is 545 (1984): mahua oil
TRANSCRIPT
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है”ह”ह
IS 545 (1984): MAHUA Oil [FAD 13: Oils and Oilseeds]
Gr 2
IS : 545· 1984
Indian StandardSPECIFICATION FOR
ill-A/IVA OIL
( Third Revision)
First Reprint AUGUST 1989
to Copyright 1984
BUR E A IJ 0 FIN D I A N S TAN DAR D SMANAK BHAVAN, 9 RAHAllUR SHAH ZAFAR MARG
NEW DELHI 110002
October J984
(Reaffirmed 2009)
IS : 545 • 1984
Indian StandardSPECIFICATION FOR
MARUA OIL
(Third Revision )Oils and Oilsccds Sectional Committee, CAFDC 5
( Conli".11 0 .. /JaIl 2 )
ReprtstntingOil Technologists .\~~O( iation of India, Kanpur
Ccutral Organization for Oi! Industry and Trade;Bombay
CI,airma11
P.ltOF 1\1. ~i. CHAKltAlJAR'l'Y
IlJemh,rs
rHOF A. c. GUPTA ( Allernat, toProf M. M. Chakrabarty)
Sun r S. N. AUABWAL
SlflU 11. I). GlJl'~r.\ ( Alt"nate )AORU:ULTlJRAL MAllKETI'NG Directorate of Marketing and Inspection, Nagpur
AnVlSEIt TO 'rUl!; GOVJ.;HN)tEN'1'OF INDIA
SHRJ R. J. VJ:;Hl\IA ( Alternate)8111&1 J. A. ASJlTAPUTBE Ministry of Defence ( DC; I )
SHUI P. N. An.\n'\·.~L ( Alt"""le )DIt B. P. B"\L'O~ Tata ()il Mills Co Ltd, Bombay
DR N. L. ~IUR'.l'Y ( .~lt"nat' )Smu M. A. IhIAT'l' Swastik Household and Industria! })rOOUCh Ltd,
BomhaySHIU C. It. KHl~JlN..\IU ItTIIY ( All.rnate )
DIt 1'. V. BR'I'fH Hlndustan Lever Ltd, BOJJlIJayDn V. V. S. lIA-s1 ( Alternflle)
SUlCI D. S. (;J1.\HJI A Central Committee for Foorl Standards (~"inistry
of Health and Famil y W r-lfare ), New DelhiSJlKllIATl DB1H ~1liJ\JI~Il,IJ':a·~ ( Alter"afe )
SUltI P. K. CJl.~Knl,lJOR'rY National Test House, CalcuttaDIt. K. C. GUllA Central Food Laboratory, Calcutta
SallY A. K. DHAR ( All""a', )SJiRI P. V. GUJABATIIJ Kharli and Village Industrjvs (:(,tnn)j~~i()nJ Bombav
SnB) V. L\X"JIIIIKANTJ1.\N ( AII'TtuJl,)Smu R. C. GUPTA Directorate General of 'I'cchnical Development,
New UcJhiSnu1 S. N. PANnEY ( Auemat« )
SJl1tl S. P. GUPTA Kusum I'rodur ts Ltd, Rishr«SURI A. R. N. Kr-r.i: ( Alternat, )
SHJn n. V. KANTAK (;uurcj Sf.MPS Lid, HOlub;,}"SJUCI M. S. r!'H.\ x u U ( Alternale )
© C.py,i,lal 19R4BUREAU OF INDIAN STANDARDS
1'lli. publication is protected under the 1,IlJin" C'I'.1,iRA, Ad (XIV of 1957 ) andreproduction in whole or in part by any means except with written permission of thepublisher than b. d~med to be an illfringempnt of copyri~ht under (iw t'ft.d Act.
( Cotditlwd/rtnn/JIl" I )
Mlmlur,
DB M. K. KUlmU
R,pr,s,nti",
Directorate of Vanaspati, Vegetable Oil. and Fata( Ministry or Civil Supplies ), New Delhi
DR G. LAXSHJlfNARAYANA Regional Research Laboratory ( CSIR ), Hyder.badUB A. J. PAJI'TULU ( A,lt""al,) .
