r

November 19 1990

Hs Anna Kruko Waste Man1gt111tnt Ohtston HSV bull CAM 5 US EPA Jfk federal Bldg Boston KA 02203

Our Ms Kruko

Enc l osed 1re coplu of various p1ects of tnforlli tton froM our files relati ng to tht tox ic waste clea nup t n Greene Rhode Island

The i nformation ls presented tn 2 groups A Ocun Spray Information

I The Greene Co pesticide reports 1986-1990 2 Protective Screen residue results 1987 1990 3 ERCO cranberry sample results 1981

B Governmental Agency report s in our files 1 Rhode Island Health Oeputment cranberry sample results 1981 2 FDA cranberry sample results 1980 3 EPA swu1p water samp le results 1980 4 Rhode Island Department of Health water sample results 1980

I had hoped to provide this package of information urller but due to a busy harvest season and Y travel schedule the process took longer than expected

If there are any questions about any of thh informati on please call me

j~~1U~ Jere 0 Downing i Agricultural Affairs

JOOhjc 0572

N Bryson C Collison J Crooks R Kepper J Ropes J Wilson

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OCEAN SPRAY CRANBERRIES INC QftOWIR RICORD Of NITlCIDI AND CHIIItCAL TREATMENT Of

CMNIIfllfiiY ACREAGE

- _ - G~tttiN~ aM VY

ltiiiTIWCnOtlll - _ ___________uot -_ ~- ~c_ ~- onea--

__ __ _ _ _CillO TIIIIATMlHT

c-eefMttN ArocllleO IAcbull auflt lelll1) middot-middot -middot shy -- middotshy

(j ~r_ Nj ~1() 761 i ~s H

S11viNbullI4 JlJ yen3-17 Gf ( umiddot S f bull

SuiNbullibull ~ 1 yen3 v7 lltih bull ( Sll

Di i N lll fl 7 r ( shbull 7bull7 sJ-shy

Cu middotr irJ N HO ~1 gtdn I bull ( ~middot sin ( 9 7Hlt4Dbull1llbull ~ ltD iff 7middot Jf ~middot- aAvo Sto i)f1 IDfnj ( ~ 7

s~ v~ Stltgt ilmiddotl7 ~Prs (f $5

8bull sa ritmiddotyen7 10h () yen0 t1o

OihutTitlll Slo JfvJJj ~ tf 7H

7 A S fJo~bull Jco 7bull~middotmiddotmiddot 1bull

a bullbullmiddot ~v

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N ~~ ~ middot ti ~ r1~ - ~ CJampS ~

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r

- ATtICKtN Al lilA Ofl-tel - PLYIIOUTH MAN 011011 Q1Q-~

CNIOIIOCEAN SPRAY CRANBERRIES INC 3 Greenll CaOanr

1-1 bull cabull lf IIITJCl All ClliUI TIITIIITDf Coventry Crnlerry cwbullbullYaciUil INITUCTtONI -bullbull_walllf- bull __MUCltfKfH kwtflll_

0 - llalleniHI _ __~ 1-ICal 011111 - lirwf

IMttt 111-1 bull ec- er- ~toc _ onto bullbullbull

middot- ~

_ --

19e7

_~ OCafIPfi Y c-- IIIMi lfOtlftUIIItd MtIOCI btllbitA AcrbullTrntM Dbull

c lroouetperAcrel

s

RO22 Sevin~ 2 ots

]()() Cueron 50 lbs 78 bull lO 18

JJO poundvital 40 lbs Ill

T~ - ~JlO Oavrino 60 lbl bullo 19

180 Lonen 3nts s J 80 ~ _ 09

R RO

713310 201 aratUon lll ots Al 80 818

Jl - 7middotmiddot eo 713~30 Dlollltltm All

1 Diauncn l qt s U l so 81

521 Koci~l 606 10 ct~ 10 5 8l)

260 Pyronon3 3 ozs All 80 8S

)7rL I -( CAll 7l~-82~

v f T320 ROU111) -+T6-tilutic~

450 Royal iH-30 l t l6 ~ilution 2 4567eu Sxlt-traa-tNn 720

ClltTI ANO WAIIIIIANTY 111 r~ 1zl) Jl

~~-w=middot ~IOWS j_) ) II bull ~~ flj bullmiddot JJ I)h~ 1 Tlolll~ ~~lt l lrulltiCICOIIMbull r-OltctOII llllllri iCIIlllonclu4o90ftMCIOCidn lu90CoctM MtOICOctM ~C I Ushy

nce--tofllllV- I COIIGnCIIOenYto9i lroll-llli~IMIO~OUirlfCIn_oflllllt cr011 1nCI

a Tlllllbullcrbulln-r1Mwii1CIIIIIIatGal-10 YOUirOM 1 croaIOIICibllloiV bull~bullbullnctllliiel ownonltroctcoonlllncbull Ml

t hCifCIQUorlrMnlloiOclbulln SpriYC~-nM Inc PCII OIcroalnOoualtiYCOntr011nclll~lt)lr0119W-Dyltl IOIOrll oiOriCIOltIIrld

M_menl

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ATlIOMENI AlIIIANII OPCI middot ~YIIIOUTH IIAII =~Will 0 70-lt76S

OCEAN SPRAY CRANBERRIES INC middot-middot----~~bmiddot~G~middot~middotaubull4bull~c~~~umiddot~bull1-IIICIIf PIITICial All CllliiiCAl TIUTIIT If _ ____~c~middotmiddot~middot~middot~t ~ middot~middot~b~middot~l~c~

CIAIIIIIT ACWII I ORR

INITUCTIONI -bull _ _ __ _ IGIMge 111bull wshyO_litt ___ _ _ llllaquottN ~ _ oc- _ er ~~~c= _ bullbullmiddot __ -- middotmiddotmiddotmiddotmiddot-middotmiddot_

_0cUIIIprty ChemiC __e lforMulltM bllibrtA Acrbull Truteo 01te

c- mciiiCIIAcIW) lectbullon

3 10 Dnr lnol SO l bs 0 I 3 4 u 9 47 41

330 Evlhl 80 l bs 0 7 0 4 l

e ron 50 lb 0 bull s s 1 33 I

22 1 s bull Qt A no i26

20 1 PHith l JNP 2 3 sbull 0 M lt

lBO 2p n 10

540 CH bo m 6

300

nn 1lt

20 1 gt~ltI on I Pt bull Al l eo ~~~

~middot bullbull dbull IL l o2il P1 RO t i~

Par thla n

52 1 20

2 1 Diu loon 2 a t 80 7oa ~ ( I

lO u Rn ~~~ - lmiddotmiddot 1-shy at e 720450

ATI AND WARIIIANTY

TO Ot_CfMMtMI IM ~ 0 ___

tnreoy cently tnabullbullrrbullMto you lt lollowt - ~ 1 Tltlllhii POrlenfll ll lruICOII111~ jiiCUIIUIIIC~ImiU I111CIIIcling tnMCIICid fllf19tC- IIOIC- C Ill

linteiMMit olletVHr i CIOPOIICIIII-Y DOIJIIIOIII WIIIC~ IIIIIII IOyOIIIIIfCIIII--ol lhl lt CIO Inlt

2 T~bullbullbullbullcbullbulln__ICIIIniiiCNI toyoulromrllrt cbulloo rornDHrolmybullbullbulleci~IIICibel-fgrownrnllncrcomoro~ncbullworn

tll ciUIIIIIIIIIII ol Ocn kbullll Cllll_l_ Inc DI09rllll ol CIOO IM OUihy ~IIIIOIIIICI IIIIIOIdl MIDIOtecl by ill IIINIIlt ol OotiCIOfl IM

hi-

OlltOWIIIt COitY bull iiINII

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r ~~~C-pe----ny----~-~~-Tb~~l~-~OCEAN SPRAY CRANBERRIES INC 1-1middot-IfrIT-111 ClU lCAI TltiTMUTIf _--COgtcolto_O_h_rYcCrc=bullbullb-y_

1989 -middot11middot- INITUCT10NI __ _-__II Mf IIIOIyshy

O_IIIII_bull__IIM ___ - 1ti-lltll bull oc- tyen Cf~f 1M _ middotmiddotshy_ _ __

OceM IPII Y CIIMiell bullbull1elfGrlftUIIM EallitiiA ACNITIM 0MI fOCIUCipetAcftllc

SOl b - 2 4 10JJO hltbulll 381 PrWrccp SO i b1 G 80 420-422 _22 1 uvln n~ bull qt s 80 62 1 2 7 amp

2 11 Dl ulnon 2qt s I- ll 80 ol1i 26 6

540 Cumiddotbbullmbulltc 61bs s 1- 11 80 617

201 t h l in E ~t s 80 718

581 Brno 720 7p t s I - l l 80 719 8 I 4$0 Rou I tti-3 ~ G I 4 5 6 ~I 1121

180 lortbu J pt s 1-11 80 8]

521 Chutp lkocl bull I I Opt s 1- 11 80 81 6

320 Robull ndup ~ 1-11 -i(f c IA-- RIbull20

340 rc edor middotmiddot~li VI 1-11 c 1 ~730

TOo- er IM C~DWAIUtANTY ~ o-~ l -lttoyC-1fIIIMIWitfl ntiOtOUbullIollowe

I Tllllllflll~llf-lti iNI IIICICOIIpiI CGr I riiCIIOCIIIIICIIOntiiI-ICIOMIunggtCltOtfleteOCidefMCIIolshy

ll-loi iiii_I CfOIIOIIC~IOflttO-Itllell to ~ou iiiYCf ollt-11 crovalld

I TIIIII I IICra_ wlliciiiMIMINIJ-IoyOU fOIIIIM 1tf1cr011_1lt11Mbellol111y -llowleclfi i M llelitoltfOWIIJII MnelCOMpiiiMewolh

tlllllfl- of0ciiiiSprly CfM-nM IIIC llfCIII-OICIOti OIIIIIIyCOIIIrOI IMIIIdlapllf~bI I IOIIdol0tltelortMd

~ AbtU-71 ~crL _Jw - G s

J poundiJ df r N I --a 1ci~ o ~-~

llly-ltltJI-IOtilllonnll- __ynOIIIdiiiiUOIIIIniCIOIIIMIHilllllllltllttiiCIIIdi011111_

All lA OfPICI bull YI UOW GIIIOWIIIICOPYmiddot HK

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Wlii

OCEAN SPRAY CRANBERRIES INC QftOWIR RICORD Of NITlCIDI AND CHIIItCAL TREATMENT Of

CMNIIfllfiiY ACREAGE

- _ - G~tttiN~ aM VY

ltiiiTIWCnOtlll - _ ___________uot -_ ~- ~c_ ~- onea--

__ __ _ _ _CillO TIIIIATMlHT

c-eefMttN ArocllleO IAcbull auflt lelll1) middot-middot -middot shy -- middotshy

(j ~r_ Nj ~1() 761 i ~s H

S11viNbullI4 JlJ yen3-17 Gf ( umiddot S f bull

SuiNbullibull ~ 1 yen3 v7 lltih bull ( Sll

Di i N lll fl 7 r ( shbull 7bull7 sJ-shy

Cu middotr irJ N HO ~1 gtdn I bull ( ~middot sin ( 9 7Hlt4Dbull1llbull ~ ltD iff 7middot Jf ~middot- aAvo Sto i)f1 IDfnj ( ~ 7

s~ v~ Stltgt ilmiddotl7 ~Prs (f $5

8bull sa ritmiddotyen7 10h () yen0 t1o

OihutTitlll Slo JfvJJj ~ tf 7H

7 A S fJo~bull Jco 7bull~middotmiddotmiddot 1bull

a bullbullmiddot ~v

j (J fu

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N ~~ ~ middot ti ~ r1~ - ~ CJampS ~

r~bullNbullN ~middotU ) ~~middotMltT11141 aot u7 ltgt Go H bullJ Z -Ucl bullbullV ~I flt r iZ~ (j rs ~jol(o JOlt $JI o - middotshy

r

- ATtICKtN Al lilA Ofl-tel - PLYIIOUTH MAN 011011 Q1Q-~

CNIOIIOCEAN SPRAY CRANBERRIES INC 3 Greenll CaOanr

1-1 bull cabull lf IIITJCl All ClliUI TIITIIITDf Coventry Crnlerry cwbullbullYaciUil INITUCTtONI -bullbull_walllf- bull __MUCltfKfH kwtflll_

