letter providing comments on revised soil leaching … · balsam environmental consultants, inc....
TRANSCRIPT
^-bull^^---^bullis Center S
BRr K H^X
ABALSAM ^ I ^ W N ENVIRONMENTAL CONSULTANTS INC
Engineering Environmental Science amp Industrial Hygiene
SDMS DocID 469118 5 Industrial Way
Salem NH 03079
(603) 893-0616
June 15 1990 Balsam Project 6185826
Mr Roger Duwart Project Manager New Hampshire Superfund Section US Environmental Protection Agency Region 1 90 Canal Street Boston Massachusetts 02203
RE Soil Leaching Study Protocol Mottolo Superfund Site RIFS Raymond New Hampshire
Dear Mr Duwart
This letter is to respond as you requested to comments received from you by telephone facsimile transmission on May 16 1990 regarding the soil leaching study protocol transmitted to you on May 1 1990 For clarity the comments and questions raised by EPAs reviewers are included
Super fund Suppor t Section Comments
Comment Cover letter What is the scientific literature that is referred to Citations should be provided
Response The reference to scientific literature in the cover letter transmitting the revised study protocol was related specifically to discussion of desorption studies using batch test methods Specific discussion of or references to difficulties of using batch methods to evaluate contaminant desorption from soil and sediments was presented in papers by Curtis et al and Schwarzenbach and Westall (see references 2 and 9 respectively in attached list)
Comment page 4 Balsam should be made aware of the Regions use of the Somers model when evaluating the need to conduct soil clean-up
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 2
levels The Somers model makes use of partition coefficients fraction of organic carbon aquifer properties and precipitation to evaluate clean-up levels for soils
Response Balsam acknowledges the comment The objective of the leaching study is to assess the ability of the downgradient soils to act as a subsidiary source of VOCs released to ground water as it may affect subsequent restoration of grovmd water It is not intended to establish soil cleanup levels although data obtained from the study may be used to evaluate action levels in which case the Somers model will be considered
Comment page 5 What reference list
Response The reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment page 7 Comment Based on Balsams description of VOC in soils an immiscible phase paradigm seems appropriate for this site Future conceptual model should evaluate this further
Response Data obtained during the remedial investigation (RI) did not indicate the presence of immiscible phases at the site Levels of VOCs detected in ground water samples from the site did not approach the concentrations that would considered to be indicative of possible immiscible dense non-aqueous phase liquid (DNAPL) phases (ie approximately 10 percent of individual DNAPL compound solubility limits) nor was visible evidence of immiscible floating phases observed during sampling of the monitoring wells
Comment page 9 Which up-gradient well will be used
Response Ground water to be used as the leaching medium will be obtained from the on-site water supply well (DW-1) located in the shed upgradient of the former drum disposal area This well is a dug well installed in the overburden Evaluation of development and purging data for upgradient overburden monitoring well MW-7S which was originally considered as a source for leaching study water indicated that recovery was too slow to be practicably used to collect the volumes of leaching water required for the study The dug well however has adequate storage to provide the required volume of water
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 3
To evaluate its suitability for use water samples were collected from well DW-1 on May 10 1990 and submitted for Level III laboratory analysis for Hazardous Substance List (HSL) parameters and the general water quality parameters nitrate and nitrite nitrogen alkalinity chloride sulfate biochemical oxygen demand (BOD) chemical oxygen demand (COD) total organic carbon (TOC) and total and fecal coliform HSL VOCs semi-volatile organic compounds pesticides and polychlorinated biphenyls and cyanide BOD COD TOC nitrite-nitrogen and total and fecal coliform were not detected in the samples collected from well DW-1 Of the 23 HSL metals analyzed 15 were not detected in the sample from the dug well The seven HSL metals detected were generally present at relatively low concentrations (less than 05 mg1) or were at levels within the ranges observed in samples from overburden monitoring wells located in the vicinity of the former disposal area or upgradient of the area The reported levels of the general water quality parameters detected were generally consistent with the ranges of values for these parameters that were detected in samples from other overburden wells as previously described The reported data were validated in accordance with the data validation procedures used for other ground water samples Copies of the laboratory reports are attached
Comment page 10 How much time will elapse between sampling in the field shipment to lab transfer to a permeameter transfer to another appropriate (what is that) container shipment to a lab and finally analysis
Response Soil samples collected in the field are planned to be transferred to the leaching study laboratory no later than the day after collection The study program calls for one sample to immediately be set up in the test system and its permeability tested It is anticipated that the initial permeability testing will be completed within 2 days at the conclusion of which testing of the leaching samples will be initiated at intervals of 1 day to allow adjustment of leaching conditions if warranted based upon the results of previous samples Accordingly allowing for a possible intervening weekend no more than 9 days are expected to elapse between sample collection in the field and sample set up in a test permeameter for a given sample
On completion of permeameter setup the soil samples intended for baseline laboratory analysis will immediately be transferred to glass jars of appropriate size as determined by the size of the sample in the permeameter and delivered to the analytical laboratory that day
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 4
The analytical laboratory is located approximately 20 minutes driving time from the leaching study laboratory Accordingly no more than 9 days are expected to elapse between collection in the field and delivery of a given baseline sample to the analytical laboratory
The date and time of collection of a given sample will be noted on the chain-of-custody form that accompanies the sample to the analjrtical laboratory Analyses are to be completed within 14 days of the date of collection as established by the Mottolo Project Operations Plan (POP)
Comment page 13 The first pore volume will be useful to evaluate partition coefficients also
Response The comment is acknowledged
