low concentration water for inorganic analysissignature : ^tyt^fraxa. taou-x6l -fvnamve : jo date:...

! -2 "J i

Client: WESTON(DELRAN)SDG: 81956(3-1)

LOW CONCENTRATION WATERFOR INORGANIC ANALYSIS

ARI 00 I 20

Client: WESTON(DELRAN)SDG: 81956(5-1)

RESULTS

3 R I O O I 2

WESTON - DELRAN 030001COVER PAGE - INORGANIC ANALYSES DATA PACKAGE

b Name: SOUTHWEST_RESEARCH_INSTIT Contract: 01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.:81956_

SOW No.: ILM02.1

WESTON Sample No. Lab Sample IDRS1 81964RS1-D_______ _81964-D__"Wl_________ .81961___"W1-D________ _81961-D__~W2_________ _81962___"W2-D________ _81962-D__"W1S_________ _81961S__"W1SD________ _81961SD__"W2S_________ _81962S___"W2SD________ _81962SD__"WIS-D_______ _81961S-D_"WISD-D______ _81961SD-D"W2S-D_______ _81962S-Dj"W2SD-D______ _81962SD-D"WID_________ _81961D__'_"W2D_________ _81962D___"WID-D_______ _81961D-D_"W2D-D 81962D-D

Were ICF interelement corrections applied ? Yes/No NO

Were ICP background corrections applied ? Yes/No NO_If yes - were raw data generated beforeapplication of background corrections ? Yes/No

Comments:SAMPLES ENDING IN -D IDENTIFY THE DISSOLVED METALS ANALYSIS.

I certify that this data package is in compliance with the terms andconditions of the cent r act, both technically and for completeness, forother than the conditions detailed above. Release of the data containedin this hardcopy data package and in the computer-readable data submittedon floppy diskette has been authorized by the Laboratory Manager or theManager's designee, as verified by the following signature.

Signature : TYT frAXa. TaOU-X6l -fvvName : Jo

Date: Q-) ..3 l U _________ Title: &rou ?

COVER PAGE - IN ILM03.0

A R I O O I 2 2

WESTON - DELRAN C30002

1 WESTON SAMPLE NO,INORGANIC ANALYSES DATA SHEET

RS1Lab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956_

Matrix (soil/water): WATER Lab Sample ID: 81964

Level (low/med): LOW_ Date Received: 12/05/96

% Solids: _0.0

Concentration Units (ug/L or mg/kg dry weight): UG/L_

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Concentration

50.05.02.05.01.01.050.05.05.05.020.02.050.05.00.205.01003.05.050.02.05.05.0

C

UUUUUUUUUUUUUUUUUUUUUUU

Q M

ppFPPPPPPPPPPPcvppFPPFPP

Color Before: _______ Clarity Before: ____ Texture:

Color After: _______ Clarity After: ____ Artifacts:

Comments:TOTAL METALS ANALYSIS

FORM I - IN ILM03.0

A R I O O I 2 3

WESTON - DELRAN

1 WESTON SAMPLE NOINORGANIC ANALYSES DATA SHEET

RS1-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER Lab Sample ID: 81964-D


% Solids: _0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

50.05.02.05.01.01.050.05.05.05.020.02.050.05.00.205.01003.05.050.02.05.05.0

C

uuuuuuuuuuuuuuuuuuuuuuu

Q M

ppFppppppppFPPcvppFPPFPP

Color Before: _______ Clarity Before: _____ Texture:


Comments:DISSOLVED METALS ANALYSIS_______ _______

FORM I - IN ILM03.0

WESTON - DELRAN t)30004


WlLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956,



% Solids: _0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

1275.02.02221.01.0

116005.05.09.620.02.0477045.30.205.020103.05.029002.05.08.8

C

UU

UU

UUBUU

UU

UU

UUB

Q

w

M

PPPPPPPPPPPPPPcvPPPPPFPP



Comments:TOTAL METALS ANALYSIS ___________ _____________ ___

FORM I - IN ILM03.0

A R I 0 0 1 2 5

WESTON - DELRAN


Wl-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956^



% Solids: _0.0


CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

1375.02.02241.01.0

116005.05.011.020.02.0480045.60.205.020603.05.029402.05.010.6

C

UU

UU

UU

UU

UU

UU

UUB

Q M

FPFPPPPPPPPFPPCVPPFPPFPP



Comments:DISSOLVED METALS ANALYSIS _____

FORM I - IN ILM03.0

WESTON - DELRAN C3000G


Lab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427W2



Level (low/med): LOW___ Date Received: 12/05/96

% Solids: _0.0

Concentration Units (ug/L or ing/kg dry weight): UG/L_

CAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

1505.02.02191.01.0

116005.05.012.220.02.0473045.00.205.020703.05.029302.05.09.2

C

UU

UU

UU

UU

UU

UU

UUB

Q M

PPFPPPPPPPPFPPCVPPFPPFPP

Color Before: _______ Clarity Before: _____ Texture:



FORM I - IN ILM03.0

flRUJOI27

WESTON - DELRAN 030007


W2-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956



% Solids: _0.0

Concentration Units (ug/L or ing/kg dry weight) : UG/L_

GAS No.

7429-90-57440-36-07440-38-27440-39-37440-41-77440-43-97440-70-27440-47-37440-48-47440-50-87439-89-67439-92-17439-95-47439-96-57439-97-67440-02-07440-09-77782-49-27440-22-47440-23-57440-28-07440-62-27440-66-6

Analyte


Concentration

1305.02.02211.01.0

116005.05.011.320.02.0477045.10.205.020203.05.029202.05.010.3

C

UU

UU

UU

UU

UU

UU

UUB

Q M

PPFPPPPPPPPFPPCVPPFPPFPP



Comments:DISSOLVED METALS ANALYSIS _______

FORM I - IN ILM03.0

A R I O O I 2 8

WESTON - DELRAN

2AINITIAL AND CONTINUING CALIBRATION VERIFICATION

030008

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.: 81956

Initial Calibration Source: INORGVEN/SPE

Continuing Calibration Source: INORGVEN/SPE

Concentration Units: ug/L

Analyte

Aluminum_Antimony_ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadium_Zinc

Initial CalibrationTrue Found %R(1)

