groundwater analysis rpts for well location 3f, water ... · nel laboratories reno • las vegas...

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POOR LEGIBILITY

ONE OR MORE PAGES IN THIS DOCUMENT ARE DIFFICULT TO READDUE TO THE QUALITY OF THE ORIGINAL

NEL LABORATORIESReno • Las VegasPhoenix • Boise

Derek ReeveDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89112

TEL: 702-431-3020

RE Project GH-3F-2631

Dear Derek Reeve:

2027897Las Vegas Division

4208 Arcata Way, Suite A • Las Vegas, Nevada 89030702-657-1010 • Fax: 702-657-1577

RECEIVED'02 MAR 18 P« 1=30

Order No.. L0203115

NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefollowing report.

There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications except where noted in the Case Narrative.

If you have any questions regarding these tests results, please feel free to call.

Stan Van WagenenLaboratory Manager

Certifications:ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers

RenoAZ05201707CertifiedCertifiedNV033Certified

Las VegasAZ05182002CertifiedCertifiedNV052CertifiedCertified

Date

P: ,r' 7

NEL LABORATORIES

rl FFN'T- Dnmpro/Silversrare

PROJECT ID: GH-3F-2631

"RO.TF.rT#: GH-3F-26?'

MATRIX: AQUBOUS

Parameter

\t Hnnt-

hrn/rne

Bromobenzene

Bromochloromclhane•lioim.1i hloforrv-Ih jn j -

Bromoform

Bromomethane

2 B.jijnuucn-Butylbenzene

sec-Butylben/ene

icd-Bul>lbcn?i;nc

Cjrbon disulfide

Carbon telrachloridc

Chlorobenzenc

Chloroc thane

2-Chloroeihyl vinyl ether

ChUirofwm

i 'hloromethanc

-'-Chlorololuene: • not • ' iM.t '

Dibromuchloromethanc

1 ,2-Dibromo-3-chloropropane1 7-Dibrornnclhane

Hihrornnnie thane

1 ,2-Dichlorobenzenc

1 ,3-nichloroben?enc1 ,4-Dichlorobenzene

Dichlorodifluoromethanc

1,1-Dichloroethane1,2 Oichloroethanc

l,l-Dichloroethen*e

v.is-1 ,2-Dn.hlnruclhenc

\rans-l ,2-Dichloroethene

1 ,2-Dichloropropane


T,J UiclikiMiprupjm.1 .1 -Dichloropropcnc

-. "M 1 Dichlornprupcnt:

irans-1 ,3-DichlorupropcneEthylbenzene

Hcxachlorobutadienc.. HcxjnuriL

lodomethane

Isopropvlhenzcne

Result Unit32 up/L

NO pg,L

ND ug/L

ND ug/L

N".i ue'L

ND ug^.

ND ug/L

ND gg.1

ND- ug/L

ND ng/L

ND i,6a.ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND Hg/L

ND Hg/L

ND MSI :ND ug/L

ND ug/L

ND MlVL

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/l.ND ug/L

ND ug/L

ND ug/L

ND jig/LND pg/L

ND ug/l-ND UK/L

ND ugn.

ND ug'L

ND (jg/L

ND US/L

ND fig/L

N!1 pg'L

ND ug/L

ND ug/L

ReportingLimit

25~j ',5.0

5.05050

5.0

2 S

5.05.050

5.0

5.0

50

5.0

5.050

5.0

5.0S A

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

50

5.0

5.0

5.05.05.0.

50

5.0

505.0

5.05.025

5.0

5.0

CLIENT ID: GH-3F-263'

DATE SAMPLED: 3 il "2

NEL SAMPLE ID: L0203115-001A

DF1i11111i1111II11111i1I1i11111I11111i11I11111

MethodSW8260B

b\V«3fiOR

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8760B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SWS760B

SW82608

SW8260BSW8260B

SW8200B

SW8260B

SW8260B

SW8260B

SW8260BSW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260BSW8260B

SW8260B

SVY8260B

SW8260BSW8260B

SW82COB

SW8260B

SW8360BSW8260B

SW8260B

Prep Date Analjzed03/11/02

OV11'0203/11/02

03/1 1/02

03/11/02

03/11/02

03/11/02

OH/ 11/02

03/11/02

03/11/0203/11/02

03/1 1/02

03/11/02

03/11/02

03/11/0203/11/02

03/1 1/02

03/1 1/02

03/11/02

03/11/02

03/11/0203/1 1/02

03/1 1/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02ovi i/n?03/11/02

03/11/02

03/11/02

03/1 1/02

03/11/0203/1 1/02

03/1 1/02

03/11/0203/1 1/02

03/1 1/02

03/11/02

03/1 1/02

03/11/02

03/1 1/02

Analyst

DRM-LV

DRM L\'DRM-LV

DRM-LVDRM-LV

DKM-LVDRM-LV

DRM-I V

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LVDKM-LV

DRM-LV

DRM-LV

DRM-I VDRM-LV

DRM-LV

UKM-LV

DRM-LV

DRM-LV

DRM-I V

DRM-LV

DRM-LV

DRM-I V

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LV

DRM I VDRM-LV

DRM-LV

DRM-LV

DRM-LS'

DRM-LV

ND - Not Delected at the Reporting Limit

DF - Dilution Factor

Pate: ll-Wnr-M

B - Analyte detected in the associated Method Blank

S - Spike Recovery outside accepted recovery limits

F - Value above quantilalion range Page 1 of 5

, NEL LABORATORIES

H I M r-'.n.p . '?•:•.

PROJFCTID: GH-3F-263'

3'RorFrrs: cu IF.WMATRIX: AQUEOUS

ParameterK,r rvl.aM,en '

Mclhylene chloride4-Methyl-2-pemanonc

M TRF.

.Vaph'halcnc

•i-Propylbenzenc

<>,r~...

1 ,1 ,1 ,2-Tetrachloroethane

1 , 1 ,2,2-Tetrachloroetnane

I'eirachlorocthene1 o'ucni.

! ,2.J-Tnchlorobenzcne

' "J 4 Tr'rh'nrobrnvenr

1 1,1-Tnchloroethanc

1 ,1 ,2-Trichloroethanc

T richloroethcric

! , 1 .2-Tri(-hlororrif!uorocthane

I 2 3-Tnchloropropane

1 .2,4- 1 nmelhylbenzene

1 ,3.5-Trimethylbenzcnc

Vinyl acetate

\ i n v t h 'in It

o-Xylenc

m.p-Xvlcnc

Surr: Dibramuftuoromtthant:

Surr: Tolucne-d8

Surr: 4-Brnmofluorohenzene

rUFNTTD:

DATE SAMPLED:

NEL SAMPLE ID:

Result

N-n19

ND

NDNU

NDNDNDNDNDNDNDNDNDNDND

ND

NDNDND

NDNO

NDND9t>.6

93.7

78.4

Unit

, J ?-L

Ug/L

ue/t-up/L

f ig- l -

Ug/LI'g'L

Ug/L

ug/1-

ug/i-MS'"

Ug/L

UZ/I-

ug/L

MS/L

Ug/L

Mg/L

Ug/L

UB/Lug/L

J»g/L

U £ ^

M-S^L

Ug/L

%REC

%REC

%REC

ReportingLimit

50

50

25

50

50

5.0

5 0

5.0

5.05.0

5 05.0S.O5.05.05.0

s n5.05.05.05.05.0t o5.010

89-102

90-102

70-106

DFiili1

i1i1iiiIi11ii1i11ii1ii1

Method

SW8260B

SW8260B

SW82GOB

SW8260B

SWK26'>n

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SWR260R

SW8260B

SW8260B

SWX260B

SW8260B

SW8260B

SWS2fiOR

SW8260B

SW8260B

SW826UB

SW8260B

SW8260B

SW8260B

SW826UB

SW8260B

SW8260B

SW8260B

SW8260B

3/11/02

L0203115-001A

Prep Date Analyzed

03/11/02

03/11/02

03/11/02

03/11/02

nvn/n?03/11/02

03/1 1/02

OJ/ 11/02

03/1 1/02

03/1 1/02

03/1 1/02

03/1 1/02

03/1 1/02

OJ/ 11/02

03/1 1/02

03/11/02

03/1 I/O?

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

nvn/0203/11/02

03/1 1/02

ovn/0303/11/02

03/1 1/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

HRM-I V

DRM-LV

DRM-LV

URM-; \DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

PRM I \

DRM-LV

DRM-LV

DRM-I V

DRM-LV

DRM-LV

DRM-I V

DRM-LV

DRM-LV

DRM-LV

URM-LV

DRM-LV

DRM-I.V

DRM-LV

DRM-LV

ND - Not Detected at the Reporting Limit


Date: 13-Mur-02

B - Analytc detected in the associated Method Blank


£ - Value above quuniiunon range Page 2 of S

NEL LABORATORY

i : r . \ l . IJui::p,.u ^hCtdl j Ic

I'KO.IKCTID: GH-3F-26"'

-•KOJi ( T . J . oii ;!-:<>?•

MATRIX: AQUEOUS

i'.irameter

i t . mi -n

Calcium

Iron

Mij l inps ium

i'lHassiutn

Sodium

^ .t iudium

Antimony

Arsenic

Hr r v l l i u m

Cadmium

C'lirnmium

I l > U . l l l

Copper

Indium

I l'3<1

Mrkt-1

Selenium

SiUtr

Thallium

Zinc

Meicurv

Result

2(1

noo200

640

110

11)00

u :&0.0028

0.23

nno7guimn0.13

n of,o0.20

ND

0.081

0.33

ND

ono?i0.0063

0.85

ND

Unit

,.«•!

mii/J.

niR/L

mp/l.

"'ft/Imc/L

nig I

171 g/L

mg/L

me/L

iHR/1

mg/L

m!('l

mg/L

mg/LrnB/1-

mg/L

mg/L

nig/'

mg/L

mg/L

mg/L

ReportingLimit

OC2 '

?.5

0.50

2 510

2.5

<M>2S

00010

0.00100.0010

U.UOIO

oooion o n i o000100.001000010

O O O I O

O O O I O

OOOIO

000040

0.00100.00020

CLIENT m-

DATE SAMPLED:

NTI.S\M1'1E ID-

DP5

5

5

5

5

5s1I!

1

1

1

1

1

1

1

1

1

1

1

I

Method

WfiOlQB-To

SW6010B-TO

SW6010B-TO

SW60!OB-To

SW f.OKin 'Io

SW60IOB-To

SW6010B-To

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SV. 6020- Fc'U

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-TotaSW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 7470-Tola

CH-^F-263'

: vn/oi1 020^1 15-001B

PrepJDate

!' VI 2/02

03/12/02

03/12/02

03/12/02

i l « I2'02

03« 2/02

01 / 17/02

03/12/02

03/12/02

03/12/02

OVI2 '02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyzed

OV12/02

03/12/02

03/12/02

03/12/02

OJ/ 17/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

ni'p'0203/12/02

03/12/02

03/12J02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyst

JTY-Rcno

JlY-Reno

JTY-Rcno

JTY-Reno

JTY-Rcno

JTY-Reno

JTY-Reno

DHG-Renu

DHG-RenoDHG-RcnoDHG-Rcpo

DHG-KcnoDHG-Reno

UHO-R(.i,o

DHG-RcnoDHG-Reno

DHO-RcnoDHG-Rcno

DHG-Reno

DHO-Rrno

DHG-Reno

FIF-Reno

ND - Not Delected al the Reporting Limit


Date: 13-Mar-02



b - Value above quannutiun range Page 3 of 5

'I'-

NEL LABORATORIES

( N K N l - l > i mpeo/S:h estate

PROJECTED- GH-3r-2(>:'I 'KOIKM H ti!l-*r--?r,- '

Mvrwix: \ourow

I'aramcterB-inum

CaUiuni

Im.i

M.nJufMUin

Poia*;*;hiin

Smhuin

Vji iddium

Anlimonv

Arsenic

H -.I ' l l T

i"«lmuim

^hromuirn

( !'(>., II

Copper

Lead

N ^ U l l

-Menium

Silver

'u hum

Zinc

Mercury

Result

onzy57»

ND1H0

509X0

ND0.0014

00020

N't>

ND

ND0.0012

0.0037

ND00019

00083

NDND

0.051

ND

Unit

me/Lmg/L

mg/I

•ii;> 1

mfi/I-nig/!.

mg/L

mg/L

mg/l

Ml 1

mg/L

mg/L

mg/L

nigA,

mg/L

inj» 1

mg/L

mg/L

mg/X

mg/L

mg/L

ReportingLimit

000502 5

0 10

2 510

2 SOOOSO0.0010

O O O I Oo 00 ' ( 1

O O O I O

0.001(1

000)0

0.0010

OOOIOC 0 0 1 0O O O I OO O O I O

U OUQ40

0.0010

0 00020

CLIENT ID: GH-3F-263'

DATE SAMPLED: 3/11 /07

NEL SAMPLE ID: L0203 1 1 5-001 C

DF Method Prep Date

1 SW6010B-Di

5 SW6010B-DI

i SW6010B-Die - w onion ui5 SW601QB-DI

5 S W 6 0 I O B D .

1 SWGOIOH-Di

1 SW 6020-Diss

1 SW 6020-DKs

1 S'A 6020-').^'.

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW OWO-Di^S

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW7470-Diss 03/13/02

Analyzed

03/12/02

03/12/02

03/12/02

03' 12/02

03/12/02

03/1 2'Q2

03/12/02

03/12/02

03/12/02

i t J / 1 2 / t J

03/12/02

0^/17/02

03/12/02

03/12/02

03/12/02

Ul/ 12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyst

JTY-Rcno

.JTY-Reno

JTY-Rcnu

JTY Reno

JTY-Reno

)TY-Rcnn

JTY-Reno

DHG-Reno

DHG-Rcno

Uhlj-Renu

DHG-Reno

DHO-Rrnn

DHG-Reno

DHG-Reno

DHG-Renn

DHG-Rcno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

FIF-Reno


Of- - Dilution l-aunr

Date: I3-Mar-02

B - Analyte delected in the associated Method Blank

S - Spike Recovery outside accepted recovery lirruti

E - Value above quan illation range Page 4 of 5

. NOL LABORATORIES

'RO.TF< 1 ID: OH "1 ?6V

: OH-3F-26.V

DATE SAMPLED: 3-11702

NK1, SANfVLF, ID: T.0703115-00) D

•M XTHIX: AQUEOUS

Parameter

fhlori,!.-

^iT'i'r, a'. N

N-it V ,; V

. t •:.-.•Mki ' in i ty . Bicarhfin»tc (As CaCfW

\i^j l -n i !v . Carhonaic (A? l"3CCH)

1 lydroxidc (As CnC03)

Alkalinity, Total (As CnCO3)

fhf in ica l Oxygen Demand

^"mon.i a..v

';..!f,dc

1 olal Dissolved Solids

Result

noni.T.

ND

260U

f,«0

Nl)

ND

680

64

ND

ND

6130

Unit

•"K'Lrr,»'l.

nsj'L

mr/l.m?.1'mg/L

mg/i.

mi-A,

mc/l.

mjc'Lmg/L

mg/I

KeportingLimit

iO

2.52 5

Ml

250

250

750

250

10

0 30

0.030

«).0

DF

500

2S

25

500

H)

10

10

10

I1

14

Method Prep Date

EPA 300 0

EPA 300 0

f PA 300.0

B'A 300 ';

SM2320 B

SM2320B

SM7370B

SM2320 B

SM5520 D

SNW500-NH3

SM4500-S D

SM2540C

Analyzed

03/11/02

03/1 1/02

03/1 1/02

OV11/D2

03/11/02

01/1 I/O?

03/11/02

03/11/02

03/12/02

0V 12/02

03/12/02

03/11/02

Analyst

PJJ-LV

PJJ-LVPJJ-LV

P J I - l V

RDA-LV

KDA-l.VRDA-LV

RDA-LV

RDA-LV

RDA-l V

RWW-LV

PJI-LV


HF - Dilution Factor

Date: 13-Mar-02


S • Spike Recovery uubide accepted recovery limits

E - Value above quantiution range Page 5 of 5

NEL Laboratories, Las Vegas

CLIENT: Dumpco Silvcrstate\VorkOrder: 1.0203115Project: C.H-3F- '63'

ANALYTICAL QC S U> IM A IT> R K1 i ' JRT

TcstCcdc: 303 ',Vi IT:

Sample ID MB-R884

Client ID- ZZZZZ

Analyte

Chloride

Nitrate, as N

Nitrite, as N

.Sulfate

Samplypc: NiHLK

Batch ID. HS84

Result

ND

ND

ND

ND

TeitCode 300 W Units: me/1. PTCTJ Date "u" ID i. '.''-I f ^C ' ! ' . "i CJ r 'O '7

TenNo E300 Analy< i Oat: 3/11/02 'M.N.. 5" '6 '33 -ni*~ |"

PQL SPK value yp< RefVal 4 R J - C LowLmit ' . i^hLimil ?:P:') Rs-' Va i /Kl ' ! ' IM'HI. - "JLJ| ^ 7{ *!*->

010 d9

o.io J7,1 Z^o.io H!010 r

Qualifiers: ND - Noi '^elected at III? Reporting Limit

Anal>'e delected h t lnw quarinot ion lirnils

S Spike Kecovcry uuuide accepted recovery ! mils

R RPD ouLsidc accepted rccovei, limits

8 \na t \ l e detected if '-,,• j,:e •'••><td Mot ' i ' i

CLIENT:

Work Order:Project:

Dumpco/Silverstale

1,0203115GH-3F-2631

ANALYTICAL QC SUMMARY REPORT

TestCode: 6010\V D

Sample ID. MB-R659

Client ID ZZZZZ

Analyte

Samp Type: MBI.K

B a U h l D : R_R659

Result

TestCode. 6010W_D Units me/1

TestNo. SW6010B

PQL SPK value SPK Ref Val

Prep Date:

Analysis Date: 3(12/02

%REC LowLimit Highl mil RPD Ref Val

Run ID SUB-659

SeqN > 6434

° RPD RPDLtmit Qual

m

DOOID

5OIDmCO

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

ND

ND

ND

ND

ND

ND

ND

00050

0.50

O.IO

0.50

2.0

0.50

00050

Qualifiers: »D - Not Delected ai >he Reportina Limit

) - Analyte nclectcd b low quantiunon limit-.

S • Spike Recovery oul^ide accepted recovery limits

R - RPD outside accep'cd recovery I mils

B • Analyte detected in r o associated Method Blank

Page 2 of 14

CLIENT:Work Order:

Project:

Dumpco/Silversiate

L0203115(.H-3F-2631


TesiCode: 6010VV t

Sample ID. MB-3SI

Client ID: 7.ZZZZ

Analyte

Samplype- MBLK

Batch ID: R_351

Result

TestCode 6010W_t Units. mg/L

TestNo SW6G10B

PQL SPK. value SPK Ref Val

Prep Date. 3/12/02

Analyse Date: 3/12/02

%REC LowLnnil HighLimit RPD RefVal

Run IU SUB-660

SrqNn 6438

%RPD RPni.imit Oual

m

ccO13

O

1 3,m

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

ND

ND

ND

ND

ND

ND

ND

Qualifiers:

0.0050

0.50

010

0.50

2.0

0.50

0.0050

VD - Not Detected at the Reporting Limit

- Analyle delected below quantiui on limits

S • Spike Recovery outside accepted iccovery limits

R - RPD outside acceptc 1 recovery limits

B Analyte delected in tlir associated Method Ulank

Page 3 of 14

CLIENT: Dumpco/Siherstate

Work Order: L( 203 11 5

Project: GH-3F-2631

Sample ID: MB-R661 SampT pe:

Client ID: Z.ZZZZ Batch ID

Analyte

AntimonyArsenic

Beryllium

CadmiumChromiumCobaltCopperLead

NickelSelenium

Silverthallium

2mc

MBLK

R R66I

Result

NDNDNDNDNDND

ND

ND

ND

ND

ND

ND

ND

ANALYTIC AL QC SUMMARY REPORT

Test( ode: 6020\V_1)

TestCode 6Q20WJ) Unit* mg/L Prep Date: Run :i) SUB-SSI

TestNo. SW6020 Analyst' Date: 3/12,02 ScqNo 6445

PQL SPKvaliiL- SPK. Ref Val %REC LowLir l HighLitr.it RP! Ref Val 7,,X"D .W.V.. m.il Ou.il

J0010

0.0010

O O O I O

0.0010

0.0010

0.0010

0.0010

0.00100.00100.0010O O O I O

'.00040

0.0010

mr~r~•>CDOD">— 1ODm09

Qualifiers: ND - Not Detcaed at t h j Reporting Limit

I Analylede' jctedbcl w quantitai,on limits

S • Spike Recovery outside accepted iccovery l i tits

R RPD outsidf acceplen recovery limits

8 • \nalyte dctctied in ttv is>uciali.-d Mclliod Itbnk

Page •' •>! 14

CLIENT: Du npco/Silvt-rstate

Work Order: LOJ03115Project: GH-3F-263'

Sanple ID: MB-350 SampTy ie.

Cli.-nllD: ZZZZZ Batch i j

Anjlyte

An:imony

Aricnic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

MBLK

R_350

Result

NDNDND

NDNDNDNDNDNDNDND

ND

ND

ANALYTIC \L QC SUMMARY JREFORT

FextCode: (,C-20W_T

TestCode 6020\V_T Units mg/L Prep )ate. 3/II/H2 l-'un ID S1'0-«5S

TestNo: SW6020 Nr.alysis )ale: 3/12,112 ^^qN'i- 64:<<

i'QL SPKvilue SPK Ref Val %R£C . / iwLim' HighLtm • RPD Ket Val %!< '0 -'.'.'Ol mt v - j l

/0010

zmr-f—03Osn

i' 0010 , 30

oOOio ! friO O O I O , ^°

000 10

u O O l O

' 0010

oooio.'lOOIO

-> 0010s iOOlO

0.0010

a.ooio

Qualifiers: ND • Not Detened at thi Reporting L.mil

J Analyte delnted belo v quanlttatitMi limits

S • Spike Recovc'y outside accepted re,every lii'.ifs

R - RPD outside icceptrd recovery limi'-s

B • Analyte dc'.ct'ci! ia l jcia'.os M-thr <i 'i j

CLIENT: Dun.pco/Silvci stateWoik Order: L02I3115Project: GH-'F-263'

Sample ID: MB R893 ''arnpTyp.

Client ID: ZZ?,ZZ Batch 11

Analytc

Acetnne

Bcnrcnc

Bromobenzcne

Bromochloro methaneBromodichloromcthane

Bromoform

Bromome thane

2-Butanone

n-Burylbenzenc

sec-Butylbenzenc

tcrt-Butylbenzcnc

Carbon disullide

Carbon tctrachlonde

Chliirobenzene

Chloroethane

2-Chloroethyl vinyl ether

ChloroformCriloromethane

2-Chlorotolucne

4-Chlorololucnc

Dibromochloromethane

1 .2 • Dibromo-3 -chloropropane

1,2 Dibromoelriane

Dihromomethanc

1,2 Dichlorobenzenc

1,3 Dichlorobcnzene

1,4 Dichlorobcnjene

Du hlorodifluorrmcthanc

1,1-Dichloroethane1,2 Dichloroethane

1,1 Dichlorocthene

MBLK

X893

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDND

ANALYTICAL QC SUMMARY MTfPOKT

TcslCodc: i:f>()_W

eslCode: 8260_W Units. ug/L PrepU.le '• n, '!) t vo*MS-I 020." HI

TestNo: SW8260B A-.alysis Pile 3/11-02 S»oN.- 0048

i'QL SPK. value SPKRcfVjl %REC LowLimil l i ighLimit R.PD ^cf Val ' J'") 1,. I i i . i n . • Cujl

25505.05.05.05050255.05050505.050

5.05.0505.0505.0

5.05.0

5.0505.05.05.05.05.05.05.0

Qualifiers: ND Not Deleck.l at the H -porting Limit

J /5 nalyte dclci.! .-d beluv, juanl i ta t ion ' imi ts

S - S|> ke Recovers outside incepted reco\ery l imns

R • RPD outside a< tcpted r. iovcry limits

B - Ai .n l j t e detCi-Ioil ir Id ,>•»'<!' ,u\,j Vet i >J O.-II

CLIENT: Dumr<_rySi!veisuteWork Order: L020^i5Project: GH-M-263 '

Sample ID MB-R893 SompType

Client ID ZZZ7Z Ja t 'h ID

Analyte

cisO,? Dichloroethene

trans 1 ,2-Dichlorof thene



2,2-Dichloropropane

1,1 Dichloropropenc

cis-1 ,3-DichIoropropene

trans- 1,3-Dichloropropcne

Ethylbcnzene

Hexachlorobutadicne

2-Hexanone

lodomc thane

Isopropylbenzenc

p-lsopropyltoluenc

Methylene chloride

4-Mcthyl-2-pentanone

MTBE

Naphthalene

n-Propylbenzene

Styrcne

1,1,1 2-Tetrachloroethane


Tetrachloroethcne

Toluene

1,2,3 Tnchlorobenzene

1 ,2 ,4 -Tnchlorobenzene

1,1,1-Tnchloroethane

1,1,2-lnchlorocthane

Tnchloroethenc

Tnthlarofluoro me thane

1 ,1 .T-TnchlorotTifluoroelhane

MBLK

R893

Result

ND

ND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

Qualifiers: ND Not Detected at the Renortmg Limn

J - Analyte detcckd below q tantilation li nils

ANALYTICAL Qt SUMM -* KY 1 1 '; POP i ,

TessCorfe: S260 W

1 >(Code 8260_\V Units, u -/I Piep Dit Hun .0 I _S O,,\'-? :_ i2f -1 ' A

festNo. SWK260B \mlys isDa ' 3/U/02 i^Nu / (Ms

"'QL SPK^alue SPKRefVal ',,AEC Lr- vLimit H ghLirin , tPr^,\al R. ") L ' 1 ,i- -,-_-u_ -— -- , .1. MI -r— _ _ _ —ii n __ -.--mi TJ [ - -.vn.i_i.- Li.r-j.murr-.. I-. -..-..!._-- -j rri-L., ._-. ---m_-. -",— it

NEL LABORATOR

•50 m5.0

505050

505050255050

5050255010

5050

50

505050

5050505050

5050

S - Spike Recovery utside t^ epted reco\ try limits B - An ji ,tt . delected i '*ie „ .. j' <*•> 1 M n

R - RP ) outside jit p i e d r * % cry limits ' > ., ~ r , i

_0

< i- N t Du.npcu ^ iht 'Matc

Pr [oct GK-1F-2f."

i -1: 1 > ••:4-K8 Simp Type MBLK TesiCode

f t I t ' H1.7L RMoh ID KS9T TestNo

*• . u R.sult PQL

1 2 " Tn h ' r op-r . ND 5 0

! :,- i n .c" iMi i t - ND 50

1 3 ' fnn i 1 i v ND 50

Vir, -c. 'H ND 50

Vn (.tin- ND 50

o-v cv ND 50n r % > ; r " ND 10

S ' " I ) 1 nfU"- -dun 4928 5 0

S IT ' . d< 45 64 50c i - i -'Vjf en j842 50

t l i f t i ' t . N j - N o t **'< < t\ t l I* i'*.p( r a(* Lirn

' AnVy ' i . ' c ' t i l Scv qunr ' ' ' I " , , ' H T I '

ANALY TLCAL QC SUMMARY REPORT

lestCode. 8260_W

8260_\V Units Mg/L Prep Date Run ID L_VOAMS-2_020311B

SW8260B AialysisDale 3/11/02 ScqNo: 6048

SP1- value S}'< R,ef Va1 %REC Li wLimit HighLimil R J ' D R e f X j l %RPD RPDLimn Qua!

50 0 98 6 89 102 0 0

50 0 91 3 90 102 0 0

50 0 768 70 106 0 0

S -Spike 1 -unery fMiside accep ' recav n- limits B - Analjte u^tected i the associau d Method Blank

R- Rl'D ov 3 Jc acc-ptsd recovc I nuli Paei'8ofl4

NEL LABORATOR

men

CLIENT: Dun.p o'SiKciitateWork Order: L020M15Project: GH-31-263'

AJs'Al/i TIC \L QC SCVMAK^ PX; OUT

TcstCodc:

SampU ID MB-R898

Client !D ZZZZ7.

Analyte

Alkalinity, Bicarbonate (A< ' )CO3)

Alkalinity, Carborutc (As Ot'CH)

Hydroxide (As CaCO3)

Alkalinity, Total (As CaC03)

Sarnpl\pe MBLK

Sat.h ID R898

Result

ND

ND

ND

ND

ic 'Code ALK_W Jmts T../L C ' cpD: " 1 > %ri"V \ ' 2 ' > > ! M

T :btNo MI3:0 B V i a l v ^ s J s ' 3, 1J 02 ^ . u N i

?QL S P K x a l u e -PK Ref Val jREC Lo\s!n t ,,SnL -ni' RJ'D - ' \ it jc,i ) 1 ' '

•>5

25

75

25

Qualifiers: ND - Not Dctccied at the Reporting Limit

J - Anjlyle de ecu d hclois q janlilation limits

S - Spike Recover) o-.tstde ai epled recovtry limits

R - Ri D outsue a u i id av >.ery limits

die

CLIENT:Work Order:Project:

Dumpto/Siherbtuc

L020V, 15

GH-21 263'

ANALYTICAL QC SUMM

' .e COD

Sample ID MB-R900

Client II) ZZZZ/

Analyte

SaripType MBLK

A tch ID .-OOO

Result

T(.«.{_id« COD

Irs lNo Mf iZ IOC

PQ' SPK. \ iluc

Units n r !

t - P K R e f V a l

i f tp Di'c

•\ra! i s D a t VI : n

RLC L o v Limit ni j ihl i ' - 1

•>„,.

