Disclosure to Promote the Right To Information

Whereas the Parliament of India has set out to provide a practical regime of right to information for citizens to secure access to information under the control of public authorities, in order to promote transparency and accountability in the working of every public authority, and whereas the attached publication of the Bureau of Indian Standards is of particular interest to the public, particularly disadvantaged communities and those engaged in the pursuit of education and knowledge, the attached public safety standard is made available to promote the timely dissemination of this information in an accurate manner to the public.

इंटरनेट मानक

“!ान $ एक न' भारत का +नम-ण”Satyanarayan Gangaram Pitroda

“Invent a New India Using Knowledge”

“प0रा1 को छोड न' 5 तरफ”Jawaharlal Nehru

“Step Out From the Old to the New”

“जान1 का अ+धकार, जी1 का अ+धकार”Mazdoor Kisan Shakti Sangathan

“The Right to Information, The Right to Live”

“!ान एक ऐसा खजाना > जो कभी च0राया नहB जा सकता है”Bhartṛhari—Nītiśatakam

“Knowledge is such a treasure which cannot be stolen”

“Invent a New India Using Knowledge”

है”ह”ह

IS 542 (1968): coconut oil [FAD 13: Oils and Oilseeds]

0,2

IS : 542 -11M(SupencdlDl IS : 3471- 1"')

Indian StandardSPECIFICATION FOR

COCONUT OILj

(Second Revision)j '< (

Sixth Reprint AUGUST 2007(Incorporatlba Amendment ijo. ~ andIncludtna Amendment Nos. 2, 3 & 4)

I :

UDC 665.353.6

" CoPY;111tI1973BUREAU or INDIA-N '8TAND~RDS~AKBHAVAN, 9 BAHADUll SHAH ZAlARMAllO

NEW DELID 110002

November 1888

(Reafllraaed 2009999==2010

1••M2-I.

Indian StandardSPECIFICATION FOR

COCONUT OIL

(Second Revision)Oils and Oil.eed. Sectional Committee, CAFOO 5

( C.IiDM • ,." 2)

&/wUlltn.,Swutik ou Milia Ltd, Bombay

CIWrIIIaDaJ. S. BADAMI

MmtlNrsS8RI V. A. PAtUER (AllmMt, to

DrJ. S. Badami)Dn K. T. ACHAYA. Reponal R~h Laboratory (CSIR.). Hyderabad

DBG. LAUBMJ_AKAY"K.. (AlII,""")SKRt V. P. AAAIft'ANAR"YAlfAtf Directorate or Marketin & IDlpeCtion (Miniatry 01

Food, Aariculture. Community DevrlopmeDt ~Co-operation ) t NalPur

Smu V. CSAlO>RAMOULY ( Ai"".,,,. )SHRI R. C. DAB GUPTA National Test HOUle, CalcuttaSaRI N. DS8IXACHAB. The Tala Oil Milia (10 Ltd, Bombay

DB B. G. GUNn. (Alima"")DR K. C. Gtn~ATI Indian Agricultural Research lrutitute, New Delhi.

atUl Indian Councilor Apicultural aaearda,New Delhi

SRRI H. P. GUPTA. East India Oil Millen AIIociation, CalcuttaSaRI R. R. MUUADJ (Alt"".u)

DRG. S. HATT1AlfGni Mindustan Lever Ltd, lIombaySftRI K. P. JAJit Directorate orsu....~ V....tt (Miniitry or rood,

Apiculture, Community ~Iopmmt • Oo-ope­ration), New Delhi

&Rftl F. G. T. MRM•• ( AI""..,,)DRS. M. KAJJ ltalab Private Ltd, Bombay

8R.IJ. C. DEY (AI",,,tll,)(CAlcutta)

8H"R1 S. S. tlOlJ.VAR (.4""",")( Madra)

SHft! N. S. MAINI Re,ional 08iee. Oilleeda Developmmt (Miniltry orPoocI, Apiculture, Community Deftlopmeat •Co-operation ), Hyderabad

S... HA'RIIW 8ftMr (Allmllt")Dn R. D. NARA.(I Cenrral C'..ommittee for Pood Standard. (Ministry or