Comment page 14 I suggest a control sample As I understand it one portion of soil will be sent to a lab immediately and a second will be subjected to the leach studies The second sample will be sent for analysis at the conclusion of the leach procedure I suggest that a third sample be kept in the leaching lab and sent out for analysis at the end of the leaching procedure This would give an indication of sample degradation during the leaching procedure
Response The initial sample will be handled the same as the leaching sample through set up in the permeameter to assess possible loss of VOCs from sample handling during set up The leaching sample will be in a system that excludes air limiting the possibility of vaporization of VOCs from the sample The permeameter will be surrounded by water that is under pressure and it is expected that migration of VOCs to the pressurizing water will be minimal especially given the relatively high flow rate of leaching water through the sample However the water in the pressure vessel outside the permeameter will be sampled at the conclusion of the leaching study and analyzed for HSL VOCs by EPA Method 624 to assess possible loss of VOCs through the permeameter membrane In summary it is expected that VOCs will be preferentially transferred from the sample to the water leached through the sample with minimal loss of VOCs to other media and that other control and check samples will provide adequate information to assess possible sample degradation
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 5
CDM Fede ra l P r o g r a m s Corpora t ion Comments
Comment Section 20 Approach Development Balsam has not attached the list of scientific references used in their literature review please provide
Response As previously discussed the reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment Section 311 Sampling Locations FPC believes that Balsam should clarify the statement Leaching results for the other three samples will be used to assess their potential to act as a VOC source Balsam states in Section 34 page 12 that four samples will undergo leaching the fourth sample is a field duplicate and will be leached at a flow rate half that of its duplicate to provide data for assessment of possible effects of the increased flow rates required to model the desired leaching period in the test time frame
Response Section 311 incorrectly referenced leaching of three samples Section 34 correctly described the number of samples to be leached as four one of which will be a duplicate sample leached at half the flow rate used for its duplicate as discussed in the sentence quoted by CDM
Comment Section 351 Leachate FPC believes that it should be a requirement for Balsam to analyze the leaching influent for HSL VOCs Balsam eludes [sic] to the fact that VOCs may diffuse from the sample back into the leaching reservoir thereby contaminating the influent Therefore samples should be analyzed on a regular schedule possibly one sample per week
Response As discussed in Section 32 ground water in the leaching medium reservoir will be replaced every 2 to 3 days with fresh ground water collected from the site to limit the effects of possible changes in ground water chemistry It is expected that this schedule of leaching medium replenishment coupled with the relatively high gradients induced into the test systems (ie 4 times greater than those in the field) will limit potential back-diffusion of VOCs from the sample to the leaching medium reservoir Furthermore as the leaching study proceeds the amount of VOCs present in the leaching samples will decrease reducing the concentration gradient between leaching water in the sample pore spaces and in the reservoir which is the potential driving force for back-diffusion Nevertheless up to 2 leaching medium samples will be collected from reservoirs early in the study to assess this potential problem The need for additional reservoir
3865
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 6
samples will be assessed based upon the results obtained for the initial samples
Please feel free to contact us if you have questions or comments regarding the information in this letter
Sincerely
y^ii^ M j i A Gilbert PE
sfasibility Study Manager
Leonard C Sarapas PE Project Manager Vice President Engineering
enclosures
cc J Peltonen M Robinette NHDES
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 2
levels The Somers model makes use of partition coefficients fraction of organic carbon aquifer properties and precipitation to evaluate clean-up levels for soils
Response Balsam acknowledges the comment The objective of the leaching study is to assess the ability of the downgradient soils to act as a subsidiary source of VOCs released to ground water as it may affect subsequent restoration of grovmd water It is not intended to establish soil cleanup levels although data obtained from the study may be used to evaluate action levels in which case the Somers model will be considered
Comment page 5 What reference list
Response The reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment page 7 Comment Based on Balsams description of VOC in soils an immiscible phase paradigm seems appropriate for this site Future conceptual model should evaluate this further
Response Data obtained during the remedial investigation (RI) did not indicate the presence of immiscible phases at the site Levels of VOCs detected in ground water samples from the site did not approach the concentrations that would considered to be indicative of possible immiscible dense non-aqueous phase liquid (DNAPL) phases (ie approximately 10 percent of individual DNAPL compound solubility limits) nor was visible evidence of immiscible floating phases observed during sampling of the monitoring wells
Comment page 9 Which up-gradient well will be used
Response Ground water to be used as the leaching medium will be obtained from the on-site water supply well (DW-1) located in the shed upgradient of the former drum disposal area This well is a dug well installed in the overburden Evaluation of development and purging data for upgradient overburden monitoring well MW-7S which was originally considered as a source for leaching study water indicated that recovery was too slow to be practicably used to collect the volumes of leaching water required for the study The dug well however has adequate storage to provide the required volume of water
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 3
To evaluate its suitability for use water samples were collected from well DW-1 on May 10 1990 and submitted for Level III laboratory analysis for Hazardous Substance List (HSL) parameters and the general water quality parameters nitrate and nitrite nitrogen alkalinity chloride sulfate biochemical oxygen demand (BOD) chemical oxygen demand (COD) total organic carbon (TOC) and total and fecal coliform HSL VOCs semi-volatile organic compounds pesticides and polychlorinated biphenyls and cyanide BOD COD TOC nitrite-nitrogen and total and fecal coliform were not detected in the samples collected from well DW-1 Of the 23 HSL metals analyzed 15 were not detected in the sample from the dug well The seven HSL metals detected were generally present at relatively low concentrations (less than 05 mg1) or were at levels within the ranges observed in samples from overburden monitoring wells located in the vicinity of the former disposal area or upgradient of the area The reported levels of the general water quality parameters detected were generally consistent with the ranges of values for these parameters that were detected in samples from other overburden wells as previously described The reported data were validated in accordance with the data validation procedures used for other ground water samples Copies of the laboratory reports are attached