0 - llalleniHI _ __~ 1-ICal 011111 - lirwf

IMttt 111-1 bull ec- er- ~toc _ onto bullbullbull

middot- ~

_ --

19e7

_~ OCafIPfi Y c-- IIIMi lfOtlftUIIItd MtIOCI btllbitA AcrbullTrntM Dbull

c lroouetperAcrel

s

RO22 Sevin~ 2 ots

]()() Cueron 50 lbs 78 bull lO 18

JJO poundvital 40 lbs Ill

T~ - ~JlO Oavrino 60 lbl bullo 19

180 Lonen 3nts s J 80 ~ _ 09

R RO

713310 201 aratUon lll ots Al 80 818

Jl - 7middotmiddot eo 713~30 Dlollltltm All

1 Diauncn l qt s U l so 81

521 Koci~l 606 10 ct~ 10 5 8l)

260 Pyronon3 3 ozs All 80 8S

)7rL I -( CAll 7l~-82~

v f T320 ROU111) -+T6-tilutic~

450 Royal iH-30 l t l6 ~ilution 2 4567eu Sxlt-traa-tNn 720

ClltTI ANO WAIIIIIANTY 111 r~ 1zl) Jl

~~-w=middot ~IOWS j_) ) II bull ~~ flj bullmiddot JJ I)h~ 1 Tlolll~ ~~lt l lrulltiCICOIIMbull r-OltctOII llllllri iCIIlllonclu4o90ftMCIOCidn lu90CoctM MtOICOctM ~C I Ushy

nce--tofllllV- I COIIGnCIIOenYto9i lroll-llli~IMIO~OUirlfCIn_oflllllt cr011 1nCI

a Tlllllbullcrbulln-r1Mwii1CIIIIIIatGal-10 YOUirOM 1 croaIOIICibllloiV bull~bullbullnctllliiel ownonltroctcoonlllncbull Ml

t hCifCIQUorlrMnlloiOclbulln SpriYC~-nM Inc PCII OIcroalnOoualtiYCOntr011nclll~lt)lr0119W-Dyltl IOIOrll oiOriCIOltIIrld

M_menl

r --

ATlIOMENI AlIIIANII OPCI middot ~YIIIOUTH IIAII =~Will 0 70-lt76S

OCEAN SPRAY CRANBERRIES INC middot-middot----~~bmiddot~G~middot~middotaubull4bull~c~~~umiddot~bull1-IIICIIf PIITICial All CllliiiCAl TIUTIIT If _ ____~c~middotmiddot~middot~middot~t ~ middot~middot~b~middot~l~c~

CIAIIIIIT ACWII I ORR

INITUCTIONI -bull _ _ __ _ IGIMge 111bull wshyO_litt ___ _ _ llllaquottN ~ _ oc- _ er ~~~c= _ bullbullmiddot __ -- middotmiddotmiddotmiddotmiddot-middotmiddot_

_0cUIIIprty ChemiC __e lforMulltM bllibrtA Acrbull Truteo 01te

c- mciiiCIIAcIW) lectbullon

3 10 Dnr lnol SO l bs 0 I 3 4 u 9 47 41

330 Evlhl 80 l bs 0 7 0 4 l

e ron 50 lb 0 bull s s 1 33 I

22 1 s bull Qt A no i26

20 1 PHith l JNP 2 3 sbull 0 M lt

lBO 2p n 10

540 CH bo m 6

300

nn 1lt

20 1 gt~ltI on I Pt bull Al l eo ~~~

~middot bullbull dbull IL l o2il P1 RO t i~

Par thla n

52 1 20

2 1 Diu loon 2 a t 80 7oa ~ ( I

lO u Rn ~~~ - lmiddotmiddot 1-shy at e 720450

ATI AND WARIIIANTY

TO Ot_CfMMtMI IM ~ 0 ___

tnreoy cently tnabullbullrrbullMto you lt lollowt - ~ 1 Tltlllhii POrlenfll ll lruICOII111~ jiiCUIIUIIIC~ImiU I111CIIIcling tnMCIICid fllf19tC- IIOIC- C Ill

linteiMMit olletVHr i CIOPOIICIIII-Y DOIJIIIOIII WIIIC~ IIIIIII IOyOIIIIIfCIIII--ol lhl lt CIO Inlt

2 T~bullbullbullbullcbullbulln__ICIIIniiiCNI toyoulromrllrt cbulloo rornDHrolmybullbullbulleci~IIICibel-fgrownrnllncrcomoro~ncbullworn

tll ciUIIIIIIIIIII ol Ocn kbullll Cllll_l_ Inc DI09rllll ol CIOO IM OUihy ~IIIIOIIIICI IIIIIOIdl MIDIOtecl by ill IIINIIlt ol OotiCIOfl IM

hi-

OlltOWIIIt COitY bull iiINII

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1989 -middot11middot- INITUCT10NI __ _-__II Mf IIIOIyshy

O_IIIII_bull__IIM ___ - 1ti-lltll bull oc- tyen Cf~f 1M _ middotmiddotshy_ _ __

OceM IPII Y CIIMiell bullbull1elfGrlftUIIM EallitiiA ACNITIM 0MI fOCIUCipetAcftllc

SOl b - 2 4 10JJO hltbulll 381 PrWrccp SO i b1 G 80 420-422 _22 1 uvln n~ bull qt s 80 62 1 2 7 amp

2 11 Dl ulnon 2qt s I- ll 80 ol1i 26 6

540 Cumiddotbbullmbulltc 61bs s 1- 11 80 617

201 t h l in E ~t s 80 718

581 Brno 720 7p t s I - l l 80 719 8 I 4$0 Rou I tti-3 ~ G I 4 5 6 ~I 1121

180 lortbu J pt s 1-11 80 8]

521 Chutp lkocl bull I I Opt s 1- 11 80 81 6

320 Robull ndup ~ 1-11 -i(f c IA-- RIbull20

340 rc edor middotmiddot~li VI 1-11 c 1 ~730

TOo- er IM C~DWAIUtANTY ~ o-~ l -lttoyC-1fIIIMIWitfl ntiOtOUbullIollowe

I Tllllllflll~llf-lti iNI IIICICOIIpiI CGr I riiCIIOCIIIIICIIOntiiI-ICIOMIunggtCltOtfleteOCidefMCIIolshy

ll-loi iiii_I CfOIIOIIC~IOflttO-Itllell to ~ou iiiYCf ollt-11 crovalld

I TIIIII I IICra_ wlliciiiMIMINIJ-IoyOU fOIIIIM 1tf1cr011_1lt11Mbellol111y -llowleclfi i M llelitoltfOWIIJII MnelCOMpiiiMewolh

tlllllfl- of0ciiiiSprly CfM-nM IIIC llfCIII-OICIOti OIIIIIIyCOIIIrOI IMIIIdlapllf~bI I IOIIdol0tltelortMd

~ AbtU-71 ~crL _Jw - G s

J poundiJ df r N I --a 1ci~ o ~-~

llly-ltltJI-IOtilllonnll- __ynOIIIdiiiiUOIIIIniCIOIIIMIHilllllllltllttiiCIIIdi011111_

All lA OfPICI bull YI UOW GIIIOWIIIICOPYmiddot HK

r

- ATtICKtN Al lilA Ofl-tel - PLYIIOUTH MAN 011011 Q1Q-~

CNIOIIOCEAN SPRAY CRANBERRIES INC 3 Greenll CaOanr

1-1 bull cabull lf IIITJCl All ClliUI TIITIIITDf Coventry Crnlerry cwbullbullYaciUil INITUCTtONI -bullbull_walllf- bull __MUCltfKfH kwtflll_

0 - llalleniHI _ __~ 1-ICal 011111 - lirwf

IMttt 111-1 bull ec- er- ~toc _ onto bullbullbull

middot- ~

_ --

19e7

_~ OCafIPfi Y c-- IIIMi lfOtlftUIIItd MtIOCI btllbitA AcrbullTrntM Dbull

c lroouetperAcrel

s

RO22 Sevin~ 2 ots

]()() Cueron 50 lbs 78 bull lO 18

JJO poundvital 40 lbs Ill

T~ - ~JlO Oavrino 60 lbl bullo 19

180 Lonen 3nts s J 80 ~ _ 09

R RO

713310 201 aratUon lll ots Al 80 818

Jl - 7middotmiddot eo 713~30 Dlollltltm All

1 Diauncn l qt s U l so 81

521 Koci~l 606 10 ct~ 10 5 8l)

260 Pyronon3 3 ozs All 80 8S

)7rL I -( CAll 7l~-82~

v f T320 ROU111) -+T6-tilutic~

450 Royal iH-30 l t l6 ~ilution 2 4567eu Sxlt-traa-tNn 720

ClltTI ANO WAIIIIIANTY 111 r~ 1zl) Jl

~~-w=middot ~IOWS j_) ) II bull ~~ flj bullmiddot JJ I)h~ 1 Tlolll~ ~~lt l lrulltiCICOIIMbull r-OltctOII llllllri iCIIlllonclu4o90ftMCIOCidn lu90CoctM MtOICOctM ~C I Ushy

nce--tofllllV- I COIIGnCIIOenYto9i lroll-llli~IMIO~OUirlfCIn_oflllllt cr011 1nCI

a Tlllllbullcrbulln-r1Mwii1CIIIIIIatGal-10 YOUirOM 1 croaIOIICibllloiV bull~bullbullnctllliiel ownonltroctcoonlllncbull Ml

t hCifCIQUorlrMnlloiOclbulln SpriYC~-nM Inc PCII OIcroalnOoualtiYCOntr011nclll~lt)lr0119W-Dyltl IOIOrll oiOriCIOltIIrld

M_menl

r --

ATlIOMENI AlIIIANII OPCI middot ~YIIIOUTH IIAII =~Will 0 70-lt76S

OCEAN SPRAY CRANBERRIES INC middot-middot----~~bmiddot~G~middot~middotaubull4bull~c~~~umiddot~bull1-IIICIIf PIITICial All CllliiiCAl TIUTIIT If _ ____~c~middotmiddot~middot~middot~t ~ middot~middot~b~middot~l~c~

CIAIIIIIT ACWII I ORR

INITUCTIONI -bull _ _ __ _ IGIMge 111bull wshyO_litt ___ _ _ llllaquottN ~ _ oc- _ er ~~~c= _ bullbullmiddot __ -- middotmiddotmiddotmiddotmiddot-middotmiddot_

_0cUIIIprty ChemiC __e lforMulltM bllibrtA Acrbull Truteo 01te

c- mciiiCIIAcIW) lectbullon

3 10 Dnr lnol SO l bs 0 I 3 4 u 9 47 41

330 Evlhl 80 l bs 0 7 0 4 l

e ron 50 lb 0 bull s s 1 33 I

22 1 s bull Qt A no i26

20 1 PHith l JNP 2 3 sbull 0 M lt

lBO 2p n 10

540 CH bo m 6

300

nn 1lt

20 1 gt~ltI on I Pt bull Al l eo ~~~

~middot bullbull dbull IL l o2il P1 RO t i~

Par thla n

52 1 20

2 1 Diu loon 2 a t 80 7oa ~ ( I

lO u Rn ~~~ - lmiddotmiddot 1-shy at e 720450

ATI AND WARIIIANTY

TO Ot_CfMMtMI IM ~ 0 ___

tnreoy cently tnabullbullrrbullMto you lt lollowt - ~ 1 Tltlllhii POrlenfll ll lruICOII111~ jiiCUIIUIIIC~ImiU I111CIIIcling tnMCIICid fllf19tC- IIOIC- C Ill

linteiMMit olletVHr i CIOPOIICIIII-Y DOIJIIIOIII WIIIC~ IIIIIII IOyOIIIIIfCIIII--ol lhl lt CIO Inlt