HNlth' Family Planning), New DeIhlSOl D. S. CRADH" (AI'"...',)

4 _ __

BUREAU OF INDIAN STANDARDSMANAK BHAVAN, 9 BAHADUR SHAH ZAFAR MARG

NEWDELHI 110002

1I,M2.1_

( t:.Ii.../,.. /UtI, I )

M,mIJ"s R.p,"",'i,.,SRal N. P. NOPANI Bombay Oilsef'd. and Oil, Ex~hanF Ltd, Bornbav

5"81 C. V. l\(ARIWALA (All"".II) .8••1 V. M. PAl GOd~j Soaps Private Ltd, Bombay

SRRI B. V. KANTAK (All"""')SHill S. S. RAX4.8WAMY The Vanupati Manufaetur~rA' Al'SOC'iation of India,

BombayOa H. G. R. a.noT Directorate G~neral of Technical Development, Nt'w

Delhia.......-r&TIV. Oil Techno1olica1lleIQrch Institute, AnantapurSHRIIU.. SHARKA Solvent Extractors' Auociation of India, Bombay

SRal P. P. 8HAJtJlA (AllmUlt,)SaRI P. V. Sa.IEA.TAo RAO Khadi and Village Industries Commission, Bomba')'

8RBI P. V. GUJARA'l'BI (.41"""")SIIBI L. R. SUD Ministry of Defence ( R It D )

SUI A. P. CRAie••VDTY ( AlImWI )8..1 P. M. TKo... Central Warehoulinl Corporation, New Delhi

SHU P. RAM»U (AI,..,..,,)SBa' D. D.u GunA, Dirr.ctor General, lSI (&-oJlicio M,mlHr)

Director (Chan )

$m'1tn7SBRIS.SUBRAHKANYAM

Deputy Director (Ch~m) t lSI

Oils and Fats Subcommittee, CAFDC 5: 1

e-rnnDa G. S. HA'l'TIANnIlJ Hindustan Lever Ltd, Bombay

Indian In.titute of Science, Ban.aloreThe But Asiatic Co (lndia) Pvt Ltd, MadruThe Ta.. on Mill. Co Ltd, Bomt.y

Mma'trJ

SURt V. U. MARBALLt (All""tJII toDr G. S. Hattianpi )

Da K. T. ACRAYA Relional Rewarch l~boratory (aSIR), HyderabadDRG. LAX.RJllflfARAYAJJA ( ~Il"".." )

S••I OoJlOLOHAlfD J. AOA.RWAL Bombay OilRed. and Oil. Exchange Ltd, BonlbaySRRI C. V. MAR1WALA ( AI,.",." ) ,

SWIU V. P. ANANTANA"AYAKA1f Dirrctorate of Mark..ting It Inspection (Ministry ofFood, Alriculturt', C'.ommunity Dcveolopmmt IeCo-opnation ), N&fIPur

8.BI V. CUAlCDUKOULY (Al'nut,)S.I\I DHORJATI PUIAD SHAftA- C.tclItta Chemi('al CeO Ltd, C..leutra

C1IARYYASaRI AWIL KUMA'R MAa,mr-

D.... (~lmIUlU)DR H. Il. CAliADRIt. C. DA:NDOlfA.SIJU N. D.IKACHA'&

DR B. G. Ot1JfDB ( AI,,,..,,)

2

S••I L. R. SUD

Ilia! P. G. T. MIl....

M.."sS.as S. C. aBO••

Rqw,smlill'

Indian Soap and Toiletries M.ktT.' AIIOciatlon,Calcutta

Directorate or 8\11IlT It Vanaapati ( Ministry or Food,Agricultule, CommuDity Development ACQ-operation ), New Delhi

s..r-au. Kla.oa. (141"""")8..1 B. S. MODI The Vanaapati Manuracturen' Association of India.