3 (, -'o

l'i"* c > •)! If

Chemical Oxygen Demand ND 1 )

Zrni""r~en*->

m

QualiTieri: ND - Noi Detected at ihe Reporting Limn

J Anal> le delected bi low quj .Illation limiu

S Spike Recover)'

f RPD uuideacc ' () iJ '

out ide accoted recovery limits B Am!)'" dt. ected 'n ') e ass

N limits

bnk

CLIENT:

Work Order:

Project:

Dumpco/Silverslaie

L 0 2 0 3 I I 5

GH-3F-263'

ANALYTICALQCSU

TcstCcde: I

.\l:\ RLi'ORT

Sample ID MB-359

Client ID- ZZZZZ

Analytt

SanpTypc MBLK

Ba ch ID. K_3S9

Result

TesiOide: HG_"'470_T Units: mg/L

li-stNo: SW7470

PQL SPKvj fue SPK Ref Val

! icp Date 3/13/02 \ur, !D •,<".* 669

\ n a K s i s D a t f .V13/02 ..^No '.45(1

"/.SEC Lov,limit ri'ghLimit R P D - ' : f \ 3 l %RI J) O J

Mercury ND 0 00020

O

IV.'

Qualincrs: ND - Nut Detected at ihe Reporting Limit

J • Analyte delected bi low quan'iiation limiii


R - RPD .jutside accepied recovery limits

B • ".nalytc Detected in the associated Me'.nyi L<l,.nk

Page U o! .'-'

('LIENT: Dumpcu/StlverstatcWork Order: L0203115

ANALYTICAL QC SUMMARY Rf.iMRT

Project:

Sample ID

Client ID

Analyle

GH-3P-2631

MB-R901 Simp Type: MQLK

ZZZZZ BakhlD: K901

Hesult

TesU ode

Tc;.:No

PQL

NH3-N_W Ur.its: mg/!.

M4500-NH3C

SPK value .SPK Ref Val

Prop Dats

\nal \5 is Date

VR&C Lov.Lirr.it !

TcslCodc: NTH3-N_\V

'.•'.-..n r.i :._.'.! _O:J" :H

3/;2,'flZ ":,:Nf •;",.>•

igM.imit R ' ' D R - j f \ j | v iRl ' l ' !••['!.;.••' 0 u.

ffir~

o1 -71

l >

^mmonla, as N ND 0.30 IO

i rr.

Qualifien: ND - Not Detected at the Reporting Limit

i - Anahte delected below quantitation limits

S • Spike Recovery ouside accepted recover, limits

R - RPD outside accep'ed recovery limits

B - Anahl'- detected in '.ho assniuin) M-ahoil II ,-II'K !

.. , .> y . j"iJg«f / . "/ . • j

CLIENT: Dumpco/Siherstate

Work Order: L0203115Project: GH-3F-26V

Sample ID MH-R879

Client ID ZZZZZ

Analyte

SampTypi. MBLK lestCodi

Batch ID R879 Tes'N

Result PQL

ANAI Y PC AX OC Sl'WARv '• Fx>

TcsiCoJc. Sl'I "_nA

SULF_W 'jmts mg/L Prep 'ijte K r 0 1 s f :_(t

vldSDO-S D \njly»is Date 11212 " i S',60

SPKvalue S P K h i - f V a l V 1LC LowLirn i Hi^i ii.nt s^D ^c Mi M'U t ' M

\T

Sulfidc ND 0030

m- r~

D3O

O'5moo

Qualifiers ND • Not Delected at the Reporting Limit

J • Analyte detected belou quantisation limits

S - Spike Recovery outside accepted r-covery limits

R- RPD outside accepted recover) .nits

B - A r d l j t e dck.tcd in the a<>nr ja t» i Method J'j ^

t 2C . 1 ',<


Dumpco/Siheistate

L0203115GPMF-26.V

ANALYTICAL QC SI MMAUY

: IDS V»'

Total DissoUcd Solids

Tl

Sample ID:

Client ID:

Analyte

MB-R307

/ZZZZ

SampTypc

Batch ID

MBLK

K907

Result

lestCodc

TestNo

PQL

TDS_W

E160.I

SPK. value

•JM

SPK Ft

• v mg/L

T Val %

Prep

Analys i s

R.EC LOV.LI.T

DJ'C K u r . i. V\.' _ ':o.l!!D

Dj'.c 3 /11 01 S-u >'„ s t ' ^ 0

, Hi^nit AO^fV.i ,-|) - ,U. . - ,,-.

ND

Qualifiers: ND • Not Di'ccled at the ^eportir,g .imit

J - Analyte detected belov. quantila'.on limits

S - Spike Recovery outside accepted iccovery limits

R - R?D outside accepted recover)' 'iruls

0 - AinlyU dc'i-lcd ir. ,! c •>MII.I.-' <* V.cihoJ .'mi A

"O A N A L Y T i C A LL A B O R A T O R I E S

Vanessa PadiiU> r.HM'.J.v,;, < ! :,

4208 AicaUt Way, Ste A

Certificate of AnalysisT'.LAV CertiDcare

05

USK Submission #• 2002030SKI

BSK Sample lOf^: \,l >'{<»>}

Submi.<3icn Connnrnb

Sarrvl-Tvp LiquidS-tniplt rviCiiptioir G i r.lF-Sample Comnient>

llojectDesc: Dumpco

Date Sampled- 03/11/2002

Time Sampled; 0851Date Received- 03/12/7002

Inorganics

AnaMe Method Result Units PQL DiluUoa DLRPrep AnalyiisDate Dale

Dissolved Organic Cutwn pOC) SMS^O-D mg/L 0 ? 5 10 03/13/200? 03/1V20C2

mg/L: Milligrams/Liter (ppm)mg/Kg: MiDigrams/Kilogiam (ppm)

>ig/L: Micrograms/Liter (ppb)Hg/Kg Micrograras/Kilogram (ppb)%Rec: Percent Recovered (surrogates)

PQL: Practical Quajititation LimitDLR; Detection Limit for Reporting

: PQL x Dilution

ND None Detected at DLR

H: Analyzed outside of hold tonePreliminary result

S: Suspect result. See Cover Letter for comments.E' Analysis performed by External laboratory.

See External Laboratory Report attachments

Pa«e2of21414 Staruskus Street Fresno, CA 93706-1 623 Phone 559-497-2888, In CA 800-877-8310 Fix 559-485-6935

?J£L LABORATORIES CHMNOF CUSTODY

^f£L f/i<£Z~

OW o inhng walai SOWW /asm Waiei AO01 C

Custody Seal ntact? Y

] Reimq jishefl by

;/^

13

Date/Time Dal; -£

•^-//~t?J.; ?1'";d

. ^

Thali»biHyo1NELUiboialofieslnc islmiiKjsIf ci,iolh«pnwolsdmple'i"aly5istortt-D_ei.amples'c~ oivedingocdcocidilonty '•JEL NELisicrticspor i 'e lor loss d^tr age itfi " p! rgcd'' =rrtci<; •> rut,«Unduding adequate sample vo/ums and nun-b«f c* i onlainers Customef ji3Ta!ure of this "cC const ILTICS a purchase order fcf NEL top*w*c rr> work and onsli Jss ucccpiaace -> 3)NGtS r i c a a l e s a ' J w i

31 NEL Slanbard List Puces lor all servi osofria/*^ lemon eêij' those acec/fiedoihem e «a ar vfL Q.j<xa'ion 'or Testing Services 10 8*ieci JMria li"" Ql saTip'e ei-îpl NE-'utraiGj o 'mss ace •" j 6j i3bo?atory»ri«i 1630 will b« eonsideieirecBivoi ".r.irie nexl i-t. vng day ;ommil/nerl o laboralci-) to ihe re^îteo 'umafo-ndtirne'ftill rucontir/ti-a ia Sanip'aC^^f naii; ansmp^c Ij •> e '»• -^r cei p

ORIGINAL

/ * ' t fif o


Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, Nevada 89030

702-657-1010 • Fax: 702-657-15771-888-368-3282

Ed CarltonDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89112

TEL: (702)431-3020

RE Project: GH-3F-263'

Dear Ed Carlton:

RECEIVED

Order No.: L0203115


There were no problems with the analyses and all data for associated QC met EPA or laboratoryspecifications unless noted in the Case Narrative.


Stan Van Wagenen »^ 'Laboratory Manager ^"^


Kv

Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CertifiedNV033 NV052Certified Certified

Certified

Date

NEL LABORATORIESV

CLIENT: Dumpco/Silverstate

PROJECTED: GH-3F-263'

PROJECT #: GH-3F-2631

MATRIX: AQUEOUS

ParameterAcetone

Benzene

Bromobenzene

Bromochloromethane

Bromodichloromethane

Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetraohlonde

Chlorobenzene

Chloroethane

2-Chloroethyl vmyl efher

Chloroform

Chlnrnmpthane

2-CHorotoluene

4-Chlorotoluene


1 ,2-Dibromo-3-chloropropane

1 ,2-Dibromoethane

Dibromomethane

1,2-Dichlorobenzene

1,3-Dichlorobenzene

1 ,4-Dichlorobenzene

Dichlorodifluoromethane

1,1-Dichloroethane

1 ,2-Dichloroethane

1 , 1 -Dichloroethene

cis-1 ,2-Dichloroethene

trans-l,2-Dichloroethene

1,2-Dichloropropane



1 , 1 -Dichloropropene

cis-1 ,3-Dichloropropene

trans-l,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodome thane

Isopropylbenzene



Date: l3~Mar-02

Result Unit

32 ng/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ReportingLimit

2550505050505025505050505050505050505050505050505050505050505050505050505050505050255050

CLIENT ED: GH-3F-263 '

DATE SAMPLED: 3/11/02

NEL SAMPLE ED: L0203115-001A

DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Analyzed

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV



E - Value above quantitation range Page 1 off

NEL LABORATORIESV



PROJECTS: GH-3F-2631

MATRIX: AQUEOUS

Parameter

p-Isopropyltoluene

Methylene chloride

4-Methyl-2-pentanone

MTBE

Naphthalene

n-Propylbenzene

Styrene

1,1,1 ,2-Tetrachloroethane

1 ,1 ,2,2-Tetrachloroethane

Tetrachloroethene

Toluene

1 ,2,3-Tnchlorobenzerie

1 ,2,4-Tnchlorobenzene

1,1,1 -Tnchloroethane

1 , 1 ,2-Tnchloroethane

Tnchloroethene

Tnchlorofluoromethane

1 , 1 ,2-Tnchlorotnfluoroethane

1 ,2,3-Tnchloropropane

1 ,2,4-Tnmethylbenzene

1,3,5-Tnmethylbenzene

Vinyl acetate

Vinyl chlonde

o-Xylene

m,p-Xylene

Surr: Dibromofluoromethane

Surr: Toluene-d8

Surr: 4-Bromofluorobenzene

Result

ND19

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND96.6

93.7

78.4

Unit

ug/L

ftg/L

ug/L

ug/L

"g/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

UR/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%REC

%REC

%REC

ReportingLimit

50502550505050505050505050505050505050505050505010

89-102

90-102

70-106

CLIENT ED: GH-3F-263'


NEL SAMPLE DO: L0203115-001A

DF Method

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Prep Date Analyzed

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV



Date: 13-Mar-02



E - Value above quantitation range Page 2 of 5

NEL LABORATORIES


PROJECT ED: GH-3F-2631


MATRIX: AQUEOUS

Parameter

Barium

Calcium

IronMagnesium

Potassium

SodiumVanadiumAntimony

Arsenic

Beryllium

Cadmium

Chromium

CobaltCopper

Indium

LeadNickelSelenium

SilverThallium

Zinc

Mercury

Result

2.0

1300200640110

10000.26

0.0028

0.230.0078

0.0037

0.130.0690.20ND

0.0810.33ND

0.0053

0.0063

0.85ND

Unit

mg/Lmg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/Lmg/L

mg/L

mg/L

mg/L

ReportingLimit

0025

25050251025

0025

0.0010

O O O I O

0.0010

0.0010

0.0010

0.0010O O O I O

OOOIO0.0010

0.0010

OOOIO0.0010

0.000400.0010

0.00020

CLIENT ID:

DATE SAMPLED

NEL SAMPLE ED:

DF

5555555111111111111111

Method

SW 6010B-TO

SW6010B-TO

SW6010B-TO

SW 6010B-TO

SW 60108-ToSW6010B-To

SW6010B-ToSW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-TotaSW 6020-TotaSW 6020-Tota


SW 6020-Tota


SW 7470-Tota

GH-3F-263'

: 3/11/02

: L0203115-001B

Prep Date

03/12/02

03/12/02

03/12/0203/12/02

03/12/02

03/12/0203/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/0203/12/0203/12/0203/12/02

03/12/02

03/12/0203/12/02

03/12/02

03/13/02

Analyzed

03/12/02

03/12/02

03/12/02

03/12/0203/12/02

03/12/02

03/12/0203/12/02

03/12/0203/12/02

03/12/02

03/12/02

03/12/02

03/12/0203/12/0203/12/02

03/12/0203/12/02

03/12/0203/12/02

03/12/02

03/13/02

Analyst

JTY-Reno

JTY-Reno

JTY-RenoJTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-RenoDHG-Reno

DHG-RenoDHG-RenoDHG-RenoDHG-Reno

DHG-Reno

DHG-RenoDHG-RenoDHG-RenoFIF-Reno



Date: 13-Mar-02



E - Value above quantitation range Page 3 of5

NEL LABORATORIES1 — _

CLEENT: Dumpco/Silverstate

PROJECT LO: GH-3F-263'

PROJECT #: GH-3F-2631

MATRIX: AQUEOUS

Parameter

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.029

570

ND18050980ND

0.0014

0.0020

ND

ND

ND0.0012

0.0037

ND

0.0019

0.0083

NDND

0.051

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0005025010251025

00050OOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIOOOOIO0 00040OOOIO0 00020



NEL SAMPLE ID: L0203115-001C

DF

l51555111111111111111

Method Prep Date

SW 60108-Di

SW6010B-Di

SW6010B-D1

SW 6010B-D1

SW6010B-Di

SW6010B-D1

SW 6010B-Di

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW7470-Diss 03/13/02

Analyzed

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyst

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

FIF-Reno



Date: 13-Mar-02




NEL LABORATORIES




MATRIX: AQUEOUS

Parameter

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

Alkalinity, Bicarbonate (As CaCO3)

Alkalinity, Carbonate (As CaC03)

Hydroxide (As CaC03)

Alkalinity, Total (As CaCO3)

Chemical Oxygen Demand

Ammonia, as N

Sulfide

Total Dissolved Solids

Result

1100

NDND2600

680NDND68064

NDND

6130

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

5025255025025025025010

0300030600



NEL SAMPLE ED: L0203115-001D

DF

5002525500101010101114

Method Prep Date

EPA 300 0

EPA 300 0

EPA 3000

EPA 300 0

SM2320 B

SM2320 B

SM2320 B

SM2320 B

SM5520 D

SM4500-NH3

SM4500-S D

SM2540 C

Analyzed

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/12/02

03/12/02

03/12/02

03/11/02

Analyst

PJJ-LV

PJJ-LV

PJJ-LV

PJJ-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RWW-LV

PJJ-LV



Date: 13-Mar-02




NEL Laboratories, Las Vegas Date: 13-M,ar-Q2


Dumpco/SilverstateL0203115GH-3F-2631

ANALYTICAL QC SUMMARY REPORTTestCode: 300 W

m

Sample ID MB-R884

Client ID ZZZZZ

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

SampType MBLK

Batch ID R884

Result

NDNDNDND

TestCode 300_W Units mg/L

TestNo E300


0 10

0 10

0 10

0 10

Prep Date Run ID L_IC-1_020311A

Analysis Date 3/11/02 SeqNo 5996

%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!

03oJO

ODOmCD

Qualifiers: ND - Not Detected at the Reporting Limit

J Analyte detected below quantitation limits


R - RPD outside accepted recovery limits


Page 1 of 14


Dumpco/SilverstateL0203115GH-3F-263'

ANALYTICAL QC SUMMARY REPORTTestCode: 6010W D

Sample ID MB-R659

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R_R659

Result

TestCode 6010W_D Units mg/L

TestNo SW6010B


Prep Date

Analysis Date 3/12/02

%REC LowLimit HighLimit RPD Ref Val

Run ID SUB-659

SeqNo 6434

%RPD RPDLimit Qual

m

03ODO

IDrn

Barium

Calcium

Iron

Magnesium

PotassiumSodium

Vanadium

NDNDNDND

NDNDND

00050

0500 10050

2 0050

00050


J - Analyte detected below quantitation limits




Page 2 of 14



ANALYTICAL QC SUMMARY REPORTTestCode: 6010W t

Sample ID MB-351

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R_351

Result

TestCode 6010WJ Units mg/L

TestNo SW6010B


Prep Date 3/12/02



Run ID STJB-660

SeqNo 6438

%RPD RPDLimit Qual

m

00ODO

ITJm

BanumCalciumIronMagnesiumPotassiumSodiumVanadium

NDNDNDNDNDNDND

000500500 1005020

05000050




R RPD outside accepted recovery limits


Page 3 of 14

CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'

Sample ID MB-R661 SampType

Client ID ZZZZZ Batch ID

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

MBLK

R_R661

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND


TestCode: 6020W_D

TestCode 6020W_D Units mg'L Prep Date Run ID SUB-661

TestNo SW6020 Analysis Date 3/12/02 SeqNo 6445

PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

O O O I O0 00040

O O O I O

TJ

\BO

RA

TO

R

mCO



S - Spike Recovery outs ide accepted recovery limits



Page 4 of 14

•


Sample ID MB-350 SampType


Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

SilverThallium

Zinc

MBLK

R_3SO

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ANALYTICAL QC SUMMARY REPORTTestCode: 6020WJT

TestCode 6020W_T Units mgTL Prep Date 3/12/02 Run ID SUB-656


PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLirmt Qual

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

OOOIOO O O I O

-••

Tj

*>»^\BO

RA

TO

RIE

S






Page 5 of 14

••




Analyte

Acetone

Benzene

Bromobenzene

Bromochloromethane


Bromoform

Bromomethane2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlondeChlorobenzene

Chloroethane


Chloroform

Chloromethane

2-Chlorotoluene

4-Chloro toluene



1 ,2-Dibromoethane

Dibromomethane





1,1-Dichloroethane

1 ,2-Dichloroethane

1,1-Dichloroethene

MBLK

R893

Result

NDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDND

NDND

ANALYTICAL QC SUMMARY REPORTTestCode: 8260_W

TestCode 8260_W Units fig/L Prep Date Run ID L_VOAMS-2_020311B

TestNo SW8260B Analysis Date 3/11/02 SeqNo 6048


255050505050502550

50505050505050

]

50505050

505050505050505050

5050

—ysJEL LABORATOR

mCO






Page 6 of 14

1




Analyte

cis-l,2-Dichloroethene

trans-1 ,2-Dichloroethene



2,2-Dichloropropane

1,1-Dichloropropene

cis-l,3-Dichloropropene

trans-1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodome thane

Isopropylbenzene

p-IsopropyltolueneMethylene chloride

4-Methyl-2-pentanoneMTBE

Naphthalene

n-Propylbenzene

Styrene


1,1,2,2-Tetrachloroethane

Tetrachloroe thene

Toluene



1,1,1 -Trichloroethane


Tnchloroe thene


1 ,1 ,2-Tnchlorotrifluoroethane

MBLK

R893

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDND

NDNDNDND

NDNDNDNDNDNDND




TestCode: 8260_W

TestCode 8260_W Units ug/L Prep Date Run ID L_VOAMS-2_020311B



50 150505050505050505025505050502550

105050

505050505050505050

5050

S - Spike Recovery outside accepted recovery limits B - Analyte detected in the associateijl Method Blank

R - RPD outside accepted recovery limits Page 7 of 1 4

' '

NEL LABORATOR

rnCO

wm




Sample ID MB-R893

Client ID ZZZZZ

Analyte




Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Surr Dibromofluoromethane

Surr Toluene-d8

Surr 4-Bromofluorobenzene

SampType MBLK

Batch ID R893

Result

ND

ND

ND

NDNDNDND

4928

4564

3842

TestCode

TestNo

PQL

50

50

50

50

5050

1050

50

50

8260_W Units pg/L

SW8260B

SPK value SPK Ref Val

50 0

50 0

50 0

Prep Date



98 6 89 102 0

91 3 90 102 0

768 70 106 0

Run ID L_VOAMS-2_0203 1 1 B

SeqNo 6048

%RPD RPDLimit Qual

0

0

0

—

O3ODO

§DOmCO

m






Page 8 of 14



ANALYTICAL QC SUMMARY REPORTTestCode: ALK W

Sample ID MB-R898

Client ID ZZZZZ

Analyte

Alkalinity, Bicarbonate (As CaCO3)Alkalinity, Carbonate (As CaCO3)Hydroxide (As CaCO3)Alkalinity, Total (As CaCO3)

SampType MBLK

Batch ID R898

Result

NDNDNDND

TestCode ALK_W Units mg'L Prep Date Run ID L_ATJTR-I_020311A

TestNo M2320B Analysis Date 3/11/02 SeqNo 6076

PQL SPK value SPK Ref Val %REC LowLirmt HighLimit RPD Ref Val %RPD RPDLimit Qual

25252525

i

. LABORATORIES

m




R - RPD outside accepte d recovery limits


Page 9 of 14

CLIENT: Dumpco/Sdverstate ANALYTICAL QC SUMMARY REPORTWork Order: L0203115 ^Project: GH-3F-263' TestCode: COD

Sample ID MB-R900 SampType MBLK TestCode COD Units mg/L Prep Date Run ID L_SPE;C-2_0203 1 2C

Client ID ZZZZZ Batch ID R900 TestNo M5220 C Analysis Date 3/12/02 SeqNo 6090

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

Chemical Oxygen Demand ND 10

? NEL

LABORATORIES






Page 10 of 14

CLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263' TestCode: HG_7470_T

ANALYTICAL QC SUMMARY REPORTWork Order: L0203115 ^

mSample ID MB-359

Client ID ZZZZZ

Analyte

Mercury

SampType MBLK

Batch ID R_359

Result

ND

TestCode HG_7470_T Units mg/L Prep Date 3/13/02 Run ID SUB-669


PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua!

0 00020

—03ODO

5mCO

Qualifiers: ND - Not Detected at the Reporting Limit S - Spike Recovery outside accepted recovery limits B - Analyte detected in the associatecl Method Blank

J - Analyte detected below quantitation limits R - RPD outside accepted recovery limits Page 11 of 14

iCLIENT: Dumpco/SilverstateWork Order: L0203115Project: GH-3F-263'

Sample ID. MB-R901 SatnpType: MBLK

Client ID: ZZZZZ Batch ID: R901

Analyte Result

Ammonia, as N ND

ANALYTICAL QC SUMMARY REPORTTestCode: NH3-N_W

TestCode NH3-NJW Units: mg/L Prep Date- Run ID' L_WC;_020312B

TestNo: M4500-NH3 C Analysis Date. 3/12/02 SeqNo. 6099


0.30

: * NEL LABORATORIES






<Page 12 of 14

1


Sample ID MB-R879 SampType MBLK

Client ID ZZZZZ Batch ID R879

Analyte Result

Sulfide ND


TestCode: SULF_W

TestCode SULF_W Units mg'L Prep Date Run ID I,_SP$C-2_020312A

TestNo M4500-SD Analysis Date 3/12/02 SeqNo 5960


0030

NEL LABORATORIES





B - Analyte detected in the associate^) Method Blank

Page 13 of 14

1




Analyte Result

Total Dissolved Solids ND


TestCode: TDS_W

TestCode TDS_W Units mg/L Prep Date Run ID L_WC,_020311D

TestNo E160.1 Analysis Date 3/11/02 SeqNo 6140


150

-.

TJ

03ODO

ODOmCO






'Page 14 of 14

03/15/2002 FRI 9:48 FAX 559 485 6935 BSK LABS §1002/002

BSK A N A L Y T I C A LLABORATORIES

Vanessa PadillaNEL Laboratories Las Vegas4208 Arcata Way, SteALas Vegas, NV 89030

BSK Submission #: 2002030581

BSK Sample ID #: 189800Project ID: L0203115

Submission Comments:

Sample Type: LiquidSample Description: GH-3F-263Sample Comments:

Certificate of AnalysisELAP Certificate #1180

Report Issue Date: 03/15/2002

Project Desc: Dumpco

Date Sampled: 03/11/2002Time Sampled: 0851Date Received: 03/12/2002

Inorganics

Analyte Method Result Units PQL Dilution DLRPrepDate

AnalysisDate

Dissolved Organic Carbon (DOC) SM5310-D 5.8 mg/L 0,2 1.0 03/13/2002 03/13/2002

PQL: Practical Quantitation LimitDLR: Detection Limit for Reporting

: PQL x Dilution

ND: None Detected at DLR

mg/L: Milligrams/Liter (ppm)rag/Kg: Milligrams/Kilogram (ppm)ug/L: Micrograms/Liter (ppb)ug/Kg: Micrograms/Kilogram (ppb)%Rec: Percent Recovered (surrogates)

Report AjfceD&ition Code: 1111119111111111111111111 ID ID II HI II

1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, m CA 800-877-8310 Fax 559-485-6935

H: Analyzed outside of hold timePreliminary resultS: Suspect result See Cover Letter for comments.E: Analysis performed by External laboratory.

See External Laboratory Report attachments.

Page 2 of2

NEL LABORATORIES CHAIN OF CUSTODY NEL Work Order: LOWReno • Las Vegas • Boise

Phoenix * Sacramento

'urchase Order NumberLas Vegas Division • 4208 Arcata Way, Suite A • Las Vegas, Nevada 89030

702-657-1010 • Fax: 702-657-1577 • 888-368-3282

ExpectadJSujJ Date

Requested Turnaround:

Time/DateSampled

N.E.LIdentificationCustomer Sample Identification

DW - Drinking Water SD - SolidWW • Waste Water AQ • AqueousOL - Oil/Organic Liquid A - Air

A, HCIB HNO3

C, H2S04'

E Ice OnlyF OtherG Not Preserved

Custody Seal intact'Con'

Relinquished by (Print) (Sjgrfature) Date/Time F.eceived by (Print) (Signa^ire) Date/Tima

The liability of NEL Laboratories Inc. is limited strictly to the price of sample analysis for those samples received in good condition by NEL. NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received in good condition,Including adequate sample volume and number of containers. Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions, Signature also constitutes acceptanced(NEL Standard (JSt Prices fot all services Oldered h6I8 on, exCBpt those specified otherwise via an NEL Quotation for Testing Servi ;es in effect at the time of sample receipt. NEL turnaround times are measured In regular vyorking days. Samples received at thelaboratory after 16:30 will be considered received on the next working day. Commitment of laboratory to the requested turnaround limp will be confirmed via Sample Confirmation transmitted to the fax number provided above,

ORIGINAL

AHORATORir.SWev Suite A • Lea Veqas Ni-va-'n {ft iO

7r>?.6.r>r-inio« r-w- -v- T -~

- . , . , . .-I <--uie•, - -\i- \* • i--y I

Las Vctv*s, N V '391

•RE Proiorr: IWH-3F-263'

Dear Derek "Reeve:

Order No.: L0203U6

NEL J^aboratories, Las Vegas received 1 sample on 3/11/02 far the analyses presented in thelnl\owingrepoti.



Lftborstorv Manager

Certifications.ArizonaCaliforniaIdahoMontanaNevadaNew MexicoUS Army Corps of Engineers

Reno Las VegasAZ0520 AZ05181707 2002Certified CertifiedCertified CeitifiedNV033 NVOS2Certified Certified

Certified

Date

Ciu:

NEL LABORATORIES CHAIN OF CUSTODY NEL Work OrderRano • Las Vegas • Boise

Phoenix • Sacramento

Purchase Ordei NunberLas Vegas DMsion • 4208 Arcala Way. Suite A- Las Vegas, Nevada 89030

702457-1010 • Fax: 7IK-65M 577 • BBB-369-3282

Requesl&d Turnaround:

Time/DateSampled

N.E.LIdentificationCustoiner Sample Identification

A.HCIB HNO,C H,60,D

C'jstody Seal intactConi

(Sigijfirffire} Date/Time (Signptura) Date/Tipn

c.

IX

Cr.tr

,inelua^a KHquat* umple volume and nurebw of eortamom. Cuttomgr signature at Ws DaC constitutes a purctmsu aider lor NEL to perfaiffl work and constitutes aooepumc* of nil NEL S'andaid Tefint a.td>Condrt!oni. Slgnalure eliooowt'duld NELSIirvdud Liit PACSI ft» all ssrv^u onte«d tww an, .except tho»« if«cltl«a »;hi(Wie v1» in NO. Quotation for Ttsting Survcei In efect a) r)w <me d sample ieoff.pl NEUIumMottrKl titia* »a measured in ngiflai \voiving Cays Srmplii nowed «l \ho

co^, »n.T 1E30 vail b« ooniidared receVad on Ihe ivisd tvoffeng d»y. CoanmHenartt or labordtory lo lh» raquesiBd turnaroirvJbm« wintua contnmet) vi» Sonip* Coflliimiuinn trorwrnced to th« lux nunrt* provided abe«».

roCO

rv>CO

Fpn;i: qi 170?47!130~'7

NEL LABORATORIESReno » las VegasPhoenix « Botes

Derek ReeveDumped/Silvers tate7900 Vegas Valley DriveLas Vegas, NV 89112

TEL: 702-431-3020

RE Project: DGH-3F-2631

Dear Derek Reeve:

Las Vegas Division4208 Arcata Way, Suite A • Laa Vegas, Nevada 89030

702-657-1010 • Fax- 702-657-15?71-888-368-3282

Order No.: L0203U6




Stan Vgft Wagofien" .Laboratory Manager


~~p


Certified

Date

I;-, r ..1 ,- rFi.l'l:-.'INRV'F i HMOf-fi

MEL LABORATORIESDuropco/Sih erstate

T.l.FPn

CLIENT ID: DGH-3F-263'

HATE SAMPLED: 3-'U/02

NEI.SAMPIYEIP: Lfl2031l6-OOlC

MVTH1X: AQUEOUS

Parameterrh'.ou.'C

Nurate, as N

>, f t- M U

SMII»UAlkalinity, B Ic»rban4t« (A* CnCO3)

Alka.u<icy. C irboiwc (A< CaCOl)

Hydroxide (As C^aCCM)

AlkaliuItVjTattl (A« C«CO3)

rii*rnic»J Otygert n^nan.!

