newfoundland and labradorgis.geosurv.gov.nl.ca/geofilepdfs/batch2016/001m_0870.pdf · 3...

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SECOND YEAR ASSESSMENT REPORT, GEOCHEMICAL SURVEYS, AND PROSPECTING

License 018902M, NTS 1M/10 & 1M/15. SAGE POND, NFLD.

ALEX HARRIS, B. Sc. Work performed, Mar 19, 2011 to, Mar 3, 2012

For: NEWFOUNDLAND FLUORSPAR EXPLORATION LTD. Total Expenditures: $18,870.64

Total Number of claims 50 March 3, 2012

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TABLE OF CONTENTS page INTRODUCTION 3 LOCATION AND ACCESS 3 PREVIOUS EXPLORATION 3 GEOLOGY 3 LAKE SEDIMENT GEOCHEMISTRY 3 HYDROGEOCHEMICAL SURVEY 4 SOIL GEOCHEMISTRY 4 PROSPECTING 4 RECOMMENDATIONS 5 REFERENCES CITED 6 APPENDIX 1 Maps:

1. SP_Key Location and Key Maps. 2. LOC2 Location of Claims, 1:100,000. 3. SMP-1. 2011 Sample Locations and Prospecting Traverses, West, 1:25,000 4. SMP-2 2011 Sample Locations and Prospecting Traverses, East; 1:25,000 5. WSP1 2010 and 2011 Fluoride in Water, West, 1:25,000 6. WSP2 2010 and 2011 Fluoride in Water, East, 1:25,000 7. SP-COMP-1 Fluoride in Water and Soils, NW of Sage Pond, 1:10,000 8. SSP1 Total Fluoride in Soils, West, 1:25,000 9. SSP2 Total Fluoride in Soils, East, 1:25,000

APPENDIX 2 Certificates of Analysis APPENDIX 3 GPS Data Listing APPENDIX 4 Statement of Expenditures APPENDIX 5 List of Personnel

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INTRODUCTION Grubstake Management (Nfld.) Ltd., acquired License 017063M totaling 63 claims at Sage Pond, Nfld., NTS sheet 1M/10 and 1M/15 late in 2009. Early in 2010 these claims were transferred to Newfoundland Fluorspar Exploration Ltd. (Newfluorex). Licence was reduced to 50 claims as 018902M in March, 2011. Claim locations are shown on map Loc 2. LOCATION AND ACCESS Sage Pond is located in Southern Newfoundland on NTS map sheets1M/10 and 1M/15 at 47 44’ north latitude, 54 52’ west longitude. Access to area is by well-developed ATV trails from Highway 211. PREVIOUS EXPLORATION Harris (2011) reviewed previous exploration work and reported on initial Hydrogeochemical Survey and Prospecting for Newfluorex. Previous prospecting (Dobbel, C.A., & Maclachan, D.C., 1953) was concentrated along the Granite Contact. They quoted Bradley (1951) as stating “Area is structurally favourable for metallization and the close association of the minerals fluorspar and molybdenite, with intrusives and faults is strikingly similar to nearby fluorspar deposits to the Southwest of St. Lawrence.” Esso Minerals (O’Sullivan, J., 1982 and 1983) explored a number of quartz topaz greisen zones close to the contact of the granite with Precambrian metasediments and volcanics. Significant but sub-economic tin values were obtained. MacGillivray, (1985) reported on exploration by Rio Algom which was largely focused south of our claims, GEOLOGY Claims are located on the Devonian Ackley Granite (Dickson, 1983). Soil is poorly developed, but bedrock exposures are sparse due to extensive frost heaving of well-jointed granite. Large areas of angular granite boulders are common. MacGillivray, (1985) reports that Glacial Striae indicates ice advanced from North to South. LAKE SEDIMENT GEOCHEMISTRY Harris (2010a) examined lake sediment geochemical data available on-line in Newfoundland Dept. of Mines and Energy database The Sage Pond Area has high fluoride values in excess of 1,000 ppm., over an area larger than license 18902M with the peak value of 3120 ppm in North part of Sage Pond. This is

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the largest Fluoride in Lake Sediment Anomaly in Newfoundland, with higher values than the former producing St. Lawrence district over a larger area. Dickson (1983) observed that a high fluoride content of the Granite in this area also coincides with that found in Lake Sediments. HYDROGEOCHEMICAL SURVEY 74 water samples were collected during June and July, 2011 from locations shown on maps WSP1 and WSP2. All samples were from surface ponds and streams. Complete Analytical data are enclosed in Appendix 2. All sample locations were recorded on a Garmin eTrex H GPS unit. A complete listing of GPS data is included in Appendix 3. All fluoride values from 2010 and 2011 are shown on maps SMP1 and SMP2 with anomalous areas defined by 0.3ppm contour. An orientation survey in the vicinity of the Mount Margaret Vein at St. Lawrence, (Harris, 2010b) showed anomalous fluoride in water values ranging from 0.2-0.8 ppm. SOIL GEOCHEMISTRY 35 soil samples were collected by digging with a Mattock. Samples were placed in 250ml glass jars in field and transported to lab for analysis. 2 samples (SSP 20 and 35) were lost after delivery to lab when jars were broken during transportation. First analysis was completed using aqueous extraction to measure soluble fluoride. All samples were below detection limit. Following a test sampling of a known anomalous area near the Mount Margaret Vein in the St. Lawrence Area, it was determined that this method of analysis was not effective and all samples were re-analyzed for total fluoride. Lab procedures and results are enclosed in Appendix 2. Over 60% of samples were below detection limit of 100ppm. A cluster of 3 samples (SSP 27, 30, 31) near NW corner of Sage Pond is the most interesting anomalous area. Single sample high values of 170, 150 and 130 ppm (SSP 23, 19 and 13) are also of potential interest. PROSPECTING Prospecting observations were made during Geochemical Survey Traverses. All Traverse lines as recorded by GPS are shown on maps SMP1 and SMP2. One probable Greisen Zone was located at RSP10 (Map SMP-2) where an area about 10meters in diameter contained large blocks of fine-grained siliceous material appearing to trend East-West, and containing minor fluorite. No metallic minerals were observed. At RSP-11 in Southwest corner of license, a stockwork of quartz veinlets up to 7cm wide trend at 070. RECOMMENDATIONS

1. Re-sample locations SSP-20 and SSP-35 where samples were lost due to breakage of glass jars by lab, and collect 1 sample mid-way between them.

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2. Collect soil samples at 100m intervals on lines through sites SSP 27, 30, and 31 perpendicular to Linear Structure along lines G, H and I on Map SSP1 and conduct detailed water sampling in this area.

3. Collect soil samples at 100-m equilateral triangular grid spacing around sites SSP-13, 19 and SSP-23 shown as grid B, on Map SSP2 and E and F on Map SSP1.

4. Collect soil samples at 100m intervals along line A on Map SSP2 also lines C, and D on Map SSP1 to give more information about areas with anomalous fluoride in water values.

Recommended additional sampling is about 25 water samples and 80 soil samples. Prospecting and Geological Observations should continue to be made during geochemical traverses. Respectfully Submitted Mar. 3, 2012 Alex Harris, B. Sc. REFERENCES CITED: Bradley, D.A., 1951, Geology of the Terrenceville – Gisburn Lake Area, Newfoundland, Unpublished Report included in Nf. Miner. Dev. Div., Assess. File 1M/32 Dickson, W.L., 1983, Geology, geochemistry and mineral potential of the Ackley Granite and parts of the North West Brook and Eastern Meelpaeg Complexes, southeast Newfoundland (parts of map areas 1M/10, 11, 14, 15, 16; 2D/1, 2, 3 and 7). Nfld. Dept. Mines and Energy, Min. Dev. Div, report 83-6. Dobbel, C.A., & Maclachan, D.C., 1953, Newfoundland Exploration, 1953: Private Report for American Zinc Company of Tennessee; Nf. Miner. Dev. Div., Assess. File 1M/32 Harris, A., 2010a, First year assessment report, compilation of geological and geochemical information, air photo interpretation, hydrogeochemical survey and prospecting licenses 16407m, 16408m, 16526m, 16561m, 16562m and 16563m, NTS 2E/09. Fogo Island, Nfld., unpublished assessment report for Newfoundland Fluorspar Exploration Ltd. Harris, A., 2010b, First And Fourth Year Assessment Report, Hydrogeochemical Survey And Prospecting Compilation Of Geological And Hydrogeochemical Information, Drilling Recommendations Licenses 13095m, 16461m, 17055m, 17062m, 17832m And 17982m, NTS 1L/14. St. Lawrence Area, Nfld., unpublished assessment report for Newfoundland Fluorspar Exploration Ltd.