10000.05000.0

50.010000.01000.01000.020000.02000.05000.02000.010000.0

50.020000.01000.0

3.05000.020000.0

50.01000.020000.0

50.05000.01000.0

10078.415136.24

50.1010042.161057.071010.6420669.432025.545093.312027.7410679.45

50.0021139.681017.94

2.914932.8420350.30

49.201039.4620306.20

49.505017.681002.76

100.8102.7100.2100.4105.7101.1103.3101.3101.9101.4106.8100.0105.7101.897.098.7101.898.4103.9101.599.0100.4100.3

Continuing CalibrationTrue Found %R ( 1 ) Found %R ( 1 )

10000.05000.050.0

10000.01000.01000.020000.02000.05000.02000.010000.0

50.020000.01000.0

3.05000.020000.0

50.01000.020000.0

50.05000.01000.0

10078.255140.0846.80

10030.961053.971009.2420637.962020.525088.602029.3310676.27

49.5021105.201016.26

2.924932.4220374.60

48.501038.5420300.80

53.905012.28998.99

100.8102.893.6100.3105.4100.9103.2101.0101.8101.5106.899.0105.5101.697.398.6101.997.0103.9101.5107.8100.299.9

10094.695145.2148.80

10042.971053.861009.3120580.842020.375088.432033.2210668.79

48.6021090.791016.08

2.914935.9119989.80

48.201038.0620076.70

52.405016.67997.17

100.9102.997.6100.4105.4lOO.o102.'101.0101.8101.7106.797.2105.5101.697.098.799.996.4103.8100.4104.8100.399.7

P*

H

PPFPPPrPPPPPFPPCVPPFPPFPP

(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

FORM II (PART 1) - IN ILM03.

A R I O Q I 2 9

WESTON - DELRAN


C30009






Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Initial CalibrationTrue Found %R ( 1 )

————

Continuing CalibrationTrue Found %R(1) Found %R(1)

10000.05000.050.0

10000.01000.01000.020000.02000.05000.02000.010000.0

50.020000.01000.0

5000.020000.0

50.01000.020000.0

50.05000.01000.0

10078.695165.2949.10

9993.571059.431016.5920676.122025.695118.222033.5010695.55

49.0021128.601018.36

4966.6020146.50

49.201037.5620106.60

54.305017.421001.72

100.8103.398.299.9105.9101.7103.4101.3102.4101.7107.098.0105.6101.8

99.3100.798.4103.8100.5108.6100.3100.2

10085.575170.8648.20

10018.701062.221013.9320598.872017.595110.242043.5310651.23

49.6021044.841015.83

4953.6720270.10

49.001036.9620131.50

51.805005.98992.32

100.9103.496.4100.2106.2101.4103.0100.9102.2102.2106.599.2105.2101.6

99.1101.498.0103.7100.7103.6100.199.2

M

PPFPPPPPPPPFPPNRPPFPPFPP

(1) Control Limits: Mercury 80-120? Other Metals 90-110; Cyanide 85-115

FORM II (PART 1) - IN ILM03.0

A R I O O I 3 0

WESTON - DELRAN







Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_j __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Initial CalibrationTrue Found %R ( 1 )

————

Continuing CalibrationTrue Found %R ( 1 ) Found %R ( 1 )

10000.05000.0

10000.01000.01000.020000.02000.05000.02000.010000.0

20000.01000.0

5000.020000.0

1000.020000.0

5000.01000.0

10090.065174.79

10025.091064.491015.5720607.942019.005109.012042.1410669.44

2.1059.341016.09

4966.9320232.50

1036.2920211.70

5011.01995.59

100.9103.5

100.3106.4101.6103.0101.0102.2102.1106.7

105.3101.6

99.3101.2

103.6101.1

100.299.6

s

————

•f

H

FPNRPPPrPPPPPNRPPNRPPNRPPNRPP

(1) Control Limits: Mercury 80-120; Other Metals 90-110; Cyanide 85-115

FORM II (PART 1) - IN ILM03

f l R I O O I 3 l

WESTON - DELRAN

2B €30011CRDL STANDARD FOR AA AND ICP



AA CRDL Standard Source: SPEX_______

ICP CRDL Standard Source: SPEX______


Analyte


CRDL J

True

4.0

5.0

0.2

5.0

20.0

Standard fc

Found

3.70

4.30

0.32

5.30

18.50

>r AA

%R

92.5

86.0

160.0

106.0

92.5

True

8.0

2.02.0

20.020.020.0

20.0

40.0

20.0

20.040.0

CRDL StarInitialFound

8.00

2.001.83

18.8218.3917.73

19.19

37.66

19.46

18.0138.34

idard 1

%R

100.0

100.091.5

94.192.088.6

96.0

94.2

97.3

90.095.8

for ICPFinai

Found

8.37

2.041.78

18.9718.7618.12

19.27

38.36

19.53

18.1738.80

L%R

104.6

102.089.0

94.893.890.6

96.4

95.9

97.6

90.897.0

FORM II (PART 2) - IN ILM03.0

A R I O O I 3 2

WESTON - DELRAN

2B 030012LINEAR RANGE STANDARD



AA CRDL Standard Source: __________

ICP CRDL Standard Source: SFEX


Analyte


LRS £

True

Standard fc

Found

>r AA

%R True

2000005000.0100.0

10000.02000.02000.02000005000.05000.05000.0200000100.02000005000.0

10.05000.0200000100.01000.0200000100.05000.010000.0

LRS StazInitialFound

211204.295360.9896.10

9872.682068.941988.81

188447.004858.935041.775471.24

193849.0299.20

209932.004907.18

9.984977.02

216259.3099.50

1066.39212294.20

99.705023.779224.09

•

idard i

%R

105.6107.296.198.7103.499.494.297.2100.8109.496.999.2105.098.199.899.5108.199.5106.6106.199.7100.592.2

Eor ICPFinaJ

Found

210858.875381.6097.30

9832.122087.992006.44

188877.384866.505072.835482.73

194179.24101.80

210064.404913.02

5019.28217254.40

98.301064.94

213894.90100.305025.109224.51

L%R

105.4107.697.396.3104.4: .3X.497.3101.5109.797.1101.8105.098.3

100.4108.698.3106.5106.9100.3100.592.2

FORM II (PART 2) - IN ILM03

{\RIOQi33


3BLANKS



Preparation Blank Matrix (soil/water): HATER

Preparation Blank Concentration Units (ug/L or mg/kg): UG/L_

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

InitialCalib.Blank(ug/L) C

50.05.02.05.01.01.0

50.05.05.05.0

20.02.0

50.05.00.25.0

100.03.05.0

50.02.05.05.0


Continuing CalibrationBlank (ug/L)

