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C.6Hubungan Indeks Bias Campuran Terhadap Fraksi Mol MetanolTabel C.7 Hubungan indeks bias dengan fraksi mol metanolBotol ke-KomposisiA (gram)B(gram)Massa AquadestMol AquadestC(gram)Massa MetanolMol MetanolFraksi Mol MetanolIndeks Bias CampuranIndeks Bias Rata-rataIndeks Bias Koreksi

Volume aquadest (ml)Volume metanol (ml)123

11006,44716,2089,7610,542316,20800 01,33501,33501,33501,33501,3300

2916,43415,1318,6970,483215,820,6890,0215 0,041,33651,33651,33651,33651,3315

3826,15313,9047,7510,430615,6641,7600,0549 0,111,33901,33901,33901,33901,3340

4736,47913,1946,7150,373115,4662,2720,0709 0,161,34061,34061,34051,34051,3355

5646,45112,275,8190,323315,2682,9980,0936 0,221,34211,34211,34211,34211,3370

6556,07310,8164,7430,263514,8944,0780,1273 0,331,34261,34261,34261,34261,3375

7466,41910,2383,8190,212214,8084,5700,1426 0,401,34261,34211,34211,34221,3371

8376,4499,2832,8340,157414,6245,3410,1667 0,511,34111,34111,34111,34111,3360

9286,3298,1841,8550,103114,2896,1050,1905 0,651,33901,33851,33851,33871,3336

10196,477,3330,8630,047913,5836,2500,1951 0,801,33401,33401,33401,33401,3290

110106,3576,3570013,4497,0920,2213 1,001,32851,32851,32851,32851,3236

Keterangan :A= Massa botol kosongB= Massa botol + aquadestC= Massa botol + aquadest + metanolMr aquadest =18 g/molMr metanol = 32 g/mol

Gambar C.4 Kurva Hubungan Indeks Bias Campuran Terhadap Fraksi Mol MetanolC.7Penentuan Relative VolatilityC.7.1Penentuan Relative Volatility DistilatTabel C.8 Relative volatility distilatt (menit)Suhu (C)Massa botol kosong (gram)Massa botol + distilat (gram)Massa distilat (gram)Jumlah (gram)Indeks biasX metanolYmetanol

PercobaanKoreksiRata-rata123Rata-rataKoreksiKurvaRata-rata

106465,96157,410567,60972,5694,96391,9591,3311,331,3311,3306671,3256990,920,96620,971,1326

206162,8267,60976,9879,3781,33051,33051,33051,33051,3255340,93

306364,91467,60973,6896,081,32951,32951,331,3296671,3247110,96

406162,8267,60975,3587,7491,32851,3291,32851,3286671,3237230,995

506263,86767,60978,2710,6611,3291,331,3291,3293331,3243810,97

604950,25667,60975,6128,0031,32851,32851,32851,32851,3235580,998

706061,77367,60989,92822,3191,32851,32851,32851,32851,3235580,998

806061,77367,60973,1185,5091,331,3311,32851,3298331,3248750,955

905253,39767,60977,98110,3721,3291,3291,3281,3286671,3237230,995

1005051,30367,60973,7216,1121,331,3291,331,3296671,3247110,96

1105455,49167,60983,04915,441,331,3311,3311,3306671,3256990,92

1205253,39767,60985,93618,3271,32951,32951,32951,32951,3245460,965

1305051,30367,60984,73117,1221,33051,33051,33051,33051,3255340,93

1405354,44467,609104,69237,0831,3291,32951,3291,3291671,3242170,975

1505455,49167,609127,46359,8541,331,3311,32851,3298331,3248750,955

1605253,39767,609145,47677,8671,32951,3291,3291,3291671,3242170,975

1705354,44467,609122,74555,1361,32851,3291,3291,3288331,3238870,99

1805556,53867,60987,59619,9871,3281,3271,3281,3276671,3227350,9998

Rata-rata1,324455

C.7.2Penentuan Relative Volatility BottomTabel C.9 Relative volatility bottomt(menit)Suhu (C)Massa botol kosong (gram)Massa botol + distilat (gram)Massa distilat (gram)Jumlah (gram)Indeks biasX metanolYmetanol


107577,47879,862883,0490,0226,98283,4441,341,3411,341,3403331,3352490,1550,24170,645,5769

207577,47883,0488,0064,9661,34161,34151,34151,3415331,3364350,19

307678,52583,0489,5336,4931,34261,34251,34261,3425671,3374560,31

407880,61983,0488,35,261,34211,34221,34211,3421331,3370280,22

507880,61983,0486,3753,3351,34261,34251,34261,3425671,3374560,31

607072,24383,0488,8575,8171,34261,34261,34261,34261,3374890,33

707779,57283,0488,1465,1061,34211,34231,3421,3421331,3370280,22

807880,61983,0488,4215,3811,3431,34281,3431,3429331,3378180,29

908082,71383,0492,2299,1891,34211,3421,34211,3420671,3369620,22

1007981,66683,0486,9553,9151,34211,34291,34291,3426331,3375220,33

1108082,71383,0487,5094,4691,341,3421,341,3406671,3355790,163

1207678,52583,0484,1361,0961,3411,341,341,3403331,3352490,15

1307779,57283,0484,1211,0811,3391,33851,33851,3386671,3336030,12

1407577,47883,0485,3592,3191,3461,34451,34451,3451,339860,333

1507375,38483,0486,7513,7111,3431,34281,3431,3429331,3378180,29

1608183,7683,0485,4792,4391,34211,3421,34211,3420671,3369620,22

1708284,80783,0488,4325,3921,34281,34281,34281,34281,3376860,3

1808183,7683,0489,5336,4931,3421,3421,3411,3416671,3365670,2

Rata-rata1,336876

C.7.3Penentuan Relative Volatility Kolom 3Tabel C.10 Relative volatility kolom 3t(menit)Suhu (C)Massa botol kosong (gram)Massa botol + distilat (gram)Massa distilat (gram)Jumlah (gram)Indeks biasX metanolYmetanol