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Harris, A., 2011, First year assessment report, Hydrogeochemical survey, prospecting and Review of previous work license 017063m, NTS 1M/10 & 1M/15.Sage Pond, Nfld. unpublished assessment report for Newfoundland Fluorspar Exploration Ltd. MacGillvray, G.C., 1985, Report on Airborne and Ground Geophysical Surveying, Geochemical Surveying, Geological Mapping and Channel Sampling, Licences 2281, 2331, 2465, 2466, 2475, 2476 and 2477, Nf. Miner. Dev. Div., Assess. File 1M/226 O’Sullivan, John, 1982, Assessment Report on Trenching and Diamond Drilling Carried out on Licences 1797 to 1804 inclusive for the period June to October, 1981, Nf. Miner. Dev. Div., Assess. File 1M/196. O’Sullivan, John, 1983, Report on Geochemical and Geological Surveys Carried out on Licence 2281 during September to December, 1982, Nf. Miner. Dev. Div., Assess. File 1M/207. Ricketts, J. & Bumgarner, J., 1954, Report on field Examinations in Newfoundland for American Zinc Company of Tennessee; Nf. Miner. Dev. Div., Assess. File 1M/42.

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APPENDIX 1 Maps: (Basemaps and Digital Air Photos from Dept. of Environment

and Conservation, Surveys and Mapping Division)

Drafting by: G. Stefanuk, C. Tech.

NewFluorEx.com Feb 25, 2012 Map: SP_Key

Key MapN.T.S.

Scale: 1 : 750,000

Location Map

Newfoundlan FluorsparExploration Ltd.

Drafting by: G. Stefanuk

660000m E

5290

000m

N

Legend

www.NewFluorEx.com February 25, 2012 Map: Loc2

Mineral Licence Boundary

650000m E 670000m E

5300

000m

N53

1000

0m N

NTS Map Reference:Terrenceville 1M/10

Gisborne Lake 1M/15UTM Zone 21, Nad 27

Sage Pond Property

MineralLicence:18902M

40000 2000

Scale: 1 : 100,000

1000

5287

000m

N52

8800

0m N

5289

000m

N52

9000

0m N

657000m E 658000m E656000m E 659000m E 660000m E

5291

000m

N


Gisborne Lake 1M/15UTM Zone 21, Nad 27 Drafting by: G. Stefanuk, C. Tech.

LegendMineral Licence Boundary

Exploration Traverse Location

Newfoundland Fluorspar Exploration Ltd.Sage Pond Claims

NewFluorEx.com Feb 25, 2012 Map: SMP-1

2011 Sample NumbersAnd Traverses, West

Linear Structures From Lansat Imagery

Trail

MineralLicence:

018902M

213

183m

198m

198m

183m

168m

152m

213m

229m

213m

9 km Trail Marker

SSP0

SSP09

SSP10

SSP11

SSP12

SSP14

SSP15

SSP16SSP17

SSP18

SSP19

SSP20

SSP27

SSP28

SSP29

SSP30SSP31SSP32

SSP33SSP34SSP35

WSP06

WSP06

WSP070

WSP

W

WSP0

WSP075

WSP076

WSP077

WSP078

WSP079WSP080

WSP081

WSP082

WSP083WSP084

WSP085

WSP086

WSP087WSP088

WSP089

WSP090

WSP091WSP092

WSP093

WSP094

WSP095

WSP096WSP097

WSP098WSP099

WSP100WSP101

WSP102

WSP103

W

WSP132

WSP133WSP134

WSP135

WSP136

WSP137

WSP138

WS

WSP

WSP1WSP148

RSP11

SSP13

Lansat Imagery Interpretation by: Alex Harris, B. Sc.

Water Sample Locations 2011WSP042

Soil Sample Locations 2011SSP03

500m0 250

Scale: 1 : 25,000

Rock Sample Locations 2011RSP03

5287

000m

N52

8800

0m N

5289

000m

N52

9000

0m N

660000m E

5291

000m

N

Trail

Trail

MineralLicence:

018902M

213m

198m

213m198m

198m

213m

229m

213m

183m

244m

Marker

SSP01

SSP02

SSP03

SSP05

SSP06

SSP07

SSP08

SSP14

SSP21

SSP22

SSP23

SSP24

SSP25

SSP26

SSP27

SSP28

SSP29

SSP30SSP31

WSP050WSP051

WSP052

WSP053

WSP054

WSP055WSP056

WSP057

WSP058

WSP059WSP060

WSP061

WSP062

WSP063WSP064

WSP065

WSP066WSP067

WSP068

WSP069

WSP070

WSP071

WSP072

WSP073

WSP074

84

85

086

87SP088

P089

SP090

WSP091WSP092

WSP093

WSP104

WSP105

WSP106WSP107 WSP108

WSP109WSP110

WSP111WSP112

WSP113

WSP114 WSP115

WSP116

WSP117

WSP118

WSP119

WSP120

WSP121

WSP122

WSP123WSP124

WSP125WSP126

WSP127

WSP128WSP129

WSP130

WSP131

WSP132

WSP133WSP134

WSP135

WSP136

WSP137

WSP138

WSP139

WSP140

WSP141WSP142

WSP143WSP144

WSP145WSP146

WSP147WSP148

RSP10

661000m E 662000m E 663000m E


NewFluorEx.com Feb 25, 2012 Map: SMP-2


2011 Sample NumbersAnd Traverses, East




Exploration Traverse Location


Water Sample Locations 2011WSP042

Soil Sample Locations 2011SSP03

500m0 250

Scale: 1 : 25,000

Rock Sample Locations 2011RSP03


5287

000m

N52

8800

0m N

5289

000m

N52

9000

0m N

657000m E 658000m E656000m E 659000m E 660000m E

5291

000m

N



NewFluorEx.com Mar 3, 2012 Map: WSP1

2010 & 2011 CompiledFluoride in Water, West

Trail

MineralLicence:

018902M

213

183m

198m

198m

183m

168m

152m

213m

229m

213m

0.3

ND

0.2

0.2

0.20.2

0.2

0.2

-ND

0.1

0.2

0.0.3

0.3

0.3

0.4

0.3

0.3

0.4

0.5

0.4

0.30.20.1

0.10.20.4

0.2

0.3

0.4

0.20.2

0.2

0.3

9 km Trail Marker

0.2

ND

0.2

0.2

0

0.1

0.1

ND

0.20.2

0.3

0.3

0.3

0.3

0.4

0.2

0.2

0.2

ND

0.3

0.2

0.2

ND0.2

0.2

0.20.2

0.2

0.2

0.10.10.2

0.2

0.2

0.10.1

0.1

ND0.3

0.1

0.1

2010 Water Disolved Fluoride (F-) mg/L0.3



Legend



500m0 250

Scale: 1 : 25,000

Lansat Imagery Interpretation by: Alex Harris, B. Sc.Fluoride In Water Anomaly >= 0.3


5287

000m

N52

8800

0m N

5289

000m

N52

9000

0m N

5291

000m

N


NewFluorEx.com Mar 3, 2012 Map: WSP2

Trail

Trail

MineralLicence:

018902M

213m

198m

213m198m

198m

213m

229m

213m

183m

244m

0.2

0.3

D

0.5

0.3

0.4

0.4

0.6

0.5

0.3

0.2

0.5

0.3

0.20.2

0.2

0.4

-ND

0.1

0.30.4

0.30.3

0.3

0.4

0.3

0.3

0.4

0.5

0.4

0.3

Marker

0.10.6

0.4

0.1 0.1 ND

0.1

0.2

0.2

0.2

0.2

0.20.2

0.1

NDND

0.2

ND

0.2

0.2

0.1

0.1 0.1

ND

ND

0.2

0.20.3 0.20.2 0.2 0.2 0.2 0.3 0.1

0.2

0.1

0.2

ND

ND

ND

ND

ND0.20.10.1

0.3

NDND

0.20.20.10.10.2

0.2

0.2

0.10.1

0.10.1

0.1

0.2

0.10.20.1

0.2

ND0.3

0.3

660000m E 661000m E 662000m E 663000m E



2010 & 2011 CompiledFluoride in Water, East




Legend



500m0 250

Scale: 1 : 25,000

Fluoride In Water Anomaly >= 0.3


5288

000m

N52

8900

0m N

659000m E 660000m E



NewFluorEx.com Mar 3, 2012 Map: SP-COMP-1

2011 CompiledWater and Soil Values

MineralLicence:

018902M

213m

229m

213m

198m

198m

183m

Grid F

Line G

Line H

Line I

Line D

Line C

0.3

ND

0.2

130

170

0.2

0.3

0.4

0.5

0.4

0.30.20.1

9 km Trail Marker

BDL

BDLBDL

BDL

170170BDL

BDL

0.2

ND

0.2

0.2

0.1

1

.1

ND

0.2

0.2

ND

ND0.3




Linear Structures From Lansat Imagery Lansat Imagery Interpretation by: Alex Harris, B. Sc.Fluoride In Water Anomaly >= 0.3

0 250m

Scale: 1 : 10,000

1252011 Soil Sample Total Fluoride (F) mg/kg130



Line of Recommended 2012 Samples

5287

000m

N52

8800

0m N

5289

000m

N52

9000

0m N

657000m E 658000m E656000m E 659000m E 660000m E

5291

000m

N

Trail

MineralLicence:

018902M

213

183m

198m

198m

183m

168m

152m

213m

229m

213m

Grid E

Grid F

Line G

Line H

Line I

Line D

Line C

130

170

BDL

BDL

BDL

110

BDL

BDL

BDL

BDLBDL

BDL

150

BDLBDL

170170BDL

BDLBDLN/A

N/A



NewFluorEx.com Mar 3, 2012 Map: SSP1

2011 Soil Sample Total Fluoride (F) mg/kg



Legend



500m0 250

Scale: 1 : 25,000


2011 SoilSample Values, West130



5287

000m

N52

8800

0m N

5289

000m

N52

9000

0m N

5291

000m

N



NewFluorEx.com Mar 3, 2012 Map: SSP2

Trail

Trail

MineralLicence:

018902M

213m

198m

213m198m

198m

213m

229m

213m

183m

244m

Grid F

Line G

Line H

Line I

Line D

Line C

Line A

Grid B

130

170

BDLBDL

BDL

BDL

130

BDL

BDL

BDL

DL

BDL

BDL

110

170

BDL

BDL

BDL

BDLBDL

170170

660000m E 661000m E 662000m E 663000m E

2011 Soil Sample Total Fluoride (F) mg/kg



Legend



500m0 250

Scale: 1 : 25,000


2011 SoilSample Values, East130



APPENDIX 2 Certificates of Analysis

MAXXAM ANALYTICS BEDFORD, NOVA SCOTIA B4B 1G9 Tel: (902) 420-0203 Fax: (902) 420-8916

Toll Free: 1-800-565-7227 www.maxxam.ca ATL FCD 00939 / 1 Page 1 of 1

METHOD SUMMARY Fluoride in Water And Soil 2009/10/07

SOP #: ATL SOP 43

Reference: Standard Methods, 20th ed. Method 4500 - F- C, 1998 1. Scope and Application This method is applicable for the determination of fluoride in water or soil matrices. Total Fluoride requires distillation prior to analysis to meet USEPA wastewater discharge requirements. Some difficulty is encountered with samples that are highly basic/acidic or samples that have dissolved solids above 10,000 mg/L. The Reporting Detection Limit (RDL) is 0.10 mg/L for water samples and 0.5 mg/kg for soil samples. 2. Summary of Method An ion specific electrode is used to measure fluoride concentration. The fluoride electrode measures the ion activity of fluoride in solution rather than concentration. Fluoride ion activity depends on the solution rather than the concentration. Fluoride ion activity depends on the solutions total ionic strength and pH, and on fluoride complexing species. Adding an appropriate buffer provides uniform ion strength background, adjusts pH, and breaks up complexes so in effect, the electrode measures concentration. 3. Quality Assurance Reagent blanks, standard reference materials, and method spikes are analyzed in the same manner as mentioned above for the samples. Spiking of samples at a level appropriate to the matrix is performed at a frequency of 5%. Duplicate samples are also analyzed at a frequency of 5 %.

METHOD SUMMRY

Total Fluoride in Soil

The soil sample is fused with sodium hydroxide and then extracted. The fluoride in extract is determined

potentiometrically using a combination‐specific ion fluoride electrode containing a silver/silver chloride

reference electrode. The agent used for the extraction is NaOH, DI Water, and concentrated HCl.

Your Project #: DB1A8918 Site Location: SAGE POND

Attention: BEDFORD CLIENT SERVICEMAXXAM ANALYTICS200 BLUEWATER ROAD, SUITE 105BEDFORD, NSCANADA B4B 1G9

Report Date: 2011/08/02This report supersedes all previous reports with the same Maxxam job number

CERTIFICATE OF ANALYSIS

MAXXAM JOB #: B166645Received: 2011/07/23, 9:40

Sample Matrix: Soil# Samples Received: 25

Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodFluoride (Extractable, sat. paste) 25 N/A 2011/07/29 AB SOP-00005 SM 4500-F Soluble Paste 15 2011/07/27 2011/07/27 AB SOP-00033 SSMA 15.2 Soluble Paste 10 2011/07/28 2011/07/28 AB SOP-00033 SSMA 15.2

* Results relate only to the items tested.

Encryption Key

Please direct all questions regarding this Certificate of Analysis to your Project Manager.

Joyce Kimani, Project Manager AssistantEmail: [email protected]# (403) 291-3077

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section5.10.2 of ISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

Total cover pages: 1

Maxxam Analytics International Corporation o/a Maxxam Analytics Calgary: 2021 - 41st Avenue N.E. T2E 6P2 Telephone(403) 291-3077 Fax(403) 291-9468

Page 1 of 5

MAXXAM ANALYTICSMaxxam Job #: B166645 Client Project #: DB1A8918Report Date: 2011/08/02 Site Location: SAGE POND

RESULTS OF CHEMICAL ANALYSES OF SOIL

Maxxam ID BB7126 BB7127 BB7128 BB7129 BB7130 BB7131 BB7132Sampling Date 2011/07/14 2011/07/14 2011/07/14 2011/07/14 2011/07/14 2011/07/14 2011/07/14

09:44 10:15 10:57 11:09 11:30 11:44 12:20Units SSP-09 SSP-10 SSP-11 SSP-12 SSP-13 SSP-14 SSP-15 RDL QC Batch

(KG4734-01R) (KG4736-01R) (KG4737-01R) (KG4738-01R) (KG4739-01R) (KG4740-01R) (KG4741-01R)Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5046665Saturation % % 56 58 34 39 64 35 45 N/A 5043936



(KG4742-01R) (KG4743-01R) (KG4744-01R) (KG4831-01R) (KG4834-01R) (KG4835-01R) (KG4836-01R)Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5046665Saturation % % 34 39 34 59 56 72 40 N/A 5043936


12:41 12:49 12:49 14:22 10:32 11:12 11:51Units SSP-33 QC Batch SSP-34 SSP-34 SSP-19 SSP-21 SSP-22 SSP-23 RDL QC Batch