1 C 2 C 3 C

50.05.02.05.01.01.0

50.05.05.05.0

20.02.0

50.05.00.25.0

100.03.05.0

50.02.05.05.0


50.05.02.05.01.01.0

50.05.05.05.0

20.02.0

50.05.00.25.0

100.03.05.0

50.02.05.05.0


50.05.02.05.01.01.0

50.05.05.05.0

20.02.0

50.05.0

5.0100.03.05.0

50.02.05.05.0

UUUUUUUUUUUUUU

UUUUUUUU

Prepa-rationBlank C

50.0005.0002.0005.0001.0001.00050.0005.0005.0005.00020.0002.00050.0005.0000.2005.000

100.0003.0005.00050.0002.0005.0005.000


M

ppFPPPPPPPPFPPCVPPFPPFPP

FORM III - IN ILM03.0

A R I O O I 3 U

WESTON - DELRAN

3 030014BLANKS



Preparation Blank Matrix (soil/water): HATER

Preparation Blank Concentration Units (ug/L or mg/kg): UG/L_

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel_j __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

InitialCalib.Blank(ug/L) C

—

Continuing CalibrationBlank (ug/L)

1 C 2 C 3 C

50.05.02.05.01.01.050.05.05.05.020.02.0-50.05.0

5.0100.03.05.0

50.02.05.05.0

UUUUUUUUUUUUUU

UUUUUUUU

50.05.0

5.01.01.050.05.05.05.020.0

50.05.0

5.0100.0

5.050.0

5.05.0

UU

UUUUUUUU

UU

UU

UU

UU

Prepa-ration ..Blank C

50.0005.0002.0005.0001.0001.00050.0005.0005.0005.00020.0002.00050.0005.0000.2005.000

100.0003.0005.00050.0002.0005.0005.000

UUUrUiUUUUUUUUUUUUUUUUUU

«

H

PPFPfPPPPPPPFPPCVPPFPPFPP

FORM III - IN ILM03

f l R I O O I 3 5

WESTON - DELRAN

ICP INTERFERENCE CHECK SAMPLE UJQ015

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract! 01-6421-427

Lab Code: SWRI_ Case No.: _____ SAS No: _____ SDG No.: 81956_

ICP ID Number: TJA TRACE__ ICS Source: INORGVEN___


TrueSol. Sol.

Analyte A AB

Aluminum_AntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

1000000

000

100000000

100000

1000000

0

0

00

1000000

0050

100000100200100

_100000

100000100

200

100

20080

Initial FoundSol. Sol.A AB %R

109704-2

-100

99774400

_96503

1071443

0

-1

1-10

102495.7-3.0

-1.6-0.149.3

98345.6102.1198.0101.1

_ 99381.2

105784.2101.6

196.8

99.1

200.883.7

102.5

98.698.3

102.199.0

101.1_99.4

105.8101.6

98.4

99.1————100.4104.6

Final FoundSol. Sol.A AB %R

109731-1

-100

99948300

_ 96582

1071873

1

-1

0-10

102421.5-2.0

-1.6-0.249.7

98506.6102.0198.8101.4

_ 99412.8

105757.8101.6

198.1

98.8

199.383.1

102.4

99.498.5

102.099.4

101.4_99.4

105.8101.6

99.0

98.8

99.6103.9

FORM IV - IN ILM03.0

f l R I O O I 3 6

WESTON - DELRAN {J30Q1G

5A WESTON SAMPLE NOSPIKE SAMPLE RECOVERY

HISLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427'


Matrix (soil/water): WATER_ Level (low/med): LOW_

% Solids for Sample: _0.0


Analyte


ControlLimit%R

75-12575-125

75-12575-12575-125

75-12575-12575-12575-125

75-125

75-125

75-125

75-12575-125

Spiked SampleResult (SSR)

591.460048.1600

417.030011.01009.7400

49.450097.150058.8900273.9600

95.7000

98.5600

50.5100

93.8100105.0200

CSample

Result (SR)

126.78005.0000

221.85001.00001.0000

5.00005.00009.650020.0000

45.2800

5.0000

5.0000

5.00008.8200

C

U

UU

UUBU

U

U

UB

SpikeAdded (SA)

500.0050.00

200.0010.0010.00

50.00100.0050.00250.00

50.00

100.00

50.00

100.00100.00

%R

92.996.3

97.6110.197.4

98.997.298.5109.6

100.8

98.6

101.0

93.896.2

Q

•~—

M

PPNRPPPNRPPs£PNRNRPNRPNRNRPNRNRPP


FORM V (Part 1) - IN ILM03.0

f l R I O O I 3 7



W1S-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427




Concentration Units (ug/L or rag/kg dry weight): UG/L_

Analyte


ControlLimit%R

75-12575-125

75-12575-12575-125

75-12575-12575-12575-125

75-125

75-125

75-125

75-12575-125


597.140049.2000

419.260010.84009.7900

49.350096.750059.3200276.3100

95.6200

96.4200

50.3500

93.7600106.1000

CSample

Result (SR)

126.78005.0000

221.65001.00001.0000

5.00005.00009.650020.0000

45.2800

5.0000

5.0000

5.00008.8200

C

u

uuuuBU

u

u

uB

SpikeAdded (SA)

500.0050.00

200.0010.0010.00

50.00100.0050.00250.00

50.00

100.00

50.00

100.00100.00

%R

94.198.4

98.7108.497.9

98.796,899.3

110.5

100.7

96.4

100.7

93.897.3

Q M

PPNRPPPNRPPPPNRNRPNRPNRNRPNRNRPP

Comments:DISSOLVED METALS ANALYSIS


A R I O O I 3 8



H1SDLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956_

Matrix (soil/water): WATER__ Level (low/med): LOW

% Solida for Sample: _0.0


Analyte


ControlLimit%R

75-12575-125

75-12575-12575-125

75-12575-12575-12575-125

75-125

75-125

75-125

75-12575-125


592.470048.3700

414.960010.95009.6800

49.060096.830059.2100269.6400

94.9600

96.5200

50.0600

93.6800104.3800

CSample

Result (SR)

126.78005.0000

221.85001.00001.0000

5.00005.00009.650020.0000

45.2800

5.0000

5.0000

5.00008.8200

C

U

UU

UUBU

U

U

UB

SpikeAdded (SA)

