infinitylab purification capillary kits technical note · 5 overview general installation notes...

InfinityLab Purification Capillary KitsTechnical Note

This note describes the capillary connections for Agilent preparative systems.

Agilent Technologies

Contents

Abbreviations 3

List of Modules 4

Overview 5General Installation Notes 5Installation Notes for 1260 Infinity II Column Organizer G9328A 6Installation Notes for 1290 Infinity II Column Compartment G7163B 8

Configurations with 1260 Infinity II Column Organizer (G9328A) 10Entry Level System Configurations (with Manual Injector) 10Standard UV/LC System Configurations 16Standard Mass-Based Systems Configuration 24

Configurations with 1290 Infinity II Preparative Column Compartment (G7163B) 28Entry Level System Configurations (with Manual Injector) 28Standard UV/LC System Configurations 34Standard Mass-Based System Configurations 40

Accessories 44UV Accessories 44MS Accessories 44

2

AbbreviationsTable 1 Abbreviations

Modules

VWD Variable wavelength detector

DAD Diode array detector

MI Manual Injector

DC Delay Coil Organizer

RC Recovery collector

FC Fraction collector

PRV Pressure relieve valve

BPR Back pressure regulator

FM Flow modulator

Fittings

R Removable fitting

for flex capillaries: 5067-5966

for rigid capillaries: 5067-5403

S Swagelock fitting

Capillaries and tubings

UV1...5 Capillaries to connect the modules of the liquid chromatographic part of the system

MS1...6 Capillaries to connect the modules of the mass spectrometric part of the system

0.3f 0.3 mm ID flex capillary

0.5r 0.5 mm ID rigid capillary

ESD Electrostatic discharge

Material

SST Stainless steel

PTFE Polytetrafluorethylene

PEEK Polyether ether ketone

3

List of ModulesTable 2 List of modules

G7161A 1260 Infinity II Preparative Binary Pump

G7161B 1290 Infinity II Preparative Binary Pump

G7114A 1260 Infinity II Variable Wavelength Detector

G7115A 1260 Infinity II Diode Array Detector WR

G7165A 1260 Infinity II Multiple Wavelength Detector

G7159B 1290 Infinity II Preparative Open-Bed Fraction Collecor

G7166A 1260 Infinity II Preparative Valve-Based Fraction Collector

G1364E 1260 Infinity II Preparative Fraction Collector

G1328D 1260 Infinity II Manual Preparative Injector

G7157A 1260 Infinity II Preparative Autosampler

G7170B 1290 Infinity II MS Flow Modulator

G9324A 1260 Infinity II Delay Coil Organizer

5067-6857 PREP Pressure Relief Valve Kit

G7163B 1290 Infinity II Preparative Column Compartment

G9328A 1260 Infinity II Column Organizer

G7110A 1260 Infinity II Isocratic Pump

5188-8053 ERI Remote and Leak Module

G6125B MSD

4

OverviewGeneral Installation Notes

Capillaries and Fittings• Capillary UV/LC kits (5067-6858, 5067-6859, 5067-6860, 5067-6809) are flow

dependent. The proper kit needs to be selected based on the desired flow range.

• The MS Upgrade kit (5067-6861) is only one kit. It contains all capillaries for all flow ranges.

• Four capillaries (UV2A, 2B, 2C, 2D) are provided to connect sampler and column.

• All capillaries with an inner diameter (ID) of 0.3 mm and 0.5 mm are flexible.

Only the MS1B capillary from column to flow modulator is always rigid. This capillary is guided between modules and needs to remain in its fixed position.

• The bypass of the flow modulator is part of accessory kit G7170-68705.

• All capillaries going to the ports of the flow modulator need UHP-FF fittings.

• The Multiple Wavelength Detector is not depicted in the drawings. The same principles as for the Diode Array Detector apply.

• Only removable fittings are used for columns.

• Either Quick Turn Fittings for flexible capillaries, or

• UHP-FF for rigid capillaries.

General rules• If the height of the stack configuration exceeds the safety limit (0.89 m), the

solvent cabinet has to be placed next to the stack on the base plate.

• The base plate is needed in case the Solvent Cabinet is placed on a bench by itself, and has to be ordered separately (p/n G1328-44111).

NOTE Do not use swagelock for the flow modulator, the ports can be damaged.

5

Installation Notes for 1260 Infinity II Column Organizer G9328A

Columns and Column Holders• To keep the capillary from column to detector as short as possible, the

column needs to be mounted at the highest possible position, and in the front of the column organizer.