(KG4837-01R) (KG4838-01R) (KG4838-01R) (KG4840-01R) (KG4842-01R) (KG4843-01R) (KG4844-01R)Lab-Dup

Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 5046665 <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5046665Saturation % % 55 5043936 40 N/A 43 46 98 64 N/A 5045781

Maxxam ID BB7148 BB7149 BB7150 BB7151 BB7152Sampling Date 2011/07/18 12:51 2011/07/18 13:18 2011/07/18 13:57 2011/07/19 09:15 2011/07/19 11:48

Units SSP-24 SSP-25 SSP-26 SSP-27 SSP-28 RDL QC Batch(KG4845-01R) (KG4846-01R) (KG4847-01R) (KG4848-01R) (KG4849-01R)

Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5048741Saturation % % 70 41 46 46 79 N/A 5045781

N/A = Not ApplicableRDL = Reportable Detection Limit

Page 2 of 5


Package 1 7.7°CEach temperature is the average of up to three cooler temperatures taken at receipt

General Comments

Page 3 of 5


QUALITY ASSURANCE REPORT

Spiked Blank Method Blank RPD QC StandardQC Batch Parameter Date % Recovery QC Limits Value Units Value (%) QC Limits % Recovery QC Limits5043936 Saturation % 2011/07/27 9.3 12 103 93 - 1075045781 Saturation % 2011/07/28 7.2 12 100 93 - 1075046665 Extractable (paste) Fluoride (F) 2011/07/29 96 86 - 117 <0.5 mg/L NC 405048741 Extractable (paste) Fluoride (F) 2011/07/29 101 86 - 117 <0.5 mg/L NC 40

N/A = Not ApplicableRPD = Relative Percent DifferenceDuplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.QC Standard: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

Page 4 of 5

Validation Signature Page

Maxxam Job #: B166645

The analytical data and all QC contained in this report were reviewed and validated by the following individual(s).

Ghayasuddin Khan, M.Sc., B.Ed., P.Chem, Senior Analyst, Water Lab

====================================================================Maxxam has procedures in place to guard against improper use of the electronic signature and have the required "signatories", as per section 5.10.2 ofISO/IEC 17025:2005(E), signing the reports. For Service Group specific validation please refer to the Validation Signature Page.

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Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodTotal Fluoride ( 1 ) 1 N/A 2011/09/08 AB SOP-00005 SM 4500 F-C Total Fluoride ( 1 ) 7 N/A 2011/09/09 AB SOP-00005 SM 4500 F-C Fluoride (Extractable, sat. paste) 8 N/A 2011/07/22 AB SOP-00005 SM 4500-F Soluble Paste 8 2011/07/22 2011/07/15 AB SOP-00033 SSMA 15.2


(1) This test was performed by Maxxam Edmonton Environmental

Encryption Key






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Maxxam ID BB2072 BB2087 BB2087 BB2088 BB2089Sampling Date 2011/06/29 2011/06/29 2011/06/29 2011/06/29 2011/06/29

Units SSP 01 QC Batch SSP 02 SSP 02 SSP 03 SSP 04 RDL QC Batch(KE4135-01R) (KE4136-01R) (KE4136-01R) (KE4137-01R) (KE4138-01R)

Lab-DupMisc. InorganicsTotal Fluoride (F) mg/kg <100 5154635 <100(1) <100 <100 <100 100 5158614Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 5031266 <0.5 N/A <0.5 <0.5 0.5 5031266Saturation % % 52 5028847 33 N/A 47 57 N/A 5028847

Maxxam ID BB2089 BB2090 BB2091 BB2092 BB2093Sampling Date 2011/06/29 2011/06/29 2011/06/29 2011/06/29 2011/06/29

Units SSP 04 SSP 05 SSP 06 SSP 07 SSP 08 RDL QC Batch(KE4138-01R) (KE4139-01R) (KE4140-01R) (KE4141-01R) (KE4143-01R)

Lab-DupMisc. InorganicsTotal Fluoride (F) mg/kg N/A 130 <100 <100 <100 100 5158614Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5031266Saturation % % 56 49 41 50 95 N/A 5028847

N/A = Not ApplicableRDL = Reportable Detection Limit(1) - Matrix Spike exceeds acceptance limits for fluoride soils ,due to matrix interference. Reanalysis yields similar results. (Recovery: 56.77 %, limits: 75-125 %)

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General Comments

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Spiked Blank Method Blank RPD QC StandardQC Batch Parameter Date % Recovery QC Limits Value Units Value (%) QC Limits % Recovery QC Limits5028847 Saturation % 2011/07/15 0.1 12 100 93 - 1075031266 Extractable (paste) Fluoride (F) 2011/07/22 110 93 - 111 <0.5 mg/L NC 405154635 Total Fluoride (F) 2011/09/08 88 80 - 120 <100 mg/kg NC 35 87 75 - 1255158614 Total Fluoride (F) 2011/09/09 82 80 - 120 <100 mg/kg NC 35 108 75 - 125

N/A = Not ApplicableRPD = Relative Percent DifferenceDuplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.QC Standard: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

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Heather Groves, Manager Inorganics Edmonton


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Date DateAnalyses Quantity Extracted Analyzed Laboratory Method Analytical MethodTotal Fluoride ( 1 ) 6 N/A 2011/09/09 AB SOP-00005 SM 4500 F-C Total Fluoride ( 1 ) 19 N/A 2011/09/10 AB SOP-00005 SM 4500 F-C Fluoride (Extractable, sat. paste) 25 N/A 2011/07/29 AB SOP-00005 SM 4500-F Soluble Paste 15 2011/07/27 2011/07/27 AB SOP-00033 SSMA 15.2 Soluble Paste 10 2011/07/28 2011/07/28 AB SOP-00033 SSMA 15.2


(1) This test was performed by Maxxam Edmonton Environmental

Encryption Key






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09:44 10:15 10:57 11:09 11:30 11:44 12:20Units SSP-09 SSP-10 SSP-11 SSP-12 SSP-13 SSP-14 QC Batch SSP-15 RDL QC Batch

(KG4734-01R) (KG4736-01R) (KG4737-01R) (KG4738-01R) (KG4739-01R) (KG4740-01R) (KG4741-01R)Misc. InorganicsTotal Fluoride (F) mg/kg <100 <100 110 <100 130 <100 5158614 <100 100 5161467Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 5046665 <0.5 0.5 5046665Saturation % % 56 58 34 39 64 35 5043936 45 N/A 5043936




Misc. InorganicsTotal Fluoride (F) mg/kg <100 <100 <100 <100 <100 170 170 100 5161467Soluble ParametersExtractable (paste) Fluoride (F) mg/L N/A <0.5 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5046665Saturation % % N/A 34 39 34 59 56 72 N/A 5043936


12:31 12:41 12:49 12:49 14:22 10:32 11:12Units SSP-32 SSP-33 QC Batch SSP-34 SSP-34 SSP-19 SSP-21 SSP-22 RDL QC Batch


Misc. InorganicsTotal Fluoride (F) mg/kg <100 <100 5161467 <100 N/A 150 <100 110 100 5161467Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 <0.5 5046665 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5046665Saturation % % 40 55 5043936 40 N/A 43 46 98 N/A 5045781


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Maxxam ID BB7147 BB7148 BB7149 BB7150 BB7151 BB7152Sampling Date 2011/07/18 2011/07/18 2011/07/18 2011/07/18 2011/07/19 2011/07/19

11:51 12:51 13:18 13:57 09:15 11:48Units SSP-23 QC Batch SSP-24 SSP-25 SSP-26 SSP-27 SSP-28 RDL QC Batch

(KG4844-01R) (KG4845-01R) (KG4846-01R) (KG4847-01R) (KG4848-01R) (KG4849-01R)Misc. InorganicsTotal Fluoride (F) mg/kg 170 5161467 <100 <100 <100 170 <100 100 5161467Soluble ParametersExtractable (paste) Fluoride (F) mg/L <0.5 5046665 <0.5 <0.5 <0.5 <0.5 <0.5 0.5 5048741Saturation % % 64 5045781 70 41 46 46 79 N/A 5045781


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General Comments

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Matrix Spike Spiked Blank Method Blank RPD QC StandardQC Batch Parameter Date % Recovery QC Limits % Recovery QC Limits Value Units Value (%) QC Limits % Recovery QC Limits5043936 Saturation % 2011/07/27 9.3 12 103 93 - 1075045781 Saturation % 2011/07/28 7.2 12 100 93 - 1075046665 Extractable (paste) Fluoride (F) 2011/07/29 96 86 - 117 <0.5 mg/L NC 405048741 Extractable (paste) Fluoride (F) 2011/07/29 101 86 - 117 <0.5 mg/L NC 405158614 Total Fluoride (F) 2011/09/09 82 80 - 120 <100 mg/kg NC 35 108 75 - 1255161467 Total Fluoride (F) 2011/09/10 91 80 - 120 93 80 - 120 <100 mg/kg NC 35 97 75 - 125

N/A = Not ApplicableRPD = Relative Percent DifferenceDuplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.QC Standard: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit a reliable calculation.

