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IDENTIFICATION AND LOCATION OF SAMPLES

SAMPLING OF JANUARY 12, 1984

ANALYSIS NO: CLIENT IDENTIFICATION

H543 STA. 01 Side of Sludge Pile

H544 STA. 02 12-18" Down into Sludge LagoonH545 STA. 03 Sediment downstream of Lagoon

H546 STA. 04 Top of LagoonH547 STA. 05 Drum No. 1 *•H548 STA. 06 Drun No. 2H549 STA. 08 Drum No. 4

H550 STA. 09 Bleach Bottle

H551 STA. 10 Drum No. 6H552 STA. 11 Drum No. 7 :'!

H553 STA. 12 Black SludgeH554 STA. 13 Green Powder in plastic bags

All information regarding these samples, location, identification, date,time, preservation, etc., where sample collection has been performed byclients' representative, is as represented to us by the client.

CENTURYLABORATORIES, INC.P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO: SE-1-011884-96Am^« r, ,_ r, SE-2-01 1984-16 1ATTN: Robert Keating

SAMPLE I.D.: STA. 01, 1/12/84, 0900, Side of Sludge PileH543

CERTIFICATE OF ANALYSIS

RESOURCE CONSERVATION AND RECOVERY ACT (RCRA)

EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/I) (mg/1).,.

D004 Arsenic 5.0 <0.002D005 Barium 100.0 0.1D006 Cadmium 1.0 <0.01D007 Chromium 5.0 <0.01D008 Lead 5.0 2.42D009 Mercury 0.2 < 0.0002D010 Selenium 1.0 <0.005D011 Silver 5.0 <0.01D012 Endrin 0.02 <0.001D013 Lindane 0.4 <0.001D014 ' . Methoxychlor 10.0 <0.001D015 Toxaphene 0.5 <0.001D016 2,4-D 10.0 <0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

——— PCB 50.0 <0.001—— pK10% solution) ——— 5.6—— Flash Point 60°C >90°C—— Corrosiveness

Reactivity(HCN) <5mg/lReactivity(H2S) <5mg/l

LAB COMMENT:

DEP Certification No. 08153

CENTURYLABORATORIES, INCP.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-1-Q11884-97

ATTN: Robert Keating

SAMPLE I.D.: STA. 02, 1/12/84, 0910: 12-18" Down into sludge lagoonH544



EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1)

D004 Arsenic 5.0 <0.002D005 Barium 100.0 <Q.lD006 Cadmium 1.0 <0.01D007 Chromium 5.0 0.20D008 Lead 5.0 4.08D009 Mercury 0.2 < 0.0002DO 10 Selenium 1.0 < 0.005D011 . Silver 5.0 <0.01D012 Endrin 0.02 <0.001D013 Lindane 0.4 ^ 0.001D014 Methoxychlor 10.0 <0.001DO 15 Toxaphene 0.5 <0.001D016 2,4-D 10.0 <0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

——— PCB 50.0 <0.001——— pH (10% Solution) ——— 5.1—— Flash Point 60°C 57°C——— Corrosiveness

Reactivity (HCN) <5mg/lReactivity(H2S) <5mg/l

LAB COMMENT:

0013



CLIENT: 'ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-1-011884-98ATTN: Robert Keating

SAMPLE I.D.: H545; STA.03:1/12/84-0915: Sediment downstream of lagoon

CERTIFICATE OF ANALYSIS ' *


EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) .„

D004 Arsenic 5.0 < 0.002D005 Barium 100.0 <r0.1 "D006 Cadmium 1.0 0.08D007 Chromium 5.0 <0.01D008 Lead • 5.0 <0.05D009 Mercury 0.2 <0.0002DO10 Selenium 1.0 <0.005D011 Silver 5.0 <0.01D012 Endrin 0.02 <0.001D013 Lindane 0.4 <T 0.001D014 Methoxychlor 10.0 <0.001D015 Toxaphene 0.5 <0.001D016 2,4-D 10.0 <-0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

—— PCB 50.0 <0.001—— pH (10% Solution) ——— 7.2——— Flash Point 60°C 56°C——— Corrosiveness


LAB COMMENT:



CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-1-011884-99

ATTN: Robert Keating TH-565-1214"163

SAMPLE I.D. : H546:STA. 04: 1/12/84-0920: Top of Lagoon



EPA MAXIMUM SAMPLEHAZARDOUS '. IE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) ,.

D004 Arsenic 5.0 < 0.002.D005 Barium 100.0 <0.1D006 Cadmium 1.0 <0.01D007 Chromium 5.0 <0.01D008 Lead 5.0 1.00D009 Mercury 0.2 < 0.0002DO 10 Selenium 1.0 <0.005D011 Silver 5.0 <:0.01D012 Endrin 0.02 <0.001DO 13 Lindane 0.4 <0.001D014 Methoxychlor 10.0 <0.001DO 15 Toxaphene 0.5 < 0.001D016 2,4-D 10.0 <0.001D017 2,4,5-TP (Silvex) 1.0 < 0.001

——— PCB 50.0 <0.001——— pH(10% Solution) ——— 5.7——— Flash Point 60°C 48°C—— Corrosiveness

Reactivity(HCN) <5mg/lReactivity(HzS) <5mg/l

LAB COMMENT:


i CENTURY•\ LABORATORIES, INC.S \ P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086?__J Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO: SE-1-011884-100 & 106ATTN: Robert Keating SE-2-011984-165

TH-565-122

SAMPLE I.D.: H547: STA.05-1/12/84-1215: Drum No. 1



EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) .

D004 Arsenic 5.0 <0.002D005 Barium 100.0 ' . 0.3D006 Cadmium 1.0 <0.01D007 Chromium 5.0 <0.01D008 Lead 5.0 <0.05D009 Mercury 0.2 < 0.0002DO10 Selenium 1.0 <0.005D011 . Silver 5.0 <0.01D012 Endrin 0.02 <0.001D013 Lindane 0.4 <0.001DO14 Methoxychlor 10.0 <0.001D015 Toxaphene 0.5 <0.001D016 2,4-D 10.0 -<0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

——— PCB 50.0 * 0.001——— pH (10% Solution) ——— 3.4——— Flash Point 60°C 28°C——— Corrosiveness


LAB COMMENT:

A_ * V_


CENTURYLABORATORIES,P.O. Box 248/1501 Grandview Avenue/Mt antic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1n5090 Central HighwayPennsauken, N.J. CHART NO; SE-1-011994-101

ATTN: Robert Keating

SAMPLE I.D.: H548: STA. 06-1/12/84-1225: Drum No. 2



EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) :rj

D004 Arsenic ' 5.0 0.031--D005 Barium 100.0 0.2D006 Cadmium 1.0 <0.01D007 Chromium 5.0 3.69D008 Lead 5.0 8.14D009 Mercury 0.2 *DO 10 Selenium 1.0 < 0.005D011 Silver 5.0. «i0.01D012 Endrin 0.02 0.001D013 Lindane 0.4 0.001D014 MetThoxychlor 10.0 *:0.001D015 Toxaphene 0.5 <:0.001D016 2,4-D 10.0 <0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

—— PCB 50.0 <0.001—— pH (10% Solution) ——— 3.1——— Flash Point 60°C 30°C——— Corrosiveness

Reactivity(HCN) <*5mg/lReactivity(H2S) <5mg/l

LAB COMMENT: * Cannot run, due to sample matrix.

II


CENTURYLABORATORIES, INCP.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-1-011984-1Q3 & 108ATTN: Robert Keating TH-565-123

SAMPLE I.D.: H549: STA. 08: 1/12/84-1520: Drum No. 4

CERTIFICATE OF ANALYSIS *


EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) .„

D004 Arsenic 5.0 <0.002_D005 Barium 100.0 0.9D006 Cadmium 1.0 <0.01D007 Chromium 5.0 <0.01D008 Lead 5.0 0.12D009 Mercury 0.2 < 0.0002DO 10 Selenium 1.0 < 0.005D011 Silver 5.0 <0.01DO 12 Endrin 0.02 <0.001D013 Lindane 0.4 <0.001D014 Methoxychlor 10.0 .0.001D015 Toxaphene 0.5 <;0.001D016 2,4-D 10.0 0.001D017 2,4,5-TP (Silvex) 1.0 -cO.OOl

——— PCB 50.0 <0.001—— pH (10% Solution) ——— 1.5——— Flash Point 60°C 54°C——— Corrosiveness


LAB COMMENT:


i CENTURY•|x LABORATORIES, INC.^S \ P.O. Box 248/1501 Grandview Avenue/Mid Atlantic Park, Thorofare, NJ 08086^___J Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-2-011984-166ATTN: Robert Keating

SAMPLE I.D.: H550: STA.09:1/12/84-1522: Bleach Bottle

CERTIFICATE OF ANALYSIS *


EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) .,

D004 Arsenic 5.0 0.26 '.D005 Barium 100.0 0.2 ""'D006 Cadmium 1.0 0.15D007 Chromium 5.0 13,800D008 Lead 5.0 2.16D009 Mercury 0.2 <0.0002DO 10 Selenium 1.0 0.74D011 Silver 5.0 0.32D012 Endrin 0.02 0.001D013 Lindane 0.4 <0.001D01 Methoxychl 10.0 <0.001D015 Toxaphene 0.5 <0.001D016 2,4-D 10.0 <0.001D017 2,4,5-TP (Silvex) 1.0 0.001

——— PCB 50.0 <0.001—— pH (10% Solution) —————— Flash Point 60°C 50°C——— Corrosiveness *

Reactivity(HCN) *Reactivity(H2S) *

LAB COMMENT: * Cannot run, insufficient sample.

<? ^ -,


I CENTURY|\ LABORATORIES, INC.^S \ P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086^ ^ Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED: 1/13/845090 Central HighwayPennsauken, N.J. CHART NO: SE-1-011984-109

SE-^-Ui 1904-10 / tt L/5ATTN: Robert Keating TH-565-124

SAMPLE I.D.: H551: STA. 10: 1/12/84-1524: Drum No. 6



EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) ...

D004 Arsenic ' 5.0 <0.002-D005 Barium 100.0 <0.1D006 Cadmium 1.0 <0.01D007 Chromium 5.0 0.03D008 Lead 5.0 <0.05D009 Mercury 0.2 <0.0002D010 Selenium 1.0 <0.005D011 Silver 5.0. <0.01D012 Endrin 0.02 <0.001D013 Lindane 0.4 <0.001DO14 Methoxychlor 10.0 <0.001DO 15 Toxaphene 0.5 < 0.001D016 2,4-D 10.0 <0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

——— PCS 50.0 <0.001——— pH(10% Solution) ——— 2.4—— Flash Point 60°C 23°C—— Corrosiveness


LAB COMMENT:

ft i I O


I CENTURYi\ LABORATORIES, INC.^S \ P.O. Box 248/1501 Grandview Avenue/MidAtlantic Park, Thorofare, NJ 08086_J Phone: (609) 848-3939 NJ 800-222-0589

CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED: 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-1-Q11984-104ATTN: Robert Keating SE-2-011984-170

SAMPLE I.D.: H552: STA.11: 1/12/84-1529: Drum No. 7

CERTIFICATE OF ANALYSIS ' v


EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) '.,

D004 Arsenic 5.0 <0.002_.D005 Barium 100.0 0^6 ""D006 Cadmium 1.0 < 0.01D007 Chromium 5.0 <0.01D008 Lead 5.0 <0.05D009 Mercury 0.2 < 0.0002DO 10 Selenium 1.0 < 0.005D011 Silver 5.0 <0.01D012 Endrin 0.02 0.001D013 Lindane 0.4 <0.001D014 Methoxychlor 10.0 <0.001D015 Toxaphene 0.5 ^rO.OOlD016 2,4-D 10.0 0.001D017 2,4,5-TP (Silvex) 1.0 0.001

——— PCS 50.0 <0.001——— pH(10% Solution) ——— 4.8——— Flash Point 60°C 46°C—— Corrosiveness


LAB COMMENT:



CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO: SE-1-011984-107ATTN: Robert Seating SE-2-011984-16

SAMPLE I.D.: H553: STA. 12-1/12/84-1531: Black Sludge



EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) :~

D004 Arsenic 5.0 < 0.002- -D005 Barium 100.0 o!lD006 Cadmium 1.0 >0.01D007 Chromium 5.0 <:0.02D008 Lead 5.0 <i.0.05D009 Mercury 0.2 0.0002DO 10 Selenium 1.0 0.005D011 Silver 5.0 0.01D012 Endrin 0.02 0.001D013 Lindane 0.4 <0.001D014 Methoxychlor 10.0 <0.001D015 Toxaphene 0.5 0.001D016 2,4-D 10.0 <.0.001D017, 2,4,5-TP (Silvex) 1.0 <:0.001

LAB COMMENT:

PCB 50.0 <£pH (10% Solution) ——— 3.6Flash Point 60°C 30°CCorrosivenessReactivity (HCN) <*5mg/lReactivity(H2S) <:5mg/l

rDEP Certification No. 08153


CLIENT: ROY F. WESTON, INC. SAMPLE RECEIVED; 1/13/845090 Central HighwayPennsauken, N.J. CHART NO; SE-1-011984-105A™™ 0 u v SE-2-011984-172ATTN: Robert Keating

SAMPLE I.D.: H554: STA. 13: 1/12/84-1539: Green Powder in Plastic Bags



EPA MAXIMUM SAMPLEHAZARDOUS WASTE CONCENTRATION VALUEI.D. NUMBER CONTAMINANT (mg/1) (mg/1) Lr;

D004 Arsenic 5.0 <0.002.D005 Barium 100.0 ' <0.1D006 Cadmium 1.0 4.2D007 Chromium 5.0 0.04D008 Lead 5.0 0.11D009 Mercury 0.2 <r 0.0002DO 10 Selenium 1.0 <: 0.005D011 . Silver 5.0 0.01DO 12 Endrin 0.02 <0.005DO13 Lindane 0.4 0.001D014 Methoxychlor 10.0 <0.001DO 15 Toxaphene 0.5 <0.001D016 2,4-D 10.0 <:0.001D017 2,4,5-TP (Silvex) 1.0 <0.001

——— PCB 50.0 <0.001—— pH(10% Solution) ——— 4.8——— Flash Point 60°C >90°C—— Corrosiveness

Reactivity(HCN) 5.6mg/lReactivity(H2S) < 5mg/l

LAB COMMENT:

\&»w»* R. .

