international workshop towards a ... · 2. neutron activation analysis –naa neutrons for...
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InternationalWorkshop
Towards aEuropean Research InfrastructureforHeritage
ScienceFlorence,2017March29th
SalaCapitolare,exConvento del Maglio,ViaCherubini5
FIXLAB:Accesstolarge-scale facilities
MichelMenu
MCC-C2RMF,PalaisduLouvre,Paris,France
CNRS,PSL,UMR8247,IRCP
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Purpose
Accesstolarge-scale facilities fortheCHcommunity:researchers inHeritage Sciencetosolve majorquestionsposed inarcheometry,conservationandpreservation.
Access provided tocomplementary nondestructiveinstrumentations
applied either onmicrosamples orwhole CHobjects
Elemental,structural,chemical analysis
NeutronandX-raycontrast radiography/tomography,chemical
analysis
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Whatistheorganic
contentofa
hermeticallyclosed
EgyptianPottery?
EmmanuelAbraham,MaryelleBessou,AnneZiegle,M.-C.Herve,L.Szentmiklosi,etal..Terahertz,X-rayandneutroncomputed tomography ofanEighteenth Dynasty Egyptiansealed pottery.Applied Physics A,SpringerVerlag,2014,117(3),pp.963-972.
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Neutronimaging +Promptgammaactivation=>thecontentcould consist ofgerminated seeds (orany other dried organicmaterial)such asbarley that was astaple cereal ofancient Egypt.
8Cork=ball oflinen
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Ionisationdesexcitation
X
Diffusion
onnucleusCoulombbarrier
P.I.X.E.
R.B.S.
Nuclearreaction
N.R.A.
p,d,
a
ERDA
IBAtechniques
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BNC-Wigner
HAS Centre for Energy Research
HAS Wigner Research Centre for Physics
The BNC-Wigner (Budapest) FIXLAB B(HU)
It takes advantages of the large-scale facilityBudapest Research Reactor operated by theCentre for Energy Research (EK). The national andinternational research programs are co-ordinatedby the Budapest Neutron Centre (BNC), aconsortium of EK and the Wigner Research Centrefor Physics (Wigner). Both EK and Wigner areresearch centres of the Hungarian Academy ofSciences.
The most attractive feature of BNC Wigner fornon-destructive study of CH objects is theavailability of a broad selection of neutron-basedexperimental techniques (PGAA, PGAI-NT, NAA,RAD, TOF-ND, SANS), in combination withcomplementary non-neutron methods (external-beam PIXE, XRF, etc.) on the same campus.
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1.PROMPTGAMMA
ACTIVATIONANALYSIS–
PGAA
2.NEUTRONACTIVATION
ANALYSIS– NAA
NEUTRONSFOR
ELEMENTALANALYSIS
NEUTRONSFORIMAGING
1. RADIOGRAPHY
2. NIPS-NORMA
Sample
chamber
Motorize
dsample
stage
NR/
NT
Neutron
beam
1.TIMEOFFLIGHT
NEUTRONDIFFRACTION– TOF-ND
2.SMALLANGLE
NEUTRONSCATTERING- SANS
NEUTRONSFOR
STRUCTURALSTUDIES
photograph,X-rayradiograph,neutronradiograph,PGAIdata
concentrationanddistributionofchloride ionsiniron artefactsWatkinson etal.Archaeometry 2013
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BNC-Wigner’s
IPERIONCHteam
BNC-WignerrepresentativeforGeneralAssembly:Dr.László [email protected]
substitute:Dr.Zsolt KASZTOVSZKY [email protected]
AccessBoardrepresentative:Dr.László SZENTMIKLÓ[email protected]
substitute:Dr.Adél [email protected]
Partner-levelresponsibleforcommunication(PCR):Prof.Dr.Zoltán SZÕ[email protected]
substitute:Dr.László [email protected]
Partner-levelqualityofficer(PQO)Dr.Zsolt [email protected]
substitute:Boglárka MARÓ[email protected]
FIXLABrepresentative(PRP):Dr.Imre KOVÁ[email protected]
substitute:György KÁ[email protected]
Responsibleforadministrative/financialissues(IPERIONCoordinationOffice(ICO)liaison:Katalin PÁNCZÉ[email protected]
BNCUserWelcomeDesk:Dr.Zsolt KASZTOVSZKY
[email protected] (technicalmatters)Katalin PÁNCZÉL-BAJNOK
[email protected] (culturalheritagematters)
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11beamlines used forcultural
heritage related research
Micro-XRFandX-rayabsorption(speciation)
XRD,small-angleX-rayscattering
FT-IRspectroscopy,UV/visluminescenceimaging
X-raymicrotomography
Photo-emission spectroscopy…
Anatomix
SoleilIPERION-CHleader:FrédériqueFraissard
[email protected],Gif-sur-Yvette,Fr
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TomographybeamlinesatSOLEIL
PSICHE
ANATOMIXFast and phase contrast imaging
PUMA
Resolution Energy
Fast imaging Phase contrast imaging
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Microbeam beamlines atSOLEIL
Energy
Spot size
LUCIA
NANOSCOPIUM
DIFFABS
PUMA
HERMES
10µm
1µm
10nm
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PUMA
“PhotonsUvliséspourlesMatériauxAnciens”Optimizedforancientmaterials60%(?)beamtimereservedforancientmaterials
Hard X-rays (4 - 60 keV)Imaging 2D
Fluorescencecontrast,diffractionandabsorptionresolution 3µm
Imaging 3DAbsorptionandphasecontrast d’absorptionresolution ≈1µm
Opentousers:early 2018
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SOLEIL‘team’
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AGLAEleader:[email protected]
LouvrePalace,Paris,Fr
IBA
2MVtandemaccelerator basedanalytical system
100%dedicated toCH
AGLAE
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AGLAE
Recent Applications
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Byzantine glassweights,6-7thcentury AD
B.Tobias,Univ.ofInnsbruck,Austria
Questionsandaims:• detailedcomposition• identificationoftracesofothercolours• connectionwithchronology,technology…
CharacterizationoftheMedievalglassartefactsfromMiranduolo site,
Chiusdino,Italy
I.Posedi,Univ.ofEvora,Portugal
Questionsandaims:• detailedcomposition• characterisationofdeteriorations• connectionswithestablishedregionalproductioncentres…
Ion beam analysis of glass objects
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MedievalKashiproject
ProjectLeader:LadanAKBARNIAInstitution:BritishMuseum– IranianWorld
AGLAE
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AGLAE
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AGLAE
E-RIHSFrattheUCP
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Ø InE-RIHS-FR
+LMC14 (Saclay,Fr)
+Museum’sanalyticalplatform(Paris,Fr)whichconsistsin
severaltechnicaltools:
- bio-organicmassspectrometrytechnicalplatform
- NuclearMagneticResonanceTechnicalplatform
- FluorescenceMicroscopyandDigitalImagingcentre
- ElectronMicroscopytechnicalplatform
- IsotopicAnalysistechnicalplatform
- AST-RX:X-RayTomographytechnicalplatform
- UMS2700:theMuseum’s5technicalplatformsfor
integrativesystematics
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Thanksforyourattention
MichelMenu
MCC-C2RMF,PalaisduLouvre,Paris,France
CNRS,PSL,UMR8247,IRCP
FIXLABFirenze,29March2017
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NewAGLAEproject
AGLAE’s adventure during M1-M18
themoveofAGLAEfortheNewAGLAEnext phase