Comment page 10 How much time will elapse between sampling in the field shipment to lab transfer to a permeameter transfer to another appropriate (what is that) container shipment to a lab and finally analysis
Response Soil samples collected in the field are planned to be transferred to the leaching study laboratory no later than the day after collection The study program calls for one sample to immediately be set up in the test system and its permeability tested It is anticipated that the initial permeability testing will be completed within 2 days at the conclusion of which testing of the leaching samples will be initiated at intervals of 1 day to allow adjustment of leaching conditions if warranted based upon the results of previous samples Accordingly allowing for a possible intervening weekend no more than 9 days are expected to elapse between sample collection in the field and sample set up in a test permeameter for a given sample
On completion of permeameter setup the soil samples intended for baseline laboratory analysis will immediately be transferred to glass jars of appropriate size as determined by the size of the sample in the permeameter and delivered to the analytical laboratory that day
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 4
The analytical laboratory is located approximately 20 minutes driving time from the leaching study laboratory Accordingly no more than 9 days are expected to elapse between collection in the field and delivery of a given baseline sample to the analytical laboratory
The date and time of collection of a given sample will be noted on the chain-of-custody form that accompanies the sample to the analjrtical laboratory Analyses are to be completed within 14 days of the date of collection as established by the Mottolo Project Operations Plan (POP)
Comment page 13 The first pore volume will be useful to evaluate partition coefficients also
Response The comment is acknowledged
Comment page 14 I suggest a control sample As I understand it one portion of soil will be sent to a lab immediately and a second will be subjected to the leach studies The second sample will be sent for analysis at the conclusion of the leach procedure I suggest that a third sample be kept in the leaching lab and sent out for analysis at the end of the leaching procedure This would give an indication of sample degradation during the leaching procedure
Response The initial sample will be handled the same as the leaching sample through set up in the permeameter to assess possible loss of VOCs from sample handling during set up The leaching sample will be in a system that excludes air limiting the possibility of vaporization of VOCs from the sample The permeameter will be surrounded by water that is under pressure and it is expected that migration of VOCs to the pressurizing water will be minimal especially given the relatively high flow rate of leaching water through the sample However the water in the pressure vessel outside the permeameter will be sampled at the conclusion of the leaching study and analyzed for HSL VOCs by EPA Method 624 to assess possible loss of VOCs through the permeameter membrane In summary it is expected that VOCs will be preferentially transferred from the sample to the water leached through the sample with minimal loss of VOCs to other media and that other control and check samples will provide adequate information to assess possible sample degradation
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 5
CDM Fede ra l P r o g r a m s Corpora t ion Comments
Comment Section 20 Approach Development Balsam has not attached the list of scientific references used in their literature review please provide
Response As previously discussed the reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment Section 311 Sampling Locations FPC believes that Balsam should clarify the statement Leaching results for the other three samples will be used to assess their potential to act as a VOC source Balsam states in Section 34 page 12 that four samples will undergo leaching the fourth sample is a field duplicate and will be leached at a flow rate half that of its duplicate to provide data for assessment of possible effects of the increased flow rates required to model the desired leaching period in the test time frame
Response Section 311 incorrectly referenced leaching of three samples Section 34 correctly described the number of samples to be leached as four one of which will be a duplicate sample leached at half the flow rate used for its duplicate as discussed in the sentence quoted by CDM
Comment Section 351 Leachate FPC believes that it should be a requirement for Balsam to analyze the leaching influent for HSL VOCs Balsam eludes [sic] to the fact that VOCs may diffuse from the sample back into the leaching reservoir thereby contaminating the influent Therefore samples should be analyzed on a regular schedule possibly one sample per week
Response As discussed in Section 32 ground water in the leaching medium reservoir will be replaced every 2 to 3 days with fresh ground water collected from the site to limit the effects of possible changes in ground water chemistry It is expected that this schedule of leaching medium replenishment coupled with the relatively high gradients induced into the test systems (ie 4 times greater than those in the field) will limit potential back-diffusion of VOCs from the sample to the leaching medium reservoir Furthermore as the leaching study proceeds the amount of VOCs present in the leaching samples will decrease reducing the concentration gradient between leaching water in the sample pore spaces and in the reservoir which is the potential driving force for back-diffusion Nevertheless up to 2 leaching medium samples will be collected from reservoirs early in the study to assess this potential problem The need for additional reservoir
3865
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 6
samples will be assessed based upon the results obtained for the initial samples
Please feel free to contact us if you have questions or comments regarding the information in this letter
Sincerely
y^ii^ M j i A Gilbert PE
sfasibility Study Manager
Leonard C Sarapas PE Project Manager Vice President Engineering
enclosures
cc J Peltonen M Robinette NHDES
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 3
