hyspec idt hyspec - hybrid spectrometer for the single crystal and polarized neutron studies at the...
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![Page 1: HYSPEC IDT HYSPEC - Hybrid Spectrometer for the Single Crystal and Polarized Neutron Studies at the SNS Steve Shapiro and Igor Zaliznyak Center for Neutron](https://reader035.vdocuments.mx/reader035/viewer/2022062721/56649f1d5503460f94c33b0a/html5/thumbnails/1.jpg)
HYSPEC - HYSPEC - HyHybrid brid SpecSpectrometer for trometer for the Single Crystal and Polarized the Single Crystal and Polarized
Neutron Studies at the SNSNeutron Studies at the SNSSteve Shapiro and Igor ZaliznyakSteve Shapiro and Igor Zaliznyak
Center for Neutron Scattering and Neutron Scattering Group
Brookhaven National LaboratoryBrookhaven National Laboratory
• Unique in its class
• Highest flux on small samples
• Easily adapted for polarized neutron studies
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OutlineOutline
• Motivation (SMS)• Science Case (SMS)• IDT and Budget (SMS)• Conceptual Design (IZ)• Performance and Comparison(IZ)• Summary (IZ)
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StatusStatus Fall, 1999
BNL initiates an effort to design a spectrometer for the SNS December, 2000
Concept of the Hybrid Spectrometer formulated and adopted March, 2001
First presented to EFAC. Received positive reply Fall, 2001
Instrument Development Team formed October: Workshop on the Hybrid Spectrometer held at BNL Refined HYSPEC concept presented to EFAC
January, 2002 HYSPEC IDT filed Letter of Intent with SNS
April, 2002 Formal presentation to EFAC
July, 2002 Letter of Intent accepted; Submit Scientific Proposal to EFAC
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MotivationMotivation
A and B category top priority - “potential day-one instrument”1 Report on the SNS Inelastic Neutron Scattering Workshop, SNS Document IS-1.1.8.2-8004-MM-A-00 (2000).
BS
HRCS
CNCS
ARCS
HYSPECHYSPEC
SNS Inelastic Neutron Scattering Workshop1
Argonne (11/99)
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Motivation from WorkshopMotivation from Workshop
Small single crystal samples Focussing Bragg optics
Broad range of standard sample environments Use of collimators and beam definers Sample environment separate from detector vacuum
Low background Time of flight Sample area out of direct beam Use of collimators
Vector Q in single crystals Moveable detector and rotatable sample
Polarization Analysis Proven and maintenance-free technology
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Motivation from WorkshopMotivation from Workshop
Page 5 of Report:
“This [high time averaged flux] opens up the possibility of utilizing triple-axis like methods to examine details of excitations when the important physics can be found at specific, well defined regions of Q and E space”
Recommended: “potential day-one instrument”
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Science CaseScience Case
Quantum critical pointsLow-D magnetismNanomagnetism and complex systemsDisordered and weakly ordered phasesAnomalous phonon behaviorStrongly correlated electron systems
– Hi Tc: YBCO experiment performed at ILL - IN22
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Polarized Neutron Study on Resonant Polarized Neutron Study on Resonant Mode in YBCOMode in YBCO6.85 6.85 (L.P. Regnault et al.)(L.P. Regnault et al.)
IN22Spin FlipP // Q
Rise due to increased counting time
• Much faster data collection
• Open new areas for polarized beam use
Sharp IC
Broad C
Unpolarized
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IDT MembershipIDT MembershipI. Zaliznyak, co-PI BNL HYPSEC INSTRUMENTHYPSEC INSTRUMENT