2 T~bullbullbullbullcbullbulln__ICIIIniiiCNI toyoulromrllrt cbulloo rornDHrolmybullbullbulleci~IIICibel-fgrownrnllncrcomoro~ncbullworn

tll ciUIIIIIIIIIII ol Ocn kbullll Cllll_l_ Inc DI09rllll ol CIOO IM OUihy ~IIIIOIIIICI IIIIIOIdl MIDIOtecl by ill IIINIIlt ol OotiCIOfl IM

hi-

OlltOWIIIt COitY bull iiINII

- r -

AT110t~ Al

r ~~~C-pe----ny----~-~~-Tb~~l~-~OCEAN SPRAY CRANBERRIES INC 1-1middot-IfrIT-111 ClU lCAI TltiTMUTIf _--COgtcolto_O_h_rYcCrc=bullbullb-y_

1989 -middot11middot- INITUCT10NI __ _-__II Mf IIIOIyshy

O_IIIII_bull__IIM ___ - 1ti-lltll bull oc- tyen Cf~f 1M _ middotmiddotshy_ _ __

OceM IPII Y CIIMiell bullbull1elfGrlftUIIM EallitiiA ACNITIM 0MI fOCIUCipetAcftllc

SOl b - 2 4 10JJO hltbulll 381 PrWrccp SO i b1 G 80 420-422 _22 1 uvln n~ bull qt s 80 62 1 2 7 amp

2 11 Dl ulnon 2qt s I- ll 80 ol1i 26 6

540 Cumiddotbbullmbulltc 61bs s 1- 11 80 617

201 t h l in E ~t s 80 718

581 Brno 720 7p t s I - l l 80 719 8 I 4$0 Rou I tti-3 ~ G I 4 5 6 ~I 1121

180 lortbu J pt s 1-11 80 8]

521 Chutp lkocl bull I I Opt s 1- 11 80 81 6

320 Robull ndup ~ 1-11 -i(f c IA-- RIbull20

340 rc edor middotmiddot~li VI 1-11 c 1 ~730

TOo- er IM C~DWAIUtANTY ~ o-~ l -lttoyC-1fIIIMIWitfl ntiOtOUbullIollowe

I Tllllllflll~llf-lti iNI IIICICOIIpiI CGr I riiCIIOCIIIIICIIOntiiI-ICIOMIunggtCltOtfleteOCidefMCIIolshy

ll-loi iiii_I CfOIIOIIC~IOflttO-Itllell to ~ou iiiYCf ollt-11 crovalld

I TIIIII I IICra_ wlliciiiMIMINIJ-IoyOU fOIIIIM 1tf1cr011_1lt11Mbellol111y -llowleclfi i M llelitoltfOWIIJII MnelCOMpiiiMewolh

tlllllfl- of0ciiiiSprly CfM-nM IIIC llfCIII-OICIOti OIIIIIIyCOIIIrOI IMIIIdlapllf~bI I IOIIdol0tltelortMd

~ AbtU-71 ~crL _Jw - G s

J poundiJ df r N I --a 1ci~ o ~-~

llly-ltltJI-IOtilllonnll- __ynOIIIdiiiiUOIIIIniCIOIIIMIHilllllllltllttiiCIIIdi011111_

All lA OfPICI bull YI UOW GIIIOWIIIICOPYmiddot HK

r --

ATlIOMENI AlIIIANII OPCI middot ~YIIIOUTH IIAII =~Will 0 70-lt76S

OCEAN SPRAY CRANBERRIES INC middot-middot----~~bmiddot~G~middot~middotaubull4bull~c~~~umiddot~bull1-IIICIIf PIITICial All CllliiiCAl TIUTIIT If _ ____~c~middotmiddot~middot~middot~t ~ middot~middot~b~middot~l~c~

CIAIIIIIT ACWII I ORR

INITUCTIONI -bull _ _ __ _ IGIMge 111bull wshyO_litt ___ _ _ llllaquottN ~ _ oc- _ er ~~~c= _ bullbullmiddot __ -- middotmiddotmiddotmiddotmiddot-middotmiddot_

_0cUIIIprty ChemiC __e lforMulltM bllibrtA Acrbull Truteo 01te

c- mciiiCIIAcIW) lectbullon

3 10 Dnr lnol SO l bs 0 I 3 4 u 9 47 41

330 Evlhl 80 l bs 0 7 0 4 l

e ron 50 lb 0 bull s s 1 33 I

22 1 s bull Qt A no i26

20 1 PHith l JNP 2 3 sbull 0 M lt

lBO 2p n 10

540 CH bo m 6

300

nn 1lt

20 1 gt~ltI on I Pt bull Al l eo ~~~

~middot bullbull dbull IL l o2il P1 RO t i~

Par thla n

52 1 20

2 1 Diu loon 2 a t 80 7oa ~ ( I

lO u Rn ~~~ - lmiddotmiddot 1-shy at e 720450

ATI AND WARIIIANTY

TO Ot_CfMMtMI IM ~ 0 ___

tnreoy cently tnabullbullrrbullMto you lt lollowt - ~ 1 Tltlllhii POrlenfll ll lruICOII111~ jiiCUIIUIIIC~ImiU I111CIIIcling tnMCIICid fllf19tC- IIOIC- C Ill

linteiMMit olletVHr i CIOPOIICIIII-Y DOIJIIIOIII WIIIC~ IIIIIII IOyOIIIIIfCIIII--ol lhl lt CIO Inlt

2 T~bullbullbullbullcbullbulln__ICIIIniiiCNI toyoulromrllrt cbulloo rornDHrolmybullbullbulleci~IIICibel-fgrownrnllncrcomoro~ncbullworn

tll ciUIIIIIIIIIII ol Ocn kbullll Cllll_l_ Inc DI09rllll ol CIOO IM OUihy ~IIIIOIIIICI IIIIIOIdl MIDIOtecl by ill IIINIIlt ol OotiCIOfl IM

hi-

OlltOWIIIt COitY bull iiINII

- r -

AT110t~ Al

r ~~~C-pe----ny----~-~~-Tb~~l~-~OCEAN SPRAY CRANBERRIES INC 1-1middot-IfrIT-111 ClU lCAI TltiTMUTIf _--COgtcolto_O_h_rYcCrc=bullbullb-y_

1989 -middot11middot- INITUCT10NI __ _-__II Mf IIIOIyshy

O_IIIII_bull__IIM ___ - 1ti-lltll bull oc- tyen Cf~f 1M _ middotmiddotshy_ _ __

OceM IPII Y CIIMiell bullbull1elfGrlftUIIM EallitiiA ACNITIM 0MI fOCIUCipetAcftllc

SOl b - 2 4 10JJO hltbulll 381 PrWrccp SO i b1 G 80 420-422 _22 1 uvln n~ bull qt s 80 62 1 2 7 amp

2 11 Dl ulnon 2qt s I- ll 80 ol1i 26 6

540 Cumiddotbbullmbulltc 61bs s 1- 11 80 617

201 t h l in E ~t s 80 718

581 Brno 720 7p t s I - l l 80 719 8 I 4$0 Rou I tti-3 ~ G I 4 5 6 ~I 1121

180 lortbu J pt s 1-11 80 8]

521 Chutp lkocl bull I I Opt s 1- 11 80 81 6

320 Robull ndup ~ 1-11 -i(f c IA-- RIbull20

340 rc edor middotmiddot~li VI 1-11 c 1 ~730

TOo- er IM C~DWAIUtANTY ~ o-~ l -lttoyC-1fIIIMIWitfl ntiOtOUbullIollowe

I Tllllllflll~llf-lti iNI IIICICOIIpiI CGr I riiCIIOCIIIIICIIOntiiI-ICIOMIunggtCltOtfleteOCidefMCIIolshy

ll-loi iiii_I CfOIIOIIC~IOflttO-Itllell to ~ou iiiYCf ollt-11 crovalld

I TIIIII I IICra_ wlliciiiMIMINIJ-IoyOU fOIIIIM 1tf1cr011_1lt11Mbellol111y -llowleclfi i M llelitoltfOWIIJII MnelCOMpiiiMewolh

tlllllfl- of0ciiiiSprly CfM-nM IIIC llfCIII-OICIOti OIIIIIIyCOIIIrOI IMIIIdlapllf~bI I IOIIdol0tltelortMd

~ AbtU-71 ~crL _Jw - G s

J poundiJ df r N I --a 1ci~ o ~-~

llly-ltltJI-IOtilllonnll- __ynOIIIdiiiiUOIIIIniCIOIIIMIHilllllllltllttiiCIIIdi011111_

All lA OfPICI bull YI UOW GIIIOWIIIICOPYmiddot HK

- r -

AT110t~ Al

r ~~~C-pe----ny----~-~~-Tb~~l~-~OCEAN SPRAY CRANBERRIES INC 1-1middot-IfrIT-111 ClU lCAI TltiTMUTIf _--COgtcolto_O_h_rYcCrc=bullbullb-y_

1989 -middot11middot- INITUCT10NI __ _-__II Mf IIIOIyshy

O_IIIII_bull__IIM ___ - 1ti-lltll bull oc- tyen Cf~f 1M _ middotmiddotshy_ _ __

OceM IPII Y CIIMiell bullbull1elfGrlftUIIM EallitiiA ACNITIM 0MI fOCIUCipetAcftllc

SOl b - 2 4 10JJO hltbulll 381 PrWrccp SO i b1 G 80 420-422 _22 1 uvln n~ bull qt s 80 62 1 2 7 amp

2 11 Dl ulnon 2qt s I- ll 80 ol1i 26 6

540 Cumiddotbbullmbulltc 61bs s 1- 11 80 617

201 t h l in E ~t s 80 718

581 Brno 720 7p t s I - l l 80 719 8 I 4$0 Rou I tti-3 ~ G I 4 5 6 ~I 1121

180 lortbu J pt s 1-11 80 8]

521 Chutp lkocl bull I I Opt s 1- 11 80 81 6

320 Robull ndup ~ 1-11 -i(f c IA-- RIbull20

340 rc edor middotmiddot~li VI 1-11 c 1 ~730

TOo- er IM C~DWAIUtANTY ~ o-~ l -lttoyC-1fIIIMIWitfl ntiOtOUbullIollowe

I Tllllllflll~llf-lti iNI IIICICOIIpiI CGr I riiCIIOCIIIIICIIOntiiI-ICIOMIunggtCltOtfleteOCidefMCIIolshy

ll-loi iiii_I CfOIIOIIC~IOflttO-Itllell to ~ou iiiYCf ollt-11 crovalld

I TIIIII I IICra_ wlliciiiMIMINIJ-IoyOU fOIIIIM 1tf1cr011_1lt11Mbellol111y -llowleclfi i M llelitoltfOWIIJII MnelCOMpiiiMewolh

tlllllfl- of0ciiiiSprly CfM-nM IIIC llfCIII-OICIOti OIIIIIIyCOIIIrOI IMIIIdlapllf~bI I IOIIdol0tltelortMd

~ AbtU-71 ~crL _Jw - G s

J poundiJ df r N I --a 1ci~ o ~-~

llly-ltltJI-IOtilllonnll- __ynOIIIdiiiiUOIIIIniCIOIIIMIHilllllllltllttiiCIIIdi011111_