Arnrruiiu, >•• N

Sulfidc

Total Distolvcil Solidi

Result

1300

ND

NTi

7<)0fl

(40

wnNO

<vU)

€1NDNO5619

Unit

me/Imt/Lirtj.t.

mc/L

nitt/L

mft/Lmp/Lmerl.

mg/Lnift/L

mg/Lmg/L

ReportingLimit

NO

2 52 i50

2502W25025010

0.300.030

600

DF5002575

50010!010101114

Method Prep Date

tPA 300.0

UPA 300.0

EPA 3000

EPA 300.0

SM2320B

SM2320 B

SM2320B

SM2320 B

SM5520 D

SM4500-NH3

SM4500-S D

BfA 160.1

Analyzed

03/J1/02

• O.Vll/02

03/11/03

03/1 1/02

03/1 1/0203/1 1/02

03/1 1/02

03/11/02

03/12/0203/12/02

03/12/02

03/11/02

Analyst

PJJ-LV

PJJ-LV

PJJ-LV

PJM,V

HDA-LV

RDA-LV

HUA-LV

RDA-LV

RTJA-LVRDA-LV

R\VW-LV

PJJ-LV

NO -Noj Oetetttd n the Reporting Unrii


Date: 12-Mar-Q2

B - Analyw delected in the wwciitcd Method Blink

S - Spfkc Recavoiy outside accepted recovery hmitiE • Value above quanriabon range Page 1 of3

FflX NO. 70<? 657 1577

NEL LABORATORIES

CLIENT: Dumpco/^ilvmtste

PROJECT 1 D: W rrf-3«-?& V

riJENT 10: DGH-3F-2631

BATE SAMPLED: 3.'J1'03

AT.L SAMPLE ID: L02 03 116-00 ID

MATRIX: AQUEOUS

'.'arametcrAtUPnu

BcrufriC

':rom« benzeneHrumocUlQro methanearomndif.hlofomtlhaner>rc.rToforn!

flronmrnrih ine2-tiuirmoiicn-Bi.rYlbcrizi.ncscc-Butylbsr,zenQim-SulvlbfriTcncCarbon disulluicCarbon ietra.:hlQridcChlorobennntChlorocthaji :.i-Chlorocrtv/l vinyl ethernilorrfarmCWorometbiins2-CWoro toluene4-CWOrotoliieni;Dibromoshbromctrmne1 ,2-DibK>nvi-3-chluroprop»pii1 ,2-D]bronv3«ihari«Dibrornomeihinci ,2-Dichlorobenzenc1 ,}-D!chlorobfln7enc1 ,4-DtCtllor:ibert2ene

Dich'.orndifloarometharie1 ,1 -DichlorotiMne1,2-Dichlotciettanc! .\-l3iohlofncthEnf....s-l 2-Dic ,|.>roethencIrarH'l ,2-Dif hlorocrthcns1.2-Dichloioprnp»ne1 ,3-Dichlo)xjprop»tic2,2-DichIwoprop«ne1,1-Dicbioiopropcn:cii-l j-Dicftloropropencitians-1 .S-KchloropropencEthylbenrencHwichloiibutadiene2-Hexatxveloctometharie[sopropylbcnzene

R«iul

••<!

MDNDNr>NDKDNDNONT)NDNI3

NDNDrVDNDNDNDNDNDNDNDNDNDNDNONDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

\t IJn!t

IIC/J.

MS'LHS/LMF/LjiJ^LU?/LH8/L

Hg'LMS/t^6/LMg/L

MB/LK8/LMB/L

H6/LM8/I-HS^-H8/L1 8 .

fg'LHfrT-HBrt-Mg/Ll^S/L

US"-H^LMg/l-

tLg/L

Hg'LHB/l-MS^-H'S-''-HE/t-JiS/LHB/L

K6/LMg/I.Ht/LHfi/LH«^HS'LM8«-JIE/LUg/L

RoportinuI'"*

?*

;.o50505.0505,025505.05.05.05.05.05.05.05.05.0SO505.05.0505.05,05.05.0505.05.05.0s.o5.0505.05.05.0505.05.050

255-05.0

DF

11i11111111111111111J111111111111111111I1I11

Method PregJSW8560BSW8260BSW8260BSW8260RSW8250BSW8260BSW8260B .SW&260DSW82606SW82SOBSV/8260BSWS260BSW8260BSW8260BSW8260BSWS260BSWR2«OflSW8260BSWS2608SW826QBSW8260ESW8260BSW82SOBSW8260BSW85SOBSW8260BSW8260BSWS260BSWS160BSW8260ESW8260BSWS2fiftBSW8260BSW8260SSW8260BSW82608S NV8260SSW8260BSWS260BSW8260BSW8260BSW82606SW8260BSW8260B

Oate AnalH^,03/11/0203/11/02OV1 1/0203/1 1/0203/11/0203/11/02Q3/1 1/02

03/1 1/0203/11/0203/11/0203/11/0203/11/0203/1 1/0203/11/0203/11/0203/11/0203/11/0203/11/0203/11/0203/1 1/0203/1 1/0203/1 1/0203/11/0203/1 1/0203/11/0203/11/0203/1 1/0203/11/0203/11/0203/11/0203/1 1/0203/1 1/0203/11/0203/1 1/0203/11/0203/11/0203/1 1/0203/11/0203/1 1/0203/1 W0203/11/0203/1 1/0203/1 1/0203/11/02

AnalystDRM-t-VDRM-LVDRM-I vDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVUliM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDKM-LVDRM-LYDRM-LVPRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LV

NO - Not Detected at the Reporting Limit

DF - Dilution Kactor

Date: 12-Mar-02

B - Armlyw detected (n the auociafed Method Blank

S - Spika Recovery outride iwcepted recovery limits

£ - Value above quwuitation range Page 2 of 3

I! ;;.»:'i J ' i i .N'H FAX NO. 70? 657 1577

NEL LABORATORIES

CLIENT: D .-nr>~n. '; .'.v^fav

PROJECT ID: 1XHI-31?-2<S,V

MATRIX: AQilfOUS

Paraineter

?-l.-opTOpy»tcluenc

M«thyl«ne cUldrirfeS-Mctliyl-Henuninw

MT«rNaphthalene

:i sv.pylfccn-m,;

Slyrens

t,l,1,a-TctrjehIarMlr,»ju:'. ,1 ,2,2-Tctrtcliloroot!ian«

TeTrachlorotiheneToluefio

1 ,2,3-TricWr.irobenmiM1 ,2,4-Yrichlijroticnzdnc

J,l.l-Tri<;hliirt>eth»n«

I,l,2-Tri«hli>roe!hurt8

Trichlorocthune

Tricrilorofluoromeirmnii

1 ,1 ,2-Tnd)l-3rotrifiuorocthiirte

1 ?.1-Trirhl5ronropanc

! ,2,4-Trimetbylbsnuenc1,3,5-Trirnsir.ylberuencVinyl accuse

Yinyl chlorde

0-Xylene

m.p-XyletwSurr: DitirtmtinuorDmrthaneSurr: Tclucnc-d8Surr: J-'.iromcfluorobcnMnc

Result

-•in1?

NDN'D

NOb?DNDNOMDNDNDNDNO

ND

NDND

ND

ND

NO

NPNDNDNDND

ND97.9

91.8

81.3

Unit»'g.'l.Iv^'L

MfL[Ig/L

Pfrt.

i* s -pjpyijJitt/C

^p/Lut/L,JilC/I*

Mg/LUR/£-

pifi/X.

ue'Lcs^HC/LH8/LKB«.fg/LHg/LMS/LHg/I-HS/LMS/LV.KEC

V.RCC

%RF,C

Reportingl.lmjt

50SOJ5

5.05.0

50

5.0

5-05.05.0

S.O5.05.0

5.0

5.05.05.05.05.0 .5,05.05.05.05.010

89-10290-102•70-106

CLIENT ID: T>nH-3F-263'

ft.YTE SAMPLED: Vll-'Q?.

NTL SAMPLE in: T,(KW*I ifi-ooiD

BF1

Iill1]lll11l1lI1'Ill1lII1111

Method

SW82SOBSWBMOBSwa?.60BSVV8260B

sw82fionSWR260S

SW8260B

SW82f300

SW8260BSW82SOBSW8260BSV/8260BSW8260BSW8260BSW8260BSW8260BSW8J60BSWS2«OBSW8260HSW8260BSW&260BSW8260BSWS260BSW8260BSW8260BSWS2608S \V8260BSWS260B

PrcjjJDate Analyzftd

03/1 1/02

03/11/02

03/1 1/02

OVU/02

OV11/02

01/11/02

03/11/02

03/1 1/02

03/1 1/02

03/11/02

03/11/02

03/1 1/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/0203/11/0203/11/0203/11/0203/1 1/0203/11/0203/11/0203/U/0203/11/02

03/1 1/0203/1 1/02

AnalystDRM-LV

DRM-l.V

DRM-LV

DRM-LVDRM-LV

DRM-l-V

DRM-LV

PRM-LV

DRM-l.V

DRM-LV

DRM-LVDRM-LV

URM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LVDRM-LVDRM-LVDRM-LV


DF - Oiluiion Ficur

; 12-Mar-Q2

B • Anilyte detect^! in (he uuociited Method Blank

S • Spifcfl Recovery outride wcepied recovery lirniu

E • Value above quuitiutian rmge Page 3 Of 3

-13-20f>? !JF'

* *r"i "* 1 "V * "*>'j i - <r * ' i -

rn.v NO. /a? nsy is:AX NO, 7?S 348 254B r. o;

ATH

cuDATE SAMPLED:

NMUiSAMPIJK !»;****•

frisft Ito'ft

rail,

(MS

0*71

M«

ND

S3Q

wet

»{/L

S*lffllusSilver

Smtiuta

ND

ND

n«offlj•J*t.75

ng/Lmg/Lrki/1-tnfi'l.

n f W l f i

(M/L

O.WI"

S S

0,0010o.oo in0-00100.0010

O.M

00010M

aOOio10

o.ooia0.0010

25ODOMO0.033

0.0010

P.?f W fft7l>.Tlji>4

SW«0»-T^!

1W«)10S-Te>«»l

SW6020-TealSW6020-TTOI

SWWlOB'TtrtuI

SW 6030-Tou!SWWloa-Toul

OVI 7A)'.

OV12/0203/IW1rrt/lZ/02

03/17/0303/tWli

1 SW<020-Tow( OVI3/liZ

Din a/02M/lt/03

03/t?«2llVll'OZ

03/13AH

03/1 ZAJl

03/13*1 JTY-It«n>

CW12A32

DHO MCBO

QJ/17/W

OVIW32

OV15AB

os/cvniOStZ/ltt03/12/02

TTY-RoeoDHG-tMBO

DHO-RWO

v:> T^^ •- *. $ *V « "p I..7;..* ..'•: -s A • • > » •-' *. . ^». .«i' -lr» ?- •..-,.- ..- A. --•- j • ' •« ' •'•'- • - "" -" '*• '"'

I 1-.'".'.'• :. ' n i - ^ r ,v-J j i

CUKNT- NGt TJ* Vem

CT ID; /Vi'»

MATRfX; AQUEW"

Awtooor

8orlu-e

Chromium

()(W

Usri

NVle!

Xrftoiatn

Sodioro

IMJS

?**»*

Kft

HO

JM

»JM«

fcfW

ND

ND044*

mp'L

•OCA,

ms/U

l/lg/L

m^U

BOf/1*

CMHNT IDj

DATUSAKfPLEO: 3'11/OJ

N-'l^*MnJRlf>: M i**"

Reporting»4nrft REf/.oom i

unosno.ootoOOOIO

3.J

O.OOIQ

(l«»004010

O.IO

U.MlO

aj0.0010

too.noioo.ooio

250.00040

SW WUft-W*!

5W60lOft-Di»

I SWMI(W-Di»

I

j ft,

OVU'02

Kunm(W/I370S

AB&*

JTTHW10

OKO-feoo

DHO-JUftO

DKC-tutoJTY-Heno

»/l?/M03/13/02 iTY-ftMO

wnaw OHQ*B»JTY-IU(*oDHC-HW5

03/12ATI

03/12VB2 /TY-dnioOM2/02

ND - N« CMtswJ rt e» Reportfflg Uwrtt»P. \ t f i\f A 13? • v'

.i Li-'M 'f-j,.L.

SCS Engineers

To: Steve Wall From: Ed Carton

Fax: (415) 947-3530 Date: March 20, 2002

Phone: (41b) 972-3380 Pages: 23 (including cover sheet)

Re: Analytical Data - DGH-3F-263' CC: Sandra Doty, Brent Lewis

O Urgent 0 For Review Q Please Comment D Please Reply D Please Recycle

•Comments:

Duplicate sample for GH-3F-263' which was faxed previously


Derek Reeve

Vegas Valley DriveLas Vegas, NV 89112

TEL: 702-431-3020

RE Project. DGH-3F-263'

Dear Derek Rcc\c

Tt. .--r-H


702-657-1010 - P a x 702-057-'57?

RECEIVED'••§•:! HftR 18 PH 1=30

Order No.: L0203116

NEL Laboratories, Las Vegas received 1 sample on 3/11/02 for the analyses presented in thefb'lrnvnq report


If you have any questions regarding these tests results, please feel free to call

Stan Van Wagenen /1 ahoratorv Manaeer

Certifications-ArizonaCaliforniaIdahoMontanaNevadaisew MexicoUS Army Corps of Engineers

) cy^~~*^



V/S:/QDate

.NEL.LABORATORIES

C L I K N l : Dumpco/Silverstate

I'RO IKCT 11): !>GH-*r-?.6V

J'KOJECT !#: PGr)-3F-;><W

MVTU1X: AQUEOUS

1' • r urn (IT

Barium

(Calcium

Iron

" '.tj'iiesMim

i'ot.iivium

v. i J i u n i

Y a n u U i u m

Antimony

Arsrnic

H c r v l l t u m

r'admium

f l i r u m i u m

Cobalt

Copper

Li-ad

-u-krl

Selenium

S.'-. tr

Thallium

Xinc

Mercury

Result

2.2

1400

220

(.90

no110(1

0.29

0.0016

0.73

0.0079

0.0018

o is0.070

0.19

O.ORO

n .wNU

ND

ND

0.75

ND

I'nil

niE/L

mg/L

me/1,

mii'i.

mg/1.

mtt !

mg/L

mg/L

mp/I.

m(j/L

mfi/L

niK/1

mg/L

mg/L

mg/1^

mjvL

mg/L

mg/I.

mg/L

rnR/L

mg/L

Reporting1. imit

0.025

2.5

050

2.5

10: s

0025

0.001Q

0.0010

O O O I O

0.0010

O O O I O

0.0010

0.0010

0.0010

G O O 10

0.00 10

O O O I O

0.00040

0.0010

0.00020

CLIENT ID;

D4.TK SAMPLED:

NEL SAMPLE U):

DF

5

5

55

5S

51il1111111II11

Method

SW6010B-To

SW 6010B-To

SW6(HOB-To

SW 60l')B-'lu

SW6010B-TO

s'A <.{)!{' '< To

SW 601 OB- To

SW 6020-Tota

SW 6020-Tota

SW f.020-Tiiu

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020 T.iu

SW 6020-Tota

SW 60?<>-Tota

SW 6020-Tota

SW 6020-Tota

SW 7470-Tota

DGH-3F-263'

.VU'O?

L0203116-001A

Prep Date

03/12/02

03/12/02

03/12/02

OJ/ 12/02

03/12/02

nvi;-o:03/12/02

03/12/02

03/17/02

01/1 2-02

03/12/02

OVP'O?

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyzed

03/12/02

03/12/02

03/12/02

u i - 12/02

03/12/02nv.j'o?03/12/02

03/12/02

03/12/02

OJ/1J/02

03/12/02

03/12/0?

03/12/02

03/12/02

03/12/02

03' 12/02

03/12/02

OV12/02

03/12/02

03/12/02

03/13/02

Analyst

JTY-Reno

JTY-Reno

JTY-Rcno

J"! Y-Kcnn

JTY-Rcno

TY-Rcr.'

JTY-Rcnn

DHG-Rcno

DHG-Reno

DHG-Rcn.i

DHG-Reno

DHn-Rt-no

UHG-Reno

DHG-Reno

DHG-Reno

inr R mDHG-Reno

DHG-Rcno

DHG-Reno

DHG-Rcno

FFF-Reno

ND - Noi Detected ai the Reporting Limit

U!- - Dilution 1-acior

Date: 13-Mar-02


S - Spike Recovery ouliidc accepted recovery limib


, - : U Y r.",. i f- i • ' _ . > . : : , _ • ' ! r - 4 • ± L

.NEL.LABORATORIES

l 1FNT:

J'KO.VKCTrf:

AQUiEOUS

e ' j lc ium

Magnesium

Sodium

Vanadium

A n t i m o n y

Beryllium

i hrcmmim

Cobalt

fm-kcl

Thallium

7ilK'

CLIENT!!): DGH-3F-263'

i)-UK SAMPLED: 3 i l ' n '

NKL SAMPLE JT>: 1,0203116-001B

Result

o.o?y57(1

NO

180

«:»

980

ND

00019

i) H)J8

ND

ND

ND

0.00130 0043

,\'O

0.0022

0.0078

ND

ND

0.046x *•

Unit

mj./L

ms/L:•"!','

me/1.

rr.K'lmR/L

mg/L

mg/L

mi} 1mg/L

mp./t

m|j,'Lmg/I^

niR/Lr,u; ,,

mg/L

mg/1,

mg/L

mg/L

mg/L, .; I

ReportingLimit

U 0050

2 5' 'if:

2 SHI

7 5

0.0050

O O O I O, , r .o ;oO O O I O

O O O I O

noo io0.0010

OOOIO

00010

O O O I O

O O O I O

0.0010

0 00040

0.0010

0 TT'»

DJb Method Prep Date

I SW6010B-D!

i SWC.OIOB-DI1 S\V f,0103 Oi

5 SW 60108-Di

i SWf,OinB-Di

5 SWoOIOB-Di1 SW6010B-Di

1 SW 6020-Diss

1 SW 6020 (•'isi

1 SW 6020-Diss

1 SW 60?0-Di«

1 SW 60?0-Diss

1 SW 6020-Diss

I SW 6020-Diss

! V.v f.0?0 Pi."

1 SW 6020-Diss

1 SW 6020-D.ss

1 SW 6020-Diss1 SW 6020-Diss

1 SW 6020-Diss, c\y ^-"i f) oim/ni

Analyzed

03/12/02

03/17/02

(.?'i?'()203/12/02

OV12TO

03/12/02

03/12/02

03/12/02

o < 12 o;03/12/02

03/12/02

03/12/02

03/12/02

03/12/02pv-i'fn

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02OV] TO?

Analyst

JTY-Reno

JTY-Rcno

1 rY Km >

JTY-Reno

JTY-Rciu)J 1'Y-Reno

JTY-Reno

DHG-Reno

DUG Ken'

DHG-Reno

DHG-Renn

DHG-Reno

DHG-RenoDHG-Renor>HP, V,,r. ,

DHG-Reno

DHG-Reno

DHG-Rtno

DHG-RenoDHG-RenoKIF »<-pn

NO • Noi Delected ai the Reporting Limit


Date: Il-Mur-02

B - Analyte delected in the aiiocntcd Method Blank


E - Value above quiinnlalion range Page 2 of 5

.NEl.LABUHAIORitS

^ 1 Ib.M

PROJECT in:PROJECTS:H< \ i i-M V

PGH-?F-?6V

CI.IF.NT ID. DGH-3F-263'

DATE SAMPLED: 3/11 /O"!

NF( SAMPLE ID: 10203116-0010

Parameter

t I.U.riiirr l V - "v

Nitute. as N

Ukalinily, Bicarbonate (As CaCO3)

Alkalinity, Carbonate (As CaCO3)

I [ydroxuV (A< C iCOl)

VIk . , :n . lv !.,!.,! (As C j( CH)

Chi'miml Oxyjjcn Driniin'l

Ammonia ^ N

S i l l i d c

Tutal Dissolved Solids

Kesitll

1703

r,;NO

2900

640ND

ND640

61

ND

ND

5610

Unit

n^l.

• J i

ine/L

me/I.mfjl.mg/t .

mo/t

inj. 1

mK/L

mg/L

mg/L

mR/L

I irmt PF

YI 5(i;,.j * ~ *2 * 25

5v 500?SO !0

?SO 10

?10 10

2'0 .'J

10 1

030 1

0 030 1

60.0 4

Method PrcgJOale

hPA 300 0

U- \ } 0 ,

EPA JOO.O

f PA 300 0

SM2320 B

SM2320 B

SM7370 R

W.2i:'> !

SM5520 D

SM4500-NH3

SM4500-S D

SM2540 C

Analyzed

03/11/0?

( • . ; ••03/11/02

03/1 1'02

O U 11/02

03/1 1/02

01/11/02

01 i : 'n?03/12/02

03/12/02

03/12/02

03/1 1/02

Analyst

P1I-I V

!•)! : \PJJ-LV

PJJ-LV

RDA-LV

RDA-LV

RDA-I.V

Rll* I V

RDA-LV

RDA-LV

kww-i \PJJ-LV

ND - Not Delected at the Reporting Limit

DF • Dilution Factor

Date: 13-Mar-02

B - Analyle detected in the associated McLhitd Blank


E - Value above quanttuuon range Page 3 of 5

f t . l l ' .ST-.

i'KO.IFCTf:: I 'CUJ-iF-.W

i~T..TKJVT ID: I)GH-3F-2<',y

j.) ATI! SAMPLED: 3 / ! 1 ••01

NrF.L SAMPLE 111: 1.020? 1 ! 6-001 0

'•'.irametcr•\.-ltl.M-

H: 'i/rru-

I'.rornohrn/erc

i-i'orr.ochlororriMhnne

HioinoiiichlflromiMh.inc

Bronofomi!'• : -."'.•-

J-Butanone

i.-F^lylben/cne

.,'.-L -Uulylhen^ene

icit-Burylbcnzcnc

C'irhon d'SuHidc•-, ' , . . , . > , ' , . . , ! ,

t..iiu)robenzcnc

H.loi. -ethane

.:-'. 'hlmc'.-'.l.yi v i n y l rllier

Chloroform

Chloro methane

?-rr,!rro'...:lu-v

— cltlnrnioluene

!.i:hromochloromcthanc

! ,2 l^ihromu-.S - th lurupropanc

1 ,2-Dibromoethane

Dihromo methane

1 7-nirhlon-.K-n--.-nr-

1 ,3-1 hchlornbenzrnc

1 ,4-Dichlorohenzene

I ' l -n l .m.d .Mu. i r . j iT ie ihane

1,1-Dichloroethane

1 ,2-Dichloroethane

1 .1 -Durhloroctbc-nc

v-::-l.2-D!cr. |or<)ethKne

trans-1 .2-Dichloroelhene

l .2-DiJi l . )n-pmpjr 'c

1 ,3-Dichloropropanc

2,2-Dichloropropane


cii-i,3-Dicnloropropen?


F'hvlhcn-/rni-

Hexachlorohutadiene

2-Hexanone

l lodomelhanc

!^piopvlr,ci,/ei,L

Hesult

Z'.'

r:nND

K'D

ND

ND

ND

ND

ND

ND

ND

ND

vnND

ND

ND

ND

ND

ND

NU

ND

N!)

ND

ND

Nf>

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NO

NDND

ND

NDNDND

Unit

w'l-•n-.'l.

1'll'f-I'C'L

I'!-/'L

Me/t,i;;'luo,'I^

Mfr'I-

Uj^/'I.

MK/Lug/L

i'".''.ug/'L

MS/LMJ-/L

MS/L-

(jg/L

MK'L

l»E'l-

Mg/L

Mf'L

Mg/LME/L

HP/I.

\i$j\.'

UK/L

M f r Lug/L

Mg/L

HK/L

jjg/'I,

ug/L

M&'Lup/L.

ug/L

"g/L

Mt'/L

Mg/L

•ie/I

ME/L

MS/L

Mg/L

H&L

ReportingLiuiii

:>5 0

50

50

5.0

50

< 0?s5.0

5.0

5.0

5.0C 0

5.0

5.0

5.0

5.0

5.0S O

5.0

5.0i 05.05.050

50

5.0

S t)

5.0

5.0

5.0•5.05.0

5.0

5,0

5.0

50

5.0

5.050

5.0

25

5.0

i o

DFi\i111!\

1

i

1

1

I

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

1

I

1

1

1

1

1

1

1

1

1

1

Method

:-\v---:v,(jH

swx;(.t>BSW$2t.GB

SW&760B

SWS260H

SVVX7.60U

SV.-«?f')P

SW8260B

SW82608

SVV8200H

SW8260D

SWS260B

swsroonSW826011

SW8?60R

SW87.60Q

SW8260B

SWS260B

SW8260R

SW82608

SW8260B

SW8260U

SW8260B

SW8260B

.SW8760R

SW8200H

SW8260B

SW8200B

SW8260B

SW8260B

SW8260B

SWS2(,OB

5>W8260B

SW8260B

SW8260B

SW8260B

SW82AOB

SWS^dOH

SW8260B

SW8260B

SW8260B

SWS260B

SW8260B

b'.VK2^0B

Prep Date Analyzed

r.viro203/11/0?

0.3.' !!'(!?

( U / l l / 0 2

03/1 1/0203/11/02

ni'!l'07

O.V 11/02

03/11/02

1)3/1 1/U2

03/11/02

03/11/02

m/i i 'o?03/1 1/02

03/11/02

03 /11 /02

03/1 1/02

03/1 1/02

03/11/0?

1)3/11/02

03/11/02

03/1 l ' 02

03/1 1/02

03/1 1/02

03/11/02

03/11/02

03/1 1/02

ft.TI I 'O?

03/1 1/02

03/1 1/02

03/11/02

03/11/02

03/11/02

03/11/02

03/1 1/02

03/11/02

03/1 1/02

OM1.02

03/11/02

t l i / l 1/02

03/1 1/02

03/1 1/02

03/11/02

'.;.i,' i I'D.'

Analyst

• )RM ! V

DRM-LV

DRM-LV

UKM-l-V

DRM-LV

DRM-LV

rm.M i vDRM-LV

DRM-LV

HKJ-.I-LV

DRM-LV

DRM-LV

DRM ! V

DRM-LV

DRM-l.V

DRM-I.V

DRM-LV

DRM-LV

DRM-l.V

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

HRM ! V

DRM-LV

DRM-LV

DRM-LV

IJKM-LV

DRM-LV

DRM-l.V

DRM-LV

DRM-LV

DRM-LV

DR,M-L\'

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

."iRAt 1 V


Ul- - Dilution t-aclor

Date: 13-Mar-Q2


S - Spike Recovery outside accepted recovery lunils

K - Value above quantitation range Page 4 of 5

. N i r L . L ' M S O R A I O H I i f i :

rnOJFfT ID: DGH-?F-?r.

M.\IK1\: / . V > : . » H H ; , >

Parameter

r t^-.-, ,>,il..wa^

i M f l h > l c n v cliloiiik-

-".-Mcthyl-2-pentanfne

M i n i :

N'jnmhHlcne

i.-Pr-ipylbei^rnr

. , .ci te

1.1,1,2- rctrachloroclhanc

i 1 ,? ?• i crr.K-hlarne(hane

Tcrrarrloroelhene

Toluene

} ,2."> Trichloruben/ene1 ! . , H V ".<.„..

1,1 ,1 -Tnchlorocthanc

1 1 2-rrict.lonx-thane

1 pchlnroethene

Tuchtorufluoronicihanc

1 .1 ,2-Trichlororrif!uorocthane

l J ' ' - t-hlon p i ' ip jnr

1 ,2,4- rnmelhylhenzem:

1 ,3.5-rrirrethylbenzene

Viny l acciatc

Vinyl chloride

'i-Xylene• , ,, V % ' . ,

Surr: DibromofluoromfthHnc

£urr: Toluene-d8

Surr: 4-Brumufluorobcnzene

3'

Result

M.'

1 1

NO

ND

ND

ND

N i J

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

NDND97.9

91 8

81 3

jjnit,ir j.M;;. 1.Mg'L

ui; 1

,'P-L

PiVL

MS: inS.iM g L

Mt','1-

W !

M;J/L,.,-T

ug/L

M6/L

ug/L

fg/L

|ig/L

M P ' L

MB/1-ng/1

JJ-^''i-

Mg/L

Mg/L

UP'!%REC%RFC%RFC

'{•'porliocf.iuiit

-^ u

-, •)25

i'G

5"

505 0S O

50

5.')