500.0050.00

200.0010.00

' 10.00

50.00100.0050.00250.00

50.00

100.00

50.00

100.00100.00

%R

93.196.7

96.6109.596.8

98.196.899.1

107.9

99.4

96.5

100.1

93.795.6

Q M

PPNRPPPNRPP>PNRNRPNRPNRNRPNRNRPP


FORM V (Part 1) - IN ILM03 0

f l R I O O I 3 9



W1SD-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427





Analyte


ControlLimit%R

75-12575-125

75-12575-12575-125

75-12575-12575-12575-125

75-125

75-125

75-125

75-12575-125


594.760048.0400

416.760010.87009.6600

48.860096.340059.6300270.5200

95.0400

96.2400

50.2600

93.3000105.3600

CSample

Result (SR)

126.78005.0000

221.85001.00001.0000

5.00005.00009.650020.0000

45.2800

5.0000

5.0000

5.00008.8200

C

U

UU

UUBU

U

U

UB

SpikeAdded (SA)

500.0050.00

200.0010.0010.00

50.00100.0050.00250.00

50.00

100.00

50.00

100.00100.00

%R

93.696.1

97.5108.796.6

97.796.3100.0108.2

99.5

96.2

100.5

93.396.5

Q M

PPNRPPPNRPPPPNRNRPNRPNRNRPNRNRPP



flRIOOUO



W2SLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421~427"





Analyte


ControlLimit%R

75-125

75-125

75-125

75-125

75-125


9.0000

25.4000

0.5000

50.9000

53.9000

C

B

SampleResult (SR)

2.0000

2.0000

0.2000

3.0000

2.0000

C

u

u

u

u

u

SpikeAdded (SA)

10.00

25.00

0.50

50.00

50.00

%R

90. a

101.6

100.0

101.8

107.8

Q

•-—

M

NRNRFNRNRNRNRNRTOrNRNRFNRNRCVNRNRFNRNRFNRNR



flRIOOUl


5A WESTON SAMPLE NO.SPIKE SAMPLE RECOVERY

W2S-DLab Name: SOUTHWEST_RESEARCHINSTIT Contract:01-6421-427


Matrix (soil/water): WATER_ Level (low/med): LOW



Analyte


ControlLimit%R

75-125

75-125

75-125

75-125

75-125


9.2000

26.0000

0.5600

49.7000

51.8000

C

B

SampleResult (SR)

2.0000

2.0000

0.2000

3.0000

2.0000

C

U

U

U

U

U

SpikeAdded (SA)

10.00

25.00

0.50

50.00

50.00

%R

92.0

104.0

112.0

99.4

103.6

Q M

NRNRFNRNRNRNRNRNRNRNRFNRNRCVNRNRFNRNRFNRNR



WESTON - DELRAN C 3 002 2


W2SDLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER_ - Level (low/med): LOW


Concentration Units (ug/L or rag/kg dry weight): UG/L_

Analyte


ControlLimit%R

75-125

75-125

75-125

75-125

75-125


10.0000

24.6000

0.4700

50.6000

52.8000

CSample

Result (SR)

2.0000

2.0000

0.2000

3.0000

2.0000

C

U

u

U

u

u

SpikeAdded (SA)

10.00

25.00

0.50

50.00

50.00

%R

100.0

98.4

94.0

101.2

105.6

Q

"1

M

NRNRFNRNRNRNRNRNR(NRNRFNRNRCVNRNRFNRNRFNRNR



A R I O O U 3



W2SD-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER_ Level (low/med): LOW



Analyte


ControlLimit%R

75-125

75-125

75-125

75-125

75-125


9.9000

26.2000

0.6200

51.0000

51.6000

C

B

SampleResult (SR)

2.0000

2.0000

0.2000

3.0000

2.0000

C

U

U

U

U

U

SpikeAdded (SA)

10.00

25.00

0.50

50.00

50.00

%R

99.0

104.8

124.0

102.0

103.2

Q M




ARIOOUl*


6 WESTON SAMPLE NO.DUPLICATES

WlDLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER Level (low/med): LOW_

% Solids for Sample: _0.0 % Solids for Duplicate: __0.0


Analyte


ControlLimit

100.0

10.0

__ 750. 0_

Sample ( S )

126.78005.0000

221.85001.00001.0000

11637.76005.00005.00009.650020.0000

4773.610045.2800

5.0000____ 2010.6000

5.00002897.1000

5.00008.8200

C

u

uuuuBU

u—u

uB

Duplicate (D)

130.64005.0000

219.33001.00001.0000

11572.63005.00005.00009.430020.0000

4733.600044.7900

5.00002060.1000

5.00002903.3000

5.000012.8100

C

U

UuuuBU

u—u

uB

RPD

3.0

1.1

0.6

2.3

0.81.1

__ 2.4_

0.2

36.9

Q

—

M

PPNRPPPPPPEPNRPPNRPPNRPPNRPP

FORM VI - IN ILM03.0

WESTON - DELRAN 0300 25


W1D-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER Level (low/med): _LOW_


Concentration Units {ug/L or mg/kg dry weight): UG/L_

Analyte


ControlLimit

100.0

10.0

10.0

750.0

Sample (S)

126.78005.0000

221.85001.00001.0000

11637.76005.00005.00009.650020.0000

4773.610045.2800

5.00002010.6000

5.00002897.1000

5.00008.8200

C

u

uuuuBU

u

u

uB

Duplicate (D)

139.28005.0000

221.74001.00001.0000

11629.92005.00005.000010.270020.0000

4787.260045.3000

5.00002074.9000

5.00002872.3000

5.00009.9200

C

U

uuuuu

u

u

uB

RPD

9.4

0.0

0.1

6.2

0.30.0

3.1

0.9

11.7

Q M

PPNRPPPPPPPPNRPPNRPPNRPPNRPP




Lab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427W2D


Matrix (soil/water): WATER Level (low/med): LOW



Analyte


ControlLimit Sample (S)

2.0000

2.0000

0.2000

3.0000

2.0000

C

U

u

U

u

u

Duplicate (D)

2.0000

2.0000

0.2000

3.0000

2.0000

C

u

B

U

u

u

RPD

200.0

Q M

NRNRFNRNRNRNRNR1Nir]NRFNRNRCVNRNRFNRNRFNRNR


flRIOQU?