II


CLIENT; RO? F. WESTON. INC._________ ANALYSIS NOS: H544,H545,H547

RESULTS OF LABORATORY ANALYSIS

DETECTIONLEVEL(mg/kg) H544 H545 H547

II. WET BENCH CHEMICAL ANALYSIS

ANTIMONY 0.5 5.8 23<2 Q>2

ARSENIC 0.5 9<1 2.9 <0.1

BERYLLIUM 0.5 <0.5 <0.3 - <0.5CADMIUM 0.5 o.5 84,400 ' * 0.9CHROMIUM(TOTAL) 0.5 343 Q.9 2.7

COPPER 0.5 1630 206 2.3LEAD 0.5 12,600 5.3 7.3MERCURY 0.5 0.2 <0.1 <0.1

NICKEL 0.5 7.3 3.4 <-'f.3SELENIUM 0.5 2.0 4.4 .O.8

SILVER 0.5 1.5 <0.3 <0.4THALLIUM 0.5 <5.0 <;4.0 <5.0ZINC 0.5 284 531,000 216


CYANIDE 1.0 5.5 0.86 1.7

PHENOL <0.1 48.o 2.6 5.3

CLIENT: ROY F. WESTON, INC._________ ANALYSIS NOS; H548,H549,H550


DETECTIONLEVEL(mg/kg) H548 H549 H55Q

ANTIMONY 0.5 0.13 <0.3 0.79

ARSENIC 0.5 0.031 0.2 0.26BERYLLIUM 0.5 <o.5 <0.2 , 0.02CADMIUM 0.5 <0.01 <0.1 0.15CHROMIUM(TOTAL) 0.5 3.69 <0.1 13,800COPPER 0.5 0.14 <0.1 0.37LEAD 0.5 8.14 <0.7 2.16MERCURY 0.5 * <0.1 < 0.-0002

NICKEL 0.5 <0.05 <0.6 1-?18SELENIUM 0.5 <0.005 -0.3 0:74SILVER 0-5 <0.01 <0.1 0.32THALLIUM 0.5 <0.1 <1.0 1.8ZINC 0.5 0.18 0.4 0.38


DETECTIONLEVEL (mg/kg) H548 H549 H550

CYANIDE 1.0 0.67 1.5 0.96

PHESOL

CLIENT; ROY F. WESTON, INC._________ ANALYSIS NOS: H551 ,H552,H553


DETECTIONLEVEL(mg/kg) R551 H552 H553


ANTIMONY 0.5 1<9 <Q>2

ARSENIC °'5 0.5 <0.1BERYLLIUM 0.5 <0.5 <Q>4CADMIUM 0.5 <0.5 <Q>4CHROMIUM(TOTAL) 0.5 3.3 g>8 131

COPPER °'5 '1.6 <0.4 <0.5LEAD °-5 99.4 <1.9 <2.4MERCURY 0.5 <0.1 <0.1 <g.lNICKEL 0.5 8.7 4.5 < g4

SELENIUM 0.5 < 0.3 <0.2 <0.-2SILVER 0.5 <0.5 <0.4 <0.5THALLIUM 0.5 <5.0 <4.0 <5.0

ZINC 0.5 4510 15.0 24.8


CYANIDE 1.0 0.10 0.10 0.10

PHENOL <0.1 3.1 0.77 0.16

CLIENT: ROY F. WESTON, INC. v_____ DATE OF ANALYSIS: 1/18/84T011684-03

ANALYSIS NO.: H544(STA.#02) CHART NO.: FRN 20080 CRN 105

( 1,2,4-trlchlorobenzene N.D. '4V) benzene___________€ hexachlorobenzene N.D. (6V) carbon tetrachloride______N.D*-._

27B

(I3B

(53B54B55B,56862B

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSMG/KG MG/KG

ERA f EPA I2lA) 2,4,6-trichlorophenol___N.D.22A) p-chloro-m-cresol N D24A) 2-chlorophenol _____N.D

73B) benzo a)pyrene_________N.D.74B)benzo b)f1uoranthene N.D.75B) benzo k)f1uoranthene N.D.

31A) 2,4-dichiorophem3T _____ N.D. ____ (76B) chrysene N.D._____ .. ____ ..34A) 2,4-dimethyl phenol N.D. (77B) acenaphthylene N.p7

j(57A) 2-rn'trophenol N.D. (78B) anthracene N.D.|(58A, 4-m'trophenol_________N.D. (79B) benzo(qhi )pery1ene ' N.D.

2,4-dinitrophenol '____N.D. (80B) fluorene ____________N.D.4,6-dinitro-2-methy1phenol N.D. (81B) phenanthrene N.D.60A . . . . . . . . _ .......... ., _______^______________

64A) pentachlorophenol '_____N.D. (82B) d1benzo(a.h)anthracene N.D.(65A) phenol N.D. (83B) indeno'(1.2.3-cd)pyrene

T84B) pvrene N.o7(61B) N-Nitrosodimethylaim'ne . N.D.

BASE/NEUTRAL COMPOUNDS ' VOLATILES "-;EPA f MG/KG ' EPA * -.-MG/KG

IB) acenaphthene N.D. (2V) acroleinBR) benzldine N.D. '3V) acrylom'trile

(12B) hexachloroethane N.D! (7V) chlorobenzene__________N.D....._18B) bis(2-cri1oroethyl Jether N.p. (10V) 1,2-dichloroethane20B) 2-chloronaphthalene N.D. ~ (11V) l.l.l-trichloroethane_____N^25BJ 1,2-dichlorobenzene N.D. ~ (13V) 1.1-dichloroethane N..D.____26B) 1,3-dichlorobenzene______N.D. (14V) 1.1.2-tn'chloroethane N.D

1,4-dlchlorobenzene 91 TBV1 1.1,2,2-tetrachloroethane28B 3,3'-dich1orobenzidine____N.D. (16V) chlorethane _______N.D.._35B 2,4-dim'trotoluene_______N.D. (19V) 2-chloroethvlvinyl ether N.D.36B 2.6-d1n1troto1uene_______N.D. (23V) chloroform ________N-D-._13TB 1.2-diphenylhydrazine_____N.D. (29V) 1.1-dichloroethene _____N_.D1_39B) fluoranthene N.D. (30V) trans-1.2-dich1oroethene N.D._40B) 4-chlorophenyl phenyl ether N.D. (32V) 1,2-dlchloropropane ______N-D-(41B) 4-bromophenyl phenyl ether N.D. (33V) trans-l,3-dich1oropropene N.D. _(42B) bis(2-ch1oroisopropy1)ether N.D. ___c1s-l,3-dich1oropropene~J——'' '!_•'_'. 4, ' . ^' "'J _ ' .' •_ i »iTiiiiii • L—"i ••• " ——- —' '"" "" "yjL1 JKT'I 't'~ ——- i, i > i i i ••-bis(2-chloroethoxy)methane N.D. (38y) ethyl benzene ________N.D..—

hexachlorobutadiene______N.D. (44V) methylene chloride ____N.D...—(52B. __________________ __ ____________hexachlorocyclopentadlene N.D. J45V) chloromethane ________ N.D..isophorone _____________ N.D. (46V) bromomethane _^ ______ N.D..naphthalene _______N.D. (47V) bromoforninitrobenzene N.D. (48V) bromodichloromethane_____NtD,,N-mtrosodl phenyl amine____N.D.

t63B) N-mtrosodipropyTamine____N.D. _______________6PQ) bis(2-ethy1hexy1)phtha1ate N.D. (51V) chlorodi bromomethane_____NJt ) benzyl butyl phthalate_____N.D. (85V) tetrachloroethene

dl-n-butyl phthalate m (86V) toluene^(69B) di-n-octyT)htha1ate N.D. (87V) trlchloroethene(70B) dTethyl"pHlTaTa"te N.D. (88V) vinyl chloride(71B) dimethyl phthalate N.D~(72B) benzo(a)anthracene N.D.Z

CLIENT: ROY F. WESTON. INC.________ DATE OF ANALYSIS: 1/18/84

TQ11684-Q3_____

ANALYSIS NO.: H544(STA.#02)_________ CHART NO.: FRN 2QQ80 CRN 105

PESTICIDES , PESTICIDES .„MG/KG MG/KG

EPA I EPA f(89P90P91P92P

aldrin N.D.dieldrin N.D.chlordane N.D.

103P) B -BHC N.D.104P) g -BHC __________N.D.105P

4.4'-DDT________________________________34 (106P4.4'-DDE _________N.D. (107P

(94P) 4,4f-DDD _______N.D. (108P95P) «x -endosulfan N.D. (109P96P) £ -endosulfan . N.D. (HOP) PCB-I24897P98PTHE

endosulfan sulfate_______N.D.

Y -BHC_____________N.D.PCB-1242 N.D.PCB-1254 N.D.PCB-1221 N.D.PCB-1232 - N.D.

M n

endrin1UP) PCB-1260 _M_n

endrin aldehyde __ N.D. (113P) toxaphen?112P) PCB-1016___________________N_n_

(lOOP) heptachlor___________N.D.101PJ heptachlor epoxide______N.D. DIOXINS102P) o< -BHC N.D. I (129B) 2.3,7,8-TCDD (Screen Only).--: **

NOTES AND COMMENTS:

COMPOUND-NOT TESTED

** SCREENED/NOT PRESENT

VOLATILE ORGANICS - N.D. =<0.1mg/kg

BASE NEUTRALS = N.D. = <5mg/kg

ACID EXTRACTABLES =» N.D. = <5mg/kg

PESTICIDES s N.D. = <5mg/kg

Thomas F. Cullen, Jr.Laboratory Director/Organics Division

LAB CERTIFICATION #: 08153

H0S44,UESTON+IS (2 + 4 )E= 1800 Mdil 20680 . |ip|l05TFC,1640,011684,SE-54 2925 SCflNS (1230 SCflNS, 24.42 MINS)r*x 8.0 Mfl S RflNGE: 4 .0, 446.5 TOTflL flBUND= 474S8J3.

I I I I I I I I I I I I I I I I I I I I I I I I 1 I3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26

WV-v vs.. ——1I I I I I I I I I I4 5 6 7 8 9 1 0 1 1 1 2 1 3

MINS

« 358 RET. TIME: 8.90 TOT flEUND= 1488. ERSE PK/RBUND: 146.0/ 275.

100-1.

80-

60-

40-

20-

0-

18.5146

1 ,4-DICHLOROBEHZEHE

44

II

75 „ 1U

50 60

, |i i i l l i l i i l l i i l l60

9384

ll III 1 ll II105

1 1 ' 1

*

iFj80 100 120 140

H0544,WESTON+IS(2 + 4) E = 1800 USil 20086 , ___TFC, 1648 ,011684,SE-54 2925 SCflNS ( 915 SCflNS, 18.62J1INS)

2.8 ' MflSS RflNGE: 41.8, $46'5 ]"OTRL ^IBUND^ , . ^

I I I I I I I I I I I I I I I I I I I27 28. 29 39 31 32 33 34 35 36 37 38 39 46 41 42 43

MINS

*1394 RET. TIME: 29.62 TOT flEUND= 718. BflSE PK/flEUND: 149.0x 162.

180-1,

80-

60-

46-

20-

0-

IH-n-BUTYL PHTHflLRTE COELUTIHG 149WITH flN UNKNOWN HYDROCflRBON

44

I

5769

1 | [ •

85 97 ^

ll| ll,l|l 1• 1 * 1 " t ' l

60 80 100

11 123

111 |l' 1 * 1 1

161

I• |

120 148 160

14.2

AB 100029179 205

, , 1 . , . ,11**

130 200

H0544 ,WESTON+IS(2 + 4) E=1800 H3!i 28080. IgsHBiasTFC,1640,011684,SE-54 2925 SCflNS (2874 SCflNS, 57.62 MINS)>x 2.0 MflSS RflNGE: 41.0, 446.5 TOTRL RBUND= 4745853.

I I—— I T r" I I I I I I I I I I I I I I i6 9 12 15 18 21 24 27 36 33 36 39 42 45 48 51 54 57

MINS

*1590 RET. TIME: 33.43 TOT flBUND= 2037. BflSE PK/flBUND: 57.2/ 189.