To evaluate its suitability for use water samples were collected from well DW-1 on May 10 1990 and submitted for Level III laboratory analysis for Hazardous Substance List (HSL) parameters and the general water quality parameters nitrate and nitrite nitrogen alkalinity chloride sulfate biochemical oxygen demand (BOD) chemical oxygen demand (COD) total organic carbon (TOC) and total and fecal coliform HSL VOCs semi-volatile organic compounds pesticides and polychlorinated biphenyls and cyanide BOD COD TOC nitrite-nitrogen and total and fecal coliform were not detected in the samples collected from well DW-1 Of the 23 HSL metals analyzed 15 were not detected in the sample from the dug well The seven HSL metals detected were generally present at relatively low concentrations (less than 05 mg1) or were at levels within the ranges observed in samples from overburden monitoring wells located in the vicinity of the former disposal area or upgradient of the area The reported levels of the general water quality parameters detected were generally consistent with the ranges of values for these parameters that were detected in samples from other overburden wells as previously described The reported data were validated in accordance with the data validation procedures used for other ground water samples Copies of the laboratory reports are attached
Comment page 10 How much time will elapse between sampling in the field shipment to lab transfer to a permeameter transfer to another appropriate (what is that) container shipment to a lab and finally analysis
Response Soil samples collected in the field are planned to be transferred to the leaching study laboratory no later than the day after collection The study program calls for one sample to immediately be set up in the test system and its permeability tested It is anticipated that the initial permeability testing will be completed within 2 days at the conclusion of which testing of the leaching samples will be initiated at intervals of 1 day to allow adjustment of leaching conditions if warranted based upon the results of previous samples Accordingly allowing for a possible intervening weekend no more than 9 days are expected to elapse between sample collection in the field and sample set up in a test permeameter for a given sample
On completion of permeameter setup the soil samples intended for baseline laboratory analysis will immediately be transferred to glass jars of appropriate size as determined by the size of the sample in the permeameter and delivered to the analytical laboratory that day
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 4
The analytical laboratory is located approximately 20 minutes driving time from the leaching study laboratory Accordingly no more than 9 days are expected to elapse between collection in the field and delivery of a given baseline sample to the analytical laboratory
The date and time of collection of a given sample will be noted on the chain-of-custody form that accompanies the sample to the analjrtical laboratory Analyses are to be completed within 14 days of the date of collection as established by the Mottolo Project Operations Plan (POP)
Comment page 13 The first pore volume will be useful to evaluate partition coefficients also
Response The comment is acknowledged
Comment page 14 I suggest a control sample As I understand it one portion of soil will be sent to a lab immediately and a second will be subjected to the leach studies The second sample will be sent for analysis at the conclusion of the leach procedure I suggest that a third sample be kept in the leaching lab and sent out for analysis at the end of the leaching procedure This would give an indication of sample degradation during the leaching procedure
Response The initial sample will be handled the same as the leaching sample through set up in the permeameter to assess possible loss of VOCs from sample handling during set up The leaching sample will be in a system that excludes air limiting the possibility of vaporization of VOCs from the sample The permeameter will be surrounded by water that is under pressure and it is expected that migration of VOCs to the pressurizing water will be minimal especially given the relatively high flow rate of leaching water through the sample However the water in the pressure vessel outside the permeameter will be sampled at the conclusion of the leaching study and analyzed for HSL VOCs by EPA Method 624 to assess possible loss of VOCs through the permeameter membrane In summary it is expected that VOCs will be preferentially transferred from the sample to the water leached through the sample with minimal loss of VOCs to other media and that other control and check samples will provide adequate information to assess possible sample degradation
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 5
CDM Fede ra l P r o g r a m s Corpora t ion Comments
Comment Section 20 Approach Development Balsam has not attached the list of scientific references used in their literature review please provide
Response As previously discussed the reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment Section 311 Sampling Locations FPC believes that Balsam should clarify the statement Leaching results for the other three samples will be used to assess their potential to act as a VOC source Balsam states in Section 34 page 12 that four samples will undergo leaching the fourth sample is a field duplicate and will be leached at a flow rate half that of its duplicate to provide data for assessment of possible effects of the increased flow rates required to model the desired leaching period in the test time frame
Response Section 311 incorrectly referenced leaching of three samples Section 34 correctly described the number of samples to be leached as four one of which will be a duplicate sample leached at half the flow rate used for its duplicate as discussed in the sentence quoted by CDM
Comment Section 351 Leachate FPC believes that it should be a requirement for Balsam to analyze the leaching influent for HSL VOCs Balsam eludes [sic] to the fact that VOCs may diffuse from the sample back into the leaching reservoir thereby contaminating the influent Therefore samples should be analyzed on a regular schedule possibly one sample per week
Response As discussed in Section 32 ground water in the leaching medium reservoir will be replaced every 2 to 3 days with fresh ground water collected from the site to limit the effects of possible changes in ground water chemistry It is expected that this schedule of leaching medium replenishment coupled with the relatively high gradients induced into the test systems (ie 4 times greater than those in the field) will limit potential back-diffusion of VOCs from the sample to the leaching medium reservoir Furthermore as the leaching study proceeds the amount of VOCs present in the leaching samples will decrease reducing the concentration gradient between leaching water in the sample pore spaces and in the reservoir which is the potential driving force for back-diffusion Nevertheless up to 2 leaching medium samples will be collected from reservoirs early in the study to assess this potential problem The need for additional reservoir
3865
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 6
samples will be assessed based upon the results obtained for the initial samples
Please feel free to contact us if you have questions or comments regarding the information in this letter
Sincerely
y^ii^ M j i A Gilbert PE
sfasibility Study Manager
Leonard C Sarapas PE Project Manager Vice President Engineering