BombayDa It. S. MUATI Tunpbhadra Industries Ltd, KurnonlDB H. G, R.. Il.DDT Directorate General or Technical Development.• New

Delhi .Ministry of nefrnre ( R &: D )

Panel for Studying Indian Standards onOils and Fatl, CAFDC 5: 1: 1

c.w..."Da 8. M. PATJ:L l{indtL~tan Jever Ltd, Bombay

M";,b,,,

SRRI V. P. AMAlft'AKARAYANAlf Directorate or Marketing It Inspcctien (Ministry nfFood, Agriculture, Community Development &:('~.o~ralion ), Nagpur

S••I V. CHAN'DRA.1I0'OLY (AllmuJU)8.a. P. V. GUIAKATKI Khadi and \'illage Industries Commission, Bombay

S8Jtl V. D. HXRVATTK (A/Urate)DR J. O. KANE In penonal capuity (ntpartrlUnt tJ/Ch,mi,,,1 r,cluuJJn(J.

. UniNtsilJ n.[ Bomb".1. BtmabIl.1)SZC'RM'ARY ~ntral Committee for Food Standard~ (Mini.try of

Health It Family Planning), New DelhiAaIII'l'AKT SBCRftAftY ( AI""..,,)

SRa, P. P. SHARMA . Solvent Fdtracton' AA.~iati()nor India, BombaySHal L. D. NANAVATl ( AI",,,ou) "

S••I SHIVJlAJ SARA-OUR IncUan Vegetable Product" Ltd. IletmhayS.R' I. D. 51.0M Ministry of J.)eitnce ( R It I)

MOIPF- 300 Deptt, or81812007-1oo

8

AMENDMENT NO. 2 JANUARY 1990TO

IS : 542 • 1968 SPECIFICATION FOR COCONUT OIL

( Second Revision )

( Page 4, clause %.1.1 ) - Substitute the following for the existingclause:

'1.1.1 Refined Coconut Oil - Refined coconut oil means oil which isobtained by expression or solvent extraction of coconut oil bearingmaterials, deacidified either with alkali or physical refining or by miscellarefining by bleaching with adsorbent earth and/or carbon and doedorizedwith steam.'

( Page 5, clause 4.3 ) - Substitute the following for the existing clause:

c4.3 Admixture witb ()ther on. - The material shall be free from admix­ture of other oils.

4.3.1 The material shan be free from non-edible oils, when tested inaccordance with 9; 10, II, 12, 14, IS and 16 of IS : 548 ( Part 2 )-1976·.'

( Page 7, clause6.1 ) - Add the following new clause after 6.2:

'6.2.1 The containers may also be marked with the Standard Mark.

NOTE - The use of the Standard Mark is governed by tho provisions 01 theBureau of Indian Standards Act. 1986 and the Rules and Replations made tbere..under. The Standard Mark on products covered by an Indian Standard cODveylthe assurance that they have been produced to comply with tbe requirements ofthat standard under a well-defined system or inspection. testin, and qualitycontrol which is devised and supervised by DIS and operated by the producer.DIS marked products arc also continuously checked by DIS for conformity tothat standard us a further safeguard. Details of conditions under which.licence for the usc of the Standard Mark may be ,ranted to manufacturen orproducers, may be obtained from the Bureau of Indian Standards.'

·Methods of sarnphng and test for oils and fats: Part 2 Purity test.

(CAFDC 5)

AMENDMENT NO. 3 DECEMBER 1995TO

IS 542: 1968 SPECIFICATION FOR COCONUf OIL( SecondRevision)

( Page 4, Foreword, clause 0.4 ) - Add the following clause 0.5 afterclause 0.4 and renumber the subsequentclause:

'0.5 A scheme for labelling environment friendly products to be knownas ECOMark bas been introduced at tbe instance of the Ministry of Environment andForests ( MEF). The ECO Mark shall be administeredby the Bureauof IndianStandards ( BIS ) under tbe BIS Act, 1986 as per the Resolution No. 71 dated 20February 1991 88 published in the Gazette of the Government of India vide GSR85(E) dated 21 February 1991. For 8 product to be eligible for marking with theECO Mark it shall also carry the Standard Mark of BIS for quality besidesmeeting additional optional environment friendly ( EF ) requirements. The EFrequirements for coconut oil, raw and refined are therefore being includedthrough an amendment.