DR B. M. LAL Indian AgriculturnJ Research Institute (ICAR),New Delhi
SunI1'. V. MATBB\V Central Agmark Laboratory, NagpurSHRI M. R. GROVER ( Alttmtlt, )
SBBI R. K. MATHUR Vanaspati Manufacturers' Association or India,Bombay
SHRI G. K. SOOD ( Alt,rn"t, )SHRJ S. C. Sr:tfORAL Shriram Foods & Fertilizer Industries, New Delhi
SHRI T. N. AOGARWAL ( Alte'''Dle)SHBI G. V. SIRUB Solvent Extractors' Association of India, Bombay
SHBI L. KRI8HAN KUMAR ( Alt""",,)DR ( SHRIJ1ATJ ) KAMLA SOJfNJE Consumer Guidance Society of India, BombayDB C. SRunvAsuLu Regional Research Laboratory ( (;SIR ),
BhubaneshwarDR ( SHRI)I.\TI ) K. VIJAY.\LAKSJfMI (Alternate)
SHBI S. D. TJURt1MAL.O\ RAO Oil Technological Research Inst itute, AnnntapurSilKI G. AZEDIODDIN ( Alt""at, )
SHRI P. R. VISIIWAIIBHARAN Central Warehousing Corporation, New DelhiSHBI K. GOPINATJlA ME~()~ ( AI,,,,,,,,, )
SHBI M. D. WA8NIK Directorate of Oilseeds Development, HyderabadSHRI S. P. JUYAL ( Alunuu« )
SHRt S. K. MATHUR, Director General, lSI ( Ex-officio 1.1,mb" )Director ( Chern )
S""/drySUIt) P. S. i\RORA
Senior Deputy Director ( Chern ), lSI
Oils and Fats Subcommittee, CAFDC 5 :
Regional Research Laboratory ( CSIR ), Hyderabad
SHRI H. P. GUJ-TA ( AII"MI')
Cont',ne,DR G. LAX8BKINABAYANA
-lllmb"sAORIClJLTUllAL MARKETfNG Directorate of Marketing and Inspection, NalPur
ADVJ8K& TO GOVEBNKEN'l' OFINDIA
SH'RIT. V. MATJIBW ( Alt,rnatt )'SDKJ J. A. AIHTA:PUTB. Ministry of Defence ( DGI )
SKal P. K. MAJUKDAlt ( Alt"ru", )ASSISTANT DIRECTOR (AQIU Indian Council or Agricultural Research Institute.
ENGG ) New OelbiSHRI V. K. SA.SAL Central Organi1.ation Cor Oil Industry and Trade,
Bombay
( COlllinu,tl on/JGIf 7)
2
IS I 545 • 198f
Tata Oil Mills Co Ltd, Bombay
SHRT R. D. SJl}~:"OI
SHRr G. K. Soon ( Alternate)DR N.J... MUR1.'Y
DR A. D. SJnT(Jr,Jo~ ( A4.lttrnate )DR S. M. PATEr.. Oil Technologists' Association of India, Kanpur
I'aoF V. V. R. SunR"H;w.~NYAM ( Alterllate )DR.I. V. PJtAllHAK.\lt Central Food Technological Research Institute
( CSIR ), MysoreIndian Confectionery Manufacturers' Association,
New DelhiDR I. S. SJfI~NOLIKAlt Indian Council of Medical Research, New Delhi
I)u R ....:UESH BHATT ( AIltrnale )DR I. A. SUJDTQUI Directorate of Vanaspati, Vegetable ODs and Fats
( Ministry of Civil Supplies), New Delhin- 1~. A. KJI.o\N' ( Altl'flnll)
SHill M. S. Tn O\K':lt Indian Soap and Toiletries Makers' AssociadoD,Bombay; and Godrej Soaps Ltd, Bombay
SUitt S. D. 'fJlllttJMAL.\ Rxo Oil Technological Research Institute, AnantapurSHRI J). AT("JfYU'I'.-\ R..'~.\Y\· A ( Alternate)
SHRJ M. D. WASNIK Directorate of Oilseeds Development, HyderabadSHIn S. P. ]ev.o\l, ( AII,rllal, )
,( Continuedfrom pag, 2 )
M""b,rs R'pr,s,nli",DR N. V. URINOI Hindustan Lever Ltd, Bombay
DR V. V. S. MANI ( Allemal, )SHRI D. S. CHADHA Central Committee for Food Standards (Ministry
of Health and Family \VelCare ), New DelhiSffRJMATI DEBI MUKlIERJEE ( Altnnate)
SURI R. D. K.'WATRA Directorate General of Technical Development,New Delhi
SHUI V. I..AKSJlJlIKANTJlAN Khadi and Village Industries Commission, BombaySaar V. K. B. NAIR ( AII,rnal,)
SURt R. K. !\f.,nPHATIA Indian Paint Associatlon, CalcuttaSHltl RAlllN S.~RK.~1t ( Alternate)