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Heather Groves, Manager Inorganics Edmonton


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Site Location: SAGE POND Your C.O.C. #: 06062

Attention: Alex HarrisNewFluorEx5-1035 Boychuk DrSaskatoon, SKCANADA S7H5B2



MAXXAM JOB #: B1A5034Received: 2011/07/14, 9:36


Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTotal Fluoride Soil (Fusion Extraction) ( 1 ) 8 2011/09/12 2011/09/13 Fluoride (Extractable, sat. paste) Solid ( 2 ) 8 2011/07/21 2011/07/25

Sample Matrix: Water# Samples Received: 25

Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceFluoride 13 N/A 2011/07/16 ATL SOP 00043 R3 Based on SM4500F-C Fluoride 12 N/A 2011/07/19 ATL SOP 00043 R3 Based on SM4500F-C

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed by Bedford to Edm Env Subcontract(2) This test was performed by Bedford to Calgary Subcontract

Encryption Key


KATIE COHOON, Bedford Client ServicesEmail: [email protected]# (902) 420-0203



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NewFluorExMaxxam Job #: B1A5034Report Date: 2011/09/13 Site Location: SAGE POND

RESULTS OF ANALYSES OF SOIL

Maxxam ID K E 4 1 3 5 K E 4 1 3 6 K E 4 1 3 7 K E 4 1 3 8 K E 4 1 3 9Sampling Date 2011/06/29 2011/06/29 2011/06/29 2011/06/29 2011/06/29

10:08 10:19 10:32 10:43 10:50COC Number 06062 06062 06062 06062 06062

U n i t s SSP 01 SSP 02 SSP 03 SSP 04 SSP 05 QC Batch

Subcontracted Analysis

Subcontract Parameter N/A ATTACHED ATTACHED ATTACHED ATTACHED ATTACHED 2557475

QC Batch = Quality Control Batch

Maxxam ID K E 4 1 4 0 K E 4 1 4 1 K E 4 1 4 3Sampling Date 2011/06/29 2011/06/29 2011/06/29

13:19 13:50 14:27COC Number 06062 06062 06062

U n i t s SSP 06 SSP 07 SSP 08 QC Batch


Subcontract Parameter N/A ATTACHED ATTACHED ATTACHED 2557475


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RESULTS OF ANALYSES OF WATER

Maxxam ID K E 4 0 9 4 K E 4 0 9 5 K E 4 0 9 6 K E 4 0 9 7Sampling Date 2011/06/29 2011/06/29 2011/06/29 2011/06/29

10:13 10:27 10:52 11:17COC Number 06062 06062 06062 06062

U n i t s Criteria A WSP 050 WSP 051 WSP 052 WSP 053 RDL QC Batch

Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.1 0.6 0.4 0.1 0.1 2553215

RDL = Reportable Detection LimitQC Batch = Quality Control BatchCriteria A: Guideline - Summary of Guidelines for Canadian Drinking Water Quality (SGCDWQ), Health Canada, Dec. 2010.

A= Maximum Acceptable Concentration (MAC) - established for substances that are known or suspected to cause adverse effects onhealth. When exceeded, minimum action required is immediate resampling. If continuous exceedance occurs, the local authorityresponsible for drinking water supplies should be consulted concerning appropriate corrective action.

C= Aesthetic Objectives (AO) - apply to characteristics of drinking water that can affect its acceptance by consumers or interfere withpractices for supplying good quality water. If a concentration is well above an AO, then there is a possibility of a health hazard.

Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatment system. For slow sand or diatomaceous earth filtration 1.0NTU and for membrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants using aluminium-based coagulants, 0.2mg/L applies to other typesof treatment systems.

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11:23 11:31 11:39 11:58COC Number 06062 06062 06062 06062


Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.1 ND 0.1 0.2 0.1 2553215

ND = Not detectedRDL = Reportable Detection LimitQC Batch = Quality Control BatchCriteria A: Guideline - Summary of Guidelines for Canadian Drinking Water Quality (SGCDWQ), Health Canada, Dec. 2010.




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12:10 12:14 12:20 12:24COC Number 06062 06062 06062 06062


Inorganics






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12:31 12:39 12:44 12:58COC Number 06062 06062 06062 06062

U n i t s Criteria A WSP 062 QC Batch WSP 063 WSP 064 WSP 065 RDL QC Batch

Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.2 2553215 0.2 0.2 0.1 0.1 2555994


A= Maximum Acceptable Concentration (MAC) - established for substances that are known or suspected to cause adverse effects on health. Whenexceeded, minimum action required is immediate resampling. If continuous exceedance occurs, the local authority responsible for drinking watersupplies should be consulted concerning appropriate corrective action.

C= Aesthetic Objectives (AO) - apply to characteristics of drinking water that can affect its acceptance by consumers or interfere with practices forsupplying good quality water. If a concentration is well above an AO, then there is a possibility of a health hazard.

Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatment system. For slow sand or diatomaceous earth filtration 1.0 NTU andfor membrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants using aluminium-based coagulants, 0.2mg/L applies to other types of treatmentsystems.

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13:32 13:37 13:50 13:59COC Number 06062 06062 06062 06062

U n i t s Criteria A WSP 066 WSP 067 WSP 068 QC Batch WSP 069 RDL QC Batch

Inorganics

Dissolved Fluoride (F-) mg/L 1.5 ND ND 0.2 2555994 ND 0.1 2556000


A= Maximum Acceptable Concentration (MAC) - established for substances that are known or suspected to cause adverse effects on health. Whenexceeded, minimum action required is immediate resampling. If continuous exceedance occurs, the local authority responsible for drinking watersupplies should be consulted concerning appropriate corrective action.


Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatment system. For slow sand or diatomaceous earth filtration 1.0 NTU andfor membrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants using aluminium-based coagulants, 0.2mg/L applies to other types of treatmentsystems.

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14:07 14:14 14:19 14:31COC Number 06062 06062 06062 06062


Inorganics






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Maxxam ID K E 4 1 1 8Sampling Date 2011/06/29

14:35COC Number 06062

U n i t s Criteria A WSP 074 RDL QC Batch

Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.1 0.1 2556000

RDL = Reportable Detection LimitQC Batch = Quality Control BatchCriteria A: Guideline - Summary of Guidelines for Canadian Drinking WaterQuality (SGCDWQ), Health Canada, Dec. 2010.

A= Maximum Acceptable Concentration (MAC) - established for substancesthat are known or suspected to cause adverse effects on health. Whenexceeded, minimum action required is immediate resampling. If continuousexceedance occurs, the local authority responsible for drinking water suppliesshould be consulted concerning appropriate corrective action.

C= Aesthetic Objectives (AO) - apply to characteristics of drinking water thatcan affect its acceptance by consumers or interfere with practices forsupplying good quality water. If a concentration is well above an AO, thenthere is a possibility of a health hazard.

Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatmentsystem. For slow sand or diatomaceous earth filtration 1.0 NTU and formembrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants usingaluminium-based coagulants, 0.2mg/L applies to other types of treatmentsystems.