50

50

' 0

5.0

10

50

5.05.05 (1

5.0

5.050

5.0

5.0

!0

89-102

90-102

70-IOfi

DATKSAMPLFD:

NKI SAMPL.F ID-

DP Method

i ^ A s . ' r t - l

1 SW.S^.OU

1 SWh2( 00

1 S \W60H

i SWX2ci!)H

1 SW8260H_-,\\.-:(»IH

1 SW8760B

1 SWS260R

1 SW8760R

1 SW8260H

1 SW8260B

1 SV\'8?rOB

I SW8260B

! SW8260B

1 SW8260B

1 SW8260B

1 SW82COB

1 SWS7COB

1 SW8260B

1 SW8260B

1 iW»2t>OU

1 SW8260B

1 SW8260B

1 SW8260R

1 SW8260B

1 SW8260B

1 SW8260B

VI 1/02

1 ( • , ' ! > < ! 16-OlJ l f )

Prep Date Analyzed

u, . , _

03/1 1/02

cn/ii '0203/11/02

03/11/07

03/11/02

(, i . 1 .12

03/11/02

03/1 1/02

1)3/11/02

03/11/02

03/1 1/02

OJ/1 1/07

03/1 1/02

03/11/02

03/11/02

03/1 1/02

03/11/02

01/1 1'02

03/1 1/02

03/1 1/07

OJ/ 11/02

03/1 1/02

03/1 1/02

03/11/02

03/1 1/02

03/1 1/02

03/1 1/02

Analyst1 XX ' .

DRM-LV

DR.M-LV

DRM-LV

DRM-LV

DRM-LV

:)R.v vDRM-LV

DRM-l.V

DRM-LV

DRM-LVDRM-LV

PWM ! V

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LVDRM-1 V

DRM-LV

DRM-LV

DRM I.V

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

ND - Not Detected at Ihe Reporting Lirrut

DK - Dilution Factor

Date: 13-Mar-02




NEL Laboratories, Las Vegas

CLIENT: Dumpco'SilveiMdteWork Order: L0203116Project: DGH-3?--263'

ANALYTICAL QC SUMMARY RI^'OR Y

TehiCvJ:: 3 , I \Vrn

Sample ID MB-H884

Client ID ZZZZZ

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

S.vnpTypc' .MHLK

i M t c h I D : R R X 4

Kisu l t

ND

ND

ND

ND

T

P

00

0

0

:stC ide: 300 W Units- m^/L Prop Date - i t . \l> :,J.',-)Ji: 1 . l \

Tcs'Nn E3QO \r. iy::s Dd'.e 3'11 02 ^Si-qNo £'.".>

3L SPK /alue SP.-^ Re fVa l ".RFC _•)•* l i m i t HighLirr.t PJ'D'.^i 'd1 rd. • K;'0 -/ , - '

10

10

10

10

• J>CO

' 21

i O

X

'

Qualifiers: ND - Not Delected ai the Reporting Limit

J - Analyte detected hi low quanti ' lion h'.

S - Spike Re. overy iii 5idc accepted recover limits

•i • RPD out uie acct; ted recovery irmts

Anaiy l i c! U 1 . ' td : 'he 2ij(^.'»\'it l,;v . ij Oh1)'-

•"« / i

CLIENT Dumpco/.Silvei.-'.jteWork Older: L0203116Project: DGH-3F-263'

4 r.1 < I -AAAL

r/::ovv i)

Sample ID ,MB-R6i9

Client ID ZZZZX

Analyle

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

,p!ype. MULK

,'d. ID R_K659

R e s u l t

TestCeJL 601CSN_D t nils- wy/l.

TestNa: S\\

PQL SPK .3luc SPK At.f Val

! rep Dale

, ' ra l . i '« i - Date 3'12/"I

•7-,'ALC Lr^1. Tfiit I ipl iLirr . :

ND

ND

ND

ND

ND

ND

ND

0.0050

0.50

0.10

0.50

2.0

0.50

0.0050

-,rn

i'O!

-Aj

rncc

QualiFieri ND - Not Delected a' 'he Reporting Limit

J - Analyle .IcttcteiJ I-.-low quantit . lion l i nn

- Spike Ref overy r u ide accepted recover limits

• RPD ou'.sij<. acc,[ '-'d recovery innts

B Ar.i'ytc Jrscclt'1 m (hi a;?.1::.!!, i' M.

CLIENT: Dumpco/S.KerstafeWork Order: 1.0203116J'roject: DGH-3F-263'

Sample ID. MB-3S1 Sar.i;- Type. MBLK

Client ID: ZZZZZ B;,' h ID. R_35:

•\nalyle Rcsi.it

Barium NO

Calcium ND

Iron NJ

Magnesium ND

Potassium NO

Sodium NO

Vanadium NO

TestCode 6010W_t Unls irj'L

TestNo SW6010B

PQL S P K v j u e SPK Kef Val

0.0050

0.50

O.IO

0.50

2.0

0.50

J.0050

AN \LYT1CAL QC SI? MM ARY KEP- )RT

'IcstO.,,!?: 601t3%,V t |^

i -p D.I-.J- .312-01 i-'.'ir : >. ^..'.'.-,oD ; 1

An2 v is Dau: ^ '11/01 » " i N - > ^ ',! ' CD

; °%P.H> Lo\ v l u.til ^ I l ^ h c i i r i t K ^ ' n / ' , ,'r.l "i : \ l ' !> •'!', '!.i".' " Ci '•! ! -^

H0

mCO

li

i

lI

i

iiiii

i

Qualifiers: ND -Not Delated at the Reporting imit

J - Analyte directed bi )'iw quantitsti m lim

Spike Rcco' cry ou'.;"!e accepted fcovcry ii

RPD outFiC.- jcccp .-ii rcco-.'ery li.-'its

\ i i a ly t> : d ^ t v i i c d in I'v. -i-.sf.ijlj'j I

CLIENT: Jumpco/SiKerstale

Work Order: L0203116Project: X5H-3F-2631

Sample ID MB-R661 SarnpF^pc

ClienUD: /.ZZZZ i J . ' i n ' D -

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

CobaltCopper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

MHI K

K_R66I

Result

ND

NDND

NDNDNDNDNDNDNDNDNDND

TcslCfidr SOiO'A _D Units m f , < l

TestNi* S\V5li:o

PQL SPK -u.ue SPK Ril Val

00010

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

00010

0.0010

0 00040

0 00)0

ANALYTICAL QC StMMAUY RE.'JRT ;

Test Co U': oO/ ,M-\ .D j^fj... „. r~

•• p Da'c ' r , i N ; •:- ,(,: , ]

JoI1S.IH L'v- 1 tmit Hs jh l i i r . i l RI'O ?..•'', ji ' !<! ' '> ' i 'Dl,. (,'- ' '] -^

i — 1

J O

m'COi

(

jiii1

Qualifiers: V «D - Not Detected at tl e Reporting Limit

' Analyle (jcfctcd (euu qua'itiwai limits

S Spike Recovery ouUhie accepted • covery I

•i RPD o'JtuV acccp'- i iecuvt'O' iu-i ib

CLIENT: 1 iumpco/Sil . muteWork Order: i 02031 16Project: r-OH-SFôJ1

Sample ID: MB-350 Samp ; ype: MBLK

ClienUD: /ZZZZ Oauh ID R 350

Analyte R:su1'

Antimony ND

Arsenic NC

lltryllium N'D

Cadmium ND

Chromium ND

Cobalt ND

Copper Ni1

Lead NP

Nickel ND

Selenium NT)

Silver ND

1 hallium ND

Zinc ND

res'.Code 6020V\_r Ui.i ' i m;/L

PestNo S\\69:<>

i'QL S P K v a i e SPK Re, Val

O O O I O

O O O I O

O O O I O

0.0010

U0010

O O O I O

O O O I O0.0010

O O O I O

O O O I OO O O I O

O O O I OO O O I O

ANALYTICAL QC SUMÂRA MEI'.JRT

•iîrod.: h O - L VJ] Zjr—

/,.,, >„.- 3/j:,o2 ;<. , , :r. s: '.-".:. , r-V.-.: :i, Or.'. 3 / i iOZ ^ . • • N : <••:: ^

C%PJ£C L&> Liri i t ' i j'-.lj'rii! ,<l > - ' t-f '-j! ' t- !'T) .-'. l\ in yuj i ID

V

QDm•JO

Qualifiers: ND - No! DciCvted at thi Reporting L nut

I Ann!}'.;: rtjItUed txluw quantilaliuri

S - .Spike RcLOv.rv cu'i ' • scceptcd Tco-'er, I'mts

.-< VDo'jlitdi. jwccvt • rftovcr)' Irnii1^

3 Twilvl--c:.".'C'i'd ,r, ."c .•,', i . i Vn.'.!) iJ ^'lail

CLIENT: Uompco/SiUerstatcWork Order: I<i203116Project: DGH-3F-26/

SomplelD: MB-R893 .iarnpl-'pe:

CI.cntlD. ZZZZZ Bale', ID

Aialyte

Acetone

Ocnzcne

'.itomobcnzcnc

Diomochloro methane

Bromodichloromelhane

rtromoform3romome1hane

2-9ulanone

n-8ury]benzenc

sc-c-Butylbenzene

vu-Butylbenzcnc

Carbon disulfide

Carbon letrachloride

Chlorobenzene

Cnlorocthanc

?-Chloroethyl vinyl ethci

Chloroform

Chloromcthanc

2 Chlorotoluene

<t Chlorotoluene

Dibromochloromethant

'. 2-Dibromo-3-chloropii'pane

i 2-Dibromoeihane

Dibromomethane

1 2-Dichlorobenzcne

1 3-Dichlorobcnzcne

1 4-Dichlorobenzene

Dichlorodifluoromelhanc

1 1 -Dichloroeihane

! 2-Dichloroe\hane

1 l-Dichloroelhene

MBLK

R893

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

TcstCoJe. 1260_W Unib- jig/L

TesiNo SW8I60U

PQL ^PK value SPK Ref Val

25

5.0

5.0

5.0

5.0

5.0

5.0

25

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

ANALYTICAL QC SCMMA RY rJIPC :>T '

7e.,r<nK -60 W i : i

Prep Date: .\J.1 ,'"> l._ • ' • • < '(JS-:?_/. S I I H j , i' f>

\n'-iy; i ^ D:t: 3;:t-02 Scr'^o C O i r ! |; .jjI -^

%KTC towLim,. H';h;.;,™ '.?nici",V ' rPP •--:.„.! C ..i ' , X

Hg

IT.•

1

,

,;

r1

Qualifiers: ND - Not Dctrt'i'd at tin Reporting I imit

J Analyte riett 'ed bc'.n v qusntitation limits

S "-pike Recovery oiiwiJ.- accepted recovery li9. • -<?D outsicli' ...xcptcii recovery lirniLs

• A lalvu flc'.^ciic r. t'l.-1 j » r o v ) 3 ' • i Mt t luo '.dunk

CLFENT: Dtimpco/Silvsrstate

Work Order: L<.'2031]6Troject: DGH-3F-263'

Sample ID: MH-R893 Sam?1>,-c

Client ID: ZZZZZ Baler, n

Analyte

cis-1, 2-Dichluroi'thcnc

trans-l ,2-Dichloroelhcne

1,2-Dichloropropane

1,3-Dichloropropane

2,2-Dichloropropane

1,1 Dichloropropcne

cis-l,3-Dichlompropcn:

trans-l ,3-Dichtnmpropenc

Elhylbenzene

Hexachlorobutadiene

2-Hexanone

lodomcthanc

Isopropylbenzene

p-lsopropyltoluene

Mcihylenc chloride


MTBE

Naphihalcnc

n-Propylbenzene

Styrcnc

1,1,1 ,2-Tetrachloroelhane

1 , 1 ,2,2-Tctrachlorocthanr

Tetrachloroethcne

Toluene

1,2,3-Trichlorobenzcne

1,2,4-Trichloro benzene

1,1,1-Trichloroethane

1, 1 ,2-Trichloroethane

Tnchlorocthenc

Trichlorofluoromelhanc

l,l,2-Trichlorotnfluoro(.''hane

MBLK

K893

RcciiU

ND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDND

NDND

NDNDNDNDNDNDND

ND

ND

TcstCod;. !)260_W Units ag/L

TesiNo: SW8260B

POT O U I/ \ f« It t i CPV '7 ff \l i lrv^i- . j r lvVaiUO jrtS. ivEI X ' j j

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

5.0

25

5.0

5.05.0

5.0255.010

5.05.0

505.05.05.05.05.05.05.05.05.05.0

ANALYTICAL QC SYM MA K Y rvEPGHT ,' '"7

rest-Code: 5:2hO_V> -^

I'rcp )atc: R u n . : ) L_V().>\;Si-J_l!::.T: 1 i( " '

A-.a!;'Si» Dale- J.".l,()2 Scqs. •> f.'i48 • 'fn

i--

~3

:fjT!i/J

ii;i

I

Qualifiers: ND - Not Dctecl'-d at the <uponing Limit

J • \nalyte deleted belr>\ t|uan[itation li

v'pi^c H c i O i c r v outside ociep'.ed rt-cmcry 1-jniu

- kPD o''"iid; "i i cptjd K ;overy limits


Dumpco/Sih asiateL02')3H6DGH-3F-263'

ANALYTICAL QC SUM>?,vR\ :'.1:POV.T

Sample ID: MB-R893

Client ID: ZZZZZ

Analyte

1,2,3-Tnchloropropanc

1,2,4-Trimcthylbcnzcnc

1 ,3,5-Tnmethytbcnzcnt

Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Surr. Dibromofluorometl.ane

Surr: Tolucne-d8

Surr 4-Bromofluorobsn?enc

:"3mpT>i - MBLK

Hatch 1!' R893

Result

NDNDNDNDNDNDND

49.28

45.64

38.42

icstCcide

IcstNo

I'QL

505.05.050

5 0

5.0

10

50

5.0

50

8260_W Ur.its. jig/L Prep Hate Xi;n :„ < _ \ i

SW8260B AnJ>^. . Hal- .Til 02 H'- t.O^A

SPK value S P K S c f V j l ",oR£C Lov.Lif.-i Hf^ .Lu t i i l R. ' l i Pcf \3'. : "',) -

50 0 986 3; 102 t. )

50 0 91 3 9'.i !02 ')

50 0 76.8 70 106 I, n

Qualifiers: ND - Not Delected ai the Reporting Limit

J - Analylc detected below viantitation linnls

S • SpKe Recover) outside accepted recovery l imits

R • RJ 1) outside L i '-p't-J r. ivcry limits

B - Am.ytc t^^vi.J i 'ht ,r '>t ; , t ! ' J ' ' . i hod lj'.i.

*' s'' *

CLIENT: Dumpio/SiiverstateWork Order: L0203I16Project: DGH-T-2631

ANALYTICAL QC SUMMAR\ R/' :OR

Tt-stC- k: M,K \V —i

Sample ID MB-R898

Client ID ZZZZZ

Analyte

Alkalinity, Bicarbonate (As C.CO3)

Alkalmi'y, Carbonate (As CaCO3)

Hydrox-de (As CaC03)

Alkal.mty, Total (As CaC03)

ân-pljpj MBLK Tc-it uiic \LK_W Uni's' mg/L Pfp Date '"'in If1 ' _ A l i . • 'IOV '

P./chlD ;<S98 ToiNo î:3208 % . lysis D v VSL02 i i,No r<-

Result ?Q1 -;?KNjlue "''K RefVal /-.libC LTV,!, rnit H.ghL i ! O'D i S a l "' R1 -v "

ND :^

ND 25

ND 2--

ND

Qualifiers: ND - No' Octet.ted at the Ropormg Limit

I • AnaK c dcUcH'd below qujrt i tat ion lim Is

S • SpiV êcovery ojlSKJea:c'-j-'cd reci< <~r 1 mils

K •IPu ts de 3c^,"e^ rs r > limits

Bu-

CLIENT: Dumpc. /SilvcrstateWork Order: L0203I16

Project: UGH-?r-263'

ANALYTICAL QC SUMMAVA RU OUT

Tcstf'o:;e: COD

Sample 1!) MB-R900

Client ID ZZZZZ

Analyle

Samp Type: MBLK

Bali h ID X900

Xcsult

TesK'oiie: COB

•H'-'.No: M5220 C

PQL SPK vf lue

Units: mg/L Pre-p 0:;?

A-.3V-SD.-:

3PK.RcfV.3l "IR£C -o'vl.i;nil :i.^

j ' .n ,D ;V.i-Ql '•'.-•-•N •. '•

iLiT, ' Ki'l'i '-'?: \ j! '.R?,

Chemical Onyjcn Dtr.-.aid

Qualifiers: ND -Not Selected al tt.c Report ng Limit

J - Analju iktcctcd be ow quari ' iiation limit.1'

S SoiVc K -cover/ oii '^i lc accept.-d recnvcr, l.mils

-i <PU uL-ide 3.:epte,: iccovt.! > limits

3 • -\na1yt. (ioicc;:1! r. 'Vic a-r." .ill ii \".' ' \' 9)jt >. I


Sample ID: MB-359

Client ID: ZZZZZ

Analyte

Dumpco .SilverslatcL0203116DGH-3F-263'

Si inplype- MliLK Tc.nCf ie: HG_74-20_T Units: niî.

O u k h l D : R_:.59 TcitNo. SW7470

3 o MI It PQL SPK value SPK Ret'Vjl

ANALYTICAL

"« .1",

P.epDsti: 3/1 3/02

Aiu!j,i.-,nat." .Vi;,02

'•-.!»cC Low Lirr.il I'-:'nL!rr,i; X

QC SUM

Codk: KG

k

'!- -<','f'.'-ji

MARY

,.7-;70_T

•j i )lj SL.1^

,",\. «0 U H - 1 '

-:;,:<PD

REi'ORT ,i .j /î «;~im

i! *~j!g

? i - n i . - • CM,, i i ^ D_;! >^

Mercury 0 00020

oo

Qualifiers: ND • Nol Dt'ected at the Rcportinp Limit

J • Analyte Ojtccted below quanti tot ion limits

S - Spike Ruin-cry oil-side accept1.! recovery Itrruis

R • K H D ouîcc accepted 'n.n-cr) i mils

B - Anaiyt': J . icc tcd i t t 'he ,iss. f.- . i1 ' .'. A'CI!'^' ' ".'.•jn'r

CLIENT:\VorkOrder:Project:

Sample ID MB-RSC

Client ID ZZZZZ

Analyte

Dumpco'3 IverslateL0203116DGH-3F-763'

1 Sun"pT>p<: MB! K Ics'Coa. \H3-N_W ' - , ( « , f-g/L

^ a ' c h i l ) R901 T -\" ^'I4"3G \V\ C

R"tjlt 'QL SPK . t'-je CIV J-f \ 'a l

AKAL\TICAL

'r< p Dote

V •> s % DJ'C Vl l /02

or s« ^ f * " \R>- '^FI.Cotlo NL'l 'MS

';> H- i M' ) i i

Ammonia, o"- N 030

Zm

1 OJ)

O5moo

Qualifiers ND • Not DcUcied at the Rcportmf ' imit

J • Analyte c.'ected bslo* juantital in limits

S - Spike R=u) cry ouNitk ^ctcpted r-coverj limits

R - RPD auU di' aLCCplcii rec i cry linuls

D - /

CLIENT: Dumpco/Sthei stateWork Order: L0203116Project: DGK-3F-7631

Sample ID MB-R879 SampT ype MBLK

Client ID: /.ZZZZ Batch 1 3 R879

Analyte P-csull

ANALV

TcstCo.i.' 3ULFJW I'.MIS ,i.g/L >>rcn '.j-i'.c

TcslN'u MJ500-S a A-Mly;-; DJ'C

!'QL SPK. value SPK. Ref Val ",tvt-X L<. ^Lim i -

riCAL QC SUMMARY UK;

T"-'Codc: SUi.rjtV

'/no: ^ '• <i')''.j

•"-t in it 'UR'. ' .W 1 J ! D ' l i l n .

^O^T

Sulfidc ND 0030

Zm

ccOID

OwU

rn00

Qualifiers: ND • Not DMrclcd at the Reporting Limit

J - Analyte detected below .juanlitauon limits

S - Sp kc Recovery ouliide accepted recovery limits

R - RI D outside- jtceplt-'d rfoscry Iirniis

8 - A'l.iKie dc:t, 'cc! in tnc S'.MIC • ' M?;!,o>, 'J .ink,

.;' : •.• ! <• f 14


Dumpco/SilveistateL0203116DGH-3F-2631

ANALYTICAL QC S f M . M , V U \

'i: .-.Cut!?: H)S 'V

Sample ID

Client ID:

MB-R907

ZZZZZ

Sa-npTypc.

Bit.;. i f >

MBI K

R307

Resell

Tts tCoi-

Tcsu-'c

POL

TDSJW 'J",,tv n-:,!.

E 160.1

?P(C \ -'uc SP'< K - f Val

;-pI^e '-., ,V !._,.

Ana ' -^ ' sOo ie .Vll-02 s -, '-i 6:-:°.

'-( ' . . , ' - 1 1 H . - " - ir-it ""~)X-- ' i '•!'[)"

Total Dissolved Solids ND '.50

•m

O

HOXfTI

Qualifiers: ND - Not Due..ltd at ih: Kcponing I imit

J - Analyte deleted below qi iant i la tun hnnLs

S - S( ike Reco\er> oubide sctcpied fcoi'crj' l

R - Rl O outsins dtv.epud recovery In iti

13 -.'.rialy'i. o^ ' . ' n-J ir, '''.' J ^ • . c ^ . ^ ; • • '

1L>JU'V L A B O R A T O R I E S

Vanessa iV.diila:-'} ;f. I ;i'o( .r;»l. >;,-: } =- V4208 Aieali "Way, Ste Af /H Vtv;;--:. My ^

Certificate of Anals is

IISK Sut, minion fe: 2«K>2030578

ONK Pji.np'c m #!

Sampk'fyTf."v«np!c De^y.Sample rVirnnicTjls-

Oil>on

Date Sampled: 03/11/2002Tune Sampled.Date RecovcA- 03/12/2002

Mrfbod Hrndt Units5 1 ine'F,

J-?L_0?

Dilution DLRPrep AratyiUDate Date

OV1V7002 OVIV7007.

H: Analyzed outside of hold toneP. Preliminary resultS: Suspect result. See Cover Letter for comments.£: Analysis performed by External laboratory.

Sec External Laboratory Report attachments.

.-•bwowfr- \nm\UmHtmuntHmimmimmn Page 2 of 2

14J4 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935

mg/L: Mfflignims/Liter (ppm)mg/Kg: MJKgrams/KJlogrsan (ppm)

: Micrograras/Liter (ppb)g' MicTogrsms.'Kflograiri (ppb)

%Rec: Percent Recovered (surrogates)

PQL: Practical Qmntitation LimitDLR: Detection Limit for Reporting

•PQLxWutionND- None Detected at DLR

::EL LABOR-TORIES CHAIN OF C'JSTQG/ ? -L t'y

^'- 8 0 * o >/ jgss * Boise

rho NX » 5ac amento

las VegdS DIVISO i •-5203 Area a ". i " _ ' i . A - as </tgas Nevada 33030/02-6E-1 1010 • Per 7C" "~ 57- • a^ 253 3282

ocT?«n, / / L'-•£ tieie.

f-roio

I i

Rcquectod

Time/DateS-jmpled

-x? -jdrLjoCiia*^V. / l/i

7,f2 day 1 day _

Custom"1

Custody Seal mtact Y<

P ojs Nan e Sjr

P.

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i

rt« ft' OA CinVnjiVaie jl jjd

AVv .asiftWataf AC Aqjeov.5D_ ClOgancûi ! ^ ~<

(Print) Signjrfijre)

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Date/Tme J W (P' nt) D j " fie

i

ab / fyc^rS/EL La ra(o/'(«s (nc »s / r-/( dj H ' y (a*h 1 - côf^Bmo" fltysis *or th" jsa-pi3l& ecpfved i goo^ rood 1 c-^ jy NEL Nh. isrciro^y-'1 sbe*o 'o=» c T\^q^caoqua'es? npevoiirT>eanGnvn-tr Mconure's Oustan"1 gnalu'octîi CoCco Muies apu ^.ssecrde Si -VEL to peâm w t fo rons jn i ^ pi

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ORIGir-'Al

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702-657-1010 • Fax: 702-657-15771-888-368-3282


TEL: (702)431-3020

RE Project: DGH-3F-263'

Dear Ed Carlton:

RECEIVED ,

Order No.: L0203116




$an Van Wagenen £H_ ,Laboratory Manager '


WV


Certified

Date

NEL LABORATORIES^


PROJECT ID: DGH-3F-263'

PROJECT*: DGH-3F-2631

MATRIX: AQUEOUS

Parameter

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

2.2

1400

220690110

1100

0.29

0.0016

0.23

0.0079

0.0018

0.15

0.070

0.19

0.080

0.38

NDNDND0.75

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

002525

050251025

0025OOOIOOOOIOO O O I OOOOIOOOOIOO O O I OO O O I OOOOIOO O O I OO O O I OOOOIO0 00040O O O I O

0 00020

CLIENT ID:

DATE SAMPLED

NEL SAMPLE ID:

DF

555555511111111111111

Method

SW6010B-To

SW6010B-TO

SW6010B-To

SW 6010B-To

SW6010B-To

SW6010B-To

SW6010B-To

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 7470-Tota

DGH-3F-263'

: 3/11/02

: L0203116-001A

Prep Date

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyzed

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyst

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

FIF-Reno



Date: 13-Mar-02

B - Analyte detected m the associated Method Blank



NEL LABORATORIES•*


PROJECT ID: DGH-3F-2631

PROJECT #: DGH-3F-2631

MATRIX: AQUEOUS

Parameter

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.029

570

ND18050

980

ND0.0019

0.0018

NDNDND

0.0013

0.0043

ND0.0022

0.0078

NDND

0.046

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0005025

0102 5

10

25

00050OOOIOO O O I OO O O I OO O O I OOOOIOOOOIOO O O I OOOOIOOOOIOOOOIOOOOIO0 00040OOOIO

0 00020

CLIENT ID: DGH-3F-2631 ^


NEL SAMPLE ID: L0203116-001B

DF

l51

5

55111111111111111

Method Prep Date

SW6010B-D1

SW 60108-Di

SW6010B-Di

SW 6010B-Di

SW6010B-Di

SW 6010B-Di

SW 60108-Di

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW7470-Diss 03/13/02

Analyzed

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/12/02

03/13/02

Analyst

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

JTY-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

FIF-Reno

ND - Not Detecied at the Reporting Limit


Date: 13-Mar-02




NEL LABORATORIES

CLIENT:

PROJECT ID:

PROJECT*:

MATRIX:

Dumpco/Silverstate

DGH-3F-263'

DGH-3F-2631

AQUEOUS




ReportingParameter Result Unit Limit DF Method

Chloride 1200 mg/L 50 500 EPA 300 0

Nitrate, as N ND mg/L 25 25 EPA 3000

Nitrite, asN ND mg/L 25 25 EPA 3000

Sulfate 2900 mg/L 50 500 EPA 3000

Alkalinity, Bicarbonate (As CaCO3) 640 mg/L 250 10 SM2320B

Alkalinity, Carbonate (As CaC03) ND mg/L 250 10 SM2320B

Hydroxide (As CaCO3) ND mg/L 250 10 SM2320 B

Alkalinity, Total (As CaCOS) 640 mg/L 250 10 SM2320 B

Chemical Oxygen Demand 61 mg/L 10 1 SM5520 D

Ammonia, as N ND mg/L 030 1 SM4500-NH3

Sulfide ND mg/L 0 030 1 SM4500-S D

Total Dissolved Solids 5610 mg/L 600 4 SM2540 C

Prep Date Analyzed

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/12/02

03/12/02

03/12/02

03/11/02



Date: 13-Mar-02




NEL LABORATORIES«.




MATRIX: AQUEOUS

ParameterAcetone

Benzene

Bromobenzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

Chlorobenzene

Chloroethane

2-CWoroethyl vinyl ether

Chloroform

Chlnrnmethane

2-Chlorotoluene

4-Chlorotoluene

Dibromocbloromethane


1 ,2-Dibromoethane

Dibromomethane

1 ,2-Di chlorobenzene




1 , 1 -Dichloroethane

1 ,2-Dichloroethane

1 ,1 -Dichloroethene





2,2-Dichloropropane




Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene



Date: 13-Mar-02

Result Unit

29 fig/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ReportingLimit

2550505050505025505050505050505050505050505050505050505050505050505050505050505050255050

B - Analyte detected

CLIENT ID: DGH-3F-2631


NEL SAMPLE ID: L0203116-001D

DF Method Prep Date Analyzed

lllllllllllll1llllllllllllllllllllllllllllll

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/1 1/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02--

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

in the associated Method Blank



NEL LABORATORIES4




MATRIX: AQUEOUS

Parameterp-Isopropyltoluene

Methylene chloride


MTBENaphthalenen-Propylbenzene

Styrene1 ,1 ,1 ,2-Tetrachloroethane


Tetrachloroethene

Toluene1 ,2,3-Tnchlorobenzene


1 ,1 ,1-Tnchloroethane


TnchloroetheneTnchlorofluorome thane

1 1 2-Tnchlorotnfluoroethane

1,2,3-Tnchloropropane1 ,2,4-Tnmethylbenzene

1 ,3 ,5-Tnmethylbenzene

Vinyl acetateVinyl chloride

o-Xylene

m,p-XyleneSurr: Dibromofluoromethane

Surr: Toluene-d8


ResultND

17

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND97.9

91.8

81.3

Unit

Mg/Lug/L

Hg/L

ug/L

Mg/LMg/LUg/L

Mg/Lug/Lug/Lug/Lug/Lug/L

ug/Lug/Lug/L

Mg/Lug/L

Mg/Lug/LMg/Lug/L

Mg/LMg/LMg/L%REC%REC%KEC

ReportingLimit

50502550505050505050505050505050505050505050505010

89-102

90-102

70-106



NEL SAMPLE ID: L0203116-001D

DF Method

1 SW8260B

1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B1 SW8260B1 SW8260B

1 SW8260B1 SW8260B

1 SW8260B

Prep Date Analyzed

03/11/0203/11/02

03/11/02

03/11/0203/11/02

03/11/0203/11/02

03/11/02

03/11/0203/11/02

03/11/02

03/11/0203/11/02

03/11/02

03/11/02

03/11/02

03/11/02

03/11/0203/11/02

03/11/0203/11/0203/11/02

03/11/0203/11/02

03/11/02

03/11/0203/11/02

03/11/02

AnalystDRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LVDRM-LVDRM-LV

DRM-LVDRM-LV

DRM-LV

DRM-LVDRM-LV

DRM-LV



Date: 13-Mar~02




NEL Laboratories, Las Vegas Date: 13-hfar-02


Dumpco/SilverstateL0203116DGH-3F-263'


TestCode: 300 W

Sample ID MB-R884

Client ID ZZZZZ

Analyte

Chloride

Nitrate, as N

Nitrite, as NSulfate

SampType MBLK

Batch ID R884

Result

NDNDNDND

TestCode 300_W Units mgO.