S. M. Shapiro, co-PI BNL DESIGN WORKING GROUPDESIGN WORKING GROUP
G. Shirane BNL
J. Tranquada BNL I. Zaliznyak (BNL)
L. Passell BNL S. Shapiro (BNL)
D. Abernathy SNS L. Passell (BNL)
L. Daemen Los Alamos V. Ghosh (BNL)
M. Greven Stanford (Monte Carlo Simulations)
B. Gaulin McMaster S. Doran (SNS/ANL)
K. Hirota ISSP (Engineering Design)
V. Kiryukhin Rutgers
G. Lander EITU
Y. Lee MIT
C.Majkrzak NIST
S. Nagler ORNL
R. Osborn ANL
L. P. Regnault CEN-Grenoble
J. Rhyne U. Missouri
C. Stassis Ames/Iowa St.
A. Zheludev ORNL
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HYSPEC IDT Organization ChartHYSPEC IDT Organization Chart
BNLBNL
Advisory CommitteeAdvisory Committee
Executive CommitteeS. Shapiro, I. ZaliznyakProject manager (TBD)
Executive CommitteeS. Shapiro, I. ZaliznyakProject manager (TBD)
SNS Instrument Group(SNS, ANL)
SNS Instrument Group(SNS, ANL)
Monte-Carlo simulationsL. Passell (BNL)
L. Daemen (LANL)
Monte-Carlo simulationsL. Passell (BNL)
L. Daemen (LANL)
Design Studies (V. Ghosh, … BNL)Design Studies
(V. Ghosh, … BNL)
Neutron Polarization TechniquesC. Majkrzak (NIST)
L.-P. Regnault (CEN-Grenoble)
Neutron Polarization TechniquesC. Majkrzak (NIST)
L.-P. Regnault (CEN-Grenoble)
Mechanical SystemsC. Stassis (Iowa State)Mechanical Systems
C. Stassis (Iowa State)
Neutron Beam Polarization(L. Passell, … BNL)
Neutron Beam Polarization(L. Passell, … BNL)
ShieldingShutters
Beam stop
ShieldingShutters
Beam stop
ChoppersChoppers
InstallationInstallation
ElectronicsElectronics
Mechanical Systems (Ames)Monochromator Drum
Analyzer vessel
Mechanical Systems (Ames)Monochromator Drum
Analyzer vessel
Detector Systems (Instrumentation Division, BNL)
Detector Systems (Instrumentation Division, BNL)
Engineering (BNL, ANL, TBD)
Engineering (BNL, ANL, TBD)
Software(LANL, SNS)
Software(LANL, SNS)
SoftwareSoftware
….….
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HYSPEC Budget EstimateHYSPEC Budget EstimateBudget estimates from:
• SNS engineering group (11/01)
• HRCS Summary (7/02)
Time Estimate:
• 5 years from funding
Primary Flight Path
Choppers 1400
Incident beam shielding 2300
Supermirror guides 500
Beam monitors 100
SUB 4300
Monochromator
Shielding 1000
Crystals and holder 400
Collimators 50
SUB 1450
Sample Stage
Goniometer, sample table 160
Ancillary equipment 250
SUB 410
Analyzer, detector
Collimator sets 200
Polarization benders 1000
PSD, electonics mounts 900
Beam Controls-DAQ 140
Detector vessel 1500
Beam stop/get lost pipe 200
SUB 3740
CAPITAL TOTAL 9900
LABOR (1/3 Capital) 3300
TOTAL 13200
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HYSPECHYSPEC: A Proposed Crystal-Time-of Flight : A Proposed Crystal-Time-of Flight HyHybrid brid SpecSpectrometer for the Spallation Neutron Sourcetrometer for the Spallation Neutron Source
Part 2: Conceptual design
T0 Chopper
Disc Chopper
Monochromator
Goniometer
Radial Collimator,or Bender Polarizers
Flight Chamber (evacuated or Ar/He filled)
Detectors
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Why Hybrid Spectrometer?Why Hybrid Spectrometer?
Monochromator vertical focusingMonochromator vertical focusing gaingain on SPINS@NIST: factor ~3factor ~3 even for m = 19 gm = 19 g sample (below)
Science challengesScience challenges
• small samples
• subtle features
• polarization analysis
• small signals, background-limited measurements
Need intensity boostNeed intensity boost
II00
3 x I3 x I00
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0 20 40 60 80 100108
109
1010
Ne
utr
on
cu
rre
nt
en
teri
ng
th
e g
uid
e (
n/s
)
Incident neutron energy Ei (meV)
Neutron current through 4x12cm2 guide entrance at 1.5 m from the moderator within E=2% of E
i
20 K coupled H2 (NISP interpolation)
20 K coupled H2 (MCSTAS interpolation)
H2O (MCSTAS interpolation)
MC calculation by E. Iverson
HYSPEC design choices: moderatorHYSPEC design choices: moderator
2.0*1012
1.6*1012
1.2*1012
0.8*1012
0.4*1012
0.0
20K H2 (decoupled)
Inte
nsi
ty (
n/s
R/μ
s/e
V/p
uls
e)
Coupled supercritical H2 moderator wins in thermal neutron range Ei<45meV
ambient H2O
0 100 200 300 400 500 600Time (μs)
Time-spectra of the neutron intensity from different moderators for EEii = 15.8 meV = 15.8 meV
Moderators useful neutron flux
coupled 20K H2
ambient H2O
Figure of merit is the total flux within t = 40-80 40-80 ss time window accepted by the spectrometer.