100-

50-

8-108-

50-

0-

57 71 85•43 ' l

97 m 125 i:1 i 1 i , 1 ll II , i ii hll 1 1 1 1 III t l i l l l hi mill, i i i i t i"J'r- ,— ' +J. i-)--i-,..iu.j-Li_il..ji|i.Lii (i in.if.1..., .ijiu , ,M I^-IUHH-J ,j_) ——— j —— _, — _! ——— ,_,.._!-_, r ., ——— j_

66 88 106 120 140 160 18£

235 *4,4'-DDT COELUTING WITH flNUNKNOWN

182 20@ 211 305i 1 i i i i i 1 1

260 220 240 ' 260 280 300

•9.28

9.28

f

CLIENT: ROY F. WESTON. INC._______ DATE OF ANALYSIS: January 16. 1984TO11684-05 ______

ANALYSIS NO.: H545 STA #3. CHART NO!: FRN-10059

Z1A

24A31A

{SlAr57AF58A59A60A

53B54B55R56B

CRN-2

ACID COMPOUNDS MG/KG BASE/NEUTRAL COMPOUNDS MG/KG

EPA * EPA t2,4,6-trichlorophenol N.D.p-chloro-m-cresol_______N.D.2-chlorophenol__________N.D.

73B74B75B

benzo(a)pyrene N.D,benzo(b)fiuoranthene___N . p_.

2.4-dichlorophenol_______N.D. (76B) chrysenebenzoTtQfluoranthene N.D,

2.4-dimethylphenol_______N.D. (77B) acenaphthylene __———JLJLi- » -r—u i HIE; v.iiJ i MIÎIW i_______________" ' ~ '_____ : .———— ———c————«————————————'—————————————————iT p,2-nitrophenol__________N.D. (78B) anthracene ——————„————M..4 - n i t r o p h e n o l N . D . (79BJ benzo(qhi)perylene ' N.D-—————————————C————————————————————————————————————————TI——K———————— I nnr. \———————rl .._.____ M n2,4-dinitrophenol • N.D- (80B) fluorene—-——-————r ——•—————[—————————————-r"—•——-=——"™—~~—~——— / f\ * r\ \ ' L. _ _ — _ ± U.4.6-dinitro-2-methylphenol N.D. (81B) phenanthrenepentachlorophenol"'"1' N'.D. (82BJ dibenzo(a.h)anthracene

- -————=————————" ' """——————"————————————~"——————=":——^~"~——™"— / f\ -%r» \ j TIfl" » / 1 O O .*4 \ ••Mfvtstna(65A.phenol""" *"""""*" N.D. (83B) indeno(1.2,3-cd)pyrene______•s——*——K——————————————————————-———— /».~v——————:———' N7D\O4P /______JJ_Y_l_CJMt_________________________________________________

(61B) iTNitrosodimethylamine N-p"BASE/NEUTRAL COMPOUNDS MG/KG VOLATILES

EPA f EPA *(IB) acenaphthene__________N.D. (2V) acrolein

benzidine N.D.1,2,4-trichlorobenzene N.D.hexachlorobenzene N.D.

] h e x a c h l o r o e t h a n e N . D .l8Bl——bis(2-chloroethyl)ether N.D.20B) 2-chloronaphthalene tLW. _______________25B)l,Z-dich1orobenzene N.D. ~ (13V) 1.1-dichloroethane"

(37B 1,2-diphenylhydrazine N.D^ (29V) 1,1-dichloroethene•39B) fluoranthene TT—— (30V) trans-1.2-dlcMor5ethene40B) 4-chlorophenyl phenyl ether N.D. (32V) 1.2-dichloropropane_——'——————*——^—p——*—^———— —— 7T3V1 fran^-1.3-dichloropropene

uZB /____n~ 11 i u i w jmj i pi ici ijr i m" * i' - ____ n . \ • — • / ' • *••*• • — _~ • • ~-•--———————————•———63B) N-nitrosodipropylamine giMQAno f(50V) dichlorodifluoromethaneV O D y M I I I U I l / O w U l p l W \*J I m" I '"-___________pttf JiJt. f~f-f-t { I *f f _ _ ~ . . . ,.,-.-— — ————i -————

F^l——bis(2-ethv1hexy1 )phtha1ate N:D.UUU^ I (51V) chlorodibromomethaneJ—————,————i——. i .' .——i . i V ^ —————————— '' ' _ '———— JOgW\————j..^.___UT-s-,«^+hor>QI )——benzyl butyl phthalate_____N.D. (85V) tetrachloroethene

..(70S) diethyl phtialate N.D. (88V) vinvl chloride71B) dimethyl phthalate ____ N.D.(72B) benzo(a)anthracene___________N

, ..1,3-dichlorobenzene N.D. (14V) l.l.Z-tricnioroeihane. —————— NJJ-tDD } J. j J—U I OH I Ul UUCIIiCIIC _____________U.K._____ > - • • /______•••»-'— '• ------————^—————————————————————————

"27B)——1,4-dichlorobenzene 39 (15V) l,1.2.2-tetrachloroethane————g_JL£/ D 1_____x^t-un.niL/1 UL/cri^-ciie____________vJJ_____ ) ' ~ '____. ' ' T — ————————————————————iT, .-.28B) 3,3'-dich1orobenzidine N.D. U6V) chlorethane——.—=^——————aik±.ÔD; J,o -u i on i ur uucii^-iuiiic__________11. L>. \ *~- / ""• "• - -••-••-—.—.——-—-—————————35B1——2,4-dinltrotoluene N.D. il9V) 2-chlnroethvlvinyl etner—————g_JL\ u jP /__t-1 "-* \-i 111 > ui u uu t ucnc ______n • L/ • . r.,... \ __— —— "————— w r^(36B) 2,6-dlnitrotoluene N.D. (23V) chloroform —:——————————C^^

tUD /_____t-QH I Ul UÎICIIJ I HCIIJf I Ullî_____n . u .

.416) 4-bromophenvl phen.vl ether N.D. .___________ , ., 0(42B) bis(2-ch1oroisopropyl)ether N.D. cis-1.3-dichloroPropene—————^(43B) bis(2-chloroethoxy)methane N.D. (38V) ethvl benzene—— _______————H-tt-(52B)——hexachlorobutadiene N.D. (44V) methylene chloride___________^.\L-

hexachlorocyclopentadiene N.D. (45V) chloromethane __——————[L.JLin^/\mv<»ii«^/i vjy»jw • \f p \-*t w ui %j > -h. i»>. n«i^« ^ - ».._ — - - - — —.—_—_—-———-—-——————— - - _

isophorone N.D. (46V) bromomethane ———————————aJi±.———C—•——-—————————————————•————————r:—r————— i till \————i—— _^-_.._ M llnaphthalene___________N'.D. (47V) bromoform —————^^nitrobenzene—————————— V.D. (48V) bromodi chloromethane__________N_îi i 1.1 uuciiêiie ______________ - "»___ v __' i_____"' ""|WM • -•• • ~ ———-—————————————: ^.N-nitrosodi phenyl amine ' n (49V) fluorotrichloromethane——————LO

T^SBl——di-n-butyl phthalate 38 (86V) toluene ————————————(69B) di-n-octyl phthalate N.D. (8™) trlchloroethene—.————————J-^L

CLIENT: ROY F. WESTON, INC.______ DATE OF ANALYSIS: January 16. 1984T011684-05________

ANALYSIS NO.: H545 STA #3. CHART NO.:CRN-2

PESTICIDES MG/KG PESTICIDES MG/KGEPA # EPA I(89P)(90PJ(91P)


103P) 0 -BHC_________________N n104P) ff -BHC _____M n105P) Y - BHC_________________N n

(92P) 4.4'-DDT_________________16 (106P) PCB-1242 M n(93P) 4.4'-DDE N.D. (107P) PCB-1254 "Fn!94P95PT96P97P98P

4,4'-DDD_______________N.D. (108P) PCB-1221-endosulfan _________N.D. (109P) PCB-1232 _____wn-endosulfan .._______N.D. (HOP) PCB-1248 ____________N.n.

endosulfan sulfate ________ N.D. (lllP) PCB-1260 _________ _endrin N.D. (112P) PCB-1016

99P) endrin aldehyde N.D. (I13P) toxaphene100P heptachlor_____________N.D.

tLJL

heptachlorepoxide________N.D. DIOXINS(102P) c* -BHC N.D. (129B) 2.3.7,8-TCDD (Screen Only^ **

NOTES AND COMMENTS:

ATILE ORGANICS: N.D. = <.lmg/kgBASE NEUTRALS: N.D. = <5 mg/kgACID EXTRACTABLES: N.D. = <5mg/kgPESTICIDES/PCB's: N.D. = <5mg/kg

*NOT TESTED FOR THIS COMPOUND**SCREENED ONLY/NOT PRESENT

100-032Thomas F. Cullen, Jr.Laboratory Director/Organics Division


H545,WESTON,20UL/25I1L.D.I ,E=2206,P/T IJSB1 10059. Ig3TCl 2CLC,011884,1820,SE39 724 SCflNS ( 724 SCflNS, 17.12 MINS)

MflSS RflNGE: 44.0, 375.2 TOTflL flBUND= 275748.

10 11 12 13 14 15 16 17 18 19MINS

flVERflGED SPECTRUM * BflSE PK/flBUNB: 57.1/ 32000. + 149 -147 -145

100-1

•

88-.

60-•

40-

20-

R - , , , . . , ,

49

50

14.457 95

62

<k

*TRICHLOROETHENE I30

"• X

60 70 80 90 100 110 120 130 . _

HS45,WESTON,20UL/2SML.D.I ,E=2200,P/T OUR] 10059, J33$LCLC,011884,1820,SE30 ' ' 724 SCflNS C 724 SCflNS, 17.12 MINS)>x 110 MflSS RflNGE: 44.0, 375.2 TOTflL flBUND= 275748.

f v, .--s- f *-S,

3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19MINS

flVERflGED SPECTRUM * BflSE PK/flBUND: 101 .0/ 32000. + 38 -40

109-1.

80-•

60-

40-

20-

0-

4

1

6

5

' ' ' 1 ' ' ' ' 1 '

50

1C

8

• 1 1*1 i | >< i i | • i < i | i • • * [ i . . i | . . . . | . . • • | . . . I |

60 70 80 90 10<

11

3

*TRICHLOROFLUOROMETHflh

l« 100033

110 120 130

-27.3

E

«

IHS45, WESTON,20UL/25ML.D.I ,E=2200.P/T MaSI 10059|CLC, 011884,1820,SE30

6420

3 4 5 6 7 8 9 10 11 12 13 14 15 16 17. -18 19

1 TRICHLOROFLUOROMETHflNE

2 TRICHLOROETHENE

*B 100031.

H0545,UESTON+I .S. (2 + 4) ,E-1800 1131120081 , Ed 105CLC,011684,1800,SE54 . 2814 SCflNS ( 653 SCflNS, 12.52 MINS)

RflNGE: ftl.0, 446.4 TllTflL flBUND^ 2854783.

I I I I I I I I I I I I I4 5 6 7 8 9 10 11 12 13 14 15

MINS

flVERflGED SPECTRUM * BflSE PK/flBUND: 145.9/ 32000. + 366 -363

100 -|.

80-•

60-•

40-

20-

0-

4

7

5

" MMt ' ( ' 1

60

5

IE

9

|!0

1

n

I I J ,t ' i100

1*

1

121

1 1 1120 140

It.

1 ,4-DICHLORQBENZENE

,

160 180 200 220

15.9

ev*>

H0545,WESTON+I .S. (2 + 4) ,E=1800 1138128081 , IBSCLC,611684,1806, SE54 2814 SCflNS (1025 SCflNS, 20.03 MINS)px 1.0 #. I MflSS RflNGE: 41.0, 446.4 TOTflL flBUND= 2854783,

•V'Vv'vW V-WVAJ V.A"•Vyy,

I I I I I I I I I I I I I I I I I I i I I31 32 33 34 35 36 37 38 39 40 41 42 43 44 45 46 47 48 49

MINS

*1605 RET. TIME: 32.85 TOT flBUND= 3074. BflSE PK/fiBUND : 149.0/ 722.

10050-

0-J

100-

50-

1-23.5DI-n-BUTYL PHTHflLflTE 149

43 5S 69 83 95 HI 12S 137.11 .

1790J-- ——— , ———

180

.1 . l . l l l .. ..I.I.. ....I.I.. . ,1 . I.I.. . . ......... ,. . ,,,n, ,,...

163i.. ... .

60 80 100 120 140 160

189 200207 219 227 237 252 "" 10003,. ... ( . .. . . . .1

-23.5

200 220 240 260 280

H0545,UESTON+I .S. (2 + 4) ,E-1800 00328081 , |§_I_]l05CLC,011684,1800,SE54 2814 SCflNS (2814 SCflNS, 54.38 MINS)

10.0 I MflSS RflNGE: 41.0, 446.4 TOTflL flBUND= 2854783.

f~i I I I I I I I I I I I I I I I I I I I I I I I I I4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52 54

MINS

*1641 RET. TIME: 33.55 TOT flBUND= 2162. BflSE PK/fiBUND : 57.2/ 158,

100-143 57 ?_

83 S? * , <50- HI i'I

Q 1 II 1 1 |lll 1 1 I l l l 1 III 1 ll 1 | ll| l l l | 1 1 ll

•S 135 I49 I65 *179nil HI hi hi 1 n 1 Mill i I 1 i Hi

100 60 80 100 120 140 160 186

*4,4'-DDT COELLITING WITH SN50. UNKNOWN

195 203 211 23S 307n 1 1 1 ll 1 1 1 1 1

200 220 240 260i * i • i • i

280 . 300

-7.31

•7.31

i

CLIENT: ROY F. WESTON. INC._____ DATE OF ANALYSIS: January 16. 1984T011684-07 & 08

ANALYSIS NO.: H547 STA. #5. CHART NO.: FRN-10056

(57A)T58A

(42B

52B53B54B55B

62B

CRN-2


EPA I EPA *21A) 2,4.6-trichlorophenol______N.D.22A) p-chloro-m-cresol N.D.24A) 2-chlorophenol ~_______N.D.