enclosures
cc J Peltonen M Robinette NHDES
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 4
The analytical laboratory is located approximately 20 minutes driving time from the leaching study laboratory Accordingly no more than 9 days are expected to elapse between collection in the field and delivery of a given baseline sample to the analytical laboratory
The date and time of collection of a given sample will be noted on the chain-of-custody form that accompanies the sample to the analjrtical laboratory Analyses are to be completed within 14 days of the date of collection as established by the Mottolo Project Operations Plan (POP)
Comment page 13 The first pore volume will be useful to evaluate partition coefficients also
Response The comment is acknowledged
Comment page 14 I suggest a control sample As I understand it one portion of soil will be sent to a lab immediately and a second will be subjected to the leach studies The second sample will be sent for analysis at the conclusion of the leach procedure I suggest that a third sample be kept in the leaching lab and sent out for analysis at the end of the leaching procedure This would give an indication of sample degradation during the leaching procedure
Response The initial sample will be handled the same as the leaching sample through set up in the permeameter to assess possible loss of VOCs from sample handling during set up The leaching sample will be in a system that excludes air limiting the possibility of vaporization of VOCs from the sample The permeameter will be surrounded by water that is under pressure and it is expected that migration of VOCs to the pressurizing water will be minimal especially given the relatively high flow rate of leaching water through the sample However the water in the pressure vessel outside the permeameter will be sampled at the conclusion of the leaching study and analyzed for HSL VOCs by EPA Method 624 to assess possible loss of VOCs through the permeameter membrane In summary it is expected that VOCs will be preferentially transferred from the sample to the water leached through the sample with minimal loss of VOCs to other media and that other control and check samples will provide adequate information to assess possible sample degradation
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 5
CDM Fede ra l P r o g r a m s Corpora t ion Comments
Comment Section 20 Approach Development Balsam has not attached the list of scientific references used in their literature review please provide
Response As previously discussed the reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment Section 311 Sampling Locations FPC believes that Balsam should clarify the statement Leaching results for the other three samples will be used to assess their potential to act as a VOC source Balsam states in Section 34 page 12 that four samples will undergo leaching the fourth sample is a field duplicate and will be leached at a flow rate half that of its duplicate to provide data for assessment of possible effects of the increased flow rates required to model the desired leaching period in the test time frame
Response Section 311 incorrectly referenced leaching of three samples Section 34 correctly described the number of samples to be leached as four one of which will be a duplicate sample leached at half the flow rate used for its duplicate as discussed in the sentence quoted by CDM
Comment Section 351 Leachate FPC believes that it should be a requirement for Balsam to analyze the leaching influent for HSL VOCs Balsam eludes [sic] to the fact that VOCs may diffuse from the sample back into the leaching reservoir thereby contaminating the influent Therefore samples should be analyzed on a regular schedule possibly one sample per week
Response As discussed in Section 32 ground water in the leaching medium reservoir will be replaced every 2 to 3 days with fresh ground water collected from the site to limit the effects of possible changes in ground water chemistry It is expected that this schedule of leaching medium replenishment coupled with the relatively high gradients induced into the test systems (ie 4 times greater than those in the field) will limit potential back-diffusion of VOCs from the sample to the leaching medium reservoir Furthermore as the leaching study proceeds the amount of VOCs present in the leaching samples will decrease reducing the concentration gradient between leaching water in the sample pore spaces and in the reservoir which is the potential driving force for back-diffusion Nevertheless up to 2 leaching medium samples will be collected from reservoirs early in the study to assess this potential problem The need for additional reservoir
3865
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 6
samples will be assessed based upon the results obtained for the initial samples
Please feel free to contact us if you have questions or comments regarding the information in this letter
Sincerely
y^ii^ M j i A Gilbert PE
sfasibility Study Manager
Leonard C Sarapas PE Project Manager Vice President Engineering
enclosures
cc J Peltonen M Robinette NHDES
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 5
CDM Fede ra l P r o g r a m s Corpora t ion Comments
Comment Section 20 Approach Development Balsam has not attached the list of scientific references used in their literature review please provide
Response As previously discussed the reference list was inadvertently omitted from the revised protocol and is enclosed with this letter
Comment Section 311 Sampling Locations FPC believes that Balsam should clarify the statement Leaching results for the other three samples will be used to assess their potential to act as a VOC source Balsam states in Section 34 page 12 that four samples will undergo leaching the fourth sample is a field duplicate and will be leached at a flow rate half that of its duplicate to provide data for assessment of possible effects of the increased flow rates required to model the desired leaching period in the test time frame
Response Section 311 incorrectly referenced leaching of three samples Section 34 correctly described the number of samples to be leached as four one of which will be a duplicate sample leached at half the flow rate used for its duplicate as discussed in the sentence quoted by CDM
Comment Section 351 Leachate FPC believes that it should be a requirement for Balsam to analyze the leaching influent for HSL VOCs Balsam eludes [sic] to the fact that VOCs may diffuse from the sample back into the leaching reservoir thereby contaminating the influent Therefore samples should be analyzed on a regular schedule possibly one sample per week
Response As discussed in Section 32 ground water in the leaching medium reservoir will be replaced every 2 to 3 days with fresh ground water collected from the site to limit the effects of possible changes in ground water chemistry It is expected that this schedule of leaching medium replenishment coupled with the relatively high gradients induced into the test systems (ie 4 times greater than those in the field) will limit potential back-diffusion of VOCs from the sample to the leaching medium reservoir Furthermore as the leaching study proceeds the amount of VOCs present in the leaching samples will decrease reducing the concentration gradient between leaching water in the sample pore spaces and in the reservoir which is the potential driving force for back-diffusion Nevertheless up to 2 leaching medium samples will be collected from reservoirs early in the study to assess this potential problem The need for additional reservoir