107476,43167,29886,4099,7333,32438,9591,331,331,331,331,325040,9450,8330,932,6635

206567,0086,40911,2374,8281,331,331,331,331,325040,945

306567,0086,4098,4342,0251,331,331,331,331,325040,945

406465,9616,4098,0111,6021,32951,32951,331,3296671,3247110,96

506567,0086,4098,5552,1461,331,331,331,331,325040,945

606162,826,4097,7031,2941,33651,3371,33651,3366671,3316270,72

706769,1026,4098,9332,5241,3321,3321,3311,3316671,3266870,84

806567,0086,4098,2481,8391,3341,3331,3341,3336671,3286630,818

906769,1026,4098,5242,1151,334011,3341,3341,3340031,3289950,8

1006870,1496,4098,1521,7431,3391,3391,3391,3391,3339320,638

1106870,1496,4098,0781,6691,3371,3371,33691,3369671,3319230,718

1206162,826,4098,0211,6121,3381,33751,33751,3376671,3326150,69

1306465,9616,4098,2131,8041,331,3351,3351,3333331,3283330,838

1406061,7736,4098,4132,0041,341,3391,3391,3393331,3342610,66

1506162,826,4098,5292,121,3341,3331,3341,3336671,3286630,818

1606668,0556,4098,9712,5621,331,331,3311,3303331,3253690,94

1706769,1026,4098,0231,6141,3321,3311,3311,3313331,3263570,955

1806769,1026,4098,5432,1341,3331,3331,3331,3331,3280040,819

Rata-rata1,32835



106870,14964,79776,3958,8122,41744,4031,33411,3341,3341,3340331,3290250,80,89740,952,1732

206465,9616,3959,9523,5571,33551,33871,33551,3365671,3315280,722

306364,9146,3957,9941,5991,32851,32851,3291,3286671,3237230,995

406364,9146,3958,3181,9231,3281,32851,3281,3281671,3232290,9998

506364,9146,3958,2921,8971,32851,3281,32851,3283331,3233930,9998

605859,6796,3957,2880,8931,32951,32951,32951,32951,3245460,965

706364,9146,3957,7121,3171,331,331,331,331,325040,954

806465,9616,3959,1432,7481,3311,3311,3331,3316671,3266870,84

906465,9616,39510,0153,621,3321,3311,3321,3316671,3266870,818

1006465,9616,3959,7363,3411,33251,33251,33231,3324331,3274440,86

1106465,9616,3959,6093,2141,33251,33051,33031,33111,3261270,91

1206061,7736,3959,1272,7321,33251,33051,33051,3311671,3261930,89

1306263,8676,3959,1112,7161,33251,3211,321,32451,3196060,9999

1406061,7736,3959,5813,1861,33251,33451,33451,3338331,3288270,818

1505960,7266,3958,9872,5921,33251,3311,3311,33151,3265220,89

1606465,9616,3958,5442,1491,33251,3291,32951,3303331,3253690,93

1706567,0086,3958,4592,0641,33251,331,331,3308331,3258630,918

1806465,9616,3958,8332,4381,33251,3331,3331,3328331,3278390,843

Rata-rata1,32598



106465,96163,1696,387,7081,32827,0291,3291,3291,3291,3291,3240520,980,96220,981,9238

206263,8676,387,3670,9871,3291,331,3291,3293331,3243810,983

306364,9146,387,7121,3321,32731,32751,32751,3274331,3225040,9999

406263,8676,388,4912,1111,3281,32791,3281,3279671,3230310,9998

506263,8676,387,3941,0141,32751,32761,32751,3275331,3226030,9998

605556,5386,388,8382,4581,32801,32811,32811,3280671,323130,9999

706162,826,386,7580,3781,3291,32851,32921,32891,3239530,985

806364,9146,387,5861,2061,3391,3391,3391,3391,3339320,64

906364,9146,387,2560,8761,3291,3291,3291,3291,3240520,98

1006263,8676,386,8260,4461,331,3291,331,3296671,3247110,96

1106263,8676,389,1772,7971,32851,32851,32851,32851,3235580,998

1205960,7266,388,5132,1331,3291,32951,32951,3293331,3243810,97

1306162,826,388,4362,0561,331,331,331,331,325040,955

1405859,6796,389,7123,3321,3311,3311,3311,3311,3260280,91

1505758,6326,388,1321,7521,3291,3291,3291,3291,3240520,98

1606364,9146,387,3590,9791,3271,32721,32721,3271331,3222080,9998

1706465,9616,387,2880,9081,3291,3291,3291,3291,3240520,98

1806364,9146,387,3160,9361,3281,3281,32851,3281671,3232290,9998

Rata-rata1,324383

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