73B) benzofi74B) benzo(l75B) benzo(k

pyrenefluoranthenefluoranthene ~N7b.

31A) 2.4-dichlorophenol________N.D. (76B) chrysene N.D.34A) 2,4-dimethylphenol N.D. (77B) acenaphthylene

2-nitrophenol N.D. (78B) anthracene __________ NJL~4-nitrophenol___________N.D. (79B) benzo(qhi )perylene „ NJ3.

2.4-dinitrophenol '_____tl.D. (BOB) fluorene_______________NJIL.60AJ 4.6-dinitro-2-methylphenol N.D. (81B) phenanthrene N.D.64A) p e n t a c h l o r o p h e n o l N . D . (82B) dibenzo(a,h)anthracene N.EK_- - . i————'—-.————r——————«•——•————————————————————-———— / _ __ t————:——:———T~i—-—~— i \ _...____ Si n

> ~ " ' '______f**~" "v».i • w, W|-.i^mi_____________________.. . _ . v^^^ ,______.__..____,..,_.._ _________________

(65A) phenol N.D. (83B) indeno(l,2.3-cd)pyrene TT'6T( 8 4 B ) p v r e n e N T O .

(FR) benzidine N.D. T3V) acrylonitrile1 }_ 1.2,4-trichlorobenzene N.D. (4V) benzene(9B) hexachlorobenzene________N.D. (6V) carbon tetrachloride(12B) hexachloroethane N.D. (7V) chlorobenzene

43B. .__________M________..._. ^_^_______________.hexachlorobutadiene_______N.D. (44V) methylene chloridehexachlorocyclopintadiene N.D. (45V) chloromethaneisophorone ________N.D. (46V) bromomethane

N-mtrosodiphenyl amine_____N.D. (49V) fluorotrichloromethane

(61B) N-NitrosodiinethylamineBASE/NEUTRAL COMPOUNDS MG/KG VOLATILES -'7

EPA i EPA I(IB) acenaphthene _____217 (2V) acrolein_______________!LJL

(18B) b1s(2-chloroethyl)ether N.D. (10V) 1.2-dichloroethane ________N_D__(20B) 2-chloronaphthalene N.D. (11V) 1,1,1-trichloroethane .....JLJL-(25B) 1,2-dichlorobenzene N.D. (13V) 1,1-dichloroethane N.D.(26B 1,3-dichlorobenzene N.D. U4V) 1.1,2-trichloroethane N.D.27B 1,4-dichlorobenzene N.D. (15V) 1,1,2,2-tetrachloroethane N.D.(28B 3,3'-dich1orobenzidine N.D. (16V) chlorethane N.D."T35T 2,4-dinitrotoluene________N n (19V) 2-chloroethvlvinyl ether N.D.(36B' 2,6-dini.trotoluene________N n (23V) chloroform N.D.(37B) 1.2-diphenylhydrazine N n (29V) 1.1-dichloroethene N.D.(39B) fluoranthene N n. (30V) trans-1.2-dichloroethene N.D.(4QB) 4-chlorophenyl phenyl ether N^n. (32V) 1,2-dichloropropane N.D...(41B) 4- bromophenyl phenyl ether N^D. (33V) trans-1.3-dichloropropene N.,D._

bis(2-chloroisopropyl)ether N.D. cis-l,3-dichloropropenebi s (2-chl oroethoxy )methane N.D. (38V) ethyl benzene ._______3J;iflO_

naphthalene_____________19.QQQ (47V) bromoform __^^________N..JXnitrobenzene N.D. (48V) bromodichloromethane ____6LJL

63B) N-nitrosodipropylamine N.D. ~ (5QV) dichlorodifluoromethanB tQQ[^^ bis(2-ethy1hexyl)phthalate N.D. (51V) chlorodibromomethane"" ' w^

benzyl butyl phthalate N.D. (85V) tetrachloroetheneai-n-butyl phthalate N . o T ( 8 6 V ) toluene

(69BJ di-n-octyl phthalate N.D. (87V) trichloroethene ______N,^(70B) diethyl phT^alate ________N.D. (88V) yinvl chloride NJL_(71B) dimethyl phthalate________N.D.(72B) benzo(a)anthracene

CLIENT: ROY F. WESTON. INC.________ DATE OF ANALYSIS: January 16. 1984T011684-07 & 08__________

ANALYSIS NO.: H547 STA. 15.________ CHART NO.: FRN-10056CRN-2

PESTICIDES MG/KG PESTICIDES MG/KGEPA t EPA f89P90P91P

aldrin____________________N.D. (103Pdieldrin__________ N.D.chlordane_________________N.D.

104P

(92P) 4,4'-DPT _____________N.D. (106P93P) 4,4'-DDE___ N.D. (107P

105P

94P) 4,4'-DDD ______________________N.D. (108P95P) <=< -endosulfan N.D. (109P96P) y3 -endosulfan N.D. ulOP97P98P99P

endosulfan sulfate N.D. (HIPendrin N.D. (112P)PCB-1016

-BHC N.D.-BHC___________________N.D.

pet-BHC N.D.1242 N.D.

PCB-1254 N.D.PCB-1221 N.D.PCB-1232 » N.D.PCB-1248 N.D.PCB-1260 N.D.

endrin aldehyde______________N.D. (113P) toxaphene ___________N.D.100P

(101P(102P

heptachl or______ ____N.D.heptachlor epoxide____________N.D. DIOXINS

"BHC————————————————^ (129B) 2.3.7,8-TCDD (Screen On1y),-n **

NOTES AND COMMENTS:

_ ,'ATILE ORGANICS: N.D. = <.lmg/kgBASE NEUTRALS: N.D. = <5mg/kgACID EXTRACTABLES: N.D. = <5mg/kgPESTICIDES/PCB's: N.D. = <5mg/kg


Thomas F. CuMen, Jr.Laboratory Director/Organics Division



January 20, 1984

CLIENT: Roy F. Western, Inc.5090 Central HighwayPennsauken, N.J.ATTN: Robert Keating

PROJECT: Analytical Laboratory Testing of saraples from:"Gettysburg Drum Site"

Project No. 1600

TESTREQUIRED: Volatile Organic Priority Pollutants, Acid Extractables

and Base Neutral Extractable Priority Pollutants alsoR.C.R.A. analysis.

METHOD OFANALYSIS: U.S.E.P.A. "Test Methods for Evaluating Solid

Waste-Physical and Chemical Methods".SW 846-July 1982-2nd Edition

DATE OFSAMPLING: January 12, 1984

DATERECEIVED': January 13, 1984

SAMPLESCOLLECTED BY: Clients' Representatives (Robert Keating & Kenneth McGill)

ANALYSISPERIOD: January 13, 1984 thru January 19, 1984

ANALYSIS NO: H543 thru H554 INVOICE NO. 3638/mp

00039

H547,WESTON,25ul/25ML.DI.,P/T,E=2200 lisTCI 10856.13311 2CLC,011784,2188,SE30____ _______ 859 SCflNS ( 859 SCflNS, 20.40 MINS)

2.0 i MflSS RflGE: 44.0, 375.3 TOTflL flBUND= 15379804.

I I I I I I I I3 4 5 6 7 8 10 11 12 13 14 15 16 17 18 19 20 21 22

MINS

* 251 RET. TIME: 8.05 TOT flBUND= 72638. BflSE PK/flBUND: 91.1/ 28650.

100-

88-

68-

40-

28-

8-

9

*TOLUENE

51 6S45 55 74 78

1

•v-

58 68 70 80 90

98I

II ' i • • i

39.4

H547,WESTON,25ul/25ML.BI.,P/T,E = 2200 igggl 16856.18371 2CLC,011784,2100,SE30____ _______ 859 SCflNS ( 859 SCflNS, 28.48 MINS)

/ MflSS RflKJGE: 44.0, 375.3 TOTflL flBUND= 15379884..0

A. 110 M 12 13 14 15 16 17 18 19 20 21 223 4-5 6 7 8

MINS

* 333 RET. TIME: 10.00 TOT flBUND= 39074. BflSE PK/RBUND: 91.1-" 16295.

100-1.

80-•

60-

40-•

20-

0-

91

51

i "1

65 77

1. .ll . Ill

•41 .7

*ETHYL BENZENE

106

1 .,.,60 , 80 100

ftfUOOQ**1 3120 140 160 180

H0547,UESTON, + I .S. (2 .0+4 .0) 0 ,E=1S80 D32I 28882 , pKnliaSCLC,011684,1900,SES4 * SCflNS, 19.72 MINS)^fl .$.0 fl n Mflss RrtNtjig RU^l, 4R4.5 TOTRL flBUND- 17907424.

9 10 11 12 13 14 15 16 17 18 19 20 21MINS

* 694 RET. TIME: 15.53 TOT flBUNB= 94455. BflSE PK/flBUNB: 128.1/ 44780.

100-

56-

0-100-1

50-

0-

i;

45 57 75 87 102...,....,....,,..,....,....,...., ....,....,....,....,....,.,.,....,....,....,... ,,l

60 80 188 120

260 280 300 320 3

NflPHTHflLENE

V

148 162i .., ........

148 168 188 288 228 248

446 -,

40 360 380 400 420 440

•47.4

•47.4

»

_

H8547 ,UESTON,+I .S. (2.0+4.8)0 ,E=1880 iaiaii 28882 . muSK* 18CLC,6116S4,1900,SE54 2988 SCflNS (1010 SCflNS, 19.72 MINS)

M fifeS gflH£S ' \l .5 TOTflL RBUND= 17907424,,

7 8 9 10 11 12 13 14 15 16 17 18 19 20 21MINS

* 938 RET. TIME: 20.15 TOT flBUND= 4107. BflSE PK/flBUND: 154.1' 628.

100-

•

80-

60-

40-

20-

0-

43

I

15.31

flCENflPHTHENE

57 71

.1 H.i.ll~— i —— r — ' — i,. il h i i

87

li l l l . . 1,,60 80

101 119 12S 140'1,1' 1 nl|lli 1 —— | -1 i < i | • | i i l » , i Hi -1 < i •• ll

54

Ift 1000 |,i III1

100 120 140 160 j

CLIENT: ROY F. WESTON. INC._____ DATE OF ANALYSIS: January 16. 1984T011684-09_________

ANALYSIS NO.: H548 STA. #6._____ CHART NO.: FRN-10064CRN-2


EPA f EPA f(21A)tfgt

21A) 2.4.6-trlchlorophenol^\ ^\ * \ •»' ' * '*_ i." 11 ii i22A) p-chloro-m-creso! JLJLJUL

73B) benzo a)pyrene N.D.

75B74B) benzo

76B

b)f1uoranthene__________N.p.benzo TTfluoranthene N.D.chrysene________________N.D.acenaphthylene____________N.D.

(24A) 2-chlorophenol N.D(31A) 2.4-dlchlorophenol —N!D(34A; 2,4-dlmethylphenol N.D". .... _..__.,.^___________„_57A 2-mtrophenol________* N.D. (78B) anthracene N.DT58A) 4-nitrophenol____^______N.D. (79B) benzo(qhi)pery1ene * N.D.

(59A) 2,4-dinltrophenol ______N.D. (80B) fluorene______________N.D.(60A) 4,6-din1tro-2-methylpheno1 N.D. (81B' phenanthrene____________N.D.J64A) pentachlorophenol________N.D. WB^ dibenzo(a,h)anthracene N.D.(65A) phenol______________N.D. (83B) indeno(l>2,3-cd)pyrene TOT

(84B) pyrene N."DT(61B) N-Nltrosodimethylamlne_____N.D.

BASE/NEUTRAL COMPOUNDS VOLATILES :__ MG/KGEPA I EPA , ^

acenaphthene ___________ N.D. (2V) acrolein _______________ N n)enzidine N^ (3V) acrylonitrile .

» 4-tr-ichiorobenzene N.D. (4Vj benzene N.D.(96) hexachlorobenzene N.D. ~ (6V) carbon tetrachloride N!D!'

nexachloroethane N.D. ~ (7V) chlorobenzene N.D.~ '

..QTSU-ch1orpethyl)ether N.D. ~ (10V) 1,2-dichloroethane

2 2-chloronaphthalene N.D. (liyj 1,1 ,1-trlchloroethane 240025B) 1,2-dichlorobenzene _______ N.D. (13V) 1.1-dichloroethane26B 1.3-dichlorobenzene _______ N.D. U4V) 1,1,2-trichloroethane27B 1,4-dichlorobenzene ______ N.D. (15V) 1.1.2.2-tetrachloroethane/ DO D o oT _i • _ i ——— T ———— ; — r^ ——— """ •• ————— n~'?r — — — . • ,. . . ———— 2 — 2. M, .-,.,, ,, — ., ,,.— — - —————————— - ——(28B) 3.3'-d1ch1orobenz1dine N.D. "[757] chlorethane

(40B) 4-chloro

N.D-35B| 2,4-dlnitrotoluene_______N.D. (19V) 2-chloroethylvinyT ether____N.D.36B 2,6-dinUrotoluene________N.D. (g3Vj chloroform N.D.37B 1.2-diphenylhydrazlne_____N.D. (29V) 1,1-dichloroethene w39B fluoranthene____________N.D. TW) trans-1.2-dich1oroethene "07

jhenyl phenyl ether N.D. (32VJ 1,2-dichloropropane N.D.•j-————a i. ——._____ __ -'•*"•%/ .. ~ . y • • A. _ _/___ * ' c. u i w 11 i v/ i VK__»__y pv ' '^-______ __ 11 • L/ •(41B) 4-bromopienyl phenyl ether N.D. (33V) trans-l,3-dich1oropropene N.D.'(42B) b1s(2-ch1oro1sopropy1)ether N.D. cis-l,3-dich1oropropene_____N.D.43B) b1s(2-ch1oroethoxy)rnethane N.D. (38V) ethyl benzene 220052B) hexachlorobutadlene N.D. (44V) methylene chloride N.D.j3B hexachlorocyclopentadlene N.D! (45V) chloromethane N.B!54B1 iso55B, naphthalene____________3n,nnn (47V) bromoform

Phorone_____________N.D. (46V) bromomethane N.D.

nitrobenzene___________N.D. (48V) bromodi chloromethane N.D.N-mtrosodiphenylamine_____N.D. T5W1 fluorotrlchloromethane N.D.N-nitrosodi propylamine,,, t jQ^ TWJ dichlorodlfluoromethane N.D.bisU-ethyihexyljphthaHflei Uf».g?FZ (51V. chlorodibromomethane ______.....benzyl butyl phthalate N.D. (85V) tetrachloroethene N.D.ai-n-buty] phthalate N.D. (86V) toluene 7andi-n-octyT?htha1ate N.D. TS7V") trichloroethene N.D.