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GENERAL COMMENTS

Results relate only to the items tested.

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NewFluorExAttention: Alex Harris Client Project #: P.O. #: Site Location: SAGE POND

Quality Assurance ReportMaxxam Job Number: DB1A5034

QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits

2553215 TPE Matrix Spike Dissolved Fluoride (F-) 2011/07/16 102 % 80 - 120QC Standard Dissolved Fluoride (F-) 2011/07/16 98 % 80 - 120Spiked Blank Dissolved Fluoride (F-) 2011/07/16 101 % 80 - 120Method Blank Dissolved Fluoride (F-) 2011/07/16 ND, RDL=0.1 mg/LRPD Dissolved Fluoride (F-) 2011/07/16 NC % 25



Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.QC Standard: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit areliable calculation.

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Maxxam Job #: B1A5034


MIKE MACGILLIVRAY, Scientific Specialist (Inorganics)


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Site Location: SAGE POND Your C.O.C. #: 06067

Attention: Alex HarrisNewFluorEx5-1035 Boychuk DrSaskatoon, SKCANADA S7H5B2



MAXXAM JOB #: B1A8918Received: 2011/07/21, 10:19


Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceTotal Fluoride Soil (Fusion Extraction) ( 1 ) 25 2011/09/12 2011/09/13 Fluoride (Extractable, sat. paste) Solid ( 2 ) 25 2011/07/25 2011/08/02

Sample Matrix: Water# Samples Received: 74

Date Date MethodAnalyses Quantity Extracted Analyzed Laboratory Method ReferenceFluoride 39 N/A 2011/07/30 ATL SOP 00043 R3 Based on SM4500F-C Fluoride 35 N/A 2011/08/01 ATL SOP 00043 R3 Based on SM4500F-C

* RPDs calculated using raw data. The rounding of final results may result in the apparent difference.

(1) This test was performed by Bedford to Edm Env Subcontract(2) This test was performed by Bedford to Calgary Subcontract

Encryption Key


KATIE COHOON, Bedford Client ServicesEmail: [email protected]# (902) 420-0203



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Maxxam ID K G 4 7 3 4 K G 4 7 3 6 K G 4 7 3 7 K G 4 7 3 8 K G 4 7 3 9 K G 4 7 4 0Sampling Date 2011/07/14 2011/07/14 2011/07/14 2011/07/14 2011/07/14 2011/07/14COC Number 06067 06067 06067 06067 06067 06067

U n i t s SSP 09 SSP 10 SSP 11 SSP 12 SSP 13 SSP 14 QC Batch


Subcontract Parameter N/A ATTACHED ATTACHED ATTACHED ATTACHED ATTACHED ATTACHED 2561020












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Maxxam ID K G 4 8 4 9Sampling Date 2011/07/19COC Number 06067

U n i t s SSP 28 QC Batch


Subcontract Parameter N/A ATTACHED 2561020


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Maxxam ID K G 4 7 5 6 K G 4 7 7 2 K G 4 7 7 3 K G 4 7 7 9 K G 4 7 9 1Sampling Date 2011/07/19 2011/07/19 2011/07/19 2011/07/19 2011/07/19COC Number 06067 06067 06067 06067 06067

U n i t s Criteria A WSP 145 WSP 146 WSP 147 WSP 148 WSP 135 RDL QC Batch

Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.1 0.2 ND 0.3 0.2 0.1 2567830




Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatment system. For slow sand or diatomaceous earth filtration1.0 NTU and for membrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants using aluminium-based coagulants, 0.2mg/L applies to othertypes of treatment systems.

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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.2 0.1 0.1 0.1 0.1 0.1 2567830





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Inorganics






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U n i t s Criteria A WSP 126 WSP 127 WSP 128 WSP 129 QC Batch WSP 130 RDL QC Batch

Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.1 0.3 ND ND 2567830 0.2 0.1 2567835


A= Maximum Acceptable Concentration (MAC) - established for substances that are known or suspected to cause adverse effects on health.When exceeded, minimum action required is immediate resampling. If continuous exceedance occurs, the local authority responsible for drinkingwater supplies should be consulted concerning appropriate corrective action.


Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatment system. For slow sand or diatomaceous earth filtration 1.0 NTU andfor membrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants using aluminium-based coagulants, 0.2mg/L applies to other types oftreatment systems.

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Inorganics






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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.2 0.1 0.2 ND ND 0.1 2567835





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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 ND ND ND 0.2 0.2 0.1 2567835





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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.2 0.3 0.3 0.2 2567835 0.2 0.1 2567850





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Inorganics






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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.2 ND 0.2 0.2 0.2 0.1 2567850





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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.2 0.2 0.2 ND 0.3 0.1 2567850





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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.4 0.2 0.2 0.2 2567850 0.2 0.1 2567885





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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 ND 0.3 ND 0.3 0.1 0.1 2567885





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Inorganics

Dissolved Fluoride (F-) mg/L 1.5 0.1 ND 0.2 0.2 0.1 0.1 2567885





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Maxxam ID K G 4 9 5 0 K G 4 9 5 1 K G 4 9 5 2 K G 4 9 5 3Sampling Date 2011/07/14 2011/07/14 2011/07/14 2011/07/14COC Number 06067 06067 06067 06067


Inorganics


RDL = Reportable Detection LimitQC Batch = Quality Control BatchCriteria A: Guideline - Summary of Guidelines for Canadian Drinking Water Quality (SGCDWQ), Health Canada, Dec.2010.

A= Maximum Acceptable Concentration (MAC) - established for substances that are known or suspected to causeadverse effects on health. When exceeded, minimum action required is immediate resampling. If continuousexceedance occurs, the local authority responsible for drinking water supplies should be consulted concerningappropriate corrective action.

C= Aesthetic Objectives (AO) - apply to characteristics of drinking water that can affect its acceptance by consumers orinterfere with practices for supplying good quality water. If a concentration is well above an AO, then there is apossibility of a health hazard.

Note 1 Turbidity guideline value of 0.3 NTU based on conventional treatment system. For slow sand or diatomaceousearth filtration 1.0 NTU and for membrane filtration 0.1 NTU.Note 2 Aluminium guideline value of 0.1 mg/L is for treatment plants using aluminium-based coagulants, 0.2mg/Lapplies to other types of treatment systems.

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GENERAL COMMENTS

Results relate only to the items tested.

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NewFluorExAttention: Alex Harris Client Project #: P.O. #: Site Location: SAGE POND

Quality Assurance ReportMaxxam Job Number: DB1A8918

QA/QC DateBatch AnalyzedNum Init QC Type Parameter yyyy/mm/dd Value Recovery Units QC Limits

2567830 KMC Matrix Spike[KG4805-01] Dissolved Fluoride (F-) 2011/07/30 110 % N/AQC Standard Dissolved Fluoride (F-) 2011/07/30 100 % 80 - 120Spiked Blank Dissolved Fluoride (F-) 2011/07/30 103 % 80 - 120Method Blank Dissolved Fluoride (F-) 2011/07/30 ND, RDL=0.1 mg/LRPD [ K G 4 8 0 5 - 0 1 ] Dissolved Fluoride (F-) 2011/07/30 NC % 25



2567885 KMC Matrix Spike Dissolved Fluoride (F-) 2011/08/01 104 % N/AQC Standard Dissolved Fluoride (F-) 2011/08/01 100 % 80 - 120Spiked Blank Dissolved Fluoride (F-) 2011/08/01 102 % 80 - 120Method Blank Dissolved Fluoride (F-) 2011/08/01 ND, RDL=0.1 mg/LRPD Dissolved Fluoride (F-) 2011/08/01 NC % 25

Duplicate: Paired analysis of a separate portion of the same sample. Used to evaluate the variance in the measurement.Matrix Spike: A sample to which a known amount of the analyte of interest has been added. Used to evaluate sample matrix interference.QC Standard: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Spiked Blank: A blank matrix to which a known amount of the analyte has been added. Used to evaluate analyte recovery.Method Blank: A blank matrix containing all reagents used in the analytical procedure. Used to identify laboratory contamination.NC (RPD): The RPD was not calculated. The level of analyte detected in the parent sample and its duplicate was not sufficiently significant to permit areliable calculation.