6 WESTON SAMPLE MO.DUPLICATES

W2D-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER Level (low/med): LOW



Analyte


ControlLimit Sample (S)

2.0000

2.0000

0.2000

3.0000

2.0000

c

u

u

u

u

u

Duplicate (D)

2.0000

2.0000

0.2000

3.0000

2.0000

C

U

U

u

u

u

RPD Q M



flRIOOUB

WESTON - DELRAN030028

LABORATORY CONTROL SAMPLE

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract:Ol-6421-427


Solid LCS Source: __________

Aqueous LCS Source: SPEX_______

Analyte

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickel^ __PotassiumSeleniumSilverSodiumThalliumVanadiumZinc

Aqueous (ug/L)True Found %R

4000.01000.010.0

4000.0100.0100.0

20000.0400.01000.0500.02000.0

25.020000.01000.0

1.01000.020000.0

50.0100.0

20000.050.0

1000.01000.0

3947.531000.59

9.804032.84105.88101.16

20186.64398.791010.43500.782089.2023.50

20781.181001.79

1.01982.92

19403.4047.40102.87

19411.3047.20993.851010.66

98.7100.198.0100.8105.9101.2100.999.7101.0100.2104.594.0103.9100.2101.098.397.094.8102.997.194.499.4101.1

Solid (mg/kg)True Found C Limits %R

—

-

-

-

-

-

-

-

—

FORM VII - IN ILM03.0

HRIOOU9

WESTON - DELRAN

7LABORATORY CONTROL SAMPLE

Lab Name! SOUTHWEST_RESEARCH_INSTIT Contract:01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: _____ SDG No.: 81956,

Solid LCS Source: _________

Aqueous LCS Source: SPEX_______

Analyte


Aqueous (ug/L)True Found %R

4000.01000.010.0

4000.0100.0100.0

20000.0400.01000.0500.02000.025.0

20000.01000.0

1.01000.020000.0

50.0100.0

20000.050.0

1000.01000.0

3936.49997.129.30

4024.20105.32100.96

20113.19397.371005.80499.812072.6123.70

20725.07997.151.12

979.3219484.70

46.60102.56

19544.5042.30990.181003.33

98.499.793.0100.6105.3101.0100.699.3100.6100.0103.694.8103.699.7112.097.997.493.2102.697.784.699.0100.3

Solid (mg/kg)True Found C Limits %R

-

_

-

-

FORM VII - IN ILM03.0

f l R I O O I S O

WESTON - DELRAN C 300 30

8STANDARD ADDITION RESULTS


Lab Code: SWRI Case No.: ____ SAS No.: SDG No.:81956


WESTONSampleNo.

1An

10 ADDABS

11 ADD

CON ABS

r2 ADD

CON ABS

13 ADD

CON ABS

1FinalCone.

1r Q

-f

FORM VIII - IN ILM03.0

A R I G O I 5 I


9 WESTON SAMPLE NOICP SERIAL DILUTION

WlLLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER Level (low/med): LOW_


Analyte


Initial SampleResult (I)

126.785.00

221.851.001.00

11637.765.005.009.6520.00

4773.6145.28

5.00____ 2010.60 _

5.002897.10

5.008.82

C

U

UU

UUBU

—

U—

U

UB

SerialDilutionResult (S)

250.0025.00

218.005.005.00

11995.8525.0025.0025.00100.00

4861.3545.30

25.00____ 1490.00 _

25.002941.50

25.0025.00

C

UU

UU

UUUU

IUB

U

UU

%Differ-ence

100.0

1.7

3.1

100.0

1.80.0

_ 25. 9_

1.5

100.0

Q

—

—

M


FORM IX - IN ILM03.0

A R I O O I 5 2

WESTON - DELRAN 03003^

9 WESTON SAMPLE NOICP SERIAL DILUTION

W1L-DLab Name: SOUTHWEST RESEARCH INSTIT Contract:01-6421-427


Matrix (soil/water): WATER Level (low/mad): LOW_


Analyte


Initial SampleResult (I)

126.785.00

221.851.001.00

11637.765.005.009.6520.00

4773.6145.28

5.00____ 2010.60 _

5.002897.10

5.008.82

C

U

uuuuBU

u—u

uB

SerialDilutionResult (S)

250.0025.00

219.005.005.00

12013.1025.0025.0025.00100.00

4884.0045.65

25.00____ 2386.50 _

25.002953.00

25.0025.00

C

Uu

uuuuuu

B

UB

U

Uu

Differ-ence

100.0

1.3

3.2

100.0

2.30.8

_ 18. 7_

1.9

100.0

Q

_

M


FORM IX - IN

1 1 0 0 1 5 3

WESTON - DELRAN030033

10Instrument Detection Limits (Quarterly)



ICP ID Number: TJAJTRACE__ Date: 06/28/96

Flame AA ID Number : __________

Furnace AA ID Number :

Comments:

Analyte


Wave-length(nm)

396.80206.83

493.40313.04228.80317.93267.71228.61324.75259.94

279.07257.61

231.60766.40

328.06588.99

292.40213.85

Back-ground

CRDL(ug/L)

1005102011

5001010101003

500100.220750510500101020

IDL(ug/L)

50.05.0

5.01.01.0

50.05.05.05.0

20.0

50.05.0

5.0100.0

5.050.0

5.05.0

M


FORM X - IN ILM03.0

A R I O O I 5 1 +

WESTON - DELRAN

10Instrument Detection Limits (Quarterly) _•*


Lab Code: SWRI_ Case No.: ____ SAS No.: ____ SDG No.: 81956,

ICP ID Number: _________ Date: 06/28/96

Flame AA ID Number : _________

Furnace AA ID Number : PE Z5100

Comments:

Analyte


Wave-length(nm)

193.70

283.30

196.00

276.80

Back-ground

BZ

BZ

BZ

BZ

CRDL(ug/L)

1005102011

5001010101003

500100.220750510

500101020

IDL(ug/L)

2.0

2.0

3.0

2.0

M

NRNRFNRNRNRNRNRNRNRNRFNRNRNRNRNRFNRNRFNRNR

FORM X - IN ILM03.0

A R I O O I 5 5

WESTON - DELRAN

10Instrument Detection Limits (Quarterly)



ICP ID Number: __________ Date: 06/28/96

Flame AA ID Number : PE_4100ZL__

Furnace AA ID Number :

Comments:

Analyte


Wave-length(nm)