• Two capillaries (UV2A, UV2B) are provided to connect sampler and column:

• UV2A is used for columns shorter than 15 cm,

• UV2B is used for long columns of 15 cm and more.

• Fix columns with the following column holders:

• M size holders (5067-6849) for 9.4 mm/10 mm, 21.2 mm and 30 mm columns,

• L size holders (G7163-60002) for 50 mm columns,

L size holders have to be ordered separately.

• The 25 cm columns require two M size holders, shorter columns need only one holder.

• One M holder can be used for pre-column.

Manual Injection Valve G1328D (MI)• The MI must be installed in the first groove of the column organizer

extrusion plate.

• The MI can be installed at any height.

• In combination with columns shorter than 25 cm, the MI can be positioned in the middle of the column organizer.

• In combination with columns 25 cm or longer, the MI needs to be installed at the lowest possible position.

• The MI requires a suitable waste container (bottle or beaker) for waste and siphoning capillaries.

NOTE The kit does not contain a waste container. The waste container must be provided by the customer. The waste container has to be placed on the leak plate.

6

• In the case that a 20 mL stainless steel loop is used, it has to be bent in the direction of the extrusion to leave enough space for the container on the leak plate. None of the other loops limit the space for the container.

• The waste and siphoning capillaries have to be bent. The end of the capillaries have to be at the same height as the position of the injection needle.

Pressure Relieve Valve (PRV, 5067-6857) and Back Pressure Regulator (BPR, 5067-6840)• PRV must be installed with every configuration.

• The PRV and BPR come with the Preparative LC system.

• The PRV is installed at the outlet of the Delay Coil Organizer, if available.

• If the PRV is used as a single item, the following measures are required:

• The PRV has to be connected with system tubing from the detector. This connection requires union 10-32 to ¼-28.

• The PRV has to be fixed to the column organizer using S holders.

• The PRV has to be placed on the upper part of the extrusion.

• The PRV waste tubing is guided to the leak plate by S holders.

• The BPR needs to be installed ahead of the Recovery Collector.

• The use of BPR is recommended only for certain flow rates, check for operating instructions.

• The BPR can be fixed at any position on the extrusion using S holders.

NOTE The PRV is required for safety reasons.

NOTE The length of the capillary from the detector to the PRV is intentionally limited.

7

Installation Notes for 1290 Infinity II Column Compartment G7163B

General• The Delay Coil Organizer must be installed at the highest valve position.

• The Flow Modulator must be installed in the second highest valve position.

• The Recovery Collector can be installed at any available free valve position.

Columns and Column Holders• The column should be mounted at the highest possible position of the

Column Compartment.

• The capillaries UV2A, UV2B, UV2C and UV2D are used to connect the column with the sampler. Select the suitable capillary length depending on the position or length of the column.

• Fix columns with the following column holders:

• M size holders (5067-6849) for 9.4 mm/10 mm, 21.2 mm and 30 mm columns,

• L size holders (G7163-60002) for 50 mm columns,

• The 25 cm columns require two M size holders, shorter columns need only one M size holder.

• One M size holder can be used for pre-column.

Manual Injection Valve G1328D (MI)• The MI should be installed on the bottom part of the small mounting plate of

the Column Compartment in the first groove.

• The MI requires a suitable waste container (bottle or beaker) for waste and siphoning capillaries.

• Columns need to be installed such that they do not collide with MI, loop or siphoning capillaries, usually on the left part of the extrusion.

NOTE The kit does not contain a waste container. The waste container must be provided by the customer. The waste container has to be placed on the plateau of the Column Compartment.

8

• The waste and siphoning capillaries have to be bent. The end of the capillaries have to be at the same height as the position of injection needle and should point down to the waste container.

Pressure Relieve Valve (PRV, 5067-6857) and Back Pressure Regulator (BPR, 5067-6840)• PRV must be installed with every configuration.

• The PRV and BPR come with the Preparative LC system.

• The PRV is installed at the outlet of the Delay Coil Organizer, if available.

• If the PRV is used as a single item, the following measures are required:

• The PRV has to be connected with system tubing from the detector. This connection requires union 10-32 to ¼-28.

• The PRV has to be fixed to the Column Compartment using S holders (5043-1356).

• The PRV has to be placed on the upper part of the extrusion.

• The PRV waste tubing is guided to the leak sensor by S holders.

• The use of BPR is recommended only for certain flow rates, check for operating instructions.

• The BPR can be fixed at any position on the extrusion using S holders.