All lA OfPICI bull YI UOW GIIIOWIIIICOPYmiddot HK

I r I

ATlJOMfNI A 1bull

OCEAIII SPRAY CRANBERRIES INC ~~~--___ou--~1$____ Grower Pesticide Use Report

ITIIUCnONI lecOId H1ow all lrHitneflll Wilt ~ICidM to DfOCIUCgtfl9 ertiV for CfOf v- 0o IIOt hi letlilllort 11NM UM - ~ne per

eMiftlnl forward CWJOI11 t nd firM copy (bolfl ~liM~ 11 Ocur~ Spray NAME---------shyeranom 1nc Mtott ap~emOlaquo 101n

bpol11bhltlblt A lectlona l~ I FoHh EbullhlbltA StellonoilbullAir SbullSprlnklet

GbullOrouncl WbullWipe A 3 _middotshy tt (forfWiawlfAcl Mti+IM

ACfIITrltlttl liD 1--dmiddotmiddot J~o~ s I~J 7~

trRI a-bullbull tt$ s A~ A1c 55 1101

5o CJ da 5 AIbullASilfA 71-7 8J ~

~

1- P

s s

illmiddot A

~ IbullA

~~~

~ Q

sJ9 bullII

6J5 Chn~Y

0 13 s Ill s~ 1JL

w o ~ ~ s Atmiddotil 111 3b AM~ b~luiC yen w AIbullA f141 J yen-yen

OFFICE USE ONLY REASONI A I c I p

Sections Delivery Date Chemical PHI

CERTIFICAU AND WARRANTY

1 That ttl rtoort pNMntt 1 1M tnd complttt ~ord oltll tgriculturtl cntmbullcals (bullncltldillnnctieldtl lungbullcldl1 herblclcll1 etc)uMd IInceheNnl ollllt v-atacrop 01 crenberry bogalrom wlncn I anan deliver to you any crenbltriea o1 tl1 ti_crop and 2 Thlt crenhrrta wnlcn t ttlllll dellVIr to you Irom ttlll 11_crop were to the best ol myt~nowledge end betlel grown In atriel

OIIance Wltn the rqulremenla end ttendardt epproved by ttlll 8011rd ot Directors and Management 11 well 11 EPA and IOA or _eunureCanada

Oatbullshy~middot------------- - shy

- r I

OCEAN SPRAY CRANBERRIES INC ~------~middot~ ~ _________ middotmiddotmiddot ~middotmiddot~~~middot~5 Grower Pntlclde Use Report

~INITRUCTIONI ilttcorG beloW- IIMIIIIeftll WliiiiJoMIICIOn to orOCiucong actea lot tt11 crop ynt Do not hit letbl11er1 PINM UN one IINI per Chtllleal -OfWircl oriOIMI lnd llrll COpy (Ill IIOMCI) 10 Oclln IOfiY HAMI --------------------CtanMIriel Inc Mlor SpMIO 10111

llorf l ahlbU Alectlont__ middot--I hlbiiAI~ AbullAir Sbulllprnk~

Obull Ongtufld WbullWipe A 3 illl (fotiiIQIM lhhltiiiA c- c_ IJINiuciiAcrt) AcrHTNt iMI -300 (_ 1()163 A ~IbullASamp A_1 AI ~f S 6J

a1o o 3obull A A$ M bull A Ilt AU a 53

~PI SOlo$ A 10 5 5sPnoltbull bull middot ~ se1 a 7Jo (pis A A 1- ~ f FfJ 5ts u s ~~~ 2 95 s A~ ASbullf -5 511

_L5t1_ 01 bulls I A AI - A9 8) 5a ~ P ~ 3bullamp A AI -Af B(J SIB

~ Sbullo illgtbull lt3 5 AI ~gtAf t1~~ middot1 l) j 3o iJJI 10 w AS 1middot 5 IJ~middot

ltrlltl c 1 116 s A4 A1middot C 15 _ 1jJ

SID c-~loJolt 1 10 l AImiddotASF llr-41 middot8 1 3

a~58 vu s At-A 8 2 1n 50 AoL fll~ middotlc D1AampIol4 G 5laquo-S AIAL A 5 ~

UI DoampZt uOOJillt ltl 5 A t - Af 9middot- 7~o

OFFICE USE ONLY REASONI A I c I p

Sectlona Delivery Date Chemical PHI

CERTIFICATE AND WARRANTY lhfieOycetllfylndWtrFinttoyouuloHows 1 Thlt 111bullbull reoon prJtenll 1 true 1ncl comolell recOltCI of 111 tgriculturll ctllmlcllt(lfCiudit~g lnMCIIcldlt lunglc1d11 hllriiiCICIU IICI uMCIIiiICIIIINUI otiUt)llrtcroooncrJn~bOQIIrom wnien I tlllll CIIIIYirtoyouJnycrtnberriltol ttll 11-croplnd 1middot Thlt 111 crtntlllfiet wiiiCII I thlll dellIf 10 yOY I rom I Ill II_ crop Wlfl to I Ill bet of my knowle-clgl lnd belie grown In llriet

~ompli1nc1 witll lhl fiQUiflmlntt lnd allndlrdl tpprold by ttll Botrd ol OifiCIOfl tnd Mtnagtmtnl 11 will 11 EPA tno FDA or

middotmiddot~middot~middot _1 asg middot~ MIN OffiCI- WHITE AlAOfFICI- YELLOW

9=cx +~ G ____

- r I

OCEAN SPRAY CRANBERRIES INC ~------~middot~ ~ _________ middotmiddotmiddot ~middotmiddot~~~middot~5 Grower Pntlclde Use Report

~INITRUCTIONI ilttcorG beloW- IIMIIIIeftll WliiiiJoMIICIOn to orOCiucong actea lot tt11 crop ynt Do not hit letbl11er1 PINM UN one IINI per Chtllleal -OfWircl oriOIMI lnd llrll COpy (Ill IIOMCI) 10 Oclln IOfiY HAMI --------------------CtanMIriel Inc Mlor SpMIO 10111

llorf l ahlbU Alectlont__ middot--I hlbiiAI~ AbullAir Sbulllprnk~

Obull Ongtufld WbullWipe A 3 illl (fotiiIQIM lhhltiiiA c- c_ IJINiuciiAcrt) AcrHTNt iMI -300 (_ 1()163 A ~IbullASamp A_1 AI ~f S 6J

a1o o 3obull A A$ M bull A Ilt AU a 53

~PI SOlo$ A 10 5 5sPnoltbull bull middot ~ se1 a 7Jo (pis A A 1- ~ f FfJ 5ts u s ~~~ 2 95 s A~ ASbullf -5 511

_L5t1_ 01 bulls I A AI - A9 8) 5a ~ P ~ 3bullamp A AI -Af B(J SIB

~ Sbullo illgtbull lt3 5 AI ~gtAf t1~~ middot1 l) j 3o iJJI 10 w AS 1middot 5 IJ~middot

ltrlltl c 1 116 s A4 A1middot C 15 _ 1jJ

SID c-~loJolt 1 10 l AImiddotASF llr-41 middot8 1 3

a~58 vu s At-A 8 2 1n 50 AoL fll~ middotlc D1AampIol4 G 5laquo-S AIAL A 5 ~

UI DoampZt uOOJillt ltl 5 A t - Af 9middot- 7~o

OFFICE USE ONLY REASONI A I c I p

Sectlona Delivery Date Chemical PHI

CERTIFICATE AND WARRANTY lhfieOycetllfylndWtrFinttoyouuloHows 1 Thlt 111bullbull reoon prJtenll 1 true 1ncl comolell recOltCI of 111 tgriculturll ctllmlcllt(lfCiudit~g lnMCIIcldlt lunglc1d11 hllriiiCICIU IICI uMCIIiiICIIIINUI otiUt)llrtcroooncrJn~bOQIIrom wnien I tlllll CIIIIYirtoyouJnycrtnberriltol ttll 11-croplnd 1middot Thlt 111 crtntlllfiet wiiiCII I thlll dellIf 10 yOY I rom I Ill II_ crop Wlfl to I Ill bet of my knowle-clgl lnd belie grown In llriet

~ompli1nc1 witll lhl fiQUiflmlntt lnd allndlrdl tpprold by ttll Botrd ol OifiCIOfl tnd Mtnagtmtnl 11 will 11 EPA tno FDA or

middotmiddot~middot~middot _1 asg middot~ MIN OffiCI- WHITE AlAOfFICI- YELLOW

9=cx +~ G ____

- r -

AllIDI1EN1 A2

bullbull IIEMOIAMDUit bullbull

T0 1 J o-tng DATE Octobor Z 1990

A I A Stth lt~~ U t PIQUCTJY $CIIQ PIGWl bull fiELQ SMPLU

~ttt1Je0 1 (fes3 J~~~~~~1tn1u~la~~~~n~ 0~~ a0~middot~middot~~ chlorinated fungtctdts (Tut II) Bravo Captan and Dtfolatln ald the dtthtocartlautts (Tut III) Ftrillll Mantb ampnd Ztntb Whtn appltcablt Car-Daryl (StYtn) usays (Test IV) wert also ptrfoiMd

The ttst for dtthtocarbatu dots not dtsttngutsh between poundSOC s (antb Ztntb and Mancoztb) and Flrbampll (a nonmiddotEBOC) Otthtocarbuatu rtstduts cl11rly tdtnttfttd u Ferbq fr011 appltcattons for11s wtll bt reported u Ftrbu All others as EBDC s

Our dtttct t on l11tts for Camprbaryl and chlor inated fungtctdts art now 110rt sensttht (0 05 PPII)

Aho a rtsapll fro~~ Grower 071 -58000 ) had Bravo rutdut above tolerance (S tl PPII) - Jtrt D~Mttng has betn nottfttd and 1 SKond rtsU~Pll wtll bt obtatnH

All other salts usayH wert wlthtn 11bull1t of toltrlnct of 050 PPII Dhz tnon 10 PPII Lorsb1n 10 PPII Mlhthton 10 PPII Pirlthton 20 PPII Guthton 50 PPII Brno 25 0 PPII Clphn 80 PPII Otfohhn 100 PPII Cubuyl (Styen1n) ud 70 PPII dlthtocrba8ltts

070 -1765 Lorsb1n 0 08 Acctptablt 8rno 0 08 Ferb11 006 Crb1ryl 0 08

J

- r -

~A2

Memorandum J OoooniFog Date October 20 1H7

bull bull Slth tL~ PESTICICpound 5CIpound[N FlfiXAAN

Thl following ta~~Plts were all anllyzecJ for the orgroptosphites (T t 1) Lorsban Hllathion Parathion Oiazinon and Guthion When tpplicable the SIIIIC)les wert also 101lyzed for tle etllorinatecl fllgicidea (Tt 2) Bnvo Captan and Oirolatllti the calOMIItes (Test J ) Cirbofuran and Cirbltyl ancJ t~ dithiocarbMites (Teat 4) Feron Haneb and Zineb

All but one of the sanples we~ within lilllit of tolerance for 0 5 ppm Oiazinon 10 PPI Lorsoan 80 ppt11 Malathion 10 ppm Parathion 20 pp11

Guthion 50 ppm Bravo 25 ppm taptan 80 ppm Oifolatan 05 PPIII Carbofuran 10 pp11 Cubaryl 70 ppn1 Maneb 7 0 ppm lineb and 70 ppm fert)am

070-2765 Lorsoan 055 Parathion 004 l

_________________2 Bravo 021

I J

J I

r

ERCO Energy ResourcH Co lnc All10HNI A )

lM-middot-111_c-_311 II171 Mi l lll twbull7bullU0-IU1

=c middot-c u- c-

Januuy 6 1981

Mr Michul Cardell Ocun Spray Cranberry Inc Bridge Street Middleboro MA 02346

Dear Mr Cardell

Enclosed are the results of the orqanic priodty pollutant acan for the cranberry sample you sent ua The

~~~rbullt~~~~~~t et~~~~r fon~~~~~~middot~~~~~~~~~ and the other half extracted for ba -neutral and acid cobullponanta Volatile compounch were analyzed by purge shyand-trap GCMS ot the homogenate The analyticlaquo paraMtua ud for the analyses conformed to the methodologies outlined in Method fi08 (pesticides) Method 624 (vohtilea) and Method 625 (acids and bue-neutrala) as detailed i n the Federal Reqisur Decellber l 1979 69464-69575 surrogate cobullpounda were used to mon i t or the recovery of primary pollutants which bulliqht be present All compounds were recovered at levell similar to those fou nd tor water e xtrac tions