253.30

Back-ground

CRDL(ug/L)

1005102011

5001010101003

500100.220750510500101020

IDL(ug/L)

0.2

M

NRNRNRNRNRNRNRNRNRNRNRNRNRNRCVNRNRNRNRNRNRNRNR

FORM X - IN ILM03.0

Q R I O O I 5 6

WESTON - DELRA*11A

ICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)



ICP ID Number: TJA TRACE Date: 04/17/96

Analyte

Aluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSelenium_SilverSodiumThallium_Vanadium_Zinc

Wave-length(run)

396.80206.83193.69493.40313.04228.80317.93267.71228.61324.75259.94

279.07_257.61 _

231.60766.40196.02328.06588.99190.86292.40213.85

Ir

Al

0.00000000.00000000.00399200.00000000.00000000.00000000.00000000.0000000-0.00002800.00000000.0000000

0.0000000_0. 0000000

0.00000000.00000000.00012000.00000000.00000000.00010200.00000000.0000000

it ere lament C

Ca

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

0.0000000_0.0000000_

0.00000000.00000000.00010500.00000000.00000000.00010600.00000000.0000000

Correction 1

Fe

0.00000000.00000000.00000000.00000000.00000000.00025300.00000000.00003800.00002500.00000000.0000000

0.0002180-0.0000140

0.00000000.00000000.00010600.00000000.00000000.00011200.00000000.0000870

''actors for

Mg

0.00000000.00000000.00000000.00000000.00000000.00000000.00014900.00000000.00000000.00000000.0000000

0.0000000J). 0000380

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000650

••

CR_

-0.00013200.00871100.00121000.0000000-0.00002500.00000000.00041100.00012500.00000000.000 00o.ooc^^eo0.0000000

_0. 0000000

0.00000000.00000000.00010400.00000000.00006300.00011400.00007300.0000000

Comments:

FORM XI (Part 1) - IN ILM03.0

R R I O O I 5 7

WESTON - DELRAN 03001""

11BICP INTERELEMENT CORRECTION FACTORS (ANNUALLY)




Analyte

Aluminum_Antimony_Arsenic _BariumBerylliumCadmiumCalciumChromiumCobalt __Copper __Iron ____LeadMagnesiumManganeseMercuryNickel __PotassiumSelenium_Silver __SodiumThallium_Vanadium__Zinc

Wave-length(nm)

396.80206.83193.69493.40313.04228.80317.93267.71228.61324.75

_259.94 _

279.07_257.61 _

231.60766.40196.02328.06588.99190.86292.40213.85

II

CU_

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0000000

_0. 0000000

0.0000000_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0026530

iterelement (

MN_

0.00000000.00000000.00000000.00000000.00000000.00000000.00015400.00000000.00000000.0000000-0.0003880_

-0.0051890_0.0000000_

0.00000000.00000000.00000000.00006800.00000000.00000000.00030000.0000580

:orrection ]

NI_

0.0000000-0.00017100.00024900.00000000.00000000.00000000.00000000.00000000.00025900.0000000

_0. 0000000

0.0000000_0. 0000000

0.00000000.00000000.00000000.00000000.00000000.00000000.00000000.0033320

?actors for

TI_

0.00000000.00075200.0000000-0.00027500.00000000.00000000.00000000.00004900.0014380"0.0000810_0. 0000000

-0.0002350_0. 0000000

0.0000000~0. 00000000.0000000

""o. ooooooo"0.0000000"0. 0000000"0.0071490-0.0001980

••

V _

0.0000000-0.00837500.00399200.00004500.00000000.00000000.00019600.00026500.00000000.0000000

_0. 0000610

-0.0000870_0. 0000000

-0.00021500.00000000.00000000.00005400.00000000.00000000.00000000.0001140

Comments:

FORM XI (Part 2) - IN ILM03.0

f l R I O O I 5 8

WESTOH - DELRAK

12ICF LINEAR RANGES (QUARTERLY)

Lab Name: SOUTHWEST_RESEARCH_INSTIT Contract: 01-6421-427

Lab Code: SWRI_ Case No.: ____ SAS No.: ____ SDG No.: 81956


Comments:

Analyte


Integ.Time( sec . )

5.005.005.005.005.005.005.005.005.005.005.00

5.005.00

5.005.005.005.005.005.005.005.00

Concentration(ug/L)

600000.0100000.0100000.0100000.010000.050000.0600000.0100000.0100000.040000.0300000.0

625000.020000.0

100000.0500000.0100000.010000.0

1000000.0100000.0250000.050000.0

M

PPPPPPPPPPPNRPPNRPPPPPPPP

FORM XII - IN ILM03.0

A R I O O I 5 9

WESTON - DELRAN C 3 0 0 T P

13PREPARATION LOG


Lab Code: SWRI_ Case No.:______ SAS No.: _____ SDG No.:81956_

Method: P

WESTONSampleNo.

LCSWLCSW1PBWPBW1RS1RS1-DWlWl-DW1DW1D-DW1SW1S-DW1SDW1SD-DW2W2-DW2DW2D-DW2SW2S-DW2SDW2SD-D

PreparationDate

12/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/96

Weight(gram)

Volume<mL)

100100100100100100100100100100100100100100100100100100100100100100

FORM XIII - IN ILM03.0

AR'100160

WESTON - DELRAN

13PREPARATION LOG

030040

Lab Name: SOUTHHEST_RESEARCH_INSTIT Contract:01-6421-427

Lab Code: SHRI_ Case No.:_____ SAS No.: _____ SDG No.:81956

Method: F

WESTONSampleNo.

LCSWLCSW1PBWPBW1RS1RS1-DWlWl-DW1DW1D-DHISW1S-DW1SDH1SD-DW2H2-DW2DW2D-DW2SW2S-DW2SDW2SD-D

PreparationDate

12/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/9612/07/96

Height(gram)

Volume(mL)

100100100100100100100100100100100100100100100100100100100100100100

FORM XIII - IN ILH03.0

f l R I O O I G


13PREPARATION LOG


Lab Code: SWRI_ Case No.:______ SAS No.: _____ SDG No.:81956_

Method: CV

WESTONSampleNo.

