A1502
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/15/16ND B6A1502
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/15/16ND B6A1502
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/15/16ND B6A1502
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/15/16ND B6A1502
5.0 ug/L 1 82602-Hexanone591-78-6 01/15/16ND B6A1502
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/15/16ND B6A1502
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/15/16ND B6A1502
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/15/16ND B6A1502
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Benzene71-43-2 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromobenzene108-86-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromoform75-25-2 01/15/16ND B6A1502
5.0 ug/L 1 8260Bromomethane74-83-9 01/15/16ND B6A1502
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/15/16ND B6A1502
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/15/16ND B6A1502
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/15/16ND B6A1502
5.0 ug/L 1 8260Chloroethane75-00-3 01/15/16ND B6A1502
1.0 ug/L 1 8260Chloroform67-66-3 01/15/16ND B6A1502
5.0 ug/L 1 8260Chloromethane74-87-3 01/15/16ND B6A1502
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/15/16ND B6A1502
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/15/16ND B6A1502
5.0 ug/L 1 8260Cyclohexane110-82-7 01/15/16ND B6A1502
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/15/16ND B6A1502
Lab Work Order # 1601058
Page 15 of 19Page 15 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-07
RLCAS #
Client ID: GP16@35
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/15/16ND B6A1502
5.0 A05ug/L 1 8260Dichlorodifluoromethane75-71-8 01/15/16ND B6A1502
5.0 ug/L 1 8260Diethyl ether60-29-7 01/15/16ND B6A1502
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/15/16ND B6A1502
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/15/16ND B6A1502
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/15/16ND B6A1502
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/15/16ND B6A1502
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/15/16ND B6A1502
1.0 ug/L 1 8260Methyl iodide74-88-4 01/15/16ND B6A1502
5.0 ug/L 1 8260Methylene chloride75-09-2 01/15/16ND B6A1502
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/15/16ND B6A1502
5.0 Xug/L 1 8260Naphthalene91-20-3 01/15/16ND B6A1502
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/15/16ND B6A1502
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/15/16ND B6A1502
1.0 ug/L 1 8260o-Xylene95-47-6 01/15/16ND B6A1502
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/15/16ND B6A1502
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/15/16ND B6A1502
1.0 ug/L 1 8260Styrene100-42-5 01/15/16ND B6A1502
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/15/16ND B6A1502
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/15/16ND B6A1502
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/15/16ND B6A1502
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/15/163.3 B6A1502
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/15/16ND B6A1502
1.0 ug/L 1 8260Toluene108-88-3 01/15/16ND B6A1502
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/15/16ND B6A1502
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/15/16ND B6A1502
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/15/16ND B6A1502
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/15/16ND B6A1502
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/15/16ND B6A1502
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/15/16ND B6A1502
85-115102 %Surrogate: Bromofluorobenzene 826001/15/16 B6A1502
82.7-11599.3 %Surrogate: Dibromofluoromethane 826001/15/16 B6A1502
85-11599.5 %Surrogate: Toluene-d8 826001/15/16 B6A1502
Lab Work Order # 1601058
Page 16 of 19Page 16 of 19
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-08
RLCAS #
Client ID: GP16@40
QC Batch
Organics-Volatiles
1.0 ug/L 1 82601,1,1,2-Tetrachloroethane630-20-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,1-Trichloroethane71-55-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,2,2-Tetrachloroethane79-34-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,1,2-Trichloroethane79-00-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,1-Dichloroethane75-34-3 01/15/16ND B6A1502
1.0 ug/L 1 82601,1-Dichloroethylene75-35-4 01/15/16ND B6A1502
5.0 ug/L 1 82601,2,3-Trichlorobenzene87-61-6 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,3-Trichloropropane96-18-4 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,3-Trimethylbenzene526-73-8 01/15/16ND B6A1502
