in house validation from direct determination of 5-hydroxymethyl-2-furfural

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  • 7/24/2019 In House Validation From Direct Determination of 5-Hydroxymethyl-2-Furfural

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    IN HOUSE VALIDATION FROM DIRECTDETERMINATION OF 5-HYDROXYMETHYL-

    2-FURFURAL (HMF) IN BRAZILIAN CORNAND CANE SYRUPS SAMPLES BY HPLC-UV

    Nadia Citta 12/329521/TP/10309Muktiadin Latifah

    12/333186/TP/10447 Imasni Satiani

    13/346395/TP/10548

    N!ma "#i S$%tian13/346454/TP/10561"uanti &ktaani

    13/346483/TP/10577'$a (anisah

    13/348620/TP/10717

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    Intro!"t#on

    C!n s)u%s a$ a%%*i$d ass#$$t$n$s and a*s! as a hum$+tant,

    Can$ s)u% has -$$n a%%*i$d as anin.$di$nt in +!nf$+ti!n$) %!du+tss!ft dinks +andi$s and $$n as as)u% su-stitut$ in +$tain t)%$s !ffuit %$s$$s,

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    S)u% M"is$as

    $s

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  • 7/24/2019 In House Validation From Direct Determination of 5-Hydroxymethyl-2-Furfural

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    M$t%r#$&

    M 99

    (+$t!niti*$ PLC .ad$*ta%u$ #at$ 0,055 =S/+mSi> +!n s)u%s sam%*$s +!d$d S1S6Si> +an$ s)u%s +!d$d CS1CS6

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    S$'&% $n St$n$rSo&!t#on Pr%$r$t#on

    Standad ; 1,05,0 m./LS1?S6 ; 0,5 . in 250 mL

    CS1CS6; 0,5 and 3,0 . in 100 mL

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    C*ro'$to+r$*#""on#t#on

    @$$:$ PLC s)st$mPh$n!m$n$> +!*umn Luna C18 5,0

    =m 4,6 > 150 mm at 30!

    CM!-i*$ %has$ ; #at$ #ith 0,5