TestNo E300


0 100 100 100 10

Prep Date Run ID LJC-1_02031 1A


%REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

1



S - Spike Recovery outs de accepted recovery limits


~TB - Analyte detected in the associated Method Blank

Page J of 14

— t -



ANALYTICAL QC SUMMARY REPORTi

TestCode: 6010W D

Sample ID MB-R659

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R_R659

Result

TestCode 6010W_D Units mg'L

TestNo SW6010B


Prep Date



Run ID SUB-659

SeqNo 6434

%RPD RPDLimit Qual

m

COO3D

§gomCO

Barium

Calcium

Iron

Magnesium

Potassium

SodiumVanadium

NDND

NDNDNDNDND

00050

0500 100502 0

05000050




R - RPD outside accepts d recovery limits

B - Analyte detected in the associate^ Method Blank

Page 2 of 14

CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGH-3F-263'

Sample ID: MB-351 SampType:

Client ID: ZZZZZ Batch ID:

Analyte

Barium

Calcium

Iron

Magnesium

PotassiumSodium

Vanadium

MBLK

R_351

Result

NDNDNDNDNDNDND

*


TestCode: 6010WJ

TestCode: 6010W_t Units: mg'L Prep Date: 3/12/02 Run ID: SUB-6^0

TestNo: SW6010B Analysis Date: 3/12/02 SeqNo: 6438 '1


0.0050

0.500.100.50

2.00.50

0.0050

T]

\BO

RA

TOR

mCO



S - Spike Recovery outsi de accepted recovery limits



! Page 3 of 14

11CLIENT: Dumpco/SilverstateWork Order: L0203116Project: DGII-3F-263'



Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

CopperLead

Nickel

Selenium

Sliver

ThalliumZinc

MBLK

R_R661

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

NDNDNDND


TestCode: 6020W_D

TestCode 6020WJO Units mg/L Prep Date Run ID SUB-661


PQL SPK value SPK Ref Val %REC LowLirmt HighLimit RPD Ref Val %RPD RPDLimit Qual

O O O I O '

O O O I O

O O O I O

O O O I O j

O O O I O

OOOIO 1

O O O I O '

O O O I O

O O O I O 1

O O O I O

O O O I O

0 00040

O O O I O

JJ

—00oID

o2mCO






1 Page 4 of 14

i ^


Sample ID: MB-350 SampType.


Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Nickel

Selenium

Silver

Thallium

Zinc

MBLK

R_350

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ANALYTICAL QC SUMMARY JREPORT

TestCode: 6020WJT

TestCode: 6020W_T Units' mg/L Prep Date: 3/12/02 Run ID: SUB-6J56

TestNo: SW6020 Analysis Date: 3/12/02 SeqNo: 6424 i


0.0010 1

O O O I O

0.0010

0.0010

0.0010

0.0010 ,

0.0010

0.0010

0.0010

0.0010

0.0010

0.0010

0.0010

'

mr~r~\B

OR

ATC

IDmCO






Page 5 of 14

i

CLIENT: Dumpco/Silveistate

Work Order: L0203116Project: DGH-3F-263'



Analyte

Acetone

Benzene

Bromobenzene

BromochlofomethaneBromodichloromethane

Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

Chlorobenzene

Chloroethane


Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene

Dibromochlorome thane


1 ,2-Dibromoethane

Dibromome thane



1 ,4-DichlorobenzeneDichlorodifluoromethane

1,1-Dichloroethane

1 ,2-Dichloroethane

1,1-Dichloroethene

MBLK

R893

Result

NDNDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDND

NDND

NDNDNDNDNDNDND

ANALYTICAL QC SUMMARY (REPORT

TestCode: 8260_W

TestCode 8260_W Units (ig/L Prep Date Run ID L_VOAMS-2_0203 11 B



25 i5050505050502550

5050 ,505050 ,5050505050

505050

505050505050

505050

—7^JEL LABORATOR

mCO




R - RPD outside accepte i recovery limits


Page 6 of 14




Analyte

cis-l,2-Dichloroethenetrans-1 ,2 -Dichloroethene1 ,2-DichIoropropane1 ,3-Dichloropropane2,2-Dichloropropane1 , 1 -Dichloropropenecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzeneHexachlorobutadiene2-Hexanonelodome thaneIsopropylbenzenep-Isopropyltoluene

Methylene chloride4-Methyl-2-pentanoneMTBENaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane

1,1 ,2,2-TetrachloroethaneTetrachloroe thene

Toluene


1 ,2,4-Tnchlorobenzene1,1,1 -Tnchloroethane1 ,1 ,2-TnchloroethaneTnchloroe theneTnchlorofluoromethane1 ,1 ,2-Tnchlorotrifluoroethane

MBLK

R893

Result

NDNDNDND

NDNDNDNDND

NDNDNDNDND

NDNDNDNDNDNDNDND

NDND

ND

NDNDNDNDNDND

1 *


TestCode 8260_W Units ug/L Prep Date Run ID L_VOAMS-2_020311B


PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD R|PDLimit Qual

50 '505050

50505050505025505050

50255010

505050

505050

50505050505050

— f^JEL LABORATOR

mCO


J - Analyle detected below quantitation limits


R - RPD outside accepts d recovery limits


Page 7 of 14


Dumpco/Silverstate

L0203116

DGH-3F-263'


TestCode: 8260 W

Sample ID MB-R893

Client ID ZZZZZ

Analyte


1 ,2,4-Tnmethy Ibenzene


Vinyl acetate

Vinyl chloride

o-Xylene

m,p-XyleneSurr Dibromofluoromethane

Surr Toluene-d8


SampType MBLK

Batch ID R893

Result

ND

NDNDNDNDNDND

492845643842

TestCode

TestNo

PQL

50

505050505010

505050

8260_W Units ug/L

SW8260B


50 0

50 050 0

Prep Date



98 6 89 102 0

91 3 90 102 0768 70 106 0

Run ID L_VOAMS-2_020311B

SeqNo 6048

%RPD RPDLimit Qual

000

—00OIDH33mCO

m

Qualifiers: ND - Not Detected at the Repotting Limit

J - Analyie detected below quantitation limits




Page 8 of 14




TestCode: ALK W m

00OID>

O

mCO

Sample ID MB-R898

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R898

Result

TestCode ALK_W

TestNo M2320 B

Units mg/L


Prep Date



Run ID L_ATITR-1_020311A

SeqNo 6076

%RPD RPDLimit Qual





NDNDNDND

25252525






Page 9 of 14

«

CLIENT: Dumpco/S.lverstate ANALYTICAL QC SUMMARY REPORTWork Order: L0203116 ^Project: DGII-3F-263' TestCode: COD

Sample ID MB-R900 SampType MBLK TestCode COD Units mg/L Prep Date Run ID L_SPEC-2_020312C

Client ID ZZZZZ Batch ID R900 TestNo M5220 C Analysis Date 3/12/02 SeqNo 6090

Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual


, * NEL LABORATORIES


J - AnaJyle delected below quantitation limits




Page 10 of 14

1


Sample ID MB-359 Samp Type MBLK

Client ID ZZZZZ Batch ID R_359

Analyte Result

Mercury ND

ANALYTICAL QC SUMMARY REPORTTestCode: HG_7470_T

TestCode HG_7470_T Units mg/L Prep Date 3/13/02 Run ID SUB-669



0 00020

NEL LABORATORIES


Page 11 of 14



S Spike Recovery outside accepted recovery limits


*




Ghent ID ZZZZZ Batch ID R901

Analyte Result

ANALYTICAL QC

TestCode

SUMMARY REPORT

: NH3-N_W

TestCode NH3-N_W Units mg/L Prep Date Run ID L_WC_020312B

TestNo M4500-NH3 C Analysis Date 3/12/02 SeqNo 6099

PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLmiit Qua!

Ammonia, as N ND 030


J - Analyte delected below quantitation limits


R - RPD outside acceptc d recovery limits


Page 12 of 14

1 *




Analyte Result

Sulfide ND


TestCode: SULF_W

TestCode SULF_W Units mg'L Prep Date Run ID L_SP$C-2_020312A

TestNo M4500-SD Analysis Date 3/12/02 SeqNo 5960 '


0030

,. y

NEL LABORATORIES





B - Anatyte detected in the associated Method Blank

Page 1 3 o f l 4

1




Analyte Result

Total Dissolved Solids ND


TestCode: TDSJW

TestCode TDS_W Units mg/L Prep Date Run ID L_WC_020311D

TestNo E1601 Analysis Date 3/11/02 SeqNo 6140


150

c

v NEL LABORATORIES






Page 14 of 14

03/15/2002 FRI 9:46 FAX 559 485 6935 BSK LABS ©002/002


Vanessa PadillaNEL Laboratories Las Vegas4208 Arcata Way, Ste ALas Vegas, NV 89030

BSK Submission #: 2002030578BSK Sample ID& 189784PiojectID: L0203116





Sample Type: Liquid Date Sampled: 03/11/2002Sample Description: DGH-3F-263 Tune Sampled:Sample Comments: Date Received: 03/12/2002

Inorganics

AnalyteDissolved Organic Carbon (DOC)

Prep AnalysisMethod Result Units PQL Dilution DLR Date DateSM5310-D 5.3 mg/L 0.2 5 1.0 03/13/2002 03/13/2002

mg/L: Milligrams/Liter (ppm)mg/Kg: Milligrams/Kilogram (ppm)Ug/L: Micrograms/Liter (ppb)ug/Kg: Micrograms/Kilogram (ppb)%Rec: Percent Recovered (surrogates)


: PQL x DilutionND: None Detected at DLR

H: Analyzed outside of hold timeP: Preliminary resultS: Suspect result See Cover Letter for comments.E: Analysis performed by External laboratory.


Page 2 of21414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935

NEL LABORATORIES CHAIN OF CUSTODY NEL Work Order:Reno • Las Vegas • Boise


'urchase Order NumberLas Vegas Division • 4208 Arcata Way, Suite A • Las Vegas, Nevada 89030

702-657-1010 • Fax: 702-657-1577 • 888-368-3282


Time/DateSampled

N.E.LIdentificationCustomer Sample Identification

Custody Seal intactCon-

E Ice OnlyF OtherG Not Preserved

DW • Drinking WaterWW • Waste WaterOL - Oil/Organic Liquid

SD • SolidAQ • AqueousA-A i r

The liability of NEL Laboratories Ino is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received in good condition,including adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceof NEL Standard Ust Prices lor all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Servic es in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received a\ \helaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided aboye

ORIfSINAI !


ILas Vegas Division

4208 Arcata Way, Suite A • Las Vegas, Nevada 89030702-657-1010 • Fax: 702-657-1577

1-888-368-3282


TEL: (702)431-3020

RE Project: RGH-3F-2631

Dear Ed Carlton:

RECEIVED

Order No.: L0203117

NEL Laboratories, Las Vegas received 2 samples on 3/11/02 for the analyses presented in thefollowing report.



St^n Van Wagenen jf^- -*Laboratory Manager


iW


Certified

Date

NEL Laboratories, Las Vegas Date: 26-Mar-02

CLIENT: Dumpco/SilverstateProject: RGH-3F-263' CASE NARRATIVELab Order: L0203117

Attached are the analytical results for samples in support of the above referenced project.

The samples submitted for this project were not sampled by NEL. Should you have any questions orcomments, please feel free to contact our Client Services Department.

Analytical Comments:

EPA 8260: Samples were evaluated for the presence of Acrylonitrile and l,4-Dichloro-2-Butene.None of these analytes were present in the samples submitted in this work order at or above 5ppb.

Page 1 of 1


PROJECT ID: RGH-3F-2631

PROJECT #: RGH-3F-263'

MATRIX: AQUEOUS

ParameterBarium

Calcium

Iron

MagnesiumPotassiumSodiumVanadiumAntimonyArsenic

Beryllium

Cadmium

Chromium

Cobalt

CopperLead

Nickel

SeleniumSilverThalliumZincMercury

Result

NDNDNDNDND0.55NDNDNDNDNDNDNDNDND

0.0015NDNDND

0.0068ND

Unitmg/L

mg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/Lmg/L

ReportingLimit0005005001005020050

0.00500.00100.00100.0010O O O I O0.00100.00100.0010O O O I O0.00100.00100.0010

0.000400.00100.00020

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ID:

DF Method

1 SW6010B-To1 SW6010B-To1 SW6010B-To1 SW6010B-TO1 SW6010B-To1 SW6010B-TO1 SW6010B-TO1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 6020-Tota1 SW 7470-Tota

RGH-3F-263'-M

; 3/11/02

L0203117-001A

Prep Date03/12/0203/12/0203/12/0203/12/0203/12/0203/12/0203/12/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/0203/19/02

Analyzed03/13/0203/13/0203/13/0203/13/0203/13/0203/13/0203/13/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/20/0203/19/02

Analyst

FIF-RenoFIF-RenoFIF-RenoFIF-RenoFIF-RenoFIF-RenoFIF-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-Reno

DHG-Reno

DHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoDHG-RenoJTY-Reno



Date: 26-Mar-02






PROJECT*: RGH-3F-2631

MATRIX: AQUEOUS

Parameter Result Unit

\cetone

Benzene

Bromobenzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

bec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

Chlorobenzene

Chloroe thane


Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene



1 ,2-Dibromoethane

Dibromomethane





1,1-Dichloroethane

1 ,2-Dichloroe thane

1,1-Dichloroethene





2,2-Dichloropropane

1 ,1 -DiUiloropropene

cib-1 ,3-Dichloropropene

tranb-1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodome thane

Isopropylbenzene



Date: 26-Mar-02

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ReportingLimit

255050505050502550505050505050505050505050505050505050505050505050505050505050505.0255050

CLLENTLD: RGH-3F-2631


NEL SAMPLE ID: L02031 17-001B

DF Method Prep Date Analyzed

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

I SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

Analyst

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV






PROJECT #: RGH-3F-263'

MATRIX: AQUEOUS

Parameter

p-lsopropyltoluene

Methylene chlonde


MTBE

Naphthalene

n-Propylbenzene

Styrene


1 , 1 ,2,2-Tetrachloroetnane

Tetrachloroethene

Toluene





Tnchloroethene





1 ,3 ,5-Tnmethylbenzene

Vmyl acetate

Vinyl chlonde

o-Xylene

m,p-Xylene


Surr: Toluene-d8


Result

NDNDNDNDNDNDNDND

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND10298.0

95.7

Unit

ug/L

ug/L

ug/L

ug/L

ug/L

Ug/L

ug/L

ug/L

ug/L

ug/L

Ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%REC

%REC

%REC

ReportingLimit

5050255050505.0505.050505050505.0505.05.05.0505.05.05.05010

808-119

848-102

562-139

CLIENT ID: RGH-3F-263'


NEL SAMPLE LD: L02031 17-001B

DF Method

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Prep Date Analyzed

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

Analyst

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV



Date: 26-Mar-02




CLIENT:

PROJECT ID:

PROJECT #:

MATRIX:

Dumpco/Silverstate

RGH-3F-2631

RGH-3F-2631

AQUEOUS

CLIENT LD: RGH-3F-263'



ReportingParameter Result Unit Limit DF Method Prep Date Analyzed

Chloride ND mg/L 0.10 1 EPA 300.0 03/11/02

Nitrate, as N ND mg/L 0.10 1 EPA 300.0 03/11/02

Nitrite, as N ND mg/L 0.10 1 EPA 300.0 03/11/02

Sulfate ND mg/L 0.10 1 EPA 300.0 03/11/02

Alkalinity, Bicarbonate (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02

Alkalinity, Carbonate (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02

Hydroxide (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02

Alkalinity, Total (As CaC03) ND mg/L 25 1 SM2320 B 03/11/02

Chemical Oxygen Demand 15 mg/L 10 1 SM5520D 03/12/02

Ammonia, as N ND mg/L 0.30 1 SM4500-NH3 03/12/02

Sulfide ND mg/L 0.030 1 SM4500-S D 03/12/02

Total Dissolved Solids 16.0 mg/L 15.0 1 SM2540 C 03/11/02



Date: 26-Mar-02




FCLIENT: Dumpco/Silverstate

PROJECT ID: RGH-3F-263'

PROJECT #: RGH-3F-2631

MATRIX: AQUEOUS

ParameterAcetone

Benzene

Bromobenzene

Bromochloromethane


Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

Chlorobenzene

Chloroethane


Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene



1 ,2-Dibromoethane

Dibromome thane





1,1-Dichloroethane

1 ,2-Dichloroethane

1,1-Dichloroethene






1 ,1 -Dichloropropene

cii-1 ,3-Dichloropropene

trans- 1 ,3-Dichloropropene

Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

ND - Not Detected at the Reporting


Date: 26-Mar-02

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

Limit

Unit

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

Ug/L

Ug/L

Ug/L

Ug/L

ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

ReportingLimit

2550

5.0505.0505.0255.05.05.05.05.05.05.05.0505.0505.05.05.0505.05.0505.05.05.05.05.05.05.05.05.0505.05.05.05.05.0255.05.0

CLIENT ID: XGH-3F-2631



DF

lll111111111l11111111111l1l11111111l11111111

Method Prep Date

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

Analyzed

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

Analyst

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV




•ACLIENT: Dumpco/Silverstate


PROJECT #: RGH-3F-2631

MATRIX: AQUEOUS

Parameter

p-Isopropyltoluene

Methylene chlonde


MTBE

Naphthalene

n-Propylbenzene

Styrene



Tetrachloroethene

Toluene





Tnchloroethene






Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene


Surr: Toluene-d8


Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND10399.2

99.0

Unit

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L

Ug/L%REC

%REC

%REC

ReportingLimit

5.050255.05.05.0505.05.05.05.050505.05.05.05.05.05.05.05.05.05.05.010

808-119

84.8-102

562-139

CLIENT ID: XGH-3F-263'


NEL SAMPLE ID: L02031 17-002A

DF Method

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Prep Date Analyzed

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

03/23/02

Analyst

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV

SKV-LV



Date: 26-Mar-02





Vanessa Padilla Certificate of AnalysisNEL Laboratories Las Vegas ELAP Certificate #11804208 Arcata Way, Ste A Report issue Date: 03/15/2002Las Vegas, NV 89030

BSK Submission #: 2002030580BSK Sample ID #: 189799Project ID L0203117 Project Desc Dumpco

Submission Comments

Sample Type- Liquid

Sample Description. RGH-3F-263

Sample Comments.

Inorganics

Analyte MethodDissolved Organic Carbon (DOC) SM 53 10-D

Date Sampled: 03/11/2002

Time Sampled 0700

Date Received: 03/12/2002

Prep AnalysisResult Units PQL Dilution DLR Date Date

0.50 mg/L 0.2 1 0.2 03/13/200203/13/2002

mg/L Milligrams/Liter (ppm) PQL: Practical Quantitation Limit H: Analyzed outside of hold timemg/Kg Milligrams/Kilogram (ppm) DLR: Detection Limit for Reporting P: Preliminary resultug/L Micrograms/Liter (ppb) : PQL x Dilution S: Suspect result. See Cover Letter for comments

ug/Kg Micrograms/Kilogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory%Rec Percent Recovered (surrogates) See External Laboratory Report attachments

Report Authentication Code. I HUH Hill HI) [HIM 111 111 Page 1 of 1

1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935


Dumpco/Silverstate

L0203117RGH-3F-263'


Sample ID L0203 11 7-001 CMS SampType MS TestCode 300_W Units mg/L Prep Date Run ID L_IC-1_020311 A

Client ID RGH-3F-263' Batch ID R884 TestNo E300 Analysis Date 3/11/02 SeqNo 5999

Analyte

Nitrite, as N

Sulfate

Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

0937 010 1 0 937 80 120 0 00855 010 1 0 855 80 120 0 0


J Analyte detected be/ow quantitation limits




Page 2 of 16

NEL Laboratories, Las Vegas Date: 26-Mai-02

CLIENT: Dumpco/SilverstateWork Order: L0203117


Project: RGH-3F-263'

Sample ID MB-R884

Client ID ZZZZZ

Analyte

Chlonde

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID LCS-R884

Client ID ZZZZZ

Analyte

Chlonde

Nitrate, as N

Nitnte, as N

Sulfate

Sample ID LCSD-R884

Client ID ZZZZZ

Analyte

Chlonde

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID L02031 1 7-001 CMS

Client ID RGH-3F-263'

Analyte

Chlonde

Nitrate, as N

SampType MBLK

Batch ID R884

Result

NDNDNDND

SampType LCS

Batch ID R884

Result

2054

09665

09612507

SampType LCSD

Batch ID R884

Result

2039

0953

0948

2494

SampType MS

Batch ID R884

Result

0974

0928

TestCode 300_W

TestNo E300

PQL SPK value

0 100100 100 10

TestCode 300JW

TestNo E300

PQL SPK value

0 10 20 10 10 10 10 10 25

TestCode 300_W

TestNo E300

PQL SPK value

010 2010 1

010 10 10 25

TestCode 300_\V

TestNo E300

PQL SPK value

0 10 10 10 1

Units mg/L

SPK Ref Val

Units mg/L

SPK Ref Val

0000

Units mg/L

SPK Ref Val

0000

Units mg/L

SPK Ref Val

00

Prep Date

Analysis Date

TestCode: 300_W

3/11/02


Prep Date



103 80966 8096 1 80100 80

Prep Date

Analysis Date

120 0120 0120 0120 0

3/11/02


102 80953 80948 80998 80

Prep Date

Analysis Date

120 2054

120 09665

120 0961120 2 507

3/11/02

%RJ5C LowLimit HighLimit RPD Ref Val

974 8092 8 80

120 0120 0

Run ID LJC-1_020311A

SeqNo 5996

%RPD RPDLimit

Run ID L_IC-1_020311A

SeqNo 5995

%RPD RPDLimit

0000


SeqNo 6000

%RPD RPDLimit

0733 25

1 41 251 36 25

0 520 25


SeqNo 5999

%RPD RPDLimit

00

Qual

Qual

Qual

Qual

Qualifiers: ND - Not Detected at the Reporting I unit

S - Anafyle delected below quantilation limits

S - Spike Recovery outside accepted iccovery limits

R RPD outside accepted icco\cry limits


Page I of 16

CLIENT: Dumpco/SilverstateWork Order: L0203117



Sample ID MB-355

Client ID ZZZZZ

Analyte

Banum

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample ID LCS-355

Client ID ZZZZZ

Analyte

Banum

Calcium

Iron

MagnesiumPotassium

Sodium

Vanadium

Sample ID R0203046-001AMS

Client ID ZZZZZ

Analyte

Banum

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

SampType MBLK

Batch ID R_355

Result

NDNDNDNDNDNDND

SampType LCS

Batch ID R_355

Result

1 0342079

10952062

2033

1980516

SampType MS

Batch ID R_355

Result

1 0414642

1 18466798056

338052

TestCode

TestNo

PQL

00050

0500 1005020

05000050

TestCode

TestNo

PQL

0005005001005020

05000050

TestCode

TestNo

PQL

00050

0500 1005020

05000050

6010W_T

SW6010B

SPK value

6010\V_T

SW6010B

SPK value

120

120202005

6010W_T

SW6010B

SPK value

120

120202005

Units mg/L

SPK Ref Val

Units mg/L

SPK Ref Val

0000000

Units mg/L

SPK Ref Val

0 03577

4385

0 1135

46146069

3200

%REC

%REC

103104

10910310299

103

%REC

101129107103

99490

104

Prep Date

Analysis Date

TestCode: 6010WJT

3/12/02

3/13/02

LowLimit HighLimit

Prep Date

Analysis Date

3/12/02

3/13/02

LowLimit HighLimit

85858585858585

Prep Date

Analysis Date

115115115115115115115

3/12/02

3/13/02

LowLimit HighLimit

75757575757575

125125125125125125125

RPD Ref Val

RPD Ref Val

0000000

RPD Ref Val

0000000

Run ID SDB-688

SeqNo 9779

%RPD RPDLimit Qual

Run ID SUB-688

SeqNo 8802

%RPD RPDLimit Qual

0000000

Run ID SUB-688

SeqNo 9132

%RPD RPDLimit Qual

00 C

00000

Qualifiers ND - Not Delected at the Reporting I imit

J Ana/ytc detected below quantitation limits

S Spike Recovery outside accepted recovery limits


B Analyte detected in the associated Method Blank

Page 3 of } 6

CLIENT: Dumpco/SilverstateWork Order: L0203117Project: RGH-3F-263'

Sample ID R0203046-001AMSD

Client ID ZZZZZ

Analyte

BanumCalciumIronMagnesiumPotassiumSodiumVanadium

SampType MSD

Batch ID R_355

Result

1 04445791 18366628023

33705195

TestCode

TestNo

PQL

0005005001005020

05000050

6010W_T

SW6010B

SPK value

1

201

20202005

Units mg/L

SPK Ref Val

0 035774385

0 113546 146069

3200

%REC

10197

107102

97785

104


TestCode: 6010W_T

Prep Date 3/12/02


LowLimit HighLimit RPD Ref Val

0000000

Run ID SUB-688

SeqNo 9781

%RPD RPDLimit Qual

00000

00





B - Analyte1 detected in the- associated Method Blank

Page 4 of 16

CLIENT: Dumpco/SilveistateWork Order: L0203117



Sample ID MB-431

Client ID ZZZZZ

Analyte

AntimonyArsenicBerylliumCadmiumChromiumCobaltCopperLeadNickelSeleniumSilverThalliumZinc

Sample ID LCS-431

Client ID ZZZZZ

Analyte

AntimonyArsenicCadmiumChromiumCobaltCopperLeadNickelSeleniumSliverThalliumZinc

SampType MBLK

Batch ID R_431

Result

NDNDNDNDNDNDNDND

NDNDNDNDND

SampType LCS

Batch ID R_431

Result

004750 104400557005590 0555

0055150 052050056850 10680053

0 0546500568

TestCode

TestNo

PQL

00050000500005000050000500005000050000500005000050000500002000050

TestCode

TestNo

PQL

000500005000050000500005000050000500005000050000500005000050

6020WJT

SW6020

SPK value

6020WJT

SW6020

SPK value

00501

00500500500500500501

005005005

Units mg/L

SPK Ref Val

Units mg/L

SPK Ref Val

000000000000

%REC

%REC

95

104

111112111110104114107106109114

Prep Date

Analysis Date

TestCode: 6020WJT

3/19/02

3/20/02


Prep Date

Analysis Date

3/19/02

3/20/02


85

8585858585858585858585

115 0

115 0115 0115 0115 0115 0115 0115 0115 0115 0115 0115 0

Run ID SUB-807

SeqNo 9751

%RPD RPDLimit Qual

Run ID SUB-807

SeqNo 9789

%RPD RPDLimit Qual

00000000000

0

Qualifiers: ND - Not Detected at the Reporting I imit

J - Analyle delected below quanlitalion limits




Page 5 of 16



Client ID ZZZZZ

Analyte

AntimonyArsenicCadmiumChromiumCopperLeadNickelSeleniumSilverThalliumZinc


Client ID ZZZZZ

Analyte

AntimonyArsenicBerylliumCadmiumChromiumCobaltCopper

LeadNickelSeleniumSilverThalliumZinc

SampType MS

Batch ID R_431

Result

0052304244005450061903558

0 044350 102

022080181200476

0 08595

SampType MSD

Batch ID R_431

Result

0053904586

ND0 057750 065950668603906004590 109802356

0 19500502

009315

TestCode

TestNo

PQL

0005000050000500005000050000500005000050000500005000050

TestCode

TestNo

PQL

00050000500005000050000500005000050000500005000050000500005000050

6020WJT

SW6020

SPK value

00501

00500500500500501

005005005

6020W_T

SW6020

SPK value

0050101

0050050050050050050 1

005005005

Units mg/L

ANALYTICAL QC SUMMARY REPORTTestCode: 6020WJT

Prep Date 3/19/02


SPK Ref Val

0033

000117503219

00 05395

012130 1406

000349

Units mg/L

%REC

105943109100

67788796199581 4952102

LowLimit

7575757575757575757575

HighLimit

125125125125125125125125125125125

RPD Ref Val

00000000000

Prep Date 3/19/02


SPK Ref Val

0033

00

0011750595

032190

0 053950 12130 1406

000349

%REC

108129

0116108147137

91 8112114109100116


0000000000000

Run ID SUB-807

SeqNo 9791

%RPD RPDLimit

00000000000

Run ID SUB-807

SeqNo 9792

%RPD RPDLimit

0000000000000

Qual

C

Qual

Jl

C

Qualifiers- ND - Not Detected at the Reporting Limit

J Anal>te detected below quantitation limits




Page 6 of 16


Sample ID: MB-R1291 SampType:


Analyte

AcetoneBenzeneBromobenzeneBromochloro methaneBromodichloromethaneBromoformBromomcthane2-Butanone

n-Butylbenzencsec-Butylbenzenetert-ButylbenzeneCarbon disulfideCarbon tetrachlorideChlorobenzeneChloroethane2-Chloroethyl vinyl etherChloroformChlorome thane2-Chloro toluene4-Chloro tolueneDibromochloromc thane1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoe thaneDibromome thane1 ,2-Dichlorobenzene1 ,3-Dichlorobenzene1 ,4-DichlorobenzeneDichlorodifluoromcthane1,1-Dichloroe thane1 ,2-Dichloroe thane1 , 1 -Dichloroethene