(/OB) diethyl pfrtha late ______N.D. (88VJ ylnvl chloride N.PT(71BJ dimethyrphthalate ______N.D.(7Z&} benzo(a)anthracene OT

CLIENT: ROY F. WESTON. INC.______ DATE OF ANALYSIS: January 16. 1984T011684-Q9______

ANALYSIS NO.: H548 STA #6.______ CHART NO.: FRN-10064CRN-2

PESTICIDES MG/KG PESTICIDES MG/KGEPA f EPA f(89P]90P91P

aldrin_________________N.D.dieldrin___ ____N.P.chlordane N.D.

103P104P105P

92P) 4,4'-DDT __________N.D. (106P

-BHC N.D.- B H C N L-BHC N.D.

1-1242 N.D.93P) 4.4'-DDE N.D. (107P) PCB-1254 lO).94P95P96P97P98P

4,4'-DDD _______N.D. (108P) PCB-1221________________N.D.-endosulfan N.D. (109P) PCB-1232 „ N.D.-endosulfan .________N.D. (HOP) PCB-1248_______________N.D.

endosulfan sulfate_________N.D. (HIP) PCB-1260_______________N.D.

(99P)endrin_______ ________N.D. (112P) PCB-1016 ___________NJ).endrin aldehyde___________N.D. (113P) toxaphene______________N.D.

100P) heptachlor______________N.D.101P(102P ]

heptachlor epoxide __ N.D. DIOXINS"BHC ——————————————— ^ (129B) 2,3,7 ,8-TCDD (Screen On1y)r7

NOTES AND COMMENTS:

VOLATILE ORGANICS: N.D.=<.img/kgBASE NEUTRALS: N.D.=<5mg/kgACID EXTRACTABLES: N.D.=<5mg/kgPESTICIDES/PCB's: N.D.=<5mg/kg


~~\0 rvCiCA3 \ jSjL*—— . .

Thomas F. Cullen, Jr. \Laboratory Director/Organics Division


**

H548,WESTON,2.0UL+20UL.I .S. ,E=2200,P/T,25ML.D.I . 13311 10B64. EHil 2CLC,011884,2130,SE30 1173 SCflNS (1173 SCflNS, 27.87 MINS)r*x 2.0JI "I J/II jfliS iftffldET JUJ4J4.0, 430.1 TOTflL flBUND= 12687248.

3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29MINS


100-

80-

68-

40-•

20-t

0-

49

jj•1 ' • • • i —— L —— • —— i —— . —— i —— . —— i —— i —

*1 ,1-DICHLOROETHENE

96

170 76

. . . . ..I.i.103 151

- T'

-34.7

60 80 100 120 140

HS48,WESTON,2.0UL+20UL.I.S.,E=2200,P/T,25ML.D.I. H3JI 18064 , B3H 2CLC,©11884,2138,SE30 __ 1173 SCflNS (1173 SCflNS, 27.87 MINS)r»x 2.0* I /——111 J/ll IfltS jftfl.l.dEn|1U4J4.e, 438.1 TOTflL flBUND= 12687248.

34 5 67 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29MINS

flVERflGED SPECTRUM * BflSE PK/flBUND: 63. 1/ 32000. + 67 -44

108-1.

80-

68-

40-

20-

63

47

L0-- i • i

•32.6

*1 ,1-DICHLOROETHflNE

96

83

, ... 1.60 80

ft' t I f tfa f\ i. ft iii 300',l.i

ik

100 120 140 160 180

H548,UIESTON,2.0UL+28UL.I .S. ,E = 2200 ,P/T ,25ML .D . I . 13311 10064. BUBl 2CLC,011884,2130,SE38 . 1173 SCflNS (1173 SCflNS, 27.87 MINS)j»x 2.0* in i/lj ffltS jferfldET)|AJ4|4.0, 430.1 TOTflL flBUND^ 12687248.

3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 28 21 22 23 24 25 26 27 28 29MINS

* 110 RET. TIME: 4.73 TOT flBUND= 41697. BflSE PK/flBUND : 97. 1/ 12497.

10080-

•60-

48-

28-

61

47. 1.,.. .....0-- —— i — • — r

68

30.097

78 82

*1 ,1 ,1-TRICHLQROETHfiNE

*

117

.1 II,88 180 120 140 160 180

H548 ,WESTON ,2 .8UL + 20UL . I .S . ,E=2200 ,P/T ,25ML .D . I . USil 10064 , ___CLC,811884,2138,SE30 ___' 1173 SCflNS (1173 SCflNS, 27.87 MINS)

tl4.8, 438.1 TOTflL flBUND= 12687248 .

i—r - i—\—r1>T*^r*""i i i i i i i i i i '\~~r~i—\—\—\—r~i——i—i—i3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29MINS

* 222 RET. TIME! 7.38 TOT flBUND= 67335. BflSE PK/flBUND: 91.1/" 27257.

100-.

80-•

60-

40-

20-.

0-

91

51 6577

Ii III i l l i . i 1' 1 ' 1 1 ' 1 ' f

1

*TOLUENE

ftSIOOOfcS107

1 1 1 1 1 . 1 . 1 . 1 . 1 . 1 i 1 t 1 . 1 t

40.55

J1

60 80 100 120 140 160 180

H548,WESTON,2.0UL+20UL.I.S.,E = 2200,P/T,25ML.D.I. 13311 10064.13311 2CLC,011884,2130,SE30 ____ il?3 SCflNS (1173 SCflNS, 27.87 MINS)

" IJ4.0, 430.1 TOTflL flBUND= 12687248.

I——I——I——I——I——I——Ii i i i i i i i i i i i i i i i i i i i i i i i iS 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29

* 332 RET. TIME: 9.98 TOT flBUND= 63098. BflSE PK/flBUND: 91.I/ 26964.

100-

88-

68-

48-

20-.

8-

91!

51 ,,_.65 77

l..,. ,.,!.1 1

68........ I I . . . . . . .

•42.7

*ETHVLBENZENE«r

106

1. .......1 ' 1 ' 1 ' 1

80 100

126 .,,i — •

t ' 1 ' 1 ' 1 * 1 ' 1 * 1 ' 1 ' 1 '

128 140 160 180

H548,U)ESTON+I .S. , (2 + 4) ,E=1S00 13311 20083 . EailiQSCLC,011684,2000,SE54 _ _3015 SCfl_NS__ *_ _ 16.00 MINS)

flL flBUND= 27810108.

10 11 12 13 14 15 16 17MINS

* 599 RET. TIME: 13.77 TOT flBUND= 87796. BflSE PK/fiBUND: 128.I/ 44540.

100-

88-

60-

48-

28-

0-

i;

NRPHTHflLENE

51 63 75 S7 10£ H9 ,...j ii.. r ..n .. ... i|.i. .f . .. ... il.. ..... ...... II

;3

»

, 13& 146 162L ....!.. .

60 88 180 . 120 140 160

50.7

fti 10001*7

CLIENT: pnv T?. WESTQN. INC.______ DATE OF ANALYSIS: 1/18/84

ANALYSIS NO.: H549(STA.//8)______ CHART NO.:

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDSEPA f MG/KG EpA MG/KG

!22A2'4,6-trichlorophenol____N.D.p-chloro-m-creso-chlorphenol

73B) benzol

75B74B)benzo

_ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ _ « .______ «31A) 2.4-dichlorophenol N.D. T76B** A > " 3; :——~———~——-- -————~———"——-———————— - ~ ————(34A)2,4-dimethylphenol N!D! (77B

/ n J i \ 5 ? " •""•"" r — ™ " """"(57AJ 2-nitrophenoj"" N!D. (78B

benzo

a)pyrene ________N.D.b)fluoranthenek)fluoranthene

chryseneacenaphthylene__________N.D.anthracene ".____________N.D.y i————— -• -.-••-••- •________________a. LI ._____ V'<->"/ 0111,111 aucnc

(58A 4-nitrophenol____________N.D. (79B) benzo(ghi)perylenef'f-dinitrophenol •'_____N.D. (80B) fluorene

60A) 4.6-dinitro-2-methylphenol N.'D. (81BJ plienanthrene N!!64A) pentachlorophenol_______N.D. (82B) dibenzo(a.h)anthracene "OT

facenaphthene ______________ N.D. (2V) acrolein _

(3V)4j

N-D' (3V) acrylonitrile

4-chloro

-c

p" N.D. T33VJ trans-1.3-dichloropropene1 — -•• -• .

sopropyl)ether N.D. ________ cis-l,3-dichloropropene

53B54B55B56B62B

hexachlorocyclopentadiene N.D. (45VJ chforomethane'nap

bromodichloromethane-R-—^——^iphenylamine N.D. (49VJ fluorotrichloromethane"N-mtrosoaipropyiamlne N.p. ~ _ _ JW}——dichlorodifluoromethanebisu-ethylhexyuphthalate H J D J J P OlS chlo'rodibromomethane'

n

i(71B) dimethyl phthalate NToT5_._Nipi. _ ARIOOO^S

N.D.

(65AJ phenol N.D. (83B) indenoU^.S-cdlpyreni" N.D.(84B) pvrene N.D.(61B.) N-Nitrosodimethylamine ____ N.D.

BASE/NEUTRAL COMPOUNDS VOLATILESHG/KG

.. .l,z.4-trlch]orobenzene N.D. 4yj benzene N.D.hexach orobenzene N.D. (6V j carbon tetrachloride N.p.hexachioroethane NtDt ~ (7V) chlorobenzene _________ N.D.

» PTSu-chloroethyl. ether N.D. (10V) 1.2-dichloroethane N.D!ll —— f-cn'o^onaphthalene N;D; (HV) 1,1,1-trichloroethane N!D!I —— l»2-dichlorobenzene ______ N.D. (13V) 1.1-dichloroethane N.D."—— 1'3-dichlorobenzene ______ N.D. U4V) 1,1,2-trichloroethane N^T—— i'^QTchlorobenzerie ______ N.D. (15V) 1.1.2,2-tetrachloroethane NJ37—— 3»3 -dichlorobenzidine N.D. (16V. chlorethane N.D.

^ —— 2.4-dimtrotoluene _______ N.D. (19V) 2-chloroethylvinyl ether N^736B( 2>6-dinitroto1uene _______ N.D. (23V) chloroform N.D.

—— l»2-diphenylhydraz1ne _____ N.D. (29V) 1,1-dichloroethene N^7fluoranthene _ _________ N.D. (30V) trans-l,2-dichloroethene

phenyl phenyl ether N.D. (32V) 1.2-dichloropropane M n'

?1SU:Ch10roeth?xy)rne^hane N.'D! (38V) ethylbenzenenexachjorobutadlene_______N.D. (44V) methylene chloride N.D.

N.D.isophprpne____________N.D. (46V) bromomethane___________N.D.

N.D. (47V) bromoform N.D.

tra]ate N'D' T8§\n tetrachloroethene(86V) toluene N.p7

phthalate N.D. (87VJ trichloroethene N.D.(88V) vinyl chloride N."D

CLIENT: ROY F. WESTON, INC. ____ DATE OF ANALYSIS: 1/18/84

ANALYSIS NO.: H549(STA.#8)__________ CHART NO.: TO 11784-0

PESTICIDES PESTICIDESMG/KG __. MG/KG

EPA i EPA *(89P90P91P

aldrin___________ N.D.dieldrin_______________N.D.chlordane___________N.D.

103P104P105P

(92P) 4.4'-DPT_____________N.D. (106P

0 -BHC_____________N.D.-BHC______________N.D.