Eullination of t he results shows only one pr iority pollut ant cobullpound present in any measurable concentration (phenol J Thh ay be present as a by-product of the acid extraction The extrac t ion may hydrolyze natural product

~~~~~~~~9~~~~n~p~~~~o~~ ~1~~~~s~hich cons ist ot po l ymers

It you have any questions about this data pl e ase do not hesitate to call

Sincerely

A Dallas Wait PhD Manager Analytical Organic

Chemistry Laboratory Environmental Sciences Division

ADW tp enc Reurosvr5 3 ve11 for dy ()Je~J o +

Sfe_ bull 8~ o migt r v f( V (ve Us ed i r) CaJltvfr ~S

r

AlI10tENl AJ

Who l e Crbullnberrlbullbull l1-7l lENT 10 ERCO JD

11~ ~ ~ Y I ac roltt n NO b9P aldrin NO

V l bullac rrlonitr-1e NO 90P dieldrin NO

v 4 ben zene NO 91P chlordane NO

V 6middottlrbon tetrachloride NO 92P 4 4-001 NO

v i middotchl OrObtnune NO 93P 4 4-00E NO

OV 1 2-dt ch lo rotttt~nt NO 94P 4 4-000 NO

I V 1 1 1 - trfchloroethane NO 9SP a-endosu1 hn NO NOJV 1 1-dtchlorotthane NO 96P 5-tndosulfan

4V 1 1 2-tr tchloroe t hane NO 97P tndosul fan sul flte NO

sv 1 11 1212-te t rac hl oroethane NO 98P end r t n NO NO6V chlor-oethane NO 99P end r i n a l deh~Cit

7V bh(chlorONthrl le ther NO lOOP he2 t ach l or NO

9V 2-chl oroethrlvt nrl ether NO 101P he2 t1c hl or e2oxt de NO NOJV chloroforw NO 102P a-BHC

9V ~ 1 1 1-ltltchloroethtltnt NO lOJP ~-BHC NO

ov 1 12- trans-111ch1orotthtlent NO 104P r -BHC NO

2V l 12-dfchloro2ro2ant NO lOSP 6middot8HC NO NOJV 113-dfchloro2rOpoundtlene NO 106P PCB-1242

~ thtl benzene NO 107P PCB-1254 NO

4V bullthtltnt chloride NO 108P PCBmiddot1221 NO

sv 111thrl chlolidt NO 109P PC8middot1232 NO NO6V methrl brOIIfde NO llOP PC8middot1248

7V brcofoMI NO 111P PCB-1260 NO

av cstchloroorOIDOIIIthant NO 112P PCB-1016 NO

gv trt ch 1orofl uoromethant NO 11JP toxa2hene NO

ov dtch1 oroel1 fl uorolltthant NO

IV c hlorodtbro~~C~~~tthant NO HO bull none de t ec t ed

sv tttrach1 o roeth~lene NO NA bull not appltcaDle

6V toluene NO bull 1-9 IJ911

o7V trtch1oroethllene Reported by _ ~Cf2----shymiddotNO _JII)fav vtn~l chloride NO checkeel by __fAAiEgtOI---- shy

SURROGATE RECOVERI ES

BASE NEUTRAL R~cov ery COIPOUNOS Recovery VOLATILES 1 Recovery

6middotpheno1 111middotnaphthalene _____ d6middot benzene wn_ da-tol uene_ill_ Cis-py r idine ~

ill

nr~~~nol ds -nf trobenzene -middotmiddot---=shyuua_ fluo roan11fne NA

fluo ronaphtlla lene ___ill__

-I

rribull-=sHmiddot e~ ti r =~r

bull I bull~-0= ~~

~~

h~~

-n

~=i

==Ul

rr AIT10MEN1 A 3 bull middotr

i~a l~ pound

(N(IttY RESOURCES CO INC SUMltIARY OF OfUiANIC PRlOAJTY POLLUTANT ANAlYSIS e~ ~ sect ~

Ll(Hl ocn SpUIJ ~R~

LIEN 10 11holbull CrbullnHrrJbullbull OATpound SAMPLE AECpound11pound0 1 DECIO bull l ~co 10 JJ-571 DATE ANAlYSIS CCMPLETEO UDlaquoIO

=-~ 0 = ACID COMPOUNDS BASE NEUTRAL COMPOUNDSILlamp lliL

l A 2 1 4 16-trtchloro~htnol NO 418 4-oromoPhtnll Jhtnyl ether NO ~ 2Abull p-chloromiddotIIImiddotCruol NO 428 bh( 2-chl orohopropyllether NO ~ 4A 2-chlorophenol NO 438 bt sl2-chloroethoxylmethane NO -~ 1A Z14-dfchl orophtnol NO 528 htuchlorobuUdiene NO ~--~5 4A z4-df~~ethy1Phtno1 NO 538 huachl orocycloPtntadt ene NO 7A Z-nttro2henol NO 548 tsophorone NO Ei

SA 4-nt tro2henol NO 558 naohthalent NO 9A Z14-dfnf t ro2henol NO 568 nt trobenzene NO ~ OA 4 6-dfnf tro-o-cruol NO 618 N- nf trosodfrnethyluint NO 4A Ptntachl oro2henol NO 628 N-ni trosoafPhtnylallf ne NO C5A Phtnol JO 638 N-nf trosodf -n-2ro2tlami ne NO

668 bi s( 2-ttnll hextlllhthi late NO shyn 678 buttl benztl 2hthalate NO

ASE[NEUTRAL COI1POUNOS 688 dfmiddotn-butrl 2hthalate NO =

middote actnllhthene NO 698 di-n-octtl (hthlhte NO =Ule benzidi ne NO 708 dietht1 lhthalate 18 1 2 4-trtchlorobenzene NO 718 dh~tthrl lhthalate NO 8 htuchl orobenzent NO 728 benzol bullIanthracene NO 28 heuchl oroethlnt NO 738 benzol a 12trtne NO 88 bfs( 2-chl oroetht1lether NO 748 3 4-benzofl uoranthtnt NO 08 2-chl oron12hthalent NO 758 benzo(klfluoranttlene NO 58 1 2-dtchlorobenzene NO 768 chrtsene NO

68 1 J-dfchlorobenzene NO 778 acena2hthtlene NO 78 1 4-dfchlorobenzene NO 788 anthracene NO 88 J J-dtchlorobenziatne NO 798 benzol ghf (ertl ene NO 58 2 4-dinttrotoluene NO 808 fluorene NO

68 2 6-dtnltrotoluene NO 818 2henanthrene NO

78 1 12-dt lhtmrl hrdrazt ne NO 828 df benzol a 1h anthracene NO gt98 fl uoranthene NO 838 fndeno(1 12 1J-cal2trtne NO oe 4-chl or olhenrl lhentl e t her NO 848 ltrene NO

1298 237 ti-Utrachloroafbenzoshy2-dfoxfn NO

_1

I r -

-HAlt VI loi iiUIJ( blAND o tROVUl(( 11ANTHK)t~

INTUbullQffl([ M(fiIO

ro Ha~op Bochosian Olief DATLf(gtbruuy Z 191

OUT HealthOfice of Health rnaineennc

fltOM ~l~~s J r PhD UJK HealthLaboratories

~UIJ[CT Cranberry Test Results

This report covers analyses by the Health Laboratory on cranberries collected by Dr James Sullivan Supervisina 0enust on OXcmber 29 1980 at Merchants Cold Storaae and 11arehouso F Section Basement The source of tho cranberries wat identified as Crecn Co Coventry Rhode Is llnd 1elve S~les representshyina lZ bins out of a total of 144 bins -ere collected and pooled for analysis nle pooled sanple was split on site with lJ Ocean Spray representative TI10 s~le was trmsportcd to the laboratory and asdned loa Nunber SZ412

The cranberry SDJflle w~s extracted by four different procedures Two subiaJl)les of the berries were IIIDShed before extnction 11d two e re left int3Ct nCn one subsat~t~le of each of these sets was extracted by soaking in water while the other two subs~lu were soaked in a mixture of water with a small uoount of pentane added The pentane extr3cts were analyzed by 0FID GCEC and CCJtIS 1ater from the two s~les which were siftl)ly soaked in water was analyzed by pur~eand trap GHall GFID 01d ams

Recovery studies were n1n for 111-trichloroethlne 1 trichloroethylene and tetrachloroethylene Hinilllllll detection limits for these con)C)unds ere 4 4 and 20 p~kg cranberries (wet wt ) 1 respectively For all otlCr c~unds

1

in the list (see below) no peJks were detected at concentrJtions that could be confirmed by CCH5

These procedures were chosen to determine if the tested co~lOunds ere ndsorbed to the outer surbce of the bcrnes or were contained wi thin the berries Penmiddot tUle extraction was used to remove more tiamphtly held co~unds

RECEIVED R I DEPARTMENT OF HEALTH

FEB ~ 1981

ASSliCIATE 0RECTOR COMMUNITY HEAUH rrb

r

ERCO Energy ResourcH Co lnc All10HNI A )

lM-middot-111_c-_311 II171 Mi l lll twbull7bullU0-IU1

=c middot-c u- c-

Januuy 6 1981

Mr Michul Cardell Ocun Spray Cranberry Inc Bridge Street Middleboro MA 02346

Dear Mr Cardell

Enclosed are the results of the orqanic priodty pollutant acan for the cranberry sample you sent ua The

~~~rbullt~~~~~~t et~~~~r fon~~~~~~middot~~~~~~~~~ and the other half extracted for ba -neutral and acid cobullponanta Volatile compounch were analyzed by purge shyand-trap GCMS ot the homogenate The analyticlaquo paraMtua ud for the analyses conformed to the methodologies outlined in Method fi08 (pesticides) Method 624 (vohtilea) and Method 625 (acids and bue-neutrala) as detailed i n the Federal Reqisur Decellber l 1979 69464-69575 surrogate cobullpounda were used to mon i t or the recovery of primary pollutants which bulliqht be present All compounds were recovered at levell similar to those fou nd tor water e xtrac tions