This amendment is based on the Gazette Notification No. 678 dated 30 August1994 for Labelling Edible Oils, Tea and Coffee as environment friendlyproducts, published by the Ministry of Environmentand Forests.'

(Page S, clause 4.4 ) - Add the following clauses after clause 4.4:

'4.5 Optional Requirements for ECO Mark

4.!.1 GeneralRequirements

4.!.1.1 The product shall conform to the requirements of quality prescribedunder clauses 4.1 to 4.4.

4.5.1.2 The manutacturers sball. produce to BIS environmental consentclearance from the concerned State Pollution Control Board ~s per the nonns laiddown under the Water ( Prevention and Control 01 Pollution) Act, 1974;Air ( Prevention and Control ofPollution ) Act, 1981; Water ( Prevention andControl01Pollution) CessAct, 1977respectively, along with the autbbrizltion,if required under the Environment ( Protection) Act, 1986, while applying forECOMark.

4.5.~ Specific Requirements

1

Amend No. J to IS 54Z : 19"

43.%.1 Theproduct shall not contain anatoxin, more than 5 mg/kg, when testedby tbe method prescribed in Appendix A.

4.5.1.% The pesticide residues, if any, shall not exceed the tolerance liouts asprescribed in the Prevention of Food Adulteration Act, 1954 and Rules Iludethereunder.

4.5.2.3 Only permitted antioxidants not exceeding the quantities specifiedagainst each as prescribed under the Prevention ofFoodAdulteration Act, 1954and Rules Dlide thereunder, shall be used, if required.

4.s.%.4 The product shall not contain any of the toxic metals in excess of thequantitiesprescribed in Table 2.

TABLE Z LIMITS FORTOXIC METAL.fit

i) Lead, mr/ka. MIl.Y S.O

ii) Arsenic, mA, Max 0.5

iii) CadmiuJD,ai~Max 1.0

iv) Mercury (Iotal) 0.25m&Jkc, MIU

• Methods of sampliDI ad test (orfoodoolours ( $«OM revision ).

SLNo. CHARACl'ERJSnc REOUIRBfENT METHOD OF TEsT, REF10

15of IS 1699: 1995­

do

do

do

( Page S, clause 5.1 ) - Add the following new clause 5.1.1 after clause5.1:

'5.1.1 For ECO Mark the product shall be packed in such packages which aremade from recyclable ( tbat is which can be re-processed to manufacture Inyuseful product) or biodegradable materials.'

( Page 5, clause 6.1 ) - Add the followil\g new clause 6.1.1 after clause'.1:

"6.1.1 For ECO Mark the containers shall be marked with the followinginformation:

I) Ust of identified critical ingredients in descending order of quantity,percentby mass, which shall include 'made fronl coconut';

b) The briefcriteria for whicbtbe producthas been labelled for Eoo Mark;and

c) Shelf life of the plOduet.·'

2

Amend No.3 to IS 541 : 1968

(Page 7, clause 8.% ) - Add the following Appepdixafter clause 8.%:

'APPENDIX A(Clause 4.5.2.1 )

DETERMINATION OF AFLATOXIN

A ..l REAGENTS

A-I.I Acetone, 70 Percent - 700 mlacetone in 300 ml distilled water.

A·l.1 Aeetonet %0 Percent - 200 81) acetone in 800 ml distilled water.

A·I.3 Lead Acetate, ZO Percent - 200 g neutral acetate in distilled water and3 ml glacial acetic acid, diluted to one litre.

A-1, PROCEDURE

A-Z.l Dissolve 30 g sample in 100 ml hexane.

A..Z.z Extract with 3 x 50 lui 70 percent acetone.

A·Z.3 To the extract add 60 ml distilled water and 20 mllead acetate.

A-Z.4 Boil to reduce volume to 150 mi. Cool to about 20°C.

A-Z.! Filter and wash with 20 percent acetone.

A-Z.' Extract filtrate and washings with 3 )( SO ml chloroform.

A·Z.7 Pass chloroform layer through anhydrous sodium sulphate.