PCTP-BHC N.D.1242

(93P) 4.4'-DDE____________ N.D. (107P) PCB-1254N n

94P95P96P97P

4,4'-DDD N.D. (108P) PCB-1221 TV-endosulfan N.D._ (109P) PCB-1232_____________M n-endosulfan . N.D. 110P) PCS-1248_____________M.n

(98P)99P

endosulfan sulfate N.D _ 111P) PCB-1260______________M_D.endrin N.D. H2P) PCB-1016 M nendrin aldehyde ______N.D. U13P) toxaphene____________\r,n

100P101P

(102P

heptachlor__________N.D.heptachlor epoxide______N.D. DIOXINS

-BHC N.D.(129B) 2,3.7.8-TCDD (Screen Only)r-r**

NOTES AND COMMENTS:

* Compounds-NOT TESTED** Screened/NOT PRESENT

VOLATILE ORGANICS = N.D. = 0. ling/kg

BASE NEUTRALS = N.D. = ^5mg/kg

ACID EXTRACTABLES - N.D. - < 5mg/kg

PESTICIDES = N.D. = <5mg/kg

I8IOOOU9

Thomas F. Cullen, Jr.Laboratory Director/Organics Division


H549,UESTON,20UL/25ML.DI.,20UL.I.S.,E=2200 IgsTCl 10060.11311 2CLC,011884,1900,SE30 769 SCflNS ( 769 SCflNS, 18.13 MINS)x #.0 MflSS RflNGE: 44.0, 375.3 TOTflL flBUND

8 9 10 11 12 13 14 15 16 17 18 19 20

9552.

flVERflGEB SPECTRUM * BflSE PK/flBUNDs 58.2/ 32000. + 32 -28

100-

80-

60-

40-

20-

0-

4

J '

5

7

|50

3 *TRI

ie

60 70 88 • 90 186

>

Jl

3

LOROFLUOROMETHflNE

V

;','

110 120 130

40.5

H549,UESTON+IS(2 + 4)E-1800 O3J] 28888 , OQQ| 186TFC,1303,011784,SE-54 _____ 1988 SCflNS (1988 SCflNS, 57.38 MINS)^x 2fi

J3 .MINS

'.0

v_*1272

100-1

88-

60-•

40-

20-

0-

44

—/ J\-.L 19 12 1

I 'ijii i i"

5 18 2'l

MflSS RflNGE: 41.0, 282.8 TOTflL flBUND= 10091988.

N.B. mi <i ^\ f\V. __ ft > i. J ^ —— " ————— •"••' ——— ———— " ... ~, „ -_• ; A.i— F — 'r* i i i — i i i ~i — i — i —24 27 30 33 36 39 42 45 48 51 54 57

RET. TIME: 39.27 TOT RBUND= 822. BflSE PK/flBUND : 80. I/ 162.

£

69

55

ill II63

8

91

136

1 ' ' 1 * 1 ' 1 ' t ' 1 • ! * 1 * 1 ' 1

80 180 128 148 168

19.7

.

H551 ,UIESTON+IS(2 + 4)E=1888 HsKl 28689 . W»KK\TFC,1415,811784,SE-54 1988 SCflNS (1592 SCflNS, 47.48 MINS)

1.0 MflSS RflNGE: 41.8, 449.5 TOTflL flBUND= 16783242.

N . D .

l l I I I —— I ——— I —— l I I I I I I I I I I4 6 8 10 12 14 16 18 2@ 22 24 26 28 38 32 34 36 38 48 42 44 46 48

*1549 RET. TIME: 48.72 TOT flBUNB= 18856. BflSE PK/flBUND: 57.2/ 951.

100-1

58-

8-188-j

58-

4 5?*T

,1 ,

7

H-68

239 253.... .

1

t_^

O

ll88

267

248 268

^ q

j

r-8.76

7111

j 125 141 155 169 179 197 207 225ll .....Illll . ...1,1,1., . ... .,.,,!.. .... . ..,,.. ....,.,., ... ... ........ .,!.... .._,| 1 | I | 1 | 1 | 1 | 1 | 1 | 1 ) . | . ( . | • | • |

100 120 140 160 180 288 228

281

288

ftiUOOOS

•8.76

t—i — • — i — • — i — • — i — i — i — i — i — i — i — i — i — i — i — i — i — i — i — i — i — ' — r -^i388 328 340 360 380 480

CLIENT: ROY F. WESTON. INC._______ DATE OF ANALYSIS: January 19, 1984

ANALYSIS NO.: H55Q___________ CHART NO.: FRN 20098 CRN 107TO11784-04

4I§5(27B

(35B(36B

43B52B

54B55B

62B63B

ACID COMPOUNDS BASE/NEUTRAL COMPOUNDS

EPA * m EPA f mg/kg[21A) 2,4.6-trichlorophenol__________N.D.,22A) p-chloro-m-cresol———————j^^ 74B7«7nn——o—IT,———:——. -.-. ________------ A.-r^ benzo(b)fluoranthene N.D.415*4——2-chlorophenol__________N.D. t75Bl——benzo(k)fluoranthene—————N^T

73B benzo(a)pyrene

f ——T-——-TT—T"Ti " • —— -— ..— ._ ..__ *_***'___________•'yHt.W \t\/

2.4-dichlorophenol________N.D. ' 76B) chrysene2»4-chmethyl phenol________N.D. (77B) acenaphthylene2-mtrophenol____________N.D. (78B) anthracene

~4——4-nitrophenql___________N.D. (79B) benzo(ghi)perylenei aÂ——^4^."ltrQPhenol •_________N.D. (80B) fluorenejbOA) 4.6-dinitro-2-methylphenol N.D. (81B(64A) pentachlorophenol_________N.D. Usfe(65A) phenol N . D . J 8 3 B

phenanthrene___________N.D.dibenzo(a,h)anthracene N.D.indenod^^-cdjpyrene N.D.

184B) pvrene N.D.(61B) N-Nitrosodimethylamine N.D.

BASE/NEUTRAL COMPOUNDS VOLATILESEPA * "_

acenaphthene____________N.D. (2V) acrolein______________*_benzifline N 7 (3V) acrylonitrile *—„-,,. ._—-, ... - _—- _. _______. ______ ___.. ,____,-_ _i.. _ _/______u v i jr i wi i i

,4-tnchlorobenzene N.D. (4V) benzeTiF______________N.D.exachiorobenzene NTD7~ T T) carbon tetrachloride O:7 , O;.-T———r-———T-T——— . i ~___________"•-" v"» / laruun ueLrcicr

} JJ, ueX?C"'ur°etha"e.. . N-D' (7V) chlofoEiHzMe_________H.D.®? blsiz-cnioroethyi.ether N.D. (10V) 1.2-dichloroethane "O:J|?!P——g-cnioronaphthalene NjpT (11V) 1.1,1-trichloroethane N.D.

——l'2-cnchlorobenzene_________N.D. (13V) 1,1-dichloroethane O:=—— _ " '—.——————,——— .. __ ....-— . - - - . . . ._ .____— _-• '-.-.—— _\ / ^ 5 J. \4l\*IIIVÎ\^V-WII yt I I . ___

1,3-dTchlorobenzene_______N.D. U4V) 1,1.2-trichloroethane

-mtrosodi jropylaminebis.2-ethyl lexyl )phthalate'I A *\ •*»«! l«r.4r..T -_ L.j.L _ *fc"~ "jtr_"" ——'

N D

N.D.^—————Ji——— —.——- •' • ' n. —— — i .1 ——— _ _ • • ___ ——— - - - * — - / A_|A<|h. ^ I I S * I « P V « * ^ V » W I I ^ » » 1 ^ -...—.

1,4-dichlorobenzene________N.D. (15V) 1,1,2,2-tetrachloroethane N.D(- *){•)#•) —————i^— _ i ——-—- —i.i .,... _——„— . _ _ — _..- • .— ..._ - _> *_______~ 7 * j._~_7 T" ..... W' . * fc* w ' ' '...'*' ' T_>* ' ** ' ' *"_*____

^»B) J.3 -dichlorobenzidine_______N.D. TT6Y)chlorethane NTo2,4-dinitrotoluene________N.D. (19V) 2-chloroethylvinyl ether N.D2,6-dinitrotoluene________N.D. J73V1 chloroform NTD]

(37B) 1,2-di phenyl hydrazine______N.D. (29V) 1,1-dichloroethene N.D.||||J——fluoranthene____________N.D. (30V) trans-1.2-dichloroethene N.D.)40B)——4-chlorophenyl phenyl ether N.D. (32V) 1,2-dichloropropane N.D:il1?. ^-bromoahenyl phenyl ether N.D. (33V) trans-1.3-dichloropropene N.D.

/ Dis(2-CTloroisopropyl )ether N.D. _____cis-l,3-dichloropropene N.D.—j—-:—— - ——•• .—ii———— - n - r^/ ^ - _-: —__•_. . ______ ____ y i j~^ J. 5 y u i y 11 i w i vjj i y p^ 11\~_____ *•' • *^ •

Dis(2-chloroethoxy)methane N.D. (38V) ethylbenzene N.D.hexachlorobutadiene_______N.D. (44V) methylene chloride N.D.TT——~~—" — . - ,T - - — i— _ _-.. ----- \ -T-T w / ||| UIIJT i cnjg uii i yi i uc *T._. •'nexachlorocyclopentadiene N.DT" J7T57) chloromethane NTD~:jsojhorone________________N.D. (46V) bromomethane N.D:naphthalene ____________N-D- T?7V1 bromoform N.D.

56B1 nitrobenzene N.D. PSY) bromodichloromethane"____N.D.•5-=——————-T-——.—————————— ___________.- ,__.-m.,_______________________.________._ \ v ' / Ul V/IIIWU |VrlllV/IV/IIICVIIUtl^ LN..U,

N-mtrosodiphenylamine_____N.D. "RW1 fluorotrichloromethane N.D"50V) di chl orodi f 1 uoromethane___N.D.51V) chlorodi bromomethane N.D.T-——? ----v • -~"j • />-••-••»• •».»>.____ti. u.- - v vr «, >i j, i / in i urua t uruiiiuiue me

benzyrbutyl phthalate N.D. " (85V) tetrachloroethene ______N.D.n-butyl phthalate N.D. " "(WJ toluene —————————^-^

]*£?.l d1"n"°5ty1. ?ntnaTate N.D. T5771 trichloroethene N!D.1 -If.*. \————————1-.————.———.——y,—— r___ - — - -_________________-• -— - \~" " / 1,1 IÎIIUI V>^^1IV.1I<-__________________________" -~ •

nu 31et?,l.ph!hglfte lr57 (88V) vinyl chloride N.D:(7IB) dimethyl phthalate N.D. ——————— ——————————————————(72B) Denzo(a)anthracene

CLIENT: ROY F. WESTON, INC.________ DATE OF ANALYSIS: January 19, 1984

ANALYSIS NO.: H55° CHART NO.: SE-2-011984-166

PESTICIDES PESTICIDESEPA f mg/kg EPA * mg/kg(89P) aldrin________;______N.D.(90P) dieldrin ________N.D.(91P) chlordane________N.D.

103P104P105P

92P) 4,4'-DDT _____________N.D. (1Q6P93P) 4.4'-DDE _____________N.D. (1Q7P(94P) 4.4'-DDD __________N.D. (1Q8P

-BHC N.D.- B H C N . D .-BHC N.D.

S-1242 N.D.PCB-1254 N.D.PCB-1221 N.D.

(95P) c< -endosulfan__________N.D. (109P) PCB-1232__________ N.D.96P97P

/$ -endosulfan _______N.D. (110Pendosulfan sulfate N.D. (11IP

98P) endrin________________N.D. (112P

PCB-1248 N.D.PCB-1260 N.D.PCB-1016 __N.D.

99P) endrin aldehyde__________N.D. (113P) toxaphene ___________N__D___(lOOP) heptachlor ________N.D.101P) heptachlor epoxide_______N.D. DIOXINS(102P) <* -BHC _ _ _ _ _ _ _ _______ NToT (129B) 2.3.7.8-TCDD (Screen Only)-" **

NOTES AND COMMENTS:

VOLATILE ORGANICS N.D. = <.l mg/kg

BASE NEUTRALS N.D. - <5 mg/kg

ACID EXTRACTABLES N.D., - <5 mg/kg

PESTICIDESTPCB's N.D. - <5 mg/kg

* NOT TESTED FOR THIS COMPOUND** SCREENED ONLY-NOT PRESENT

s\———Thomas F. Cullen, Jr.Laboratory Director/Organics Division


H0550,UESTON+IS(4 + 4)E-1800 11311 20098 , 113!ll07TFC, 1100, 011984, SE-54 1707 SCflNS (1707 SCflNS, 49.57 MINS)

4.0 MflSS RflNGE: 41.0, 446.3 TOTflL flBUNB= 718861.

i i i i i • ,—|— --r-—i—|—T T™I—i—T—r"T"T~r""~r i i i i4 6 8 10 12 14 16 18 20 22 24 26 28 30 32 34 36 38 40 42 44 46 48 50 52

MINS

* 363 RET. TIME: 13.55 TOT flBUNB= 3666. BflSE PK/flBUNB: 136.1/ 1788.

100-1

88-

60-

40-

20-

8 J

i;

N . D .

44 54 68 82 90 100 108 119

50 60 70 80 90 180 110 120 130

:6

«.

-

p48.8

i

..

CLIENT: ROY F. WESTON, INC. _____ DATE OF ANALYSIS: January 17. 1984

ANALYSIS NO.: H551 CHART NO.: TO 11784-09

59A60A

27B28B

U3B52B53B


EPA f mg/kg EPA f21A) 2.4.6-trichl orophenol___ N.D.22A) p-chloro-m-cresol __ N.D.24A) 2-chlorophenol___________N.D.

73B) benzo(a)pyrene_______N.D.74B75B

benzo(b)fluoranthene N.D.benzo(k)f 1uoranthene

31A) 2,4-dichlorophenol N.D. (76B) chrysene N-D:34A) 2.4-dimethylphenol N.D. (77B) acenaphthylene ______N-D-(57A) 2-nitrophenol N.D. " (78B) anthracene N.D.(58A) 4-nitrophenol N.D.~ (79B) benzo(qhi )perylene " N.D.