"SHRt R. K. MA'I'IfUlt Vnnaspati Manufacturers' Association of India,Bombay
7
IS : 545 - 1984
AMENDMENT NO. 1 JANUARY 1990, TO
IS: 545 -1984 SPECIFICATION FOR MAHUA OIL
( Third Revision )
( Page 4, claus, 4.3 ) - Substitute the following for the existing clause:
'4.3 Admixture with Otber OUs - The material shall be free from admixture of other oils.
4.3.1 The material shall be free from non-edible oils. when tested inaccordance with 9, 10, 11, 1%, 14, 15 and 16 of IS : 548 ( Part 2 )-1976·.
(!age 6, clause S.2.1 ) - Add the following new clause after 5.2.1:
5.2.1 The containers may also be marked with the Standard Mark.
Nol'l- The use or the Standard Mark Is governed by the provisions of theBureau or Indian Standard. Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark on products covered by an Indian Standard convey.the assurance that they havo been produced to comply with the requirements ofthat standard under a well-defined system of inspection. tetlin. and qualitycontrol which is devised and supervised by DIS and operated by the producer,DIS marked products are also continuously checked by SIS for conformity tothat standard .s a further aafeluard. Details of conditions under which alicence (or tho use or the StaDdard Mark may be granted to l11anufacturers, orproducer. may be obtained from tho Bureau of Indian Staudurds,
·MClhodl of samplinl and tcst for oila and fals : Part 2 Purity test.
(CAFDC5 )
AMENDMENT NO. 2 SEPTEMBER 1995TO
IS 545: 1984 SPECIFICATION FORMAHUA OIL( TIUnI R.NiOll )
( Page 3, Foreword, clllwl! 0.3 ) - Add tbe following clause 0.4 afterclause0.3and renumber tbe subsequent clause:
'0.4 A scheme for labellingenvironment friendly products to be kDoWR I. BeOMark bas been Introduced It the instance of the Ministry of Environment IndForaCl ( MEF). The BCOMark sllln be administered by the Bureauof IndilDStandards (BIS) under the BIS Act, 198611 per tbe Resolution No. 71 dated 20February 1991 IS published in the Glzeneof tbe Government of India vide GSR8S(E) dated 21 February 1991. For I plOdUd to beeligible for mlrking witb tbeEeQ Mark it .hllI .Iso carry the Stanc!ard Mark of BIS for qUllity besidesmeeting additional optional enYirollD1eDt friendiy ( EF ) requiremenb. The EFrequirements forMal"'a oil lie therefore being includedtbroughIn amendment.
This amendment is blsed on tbe Glzetle Notification No. 678 d.ted 30 August1994 for Labelling Edible Oib, Tea and Coffee IS environment friendlyproducts, pubJisbed by the Ministry of Environnleftl and Forests.'
(PageS, Table 1 ) - Add tbe following cl.uses .fter Table 1:
'4.5 Optlona. Requirements for ECO Mark
4.5.1 Gener.' RequiTe_'s
4.5.1.1 The product sh.1I conform to the ~quirements of quality prescribedunder clauses 4.1 to4.4.
4.5.1.2 The manuCldurell shill produce to BIS environmenr.1 consentclelnnce fromtbe coDcemed Slale Pollution ControlBoard II per tbe norma laiddown under tbe Waler ( PreW!ntiol'l and COnlrol of Pollution) Act, 1974;Air (Prevention lindCOIItrol ofPolllllion ) Act, 1981; WQ'er (Prevention andControl 01PoU"tion) Cas Act, 1977respectively, Iiong witb the autborization,if requiRd under tbe En"ironmelll ( Protection) Act, 1986, while applying forECOMart.