NOTE The PRV is required for safety reasons.

NOTE The length of the capillary from the detector to the PRV is intentionally limited.

9

Configurations with 1260 Infinity II Column Organizer (G9328A)Entry Level System Configurations (with Manual Injector)Entry Level System ConfigurationsTable 3 Capillary Kit Prep UV/LC Overview

System Capillary Kit Prep LC/UV 5067-6858 5067-6859 5067-6860 5067-6809 1 kit for each flow rate

Flow range 4 – 8 mL/min

15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings

UV1 Pump Sampler 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage

UV2A Sampler Column 50 0.3f 5500-1316

0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable

UV2B Sampler Column 65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage

10

Table 4 Preparative Open-Bed Fraction Collector tubing kits (G7159B)

P/N 5067-6858 5067-6859 5067-6860 5067-6809

Preparative Open-Bed Fraction Collector tubing kit

Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)

Suitable for the flow up to

1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

Table 5 Preparative Fraction Collector tubing kits (G1364E)

P/N 5067-6858 5067-6859 5067-6860 5067-6809

Preparative Fraction Collector tubing kit

G1364-68603 G1364-68604 G1364-68605

Comment 4 – 8 mL/min 15 – 40 mL/min

40 – 100 mL/min

11

Entry Level System Configurations with Delay Coil Organizer (G9324A)Table 6 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

13


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

14

Standard UV/LC System ConfigurationsConfiguration with Preparative Open-Bed Fraction CollectorTable 9 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

16

Configuration with Preparative Open-Bed Fraction Collector and Delay Coil Organizer (G9324)Table 11 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

18

Configuration with Preparative Fraction CollectorTable 13 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

20

Configuration with Preparative Fraction Collector and Delay Coil Organizer (G9324)Table 15 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

22

Standard Mass-Based Systems ConfigurationTable 17 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

UV5 VWD/DAD

PRV 65 0.3f 5500-1308

0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage

24

-

-

N

Table 18 Upgrade Capillary kit MS-Based Prep LC

Upgrade Capillary kit MS-Based Prep LC Part No. 5067-6861

1 kit 4 – 8 mL/min

15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

1 kit only

From module

To module

Length /cm

ID / mm

Part No.

ID / mm

Part No.

ID / mm

Part No.

ID / mm

Part No.

Fittings

MS1B Column Flow modul.

90 0.3r 5500-1321

0.5r 5500-1322

0.6r 5500-1323

0.94r 5500-1403

RemovableRemovable

MS2 Flow modul.

VWD/DAD

55 0.3f 5500-1397

0.5f 5500-1400

0.6r 5500-1402

0.94r 5500-1405

RemovableSwage

MS3 Make up Flow modul.

120 0.12 5500-1398

FLOW INDEPENDENT CAPILLARIES Swage-Swage

MS4 Flow modul.

MS 120 0.12 5500-1398

Swage-Swage

MS5 MS restriction capillary

7 0.12 5500-1329

Swage-Swage

MS6 MS waste capillary

70 0.25 5500-1330

Swage-NO


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

25


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

Length/cm ID/mm Part No. Fittings

FM1 8 0.25 5067-6820 Removable-Swage

FM2 10 0.12 5067-6821 Swage-Swage

26

Configurations with 1290 Infinity II Preparative Column Compartment (G7163B)Entry Level System Configurations (with Manual Injector)Entry Level System ConfigurationTable 21 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable

UV2C Sampler Column 80 0.3f 5500-1406

0.5f 5500-1384

0.6r 5500-1387

0.94r 5500-1392

Swage-Removable

UV2D Sampler Column 100 0.3f 5500-1407

0.5f 5500-1385

0.6r 5500-1388

0.94r 5500-1394

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

28


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

29

Entry Level System Configuration with Delay Coil Organizer (G9324A)Table 24 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable


0.5f 5500-1384

0.6r 5500-1387

0.94r 5500-1392

Swage-Removable


0.5f 5500-1385

0.6r 5500-1388

0.94r 5500-1394

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

31


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

32

Standard UV/LC System ConfigurationsStandard UV/LC System ConfigurationsTable 27 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable


0.5f 5500-1384

0.6r 5500-1387

0.94r 5500-1392

Swage-Removable


0.5f 5500-1385

0.6r 5500-1388

0.94r 5500-1394

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

34


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

35

Standard UV/LC System Configurations with Delay Coil Organizer (G9328A)Table 30 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable


0.5f 5500-1384

0.6r 5500-1387

0.94r 5500-1392

Swage-Removable


0.5f 5500-1385

0.6r 5500-1388

0.94r 5500-1394

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

37


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

38

Standard Mass-Based System ConfigurationsTable 33 Capillary Kit Prep UV/LC Overview



15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

From module

To module

Length/cm

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

ID/mm

Part no.