20K H2 (coupled)
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HYSPEC design choices: energy resolutionHYSPEC design choices: energy resolutiontt t/tt/tff E/EE/Eff
EEff=5.0 meV =5.0 meV 40 μs 0.0087 1.74%80 μs 0.0173 3.47%
EEff=15.0 meV=15.0 meV40 μs 0.015 3.0%80 μs 0.03 6.0%
EEff=30.0 meV=30.0 meV40 μs 0.021 4.25%80 μs 0.0425 8.5%
EEff=60.0 meV=60.0 meV40 μs 0.03 6.0%80 μs 0.06 12.0%
EEff=90.0 meV=90.0 meV40 μs 0.0368 7.36%80 μs 0.0736 14.7%
For given incident pulse length t instrument energy resolution is determined by the analyzer flight-path
Sample and detector size contribution to the instrument resolution is less than 0.5% each
TOF analyzer energy resolution for the length of the secondary flight-path LLSDSD=4.5 m=4.5 m and pulse lengths 40 μs to 80 μs is in the range 1.7% to 15%
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HYSPEC design choices: guide curvatureHYSPEC design choices: guide curvatureFlux on sample for different guide curvatures, parametrized by the corresponding offset at monochromator position.
Straight guide with m=3 supermirror coating is an optimal solution
0 20 40 60 80 100
105
106
107
HYSPEC flux simulated using MCSTASN
eut
ron
flux
on s
ampl
e (
n/s/
cm2 )
Energy(meV)
Beam offset at monochromator
0.0 cm 8.0 cm 12.0 cm 16.0 cm
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HYSPEC performance: vertical focusing gainHYSPEC performance: vertical focusing gain
Crystal-monochromator hybrid spectrometer (HYSPEC, top scheme) vs traditional “straight-through” TOF setup (MCST, bottom scheme).
HYSPEC wins except at 5 meV, where both concepts are rougthly equal.HYSPEC wins except at 5 meV, where both concepts are rougthly equal.
0 20 40 60 80 1000
2
4
6
8
Inte
nsi
tyH
YS
PE
C/I
nte
nsi
tyM
CS
T
Energy (meV)
simulation with MCSTAS
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HYSPEC performance: comparison with other HYSPEC performance: comparison with other inelastic instruments planned for the SNSinelastic instruments planned for the SNS
MC simulations by MCSTAS, V. Ghosh (2002)
CNCS, ARCS and HRCS intensities are re-scaled to HYSPEC energy resolution (such rescaling may over-estimate the actual intensity)
0 20 40 60 80 100
104
105
106
107
1CNCS model based on "Optimization...",J.V.Pearce et al. 2G.Granroth, Private communication
Neu
tron
flu
x on
sam
ple
(n/
s/cm
2 )
E (meV)
HYSPEC (no offset), coupled H2
CNCS1, coupled H2
ARCS2, H2O
HRCS2, H2O
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HYSPEC polarization analysis scheme: HYSPEC polarization analysis scheme: experimental demonstrationexperimental demonstration
S.-H. Lee, C. F. Majkrzak, Physica B 267-268, 341 (1999)
Heusler
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HYSPEC setup for polarization analysisHYSPEC setup for polarization analysis
Polarized incident beam is supplied by reflection from the vertically focusing Cu2MnAl (Heusler alloy) crystal monochromator
10meV < E10meV < Eiipolpol < 90meV < 90meV
Polarization analysis of the scattered neutrons is done by a set of 11-22 supermirror-bender transmission polarizers, each 2 cm wide, 5 cm thick and 15 cm high,
5meV < E5meV < Effpolpol < 25meV < 25meV
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HYSPEC layout in the polarized beam modeHYSPEC layout in the polarized beam mode
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HYSPEC performance in the polarized beam modeHYSPEC performance in the polarized beam mode
-10 -5 0 5 10 15 20
0
50
100
150