MBLK

R1291

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDND


TestCode: 8260_W Units: ng/L Prep Date: Run ID: L_VOAMS-2_020323B

TestNo: SW8260B Analysis Date: 3/23/02 SeqNo: 8763


255.05.05.05.05.05.0255.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.05.0


J - Analyte dete-cted below quantitation limits




Page 7 of 16


Sample ID. MB-R1291 SampType:

Client ID: ZZZZZ Batch ID'

Analyte

cis-1 ,2-Dichloroethenetrans-1 ,2-Dichloroethene1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-Dichloropropane1,1 -Dichloropropenecis-1 ,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzeneHexachlorobutadtene2-Hexanone

lodome thaneIsopropylbenzenep-Isopropyltoluene

Methylene chloride4-Methyl-2-pentanoneMTBENaphthalenen-PropylbenzeneStyrenc1,1,1 ,2-Tetrachloroethane1 ,1 ,2,2-TetrachloroethaneTetrachloroetheneToluene

1 ,2,3-Trichlorobenzene1 ,2,4-Trichlorobenzene1,1,1 -Trichloroethane1 , 1 ,2-TrichloroethaneTrichloroctheneTrichlorofluoro methane1 ,1 ,2-Trichlorotnfluoroethane

MBLK

R1291

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND


TestCode: 8260_W Units: fig/L Prep Date: Run ID L_VOAMS-2_020323B

TestNo: SW8260B Analysis Date: 3/23/02 SeqNo: 8763


5.05.05.05.05.05.05.05.05.05.0255.05.05.05.0255.010

5.05.05.05.05.05.05.05.05.0

5.05.05.05.0






Page 8 of 16


Sample ID MB-R1291

Client ID ZZZZZ

Analyte




Vinyl acetate

Vinyl chlonde

o-Xylenem,p-Xylene

Surr Dibromofluoromethanc

Surr Toluene-d8


Sample ID LCS-R1291

Client ID ZZZZZ

Analyte

Benzene

Bromome thane

ChlorobenzeneChloromethane


1,1-Dichloroe theneToluene

Tnchloroe thene

Vinyl chlonde


Surr Toluene-d8


SampType MBLK

Batch ID R1291

Result

ND

ND

ND

ND

ND

ND

ND

5053

5023

4803

SampType LCS

Batch ID R1291

Result

4994

5571

51 62

5057

5329

4963

5064

51 23

483

5065

5052

509

TestCode

TestNo

PQL

50

50

50

50

50

50

10

50

50

50

TestCode

TestNo

PQL

50

50

50

50

50

50

50

50

50

50

50

50

8260_W

SW8260B

SPK value

50

50

50

8260_W

SW8260B

SPK value

50

50

50

50

50

50

50

50

50

50

50

50

Units (ig/L


TestCode: 8260_W

Prep Date


SPK Ref Val

0

0

0

Units (ig/L

%REC

101

100

96 1

LowLimit

808

848

562

HighLimit

119

102

139

RPD Ref Val

0

0

0

Prep Date


SPK Ref Val

0

0

0

0

0

0

0

0

0

0

0

0

%REC

999

111

103101107

993

101

102

966

101

101

102

LowLimit

70

70

70

70

70

80

80

70

80

8080

90

70

HighLimit

130

130

130

130

130

120

120

130

120

102

102

106

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

0


SeqNo 8763

%RPD RPDLimit

0

0

0

Qual


SeqNo 8764

%RPD RPDLimit

0

0

0

0

0

0

0

00

0

0

0

Qual

S

Qualifiers: ND - Not Detected at the Reporting 1 milt

J - Analyte detected below quant i ta t ion l imits


R - RPD outside accepted recovery limits'


Page 9 of 16


Sample ID L0203117-001BMS


Analyte

BenzeneBromo methaneChlorobenzeneChloromcthaneDichlorodifluoromethane1,1-DichloroetheneTolueneTnchloroe theneVinyl chlonde

Surr DibromofluoromcthaneSurr Toluene-d8Surr 4-Bromofluorobenzene

Sample ID L0203U7-001BMSD

Client ID RGH-3F-2631

Analyte

BenzeneBromomethaneChlorobenzeneChloromethaneDichlorodi fluoromethane1,1-DichloroetheneTolueneTnchloroetheneVinyl chlonde

Surr DibromofluoromethaneSurr Toluene-d8Surr 4-Bromofluorobenzenc

SampType MS

Batch ID R1291

Result

442541 535026428548 183924456845743367499348954852

SampType MSD

Batch ID R1291

Result

4256368448 19334

41 33362

436443 672908499448394869

TestCode

TestNo

PQL

505050505050505050

505050

TestCode

TestNo

PQL

505050505050505050505050

8260_W

SW8260B

SPK value

505050505050505050505050

8260_W

SW8260B

SPK value

505050505050

505050505050

Units ug/L


Prep Date


SPK Ref Val

000000000

000

Units ng/L

%REC

88583 1101

85796478591 491 5673

999979

97

LowLimit

70707070708080

7080899070

HighLimit

130130130130130120120130120102102106

RPD Ref Val

000000000000

Prep Date


SPK Ref Val

000000000000

%REC

85 I737964668827724

87 3873582999968974

LowLimit

707070707080807080899070

HighLimit

130130130130130120120

130120102102106

RPD Ref Val

442541 535026428548 183924456845743367

000


SeqNo 8765

%RPD

000000000

000

Run ID L_

RPDLimit Qual

S

S

VOAMS-2_020323B

SeqNo 8766

%RPD

3891204 2 1248153806457463146

000

RPDLimit

252525252525252525000

Qual

S

S

S

Qualifiers: ND - Not Detected at the Reporting 1 imit

J Ana l> te detected below quantitation l imits




Page 10 of 16


Dumpco/Silvei state

L0203117

RGH-3F-263'


TestCode: ALK W

Sample ID MB-R898

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R898

Result

TestCode ALK_W Units mg/L

TestNo M2320 B


Prep Date



Run 1 D L_ATITR-1 _0203 1 1 A

SeqNo 6076

%RPD RPDLimit Qual





NDNDNDND

25252525

Sample ID LCS-R898

Client ID ZZZZZ

Analyte

SampType LCS

Batch ID R898

Result

TestCode ALKJW Units mg/L

TestNo M2320B


Prep Date




SeqNo 6075

%RPD RPDLirnit Qual

Alkalinity, Total (As CaCO3) 1255 25 125 100 80 120

Sample ID LCSD-R898

Client ID ZZZZZ

Analyte

SampType LCSD

Batch ID R898

Result


TestNo M2320 B


Prep Date



Run ID L_ATITR-1 J)203 1 1 A

SeqNo 6077

%RPD RPDLimit Qual

Alkalinity, Total (As CaCO3) 1256 25 125 100 80 120 1255 00796 25

Sample ID L0203071-001ADUP SampType DUP


Analyte





Result

200NDND

200

TestCode ALK_W Units mg/L Prep Date

TestNo M2320B

PQL

252525

25

SPK value

0000

SPK Ref Val

20000

200

%REC

000

0


LowLimit

000

0

HighLimit

000

0

RPD Ref Val

0000


SeqNo 6078

%RPD RPDLimit

000

0

Qual


J - Anal>te detected below quantitation limits


R - RPD outside accepted iccovery limits


Page 11 of 16


Dumpco/Silverstate

L0203117RGH-3F-263'


TestCode: COD

Sample ID

Client ID

Analyte

MB-R900

ZZZZZ

SampType

Batch ID

MBLK

R900

Result

TestCode

TestNo

PQL

COD

M5220 C

SPK value

Units mg/L

SPK Ref Val

Prep Date



Run ID L_SPEC-2

SeqNo 6090

%RPD RPDI

_020312C

limit Qual


Sample ID LCS-R900

Client ID ZZZZZ

Analyte

SampType LCS

Batch ID R900

Result

TestCode COD Units mg/L

TestNo M5220C


Prep Date



Run ID L_SPEC-2_020312C

SeqNo 6089

%RPD RPDLimit Qual

Chemical Oxygen Demand 529 10 500 106 80 120

Sample ID LCSD-R900

Client ID ZZZZZ

Analyte

SampType LCSD

Batch ID R900

Result

TestCode

TestNo

PQL

COD Units mg/L

M5220 C


Prep Date

Analysis Date


3/12/02


SeqNo 6093

%RPD RPDLimit Qual

Chemical Oxygen Demand 519 10 500 104 80 120 529 1 91 15

Sample ID L0203 117-001 CMS


Analyte

SampType MS

Batch ID R900

Result


TestNo M5220C


Prep Date




SeqNo 6091

%RPD RPDLimit Qual

Chemical Oxygen Demand 544 10 500 15 106 70 130

Sample ID

Client ID

Analyte

L0203117-001CMSD

RGH-3F-263'

SampType

Batch ID

MSD

R900

Result

TestCode

TestNo

PQL

COD

M5220 C

SPK value

Units mg/L

SPK Ref Val

Prep Date

Analysis Date


3/12/02


SeqNo 6092

%RPD RPDLimit Qual

Chemical Oxygen Demand 535 10 500 15 104 70 130 544 1 67 25

Qualifiers: ND - Not Detected at the Reporting I innt

J - Anal>tc detected below quantitation limits


R - RPD outside accepted reco\cn, limits


Page 12 of 16


Dumpco/Silverstate

L0203117RGH-3F-263'


TestCode: HG 7470 T

Sample ID

Client ID

Analyte

MB-419

ZZZZZ

SampType

Batch ID

MBLK

R_419

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPK Ref Val

Prep Date

Analysis Date

3/19/02

3/19/02


Run ID SUB-787

SeqNo 9785

%RPD RPDI imit Qual

Mercury ND 0 00020

Sample ID

Client ID

Analyte

LCS-419

ZZZZZ

SampType

Batch ID

LCS

R_419

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

3/19/02

3/19/02


Run ID SUB-787

SeqNo 9408

%RPD RPDLimit Qual

Mercury 0 00474 0 00020 0005 948 85 115

Sample ID

Client ID

Analyte

L02031 17-001 A

RGH-3F-263'-M

SampType

Batch ID

MS

R_419

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

3/19/02

3/19/02


Run ID SUB-787

SeqNo 9786

%RPD RPDLimit Qual

Mercury 00048 0 00020 0005 96 85 115

Sample ID

Client ID

Analyte

L02031 17-001 A

RGH-3F-263'-M

SampType

Batch ID

MSD

R_419

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

3/19/02

3/19/02


Run ID SUB-787

SeqNo 9748

%RPD RPDLimit Qual

Mercury 0 00491 0 00020 0005 982

Sample ID

Client ID

Analyte

L0203117-001A

RGH-3F-263'-M

SampType

Batch ID

DUP

R_419

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPK Ref Val

Prep Date

Analysis Date

3/19/02

3/19/02


Run ID SUB-787

SeqNo 8594

%RPD RPDLimit Qual

Mercury ND 0 00020

Qualifiers: ND • Not Detected at the Reporting I miit

* J Analv te detected below quant i ta t ion l imits


R - RPD outside accepted recovery l imits


Page 13 of 16


Dumpco/SilverstateL0203117RGH-3F-263'

ANALYTICAL QC SUMMARY REPORTTestCode: NH3-N W

Sample ID MB-R901

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R901

Result

TestCode NH3-N_W Units mg/L

TestNo M4500-NH3 C

PQL SPK value SPKRefVai

Prep Date



Run ID L_WC_020312B

SeqNo 6099

%RPD RPDLimit Qual


Sample ID LCS-R901

Client ID ZZZZZ

Analyte

SampType LCS

Batch ID R901

Result


TestNo M4500-NH3C


Prep Date



Run ID L_WC_020312B

SeqNo 6098

%RPD RPDLimit Qual

Ammonia, as N 1008 030 101 839 117

Sample ID LCSD-R901

Client ID ZZZZZ

Analyte

SampType LCSD

Batch ID R901

Result


TestNo M4500-NH3 C


Prep Date



Run ID L_WC_020312B

SeqNo 6100

%RPD RPDLimit Qual

Ammonia, as N 1 12 030 112 839 117


f 3 - Anal>te detected below quantitation limits




Page 14 of 16


Dumpco/SilverstateL0203117RGH-3F-263'


TestCode: SULF W

Sample ID MB-R879

Client ID ZZZZZ

Analyte

SampType MBLK

Batch ID R879

Result

TestCode SULF_W Units mg/L

TestNo M4500-SD


Prep Date



Run ID L_SPEC-2_020312A

SeqNo 5960

%RPD RPDLimit Qual

Sulfide ND 0030

Sample ID LCS-R879

Client ID ZZZZZ

Analyte

SampType LCS

Batch ID R879

Result


TestNo M4500-SD


Prep Date




SeqNo 5959

%RPD RPDLimit Qual

Sulfide 0 118 0030 0107 110 80 120

Sample ID LCSD-R879

Client ID ZZZZZ

Analyte

SampType LCSD

Batch ID R879

Result


TestNo M4500-SD


Prep Date




SeqNo 5961

%RPD RPDLimit Qual

Sulfide O i l 0030 0107 103 80 120 0 118 702 25

Sample ID

Client ID

Analyte

L0203117-001CMSD

RGH-3F-263'

SampType

Batch ID

MSD

R879

Result

TestCode

TestNo

PQL

SULF_W

M4500-S D

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date


3/12/02


SeqNo 5963

%RPD RPDLimit Qual

Sulfide 0 107 0030 0 107 100 70 130 25


J - Anal^te detected below, quantitation limits


R - RPD outside accepted recoveiy limits

B - Analyte detected in trie associated Method Blank

Page 15 of 16


Sample ID MB-R907

Client ID ZZZZZ

Analyte


Sample ID: LCS-R907

Client ID ZZZZZ

Analyte


Sample ID: L02031 07-005 ADUP

Client ID: ZZZZZ

Analyte

SampType- MBLK

Batch ID: R907

Result

ND

SampType: LCS

Batch ID: R907

Result

997

SampType: DUP

Batch ID: R907

Result

TestCode: TDS_W Units: mg/L

TestNo: E160.1


15.0


TestNo: E160.1


15.0 1000 0


TestNo: E160.1


ANALYTICAL QC SUMMARY REPORTTestCode: TDS_W

Prep Date:

Analysis Date: 3/11/02


Prep Date:



99.7 80 120 0

Prep Date:



Run I D L_WC_0203 1 1 D

SeqNo 6140

%RPD RPDLimit

Run ID: L_WC_0203 1 1 D

SeqNo: 6139

%RPD RPDLimit

0

Run ID: L_WC_020311D

SeqNo: 6141

%RPD RPDLimit

Qual

Qual

Qual

Total Dissolved Solids 1133 15.0 2360 70.3 25






Page 16 of 16

NEL LABORATORIESReno • Las Vegas • Boise


CHAIN OF CUSTODY NEL Work Order:

Las Vegas Division • 4208 Arcata Way, Suite A • Las Vegas, Nevada 89030702-657-1010 • Fax. 702-657-1577 • 888-368-3282

Company:,- Attentioi

Address:

Phone NumbSr

Billing Address:'*'•<" s?^)JLs»icr xvcjr

Requested Turnaround: jf 5-day 2-day 1-day

Time/Date N.E.L.Sampled Customer Sample Identification Identification

Project Name1

Purchase Order Number

Project Number

Sampled By

B3

Custody Seal intact?/ Y

CondTtttfn

Box#1 DW • Drinking WaterWW - Waste WaterOL - Oil/Organic Liquid

SO • SolidAQ • AqueousA • Air

Box #2 A HCIB HMO,C HjSO,,D NaOH

E Ice OnlyF OthwG Not Preserved

Relinquished by (Print) (Sigrgfure) Date/Time Received by (Print) (Signature)

Z^Date/Timee/Tirae

The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received m good condition by NEL NEL is not responsible for loss damage, resampling costs and/or qualified data related to samples not received in good condition,intruding adeQuate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceo1 M£\- Standard hsi Prices lot att services otdeted t\eie on, except those specilied otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided above

ORIGINAL

NEL LABORATORIESReno • Las-Vegas- — -Phoenix • Burbank

Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, NV 89030

(702)657-1010 -Fax: (702) 657-15771-888-368-3282

Nick SainesDumpco/Silverstate7900 Vegas Valley DriveLas Vegas, NV 89142

TEL: 702-431-3020

RE Project: GH-3F

Dear Nick Saines:

Order No.: L0204322




<m^tA{MJ>o/Stan Van vagenea^ ALaboratory Manager


'<(«<



Corporate Office & Reno Division • 1030 Matley Lane • Reno, NV 89502 • (702) 348-2522

NEL LABORATORIES

NEL Laboratories, Las Vegas Date: 17-May-02

CLIENT:

Project:Lab Order:

RSSN

GH-3F

L0204322CASE NARRATIVE




EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Neither of these two compounds were present in the samples submitted in this work-order at or above5ppb.

Page 1 of 1

NEL LABORATORIESI

CLIENT: RSSN

PROJECT ID: GH-3F

PROJECTS: GH-3F

MATRIX: AQUEOUS

Parameter

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

Alkalinity, Bicarbonate (As CaCOS)


Hydroxide (As CaC03)



Ammonia, as N

Sulfide


CLIENT ID: GH-3F



Result

2200

ND

ND

3000

ND75

ND75

76

NDND

7220

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

200

2525200252525

25

10

0300030

150

DF

2000

2525

2000

1111111

10

Method Prep Date

EPA 300 0

EPA 300 0

EPA 300 0

EPA 300 0

SM2320 B

SM2320 B

SM2320 B

SM2320 B

SM5520 D

SM4500-NH3

SM4500-S D

SM2540 C

Analyzed

04/30/02

04/23/02

04/23/02

04/30/02

04/29/02

04/29/02

04/29/02

04/29/02

04/29/02

04/30/02

04/26/02

04/24/02

Analyst

PJJ-LV

PJJ-LV

PJJ-LV

PJJ-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RDA-LV

RWW-LV

CRA-LV

ND -Not Detected at the Reporting Limit


Date: 16-May-02




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: GH-3F

PROJECT #: GH-3F

MATRIX: AQUEOUS

Parameter

Aluminum

Barium

Calcium

IronMagnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.88

0.028

6200.78

19095

1600

NDND

0.021

ND

ND0.0081

0.0024

0.014

NDND

0.0065

NDNDND0.14

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0050000500200100202050

00050OOOIOOOOIOO O O I OOOOIOO O O I OOOOIOOOOIOOOOIOO O O I OO O O I OOOOIOOOOIO

0 00040O O O I O

0 00020

CLIENT ID:

DATE SAMPLED:

NEL SAMPLE ID:

DF

111111

1001111111111111111

Method

SW 6010B-To

SW6010B-To

SW 6010B-TO

SW6010B-TO

SW6010B-To

SW6010B-To

SW6010B-To

SW6010B-TO

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 7470-Tota

GH-3F-M

: 4/22/02

; L0204322-002A

Prep Date

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/24/02

Analyzed

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

Analyst

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

A



Date: 16-May-02




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: GH-3F

PROJECT*: GH-3F

MATRIX: AQUEOUS

Parameter

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.099

0.020

620ND18088

1500

ND0.0011

0.019

NDND

0.0022

0.0014

0.0069

ND0.0024

0.0034

NDNDND

0.084

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0050

00050

0500100502050

00050

O O O I O

OOOIO

OOOIO

OOOIO

OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

OOOIO

0 00040

OOOIO

0 00020

CLIENT ID: GH-3F-FFM



DF Method Prep Date

1 SW 6010B-Di

1 SW 6010B-Di

1 SW 6010B-Di

1 SW 6010B-D1

1 SW 60108-Di

1 SW 6010B-D1

10 SW 6010B-D1

1 SW6010B-D1

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 6020-Diss

1 SW 7470-Diss 04/24/02

Analyzed

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

Analyst

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

A

ND - Not Detected at the Repoitmg I unit

DF - Dilution Facun

Date: I6-Mav-02




NEL LABORATORIES

CLIENT: RSSN

PROJECTED: GH-3F

PROJECTS: GH-3F

MATRIX: AQUEOUS

Parameter


• 1,1,1-Tncbloroethane1,1,2,2-Tetrachloroethane1,1,2-Tnchloroethane1 , 1 ,2-Tnchlorotrifluoi oethane1 , 1 -Dichloroethane1 1 -Dichloroethene

1 , 1 -Dichloropropene1 ,2,3-Tnchloroben7ene1 ,2,3-Tnchloropropane1 ,2,4-Tnchlorobenzene1 ,2,4-Tnmethylbenzene

1 ,2-Dibromo-3-chloropi opane

1 ,2-Dibromoethane1 ,2-Dichlorobenzene1,2-Dichloroethane1 ,2-Dichloropropane1 ,3,5-Tnmethylbenzene1 ,3-Dichlorobenzene1 ,3-Dichloropropane1 ,4-Dichlorobenzene2,2-Dichloropropane2-Butanone2-Chloroethyl vinyl ether

2-Chlorotoluene2-Hexanone4-Chlorotoluene

4-Methyl-2-pentanoneAcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformBromomethaneCarbon disulfideCarbon tetrachlondeChlorobenzeneChloroethaneChloroformChloromethanecis-1 ,2-Dichloroethenecis-1 ,3-DicliloropropeneDibromochloromethane



Date: l6-May-02

CLIENT ED: FGH-3F (Field Blank)



Result Unit

ND ug/LND ug/LND ug/LND ug/LND ng'LND ug/LND ug/L

ND ug/L

ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L

ND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L

ND ug/L

ND ug'LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/LND ug/L

ReportingLimit DF Method Prep Date Analyzed

50 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 125 150 150 125 150 125 125 150 150 150 150 150 150 150 150 150 150 150 150 150 150 150 1

SW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260BSW8260B

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/0204/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/0204/23/02

Analyst

DRM-LVDRM-LVDRM-LVDRM-LV

DRM-LVDRM-LVDRM-LVDRM-LVDRM-LV

DRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LVDRM-LV




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: GH-3F

PROJECTS: GH-3F

MATRIX: AQUEOUS

Parameter

Dibromomethane


Ethylbenzene

Hexachlorobutadiene

lodomethane

Isopropylbenzene

m,p-Xylene

Methylene chlonde

MTBEn-Butylbenzene

n-Propylbenzene

Naphthalene

o-Xylene

p-Isopropyltoluene

sec-Butylbenzene

Styrene

tert-Butylbenzene

Tetrachloroethene

Toluene



Tnchloroethene


Vinyl acetate

Vinyl chlonde


Surr: Dibromofluoi omethanc

Surr: Tolucne-d8

Result


96.3

109

Unit

ug/L

ug/L

ug/L

Ug/L

HS/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%REC

%REC

%REC

ReportingLimit

50505050505010505050501050505050505050505050505050

85 3-104

92 6-108

957-112

CLIENT ID: FGH-3F (Field Blank)



DF

llllllllllllllllllllllllllll

Method

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

SW8260B

Prep Date Analyzed

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

ND - Not Detected at the Repotting Limit


Date: 16-May-02




BSK A N A L Y T I C A L

Vanessa Padilla Certificate of AnalysisNEL Laboratories Las Vegas ELAP Certificate #11804208 AjCata Way, Ste A Report Issue Date: 05/01/2002

Las Vegas, NV 89030

BSK Submission #: 2002041149BSK Sample ID #: 201120Project ID L0204322 Project Desc Dumpco

Submission Comments

Sample Type:Sample Description:Sample Comments-

Inorganics

Analyte

LiquidGH-3F

Method

Date Sampled. 04/22/2002Time Sampled: 0940Date Received: 04/23/2002


Dissolved Organic Carbon (DOC) SM5310-D 4.2 mg/L 02 5 10 04/29/200204/29/2002

mg/L: Milligrams/Liter (ppm) PQL: Practical Quantitation Limit H: Analyzed outside of hold timemg/Kg: Milligrams/Kilogram (ppm) DLR: Detection Limit for Reporting P: Preliminary resultUg/L: Micrograms/Liter (ppb) : PQL x Dilution S: Suspect result. See Cover Letter for commentsug/Kg: Micrograms/Kilogram (ppb) ND: None Detected at DLR E: Analysis performed by External laboratory.%Rec- Percent Recovered (surrogates) See External Laboratory Report attachments

Report Authentication Code: IllOIIIIIIiniilllllllllllllililliliiilllflllll page 1 uf [

1414 Stanislaus Street Fresno, CA 93706-1623 Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935

BSICA N A L Y T I C A LLABOR-A-T-ORILS

QC Summary Report 05/01/2002

BSK Submission:Client:Date Submitted:Project ID :Project Desc:

2002041149NEL Laboratories Las Vegas04/23/2002L0204322Dumpco

BSK StarLims Run #: 36194Analyst Initials: DONNAHAnalyte Results MatrixAnalyte QCType Spike ID Result

Instrument ID:

Method Number: DOC%Rec Spike Spk Matrix

Units or RPD RPD Cone Cone UCL LCL Date

Dissolved Organic Carbon (DOC)





LCS

LCSD

MS

MSD

RBLK

N/A

N/A

201118

201118

N/A

1.03

1.01

23.87

23.78

0

mg/L

mg/L

mg/L

mg/L

mg/L

103

101

110

110

<0.2

1

2 1

10

0.37 10

ND

ND

12

12

130

130

130

130

0.2

70

70

70

70

N/A

04/29/02

04/29/02

04/29/02

04/29/02

04/29/02

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Approved by:

%Rec: Percent Recovered

RPD: Relative Percent Difference

UCL: Upper Control Limit

LCL: Lower Control Limit

Parent Sample: Sample used as background matrix for MS/MSD

DOS-High: QC Result Above UCL

DOS-Low: QC Result Below LCL

Page 1 of 1

NEL LABORATORIES,^-:— 3JH|

i^•BK^^^•k-JOUHHBUI BIBBHIIIMh.