4.5.2 Sp«i(~ Requirement.l
1
Amead No. 2 to IS 545 : 1*
4.5-Z.1 The pJOdad111I0 DOt eoIDI. anatoxin, mole than 5 IIIIIk& when testedby~metbocl plaCribed 18 Appeadix A.
U.2.Z The pelddde JaidueI, If la,. shlD IIOt exceed the lolellllCe limits IIpracnbecl iD tile PretJellioll ofFoodAdMltertltioft Act, 1954 aDd Rules IIIIdetbeleUDCler.
4.5.2.3 Only pemitted antioxidants DOt exceedilll Ibe qUiDdlia specifiedas!li..l alc" I. pracribecl under tile Prevmlioll ofFoodAdMltertlliOll Act, 1954'.lnd·Ru·. nllde tllereunder, .11I0 beued, if required.
4.5.2.4 .The plOducl ....11 not coRllia any of die Ioxic mer-II in exceu of thequalities plelCnbed in Tlble 2.
TABLE 2 uMrrs. IiOR'roXie METALI
RiIMIDIINT5.0
0-'1.0
0.25
,SLNo. CH.uAcn1811C
. i) Lead. IDAlIa
.: ii) ArMDie, IBN.M.
,·Jil) CIcI.i _.,. lIa
~\') Me.." ( )"'1/•.:' ·M.....or....pli...... '.food 001...( ........ ).
MI1HDD OfTan. REFm15 of IS 1699 : 1995
do
de
do
(Pille S, cltlust! 5.1 ) - Add lbe followilll da.e 5.1.1 after ellale 5.1:
'5.1.1 For !CO Mark tbe plOClaet aball be packed il\ lucb pacaga wbicll lie
made from recyclable ( tbat il wbicb· ClD be Ie-processed to mIDuf.ctu~ layuseful plOdUd) orbiodelllclible materia~.'
(P.,. 6, c/GlUe '.1 ) - Add the followinaclause '.1.1 after cllUse6.1:
'~'.I.l For ECO Mark the co.lli." ablll be marked willa the ColloWiagiftfolDlltion:
a) Uat of identified critical inpeclic".. iD daceDdiag order of qUlntity,percentby ..... wbicla ....11 iaclacle 'DlIde rlOlD AI.- oil';
b) The briefmien. fornidi tileplOd.a baa bee. I.belled for BOO Mark;lad
c) SbelflifeofdiepIOdact.··
2
Amend No.2 to IS 545 : 19M
( Pd. 6, cllJlU~ 7.2 ) - Add the following Appendix after clause 7.1:
'APPENDIX A(Cltlll2 4.5.2.1)
DETE~ATIONOFAnATOX~
A-I REAGENTS
A·I.I Acetone, 78 Pelftllt - 700 mll~tone in 300 mI distilled Wiler.
1\-1.2 Acetone, lO PelUDt - 200 mlacelone in 800 ml distilled Wlter.
A-I.J Lead Acetate, 20 PeIftDt - 200 g neutral acetate in distilled wlter and3 mI glicialicelie acid, diluted to one litre.
A·2 PROCEDURE
A-2.t Dissolve 30 g IIfdple in 100 ml hexane.
A-Z.z Extractwitb 3 )( SO mI 70 pelCent aceloDe.
A-2.3 To the extract add 60 ml distilled wlter and 20 mllead lcetate.
A·2.4 Boil to reduce volume to ISO mi. Cool to about 'lOGe.
A·2.5 Filter and Wish with 20 percentlcetone.
A·ZA Extract filtrate Ind wasbinp witla 3 )( SOml chloroform.
A-Z.7 Piss cblorofonn layer througbanhydrous sodium sulpblte.
A·Z.a Concentrate to SO mllnd spot OD TLC plate.