3865
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 6
samples will be assessed based upon the results obtained for the initial samples
Please feel free to contact us if you have questions or comments regarding the information in this letter
Sincerely
y^ii^ M j i A Gilbert PE
sfasibility Study Manager
Leonard C Sarapas PE Project Manager Vice President Engineering
enclosures
cc J Peltonen M Robinette NHDES
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
3865
BALSAM ENVIRONMENTAL CONSULTANTS INC
Balsam Project 6185826 June 15 1990 Page 6
samples will be assessed based upon the results obtained for the initial samples
Please feel free to contact us if you have questions or comments regarding the information in this letter
Sincerely
y^ii^ M j i A Gilbert PE
sfasibility Study Manager
Leonard C Sarapas PE Project Manager Vice President Engineering
enclosures
cc J Peltonen M Robinette NHDES
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
1) Bouchard DC et al Sorption Nonequilibrium During Solute Transport Journal of Contaminant Hydrology Vol 2 pp 209-223 1988
2) Curtis GP et alA Natural Gradient Experiment on Solute Transport in a Sand Aquifer 4 Sorption of Organic Solutes and its Influence on Mobility Water Resources Research Vol 22 No 13 pp 2059-2067 December 1986
3) Fetter CW Applied Hvdrogeologv 2nd ed Merrill Publishing Company Toronto 1988 pp397-400
4) Freeze R and Cherry J Groundwater Prentice-Hall Inc Englewood Cliffs New Jersey 1979 pp 432-434
5) Hunt JR et al Nonaqueous Phase Liquid Transport and Cleanup Water Resources Research Vol 24 No 8 pp 1247-1269 August 1988
6) Hutzler NJ et al Transport of Organic Compounds With Saturated Groundwater Flow Experimental Results Water Resources Research Vol 22 No 3 pp 285-295 March 1986
7) Lee LS et al Nonequilibrium Sorption of Organic Contaminants During Flow Through Columns of Aquifer Materials Environmental Toxicology and Chemistry Vol 7 No 10 pp779-793 1988
8) Oliver BG Desorption of Chlorinated Hydrocarbons from Spiked and Anthropogenically Contaminated Sediments Chemosphere Vol 14 No 8 pp 1087-1106 1985
9) Schwarzenbach RP and Westall J Transport of Nonpolar Organic Compounds from Surface Water to Groundwater Laboratory Sorption Studies Environmental Science amp Technology Vol 15 No 11 pp 1360shy1367 November 1981
10) Staples CA and Geiselmann SJ Cosolvent Influences on Organic Solute Retardation Factors Ground Water Vol 26 No2 pp 192-198 March-April 1988
May 1 1990 Balsam Project 61858263102a
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
BALSAM ENVIRONMENTAL CONSULTANTS INC
REFERENCES (continued) SOIL LEACHING STUDY PROTOCOL
MOTTOLO SUPERFUND SITE RAYMOND NEW HAMPSHIRE
11) US Environmental Protection Agency Determining Soil Response Action Levels Based on Potential Contaminant Migration to Ground Water A Compendium of Examples EPA5402-89057 October 1989
12) Wu S and Gschwend PM Sorption Kinetics of Hydrophobic Organic Compounds to Natural Sediments and Soils Environmental Science amp Technology Vol 20 No 7 pp 717-725 July 1986
May 1 1990 Balsam Project 61858263102a
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
A BALSAM ^ ^ ENVIRONMENTAL CONSULTANTS INC
5 Industrial Way Salem NH 03079 (603) 893-0616
MEMORANDUM OF TRANSMITTAL DATE June 20 1990
PROJECT 6185826
TO Roger Duwart RE Soil Leaching Study Protocol USEPA Region I Mottolo Superfund Site RIFS NH Superfund Section 90 Canal Street Boston MA 02203
ENCLOSED - THE FOLLOWING
X Analytical Data
Report Copies
Plans
Instructions and Requests
REMARKS Enclosed data were inadvertantly omitted from response to comments on protocol referenced above
BY
A G i l b e r t P E l i b i l i t y Manager
(1592)
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
73 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 25 May 1990 Aquatec Lab No 114675 ETRNor 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heotachlcr epoxide achlordane Rchlordane
Balsam Environmental Consultants Inc labeled DW-1 51090 at 0840 hours
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b-BHC d-BHC p-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
water sample
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U 050 U 050 U 050 U 10 U
050 U
Dibutyl Chlorendate Surrogate Recovery 74
Key to the letters used to qualify the results of the analysis
The compound was analyzed for but not detected The number is the detection limit for the compound
C - The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No PBLKB3 ETR No 21371 Project 90000 Sample Received On Sample Identification
aldrin dieldrin 44-DDT 44-DDE 44-DDD a-endosulfan b-endosulfan endosulfan sulfate endrin endrin ketone heptachlor heptachlor epoxide achlordane gchlordane
Method Blank for Aquatec Lab No 114675
Pesticides and PCBs in ugL EPA Method 608
005 U 010 U 010 U 010 U 010 U 005 U 010 U 010 U 010 U 010 U 005 U 005 U 050 U 050 U
a-BHC b^BHC d-BHC g-BHC (lindane) methoxychlor toxaphene PCB-1242 PCB-1254 PCB-1221 PCB-1232 PCB-1248 PCB-1260 PCB-1016
005 U 005 U 005 U 005 U 050 U 10 U 050 U 10 U
050 U 050 U 050 U 10 U 050 U
Dibutyl Chlorendate Surrogate Recovery 84
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for but not detected The number is the detection limit for the compound
The result has been corrected for the presence of the comshypound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Da te 0 6 0 5 9 0
Balsam E n v i r o n m e n t a l ETR Number 21371 C o n s u l t a n t s I n c P r o j e c t N o 90000 5 I n d u s t r i a l Way No S a m p l e s 2 Sa lem NH 03079 A r r i v e d 0 5 1 1 9 0
A t t e n t i o n B r i a n Q u i n l a n 1
Page 1
standard analyses were performed in accordance with Methods for Analysis of Uater atxi Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examinati on of Water and Wastewater
All results are in mgl unless othe rwise noted
Lab No Sample D e s c r i p t i o n
114675 DW- l 05 10 90 0840(Water)
Method No P a r a m e t e r R e s u l t
2 0 0 7 Aluminum T o t a l lt 0 0 5 1 2 0 4 2 Antimony T o t a l lt0-06
2 0 6 2 A r s e n i c T o t a l lt 0 -0 1 2 0 0 7 Barium T o t a l lt0 02 2 0 0 7 B e r y l l i u m T o t a l lt 0 0 1 2 0 0 7 Cadmium T o t a l lt 0 - 0 1 2 0 0 7 Calc ium T o t a l 5 2 200-7 Chromium T o t a l lt0 02 2 0 0 7 C o b a l t T o t a l lt 0 0 5 200 7 Copper T o t a l lt 0 0 2 5 2 0 0 7 I r o n T o t a l 0-03 239 2 Lead T o t a l lt 0 0 0 5 2 0 0 7 Magnesium T o t a l 0 44 2 00-72 4 5 12 00-7
Manganese T o t a l Mercury T o t a l N i c k e l T o t a l
0 027 lt0 0002
lt0 04 200 7 P o t a s s i u m T o t a l 1-05 270-2 Se len ium T o t a l lt0-005 200-7 Sodium T o t a l 2 - 4 2 7 9 2 T h a l l i u m T o t a l lt 0 - 0 1 200 7 Vanadium T o t a l lt0-02 200-7 Z i n c T o t a l 0 09 3 35-2 Cyan ide T o t a l lt 0 -01 3 5 3 3 N i t r a t e N i t r i t e N i t r o g e n 0-02 3 5 4 - 1CALC-IQ