.A·Z..8 Concentrateto SO mland spot on TLC plate.

A·3 CALCULATION

Aft t · .nnrJlu.. V X S x 1 000a oxm, &U&,-t'J =# vxm

where

V =volume of extract in ml,

v =volume ofextract giving minilllumobservable tluorescence in Jj,1,

m II: mass of sample in g, and

s =standard toxin giving minimum observablefluomsce~ce in ~g.'

(FAD44)

3

AMENDMENT NO. 4 MARCH 2002TO

IS 542: 1968 SPECIFICATION FOR COCONUT OIL( Second Re,illon )

( Amendment /\'0. 3, page 2, clause 4.5.2.1] - Substitute '5 J.lg/kg' for '5mg/kg '.

(FAD44 )

Indian StandardSPECIFICATION FOR

COCONUT OIL

(Second Revision)

o. FOREWORD

0.1 This Indian Standard (Second Revision) was adopted by the IndianStandards Institution on 28 August 1968, after the draft finalized by theOils and Oilseeds Sectional Committee had been approved by the ChemicalDivision Council and the Agricultural and Food Products Division Council.

0.2 India ranks among the largest coconut producing countries of theworld. The chief coconut growing states in India are Madras, Kerala,

. Mysore, Orissa, and West Bengal. Considerable quantities of coconut oil,both in the raw and refined state, are used in India for edible purposes andfor margarine and bakery fatl. Furthermore, the oil finds wide use in themanufacture of soaps and various types of cosmetic and toilet preparations.The requirements for various grades of the oil have, therefore, been SOpres­cribed in this standard that these grades are suitable for the foregoingpurposes. The oil is also used for pharmaceutical purposes.

0.3 This standard was originally issued in 1954. In ita first revision issuedin 1963, the limits of acid value, colour and the moisture and insolubleimpurities were modified in the light of experience. As the standardcovered only the expressed type of oil, and since there was an urgent needfor formulation of an Indian Standard for the so!vent-extracted type,15:3471·1966* was issued al an emergency standard based on the datamade available to the ad hoe Consultative Group let up for the purpose.After having decided to normalise this emergency standard the need forrationalizing the grades of the oil covered in these standards was keenlyfelt. Thls second revision of IS: 542..1954 hal been prepared amalgarnatinJrits.earlier revision and 18:3471·1966*. As a consequence, IS: 3471·1966inow stands withdrawn.

0.4 The requirements laid down in this standard for the expressed type ofthe ail correspond to the specifications prescribed by the Directorate of~farketing and Inspection in their Vegetable Oils Grading and Marking

·Specification for solvent extracted coconut oil.

3

llulel, 1955. For the purpose of regulating the quality of the 101v( ".t­extracted type of this oil, the concerned Indian Standard on the solvent­extracted type or the oil which is incorporated now had been adopted inthe relevant schedule of the Solvent-Extracted Oil, De-oiled Mt\,al andEdible Flour (CQntrol) Order, 1967. In so far al the edible grades areconcerned, this standard takes care of the provisions of the Prevention AfFood Adulteration Rule., 1954, as modified from time to time.

U For the purpose of deciding whether a particular requirement of thisltandard i. complied with, the final value, observed or calculated, express­in, the result of a test or analysis, shall be rounded off in accordanceWith 18:2-1960·. The number oflignificant places retained in the roundedoffvalue lhould be the same .1 that of the specified value in this standard.

I. ICOPB

1.1 Thilltandard preacnDea the requirements and the methods ofsamplingand test for coconut oil used for edible and industrial purposes.

. 2. TZRMINOLOGY

2.1 For ~he purpole of thil standard, the definitions given under 2 of18:548-1964t and a110 thole given below, shall apply.

2.1.1 RlfittldCoeo,"" Oil- Coconut nil obtained by the process of expres­,ion or 101vent extraction which hal been refined by neutralization withalkali, bleached with bleaching earth or activated carbon or both, anddeodorized with Iteam, no other chemical agents being used.