A·3 CALCUlATION
. V)(s)(lOOOAfl.loxln, mgIkg = v x m
wbere
V • volumeof eXillel in mI,
" • volume of extlld giving minimum observable fluorescence in 111,
III • 81111 orIImple in I, Ind
I -standant toxingivingminimum observable Ouorescence in PI. t
(FAD~)
Jlepropphy Uni.. DIS. New Del.......
AMENDMENT NO. 3 MARCH 2002TO
IS 545: 1984 SPECIFICAnON FOR MANOA OIL(TIdnIRnuiDII)
(Amendm~II' No. 2.ptJg~ 2, clsus. 4.5.2.1) - Substitute ·S )l&!ks' for;m&!k8 e.
,fAD44 ) RcpIopaphy Unit. 81S.New Delbi. IDdia
IS : 545 • 1914
Indian StandardSPECIFICATION FOR
MAHUA OIL
(Third Revision)
o. FOREWORD
0.1 This Indian Standard ( Third Revision) was adopted by the IndianStandards Institution on 13 August 1984, after the draft finalized by theOils and Oilseeds Sectional Committee had been approved by theChemical Division Council.
0.2 This standard was first published in 1954. The first revision wasissued in 1963 in which the limit for titre was amended and the limit formoisture was prescribed so as to' include both the moisture and theinsoluble impurities. The second revision in 1968 amalgamatedIS : 545·1954· with IS : 3475-1966t, which was subsequently withdrawn.
0.2.1 In this revision, another grade of MAHUA oil, namp!y~ ~dib)e
grade, has been incorporated and the assistance ~Cn ihis has beendrawn from PF~ rules.
0.3 MAHUA oil, also known 8S MOJVRAlloil, is obtained from the seedsof two trees: Madiwtfl indica J.F. Gmelin. syn. Madhuca latifoliG ( Roxb, )
. Macbride and Madhuca longifolia ( Koenig) Macbride; both belonging tothe family Sapotaceae. Mlldhuca i"dic(I grows chiefly in Madhya Pradesh,Uttar Pradesh, Bihar, Gujarat and in parts of West Bengal, Maharashtra,Andhra Pradesh and South India; while AflldhucfJ longifolia grows only inSouth India. The oil is extensively used in the manufacture of SO:lP! andlubricating greases and for edible purposes.
0." For the purpose of deciding whether a particular requirement of thisstandard is complied with, the final value, observed Or calculated,expressing the result of a test or analysis, shall be rounded off in accordance with IS : 2-1960:. The number of significant places ret~ed in therounded oft'value should be the same as that of the specified value inthis atandard. '
.Specification for MAHUA oil ( sttolltl,-u;." ).tSpecification for lolvent-extracted MA.NUA ( MOWRAH ) oil.
, lRules for rouDdiDgoff numericai values ( ,«Iis.tl).
IS : 545 • 1984
I. SCOPE
1.1 This standard prescribes the requirements and the methods ofsampling and test for AJAHUA oil intended for both edible and nonedible industrial purposes.
2. TERMINOLOGY
2.1 For the purpose of this standard, the definitions given under 2 ofIS : 548 ( Part 1 )·19fi/~. shall apply.
3. GRADES
3.1 The material shall he of the following three grades:
a) Refined Grade - Suitable for edible purposes.b) Raw Grade 1 - Suitable for making uanaspati and refined oil and.
not for direct human consumption.c) Raw Grade 2 - Suitable for industrial purposes.
4. REQ,UlREMENTS
4.1 De.criptioD
t.I.1 For Refuud Grad« - The material shall be expressed from cleanand sound kernels of either Madhuca indica J.F. Gmelin, syn, Madhuc«latifolia ( Roxb. ) Machride or Madlluca longifolia ( Koenig J Macbride, ora mixture of both. It shall be clear and shall be free frorn rancidity,suspended or other foreign matter, separated water, added colouring orflavouring substances or mineral oil.