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Maxxam Job #: B1A8918


ERIC DEARMAN, Scientific Specialist

KEVIN MACDONALD, Inorganics Supervisor

MIKE MACGILLIVRAY, Scientific Specialist (Inorganics)


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APPENDIX 3 GPS Data Listing

Fluoride in Water (F) mg / Litre Grid: UTM

Sage Pond 2011 Datum: NAD27 Canada

Name mg / L Date Time Zone UTM East North Elev. Units

WSP050 0.1 29‐Jun‐11 10:13AM 21 T 661059 5289591 225 m

WSP051 0.6 29‐Jun‐11 10:27AM 21 T 661322 5289649 208 m

WSP052 0.4 29‐Jun‐11 10:52AM 21 T 661921 5289995 188 m

WSP053 0.1 29‐Jun‐11 11:17AM 21 T 662205 5289792 228 m

WSP054 0.1 29‐Jun‐11 11:23AM 21 T 662386 5289792 244 m

WSP055 ND 29‐Jun‐11 11:31AM 21 T 662669 5289808 245 m

WSP056 0.1 29‐Jun‐11 11:39AM 21 T 662578 5289881 241 m

WSP057 0.2 29‐Jun‐11 11:58AM 21 T 662312 5290369 197 m

WSP058 0.2 29‐Jun‐11 12:10PM 21 T 662536 5290742 197 m

WSP059 0.2 29‐Jun‐11 12:14PM 21 T 662444 5290756 191 m

WSP060 0.3 29‐Jun‐11 12:20PM 21 T 662344 5290775 186 m

WSP061 0.2 29‐Jun‐11 12:24PM 21 T 662237 5290715 186 m

WSP062 0.2 29‐Jun‐11 12:31PM 21 T 662065 5290609 190 m

WSP063 0.2 29‐Jun‐11 12:39PM 21 T 661844 5290367 182 m

WSP064 0.2 29‐Jun‐11 12:44PM 21 T 661760 5290265 181 m

WSP065 0.1 29‐Jun‐11 12:58PM 21 T 661182 5289844 217 m

WSP066 ND 29‐Jun‐11 1:32PM 21 T 660789 5289462 229 m

WSP067 ND 29‐Jun‐11 1:37PM 21 T 660519 5289362 221 m

WSP068 0.2 29‐Jun‐11 1:50PM 21 T 660051 5289115 207 m

WSP069 ND 29‐Jun‐11 1:59PM 21 T 660016 5289273 209 m

WSP070 0.2 29‐Jun‐11 2:07PM 21 T 660023 5289487 206 m

WSP071 0.2 29‐Jun‐11 2:14PM 21 T 660144 5289606 216 m

WSP072 0.1 29‐Jun‐11 2:19PM 21 T 660244 5289757 208 m

WSP073 0.1 29‐Jun‐11 2:31PM 21 T 660400 5290095 218 m

WSP074 0.1 29‐Jun‐11 2:35PM 21 T 660469 5290152 221 m

WSP075 0.1 14‐Jul‐11 9:41AM 21 T 658488 5289248 198 m

WSP076 0.1 14‐Jul‐11 9:49AM 21 T 658498 5289431 192 m

WSP077 ND 14‐Jul‐11 9:58AM 21 T 658541 5289557 194 m

WSP078 0.2 14‐Jul‐11 10:01AM 21 T 658597 5289723 184 m

WSP079 0.2 14‐Jul‐11 10:06AM 21 T 658615 5289811 181 m

WSP080 0.1 14‐Jul‐11 10:12AM 21 T 658633 5289941

WSP081 0.3 14‐Jul‐11 10:21AM 21 T 658592 5290139 175 m

WSP082 0.3 14‐Jul‐11 10:27AM 21 T 658540 5290315 176 m

WSP083 0.3 14‐Jul‐11 10:31AM 21 T 658744 5290501 173 m

WSP084 0.3 14‐Jul‐11 10:43AM 21 T 658923 5290600 171 m

WSP085 0.3 14‐Jul‐11 10:50AM 21 T 658953 5290477

WSP086 0.4 14‐Jul‐11 10:55AM 21 T 658965 5290359 176 m

WSP087 0.2 14‐Jul‐11 11:02AM 21 T 658950 5290238 177 m

ND = Not Detected

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WSP088 0.2 14‐Jul‐11 11:06AM 21 T 658985 5290092 182 m

WSP089 0.2 14‐Jul‐11 11:13AM 21 T 659024 5289967 185 m

WSP090 0.2 14‐Jul‐11 11:17AM 21 T 659041 5289830 186 m

WSP091 ND 14‐Jul‐11 11:23AM 21 T 659081 5289657 190 m

WSP092 0.3 14‐Jul‐11 11:29AM 21 T 659112 5289480 198 m

WSP093 ND 14‐Jul‐11 11:41AM 21 T 659148 5289084 209 m

WSP094 0.3 14‐Jul‐11 12:58PM 21 T 657205 5288046 211 m

WSP095 0.2 14‐Jul‐11 1:09PM 21 T 657110 5287890 222 m

WSP096 0.2 14‐Jul‐11 1:14PM 21 T 657082 5287765 211 m

WSP097 ND 14‐Jul‐11 1:22PM 21 T 656866 5287670 210 m

WSP098 0.2 14‐Jul‐11 1:28PM 21 T 656725 5287583 210 m

WSP099 0.2 14‐Jul‐11 1:33PM 21 T 656666 5287661 200 m

WSP100 0.2 14‐Jul‐11 1:57PM 21 T 656647 5287889 203 m

WSP101 0.2 14‐Jul‐11 2:02PM 21 T 656664 5287987 204 m

WSP102 0.2 14‐Jul‐11 2:08PM 21 T 656708 5288070 202 m

WSP103 0.2 14‐Jul‐11 2:18PM 21 T 656817 5288238 208 m

WSP104 ND 18‐Jul‐11 10:41AM 21 T 660576 5290436 217 m

WSP105 0.2 18‐Jul‐11 10:49AM 21 T 660690 5290679 202 m

WSP106 0.2 18‐Jul‐11 10:55AM 21 T 660637 5290890 199 m

WSP107 0.3 18‐Jul‐11 11:01AM 21 T 660783 5290894 189 m

WSP108 0.3 18‐Jul‐11 11:18AM 21 T 661088 5290893

WSP109 0.2 18‐Jul‐11 11:31AM 21 T 661341 5290869 177 m

WSP110 0.2 18‐Jul‐11 11:41AM 21 T 661761 5290965 176 m

WSP111 0.2 18‐Jul‐11 11:57AM 21 T 662126 5290980 182 m

WSP112 0.2 18‐Jul‐11 12:05PM 21 T 662355 5291009 180 m

WSP113 0.2 18‐Jul‐11 12:11PM 21 T 662592 5291037 178 m

WSP114 0.3 18‐Jul‐11 12:17PM 21 T 662736 5291030 183 m

WSP115 0.1 18‐Jul‐11 12:24PM 21 T 662953 5291017 175 m

WSP116 0.2 18‐Jul‐11 12:31PM 21 T 662940 5290863 205 m

WSP117 0.1 18‐Jul‐11 12:37PM 21 T 662930 5290677 210 m

WSP118 0.2 18‐Jul‐11 12:44PM 21 T 662923 5290429 220 m

WSP119 ND 18‐Jul‐11 12:57PM 21 T 662915 5290250 227 m

WSP120 ND 18‐Jul‐11 1:03PM 21 T 662892 5290044 239 m

WSP121 ND 18‐Jul‐11 1:12PM 21 T 662937 5289805 257 m

WSP122 ND 18‐Jul‐11 1:24PM 21 T 662992 5289608 271 m

WSP123 ND 18‐Jul‐11 1:33PM 21 T 662852 5289500 269 m

WSP124 0.2 18‐Jul‐11 1:40PM 21 T 662666 5289454 262 m

WSP125 0.1 18‐Jul‐11 2:02PM 21 T 662275 5289562 239 m

WSP126 0.1 18‐Jul‐11 2:08PM 21 T 662093 5289584 219 m

ND = Not Detected

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WSP127 0.3 18‐Jul‐11 2:15PM 21 T 661989 5289715 205 m