Eullination of t he results shows only one pr iority pollut ant cobullpound present in any measurable concentration (phenol J Thh ay be present as a by-product of the acid extraction The extrac t ion may hydrolyze natural product

~~~~~~~~9~~~~n~p~~~~o~~ ~1~~~~s~hich cons ist ot po l ymers

It you have any questions about this data pl e ase do not hesitate to call

Sincerely

A Dallas Wait PhD Manager Analytical Organic

Chemistry Laboratory Environmental Sciences Division

ADW tp enc Reurosvr5 3 ve11 for dy ()Je~J o +

Sfe_ bull 8~ o migt r v f( V (ve Us ed i r) CaJltvfr ~S

r

AlI10tENl AJ

Who l e Crbullnberrlbullbull l1-7l lENT 10 ERCO JD

11~ ~ ~ Y I ac roltt n NO b9P aldrin NO

V l bullac rrlonitr-1e NO 90P dieldrin NO

v 4 ben zene NO 91P chlordane NO

V 6middottlrbon tetrachloride NO 92P 4 4-001 NO

v i middotchl OrObtnune NO 93P 4 4-00E NO

OV 1 2-dt ch lo rotttt~nt NO 94P 4 4-000 NO

I V 1 1 1 - trfchloroethane NO 9SP a-endosu1 hn NO NOJV 1 1-dtchlorotthane NO 96P 5-tndosulfan

4V 1 1 2-tr tchloroe t hane NO 97P tndosul fan sul flte NO

sv 1 11 1212-te t rac hl oroethane NO 98P end r t n NO NO6V chlor-oethane NO 99P end r i n a l deh~Cit

7V bh(chlorONthrl le ther NO lOOP he2 t ach l or NO

9V 2-chl oroethrlvt nrl ether NO 101P he2 t1c hl or e2oxt de NO NOJV chloroforw NO 102P a-BHC

9V ~ 1 1 1-ltltchloroethtltnt NO lOJP ~-BHC NO

ov 1 12- trans-111ch1orotthtlent NO 104P r -BHC NO

2V l 12-dfchloro2ro2ant NO lOSP 6middot8HC NO NOJV 113-dfchloro2rOpoundtlene NO 106P PCB-1242

~ thtl benzene NO 107P PCB-1254 NO

4V bullthtltnt chloride NO 108P PCBmiddot1221 NO

sv 111thrl chlolidt NO 109P PC8middot1232 NO NO6V methrl brOIIfde NO llOP PC8middot1248

7V brcofoMI NO 111P PCB-1260 NO

av cstchloroorOIDOIIIthant NO 112P PCB-1016 NO

gv trt ch 1orofl uoromethant NO 11JP toxa2hene NO

ov dtch1 oroel1 fl uorolltthant NO

IV c hlorodtbro~~C~~~tthant NO HO bull none de t ec t ed

sv tttrach1 o roeth~lene NO NA bull not appltcaDle

6V toluene NO bull 1-9 IJ911

o7V trtch1oroethllene Reported by _ ~Cf2----shymiddotNO _JII)fav vtn~l chloride NO checkeel by __fAAiEgtOI---- shy

SURROGATE RECOVERI ES

BASE NEUTRAL R~cov ery COIPOUNOS Recovery VOLATILES 1 Recovery

6middotpheno1 111middotnaphthalene _____ d6middot benzene wn_ da-tol uene_ill_ Cis-py r idine ~

ill

nr~~~nol ds -nf trobenzene -middotmiddot---=shyuua_ fluo roan11fne NA

fluo ronaphtlla lene ___ill__

-I

rribull-=sHmiddot e~ ti r =~r

bull I bull~-0= ~~

~~

h~~

-n

~=i

==Ul

rr AIT10MEN1 A 3 bull middotr

i~a l~ pound

(N(IttY RESOURCES CO INC SUMltIARY OF OfUiANIC PRlOAJTY POLLUTANT ANAlYSIS e~ ~ sect ~

Ll(Hl ocn SpUIJ ~R~

LIEN 10 11holbull CrbullnHrrJbullbull OATpound SAMPLE AECpound11pound0 1 DECIO bull l ~co 10 JJ-571 DATE ANAlYSIS CCMPLETEO UDlaquoIO

=-~ 0 = ACID COMPOUNDS BASE NEUTRAL COMPOUNDSILlamp lliL

l A 2 1 4 16-trtchloro~htnol NO 418 4-oromoPhtnll Jhtnyl ether NO ~ 2Abull p-chloromiddotIIImiddotCruol NO 428 bh( 2-chl orohopropyllether NO ~ 4A 2-chlorophenol NO 438 bt sl2-chloroethoxylmethane NO -~ 1A Z14-dfchl orophtnol NO 528 htuchlorobuUdiene NO ~--~5 4A z4-df~~ethy1Phtno1 NO 538 huachl orocycloPtntadt ene NO 7A Z-nttro2henol NO 548 tsophorone NO Ei

SA 4-nt tro2henol NO 558 naohthalent NO 9A Z14-dfnf t ro2henol NO 568 nt trobenzene NO ~ OA 4 6-dfnf tro-o-cruol NO 618 N- nf trosodfrnethyluint NO 4A Ptntachl oro2henol NO 628 N-ni trosoafPhtnylallf ne NO C5A Phtnol JO 638 N-nf trosodf -n-2ro2tlami ne NO

668 bi s( 2-ttnll hextlllhthi late NO shyn 678 buttl benztl 2hthalate NO

ASE[NEUTRAL COI1POUNOS 688 dfmiddotn-butrl 2hthalate NO =

middote actnllhthene NO 698 di-n-octtl (hthlhte NO =Ule benzidi ne NO 708 dietht1 lhthalate 18 1 2 4-trtchlorobenzene NO 718 dh~tthrl lhthalate NO 8 htuchl orobenzent NO 728 benzol bullIanthracene NO 28 heuchl oroethlnt NO 738 benzol a 12trtne NO 88 bfs( 2-chl oroetht1lether NO 748 3 4-benzofl uoranthtnt NO 08 2-chl oron12hthalent NO 758 benzo(klfluoranttlene NO 58 1 2-dtchlorobenzene NO 768 chrtsene NO

68 1 J-dfchlorobenzene NO 778 acena2hthtlene NO 78 1 4-dfchlorobenzene NO 788 anthracene NO 88 J J-dtchlorobenziatne NO 798 benzol ghf (ertl ene NO 58 2 4-dinttrotoluene NO 808 fluorene NO

68 2 6-dtnltrotoluene NO 818 2henanthrene NO

78 1 12-dt lhtmrl hrdrazt ne NO 828 df benzol a 1h anthracene NO gt98 fl uoranthene NO 838 fndeno(1 12 1J-cal2trtne NO oe 4-chl or olhenrl lhentl e t her NO 848 ltrene NO

1298 237 ti-Utrachloroafbenzoshy2-dfoxfn NO

_1

I r -

-HAlt VI loi iiUIJ( blAND o tROVUl(( 11ANTHK)t~

INTUbullQffl([ M(fiIO

ro Ha~op Bochosian Olief DATLf(gtbruuy Z 191

OUT HealthOfice of Health rnaineennc

fltOM ~l~~s J r PhD UJK HealthLaboratories

~UIJ[CT Cranberry Test Results

This report covers analyses by the Health Laboratory on cranberries collected by Dr James Sullivan Supervisina 0enust on OXcmber 29 1980 at Merchants Cold Storaae and 11arehouso F Section Basement The source of tho cranberries wat identified as Crecn Co Coventry Rhode Is llnd 1elve S~les representshyina lZ bins out of a total of 144 bins -ere collected and pooled for analysis nle pooled sanple was split on site with lJ Ocean Spray representative TI10 s~le was trmsportcd to the laboratory and asdned loa Nunber SZ412

The cranberry SDJflle w~s extracted by four different procedures Two subiaJl)les of the berries were IIIDShed before extnction 11d two e re left int3Ct nCn one subsat~t~le of each of these sets was extracted by soaking in water while the other two subs~lu were soaked in a mixture of water with a small uoount of pentane added The pentane extr3cts were analyzed by 0FID GCEC and CCJtIS 1ater from the two s~les which were siftl)ly soaked in water was analyzed by pur~eand trap GHall GFID 01d ams

Recovery studies were n1n for 111-trichloroethlne 1 trichloroethylene and tetrachloroethylene Hinilllllll detection limits for these con)C)unds ere 4 4 and 20 p~kg cranberries (wet wt ) 1 respectively For all otlCr c~unds

1

in the list (see below) no peJks were detected at concentrJtions that could be confirmed by CCH5

These procedures were chosen to determine if the tested co~lOunds ere ndsorbed to the outer surbce of the bcrnes or were contained wi thin the berries Penmiddot tUle extraction was used to remove more tiamphtly held co~unds

RECEIVED R I DEPARTMENT OF HEALTH

FEB ~ 1981

ASSliCIATE 0RECTOR COMMUNITY HEAUH rrb

r

AlI10tENl AJ

Who l e Crbullnberrlbullbull l1-7l lENT 10 ERCO JD

11~ ~ ~ Y I ac roltt n NO b9P aldrin NO

V l bullac rrlonitr-1e NO 90P dieldrin NO

v 4 ben zene NO 91P chlordane NO

V 6middottlrbon tetrachloride NO 92P 4 4-001 NO

v i middotchl OrObtnune NO 93P 4 4-00E NO

OV 1 2-dt ch lo rotttt~nt NO 94P 4 4-000 NO

I V 1 1 1 - trfchloroethane NO 9SP a-endosu1 hn NO NOJV 1 1-dtchlorotthane NO 96P 5-tndosulfan

4V 1 1 2-tr tchloroe t hane NO 97P tndosul fan sul flte NO

sv 1 11 1212-te t rac hl oroethane NO 98P end r t n NO NO6V chlor-oethane NO 99P end r i n a l deh~Cit

7V bh(chlorONthrl le ther NO lOOP he2 t ach l or NO

9V 2-chl oroethrlvt nrl ether NO 101P he2 t1c hl or e2oxt de NO NOJV chloroforw NO 102P a-BHC

9V ~ 1 1 1-ltltchloroethtltnt NO lOJP ~-BHC NO

ov 1 12- trans-111ch1orotthtlent NO 104P r -BHC NO

2V l 12-dfchloro2ro2ant NO lOSP 6middot8HC NO NOJV 113-dfchloro2rOpoundtlene NO 106P PCB-1242

~ thtl benzene NO 107P PCB-1254 NO

4V bullthtltnt chloride NO 108P PCBmiddot1221 NO

sv 111thrl chlolidt NO 109P PC8middot1232 NO NO6V methrl brOIIfde NO llOP PC8middot1248

7V brcofoMI NO 111P PCB-1260 NO

av cstchloroorOIDOIIIthant NO 112P PCB-1016 NO

gv trt ch 1orofl uoromethant NO 11JP toxa2hene NO

ov dtch1 oroel1 fl uorolltthant NO

IV c hlorodtbro~~C~~~tthant NO HO bull none de t ec t ed

sv tttrach1 o roeth~lene NO NA bull not appltcaDle

6V toluene NO bull 1-9 IJ911

o7V trtch1oroethllene Reported by _ ~Cf2----shymiddotNO _JII)fav vtn~l chloride NO checkeel by __fAAiEgtOI---- shy

SURROGATE RECOVERI ES

BASE NEUTRAL R~cov ery COIPOUNOS Recovery VOLATILES 1 Recovery

6middotpheno1 111middotnaphthalene _____ d6middot benzene wn_ da-tol uene_ill_ Cis-py r idine ~

ill

nr~~~nol ds -nf trobenzene -middotmiddot---=shyuua_ fluo roan11fne NA

fluo ronaphtlla lene ___ill__

-I

rribull-=sHmiddot e~ ti r =~r

bull I bull~-0= ~~

~~

h~~

-n

~=i

==Ul

rr AIT10MEN1 A 3 bull middotr

i~a l~ pound

(N(IttY RESOURCES CO INC SUMltIARY OF OfUiANIC PRlOAJTY POLLUTANT ANAlYSIS e~ ~ sect ~

Ll(Hl ocn SpUIJ ~R~

LIEN 10 11holbull CrbullnHrrJbullbull OATpound SAMPLE AECpound11pound0 1 DECIO bull l ~co 10 JJ-571 DATE ANAlYSIS CCMPLETEO UDlaquoIO

=-~ 0 = ACID COMPOUNDS BASE NEUTRAL COMPOUNDSILlamp lliL

l A 2 1 4 16-trtchloro~htnol NO 418 4-oromoPhtnll Jhtnyl ether NO ~ 2Abull p-chloromiddotIIImiddotCruol NO 428 bh( 2-chl orohopropyllether NO ~ 4A 2-chlorophenol NO 438 bt sl2-chloroethoxylmethane NO -~ 1A Z14-dfchl orophtnol NO 528 htuchlorobuUdiene NO ~--~5 4A z4-df~~ethy1Phtno1 NO 538 huachl orocycloPtntadt ene NO 7A Z-nttro2henol NO 548 tsophorone NO Ei

SA 4-nt tro2henol NO 558 naohthalent NO 9A Z14-dfnf t ro2henol NO 568 nt trobenzene NO ~ OA 4 6-dfnf tro-o-cruol NO 618 N- nf trosodfrnethyluint NO 4A Ptntachl oro2henol NO 628 N-ni trosoafPhtnylallf ne NO C5A Phtnol JO 638 N-nf trosodf -n-2ro2tlami ne NO

668 bi s( 2-ttnll hextlllhthi late NO shyn 678 buttl benztl 2hthalate NO

ASE[NEUTRAL COI1POUNOS 688 dfmiddotn-butrl 2hthalate NO =