CLIENT: RSSNWork Order: L0204322Project: GII-3F

Sample ID MB-R2742

Analyte

Chlonde

Nitrate, as N

Nitnte.asNSulfate

Sample ID MB-R2993

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID LCS-R2742

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

SampType MBLK

Batch ID R2742

Result

NDNDNDND

SampType MBLK

Batch ID R2993

Result

NDNDNDND

SampType LCS

Batch ID R2742

Result

2010994

096272


300_W Test Method: EPA 300.0

TestCode 300_W Units mg/L Piep Date Run ID L_IC-I_020423A


PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

0 100 100 100 10

TestCode 300_W Units mg/L Prep Date Run ID L_1C-1_020430A



0100 100 100 10

TestCode 300_W Units mg/L Prep Date Run ID L_IC-1_020423A

TestNo E300 Analysis Date 4/23/02 StqNo 20974


010 2 0 101 80 120 0 0010 1 0 994 80 120 0 0010 1 0 96 80 120 0 0

010 25 0 109 80 120 0 0

Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked

Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits

j - This conccntiation is consideied an estimate due to LCS fa i lu ie


Page 1 of'26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F

Sample ID LCS-R2993

Analyte

Chloride

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID LCSD-R2742

Analyte

Chloi ide

Nitiate, as N

Nitrite, as NSulfate


Analyte

Chlonde

NiUate, as N

Nitute, asN

Sulfate


Analyte

Nitiate, as N

Nitrite, as N


SampType LCS

Batch ID R2993

Result

20130986

1 0152547

SampType LCSD

Batch ID R2742

Result

2067

0994

0982719

SampType LCSD

Batch ID R2993

Result

2060972

1 022602

SampType MS

Batch ID R2742

Result

2463082

TestCode 300_W

TestNo E300

PQL SPK value

010 20 10 10 10 10 10 25

TestCode 300_W

TestNo E300

PQL SPK value

0 10 20 10 1

010 10 10 25

TestCode 300_W

TestNo E300

PQL SPK value

010 20 10 10 10 10 10 25

TestCode 300_W

TestNo E300

PQL SPK value

2 5 2525 25

300_W

Units mg/L

SPKRefVai

0000

Units mg/L

SPKRefVai

00

00

Units mg/L

SPKRefVai

0000

Units mg/L

SPKRefVai

00

Test Method: EPA 300.0 1

%REC

101986102102

%REC

103994

98109

%REC

103972102104

%R£C

984123

Piep Date



80808080

Pi ep Date

Analysis Date

120 0120 0120 0120 0

4/23/02


80808080

Piep Date

Analysis Date

120 201120 0 994120 096120 272

4/30/02


80808080

Piep Date

Analysis Date

120 2013120 0 986120 1 015120 2 547

4/23/02


8080

120 0120 0


SeqNo 23005

%RPD RPDLimit Qual

0000

Run ID L IC-1 020423A

SeqNo 20976

%RPD RPDLimit Qual

280 250 25

206 2500368 25


SeqNo 23007

%RPD RPDLimit Qual '

231 25

1 43 250491 25

2 14 25 i


SeqNo 20977

%RPD RPDLimit Qual

00 S i

Qualif icis- ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked

Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits

J This concentiation is consideied an estimate due to LCS failure


Page 2 of 26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F 300 W

ANALYTICAL QC SUMMARY REPORTTest Method: EPA 300.0

Sample ID L0204261-001 AMS

Analyte

Chlonde

Sulfate

Sample I D L0204323-00 1 BMS

Analyte

Chlonde

Sulfate

Sample ID L02042 1 7-00 1 AMS

Analyte

SampType MS

Batch ID R2742

Result

131 6

3659

SampType MS

Batch ID R2993

Result

3970

5130

SampType MS

Batch ID R2993

Result

TestCode 300_W

TestNo E300

PQL SPK value

10 100

10 100

TestCode 300_W

TestNo E300

PQL SPK value

200 2000

200 2000

TestCode 300_W

TestNo E300

PQL SPK value

Units mg/L

SPKRefVai

353

2592

Units mg/L

SPKRefVai

2200

3512

Units mg/L

SPKRefVai

Piep Date



963 80 120 0

107 80 120 0

Prep Date



88 5 80 120 0

809 80 120 0

Prep Date




SeqNo 20978

%RPD RPDLimit Qual

0

0


SeqNo 23008

%RPD RPDLimit Qual

0

0

Run ID L_IC-I_020430A ,

SeqNo 23541

%RPD RPDLimit Qual

Nitrate, as N 2448 1 0 10 1422 103 80 120


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits

J - This concentiation is consideied an estimate due to LCS failure


Page 3 of 26

Date: 16-May-02


Sample ID MB-R1591

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample ID LCS-R1591

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample ID L0204322-003A

Analyte

Aluminum

Barium

Calcium

Iron


SampType MBLK

Batch ID RJU591

Result

NDNDNDNDND

NDNDND

SampType LCS

Batch ID R_R1591

Result

1 041 024

2059

1 1052033

2079

19405161

SampType MS

Batch ID R_R1591

Result

1 15

0969

6461 008

TestCode

TestNo

PQL

0050

00050

0500 1005020

05000050

TestCode

TestNo

PQL

0050

00050

0500 1005020

05000050

TestCode

TestNo

PQL

0050

00050

0500 10

6010WJD

SYV6010B

SPK value

6010W_D

SW6010B

SPK value

11

201

2020

2005

6010W_D

SW6010B

SPK value

11

201

6010W_D

Units mg/L

SPKRefVai

Units mg/L

SPKRefVai

00

0000

00

Units mg/L

SPKRefVai

0099

001958

6180

Test Method: SW 6010B-Diss

Pi cp Date



Piep Date



104 85102 85103 85110 85102 85104 85

97 85103 85

Piep Date

Analysis Date

115 0115 0115 0115 0

115 0115 0

115 0115 0

4/23/02

%REC LowLimit HighLnnit RPD Ref Val

105 75949 75140 75101 75

125 0125 0125 0125 0

Run ID SUB-1591

SeqNo 29920

%RPD RPDLimit

Run ID SUB-1591

SeqNo 29919

%RPD RPDLimit

00000000

Run ID SUB-1591

SeqNo 29996

%RPD RPDLimit

0000

Qual

Qual

Qual

C

Qualifiers: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked


J - This concentiation is consideied an estimate due to LCS fai luie


Page 4 of 26

Date: 16-May-02



Analyte

Magnesium

Potassium

Vanadium


Analyte

Aluminum

Banum

Calcium

Iron

Magnesium

Potassium

Vanadium

Sampl ype MS

Batch ID R_R1591

Result

19341057

05005

SampType MSD

Batch ID R_R1591

Result

1 110951

6491 014192310320497

TestCode

TestNo

PQL

0502 0

00050

TestCode

TestNo

PQL

0050

00050

0500 1005020

00050

6010W_D

SW6010B

SPK value

202005

6010W_D

SW6010B

SPK value

1

1

201

202005

6010W_D

Units mg/L



Prep Date


SPKRefVai

178875

0

Units mg/L

%REC

7791

100

LowLimit

757575

HighLimit

125125125

RPD Ref Val

000

Prep Date


SPKRefVai

0099

001958

6180

178875

0

%REC

10193 1155101

71 5785994

LowLimit

75757575757575

HighLimit

125

125125125125125125

RPD Ref Val

0

000000

Run ID SUB-1591

SeqNo 29996

%RPD RPDLimit

000

Run ID SUB-1591

SeqNo 29923

%RPD RPDLimit

0

000000

Qual

Qual

C

C


Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits

J - This concentiation is consideied an estimate due to LCS f a i l u i e


Page 5 of 26

Date: 16-May-02


Sample ID MB-793

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample ID LCS-793

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample ID R02Q4220-001BMS

Analyte

Barium

Sodium


SampType MBLK

Batch ID R_793

Result

NDNDNDNDNDNDNDND

SampType LCS

Batch ID R_793

Result

1 071 081209

1 11621 1921 26

197

05509

SampType MS

Batch ID R_793

Result

1 461520

TestCode

TestNo

PQL

0050

00050

0500 1005020

05000050

TestCode

TestNo

PQL

0050

00050

0500 100502 0

050

00050

TestCode

TestNo

PQL

00050

050

6010WJT

6010WJT Units mg/L

SW6010B

SPK value SPKRefVai

6010W_T Units mg/L

SW6010B

SPK value SPKRefVai

1 01 0

20 01 0

20 020 0

20 0

05 0

6010\V_T Units mg/L

SW6010B

SPK value SPKRefVai

1 0446

20 1490

Test Method: SW 6010B-Total

Prep Date

Analysis Date

4/23/02

4/24/02


Piep Date

Analysis Date

4/23/02

4/24/02


107 85108 85104 85112 85106 85106 85

98 5 85

110 85

Piep Date

Analysis Date

115 0115 0115 0115 0115 0115 0115 0

115 0

4/23/02

4/24/02


101 75150 75

125 0125 0

Run ID SUB-1616

SeqNo 29974

%RPD RPDLimit Qual

Run ID SUB-1616

SeqNo 29973

%RPD RPDLimit Qual

00000000

Run ID SUB-1616

SeqNo 29975

%RPD RPDLimit Qual

00 C

Qualifiers: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted iccovery limits

J - This concenliation is consideied an estimate due to LCS fai luie


Page 6 of 26

Date; 16-May-02


Sample ID R0204220-001BMSD

Analyte

Barium

Sodium

Sample ID R0204220-001BDUP

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium


SampType MSD

Batch ID R_793

Result

1 452

1490

SampType DUP

Batch ID R_793

Result

NDNDND

NDNDNDNDND

TestCode

TestNo

PQL

00050

050

TestCode

TestNo

PQL

0050

00050

050

0 100502 0

05000050

6010WJT

SW6010B

SPK value

1

20

6010WJT

SW6010B

SPK value

000

00000

6010WJT

Units mg/L

SPKRefVai

0446

1490

Units mg/L

SPKRefVai

000

00000

Test Method: SW 6010B-Total

%REC

101

0

%REC

00000000

Piep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

Piep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

00000000

00000000

RPD Ref Val

00

RPD Rei Val

00

000000

Run ID SUB-1616

SeqNo 29976

%RPD RPDLimit Qual

0

0

Run ID SUB-1616

SeqNo 29972

%RPD RPDLimit Qual

00000000

Quahfiei s: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked

II - MS 01 MSD outside acccpance limits LCS acceptable R - RPD outside accepted recovery limits

] - This concentiation is consideied an estimate due to LCS failure

B - Analytt detected in the associated Method Blank

Page 7 of 26

Date: l6-May-02


Sample ID MB-R1615

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chiomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Sample ID LCS-R1615

Analyte

Antimony

Arsenic

Beiyllium

Cadmium

Chromium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium

Quahficis: ND -

SampType MBLK

Batch ID R_R1615

Result

NDNDNDNDND

NDNDNDNDNDNDNDNDND

SampType LCS

Batch ID R_R1615

Result

0 056280 09946

009871

0 05657

005339

005418

005261

0 05243

005574

0 05439

0 1082

Not Detected at the Repoiting Limit


6020W_D Test Method: SW 6020-Diss I

TestCode 6020 W_D Units mg/L Piep Date

TestNo SW6020 Analysis Date 4/24/02

PQL SPK value SPKRefVai %REC LowLimit HighLimit

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

0 00040

O O O I O

TestCode 6020W_D Units mg/L Piep Date

TestNo SW6020 Analysis Date 4/24/02

PQL SPK value SPKRefVai %REC LowLimit HighLimit

O O O I O 005 0 113 85 115

O O O I O 01 0 995 85 115

O O O I O 01 0 987 85 115

O O O I O 005 0 113 85 115

O O O I O 005 0 107 85 115

O O O I O 005 0 108 85 115

O O O I O 005 0 105 85 115

OOOIO 005 0 105 85 115

O O O I O 005 0 111 85 115

O O O I O 005 0 109 85 115

O O O I O 01 0 108 85 115

C - Unspiked sample >5 times the amount spiked

Run ID SUB-1615

SeqNo 29928

RPD Ref Val %RPD RPDLimit Qual

<

Run ID SUB-1615

SeqNo 29927


0 00 00 00 00 0

0 0

0 0

0 00 0

0 0

0 0


Jl - MS or MSD outside acccpance limits LCS acceptable R - RPD outside accepted recovery limits

J - This concentialion is consideied an estimate due to LCS fa i lu ie

Page 8 of 26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322

Project: GII-3F

Sample ID LCS-R1615

Analyte

Silver

Thallium

Zinc


Analyte

Antimony

Arsenic

Beiylhum

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silvci

Thal l ium

Zinc


Analyte

Antimony

Arsenic

Beiylhum

SampType LCS

Batch ID R_R1615

Result

0 111

0 05628

005417

SampType MS

Batch ID R_R1615

Result

0 04629

0 1462

0 1402

00442

00634

005759

006179

004691

3573

0 06069

0 1298

0 1021

005421

0223

Samp I ype MSD

Batch ID R_R1615

Result

0 05058

0 1459

0 1423

TestCode

TestNo

PQL

O O O I O

0 00040

O O O I O

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

O O O I OO O O I O

O O O I O

0 00040

O O O I O

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

6020W_D

SW6020

SPK value

0 1

005

005

6020W_D

SW6020

SPK value

005

0 1

0 1

005

005

005

005

005

005

005

0 1

0 1

005

005

6020\V_D

SW6020

SPK value

005

0 1

0 1

6020W_D

Units mg/L

SPKRefVai

0

0

0

Units mg/L

SPKRefVai

000135

00376

0

00 00384

0 00277

000489

0

4014

0 00706

0 00596

0

0

0 104

Units mg/L

SPKRefVai

000135

00376

0

ANALYTICAL QC SUMMARY REPORTTest Method: SW 6020-Diss

%REC

111113

108

%REC

899

109

140

884

119

110

114

93 8

-882

107

124

102

108

238

%REC

985

108

142

Piep Date


LowLimit HighLimit

85

85

85

Pi ep Date

Analysis Date

115

115

115

4/24/02

LowLimit HighLimit

75

75

75

75

75

75

75

75

75

75

75

75

75

75

Piep Date

Analysis Date

125

125

125

125

125

125

125

125

125

125

125

125

125

125

4/24/02

LowLimit HighLimit

RPD Ref Val

0

0

0

RPD Ref Val

0

0

0

0

0000000000

RPD Ref Val

000

Run ID SUB-1615

SeqNo 29927

%RPD RPDLimit

0

0

0

Run ID SUB-1615

SeqNo 29929

%RPD RPDI unit

0

0

0

00

0

0

0

0

0

0

0

0

0

Run ID SUB-1615

SeqNo 29930

%RPD RPDLimit

0

0

0

Qual

Qual

Jl

C

Jl

Qual

Jl


Jl - MS or MSD outside accepance l imits LCS acceptable R- RPD outside accepted lecovery limits

J - I his conccnlialion is consideied an estimate due to LCS failure


Page 9 of 26

Date: !6-May-02

CLIENT: RSSN

Work Order: L0204322Project: GH-3F


Analyte

Cadmium

Cluomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


Analyte

Antimony

Arsenic

Beiylhum

Cadmium

Chiomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thall ium

Zinc


SampType MSD

Batch ID R_R1615

Result

00441

0 06237

00572

005881

004616

3581

006051

0 1274

0 101

0 05398

01804

SampType DUP

Batch ID R_R1615

Result

ND0 03632

NDND

0 00466

0 00294

0 00568

ND407

0 00724

NDNDND

0 108

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

O O O I O

O O O I OOOOIOO O O I O

0 00040

O O O I O

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

O O O I O

O O O I O

O O O I O

O O O I O

0 00040

O O O I O

6020W_D

SW6020

SPK value

0050050050050050050050 1

0 1

005005

6020W_D

SW6020

SPK value

00000000000000

6020W_D

Units mg/L

SPKRefVai

00 00384

0 00277

0 00489

04014

0 00706

0 00596

00

0 104

Units mg/L

SPKRefVai

0000

0

000000000

Test Method: SW 6020-Diss

%REC

88 2

117109

108923

-866

107121101108153

%REC

00000

0000000

00

Prep Date


LowLimit HighLimit

Piep Date


LowLimit HighLimit

00000

0000000

00

00000

000000000

RPD Ref Val

00000000000

RPD Ref Val

000000000

00000

Run ID SUB-1615

SeqNo 29930

%RPD RPDLimit Qual

0

00000 C

00000 Jl

Run ID SUB-1615

SeqNo 29926

%RPD RPDLimit Qual

00000000000000

— rQualifiers: ND - Not Detected at the Repotting Limit C Unspiked sample >5 times the amount spiked

Jl - MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted lecoveiy limits

J - This concentration is consideied an estimate due to LCS fai luie


Page 10 of 26

Date: 16-May-02

r


Sample ID MB-795

Analyte

AntimonyArsenic

BerylliumCadmiumChromiumCobaltCopperLeadManganeseNickel

SeleniumSilverThalliumZinc

Sample ID LCS-795

Analyte

AntimonyArsenicBeiyl l iumCadmium

Chromium

CobaltCopperLeadManganeseNickelSelenium

SampType MBLK

Batch ID R_795

Result

NDNDNDNDNDNDNDNDNDND

NDNDNDND

SampType LCS

Batch ID R_795

Result

0 056950 094 1 5

0 1524

0051900537

005475005670054500494

0055400956

6020WJT

TestCode 6020WJT Units mg/L

TestNo SW6020


0005000050000500005000050000500005000050000500005000050000500005000050

TestCode 6020WJT Units mg/L

TestNo SW6020


0 0050 0 05 00 0050 0 1 00 0050 0 1 00 0050 0 05 0

0 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 05 00 0050 0 1 0


Pi ep Date

Analysis Date

Test Method: SW 6020-Total

4/23/02 Run ID SUB-1627

4/24/02 SeqNo 29953


Piep Date

Analysis Date

4/23/02 Run ID SUB-1627

4/24/02 SeqNo 29952


114 85942 85152 85

104 85107 85

110 85113 85109 85

988 85

111 8595 6 85

115 0 0115 0 0115 0 0

115 0 0115 0 0115 0 0115 0 0115 0 0115 0 0115 0 0115 0 0


Jl MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted lecoveiy limits

} - This concentiation is consideied an estimate due to LCS fa i lu ie


Page 11 of 26

Date: 16-May-D2


Sample ID LCS-795

Analyte

Silver

Thallium

Zinc

Sample ID R0204208-001BMS

Analyte

Antimony

Arsenic

Beiyllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silvei

Thallium

Zinc


Analyte

Antimony

Aisemc

Beiylhum


SampType LCS

Batch ID R_795

Result

0 1364

00547

0 04785

SampType MS

Batch ID R_795

Result

00629

0 1046

0 1637

0 05525

0 05645

0059

006515

005685

00643

0 06255

0 1049

0 1384

0 06405

0 1304

SampType MSD

Batch ID R_795

Result

0 05965

0 0966

0 1534

TestCode

TestNo

6020WJT

SW6020

PQL SPK value

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

0 1

005

005

6020WJT

SW6020

SPK value

005

0 1

0 1

005

005

005

005

005

005

005

0 1

01

005

005

6020W_T

SVV6020

SPK value

005

0 1

0 1

6020W_T

Units mg/L

SPKRefVai

0

0

0

Units mg/L

SPKRefVai

0

0

0

0

00055

0

0 00675

0

00105

0

0

0

0

008105

Units mg/L

SPKRefVai

0

0

0

Test Method: SW 6020-TotaI

%REC

136

109

957

%REC

126

105

164

110

102

118

117

114

108

125

105

138

128

987

%REC

119

966

153

Piep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

85

85

85

Piep Date

Analysis Date

115

115

115

4/23/02

4/24/02

LowLimit HighLimit

75

75

75

75

75

75

75

75

75

75

75

75

75

75

Pi ep Date

Analysis Date

125

125

125

125

125

125

125

125

125

125

125

125

125

125

4/23/02

4/24/02

LowLimit HighLimit

RPD Ref Val

0

0

0

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

0

0

0

RPD Ref Val

0

0

0

Run ID SUB-1627

SeqNo 29952

%RPD RPDLimit Qual '

0

0

0

Run ID SUB-1627

SeqNo 29954

%RPD RPDLimit Qual

0

0

0 Jl

0

0

0

0

0

0

0

0

0 II

0 Jl

0

Run ID SUB-1627

SeqNo 29955

%RPD RPDLimit Qual

000 Jl



J - This concentiation is consideied an estimate due to LCS failuie


Page 12 of 26

Date: 16-May-02



Analyte

Cadmium

Chiomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


Analyte

Antimony

Arsenic

BeiyHium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc


SampType MSD

Batch ID R_795

Result

00516

005325

0 05525

0 06085

00528

0 05925

0 05675

0 1026

0 1308

005930 1252

SampType DUP

Batch ID R_795

Result

ND

ND

ND

NDNDND

00061ND

00094NDNDNDND

0 07405

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

0005000050

000500005000050

00050

00050

00050

6020WJT

SW6020

SPK value

005

005

005

005

005

005

005

0 1

01

005

005

6020W_T

SW6020

SPK value

0

0

0

0

0

0

0

0

0

0

0

0

0

0

6020WJT

Units mg/L

SPKRefVai

0

00055

0

0 00675

0

00105

0

0

0

0

008105

Units mg/L

SPKRefVai

0

0

0

0

0

0

0

0

0

0

0

0

0

0


%REC

103

955

110

108

106

975

114

103

131

119

884

%REC

0

0

0

0

0

0

0

0

0

0

0

0

0

0

Pi ep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

Piep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

0

0

0

Run ID SUB-1627

SeqNo 29955

%RPD RPDLimit Qual

0000000

o0 Jl

00

Run ID SUB-1627

SeqNo 29951

%RPD RPDLimit Qual

0

0

0

0

0

0|

00000000


Jl - MS or MSD oukidc accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits


B - Analyte detected in the assouated Method Blank

Page 13 of 26

Date: 16-May-02


Sample ID Method Blank 02

Analyte

1 ,1 ,2-Ti ichloroti ifluoroethane

MTBE

Acetone

Benzene

Bi omobenzene

Biomochlotomethane

Bi omodichloromethane

Biomoform

Bromomethane

2-Butanone

n-Butylbcnzene

sec-Butylbenzene

tei t-Butylbenzene

Carbon disulfide

Carbon tetrachlonde

ChlorobenzeneChloroethane

2-Chloioethyl vinyl etheiChloioform

Chloiome thane

2-Chloiotoluene

4-Chloiotolucne

Dibi omochloi omcthane

1 ,2-Dibi omo-3-chloropi opane

1 ,2-Dibiomoethane

Dibi omome thane

1 ,2-Dichloi obenzene



Dichloiodifluoiomethane

Qualifiers: N D - N o t

SampType MBLK

Batch ID R2684

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDND

ND

NDNDND

Detected at the Reporting Limit


8260_W Test Method: SW8260B

TestCode 8260_W Units ng/L Piep Date Run ID L_VOAMS-2_020423A



505025505050505050255050505050

50505050505050

505050

50

50505050

C - Unspiked sample >5 times the amount spiked B - Analyte detected in the associated Method Blank

Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits

J - This concentiation is consideied an estimate due to LCS fa i lu ie

Page 14 of 26

Date: 16-May-02


ANALYTICAL QC SUMMARY REPORT8260 W Test Method: SW8260B

Sample ID Method Blank 02 SampType MBLK

Analyte

Batch ID R2684

Result

TestCode 8260_W Units ug/L

TestNo SW8260B


Prep Date



Run ID L_VOAMS-2_020423A '

SeqNo 20642

%RPD RPDLimit Qual

1,1-Dichloioethane1,2-Dichloi oethane1,1-Dichloioethene

cis-1,2-Dichloroetheneti ans-1,2-Dichloi oethene1,2-Dichloropropane1,3-Dichloropropane2,2-Dichloropropane1,1-Dichloropropenecis-l,3-Dichloropropene

trans-1,3-DichloiopropcneEthylbcnzeneHexachloi obutadiene2-HexanonelodomethaneIsopropylbenzenep-IsopiopyltolueneMethylene chlonde4-Methyl-2-pentanoneNaphthalene

n-PiopylbenzeneStyiene

1,1,2,2-Teti achloi oethaneTetiachloi oetheneToluene

1,2,3-Ti ichloiobenzcne1,2,4-Tnchloiobenzene

1,1,2-Tnchloi oethaneTnchloroctheneTiichlorofluoiomethane

NDND

NDNDNDNDNDNDNDND

NDNDND

NDNDNDNDNDNDND

NDND

NDNDNDNDNDNDNDND

5050

505050

5050

505050505050255050505025105050

5050

505050505050


11 - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecoveiy limits



Page 15 of 26

Date: !6-May-02



Analyte



1 ,3,5-Tnmethylbenzeiie

Vinyl acetate

Vinyl chlonde

o-Xylene

m,p-Xylene


Surr Toluene-d8

Surr 4-Biomofluorobenzene

Sample ID Vstd050CCV02042

Analyte

Acetone

Benzene

Bi omoform

Biomomethane

Chlorobenzene

Chlorofoim

Chloiomethane

Dichloiodifluoiornethane

1,1-Dichloi oethane

1,1-Dichloroethene

1,2-Dichloropiopane

Clhylbcnzene

1 , 1 ,2 ,2 -Teti achloi oethane

Toluene

Tnchloi oethene

SampType MBLK

Batch ID R2684

Result

NDNDNDNDNDNDND

4804

5357

4476

SampType LCS

Batch ID R2684

Result

37814857

3986

78 3451 774996

6859

6665249

4887

49 165039

5234

4647

47 15

TestCode

TestNo

PQL

5 050505050

5010

505050

TestCode

TestNo

PQL

2550505050505050505 05050

505050

8260_W

SW8260B

SPK value

505050

8260_W

SW8260B

SPK value

505050505050505050

505050505050

8260_W

Units ug/L

SPKRefVai

000

Units ug/L

SPK Ref Val

000000000000

000


Test Method: SW8260B

%REC

96 1107

895

%REC

75697 1

797157104

999137133105

97798 3

101105

929943

Prep Date


LowLimit HighLimit

80808562

Piep Date

Analysis Date

120119139

4/23/02

LowLimit HighLimit

7070707070807070708080

80708070

130130130130130120130130130

120120120

130120130

RPD Ref Val

000

RPD Ref Val

000000000000000

Run ID L_VOAMS-2_020423A

SeqNo 20642

%RPD RPDLimit Qual

i

000


SeqNo 20645

%RPD RPDLimit Qual

00

00 S

000 S

0 S

0000000

Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked


J - This concentiatlon is consideied an estimate due to LCS fai luie


Page 16 of 26

Date: 16-May-02



Analyte

Vinyl chlonde

Sun Dibiomofluoiomethanc

Sun Toluene-d8

SUIT 4-Bromofluorobcnzene

Sample ID L0204322-001A MS

Analyte

Acetone

BenzeneBromomethane

Chlorobenzene

Chloiome thane

Dichloiodifluoiomethane

1,1-Dichloroethene

Toluene

Trichloioethene

Vinyl chlonde

Sun Dibiomofluoiomethane

Sun Toluene-d8

Sun 4-Biomofluorobcnzene

Sample ID L0204322-001 A MSD

Analyte

Acetone

Benzene

Bromomethane


SampType LCS

Batch ID R2684

Result

58 1744955268

42 1

SampType MS

Batch ID R2684

Result

51 335436

75.95366

8647

8365

58 155299

52 186921

46695546

4873

SampType MSD

Batch ID R2684

Result

4805

4938

67 13

Qualifiers: ND - Not Detected at the Repoiting Limit

TestCode 8260_W

TestNo SW8260B

PQL SPK value

50 5050 5050 5050 50

TestCode 8260_W

TestNo SW8260B

PQL SPK value

25 5050 505.0 5050 5050 5050 5050 5050 5050 5050 5050 5050 50

50 50

TestCode 8260_W

TestNo SW8260B

PQL SPK value

25 5050 5050 50

8260_W

Units ng/L

SPKRefVai

0000

Units ug/L

SPKRefVai

0000000000000

Units ug/L

SPKRefVai

00

0

C - Unspiked sample >5 times


Piep Date


%REC LowLimit HighLimit

116 80 120899 80 120105 808 119

842 562 139

Piep Date



103 70 130109 70 130152 70 130107 70 130173 70 130167 70 130116 80 120106 80 120104 70 130138 80 120

93 4 92 6 108111 957 112

97 5 85 3 104

Pi ep Date



96 1 70 130988 70 130

134 70 130

the amount spiked

RPD Ref Val

0000

RPD Ref Val

0000000000000

RPD Ref Val

51 3354 36

759


SeqNo 20645

%RPD RPDLimit Qual

0000


SeqNo 20643

%RPD RPDLimit Qual

000 S00 S

0 S

0000 S

00

o


SeqNo 20644

%RPD RPDLimit Qual

660 25960 25123 25 S


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recovery limits


Page 17 of 26

Date: !6-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F 8260 W

ANALYTICAL QC SUMMARY REPORTTest Method: SW8260B

Sample ID L0204322-001A MSD SampType MSD

Batch ID R2684

Analyte

Chlorobenzene

ChloiomethaneDichlorodifluoiomethane

1 , 1 -Dichloi oethene

Toluene

Tnchloi oethene

Vinyl chlorideSurr Dibiomofluoiomethane

Surr Toluene-d8Sun 4-Bromofluorobenzene

Result

4966

6853

7924

5277

47 214778

5748

4707

5357

4505

TestCode 8260_W Units ug/L Prep Date

TestNo SW8260B

PQL

50505050505050505050

SPK value

5050505050

5050505050

SPKRefVai

0000000000

%REC

993137158106

944956115

94 1

10790 1


LowLimit

70707080807080

92 6

957853

HighLimit

130130130120120130

120108112104

RPD Ref Val

53 668647

8365

581552 9952 186921

000


SeqNo 20644

%RPD

77423 154197011 5880185

0

00

RPDLimit Qual ,

2525 S25 S

2525

2525000


Jl - MS or MSD outside accepance l imits LCS acceptable R - RPD outside accepted lecoveiy limits



Page 18 of 26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322Project: GII-3F ALK W

ANALYTICAL QC SUMMARY REPORTTest Method: SM2320 B

Sample ID MB-R2983

Analyte

Alkalinity, Bicaibonate (As CaCO3)

Alkalinity, Caibonate (As CaCO3)Hydioxide(AsCaCO3)


Sample ID LCS-R2983

Analyte



Analyte


Sample ID L0204322-001BDUP

Analyte


Alkalinity, Caibonate (As CaCO3)

Hydioxide(AsCaCO3)


SampType MBLK

Batch ID R2983

Result

NDNDNDND

SampType LCS

Batch ID R2983

Result

144

SampType LCSD

Batch ID R2983

Result

122

SampType DUP

Batch ID R2983

Result

ND

74ND

74

TestCode

TestNo

PQL

25252525

TestCode

TestNo

PQL

25

TestCode

TestNo

PQL

25

TestCode

TestNo

PQL

252525

25

ALK_W

M2320 B

SPK value

ALK_W

M2320 B

SPK value

125

ALK_W

M2320 B

SPK value

125

ALK_W

M2320 B

SPK value

000

0

Units mg/L

SPKRefVai

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

0

00

0

Prep Date



Prep Date



115 80

Pi ep Date

Analysis Date

120 0

4/29/02


976 80

Prep Date

Analysis Date

120 144

4/29/02

%RBC LowLimit HighLimit RPD Rei Val

0 0

0 00 0

0 0

0 00 750 0

0 75

Run ID L_AT1TR-1_020429A '

SeqNo 22904

%RPD RPDLimit Qual j

Run ID L_ATJTR-1_020429A

SeqNo 22903

%RPD RPDLimit Qual

0


SeqNo 22906

%RPD RPDLimit Qual

165 25

Run ID L_A1 ITR-1_020429A

SeqNo 22905

%RPD RPDLimit Qual

0 101 34 10

0 .10

1 34 10


II - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits

I - This concentiation is consideied an estimate due to LCS failuie


Page 19 of 2 6

Date: 16-May-02

CLIENT: RSSN

Work Order: L0204322Project: GH-3F COD

ANALYTICAL QC SUMMARY REPORTTest Method: SM5520 D

Sample ID MB-R2949

Analyte


SampType MBLK

Batch ID R2949

Result

ND


TestNo M5220C


10

Piep Date Run ID L_WC_020429C


%R£C LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

Sample ID LCS-R2949

Analyte



Analyte

SampType

Batch ID

SampType

Batch ID

LCS

R2949

Result

533

LCSD

R2949

Result

TestCode

TestNo

PQL

10

TestCode

TestNo

PQL

COD

M5220 C

SPK value

500

COD

M5220 C

SPK value

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

Pi ep Date



107 80

Prep Date

Analysis Date

120 0

4/29/02


Run ID

SeqNo

L_WC_020429C

22626

%RPD

Run ID

SeqNo

0

L_

RPDLimit

\VC_020429C

Qual

22630

%RPD RPDLimit Qual

Chemical Oxygen Demand 503 10 500 101 120 533 579 15

Sample ID L0204310-001BMS SampType MS

Analyte

Batch ID R2949

Result


TestNo M5220C


Prep Date



Run ID L WC 020429C

SeqNo 22628

%RPD RPDLimit Qual

Chemical Oxygen Demand 554 10 4625 75 104 70 130

Sample ID L0204310-001BMSD SampType MSD TestCode COD Units mg/L Piep Date Run ID L_WC_020429C '

Analyte

Batch ID R2949 TestNo M5220 C Analysis Date 4/29/02 SeqNo 22629

Result PQL SPK value SPKRefVai %R£C LowLimit HighLimit RPD Ref Val %RPD RPDI.imit Qual

Chemical Oxygen Demand 546 10 462 5 75 102 70 130 546 25

Qualifieis: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked


1 - This concentiation is consideied an estimate due to LCS fa i l u i e


Page 20 of 26

Date: 16-May-02

T

CLIENT: RSSN

Work Order: L0204322Project: GH-3F HG 7470 D


Sample ID MB-799

Analyte

SampType

Batch ID

MBLK

R_799

Result

TestCode

TestNo

PQL

HG_7470_D

SW7470

SPK value

Units mg/L

SPKRefVai

Piep Date

Analysis Date

%REC LowLimit Hi

4/24/02

4/24/02

ghLimit RPD Ref Val

Run ID

SeqNo

SUB-1625

29941

%RPD RPDLimit Qual

Meicuiy ND 0 00020

Sample ID LCS-799

Analyte

Meicury


Analyte

Mercury

SampType LCS

Batch ID R_799

Result

0 00499

SampType MS

Batch ID R_799

Result

000521

TestCode HG_7470_D

TestNo S\\7470

PQL SPK value

0 00020 0 005

TestCode HG_7470_D

TestNo SW7470

PQL SPK value

0 00020 0 005

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

0

Prep Date

Analysis Date

4/24/02

4/24/02


998 85

Pi ep Date

Analysis Date

115 0

4/24/02

4/24/02


104 85 115 0

Run ID SUB-1625

SeqNo 29940

%RPD RPDLimit

0

Run ID SUB-1625

SeqNo 29942

%RPD RPDLimit

0

Qual

Qual


Analyte

SampType

Batch ID

MS

R_799

Result

TestCode

TestNo

PQL

HG_7470.