200Neutron energy 15meV
Inte
nsi
ty(a
rb.u
nits
)
Detector X co-ordinate (cm)
Bender width = 2cm All neutrons Spin up neutrons Spin down neutrons
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HYSPEC performance in the polarized beam modeHYSPEC performance in the polarized beam mode
0 5 10 15 20 25 30 350.0
0.2
0.4
0.6
0.8
1.0
Be
am
po
lari
zatio
n
Energy(meV)
Straight beam Deflected beam
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HYSPEC place in the SNS inelastic instrument suiteHYSPEC place in the SNS inelastic instrument suite
HYSPEC CNCS ARCS HRCSIncident energy range 5 – 90 meV 2 – 20(50?) meV 10 – 1000 meV 15 – 1000 meV
Maximum flux on sample
1.1 x 101.1 x 1077 at 15 meVat 15 meV
5.6 x 105.6 x 1066
at 5 meVat 5 meV7.8 x 107.8 x 1055
at 100 meVat 100 meV9.6 x 109.6 x 1055
at 100 meVat 100 meV
Energy resolution ΔE/E 0.017 – 0.15 0.01 – 0.1 0.02 – 0.05 0.015 – 0.05
Polarized beam YesYes NoNo NoNo NoNo
Intended sample size 4 (w) x2 (h) cm2 1.5 (w) x5 (h) cm2 5 (w) x7.5 (h) cm2 5 (w) x7.5 (h) cm2
Moderator-sample dist. 21.8m 36.2m 13.6m 17.5m
Sample-detector dist. 4.5 m 3.5 m 2.5 m 6.0 m
Angular acceptance 0.27 – 0.41 sR 3.1 sR 1.2 sR
Beamline # 15 5 18 17
Guide coating m = 3 m = 3.5 m = 3 – 3.5 m = 3 – 3.5
Guide Apertures (width x height, cm2)
entrance 4x12.8
main 4 x 15 exit 4 x 10
entrance 5 x 10main 5 x10 exit 1.5 x 5
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SummarySummary
HYSPEC will be a unique resource for probing correlations in condensed matter for
E [5,90] meV∈E [5,90] meV∈ E/E [0.05,0.15]∈E/E [0.05,0.15]∈
Q [0.3,10] ∈Q [0.3,10] ∈ ǺǺ-1-1 Q/Q [0.005,0.2]∈Q/Q [0.005,0.2]∈ Worlds most intense thermal neutron beam at a pulsed sourceWorlds most intense thermal neutron beam at a pulsed source Can optimize range of energy transfer and resolutionsand resolutions for
experiment Independent variation of Q and E resolution Polarization analysis capabilityPolarization analysis capability
The ultimate questionThe ultimate question: Do we need HYSPEC?LeadLead: Do we need 2 to 5 times larger flux2 to 5 times larger flux on sample compared to other SNS spectrometers and a polarized beam optionpolarized beam option?Our answerOur answer: Yes, we do.
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Appendix. HYSPEC performance: monochromator Appendix. HYSPEC performance: monochromator resolution functionresolution function
14 15 16 17 180.0
2.0x105
4.0x105
6.0x105
8.0x105
1.0x106
Inte
nsi
ty (
arb
.un
its)
Incident energy(meV)
MCSTAS,15meVstraight guides
before PG after PG
Significant part of the incident beam intensity - in the unwanted high-E tail
Requires a pulse-shaping chopper in a standard TOF setup
Is removed by reflection from the monochromator in HYSPEC
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Appendix. HYSPEC design choices: guide coatingAppendix. HYSPEC design choices: guide coating
Straight guide with m=3 supermirror coating is an optimal solution
Flux on sample for m=2, 3, and 3.5 supermirror guides (for 8 cm offset at the monochromator position).
0 20 40 60 80 100
105
106
107N
eu
tro
n f
lux
on
sa
mp
le(n
/s/c
m2 )
Energy(meV)
m=3.0 m=3.5 m=2.0
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Appendix. Intensity and pulse length of SNS Appendix. Intensity and pulse length of SNS moderatorsmoderators
1013
1012
1011
1010
109
103
102
101
100
10-1
10-1 100 101 102 103 104 105
Energy (eV)
E*I
(E)
(n/s
R/p
uls
e)
Pu
lse
len
gth
(F
WH
M,
μs)
20K H2 (decoupled)
20K H2 (coupled)
ambient H2O