middote actnllhthene NO 698 di-n-octtl (hthlhte NO =Ule benzidi ne NO 708 dietht1 lhthalate 18 1 2 4-trtchlorobenzene NO 718 dh~tthrl lhthalate NO 8 htuchl orobenzent NO 728 benzol bullIanthracene NO 28 heuchl oroethlnt NO 738 benzol a 12trtne NO 88 bfs( 2-chl oroetht1lether NO 748 3 4-benzofl uoranthtnt NO 08 2-chl oron12hthalent NO 758 benzo(klfluoranttlene NO 58 1 2-dtchlorobenzene NO 768 chrtsene NO

68 1 J-dfchlorobenzene NO 778 acena2hthtlene NO 78 1 4-dfchlorobenzene NO 788 anthracene NO 88 J J-dtchlorobenziatne NO 798 benzol ghf (ertl ene NO 58 2 4-dinttrotoluene NO 808 fluorene NO

68 2 6-dtnltrotoluene NO 818 2henanthrene NO

78 1 12-dt lhtmrl hrdrazt ne NO 828 df benzol a 1h anthracene NO gt98 fl uoranthene NO 838 fndeno(1 12 1J-cal2trtne NO oe 4-chl or olhenrl lhentl e t her NO 848 ltrene NO

1298 237 ti-Utrachloroafbenzoshy2-dfoxfn NO

_1

I r -

-HAlt VI loi iiUIJ( blAND o tROVUl(( 11ANTHK)t~

INTUbullQffl([ M(fiIO

ro Ha~op Bochosian Olief DATLf(gtbruuy Z 191

OUT HealthOfice of Health rnaineennc

fltOM ~l~~s J r PhD UJK HealthLaboratories

~UIJ[CT Cranberry Test Results

This report covers analyses by the Health Laboratory on cranberries collected by Dr James Sullivan Supervisina 0enust on OXcmber 29 1980 at Merchants Cold Storaae and 11arehouso F Section Basement The source of tho cranberries wat identified as Crecn Co Coventry Rhode Is llnd 1elve S~les representshyina lZ bins out of a total of 144 bins -ere collected and pooled for analysis nle pooled sanple was split on site with lJ Ocean Spray representative TI10 s~le was trmsportcd to the laboratory and asdned loa Nunber SZ412

The cranberry SDJflle w~s extracted by four different procedures Two subiaJl)les of the berries were IIIDShed before extnction 11d two e re left int3Ct nCn one subsat~t~le of each of these sets was extracted by soaking in water while the other two subs~lu were soaked in a mixture of water with a small uoount of pentane added The pentane extr3cts were analyzed by 0FID GCEC and CCJtIS 1ater from the two s~les which were siftl)ly soaked in water was analyzed by pur~eand trap GHall GFID 01d ams

Recovery studies were n1n for 111-trichloroethlne 1 trichloroethylene and tetrachloroethylene Hinilllllll detection limits for these con)C)unds ere 4 4 and 20 p~kg cranberries (wet wt ) 1 respectively For all otlCr c~unds

1

in the list (see below) no peJks were detected at concentrJtions that could be confirmed by CCH5

These procedures were chosen to determine if the tested co~lOunds ere ndsorbed to the outer surbce of the bcrnes or were contained wi thin the berries Penmiddot tUle extraction was used to remove more tiamphtly held co~unds

RECEIVED R I DEPARTMENT OF HEALTH

FEB ~ 1981

ASSliCIATE 0RECTOR COMMUNITY HEAUH rrb

rr AIT10MEN1 A 3 bull middotr

i~a l~ pound

(N(IttY RESOURCES CO INC SUMltIARY OF OfUiANIC PRlOAJTY POLLUTANT ANAlYSIS e~ ~ sect ~

Ll(Hl ocn SpUIJ ~R~

LIEN 10 11holbull CrbullnHrrJbullbull OATpound SAMPLE AECpound11pound0 1 DECIO bull l ~co 10 JJ-571 DATE ANAlYSIS CCMPLETEO UDlaquoIO

=-~ 0 = ACID COMPOUNDS BASE NEUTRAL COMPOUNDSILlamp lliL

l A 2 1 4 16-trtchloro~htnol NO 418 4-oromoPhtnll Jhtnyl ether NO ~ 2Abull p-chloromiddotIIImiddotCruol NO 428 bh( 2-chl orohopropyllether NO ~ 4A 2-chlorophenol NO 438 bt sl2-chloroethoxylmethane NO -~ 1A Z14-dfchl orophtnol NO 528 htuchlorobuUdiene NO ~--~5 4A z4-df~~ethy1Phtno1 NO 538 huachl orocycloPtntadt ene NO 7A Z-nttro2henol NO 548 tsophorone NO Ei

SA 4-nt tro2henol NO 558 naohthalent NO 9A Z14-dfnf t ro2henol NO 568 nt trobenzene NO ~ OA 4 6-dfnf tro-o-cruol NO 618 N- nf trosodfrnethyluint NO 4A Ptntachl oro2henol NO 628 N-ni trosoafPhtnylallf ne NO C5A Phtnol JO 638 N-nf trosodf -n-2ro2tlami ne NO

668 bi s( 2-ttnll hextlllhthi late NO shyn 678 buttl benztl 2hthalate NO

ASE[NEUTRAL COI1POUNOS 688 dfmiddotn-butrl 2hthalate NO =

middote actnllhthene NO 698 di-n-octtl (hthlhte NO =Ule benzidi ne NO 708 dietht1 lhthalate 18 1 2 4-trtchlorobenzene NO 718 dh~tthrl lhthalate NO 8 htuchl orobenzent NO 728 benzol bullIanthracene NO 28 heuchl oroethlnt NO 738 benzol a 12trtne NO 88 bfs( 2-chl oroetht1lether NO 748 3 4-benzofl uoranthtnt NO 08 2-chl oron12hthalent NO 758 benzo(klfluoranttlene NO 58 1 2-dtchlorobenzene NO 768 chrtsene NO

68 1 J-dfchlorobenzene NO 778 acena2hthtlene NO 78 1 4-dfchlorobenzene NO 788 anthracene NO 88 J J-dtchlorobenziatne NO 798 benzol ghf (ertl ene NO 58 2 4-dinttrotoluene NO 808 fluorene NO

68 2 6-dtnltrotoluene NO 818 2henanthrene NO

78 1 12-dt lhtmrl hrdrazt ne NO 828 df benzol a 1h anthracene NO gt98 fl uoranthene NO 838 fndeno(1 12 1J-cal2trtne NO oe 4-chl or olhenrl lhentl e t her NO 848 ltrene NO

1298 237 ti-Utrachloroafbenzoshy2-dfoxfn NO

_1

I r -

-HAlt VI loi iiUIJ( blAND o tROVUl(( 11ANTHK)t~

INTUbullQffl([ M(fiIO

ro Ha~op Bochosian Olief DATLf(gtbruuy Z 191

OUT HealthOfice of Health rnaineennc

fltOM ~l~~s J r PhD UJK HealthLaboratories

~UIJ[CT Cranberry Test Results

This report covers analyses by the Health Laboratory on cranberries collected by Dr James Sullivan Supervisina 0enust on OXcmber 29 1980 at Merchants Cold Storaae and 11arehouso F Section Basement The source of tho cranberries wat identified as Crecn Co Coventry Rhode Is llnd 1elve S~les representshyina lZ bins out of a total of 144 bins -ere collected and pooled for analysis nle pooled sanple was split on site with lJ Ocean Spray representative TI10 s~le was trmsportcd to the laboratory and asdned loa Nunber SZ412

The cranberry SDJflle w~s extracted by four different procedures Two subiaJl)les of the berries were IIIDShed before extnction 11d two e re left int3Ct nCn one subsat~t~le of each of these sets was extracted by soaking in water while the other two subs~lu were soaked in a mixture of water with a small uoount of pentane added The pentane extr3cts were analyzed by 0FID GCEC and CCJtIS 1ater from the two s~les which were siftl)ly soaked in water was analyzed by pur~eand trap GHall GFID 01d ams

Recovery studies were n1n for 111-trichloroethlne 1 trichloroethylene and tetrachloroethylene Hinilllllll detection limits for these con)C)unds ere 4 4 and 20 p~kg cranberries (wet wt ) 1 respectively For all otlCr c~unds

1

in the list (see below) no peJks were detected at concentrJtions that could be confirmed by CCH5

These procedures were chosen to determine if the tested co~lOunds ere ndsorbed to the outer surbce of the bcrnes or were contained wi thin the berries Penmiddot tUle extraction was used to remove more tiamphtly held co~unds

RECEIVED R I DEPARTMENT OF HEALTH

FEB ~ 1981

ASSliCIATE 0RECTOR COMMUNITY HEAUH rrb

I r -

-HAlt VI loi iiUIJ( blAND o tROVUl(( 11ANTHK)t~

INTUbullQffl([ M(fiIO

ro Ha~op Bochosian Olief DATLf(gtbruuy Z 191

OUT HealthOfice of Health rnaineennc

fltOM ~l~~s J r PhD UJK HealthLaboratories

~UIJ[CT Cranberry Test Results

This report covers analyses by the Health Laboratory on cranberries collected by Dr James Sullivan Supervisina 0enust on OXcmber 29 1980 at Merchants Cold Storaae and 11arehouso F Section Basement The source of tho cranberries wat identified as Crecn Co Coventry Rhode Is llnd 1elve S~les representshyina lZ bins out of a total of 144 bins -ere collected and pooled for analysis nle pooled sanple was split on site with lJ Ocean Spray representative TI10 s~le was trmsportcd to the laboratory and asdned loa Nunber SZ412

The cranberry SDJflle w~s extracted by four different procedures Two subiaJl)les of the berries were IIIDShed before extnction 11d two e re left int3Ct nCn one subsat~t~le of each of these sets was extracted by soaking in water while the other two subs~lu were soaked in a mixture of water with a small uoount of pentane added The pentane extr3cts were analyzed by 0FID GCEC and CCJtIS 1ater from the two s~les which were siftl)ly soaked in water was analyzed by pur~eand trap GHall GFID 01d ams

Recovery studies were n1n for 111-trichloroethlne 1 trichloroethylene and tetrachloroethylene Hinilllllll detection limits for these con)C)unds ere 4 4 and 20 p~kg cranberries (wet wt ) 1 respectively For all otlCr c~unds

1

in the list (see below) no peJks were detected at concentrJtions that could be confirmed by CCH5

These procedures were chosen to determine if the tested co~lOunds ere ndsorbed to the outer surbce of the bcrnes or were contained wi thin the berries Penmiddot tUle extraction was used to remove more tiamphtly held co~unds

RECEIVED R I DEPARTMENT OF HEALTH

FEB ~ 1981

ASSliCIATE 0RECTOR COMMUNITY HEAUH rrb

r

~81

~ lQh ~alk fresh crabcrrie~ upoundlamp frcs1 cranocn es

l1br chlorout rcomiddot oro1

1shyltroon [etO on1 middotichl 0it1i bullno

Tiiii

OT

OTO I

lorebull loroocO

ci ~l~~~~~)P lcrcbennno

Bonzene Ml TOTuno middot

liO - liOJ DltTECTED at concen trbulltions ibove t fe Uni~u~ Otcction (irnft middot(HDL)

lmiddotJL - rmiddotmImiddotIJ ~ OETECTO~I U iJIT iht is the l enl b~l obull ih ich the ch~micai c~nro~ be middotcetectc Jith p-osently lvailble instnrnentation

~101 ~gt-ere not detc~ed (see above)

ATTIOHENl B 2

- IIO II OlampllwtllllOMIJUM IIHJCJliOIII I UUUI

Food and Drug Administration585 Conntrthl StrutBoston Massachusetts 02109

Mrs P Robert S1tner Manager 80-155-891Coventry Cranberry CoDtvtston of Greene CoNarrow Lane 9119180Greene Rl 02827

Roger J Patenaude

CRANBERRIES SIMPIt consists of 121 qt jars of rresh rmiddotaw cranberrfes wet hHviSttd~ndomly from each of 4 different wooden boxes hotdfng aoprox 250 l bs each - -middotmiddotmiddotmiddot-____