N i t r i t e N i t r a t e
N i t r o g e n N i t r o g e n
lt0-002 0-02
lt Cent- Next Page gt
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mtiuntain Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 060590
Balsam Environmental ETR Number 21371 ConsultantsInc- Project No 90000 5 Industrial Way No Samples 2 Salem NH 03079 Arrived 051190
Attention Brian Quinlan
Page
standard analyses were performed in accordance with Methods for Artalysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Lab No Sample Description
114675 DW-1051090 sect0840(Water)
Method No- Parameter Result
3101 Alkalinity (as CaC03) 16 1 3000 Chloride 1-7 3000 Sulfate 4 9 200-7 Silver Total lt0- 32
lt Last Page gt Submitted By Aqua tec I n c
(POOIA
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT Date 29 May 1990
Balsam E n v i r o n m e n t a l Project No 90000 ETR No 2 1 3 7 1
Sample(s) Received On 1 1 May 1 9 9 0
Page 1 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgI unless otherwise noted
Pa ramete r PBLK
Aluminum lt005
Antimony lt0 06
A r s e n i c lt0 01
Barium lt002
B e r y l l i u m lt0 01
Cadmium lt0 01
Ca lc ium lt0 05
Chromium lt002
C o b a l t lt0-05
Copper lt0-025
I r o n lt002
Lead lt0 005
Magnesium lt002
Lab No Sample Descripl ion
PBLK P r e p a r a t i o n E(lank f o r sample I)W-1
Submitted By Aquatec Inc y ryy^ t r^
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So BuHington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T Balsam E n v i r o n m e n t a l raquo= 29 May 1990
Project No 9 0 0 0 0
ETR No 2 1 3 7 1
Sample(8) Received On 1 1 M a y 1 9 9 0
Page 2 of 2
Standard analyses were performed in accordance with Methods for Analysis of Water and Wastes EPA-600479-020 Test Methods for Evaluating Solid Waste SW-846 or Standard Methods for the Examination of Water and Wastewater
All results are in mgl unless otherwise noted
Parameter PBLK
Manganese lt0 015
Mercury lt0-0002
N i c k e l lt0 04
P o t a s s i u m lt0-5
Se l en ium lt0005
Sodium lt0 2
T h a l l i u m lt0 01
Vanadium lt0 02
Z inc lt0-02
S i l v e r lt0 02
Cyanide lt0 01
Lab No Sample Descript ion |
PBLK P r e p a r a t i o n IJ l ank f o r sample 13U-1
Submitted By Aquatec Inc pound fygtAin fh^ph^^
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec
Parameter
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Chloride
Cobalt
Copper
Cyanide
Iron
Lead
EPA Standard
IVQCS
1183-11 2
378-4
IVQCS
IVQCS
IVQCS
IVQCS
IVQCS
11881288
IVQCS
IVQCS
Standard
IVQCS
378-5
QC Summary
ETR 21371 Page 1 of 2
Found fuq1)
99081 100184
9333 9453
2578 2502 2440
48748 51077
48843 51602
50833 53128
54683 54009
51349 52796
544371
50512 54591
50262 50134
10171 10211
51042 51842
3219 3270
True (ua1)
10000 10000
1015 1015
250 250 250
5000 5000
5000 5000
5000 5000
5000 5000
5000 5000
516000
5000 5000
5000 5000
1000 1000
5000 5000
340 340
Recovery
991 1002
920 931
1031 1001 976
975 1022
977 1032
1017 1063
1094 1080
1027 1056
1055
1010 1092
1005 1003
1017 1021
1021 103-7
947 962
3372 340 99-2
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec
Parameter
Magnesium
Manganeses j
Mercury
Nickel
Nitrate Nitrite-N
Potassium
Selenium
Silver
Sodium
Sulfate
Thallium
Vanadium
Zinc
EPA Standard
IVQCS
IVQCS
Standard
IVQCS
284-2
IVQCS
Standard
ICV-4
IVQCS
11881288
581-31
IVQCS
IVQCS
QC Summary
ETR 21371 Page 2 of 2
Found (ua1)
1035240 1010510
48873 52343
204 189 184 179 189
49740 53818
15900
5087490 5272870
1517 1384
10385 10139
53422 53608
207956
2441 2441
50843 54664
50456
True (ua1)
100000 100000
5000 5000
18 18 18 18 18
5000 5000
16000
500000 500000
150 150
975 975
5000 5000
200000
252 252
5000 5000
5000
Recovery
1035 1011
97-7 1047
1133 1050 1022 994
1050
995 1076
994
1017 1055
1011 923
1065 1040
1068 1072
1040
969 969
101-7 1093
1009 51926 5000 103-9
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 u chloromethane 10 U chlorobenzene 5 u bromomethane 10 U 12-diehloroethane 5 u bromoform 5 U 111-trichloroethane 5 u bromodichloromethane 5 U 11-diehloroethane 5 u dibromochloromethane 5 U 112-trichloroethane 5 u tetrachloroethene 5 U 1122-tetrachloroethane 5 u toluene 5 U chloroethane 10 u trichloroethene 5 U 2-chloroethvl vinvl ether 10 u vinvl chloride 10 U chloroform 5 u acetone 10 U 11-dichloroethene 5 u 2-butanone 10 U 12-dichloroethenes 5 u carbon disulfide 5 U 12-dichloropropane 5 u 2-hexanone 10 U trans-13-dichloropropene 5 u 4-methyl-2-pentanone 10 U cis-13-dichloroprot)ene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 u total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 101 toluene-dg 102 p-bromofluorobenzene 91
No other volatile organic compounds vlaquo7ere found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U shy The compound was analyzed for J shy An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive SKI Bur i ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No 114674 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Analyzed On 21 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled Trip Blank 5490 at 1700 hours
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans -13-dichloropropene 5 U 4-me thy1-2 -pentanone 10 U cis-13-dichloropropene 5 U styrene 5 U ethylbenzene 5 U vinyl acetate 10 U tetrahydrofuran 10 U total xylenes 5 U
methyl t-butyl ether 10 U
Summary of Surrogate Recoveries Rec
12-diehloroethane-d4 100 toluene-dg 98 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT 05403
TEL 802658-1074
ANALYTICAL REPORT
Date 25 May 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank CKTB002AV for Aquatec Lab Nos 114674
and 114675
Volatile Organic Compounds in ug1 EPA Method 624
benzene 5 U methylene chloride 5 U carbon tetrachloride 5 U chloromethane 10 U chlorobenzene 5 U bromomethane 10 U 12-diehloroethane 5 U bromoform 5 U 111-trichloroethane 5 U bromodichloromethane 5 U 11-dichloroethane 5 U dibromochloromethane 5 U 112-trichloroethane 5 U tetrachloroethene 5 U 1122-tetrachloroethane 5 U toluene 5 U chloroethane 10 U trichloroethene 5 U 2-chloroethyl vinyl ether 10 U vinyl chloride 10 U chloroform 5 U acetone 10 U 11-dichloroethene 5 U 2-butanone 10 U 12-dichloroethenes 5 U carbon disulfide 5 U 12-dichloropropane 5 U 2-hexanone 10 U trans-13-dichloropropene 5 U 4-methyl-2-pentanone 10 U cis-13-dichloropropene 5 u styrene 5 U ethylbenzene 5 u vinyl acetate 10 U tetrahydrofuran 10 V total xylenes 5 U
methyl t-butyl ether 10 U
Svjnimary of Surrogate Recoveries Rec
12-diehloroethane-d4 103 toluene-dg 104 p-bromofluorobenzene 91
No other volatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
The compound was analyzed for J - An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for this compound
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive Stgt Bur l ington VT 05403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 199C ) Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water sample |
labeled DW-1 51090 at 0840 hours -
BaseNeutral Extractable Semivo latile Organic Compounds in u g1 EPA Method 625