WSP128 ND 18‐Jul‐11 2:43PM 21 T 661049 5289995 219 m

WSP129 ND 18‐Jul‐11 2:49PM 21 T 660814 5290044 222 m

WSP130 0.2 19‐Jul‐11 9:20AM 21 T 660503 5290737 198 m

WSP131 0.2 19‐Jul‐11 9:26AM 21 T 660334 5290713 193 m

WSP132 0.1 19‐Jul‐11 9:30AM 21 T 660174 5290689 195 m

WSP133 0.1 19‐Jul‐11 9:39AM 21 T 659911 5290664 185 m

WSP134 0.2 19‐Jul‐11 9:46AM 21 T 659624 5290590 174 m

WSP135 0.2 19‐Jul‐11 9:53AM 21 T 659746 5290446 184 m

WSP136 0.2 19‐Jul‐11 9:58AM 21 T 659837 5290331 186 m

WSP137 0.1 19‐Jul‐11 10:04AM 21 T 659970 5290204 204 m

WSP138 0.1 19‐Jul‐11 10:08AM 21 T 660077 5290113 206 m

WSP139 0.1 19‐Jul‐11 10:14AM 21 T 660165 5290254 209 m

WSP140 0.1 19‐Jul‐11 10:19AM 21 T 660313 5290358 209 m

WSP141 0.1 19‐Jul‐11 10:24AM 21 T 660416 5290501 201 m

WSP142 0.2 19‐Jul‐11 10:29AM 21 T 660494 5290619 199 m

WSP143 0.1 19‐Jul‐11 10:57AM 21 T 660913 5289198 215 m

WSP144 0.2 19‐Jul‐11 11:01AM 21 T 660806 5289188 214 m

WSP145 0.1 19‐Jul‐11 11:07AM 21 T 660613 5289148 210 m

WSP146 0.2 19‐Jul‐11 11:12AM 21 T 660414 5289101 203 m

WSP147 ND 19‐Jul‐11 11:20AM 21 T 660094 5288961 199 m

WSP148 0.3 19‐Jul‐11 11:25AM 21 T 659964 5288928 197 m

ND = Not Detected

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Sage Pond 2011 Grid: UTM

Fluoride in Soil Datum: NAD27 Canada

Name mg / kg Date Time Zone UTM East North Elev. Units

SSP01 BDL 29‐Jun‐11 10:08AM 21 T 661001 5289557 228 m

SSP02 BDL 29‐Jun‐11 10:19AM 21 T 661144 5289595 225 m

SSP03 BDL 29‐Jun‐11 10:32AM 21 T 661415 5289718 200 m

SSP04 BDL 29‐Jun‐11 10:43AM 21 T 661797 5289955 187 m

SSP05 130 29‐Jun‐11 11:50AM 21 T 662380 5290117 223 m

SSP06 BDL 29‐Jun‐11 1:19PM 21 T 660907 5289507 233 m

SSP07 BDL 29‐Jun‐11 1:50PM 21 T 660053 5289202 208 m

SSP08 BDL 29‐Jun‐11 2:27PM 21 T 660422 5289999 218 m

SSP09 BDL 14‐Jul‐11 9:44AM 21 T 658493 5289312 197 m

SSP10 BDL 14‐Jul‐11 10:15AM 21 T 658645 5289967 183 m

SSP11 110 14‐Jul‐11 10:57AM 21 T 658929 5290318 184 m

SSP12 BDL 14‐Jul‐11 11:09AM 21 T 659007 5290035 185 m

SSP13 130 14‐Jul‐11 11:30AM 21 T 659108 5289455 202 m

SSP14 BDL 14‐Jul‐11 11:44AM 21 T 659126 5289025 213 m

SSP15 BDL 14‐Jul‐11 12:20PM 21 T 658443 5289165 198 m

SSP16 BDL 14‐Jul‐11 12:59PM 21 T 657242 5288076 229 m

SSP17 BDL 14‐Jul‐11 2:04PM 21 T 656707 5288003 206 m

SSP18 BDL 14‐Jul‐11 2:12PM 21 T 656831 5288160 214 m

SSP19 150 14‐Jul‐11 2:22PM 21 T 657031 5288298 211 m

SSP20 N/A 14‐Jul‐11 2:43PM 21 T 657726 5288293

SSP21 BDL 18‐Jul‐11 10:32AM 21 T 660616 5290148 225 m

SSP22 110 18‐Jul‐11 11:12AM 21 T 660875 5290895 192 m

SSP23 170 18‐Jul‐11 11:51AM 21 T 661917 5290988 183 m

SSP24 BDL 18‐Jul‐11 12:51PM 21 T 662924 5290374 222 m

SSP25 BDL 18‐Jul‐11 1:18PM 21 T 662968 5289699 267 m

SSP26 BDL 18‐Jul‐11 1:57PM 21 T 662412 5289509 246 m

SSP27 170 19‐Jul‐11 9:15AM 21 T 659699 5288864

SSP28 BDL 19‐Jul‐11 11:48AM 21 T 659862 5289043 203 m

SSP29 BDL 19‐Jul‐11 11:58AM 21 T 659628 5288951 208 m

SSP30 170 19‐Jul‐11 12:09PM 21 T 659397 5288778 210 m

SSP31 170 19‐Jul‐11 12:20PM 21 T 659153 5288790 209 m

SSP32 BDL 19‐Jul‐11 12:31PM 21 T 658918 5288727 214 m

SSP33 BDL 19‐Jul‐11 12:41PM 21 T 658696 5288561 211 m

SSP34 BDL 19‐Jul‐11 12:49PM 21 T 658439 5288502 209 m

SSP35 N/A 19‐Jul‐11 1:01PM 21 T 658215 5288414 214 m

DBL = Below Detection Limit <100

N/A = Sample Damaged in Transit

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Rock Sample Locatons Grid: UTM


Name Date Time Zone UTM East North Elev. Units

RSP10 29‐Jun‐11 10:54AM 21 T 662043 5289892 221 m

RSP11 14‐Jul‐11 1:46PM 21 T 656585 5287752 197 m

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APPENDIX 4 Statement of Expenditures Field Labour, 2011 $ 6,510.00 Lab costs 5,906.10 Hotels 332.22 Meals 42.71 ATV Rental and Gas 202.99 Personal Vehicles used at $0.50/km. 919.36 Software for converting files 78.90 Evaluation of Field Results Report Preparation, Research 1,095.00 Drafting and Data Processing, 1,020.00 Subtotal $16,409.25 15% Overhead Expense 2,461.39 TOTAL $18,870.64

APPENDIX 5 List of Personnel Alex Harris, B. Sc., Geologist, Saskatoon, Sask. Field Work: June 29; July 14, 18, 19, 2011.

Research and Planning: Mar. 25, 2011; Apr. 11, 2011; Jun. 11, 27, 28, 2011; July 5, 12, 13, 15, 20, 25, 2011; Aug. 4, 8, 2011; Oct. 3, 2011; Jan. 20, 23, 2012. Report Preparation: Feb. 4, 18, 24, 25, 2012; Mar. 1, 3, 2012.

Gordon Stefanuk, C. Tech., Draftsman, GIS and Data Processing, Lloydminster, AB.

Drafting, Data Processing etc.: Mar. 19, 2011; Apr. 10, 2011; Jul.28, 2011; Jan. 17, 18, 19, 20, 21, 22, 23, 2012; Feb. 16, 24, 25, 27, 2012; Mar. 1, 3, 2012.

Bill Taylor, Prospector, Marystown, NL. Field Work:June 29; July 14, 18. 19, 2011.

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