5.0 ug/L 1 82601,2,4-Trichlorobenzene120-82-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,2,4-Trimethylbenzene95-63-6 01/15/16ND B6A1502
5.0 ug/L 1 82601,2-Dibromo-3-chloropropane96-12-8 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dibromoethane106-93-4 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichlorobenzene95-50-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichloroethane107-06-2 01/15/16ND B6A1502
1.0 ug/L 1 82601,2-Dichloropropane78-87-5 01/15/16ND B6A1502
1.0 ug/L 1 82601,3,5-Trimethylbenzene108-67-8 01/15/16ND B6A1502
1.0 ug/L 1 82601,3-Dichlorobenzene541-73-1 01/15/16ND B6A1502
1.0 ug/L 1 82601,4-Dichlorobenzene106-46-7 01/15/16ND B6A1502
5.0 ug/L 1 82602-Butanone (MEK)78-93-3 01/15/16ND B6A1502
5.0 ug/L 1 82602-Hexanone591-78-6 01/15/16ND B6A1502
5.0 Xug/L 1 82602-Methylnaphthalene91-57-6 01/15/16ND B6A1502
20 ug/L 1 82602-Propanone (acetone)67-64-1 01/15/16ND B6A1502
5.0 ug/L 1 82604-Methyl-2-pentanone (MIBK)108-10-1 01/15/16ND B6A1502
5.0 ug/L 1 8260Acrylonitrile107-13-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Benzene71-43-2 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromobenzene108-86-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromochloromethane74-97-5 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromodichloromethane75-27-4 01/15/16ND B6A1502
1.0 ug/L 1 8260Bromoform75-25-2 01/15/16ND B6A1502
5.0 ug/L 1 8260Bromomethane74-83-9 01/15/16ND B6A1502
1.0 ug/L 1 8260Carbon disulfide75-15-0 01/15/16ND B6A1502
1.0 ug/L 1 8260Carbon tetrachloride56-23-5 01/15/16ND B6A1502
1.0 ug/L 1 8260Chlorobenzene108-90-7 01/15/16ND B6A1502
5.0 ug/L 1 8260Chloroethane75-00-3 01/15/16ND B6A1502
1.0 Tug/L 1 8260Chloroform67-66-3 01/15/160.99 B6A1502
5.0 ug/L 1 8260Chloromethane74-87-3 01/15/16ND B6A1502
1.0 ug/L 1 8260cis-1,2-Dichloroethylene156-59-2 01/15/16ND B6A1502
1.0 ug/L 1 8260cis-1,3-Dichloropropylene10061-01-5 01/15/16ND B6A1502
5.0 ug/L 1 8260Cyclohexane110-82-7 01/15/16ND B6A1502
1.0 ug/L 1 8260Dibromochloromethane124-48-1 01/15/16ND B6A1502
Lab Work Order # 1601058
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P.O. Box 30270
Lansing, MI 48909
TEL: (517) 335-9800
FAX: (517) 335-9600
MICHIGAN DEPARTMENT OF ENVIRONMENTAL QUALITY
ENVIRONMENTAL LABORATORY
ResultAnalyte
Analyzed
Date Method QualifierDilutionUnits
Lab ID: 1601058-08
RLCAS #
Client ID: GP16@40
QC Batch
Organics-Volatiles
1.0 ug/L 1 8260Dibromomethane74-95-3 01/15/16ND B6A1502
5.0 A05ug/L 1 8260Dichlorodifluoromethane75-71-8 01/15/16ND B6A1502
5.0 ug/L 1 8260Diethyl ether60-29-7 01/15/16ND B6A1502
5.0 ug/L 1 8260Diisopropyl Ether108-20-3 01/15/16ND B6A1502
1.0 ug/L 1 8260Ethylbenzene100-41-4 01/15/16ND B6A1502
5.0 ug/L 1 8260Ethyltertiarybutylether637-92-3 01/15/16ND B6A1502
5.0 ug/L 1 8260Hexachloroethane67-72-1 01/15/16ND B6A1502
1.0 ug/L 1 8260Isopropylbenzene98-82-8 01/15/16ND B6A1502
2.0 ug/L 1 8260m & p - Xylene1330-20-7 01/15/16ND B6A1502
1.0 ug/L 1 8260Methyl iodide74-88-4 01/15/16ND B6A1502
5.0 ug/L 1 8260Methylene chloride75-09-2 01/15/16ND B6A1502
1.0 ug/L 1 8260Methyltertiarybutylether1634-04-4 01/15/16ND B6A1502
5.0 Xug/L 1 8260Naphthalene91-20-3 01/15/16ND B6A1502
1.0 ug/L 1 8260n-Butylbenzene104-51-8 01/15/16ND B6A1502
1.0 ug/L 1 8260n-Propylbenzene103-65-1 01/15/16ND B6A1502
1.0 ug/L 1 8260o-Xylene95-47-6 01/15/16ND B6A1502
1.0 ug/L 1 8260p-Isopropyl toluene99-87-6 01/15/16ND B6A1502
1.0 ug/L 1 8260sec-Butylbenzene135-98-8 01/15/16ND B6A1502
1.0 ug/L 1 8260Styrene100-42-5 01/15/16ND B6A1502
1.0 ug/L 1 8260tert-Butylbenzene98-06-6 01/15/16ND B6A1502
50 ug/L 1 8260tertiary Butyl Alcohol75-65-0 01/15/16ND B6A1502
5.0 ug/L 1 8260tertiaryAmylmethylether994-05-8 01/15/16ND B6A1502
1.0 ug/L 1 8260Tetrachloroethylene127-18-4 01/15/167.5 B6A1502
5.0 ug/L 1 8260Tetrahydrofuran109-99-9 01/15/16ND B6A1502
1.0 ug/L 1 8260Toluene108-88-3 01/15/16ND B6A1502
1.0 ug/L 1 8260trans-1,2-Dichloroethylene156-60-5 01/15/16ND B6A1502
1.0 ug/L 1 8260trans-1,3-Dichloropropylene10061-02-6 01/15/16ND B6A1502
5.0 ug/L 1 8260trans-1,4-Dichloro-2-butene110-57-6 01/15/16ND B6A1502
1.0 ug/L 1 8260Trichloroethylene79-01-6 01/15/16ND B6A1502
1.0 ug/L 1 8260Trichlorofluoromethane75-69-4 01/15/16ND B6A1502
1.0 ug/L 1 8260Vinyl chloride75-01-4 01/15/16ND B6A1502
85-115102 %Surrogate: Bromofluorobenzene 826001/15/16 B6A1502
82.7-115101 %Surrogate: Dibromofluoromethane 826001/15/16 B6A1502
85-11597.3 %Surrogate: Toluene-d8 826001/15/16 B6A1502
Lab Work Order # 1601058
Page 18 of 19Page 18 of 19
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