r K~ middot~ middot~middot -middot ~ E ~~ -~ - c--middot--middot-- bull l U l lII fty ~middotmiddot I M I middot - M I bull middot shy(t ) bullh middot middotmiddotmiddot -u tk CIMIIIUtl_ IIbullbullbullbullbullU l l l Clu lbulltl bullbullCw bullutlc ltlo rul t~n ltlgth th onbull bull t l rbull ~~~bullmiddot

EEE~~rmiddot~27~~~~~~~~fmiddot ebullbullmiddotIIIUCtll ( _hi UIIOliiU )-~IICIOilCh ( bullbull h ) I OlfiiCIIIll lltfiOI)01_u ( t bull lbullbull ) NCCMIIOUACIO~ ( toU11I11 t t_)l ltl iGUoiU ( oooho U Ut)

~=IICpC~OIQI ( h i LOt U I(IUl) -middot x

B u UGuurcu acTIIIII uno cbull tus sbullu0 IIU IUl U ll lUII 1-lltATU IUIOUl OW(I TOL[IUIIC( Dl IUIDUU I CI W ICII fll(l( II II)

TOLWIICt su bullbullmiddot MlOw ra- bulluuus a bulloon tOIOIL Alnrs

bullbullmiddot h t ru t) l lotbullbull hl bull 1 bull ur lhbull u hUbullbull

~c Henry N Arnold Prestd~nt

- r -

ATlJCtt1Dfl 82

fiOMo ll l DUfloi( IH 0 IIIALTII IOY(U IChluii WftUI

Food and Orug Adm1nlst rat1on 585 Comerchl Strttt Boston Husachusetts 02109

Mrs P Robert Stener Manager 81-155-898 COventry Cranberry Co Dh1ston of Greene Co Nlrrov Lane 102880Greene RI 02827

Aolt1er J Patenaude

CRANBERRiES S~~le consists of 121 qt jars of fresh raw cranbtrrtu wet harvested co llecttifrbullndomly from 4X4XJ wooden box trrmed1ately atter conveying from bog

a bullbull bullbullbull ~ ~=bullbull i - c_ _ __ middot-middotmiddot-middot _

MbullLbull bulllt I Miftd middot ~ t~e _ lo (o) II ft tetIIU fgtIIII M the I Uh~ ltill u io l (h iul bull~bullJ f 4~1bullhh ou l4ltobullbull bull lllol o t~bull IH~ubullbull tbulll bull ~middot bull-u

bullI

EZlF~~~~~f~~~1 eIIOa UCIU (ohl CUIOniU I ) UMOJIIOII ( uo h ) l DIITIIOPIIllftPMIIOl) 11yen1( -IIOI IU ( bullbullbullbullphoWL0amp1111) CIIampCitCPIIUOUACID ( uoho t -1) ---1-middotmiddot-middotmiddotmiddotmiddotmiddot middot---middot llfllltCAIUWTI (ooo loo l Ull) IIIC PCJ~ ~_I)l (ubullhbull LUO All(IIH~) -middot rJnr middot bull

(j h bullbullbull hllhll

B -0 11411LATCTACTIOIIII ICAUOOIITMIISAWU

C ~~~~~l~middot~o~~~~s~~l~~~~~~~~R~~~~~~ robull WICK Tmt 1110

- r -

ATlJCtt1Dfl 82

fiOMo ll l DUfloi( IH 0 IIIALTII IOY(U IChluii WftUI

Food and Orug Adm1nlst rat1on 585 Comerchl Strttt Boston Husachusetts 02109

Mrs P Robert Stener Manager 81-155-898 COventry Cranberry Co Dh1ston of Greene Co Nlrrov Lane 102880Greene RI 02827

Aolt1er J Patenaude

CRANBERRiES S~~le consists of 121 qt jars of fresh raw cranbtrrtu wet harvested co llecttifrbullndomly from 4X4XJ wooden box trrmed1ately atter conveying from bog

a bullbull bullbullbull ~ ~=bullbull i - c_ _ __ middot-middotmiddot-middot _

MbullLbull bulllt I Miftd middot ~ t~e _ lo (o) II ft tetIIU fgtIIII M the I Uh~ ltill u io l (h iul bull~bullJ f 4~1bullhh ou l4ltobullbull bull lllol o t~bull IH~ubullbull tbulll bull ~middot bull-u

bullI

EZlF~~~~~f~~~1 eIIOa UCIU (ohl CUIOniU I ) UMOJIIOII ( uo h ) l DIITIIOPIIllftPMIIOl) 11yen1( -IIOI IU ( bullbullbullbullphoWL0amp1111) CIIampCitCPIIUOUACID ( uoho t -1) ---1-middotmiddot-middotmiddotmiddotmiddotmiddot middot---middot llfllltCAIUWTI (ooo loo l Ull) IIIC PCJ~ ~_I)l (ubullhbull LUO All(IIH~) -middot rJnr middot bull

(j h bullbullbull hllhll

B -0 11411LATCTACTIOIIII ICAUOOIITMIISAWU

C ~~~~~l~middot~o~~~~s~~l~~~~~~~~R~~~~~~ robull WICK Tmt 1110

- I

AT110MNI B 2

II ICl41TMIMT01114LTMl0UCU10M 4101 bull fr4U

- Food nd Drug Admtntstrltton 585 Cocnmerc111 Street Boston Hnuchusetu 02109

81-155-893 Mrs P Robert Stener ManagerCoventry Cranberry Co Dhtston of Greene Co 101580Narrow lane Greene RI 02827

Roger J Patenaude

CWi[RRiEbullSS~le consists of 121 qt jars of fresh raw cranberries wet harvested ~andomly fro~~~ a 4X4X3 wooden box hrmedtttely after conveying from bogbull

bull _ 1 1yu4 r~ tilt bull-bull bull bullbullM Ibull (o ) bullbull _ dethr tlllmiddot t middot---- shybullbull bull tbulllbulltll _ 1 c~itbull l bull~Ibull~ th bull u ~iUIbull thbull nul tchrbull ltu

(bull)

===~~1u~7iebull~IUtlll (uoltt CUIOniiU ) CIIMOIJChl ( uoh) t OITIIOIIIIlVIICI Ol) IIIIICIOIII( ( ooo ho llloliiiU) ----middot CIIICIIGIMIIUfACIU(eubulllu 1 1bull1) tltlltullllbulln (1 tr bullnl

~=11Cb~010raquo1 (oltl UAI 1U(I4H) -- osnrr t t

() l n 1u u ttu

~ 10 IIGUIlT~IlACTICJ IICAofiiiOI TMIS YWl(

0 UiiTIAL AlloUSII loOICAoTU IUIOU( 0yenU TOlUHIC( DR IUIDUU 1CI 1U CM JM(I( II 10 TOUAIIIIC( IU II lll0- 0IIUUllSOIampDOITIOIOAL AIIAUSI I

cc Henry N Arnol d President

) ~

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ATlAOMENl 8 3

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY lt(GIONI

IOWIITVIIWITIII Ilf LI bull INGJON MASIACHUIETTII21Jl

middot

July a ltiO

Dr M Starr ac~n lpu y Cranberry copny aD l~o~Uding lrldtbull ltreat Mld4bboro MA OU41

oar Dr I Urt l

Aa diMY-cl on July 1 no detectable levela of o r9anica wan round in HIIIPlbullbull collected of your cranberry bo9 downatrabull of the Picillo haaartolle wut a dup Jta in Coventry RhOda Ishnd However andyaaa of lea collected in the bull-P IPF02al adjacent t o thia tu indishy~ted the pre~ of the followinqbull

1 11-tridlloroethana 1600 ppb t richlocoethylane U Oppb

510 Pllb tol~Mna 1400 ppb MUylane ctlorida 840 ppb

tatuchloroethylane 250 ppb ethyl beftaeM 700 ppb

ylene u---nl 1700 ppb chlorofom 1000 ppb

1

5625 ppb

Aleo prnt but not q~~utltated were acetone MU a nd HIBK u well u ul unidentified ~nda

At praHnt tbia ancy h inithtin9 a atudy of pract icable optionbull on conui_t of thb leachllte siM~llhneoudy with buried dr u111 r~bulll actilitiea beint conducted by the IUiode I s bncl Dept o f Environshybullental M~t IPA h 1bo fundinq a hydroqeol09ical s tudy o f thh uebull wtlldl ahOuW prcwlda additional information such that we will be able to aaMbullbull potantill l ontmiddot tbullrbull effecta on the downatreu drainage

)

J I

r

ATlAOMENl 8 3

UNITED STATES ENVIRONMENTAL PROTECTION AGENCY lt(GIONI

IOWIITVIIWITIII Ilf LI bull INGJON MASIACHUIETTII21Jl

middot

July a ltiO

Dr M Starr ac~n lpu y Cranberry copny aD l~o~Uding lrldtbull ltreat Mld4bboro MA OU41

oar Dr I Urt l

Aa diMY-cl on July 1 no detectable levela of o r9anica wan round in HIIIPlbullbull collected of your cranberry bo9 downatrabull of the Picillo haaartolle wut a dup Jta in Coventry RhOda Ishnd However andyaaa of lea collected in the bull-P IPF02al adjacent t o thia tu indishy~ted the pre~ of the followinqbull

1 11-tridlloroethana 1600 ppb t richlocoethylane U Oppb

510 Pllb tol~Mna 1400 ppb MUylane ctlorida 840 ppb

tatuchloroethylane 250 ppb ethyl beftaeM 700 ppb

ylene u---nl 1700 ppb chlorofom 1000 ppb

1

5625 ppb

Aleo prnt but not q~~utltated were acetone MU a nd HIBK u well u ul unidentified ~nda

At praHnt tbia ancy h inithtin9 a atudy of pract icable optionbull on conui_t of thb leachllte siM~llhneoudy with buried dr u111 r~bulll actilitiea beint conducted by the IUiode I s bncl Dept o f Environshybullental M~t IPA h 1bo fundinq a hydroqeol09ical s tudy o f thh uebull wtlldl ahOuW prcwlda additional information such that we will be able to aaMbullbull potantill l ontmiddot tbullrbull effecta on the downatreu drainage

)

J I

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-All10foffNl B )

-middotshyflture -pliftll aM analyua wMft bullnilable will be f o rwuded to you tleue call if 1 can C of further ahtance

11nceuly

lnvlrD~W~Htal lclantht OU bull u rtoua Matar iab lection

r

AlI10MENl 83

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-n = =Ul

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ATr10f4ENl B 4

Tetrachlor1deltl pJIb ~o f D bull 6 3 b Tttrachloroethylenebulll ppb Tr2i~~pound~__ _ 4139 11-iri cloroellneltl ppb

-

L

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ATlJOfoiENI 8 4 bull

h

c- Totnchlor1cle~l ppll - ~ F bulls 3 eTotnchl-tloyl_l ppb

lil~==~~If _ _

l ~y-~~middotmiddot

_jL

--- -----

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AllNlMENT 8 4

o 6 3 SJ ~ _

41396 71 ehlorootltyllloo 1600 ppb MS l~Trfehloroetlar Jltl pptt

P1111 c ~ -1

John OU1nn

l

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1. barcode 575200
2. barcodetext SDMS Doc ID 575200

r

AlI10MENl 83

~ ~~

-n = =Ul

r

ATr10f4ENl B 4

Tetrachlor1deltl pJIb ~o f D bull 6 3 b Tttrachloroethylenebulll ppb Tr2i~~pound~__ _ 4139 11-iri cloroellneltl ppb

-

L

r __

ATlJOfoiENI 8 4 bull

h

c- Totnchlor1cle~l ppll - ~ F bulls 3 eTotnchl-tloyl_l ppb

lil~==~~If _ _

l ~y-~~middotmiddot

_jL

--- -----

r

AllNlMENT 8 4

o 6 3 SJ ~ _

41396 71 ehlorootltyllloo 1600 ppb MS l~Trfehloroetlar Jltl pptt

P1111 c ~ -1

John OU1nn

l

r

1. barcode 575200
2. barcodetext SDMS Doc ID 575200

r

ATr10f4ENl B 4

Tetrachlor1deltl pJIb ~o f D bull 6 3 b Tttrachloroethylenebulll ppb Tr2i~~pound~__ _ 4139 11-iri cloroellneltl ppb

-

L

r __

ATlJOfoiENI 8 4 bull

h

c- Totnchlor1cle~l ppll - ~ F bulls 3 eTotnchl-tloyl_l ppb

lil~==~~If _ _

l ~y-~~middotmiddot

_jL

--- -----

r

AllNlMENT 8 4

o 6 3 SJ ~ _

41396 71 ehlorootltyllloo 1600 ppb MS l~Trfehloroetlar Jltl pptt

P1111 c ~ -1

John OU1nn

l

r

1. barcode 575200
2. barcodetext SDMS Doc ID 575200

r __

ATlJOfoiENI 8 4 bull

h

c- Totnchlor1cle~l ppll - ~ F bulls 3 eTotnchl-tloyl_l ppb

lil~==~~If _ _

l ~y-~~middotmiddot

_jL

--- -----

r

AllNlMENT 8 4

o 6 3 SJ ~ _

41396 71 ehlorootltyllloo 1600 ppb MS l~Trfehloroetlar Jltl pptt

P1111 c ~ -1

John OU1nn

l

r

1. barcode 575200
2. barcodetext SDMS Doc ID 575200

r

AllNlMENT 8 4

o 6 3 SJ ~ _

41396 71 ehlorootltyllloo 1600 ppb MS l~Trfehloroetlar Jltl pptt

P1111 c ~ -1

John OU1nn

l

r

1. barcode 575200
2. barcodetext SDMS Doc ID 575200

r

1. barcode 575200
2. barcodetext SDMS Doc ID 575200