LCSWLCSW1PBWPBW1RS1RS1-DWlWl-DW1DW1D-DHISW1S-DW1SDW1SD-DW2W2-DH2DW2D-DW2SW2S-DW2SDW2SD-D

PreparationDate

12/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/9612/17/96

Weight(gram)

Volume<mL)

10101010101010101010101010101010101010101010

FORM XIII - IN ILM03.0

f l R I O O I 6 2

WESTON - DELRAK

14ANALYSIS RUN LOG


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956

Instrument ID Number: TJA TRACE___ Method: P_

Start Date: 12/19/96 End Date: 12/19/96

WESTONSampleNo.

SOS4SIS5S2S3S6ICVICBCCVCCBCRILRSZZZZZZICSAICSABZZZZZZCCVCCBPBWPBH1LCSWLCSW1Wl-DW1D-DW1L-DW1S-DW1SD-DW2-DCCVCCBRS1-D

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.00

Time

11001102110411061108111011121114111811221127113111361140114411491153115812021206121112151219122412281233123712411246125012541259

% R

Analytes

AL

X

X

XXXX

X

XX

XXXXXXXXXXXXXXX

sB

XX

XXXXXX

XX

XXXXXXXXXXXXXXX

As

—

BA

X

X

XXXX

X

XX

XXXXXXXXXXXXXXX

BE

X

X

XXXXXX

XX

XXXXXXXXXXXXXXX

cD

X

X

XXXXXX

XX

XXXXXXXXXXXXXXX

cA

X

X

XXXX

X

XX

XXXXXXXXX

XXXX

cR

X

X

XXXXXX

XX

XXXXXXXXXXXXXXX

c0

X

X

XXXXXX

XX

XXXXXXXXXXXXXXX

cuX

X

XXXXXX

XX

XXXXXXXXXXXXXXX

FE

X

X

XXXX

X

XX

XXXXXXXXXXXXXXX

pB

_

HG

X

X

XXXX

X

XX

XXXXXXXXX

XXXX

NN

X

X

XXXXXX

XX

XXXXXXXXXXXXXXX

HG

—

NIX

X

XXXXXX

XX

XXXXXXXXXXXXXXX

K

—

—

sEAG

XX

XXXXXX

XX

XXXXXXXXXXXXXXX

NA

—

TL

—

V

X

X

XX

r*1XX

XX

XXXXXXXXXXXXXXX

zN

X

X

XXXXXX

XX

XXXXXXXXXXXXXXX

FORM XIV - IN

S R I O O I 6 3

WESTON - DELRAN

14 C30043ANALYSIS RUN LOG


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956_



WESTONSampleNo.

WlW1DW1LW1SW1SDW2RS1ccvCCBCRILRSZZZZZZICSAICSABZZZZZZCCVCCB

D/F

1.001.005.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

13031308131213161321132513291334133813431347135113561400140414091413

———

———

% R

Analytes

AL

XXXXXXXXX

X

XX

XX

sB

XXXXXXXXXXX

XX

XX

As

—

BA

XXXXXXXXX

X

XX

XX

BE

XXXXXXXXXXX

XX

XX

cD

XXXXXXXXXXX

XX

XX

cA

XXX

XXXX

X

XX

XX

cR

XXXXXXXXXXX

XX

XX

c0

XXXXXXXXXXX

XX

XX

cuXXXXXXXXXXX

XX

XX

FE

XXXXXXXXX

X

XX

XX

pB

—

HG

XXX

XXXX

X

XX

XX

MN

XXXXXXXXXXX

XX

XX

HG

—

NIXXXXXXXXXXX

XX

XX

K

—

sE

—

AG

XXXXXXXXXXX

XX

XX

NA

—

TL

—

—

V

XXXXXXXXXXX

XX

XX

zN

XXXXXXXXXXX

XX

XX

FORM XIV - IN ILM03

AR I 00 I 61*

WESTON - DELRANC3004414

ANALYSIS RUN LOG





WESTONSampleNo.

SOSIICVICBCCVCCBCRILRSzzzzzzICSAICSABZZZZZZFBWPBW1LCSWLCSW1CCVCCBWl-DW1D-DW1L-DW1S-DW1SD-DW2-DRS1-DWlW1DW1LCCVCCBW1SW1SD

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.005.001.001.001.001.001.001.005.001.001.001.001.00

Time

10341038104210461050105210541056105811021104110611081110111211161118112011221124112611301132113411361138114211441146114811501154

% R

Analytes

ALSBASBABECDCACRC0CUFEPBHGHNHGNIK

XXXXXX

X

XX

XXXXXXXXX

XXXXXX

SEAG

NA

XXXXXX

X

XX

XXXXXXXXX

XXXXXX

TL

_>

V

<_

zN

FORM XIV - IN

A R I O O I 6 5

WESTON - DELRAN14 03004'

ANALYSIS RUN LOG





WESTONSampleNo.

W2RS1ZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZZccvCCBW2W2-DCRILRSZZZZZZICSAICSABZZZZZZCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

11561158120012021204120812101212121412161222122612281232123412361238124012421246

———

% R

Analytes

ALSBASBA

BECDCACRC0CUFEPBMGHN

HGNIK

X

XXXX

X

XX

XX

SEAG

NA

X

XXXX

X

XX

XX

TLV Z

N

FORM XIV - IN ILM03

AR I 00 I 66

WESTON - DELRAN

14ANALYSIS RUN LOG

0-3 GO 45


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956,

Instrument ID Number: PE Z5100____ Method: F_


WESTONSampleNo.

SOS10S25S50S100ICVICBCRALRSPBWPBWALCSWLCSWAWlW1AW2W2ACCVCCBW2DW2DAW2SW2SAW2SDW2SDARS1RS1APBW1PBW1ACCVCCBLCSW1

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

12301234123912441248131313181322132713321336134113451350135513591404140814131417142214271431143614411445145014541459150415081513

% R

__ 95.3

92.3

__ 98.0

__ 97.3

96.7

__ 99.7

__ 93.3

94.7

__ 97.7

Analytes

ALSBAS

XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX

BABECDCACRC0CuFEPBMGMNHGNIK SEAGNATL

^

V

~s

zN

FORM XIV - IN ILM03

f l R I U O I 6 7

WESTON - DELRAN C 3 DO 47

14ANALYSIS RUN LOG



Inatrument ID Number: PE Z5100____ Method: F_


WESTONSampleNo.