2,4-dinitrophenol '_______N.D. (80B) fluorene ___________N-D-4,6-dinitro-2-methylphenol N.D. (81B) phenanthrene N.D.4,6-dinitro-2-methyl phenol N.D. (81B) phenanthrene___________________

I64A) pentachlorophenol_________N.D. (82BJ dibenzo(a.h)anthracene N.D.[65A) phenol N.D. (83B) indeno(1.2,3-cd)pyrene N.D.

(84B) pvrene(61B) N-Nitrosodimethylamine____N.D.

BASE/NEUTRAL COMPOUNDS VOLATILES ^EPA t EPA |(IB) acenaphthene _______N.D. (2V) acroleinTRT ————— —————benzldine N.D.

1.2,4-trichlorobenzene N.D.3V) acr.ylonitrileW)benzene

(9b) hexachlorobenzene N.D." (6V) carbon tetrachjoricje_____N.D.(12B) hexachloroethane N.D." (7V) chlorobenzene_________N.D.18B) b1s(2-ch1oroethy! )ether N.D."~ (10V) 1.2-dichloroethane20B) 2-chloronaphthalene N.D. (11V) 1,1,1-trichloroethane N.D.25B) 1,2-dlchlorobenzehe________N.D. (13V) 1,1-dichloroethane _____N.D.26B) 1,3-dichlorobenzene _____N.D. U4V) 1.1,2-trichloroethane N.D.

1,4-dichlorobenzene N.D. (15V) 1.1.2.2-tetrachloroethane N.D.3,3'-dichlorobenzidine N.D. (16V) chlorethane

35B) 2,4-dinltrotoluene_________N.D. (19V) 2-chloroethvlvinyl ether N.D.2.6-dinttrotoluene_________N.D. (23V) chloroform _____N-D-

37B) 1.2-diphenylhydrazine______N.D. (29V) 1.1-dichloroethene N.D.39B) fluoranthene N.D. ' (30V) trans-l,2-dich1oroethene N.D.40B) 4-chlorophenyl phenyl ether N.D. (32V) 1.2-dichloropropane N.D.- - -•'———————=——=——————————!——————*———!——————*———r^—————————————————————— i JIJMI i——————;—————————;—————, - , . _..__.__ _ _ _ _ \f n;41B) 4-brotnophenyl phenyl ether N.D. (33V) trans-l,3-dichloropropene~4?B) bis(2-chloroisopropy1 )ether N.D.~ cis-l,3-dichloropropene N.D.

bis(2-ch1oroethoxy)methane N.D. (38V) ethyl benzene _____18°hexachlorobutadiene N.pT" (44V) methylene chloride _______iLfi,hexachlorocyclopentadiene N.D.~ (45V) chloromethane• _ . , ——————————E———————————•————,, ^—— ; *£\l \———i ..____j.i_-__54'BT" isophorone____________ N.D. (46V) bromomethane „________ N.D-

55B) naphthalene _________N.D. (47V) bromoform N.D.nitrobenzene_____________N.D. (48V) bromodi chl oromethane ____N.D.

62BT Fl-nitrosodi phenyl ami ne N.D~ (49V) fluorotri chl oromethane 8.263B) N-nitrosodipropylamine flg f jTTfl g "(50V) dichlorodifluoromethane N.D

^. bis(2-ethylhexyl)phthalate N.TD;?'Uu J (51V) chlorodibromomethane_____N.DI ) benzyl butyl phthalate N.D." (85V) tetrachloroethene N.D(68B) di-n-butyl phthalate N.oT" (86V) toluene N.D(69B) di-n-octyl phthalate N.oT (87V) trichloroethene(70B) diethyl phtillate N.oT (88V) vinyl chloride(TIB) dimethyl phthalate N.D.(72B) benzo(a)anthracene N.D."

CLIENT: ROY F. WESTON, INC. DATE OF ANALYSIS: January 17, 1984

ANALYSIS NO.: H551 ___ CHART NO.: T011784-09

PESTICIDES PESTICIDESEPA f mg/kg EPA # mg/kg(89P) aldrin_____________N.D. (103P) 0 -BHC______________N.D.90P91P92P93P

dieldrin N.D.chlordane N.D.4,4'-DDT N.D.4,4'-DDE N.D.

(94P) 4,4'-DDD_______________N.D.(95P96P97P(98P99PJ

<X. -endosulfan N.D.

104P) g -BHC105P) V -BHC __________N.D.106P) PCB-1242CB-107P)PCB-1254 N.D.108P)PCB-1221 N.D.109P

>g -endosulfan ___________N.D. (HOPendosulfan sulfate N.D. (HIPendrin N.D. (112P

PCB-1232 „ N.D.PCB-1248 N.D.PCB-1260 N.D.PCB-1016 N.D.

endrin aldehyde_________N.D. (113P) toxaphene ___N.D.100P) heptachlor ________N.D.101P) heptachlor epoxide N.D. DIOXINS

**(102P'———** "BHC————————————Mi- (129B) 2,3.7.8-TCDD (Screen Only}.- ,* ^

NOTES AND COMMENTS:

'OLATILE ORGANICS N.D. = <0.1 mg/kg

BASE NEUTRALS N.D. = «65 mg/kg

ACID EXTRACTABLES N.D. = <5 mg/kg

PESTICIDES?PCB's N.D. = <5 mg/kg

* NOT TESTED FOR THIS COMPOUND** SCREENED ONLY-NOT PRESENT

Thomas F. Cullen, Jr. 1Laboratory Director/Organics Division


HS51 .WESTON,20UL/25ML.D.I . ,E=2200,P/T u*,CLC,011884,1930,SE30 _ _ ____________777 SCflNS ( 777 SCfl

MflSS RWNGE:44.0, 431 .2 TOTtfU~S, 18.90 MINS)

5 6 7 8 9 18 l'l 12 13 14 15 16 17 18 19 20MINS

flVERflGED SPECTRUM * BflSE PKxflBUND: 64.I/ 32000. + 14 -10

100-j

58 -

0-

108-

58-

4

r-50.364

8

i

*CHLOROETHflNE*•

i60 88 180 128 148 160 188 288

375 r~

•50.3

.

228 240 268 280 300 320 340 368

H551 ,WESTON .28UL/2SML.B.I . ,E=2280,FvT UUiil 18861 , ____CLC, 011884,1938, SE38 _ _ __________777 SCflNS ( 777 SCftNS , 18.9© MINS

VMRSS RfflNGE:44.8, 431.2 TOTlfiL~l )|]H = 13111386.

4 5 6 7 8 9 10 l'l 12 13 14 15 16 17 18 19 28MI MS

flVERflGED SPECTRUM * BflSE PK/flBUND: 58.1/ 32000. + 39 -31

100-1

•

80-

60-

48-

20-

50

&S . 101

60 7

72 *TRICHLOROFLUOROMETHflNE

'0

IB 100 3ii?

r 1 5 . 9

480 98 180

»

H551 ,WESTON,20UL/2SML.D.I . ,E=2200,P/T B99 10061 , EE&I 2CLC,011884,1930,SE30 777 SCflNS ( 777 SCflNS, 18.90 MINS),+x 3.0 P FIftPftfV—44.0, 43lll2ni1Wl|LHflBqND= 13111306.

3 4 5 6 78 9 10 11 12 13 14 15 16 17 18 19 20

* 214 RET. TIME: 7.27 TOT flBUND= 12532. BflSE PK/flBUND : 91. 1/ 3725,

i eel-

s' e -

68-

48-'

20-,

51

1, . i l l , . . , . . i l0., —— , —— , —— ,_60

1-29.791

7765

|' • • • [ • • • • i - ',- - - , - • '

*•*TOLUENE

98 107 158 ; ;1 . . . . .

80 100 120 140

H551 , WESTON,20ULx2SML.il. I . ,E=22@0,P/T W33!t 10661 . BTK1 2CLC,811884,1938,SE30 777 SCflNS ( 777 SCflNS, 18.98 MINS)r»x 3.0 MjflS/TmrNttfli'——44.0, 43Jt(|f|.2nr[anrf|LVfiBUNB= 13111306.

I I I I I I I I I I I3 4' 5 6 7 9 10 11 12 13 14 15 16 17 18 19 20

MINS

* 322 RET. TIME: 9.88 TOT RBUND= 13629. BflSE PK/flBUND: 91.1/ 4118.

100-1

88-

60-

40-

20-

91

51

10-' —— r

65

|. Ii ,1,60

77

, ...III . „, ,

*ETHYL BENZENE

106 _ . x-v n f\ C Q

1 ..... ....80 100

1261

-30.2

120 140

CLIENT: ROY F. WESTON, INC.______ DATE OF ANALYSIS: January 17, 1984

ANALYSIS NO.: H551: _____ CHART NO.: T011784-12

21A22A24A

58A59A60A

8B

T42BT43B52B

54B55B56B

63B

1


EPA f nig/kg EPA f2.4.6-trichlorophenol________N«P-p-chloro-m-cresol ________N.D.2-chlorophenol ________N.D.

73B) benzo(a)pyrene________N.D.) benzoj) benzo(benzo(b)fluoranthene N.D.

75B)ben2o(k)fluoranthene N.D.(31A) 2.4-dichlorophenol______________N-D- (76B) chrysene N-D-(34A) 2,4-dimethylphenol N.D. (77B) acenaphthylene _____N^D.(57A) 2-nitrophenol N.D. (78B) anthracene ________N-li.

4-nitrophenol N.D. (79B) benzotqhi )perylene * N-L)-•—————————-t_——.——————————„.———————•••• I........——-————••• • •'_ • r -. _ -. t"———... •..-.»-—— —-— — -_ _2,4-dinitrophenol •' _____N.D. (SOB) fluorene ________________N-D-—r-—-———-—-———. n.. i ...———.-—-———————-——-——rr—?r-~— / x v^~\—————r _ ±. L .r~_ _ M r\4,6-dinitro-2-methy1 phenol N.D. (81B) phenanthrene _______N.D.———————————————————*—c———————————————— i - — \———cm—————i——. v._J.i_... ____———————M n '.64A T pentachlorophenol ________N.D. (82B) dibenzo(a.h)anthracene N.D.

765A]——phenol——— ———————————NToT (83B) indeno(l,2.3-cd)pyrene N.D.——————————————————————————- (84B) nvrene . nr°7

(61B) N-Nitrosodimethylamine____N-D-BASE/NEUTRAL COMPOUNDS VOLATILES ''.',

EPA f EPA f(IB) acenaphthene__________ N.D. (2V) acrolein

. benzidine N.D~ T3V) acrylonitrile) 1,2.4-trichlorobenzene N.D.77")benzene ____________22

(9B) hexachlorobenzene N.D. (6V) carbon tetrachloride(12B) hexachloroethane N.D. (7V) chlorobenlene" —— bis(2-cMoroethyT)ether N.D.' (10V) 1.2-dichloroethane_____ N.D.,

2-chloronaphthalene N.D.' (11V) 1.1,1-trichloroethane N.D..20B, ___________^5B) 1,2-dichlorobenzene N.D. (13V) 1,1-dichloroethane•——"——'" '••-———————————————————————•———————————————————————:—"— • • 11 i s————z——~——^ • i •* ~'~~ j. i_T.26B) 1,3-dichlorobenzene________N.D. U4V) 1,1,2-trichloroethane

(27B 1,4-dichlorobenzene N.pT (15V) 1.1.2,2-tetrachloroethane N.D.(28B) 3,3'-dichloroDenzidine N.D. (16V) chlorethane _____N.D:_. . . .... • ________ _(35B) 2.4-dinitrotoluene NToT (19V) 2-chloroeth.vl vinyl ether ——— N.D.(36B 2,6-dinitrotoluene N.D. (23V) chloroform ____________ -(37B) 1.2-diphenylhydrazine N.pT (29V) 1.1-dichloroethene^ —— fluoranthene ———————————— N.D. (30V) trans-1.2-dichloroethene N.D,,

40B) 4-chlorophenyl phenyl ether N.D. (32V) 1,2-dichToropropane______N.D,.41BJ 4-bromophenyl phenyl ether N.D. (33V) trans-l,3-dichloropropene N.D.•nr*x L - - ' " - r i . _ j ._.....__. .n i _j.i__._ »T r> _j_ 1 o w^/>kl nv</->n^nnono M nbis(2-ch1oroisopropyl)ether N.D." cis-l,3-dichloropropene

bis(2-chloroethoxy)methane N.D." (38V) ethvlbenzene ____________650..hexachlorobutadiene_______N.D. (44V) methylene chToride_______N.D._

53B) hexachlorocyclopentadiene N.D. (45V) chloromethane N.D.isophorone______________N.D. (46V) bromomethane UTo.naphthalene______________1100 (47V) bromoform N.oT

- - - — • • -HT T\nitrobenzene——— N.D. (48V) bromodi chl oromethane______NJ).._N-nitrosodiphenyl amine ______N.D. (49V) fluorotrichloromethanat p iTI————«-:————————i-rJ-———————.————!————————————————————————— I PAII I—————————T"5————_ i- fl .._„«„». 4. U,JTk» * *N-nitrosodipropylamine N.D.~ (50V) dichlorodifluoromethariETsl2-ethylhexyl)phthalate N.D. (51V) chlorodibromomethane

) benzyl butyl phthalate N.D. (85V) tetrachloroethene.(685) di-'rJ-butyTphthaUtV'' NTpT (86V j toluene" 135(69B) di-n-octyr)htha1ate N.D. (87V) trichloroethene(70B) diethyl phtialate N.D. (88V) vinyl chloride(71B) dimethyl phthalate N.D.(72B)benzo(a)anthracene N.D.