4.1.2 For Raw Grade 1 and Raw Grade 2 - The material shall beobtained from good quality MAHrlA cake or from the clean and soundkemels of either Madlauca indica J.P. Gmelin. syo. Madkuca latifolid( Roxb, ) Macbride Madhuca longifolia ( Koenig) Macbride, or a mixtureof both, by a process of solvent-extraction or from MAIIUA kernels by aprocess of expression. The material shall be clear and free fromrancidity, adulterants, sediment, suspended and other foreign matter,separated water and added colouring and flavouring substances.
4.2. The clarity of the material shall be judged by the absence ofturbidity after keeping the filtered sample at 50°C for 24 hOU1·S.
4.3 Admlstare with Other Oil. - The material shall be free Iromadmixture with other oils, when tested according to the methods prescribed under 20 of IS : 548 ( Part 1 )-1964-.
-Method. of sampling and test Cor oils and fats: Part 1 Sampling, physical andchemical t.t. ( ,niud ).
IS: 545·19"
4.4 The material shall comply wilh the requirements given in Table I.
TABLE 1 REQUIREMENTS POR M,4HUA OIL( Claus,s4.4 tlnd 7.1 )
SLNo.
REQUIRl<:MENT 1"OB
r------A - - - --.Refined Raw RawGrade Grade 1 Grade 2
MBTHOD OJ'TEST, REP TO
CLNo.
(6)
5&61II
13 III,
10 I~ orIS: S.f8
II I (Part I )-, 196f·
15 ,
Af I7 (12 J
P: 21 of IS :1448t
50
187·19658-70
3-0
0°875
'(5)
0·5
Above 2040100
30
(4)
0-25
20-040100
187-19658-70
3-0
10
1-4590
0-540250
(3)
0-10
O'8G2
187-19G58-70
2°0
(2)(1)
i) Moisture and insoluble i mpurlties, percent by mass, Alax
ii) Colour in a i-in cellon the Lovibondscale, expressed asT + 5 R, not deeperthan
iii) Refractive index at40°0
iv) Specific gravity at 90/30°0
v) Saponification valuevi) Iodine value
vii) Unsaponifiable matter,percent by mas."Afa:t
viii) Acid value, Ma»ix) Tilr" ( I)C ), Minx) Flash point Pensky
Martens (closed)°C, Mill
• Methods of sampling and test for oils and rats: Part I Samplin., physical and.chemical testl ( "Dis,tl)_
tMethodl of tese Cor petroleum and itl products: P: 21 Flash point (closed) byPensky-Martens apparatus (first "vision ).
5. PACKING AND MARKING
5.1 Paekl•• - The material shaJl be supplied in suitable well-closedcontainers, as agreed to between the purchaser and the supplier•
.5.2 Markial - Each container shall be marked with the following:
a) Manufacturer's name and his recognized trade-mark, if any;b) Name and grade of the material;c) Mass or the material in the container;d) Batch No. or lot No. in code or otherwise; ande) Month and year of manufacture.
5
Ila545·1914
~.I In case of Raw Grade 2, the containers shall also be suitablymarked 'FOR INDUS1'1RIAL USES'.
6. SAMPLING
6.1 Representative samples of the material shall be drawn as prescribedunder 3 of IS : 548 ( Part 1 )-1964·.
7. TESTS
7.1 Tests shall be carried out as prescribed in IS: 548 (Part 1 )-1964.and IS : 1448t. References to the relevant clauses of these standards aregiven in col 6 of Table 1.
7.2 Q,aalltyof RealeDts - Unless specified otherwise, pure chemicalsand distilled water ( 3fe IS : 1070-1977: ) shall be used in tests.
NOTB - • Pure chemicals t shall mean chemicals that do not contain impuritieswhich affect the resul ts of analysis.
-Methods or .mpliDa and teat Cor oil. and Catl: Part I Samplm,. pbyaical andchemical teItI ( ,mI. ).
tMethods of t.a Cor petroleum aDd ita products.fSpecI&~ lor wat. Cor lenerallabOratory we ( $,..tl,1fJi.rin )•
. 6
BUREAU Of INDIAN STANDARDS
H·.tklu.n.,.,M.n.k Bha"..., I Bahadur Sbah Zatar Maru, NEW DELHI 110002Telephone. I 331 01 31, 331 13 11 Telegram. I Manaksanstha
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