inventory tag-out biodiesel process overview reactor glycerin isolated shipment lot shipping...

Inventory

tag-out

Biodiesel Process Overview

Reactor

Glycerin

IsolatedShipment

Lot

Shippingsample/test

PurchasingInventory Production

SalesShipping

CustomerSupport

Purchase Order

Receiving

Receiving Inspection

per material spec

Method Cut Tank “I” Reactor

SourceReactor or Holding Tank

MWTMonomer

Weigh Tank

MethanolGlycerin Recovery

MethanolBulk Methanol

Biodiesel Recovery

Glyce

rin

Me

tha

no

l

Me

tha

no

l

Me

tha

no

l

Acid Wash

Ca

taly

st

Fe

ed

sto

ck

Mu

ltip

leB

atc

he

s

D6751

Reactor-F or I

Multiple BulkStorage Tanks

INSPECTION POINTS

ReceivingList

Checklistmaterial

dependent

Glycerin Demethylation

Glycerinsales or scrap

Biodiesel

CatalystSodium Methylate

Water

Step-01

Step-02

Demethylationof Biodiesel

Step-03

Water Wash

recovery

Step-04a

Step-04b

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3/27/07

Shipment Lot Inspect

Step-05

BatchFinal

DryStep-04c

FeedstockSoybean Oil

COA

References

1. Purchase Order

01-12-0005 Listing of Quality Records 19-02-0001 Receiving & Unloading Tanker Trucks

06-09-0001 Purchase Order Procedure 19-02-0009 Receiving & Unloading Railcars

06-12-0002 Purchase Order Form 19-02-0010 Shipping Product by Tanker or Railcar

2. Receiving

06-09-0001 Purchase Order Procedure 19-12-0004 Bulk Receiving Checklist

19-02-0001 Receiving & Unloading Tanker Trucks 19-12-0005 Inventory Checklist for Bulk Receiving

19-02-0009 Receiving & Unloading Railcars 19-12-0007 Daily Receiving Report Log

19-12-0003 Railcar Checklist (Ship & Receive)

3. Receiving Inspection

11-02-0002 QA Lab Specification Transmittal Sheet (except shipment samples) 11-11-0002 Lab Spec Methanol

11-02-0013 Work Instruction for Providing Samples to QA 11-11-0003 Lab Spec Sodium Methoxide

11-11-0001 Lab Spec Soybean Oil

4. Step 01 - Reactor

23-12-0001 “I” Reactor Log Sheet 11-11-0006 Lab Spec-”I” Reactor Demethylation of Glycerin

23-12-0002 “I” Reactor Demethylation Log Sheet 11-11-0010 Lab Spec-”I” Reactor (In-Process)

23-12-0003 “H” Reactor Log Sheet 11-13-0001 Batch Step 1-Biodiesel “I” Reactor

11-02-0006 Glycerin Determination in Reactor Sample 11-13-0011 Batch Step 1-Biodiesel “H” Reactor

11-02-0008 Test Method Oil in Glycerin 23-13-0002 Biodiesel, “I” Reactor SOP

11-11-0004 Lab Spec Reactor (In-Process) 23-13-0005 Biodiesel, “H” Reactor SOP

5. Step 02 - Glycerin

11-02-0009 K-F Water Determination Method 11-11-0011 Lab Spec-”F” Reactor Demethylation of Biodiesel

11-11-0006 Lab Spec-”I” Reactor Demethylation of Glycerin 11-13-0002 Batch Step 2-Biodiesel Glycerin

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References

6. Step 03 – Demethylation of Biodiesel

11-11-0006 Lab Spec-”I” Reactor Demethylation of Glycerin 23-12-0002 “I” Reactor Demethylation Log Sheet

11-11-0009 Lab Spec Demethylation of Biodiesel 24-12-0001 Cut Tank Log Sheet

11-13-0004 Batch Step 3-Biodiesel Demethylation by Cut Tank 24-13-0001 Cut Tank Demethylation Procedure

7. Step 04 – Blend Tank

11-11-0005 Lab Spec Blend (In-Process) 23-12-0006 Isolation of Bulk Tanks Ready for Shipment

11-13-0007 Batch Step 4-Biodiesel Wash by Blend Tank 23-13-0003 Recovery of Biodiesel from Water Wash

11-13-0012 Batch Card Citric Acid Solution 23-13-0004 Biodiesel Single or Double Water Wash SOP

11-13-0013 Batch Card Biodiesel from Water Wash

8. Step 05 – Shipment Lot

11-02-0002 QA Lab Specification Transmittal Sheet (except shipment samples) 11-02-0014 WI for Relative Density Determination

11-02-0011 Determining Significant Process Change 11-02-0015 WI for COA for Shipment of Biodiesel (D6751)

11-02-0012 Shipment Lot Tank Homogeneity 11-13-0006 Batch Step 5-Biodiesel Lot D6751 COA

11-02-0013 Work Instruction for Providing Samples to QA 23-13-0006 Isolation of Bulk Tanks Ready for Shipment

9. Shipment D6751

03-02-0001 Shipment & Billing of Finished Goods Procedure 11-11-0008 Lab-Ship Sample Test

03-12-0003 Open Sales Orders Form 19-02-0010 Shipping Product by Tanker or Railcar

11-02-0003 QA STS Definitions (for D6751 Shipment) 19-12-0006 Daily Shipping Report Log

11-02-0015 WI for COA for Shipment of Biodiesel (D6751) 19-02-0004 Pulling Samples from Tankers Loaded for

11-02-0016 WI for QA STS for Ship or Past 30 Days Sample Shipment

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Document Approvals

Role/Position

(Normative)

Owner:

(informational)

Approval Date

COO Bill McIlwain

CTO Terry Boone

Role/Position Reviewed By:

QA Ravi Doshi

HSE John Roberts

Purchasing Peggy Davis

Approved By:

Document Control Jan Rector

Instructions for filling out Document Approval Form1. Identify the owner of the document who has technical authority for content.2. Identify the authority required to review and approve (authority role).3. Identify who acts within required authority for this release.4. Approval date signifies that Document Control has received acceptance of approval.5. Document Control has structural control as defined in 01-01-0001 Preparation & Release of Controlled Documents.

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Revision HistoryDate Revision No. Modification Reason

10/31/06 00 Original issue

12/7/06 01 Multiple clerical updates.

1/12/07 02 Deleted tanks under Feedstock, added Tank 81; deleted tanks under Methanol

Glycerin Recovery and Biodiesel Recovery; updated doc. number for H Reactor BC;

Deleted inspection checkpoint under Glycerin.

3/27/07 03 Add References; deleted tank numbers & document numbers in flow chart.

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