ANALYSIS NO.: H552 _____ CHART NO.: T011784-12

PESTICIDES PESTICIDESEPA * ms/kg EPA t mg/kg

(89P90P91P

aldrin________________N-D- (103Pdieldrin N.D. (104Pchlordane N.D. (105P

(92P) 4.4'-DDT_____________N.D. (1Q6P

0 -BHC____________________N.D.-BHC_______________N.D.

PCB^-BHC N.D.1242 N.D.

93P) 4.4'-DDE_______________________N.D. (107P) PCB-1254 ______________N.D.[94P) 4.4'-DDD N.D. (108P)(95P) «* -endosulfan N.D. (109P

PCB-1221 N.D.PCB-1232 ~ N.D.

(96P y8 -endosulfan .__________N.D. (HOP) PCB-1248 _______N.D.97P) endosulfan sulfate N.D. (HIP) PCB-126098P) endrin _________ N.D. (112P) PCB-1016 __________N.D.99P) endrin aldehyde N.D. (TOP) toxaphene_100P) heptachlor N.D.(101P) heptachlor epoxide N.D. DIOXINS

** "BHC—————————————M^. (129B) 2,3,7,8-TCDD (Screen Only); ; **

NOTES AND COMMENTS:

OLATILE ORGANICS N.D. =^0.1 mg/kg

BASE NEUTRALS N.D. = <5 mg/kg

ACID EXTRACTABLES N.D. = <5 mg/kg

PESTICIEDS/PCB's N.D. = <5 mg/kg

* NOT TESTED FOR THIS COMPOUND

** SCREENED ONLY-NOT PRESENT

'-A_____

Thomas F. Cull en, Jr.Laboratory Director/Organics Division


HS52,UESTON,5.0UL+20UL.I .S. .2SML.D.I . ,E*2200 13311 18065. JggCT '?.CLC,011884,2055,SE30 ______ 574'SCflNS ( 574 SCflNS, 26.73 MINS)

5.0 I IllirWFfMs¥flTBEJ 44.0, 431.1 TOTflL flBUND- 4810654.

3 4 5 6 7 8 9 10 1"! 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28MINS

* 58 RET. TIME: 4.80 TOT flBUND= 305. BflSE PKVflBUND: 78.1/ 57.

100-1.

88-•

68-

48-"

28-

8-

45

5

-.•(••

L

c7

60

6

• i -

7

7

'0

8

*BEN2ENE

IE

88 90 100

35

r-r

110 128 130 -

1 8 . 7

H552,UESTON,5.8UL+28UL.I.S.,25ML.D.I.,E=2208 pga l 10863,___CLC, 011884,2855, SE38 ______ 574 SCflNS ( 574 SCflNS, 26.73 MINS)r»x 5.8 J II irmi——MflSSirfflN). Mfl | 44.8, 431.1 TOTflL flBUND= 4818654.

I I I I I4 5 6 7 S 9 18 11 12 13 14 15 16 17 IS 19 28 21 22 23 24 25 26 27 28

MINS

* 110 RET. TIME: 7.18 TOT flBUND= 6849. BflSE PK/flBUND: 91.1/ 1817

100-1

80-

60-

40-

20-

0-

545

lU5«

1

1 1 ! [ 1 1 . . | l-l

9 68

6

4-

5 ?

i i . i | i . i » | i70

9

7

.l|....,...l.80 9£

L

*TOLUENE

Ml -0006198 107

J 100 110 120 138

38 ,,0

J

"1

H552,WESTON,S.0UL + 20UL.I.S.,25ML.D.I.,E = 2200 11311 18863. 18 1 2CLC,011884,2055,SE30 ______ 574 SCflNS ( 574 SCflNS, 26.73 MINS)

5.0 I llflfV.] iNflssirprflM Ifl i 44.0, 431.1 TOTRL RBUND= 4810654.

i i i i i i i i i i i i T — i — i —— i — T — i — r9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28

* 169 RET. TIME: 9.95 TOT flBUND= 24726. BflSE PK/flBUND : 91. lx 8192.

100-1.

80 -

68-

48-•

28-•

0- I ... 1c

5

;c

i56

h . i . u . i . i l') 60

9

7765

1 84

78 88 9(

1*ETHYL

1

97

3 188

6

BENZENE*•

)6

111 126 ; ;ll l|l II l|l III |l 1 II |ll •! |ll ""

118 120 130 -

33.1

H05S2, UESTON+IS(2 + 4)E=1800 O3QJ 28898 , GUI 186TFC,1550,011784,SE-54 1941 SCflNS ( 422 SCflNS, 12.48 MINS)*x 2.0 M |: Rp^jEt: r\41 -0JI, 446.1 TOTflL flBUNB= 10715044

3 4MINS


100-

88-

68-

48-

20-

0-

K

NflPHTHflLENE COELUTING WITHINTERNflL STflNDflRD (d-8 NflPHTHflLENE)

128

44 55 69 81 95 108 119

iii .ii, lid .ii.illlii ..iinilliii.. ..i.i.l.i....i..ii,li.i. ... lb.iMll 1 ,,,ll

;6

V

149 166.1... . l. '••JJ_, —— I -"---.-"- | l l l | l MUJJ —— l|l 1 11 | II 11. ,.,,, .[1.11 | 1 1 1 I J.,1 ...) 1 l l l [ l , —— 1-^ 1|"H|HI , ———— . ———— | ———— , —— , ,...., , ,

68 88 188 128 148 168

19.9

8RIQG063

CLIENT: ROY F. WESTON. INC._____ DATE OF ANALYSIS: January 18, 1984

ANALYSIS NO.: H553____________ CHART NO.: T011884-04


EPA" """" EPA* . mg/kg

_ -... ____(31A) 2.4-dichlorophenol/ -D*J\ ——— z^— = — — — — -= — =-"=

N-D-»hbenzo (b)fluoranthene

75B) benzol k)fluorantheni OTT

_-. ... ..i uîienui____________________^-^- (78B) anthracene______4-nitrophenol N.D. (79B) benzo(ghi )perylene2,4-dlnitrophenol ••'_______N.D. (BOB) fluorene/I f. __ J - J ~ -- «i—:——n——5—:————=———————————— ——————-r,w-u 1111 Lru-<:-metnyipnenoi___N.D. (81B) phenanthrenepentachlorophenol___________N.D. (82B) dibenzo(ath)anthra'cenephenol N.D. iota\ -t-j—/1 o -5 _j\_...-._-

(28B"356 fflj-dichlorobenzidine •—OT ifeV

2.6-dimtrotoluene

ethvl benzeneetnioeMzene

N.D.K ! .-aar-"—— -«-,t-uinnropnenoi ••_______N.D. (BOB) fluorene " ' N.D4»6-dinitro-2-methylphenol N.D. (81B) phenanthrene "

_____ -.--..--,-..., —,...- >... _______N.D.N-D- (83B) indeno(1.2.3-cd)pyrene N.D.

(84B) pvrene N.D.(61B) N-Nitrosodimethylamine_____N.D.

BASE/NEUTRAL COMPOUNDS VOLATILESEPA ' EPA # "^———acenaphthene_____________N.D. (2V) acrolein_______________*_JH———re!lz! ]ne _, __________N.D. '3V) acrylonitrile *~WP——^'^^-trichiorobenzene N.D. '4V) benzene N.D.TrlsT——êxacniorobenzene N^~ (6V) carbon tetrachloride N.D.

hexacnioroethane N.D. (7V) chlorobenzeî—— N.D.bisu-chloroethyljether 1TFT (10V) 1.2-dicMoroethane N.D.^-chloronaphthalene N.p. (11V) 1,1,1-trichloroethane"I.^-dichlorobenzene N.n. n?\i\ i i J.--UT_—_J.L.-_________^_^^^^_________N.D. (13V) 1,1-dichloroethane"_________N.D.1,3-dichlorobenzene__________N.D. (14V) 1,1.2-trichloroethane N.D.1,4-dichlorobenzene_________N.D. (15V) 1.1.2,2-tetrachloroethane N.D.3,3 -dl rhl nrr)hon-7irlino w n ' ' '•" ' ~ r~

2-chloroethyl vinyl ether N.oT(23V) chloroform • N~D7—————————

1.1-dichloroethene________N.D.trans-1.2-dichloroethene____N^D.

methylene chloride________N.D.chloromethane_______________N.D.bromomethane__________________N.P._bromoform______________N.D.bromodichl oromethane_______N.D.f 1 uorotri chl oromethane_____N.D.dichlorodifluoromethane____N.D.

1 5 1 V ) c h l o r o d i b r o m o m e t h a n e N . D .(85V) tetrachloroethene N.D.(86V) toluene 24

trichloroethene N.D.


ANALYSIS NO.: H553 CHART NO.: T011884-04

PESTICIDES PESTICIDESEPA # mg/kg EPA f mg/kg(89P(90P(91P


103P) 0 -BHC N.D.104P)# -BHC N.D,105P) V - BHC _______________N-D,

PCTP92P 4,4'-DDT________________N.D. (106P) PCB-1242________________N.D.(93P) 4.4'-DDE N.D. (107P) PCB-1254 NTo:(94P95P96P97P98P99P

4,4'-DDD_______________N.D. (108P) PCB-1221 __________N.D.c< -endosulfan N.D. (109Pjg -endosulfan . N.D. (HOPendosulfan sulfate N.D.endrin N.D.endrin aldehyde N.D.

111P112P

PCB-1232 * N.D.PCB-1248 N.D.PCB-1260 N.D.PCB-1016 N.D.

113P) toxaphene_____________________N-D-100P) heptachlor_____________N.D.(IQlPj heptachlor epoxide N.D. DIOXINS(102P) c -BHC N.D. (129B) 2.3.7.8-TCDD (Screen Only):;? **

NOTES AND COMMENTS:

VOLATILE ORGANICS N.D. = <0.1 mg/kg

BASE NEUTRALS N.D. = <5 mg/kg

ACID EXTRACTABLES N.D. •= <5 mg/kg

PESTICIDES ?PCB's N.D. =• <5 mg/kg

* NOT TESTED FOR THIS COMPOUND

** SCREENED-NOT PRESENT

P-\Thomas F. Cullen, Jr.

Laboratory Director/Organics DivisionLAB CERTIFICATION #: 08153

IHS53,WESTON, 10UL/25ML.D.I . ,20UL.I .S. ,E=2200 HID 10062JCLC,011884,2020, SE30

555

2482

147.7148.6

929

110.7111.6

72638

I I I i F I I I \ I I

i i i i TIT i i i i r i i4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 -19

UESTON.H0553+I .S. (2 + 4) ,E=1808 1J3B1 28891 , Q3H107CLC,011784,1710,SE54 1965 SCflNS ( 429 SCflNS, 12.48 MINS)r»X 2.0 iflSS tf^'GE " ,41.0, 447.41 TOTflL flBUND* 10407586.

18 11 12 13 14MINS

* 377 RET. TIME: 13.48 TOT flBUND= 7451. BflSE PK/flBUND: 136.I/ 1635.

100-

88-.

68-

40-

20-

136NflPHTHflLENE COELUTING WITHTHE INTERNflL STflNDflRD(d-8 NflPHTHflLENE) i;

44 55 69 81 95 188

ill .11.1 ll .M.llllll i l l l l . , l l l l . 1 . .. , 1. ll ll.l . . . 1 ..18 J ' 1 1 ' T ' " 1 ' 1 1 ' 1 ' 1 '

'.8

l.illll

*.

. 151 1661. . . . . . . . l.

21 .9

" T*t

ul 1 r . — y i | i | i | i | i |60 88 100 128 140 160 180 200

H553,UESTON,10UL/25ML.D.I.,20UL.I.S.,E=2200 H5HJ10062. WO-Ot 2CLC,011884,2820,SE30 743 SCflNS ( 743 SCflNS, 18.03 MINS)r*x 3.0 Mfl S MNfiEtft /MTFTT-lir lfOTflqnflftflhfiW 103.77000.

L I . I I I I I I I I I6 7 8 9 10 11 12 13 14 15 16 17 18 19

* 217 RET. TIME: 7.32 TOT flBUND= 1930. BflSE PK/flBUND : 91. 1/ 453.

100-

80-•

68-.

48-•

20-

0-

5145

Lu4J

77

6355

4-4-4-i50

--4-60

70

1 l . 1 | 1 , , 1 | 1 -.-,i78

91

81 85

M I 1 1 I ' • • 1 1 T-188 98

•23.5

*TOLUENE

98 107

1 . ! . . 1 . I . . .. I . 1 . . '•'•100

H553,WESTON, 10UL/25ML .D . I . ,28UL.I .S. ,E=2200 iigTCi 18862. BiHl 2.CLC,011884,2020,SE30 743 SCflNS ( 743 SCflNS, 18.83 MINS)j*-x 3.8 ' MflJS ^flNpE/; f .44 .0 ,. 3715 . ffoT: Qf *W *$.*} 10377000,

I I I I I I9 10 11 12 13 14 15 16 17 18 19

MINS

* 331 RET. TIME: 10.07 TOT flBUND= 34779. BflSE PK/OBUND: 91.1/ 11398.

180-.•

80-

60-•

40-

20-

.E

5

J;c

i

J3

656

60

3

l 69|||M. l|i nl|l 170

r32.891 *ETHYL BENZENE

784

II in n in il i ..,,....,....

106

97. . . . . . . 1 ,

80 90 108

ftiltOOSp111 126 P

i . . . 1110 120

if 8 - united states environmental protection agency · 2020. 7. 29. · do10 selenium 1.0

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