LCSW1AWl-DWl-DAW2-DW2-DAW2D-DW2D-DAW2S-DW2S-DACCVCCBW2SD-DW2SD-DARS1-DRS1-DAZZZZZZLRSCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

1517152215261531153615401545154915541558160316071612161616211626163116361640

% R

94.7

95.0

95.7

__ 99.0

95.0

94.7

95.0

Analytes

ALSBAS

XXXXXXXXXXXXXXX

XXX

BABECDCACRC0CUFEPBMGHNHGNIK SEAGNATLV Z

N

FORM XIV - IN ILM03

100168

WESTON - DELRAN

14 C30043ANALYSIS RUN LOG





WESTONSampleNo.

SOS3S25S50S100ICVICBCRALRSPBWPBWALCSWLCSWAWlW1AW2W2ACCVCCBW2DW2DAW2SW2SAW2SDW2SDARS1RS1APBW1PBW1ACCVCCBLCSW1

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

18131818182218271832184618501855185919041909191319181922192719321937194119461950195520002004200920142018202320282032203720412046

% R

92.7

91.0

94.3

96.0

89.3

92.0

94.7

88.7

89.0

Analytes

ALSBASBABECDCACRC0CuFEPB

XXXXXXXXXXXXXXXXXXX

XXXXXXXXXXX

MGHN

HG

NIK SEAGNATL

-

V

_-"

zN

FORM XIV - IN

A R I O O I 6 9

WESTON - DELRAN

14ANALYSIS RUN LOG





WESTONSampleNo.

LCSW1AWl-DWl-DAW2-DW2-DAW2D-DW2D-DAW2S-DW2S-DACCVCCBW2SD-DW2SD-DARS1-DRS1-DAZZZZZZZZZZZZW2DW2DAZZZZZZLRSCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

20512056210021052109211421182123212821322137214121462151215522002204221322172222222722312236

% R

__ 87.7

93.7

96.0

96.0

92.3

90.0

87.7

89.7

Analytes

ALSBASBABECDCACRC0CUFEPB

XXXXXXXXXXXXXXX

XX

XXX

HGMNHG

NIK SEAG

NATLV ZN

FORM XIV - IN ILM03.C

ARI 00 I 70

WESTON - DELRAN 0 3 OO

14ANALYSIS RUN LOG





WESTONSampleNo.

SOS5S25S50S100ICVICBCRALRSPBWFBWALCSWLCSWAWlW1AW2W2ACCVCCBW2DW2DAW2SW2SAW2SDW2SDARS1RS1AFBW1FBW1ACCVCCBLCSW1

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

09360941094509500955100810131017102210261031103610411045105010541059110311081112111711221126113111361141114511501155115912041209

% R

106.0

105.7

_ 104.7

113.0

113.0

105.7

_ 108.0

106.0

_ 104.7

Analytes

ALSBASBABECDCACRC0CUFEPBHGHNHGNIK SE

XXXXXXXXXXXXX

XXXXXXXXXXXXXXXXX

AGNATL

_a-

V

ff

zN

FORM XIV - IN ILM03

ARioom

030051WESTON - DELRAN

14ANALYSIS RUN LOG


Lab Code: SWRI_ Case No.: _____ SAS No.; _____ SDG No.:81956_



WESTONSampleNo.

LCSW1AWl-DWl-DAW2-DW2-DAW2D-DW2D-DAW2S-DW2S-DACCVCCBW2SD-DW2SD-DARS1-DRS1-DAWlW1AWl-DWl-DAZZZZZZLRSCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

12131218122312271232123712411246125012551300130413091313131813291333133813431347135213571401

% R

_ 112.3

_ 103.0

_ 113.7

_ 115.0

_ 108.7

_ 111.3

_ 106.0

109.3

104.0

Analytes

ALSBASBABECDCACRC0CuFEPBHGNNHGNIK SE

X

XXXXXXXXXXXXXXXX

XXX

AGNATLV ZN

-

-

-

FORM XIV - IN ILM03.0

A R I O O I 7 2

WESTON - DELRAN 030'05

14ANALYSIS RUN LOG





WESTONSampleNo.

SOS10S25S50S100ICVICBCRALRSPBWPBWALCSWLCSWAWlW1AW2W2ACCVCCBW2DW2DAW2SW2SAW2SDW2SDARS1RS1APBH1PBW1ACCVCCBLCSW1

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

15101515152015241529154415481553155716021607161116161621162516301635164016441649165316581703170717121717172117261731173517401745

% R

_ 100.0

94.0

_ 119.7

_ 107.3

109.0

93.3

99.7

91.3

__ 95.7

Analytes

ALSBASBABECDCACRC0CUFEPBHGHN

HGNIK SEAGNATL

XXXXXXXXXt4

K]XXXXXXXXXXXXXXXXXXXXX

V

•**

zN

FORM XIV - IN

A R I O O I 7 3

WESTON - DELRAN 0300o3

14ANALYSIS RUN LOG





WESTONSampleNo.

LCSW1AWl-DWl-DAW2-DW2-DAW2D-DW2D-DAW2S-DW2S-DACCVCCBW2SD-DW2SD-DARS1-DRS1-DAZZZZZZLRSCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

1749175417581803180818121817182218261831183518401844184918531858190319071912

% R

_ 125.3

_ 113.7

_ 111.0

_ 107.3

__ 98.0

_ 108.3

98.7

Analytes

ALSBASBABECDCACRC0CUFEPBHGHNHGNIK SEAGNATL

XXXXXXXXXXXXXXX

XXX

V zN

-

FORM XIV - IN

f l R l O O I 7 » 4


14ANALYSIS RUN LOG

••**•


Lab Code: SWRI_ Case No.: _____ SAS No.: _____ SDG No.:81956,

Instrument ID Number: PE 4100ZL___ Method: CV


WESTONSampleNo.

SOSO. 5SIS2S5S10ICVICBCRAFBWLCSWW2W2DW2SW2SDRS1WlCCVCCBFBH1LCSW1W2-DW2D-DW2S-DW2SD-DRS1-DWl-DLRSZZZZZZCCVCCB

D/F

1.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.001.00

Time

2333233623392341234423472357235900050007001000130015001800210023002600290031003400370039004200450048005000530056005801010104

% R

Ana ly tea

ALSBASBABECDCACRCOCUFEPBHGMN

HG

XXXXXXXXXXXXXXXXXXXXXXXXXXXX

XX

NIK SEAGNATLV Z

N

FORM XIV - IN ILM03.

f l R I O O I 7 5

low concentration water for inorganic analysissignature : ^tyt^fraxa. taou-x6l -fvnamve : jo date:...

Documents