Fittings


0.5f 5500-1309

0.6r 5500-1318

0.94r 5500-1390

Swage-Swage


0.5f 5500-1317

0.6r 5500-1320

0.94r 5500-1391

Swage-Removable


0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Swage-Removable


0.5f 5500-1384

0.6r 5500-1387

0.94r 5500-1392

Swage-Removable


0.5f 5500-1385

0.6r 5500-1388

0.94r 5500-1394

Swage-Removable

UV3 Column VWD/DAD

65 0.3f 5500-1314

0.5f 5500-1315

0.6r 5500-1319

0.94r 5500-1393

Removable-Swage

UV4 VWD/DAD

DC Box/PRV

55 0.3f 5500-1408

0.5f 5500-1386

0.7r 5500-1389

0.94r 5500-1395

Swage-Swage

40

-

-

N

Table 34 Upgrade Capillary kit MS-Based Prep LC

Upgrade Capillary kit MS-Based Prep LC Part No. 5067-6861

1 kit 4 – 8 mL/min

15 – 40 mL/min

40 – 80 mL/min

80 – 200 mL/min

1 kit only

From module

To module

Length /cm

ID / mm

Part No.

ID / mm

Part No.

ID / mm

Part No.

ID / mm

Part No.

Fittings

MS1A Column Flow modul.

50 0.3f 5500-1396

0.5f 5500-1399

0.6r 5500-1401

0.94r 5500-1404

RemovableRemovable

MS2 Flow modul.

VWD/DAD

55 0.3f 5500-1397

0.5f 5500-1400

0.6r 5500-1402

0.94r 5500-1405

RemovableSwage

MS3 Make up Flow modul.

120 0.12 5500-1398

FLOW INDEPENDENT CAPILLARIES Swage-Swage

MS4 Flow modul.

MS 120 0.12 5500-1398

Swage-Swage

MS5 MS restriction capillary

7 0.12 5500-1329

Swage-Swage

MS6 MS waste capillary

70 0.25 5500-1330

Swage-NO


P/N 5067-6858 5067-6859 5067-6860 5067-6809


Tubing Kit 8 (G9321-60953)

Tubing Kit 50 (G9321-60952)

Tubing Kit 150 (G9321-60954)

Tubing Kit 200 (G9321-60951)


1 – 8 mL/min 15 – 50 mL/min

50 – 150 mL/min

150 – 200 mL/min

41


P/N 5067-6858 5067-6859 5067-6860 5067-6809


G1364-68603 G1364-68604 G1364-68605


40 – 100 mL/min

Length/cm ID/mm Part No. Fittings

FM1 8 0.25 5067-6820 Removable-Swage

FM2 10 0.12 5067-6821 Swage-Swage

42

AccessoriesUV Accessories

MS Accessories

Table 37 Accessories for kits 5067-6858, 5067-6859, 5067-6860, 5067-6809

A-Line Quick Turn LC Fitting for Column 2 pcs for kits 5067-6858 and 5067-6859 5067-5966

UHP-FF FITTING for Column 2 pcs for kits 5067-6860 and 5067-6809 5067-5403

3m Tube ESD PTFE OD2.5 ID1.6 5023-3086

ESD-Fitting OD-2.5mm 5023-2871

Union Flat-Bottom 1/4-28 ESD 5023-2508

Plastic and PEEK tubing cutter 8710-1930

Fitting-Handle 5043-1471

Sealtight-Handle 5043-0915

Table 38 Accessories

3 m Tube ESD PTFE OD 2.5 ID 1.6 5023-3086

ESD-Fitting OD-2.5 mm 5023-2871

Fitting adapter 10-32 to 1-4-28 SST 5023-2875

TEE-LOW DEAD VOLUME 0100-1818

Fitting-Handle 5043-1471

Sealtight-Handle 5043-0915

NOTE The flow modulator bypass is part of the G7170-68705 Flow Modulator Accessory Kit.

*G7161-90201**G7161-90201*G7161-90201

Part Number:G7161-90201

Edition: 11/2017Printed in Germany

© Agilent Technologies, Inc 2017

Agilent Technologies, IncHewlett-Packard-Strasse 8

76337 Waldbronn, Germany

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