acenaphthene 10 _U benzyl butylphthalate 10 U 124-trichlorobenzene 10 U di-n-butvl phthalate 10 u hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (bull2-chloroethyl) ether 10 U dimethyl phthalate 10 u 2-chloronaphthalene 10 _U benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13-dichlorobenzene 10 U benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 U anthracene 10 u fluoranthene 10 U benzo(phi)perylene 10 u 4-chlorophenyl phenyl ether 10 _U fluorene 10 u 4-bromophenyl phenyl ether 10 _U phenanthrene 10 u bis (2-chloroisopropyl) ether 10 U dibenzo(ah)anthracene 10 u bis (2-chloroethoxy)methane 10 U indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 U pyrene 10 u hexaehlorocyelopentadiene 10 JJ benzyl alcohol 10 u isophorone 10 U 4-chloroaniline 10 u naphthalene 10 U dibenzofuran 10 u nitrobenzene 10 U 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 U 2-nitroaniline 50 U N-nitrosodipropylaraine 10 U 3-nitroaniline 50 U bis (bull2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qualify the results of the analysis U - The compound was analyzed for J - An estimated value The mass
but not detected The number spectrum indicates the p resence is the detection limit for the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank + Cannot be separated from diphenylamine Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results 3f these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mounta in Drive So Bur l ington VT (15403
TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No 114675 ETR No 21371 Project 90000 Sample Received On 11 May 1990 Extracted On 16 May 1990 Sample Identification Balsam Environmental Consultants Inc water
sample labeled DW-1 51090 at 0840 hours
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246- trIchlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dime thyIpheno1 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachloropheno1 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 50 nitrobenzene-d5 85 phenol-dg 34 2-fluorobiphenyl - 79 246-tribromophenol 86 terphenyl-d]^^ 96
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that In the blank Quantitashy The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive So Burlington VT 05403 TEL 802658-1074
ANALYTICAL REPORT Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No 114675
BaseNeutral Extractable Semivo latile Organic Compounds in ug1 =
EPA Method 625
acenaphthene 10 JJ benzyl butylphthalate 10 u 124-trichlorobenzene 10 U di-n-butvl phthalate 10 U hexaehlorobenzene 10 U di-n-octyl phthalate 10 u hexachloroethane 10 U diethyl phthalate 10 u bis (2-chloroethyl) ether 10 JJ dimethyl phthalate 10 u 2 -chloronaphthalene 10 JJ benzo(a)anthracene 10 u 12-dichlorobenzene 10 U benzo(a)pyrene 10 u 13 -dichlorobenzene 10 u benzo(b)fluoranthene 10 u 14-dichlorobenzene 10 U benzo(k)fluoranthene 10 u 33-diehlorobenzidine 20 U chrysene 10 u 24-dinitrotoluene 10 U acenaphthylene 10 u 26-dinitrotoluene 10 u anthracene 10 u fluoranthene 10 u benzo(ghi)perylene - 10 u 4-chlorophenyl phenyl ether 10 JJ fluorene 10 u 4-bromophenyl phenyl ether 10 JJ phenanthrene 10 u bis (2-chloroisopropvl) ether 10 u dibenzo(ah)anthracene 10 u bis (2-chloroethoxv)methane 10 u indeno(123-cd)pyrene 10 u hexachlorobutadiene 10 u pyrene 10 u hexaehlorocyelopentadiene 10 u benzyl alcohol 10 u shyisophorone 10 u 4-ehloroaniline 10 u naphthalene 10 u dibenzofuran 10 u nitrobenzene 10 JJ 2-methylnaphthalene 10 u N-nitrosodiphenylamine+ 10 u 2-nitroaniline 50 U N-nitrosodipropylamine 10 u 3-nitroaniline 50 U bis (2-ethylhexyl) phthalate 10 JJ 4-nitroaniline 50 U
Key to the letters used to qual Lfy the results of the analysis U - The compound was analyzed for J - An estimated value The mass
r but not detected The number spectrum indicates the p resence ( is the detection limit foi r the of the compound but the calcu shycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the corashy
pound in the blank + Cannot be separated from diph( jnylamine Quality controls were analyzed with Che sample as part of Aquatecs standa rd analytical procedures The results ltDf these are maintained on f ile at Aquatec
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
aquatec ENVIRONMENTAL SERVICES
75 Green Mountain Drive Sltraquo Burlington VT 05403 TEL 802658-1074
A N A L Y T I C A L R E P O R T
Date 5 June 1990 Aquatec Lab No ETR No 21371 Project 90000 Sample Received On Sample Identification Method blank DB0516W7I3S for Aquatec Lab No
114675
Acid Extractable Semivolatile Organic Compounds in ug1 EPA Method 625
246-trichlorophenol 10 U p-chloro-m-cresol 10 U 2-chlorophenol 10 U 24-dichlorophenol 10 U 24-dimethylphenol 10 U 2-nitrophenol 10 U 4-nitrophenol 50 U 24-dinitrophenol 50 U 46-dinitro-2-methylphenol 50 U pentachlorophenol 50 U phenol 10 U benzoic acid 50 U 2-methylphenol 10 U 4-methyIphenol 10 U 245-trichlorophenol 50 U
Summary of Surrogate Recoveries Rec Rec
2-fluorophenol 42 nitrobenzene-d5 79 phenol-dg 30 2-fluorobiphenyl 74 246-tribromophenol 74 terphenyl-d2^4 84
No other semivolatile organic compounds were found in reportable concentrations
Key to the letters used to qualify the results of the analysis
U - The compound was analyzed for An estimated value The mass but not detected The number spectrum indicates the presence is the detection limit for the of the compound but the calcushycompound lated result is less than the
reliable detection limit for LCB - Compound was found but at low this compound
concentration comparable to that in the blank Quantitashy C - The result has been corrected tion is not possible for the presence of the comshy
pound in the blank
Quality controls were analyzed with the sample as part of Aquatecs standard analytical procedures The results of these are maintained on file at Aquatec
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
AA E a s t e r n A n a l y t i c a l i n c i30HaiistconcordNH 03301 (603)228-0525
May 22 1990
Brian Quinlan Sample Ident i f icat ion Balsam Environmental Consultants Inc Client ID Mottolo RIFS 5 Industrial Way Sample QtyType 1 aqueous Salem NH 03079 Date Recvd May 10 1990
EAI ID 8991 BEC
Dear Mr Quinlan
Enclosed please find the results of the analysis of the sample(s) identified above This report contains the following sections
ANALYSIS TYPE NO OF PAGES bull Organics and Microbiology 1
The following standard abbreviations and conventions apply throughout all Eastern Analytical Inc reports
bull lt = Less tiian followed by the detection limit bull TNR = Testing Not Requested bull ND = None detected no established detection limits
If you have any questions regarding the results contained within feel free to directly contact the chemist who performed the analysis We appreciate this opportunity to be of service and look forward to your continued patronage
Sincerely
Jt William Brunkhorst QAQC Coordinator
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor
LABORATORY REPORT
Eastern Analyt ical Inc Designation sggi BEC
Client Balsam Environmental Consultants IneSample QtyType 1 aqueous
Client Designation Mottolo RIFS Date Received May 10 1990
Organics and Microbiology
SampleMatrix
ID DW-1 Aqueous
Date of Analysis Analyst
EPA Method
Organics (mgL)
BODCODTOC
lt6 lt 10 lt1
51190 51690 51790
LB LB LO
4051 4104 4151
Microbiology (ctsIOOmL)
Total ColiformFecal Coliform
lt 1 lt 10
51090 51090
LB LB
SM909A SM909C
l m pound U m L fypoundul^MlAA Approved By Lorraine Olashaw Inorganics Supervisor