2.1.2 hi·"fillltl CueOtlrl' 0;1- Coconut oU obtained by the process of101veDt extraction which ha. been neutralized with alkali, and with orwithout bleachinl with bleachins earth or activated carbon or both, noother chemical agerttl beins used,

S. TYPBI AND GIlADES

1.1 The material shall he of the following types and Rradea:

a) Ex/WusttlRefined Grade,Grade lA (Raw»)Grade IB (Raw), andGrade 2 (Raw).

..... for fOUDClbw off numerical valuet (,..iIM).tMethrxla of ampIiJII and tat rot oil. and rats (,..;,. ).

4

b) SOi,,,,,, Exlraeted

Refined Grade,Semi-refined Grade, andGrade 1 (Raw).

3.1.1 The Refined Grades of the expressed and solvent-extracted typesand the Raw Grades lA and lB of the expressed type are suitable fordirect edible consumption.

3.1.2 Raw Grade 2 of the expressed type and the other two grades of thesolvent-extracted type are suitable for hydrogenation, refining and otherindustrial uses, and not for direct edible consumption.

4. REQ,UlREMENTS

4.1 o.aerlpdoD-The material shall be obtained from good quality coco­nut cake or from clean and sound copra Cocos nucif,,(J Linn., fame Palmle,by a process of expression, .

4.1.1 Solvent-extracted oil shall be obtained from the oieaginoulmaterial using solvent hexane conforming to IS: 3470-1966*.

4.2 The material shall be clear and free from rancidity, adulterants, sedi­ment suspended and other foreign matter, separated water, and addedcolouring and flavourlng substances.

4.2.1 The clarity of the material shall be judged by the absence of turbi­dity after keeping the filtered sample at 30°C for 24 hours,

4.3 Admi.tare with Other ons - The material shall be free fromadmixture with other oils, when tested according to the methods pre..crihed under 20 of IS: 548-1964t_

4.4 'The material shall also comply with the requirements given in Table 1.

5. PACKING

.5.1 The material shall be supplied in suitable well-closed container, asagreed to between the purchaser and the supplier.

6. MARKING

6.1 The containers shall be marked with the name, including the type andgrade, and weight of the material in the container; manufacturer's nameand trade-mark, if any: batch number; and the year of manufacture.

. ·~pt'cili(".tinn (Ir hexane, food Rrade.·tt\{rthodl of ..."pling and fe-51 fill' ()il8 and fatl (r,vj,s,~).

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6.2 In addition, in the case of Grade 2 (Raw) of the expressed type oiland the Semi-refined Grade and the Grade 1 (Raw) of the solvent extractedoil, the containers shall also be suitably marked C NOT FOR DIREGrEDIBLE CONSUMPTION' (either printed on the label affixed to thecontainer or lithographed or stencilled thereon with indelible ink) in atype size of not less than 50 mm, ·

7. SAMPLING

7.1 Representative samples of the material .hall be drawn as prescribedunder" of IS: 548·1964·.

I. TESTS

1.1 Tests shall be carried out as prescribed in IS: 548-1964* and IS: 1448t.Reference to the relevant clauses of those standards is given in col 10ofTable 1.

8.2 ~Iity of RealeBa - Unless specified otherwise, pure chemicalsand distilled water (s" IS: 1070-1960:) shall be used in the tests.

No'll': - , Pure chemical. t shall mean ch~miC'.al1 that do Dot contain impuritiel whichafFrct the rt'luh. of analrlil.

·~ff'thodant IIJnplin. and t~.t for oila and fata ( r"u,4).tMethodi or tr.st Cor petroleum and itt ~Uetl.tSpecification for water di.till~ quality ( "l1fui). ~

7

BUREAU OF INDIAN STANDARDSHeadq.."".:Manlk Shlvln, 8 81hldurShih ZItIr Mlrg, NEW OELHI11 0002T~..:23230131.23233375,23238402 Fax:81+01123239398.23238382I- Mill: InfoObll.org.tn -website: http:/twww.bll.org.ln

c.n"",UbotItory:Plot No: 2018, Siterv, Sahib.bldIndultrlllAtel, SAHIBABAD 201010

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