SW7470

SPK value

_D Units mg/L

SPKRefVai

Piep Date

Analysis Date

4/24/02

4/24/02


Run ID

SeqNo

SUB-1625

30020

%RPD RPDLimit

]

Qual

Meicuty 000521 0 00020 0005 104 85 115

Sample ID L02043IO-003A

Analyte

SampType

Batch ID

MSD

R_799

Result

TestCode

TestNo

PQL

HG_7470_D

SW7470

SPK value

Units mg/L

SPKRefVai

Piep Date

Analysis Date

4/24/02

4/24/02

%R£C LowLimit HighLimit RPD Ref Val

Run ID

SeqNo

%RJ

SUB-1625

29943

JD RPDLimit Qual

Meicuiy 00051 0 00020 0005 102


Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted lecoveiy limits

J - This concent!ation is consideied an estimate due to LCS failure


Page 21 of 26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F HG 7470 D


Sample ID. R0204242-003AMSD SampType. MSD TestCode: HG_7470_D Units: mg/L Prep Date: 4/24/02 Run ID: SUB-1625

Analyte

Batch ID: R_799 TestNo: SW7470 Analysis Date. 4/24/02 SeqNo: 30021

Result PQL SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

Mercury 0.0051 0.00020 0.005 102


Jl - MS or MSD outside accepance limits. LCS acceptable. R - RPD outside accepted recovery limits

J - This concentration is considered an estimate due to LCS failure.


Page 22 of 26

Date: I6-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F HG 7470 T

ANALYTICAL QC SUMMARY REPORTTest Method: SW 7470-Total

Sample ID MB-800

Analyte

SampType

Batch ID

MBLK

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

4/24/02

4/24/02


Run ID

SeqNo

SUB-1626

29947

%RPD RPDLimit Qual

Meicury ND 0 00020

Sample ID LCS-800

Analyte

Mercury

Samp Type LCS TestCode HG_7470_T Units mg/L Prep Date 4/24/02 Run ID SUB-1626

Batch ID R_800 TestNo SW7470 Analysis Date 4/24/02 SeqNo 29946

Result PQL SPK value SPKRefVai %R£C LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

000518 000020 0005 0 104 85 115 0 0


Analyte

SampType

Batch ID

MS

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

4/24/02

4/24/02


Run ID

SeqNo

SUB-1626

29948

%RPD RPDLimit Qual

Mercury 000541 0 00020 0005 108 85 115


Analyte

SampType

Batch ID

MSD

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

4/24/02

4/24/02


Run ID

SeqNo

%RJ

SUB-1626

29949

'D RPDLimit

!

Qual

Meicuiy 000539 0 00020 0005 108


Analyte

SampType

Batch ID

DUP

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Pi ep Date

Analysis Date

4/24/02

4/24/02


Run ID

SeqNo

SUB-1626

29945

%RPD RPDLimit Qual

Meicuiy ND 0 00020



J - This concentiation is considcicd an estimate due to LCS failure


Page 23 of 26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F NH3-N W

ANALYTICAL QC SUMMARY REPORTTest Method: SM4500-NII3 C

Sample ID MB-R2996

Analyte

Ammonia, as N

SampType MBLK

Batch ID R2996

Result

ND


TestNo M4500-NH3 C


030

Prep Date Run ID L_\VC_020430A



Sample ID LCS-R2996

Analyte

Ammonia, as N


Analyte

SampType

Batch ID

SampType

Batch ID

LCS

R2996

Result

1 008

LCSD

R2996

Result

TestCode

TestNo

PQL

030

TestCode

TestNo

PQL

NH3-NJW

M4500-NH3

SPK value

1

NH3-N_W

M4500-NH3

SPK value

Units mg/L

C

SPKRefVai

0

Units mg/L

C

SPKRefVai

Piep

Analysis

Date

Date 4/30/02


101 83

Piep

Analysis

9

Date

Date

117 0

4/30/02


Run ID

SeqNo

L_WC_020430A

23034

%RPD RPDLimit

Run ID

SeqNo

0

L_WC_020430A

23037

%RPD RPDLimit

Qual

Qual

Ammonia, as N 101 030 101 839 117 1 008 0 198 25


Analyte

Ammonia, as N

SampType MS TestCode NH3-NJVY Units mg/L Prep Date Run ID L_WC_020430A

Batch ID R2996 TestNo M4500-NH3 C Analysis Date 4/30/02 SeqNo 23036 ,


1 12 030 1 0 112 764 124 0 0



j - This concentiation is consideied an estimate due to LCS fa i lu ie


Page 24 of 26

Date: 16-May-02

CLIENT: RSSNWork Order: L0204322Project: GH-3F SULF W


Test Method: SM4500-S D


Analyte

Batch ID R2855

Result


TestNo M4500-S D


Piep

Analysis

Date

Date 4/26/02



SeqNo 21795

%RPD RPDLimit Qual

Sulfide ND 0030

Sample ID LCS-R2855

Analyte

Sulfide


Analyte

SampType

Batch ID

SampType

Batch ID

LCS

R2855

Result

0 107

LCSD

R2855

Result

TestCode

TestNo

PQL

0030

TestCode

TestNo

PQL

SULF_W

M4500-S D

SPK value

0 107

SULF_W

M4500-S D

SPK value

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

Piep Date



100 80

Prep Date

Analysis Date

120 0

4/26/02


Run ID

SeqNo

L_SPEC-2_020426A

21794

%RPD RPDLimit

Run ID

SeqNo

%R

0

Qual

L_SPEC-2_020426A '

21796

>D RPDLimit Qual

Sulfide 0 111 0030 0 107 104 80 120 0 107 367 25

Sample ID L0204310-001BMS SampType MS TestCode SULF_W Units mg/L Prep Date Run ID L_SPEC-2_020426A

Analyte

Sulfide

Batch ID R2855 TestNo M4500-S D Analysis Date 4/26/02 SeqNo 21797


O H 4 0030 0107 0 107 70 130 0 0

Sample ID L0204310-

Analyte

001BMSD SampType MSD

Batch ID R2855

Result

TestCode SULFJW Units mg/L

TestNo M4500-SD


Piep

Analysis

Date

Date 4/26/02


Run ID L_SI'EC-2_020426A

SeqNo 21798

%R1'D RPDLimit Qual }

Sulfide 0 109 0030 0 107 102 70 130 0 114 4 48 25



J - This concent!ation is consideied an estimate due to LCS failuie


Page 25 of 26

Date: 16-May-02

CLIENT: RSSN

Work Order: L0204322Project: GII-3F TDS W

ANALYTICAL QC SUMMARY REPORTTest Method: SM2540 C

Sample ID MB-R2814

Analyte

SampType MBLK

Batch ID R2814

Result

TestCode TDS_W Units mg/L

TestNo E160.1


Prep Date



Run ID L_WC_020424I

SeqNo 21508

%RPD RPDLimit Qual

Total Dissolved Solids ND 150

Sample ID LCS-R2814

Analyte

SampType

Batch ID

LCS

R2814

Result

TestCode

TestNo

PQL

TDS_W

E160.1

SPK value

Units mg/L

SPKRefVai

Piep Date



Run ID

SeqNo

L_WC_020424I

21507

%RPD RPDLimit Qual

Total Dissolved Solids 967 150 1000 967 80 120

Sample ID L0204356-003EDUP SampType DUP

Analyte

Batch ID R2814

Result


TestNo E160.1


Prep Date



Run ID L_\VC_020424I

SeqNo 21509

%RPD RPDLimit

1

Qual

Total Dissolved Solids 346 150 367 589 25


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccovery limits

J - This concentration is consideied an estimate due to LCS f a i l u i e


Page 26 of 26

Date: 16-May-02



CHAIN OF CUSTODY NEL Work Order: LQ L& *f

Project Name

Phoenix Division • 3201 So. 35th Street, Suite B6 • Phoenix, Arizona 85034602-437-0099 • Fax. 602-437-2225 • 888-238-2514

Attention

Address.


Time/DateSampled Customer Sample Identification

N.E.LIdentification

'urchase Order Number

Project Number

Sampled By

Remarks

/-J2-03.

Y

oV

Custody Seal intact? YCondition

Box#1 DW - Drinking Water SD - SolidWW - Waste Water AQ - AqueousOL • Oil/Organic Liquid A - Air

Box #2 A HCIB HNO3

C HjSO,D NaOH

E Ice Only IF Other IG Not PreserVW

Relinquished by (Print) Date/Time Received by (Print) Date/Time/

The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss, damage, resampling costs and/or qualified data related to samples not received In good condition,including adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptance<jfNEL Standard List Pnce5 for all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time will be confirmed via Sample Confirmation transmitted to the fax number provided above

ORIGINAL

NEL LABORATORIESReno • Las VegasPhoenix • Burbank

Las Vegas Division4208 Arcata Way, Suite A • Las Vegas, NV 89030

(702) 657-1010 • Fax: (702) 657-15771-888-368-3282

Nick SainesRSSN7900 Vegas Valley DriveLas Vegas. NV 89142

TEL: 702-431-3020

RE Project: DGH-3F

Dear Nick Saines:

Order No.: L0204323




?/Uu--a^-vy// .r-'-v y :Stan VaiiWagefien JLaboratory Manager


"V


Certified

Date

Corporate Office & Reno Division • 1030 Matley Lane • Reno, NV 89502 • (702) 348-2522

NEL LABORATORIES

NEL Laboratories, Las Vegas Date:

CLIENT: RSSN

Project: DGH-3F CASE NARRATIVELab Order: L0204323




EPA 8260: Samples were evaluated for the presence of Acrylonitrile and trans-l,4-Dichloro-2-butene.Neither of these two compounds were present in the samples submitted in this work-order at or above5ppb.

Page 1 of 1

NEL LABORATORIES

CLIENT: RSSN

PROJECTED: DGH-3F

PROJECT #: DGH-3F

MATRLX: AQUEOUS

Parameter

Acetone

Benzene

Bromobenzene

Bromochloromethane

Bromodichloiomethane

Bromoform

Bromomethane

2-Butanone

n-Butylbenzene

sec-Butylbenzene

tert-Butylbenzene

Caibon disulfide

Carbon tetrachlonde

Chloiobenzene

Chloroethane

2-Chloroethyl vinyl ethei

Chloroform

Chloromethane

2-Chlorotoluene

4-Chlorotoluene



1 ,2-Dibromoethane

Dibromomethane

1 ,2-Oichlorobenzene




1,1-Dichloroethaiie

1 ,2-Dichloroethane

1,1-Dichloroethene

cis-l,2-Dichloroethene




2,2-Dichloropropane




Ethylbenzene

Hexachlorobutadiene

2-Hexanone

lodomethane

Isopropylbenzene

ND - Not Detected at the Reporting I imit


Date: 16-May~02

Result Unit

ND ug/L

ND ug/L

ND ng/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND p.g/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND (ig/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND ug/L

ND (ig/L

ND Mg/L

ND ug/L

ND ug/L

ND (ig/L

ND ug/L

ND ug/L

ND ng/L

ND ug/L

ND (ig/L

ND ug/L

ReportingLimit

2550505050505025505050505050505050505050505050505050505050505050505050505050505050255050

CLIENT ED: DGH-3F


NEL SAMPLE ID: L0204323

DF Method Prep Date

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

-001A

Analyzed

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04'23/02

04/23/02

04/23/02

04/23/02

04/23/02

04'23'02

04/23/02

04/23/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-I V

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV


S - Spike Recovery outside accepted reco\ ery limits


NEL LABORATORIES

CLIENT: RSSN

PROJECTED: DGH-3F

PROJECTS: DGH-3F

MATRIX: AQUEOUS

Parameter

p-Isopropyltoluene

Methylene chlonde


MTBE

Naphthalene

n-Propylbenzene

Styrene


1,1,2,2-Tetrachloroethane

Tetrachloroethene

Toluene1 ,2,3-Tnchlorobenzene

1 ,2,4-Tnchloi obenzene



Tnchloroethene

1 nchlorofluoromethane

1 ,1 ,2-Tnchlorotnfluoroethane

1 ,2 ,3 -Tuchl oropropane


1 ,3 ,5-Tnmethylbenzen e

Vinyl acetate

Vinyl chlonde

o-Xylene

m,p-Xylene


Surr: Toluene-d8


Result


10989.3

Unit

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

ug/L

%REC

%REC

%REC

ReportingLimit

50502550505050505050505050505050505050505050505010

92 6-108

957-112

85 3-104

CLIENT ED: DGH-3F



DF Method

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

1 SW8260B

Prep Date Analyzed

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

Analyst

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV

DRM-LV



Date: 16-May-02




NEL LABORATORIES

CLIENT:

PROJECT ID:

PROJECTS:

MATRIX:

RSSN

DGH-3F

DGH-3F

AQUEOUS

CLEENTD3: DGH-3F



ReportingParameter Result Unit Limit DF Method

Chloride 2200 mg/L 200 2000 EPA 3000

Nitrate, as N ND mg/L 25 25 EPA 3000

Nitrite, as N ND mg/L 25 25 EPA 300 0

Sulfate 3500 mg/L 200 2000 EPA 300 0

Alkalinity, Bicarbonate (As CaC03) ND mg/L 25 1 SM2320B

Alkalinity, Carbonate (As CaC03) 75 mg/L 25 1 SM2320 B

Hydroxide (As CaC03) ND mg/L 25 1 SM2320B

Alkalinity, Total (As CaCO3) 75 mg/L 25 1 SM2320B

Chemical Ox> gen Demand 78 mg/L 10 1 SM5520 D

Ammonia, as N ND mg/L 030 1 SM4500-NH3

Sulfide ND mg/L 0030 1 SM4500-S D

Total Dissolved Solids 6990 mg/L 150 10 SM2540 C

Prep Date Analyzed

04/30/02

04/23/02

04/23/02

04/30/02

04/29/02

04/29/02

04/29/02

04/29/02

04/29/02

04/30/02

04/26/02

04/24/02

ND - Not Detected at the Reporting I imit


Date: 16-May-02




NEL LABORATORIES

CLIENT: RSSN

PROJECT ID: DGH-3F

PROJECT #: DGH-3F

MATRIX: AQUEOUS

Parameter

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

3.2

0.047

6902.2

210

110

1800

0.0088

ND0.021

ND

ND0.011

0.0025

0.014

00011

0.049

00088

NDNDND0.14

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0050

00050

0200 100202050

00050

O O O I O

O O O I O

OOOIO

OOOIO

O O O I O

O O O I O

OOOIO

OOOIO

OOOIO

OOOIO

OOOIO

OOOIO

0 00040

OOOIO

0 00020

CLIENT ED:

DATE SAMPLED:

NEL SAMPLE ID:

DF

lll111

1001111111111111111

Method

SW6010B-To

SW 6010B-To

SW6010B-To

SW 6010B-TO

SW6010B-To

SW6010B-To

SW6010B-To

SW6010B-To

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 6020-Tota

SW 7470-Tota

DGH-3F-M

: 4/22/02

: L0204323-002A

Prep Date

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/24/02

Analyzed

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

Analyst

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

FIF-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

A



Date: 16-May-02




NEL LABORATORIES

CLIENT: RSSN

PROJECTED: DGH-3F

PROJECTS: DGH-3F

MATRIX: AQUEOUS

ParameterAluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Mercury

Result

0.0810.016

680ND

180

881500

ND0.0010

0.019

NDND

0.0016

0.0013

0.0063

ND0.0012

0.0032

NDNDND

0.075

ND

Unit

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

mg/L

ReportingLimit

0050

00050

0200100202050

00050

OOOIO

OOOIO

O O O I O

OOOIO

OOOIO

O O O I O

O O O I O

OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

0 00040

O O O I O

0 00020

CLIENT ED: DGH-3F-FFM



DF

111l1l

101111111111111111

Method Prep Date

SW6010B-Di

SW 6010B-Di

SW6010B-Di

SW6010B-Di

SW6010B-Di

SW 6010B-Di

SW6010B-Di

SW6010B-Di

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 6020-Diss

SW 7470-Diss 04/24/02

Analyzed

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/23/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

04/24/02

Analyst

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

RAA-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

DHG-Reno

A



Date: 16-Mav-02




A N A L Y T I C A LLABORATORIES

Vanessa PadillaNEL Laboratories Las Vegas4208 Arcata Way, SteXLas Vegas, NV 89030

BSK Submission #: 2002041150BSK Sample ID #: 201121Project ID: L0204323





Sample Type: LiquidSample Description: DGH-3FSample Comments:

Inorganics

Analyte MethodDissolved Organic Carbon (DOC) SM 5310-D

Date Sampled: 04/22/2002Time Sampled: 0940Date Received: 04/23/2002


4.0 mg/L 0.2 5 1.0 04/29/200204/29/2002

mg/L: Milligrams/Liter (ppm)mg/Kg: Milligrams/Kilogram (ppm)Ug/L: Micrograms/Liter (ppb)Hg/Kg: Micrograms/Kilogram (ppb)%Rec: Percent Recovered (surrogates)

Report Authentication Code:

1414 Stanislaus Street Fresno, CA 93706-1623


: PQL x Dilution

ND: None Detected at DLR

H: Analyzed outside of hold timeP: Preliminary resultS: Suspect result. See Cover Letter for comments.E: Analysis performed by External laboratory.


Page 1 of 1

Phone 559-497-2888, In CA 800-877-8310 Fax 559-485-6935


QC Summary Report 05/01/2002

BSK Submission

Client

Date Submitted

Project ID

Project Desc

2002041150NEL Laboratories Las Vegas04/23/2002L0204323Dumpco

BSK StarLims Run #: 36194

Analyst Initials DONNAHAnalyte Results MatrixAnalyte QCType Spike ID Result

Instrument ID

Method Number DOC

%Rec Spike Spk Matrix

Units or RPD RPD Cone Cone UCL LCL Date






LCS

LCSD

MS

MSD

RBLK

N/A

N/A

201118

201118

N/A

103

101

2387

2378

0

mg/L

mg/L

mg/L

mg/L

mg/L

103

101

110

110

<02

1

2 1

10

037 10

ND

ND

12

12

130

130

130

130

02

70

70

70

70

N/A

04/29/02

04/29/02

04/29/02

04/29/02

04/29/02

Acceptable

Acceptable

Acceptable

Acceptable

Acceptable

Approved by

%Rec Percent Recovered

RPD Relative Percent Difference

UCL Upper Control Limit

LCL Lower Control Limit

Parent Sample Sample used as background matrix for MS/MSD

OOS-High QC Result Above UCL

DOS-Low QC Result Below LCL

Page 1 ofl

NEL LABORATORIES

ffBrmi^ff ffliniiiTfiBli '

CLIENT: RSSNWork Order: L0204323Project: DGH-3F

Sample ID MB-R2742

Analyte

Chlonde

Nitiate, as N

Nitrite, as N

Sulfate

Sample ID MB-R2993

Analyte

Chlonde

Nitrate, as N

Nitrite, as N

Sulfate

Sample ID LCS-R2742

Analyte

Chlonde

Nitiate, as NNitrite, as N

Sullate

SampType MBLK

Batch ID R2742

Result

NDNDNDND

SampType MBLK

Batch ID R2993

Result

NDNDNDND

SampType LCS

Batch ID R2742

Result

201

0994

096272


300_W Test Method: EPA 300.0

TestCode 300_W Units mg/L Prep Date Run ID L_IC-1_020423A



0 10

0 100 100 10

TestCode 300_W Units mg/L Piep Date Run ID L_IC-1_020430A



0 100 100 100 10

TestCode 300_W Units mg/L Piep Date Run ID l,_IC-l_020423A



0 10 2 0 101 80 120 0 0

010 1 0 994 80 120 0 0

010 1 0 96 80 120 0 0010 25 0 109 80 120 0 0

Qualifici s: ND - Not Detected at the Repotting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS 01 MSD outside accepance l imits LCS acceptable R - RPD outside accepted recoveiy limits



Page 1 of 28

Date: 16-May-02


Sample ID LCS-R2993 SampType LCS

Batch ID R2993

Analyte

ChlondeNitiate, as NNitnte.asNSulfate

Sample ID

Analyte

ChlondeNitrate, as NNitrite, as NSulfate

Sample ID

Analyte

ChlondeNitrate, as NNitrite, as NSulfate

Sample ID

Analyte

Result

201309861 0152547

LCSD-R2742 SampType LCSD

Batch ID R2742

Result

20670994

0982719

LCSD-R2993 SampType LCSD

Batch ID R2993

Result

2060972

1 022602

L0204322-001BMS SampType MS

Batch ID R2742

Result

Nitiate, as N 246Nitute, asN 3082

Qualiflcis: ND - Not Detected at the Repoitmg Limit

11 - MS 01 MSD outside accepance limits

TestCode

1 eslNo

300_W

300_W Units mg/L

E300


0 100 100 100 10

TestCode

1 estNo

PQL

0 100 100 100 10

TestCode

TestNo

PQL

0 100 100 100 10

TestCode

TestNo

PQL

2 525

LCS acceptable

J - Th i s concentiation is consideied an estimate due to LCS

2 01 01 0

2 5 0

300_W Units mg/L

E300

SPK value SPKRefVai

2 01 01 0

25 0

300_W Units mg/L

E300

SPK value SPKRefVai

2 0

1 01 0

25 0

300_W Units mg/L

E300

SPK value SPKRefVai

25 025 0


Test Method: EPA 300.0

%REC

101986102102

%REC

103994

98109

%REC

103972102104

%REC

984123

Piep Date


LowLimit HighLimit

80808080

Piep Date

Analysis Date

120120120120

4/23/02

LowLimit HighLimit

80808080

Piep Date

Analysis Date

120120120120

4/30/02

LowLimit HighLimit

80808080

Piep Date

Analysis Date

120120120120

4/23/02

LowLimit HighLimit

8080

120120


R - RPD outside accepted recoveiy limits

failuie

Run ID L_IC-1_

SeqNo 23005

020430A

RPD Ret Val %RPD RPDLimit Qual 1

0 00 00 00 0

Run ID L_IC-1_

SeqNo 20976

RPD Ref Val %RPD RP

201 2800994 0

0 96 2 062 72 0 0368

Run ID LJC-I.

SeqNo 23007

i

.020423A

DLimit Qual

25252525

_020430A


2013 2310 986 1 431 015 04912547 2 1 4

Run ID LJC-1

SeqNo 20977

RPD Ref Val %RPD RI

0 00 0

B - Analyte detected in the associated

252525 i25

_020423A

'DLimit Qual

S

Method Blank

Page 2 of 28

Date: l6-May-02

CLIENT: RSSNWork Order: L0204323Project: DGH-3F 300 W

ANALYTICAL QC SUMMARY REPORTTest Method: EPA 300.0

Sample ID L0204261-001AMS

Analyte

Chloi ide

Sulfate


Analyte

ChlondeSulfate

Sample ID L0204217-001AMS

Analyte

SampType MS

Batch ID R2742

Result

131 63659

SampType MS

Batch ID R2993

Result

3970

5130

SampType MS

Batch ID R2993

Result

TestCode 300_W

TestNo E300

PQL SPK value

10 10010 100

TestCode 300_\V

TestNo E300

PQL SPK value

200 2000

200 2000

TestCode 300_W

TestNo E300

PQL SPK value

Units mg/L

SPKRefVai

3532592

Units mg/L

SPKRefVai

22003512

Units mg/L

SPKRefVai

Piep Date



963 80 120 0107 80 120 0

Piep Date



885 80 120 0809 80 120 0

Prep Date




SeqNo 20978

%RPD RPDLimit Qual

00

Run ID L_IC-1_020430A 1

SeqNo 23008

%RPD RPDLimil Qual

00


SeqNo 23541

%RPD RPDLimit Qual

Nitrate, as N 2448 1 0 10 1422 103 80 120


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits

J - Tins concentiation is consideied an estimate due to LCS fai luie


Page 3 of 28

Date: 16-May-02


Sample ID MB-R1591

Analyte

AluminumBarium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample iD LCS-R1591

Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium


Analyte

Aluminum

Banum

Calcium

Iron


SampType MBLK

Batch ID R_R1591

Result

NDNDNDNDND

NDNDND

SampType LCS

Batch ID R_R1591

Result

1 041 02420591 1052033

2079194

05161

SampType MS

Batch ID R_R1591

Result

1 150969

6461 008

TestCode

TestNo

PQL

0050

00050

0500 10050

20050

00050

TestCode

TestNo

PQL

0050

00050

0500 100502 0

05000050

TestCode

TestNo

PQL

0050

00050

0500 10

6010\V_D

SW6010B

SPK value

6010W_D

SW6010B

SPK value

11

201

20202005

6010W_D

SW6010B

SPK value

11

201

6010W_D

Units mg/L

SPKRefVai

Units mg/L

SPKRefVai

0000

0000

Units mg/L

SPKRefVai

0099

001958

6180


Piep Date



Piep Date



104 85102 85103 85110 85102 85104 8597 85

103 85

Piep Date

Analysis Date

115 0115 0115 0115 0115 0115 0115 0115 0

4/23/02


105 75949 75140 75101 75

125 0125 0125 0

125 0

Run ID SUB-1591

SeqNo 30037

%RPD RPDLimit Qual

Run ID SUB-1591

SeqNo 30036

%RPD RPDLimit Qual

000 i00000

Run ID SDB-1591

SeqNo 29996

%R!'D RPDLimit Qual

000 C '

0


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits

J - This concenuation is consideied an estimate due to LCS f a t l u i e


Page 4 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project: DGH-3F 6010W D

ANALYTICAL QC SUMMARY REPORTTest Method: SW 6010B-Diss


Analyte

Magnesium

Potassium

Vanadium


Analyte

Sodium

Sampl ype MS

Batch ID R_R1591

Result

1934

1057

05005

SampType MS

Batch ID R_R1591

Result

1750

TestCode

TestNo

PQL

0502 0

00050

TestCode

TestNo

PQL

50

6010W_D

SYV6010B

SPK value

202005

6010W_D

SW6010B

SPK value

200

Units mg/L Pi ep Date


SPKRefVai

178875

0

Units mg/L

%RJCC

7791

100

LowLimit

757575

HighLimit

125125125

RPD Rei Val

000

Prep Date


SPKRefVai

1520

%REC

115

LowLimit

75

HighLimit

125

RPD Ref Val

0

Run ID SUB-1591

SeqNo 29996

%RPD RPDLimit

000

Run ID SUB-1591

SeqNo 30039

%RPD RPDLimit

0

Qual

Qual


Analyte

Aluminum

Barium

Calcium

lion

Magnesium

Potassium

Vanadium


Analyte

Sodium

SampType MSD

Batch ID R_R1591

Result

1 11

0951

6491 014

192 3

1032

0497

SampType MSD

Batch ID R_R1591

Result

1760

TestCode

TestNo

PQL

0050

00050

0500 10

05020

00050

TestCode

TestNo

PQL

50

6010W_D

SW6010B

SPK value

1

120

12020

05

6010W_D

SW6010B

SPK value

200

Units mg/L

SPKRefVai

0099

001958

6180

178875

0

Units mg/L

SPKRefVai

1520

%REC

10193 1

155101

71 5

785

994

%REC

120

Prep Date


LowLimit HighLimit

757575757575

75

Pi ep Date

Analysis Date

125125125125125125

125

4/23/02

LowLimit HighLimit

75 125

RPD Ref Val

000000

0

RPD Ref Val

0

Run ID SUB-1591

SeqNo 29923

%RPD RPDLimit Qual

000 C

00 C

0

0

Run ID SUB-1591

SeqNo 30041

%RPD RPDLimit Qual

0



J - Tins conccntialioii is consideied an estimate due lo LCS failuie


Page 5 of 28

Date: 16-May-02

CLIENT: RSSNWork Oi dor: L0204323Project: DGH-3F

Sample ID MB-793

Analyte

Aluminum

Bai mmCalcium

Iron

Magnesium

Potassium

Sodium

Vanadium

Sample ID LCS-793

Analyte

Aluminum

Barium

Calcium

lion

Magnesium

Potassium

Sodium

Vanadium


Analyte

Banum

Sodium

ANALYTICAL QC SUMMARY REPORT i

SampType IMBLK

Batch ID R_793

Result

NDNDNDNDNDNDNDND

SampType LCS

Batch ID R_793

Result

1 07

1081209

1 11621 1921 26

197

05509

SampType MS

Batch ID R_793

Result

1 46

1520

TestCode

TestNo

PQL

0050

00050

050

0 1005020

05000050

TestCode

TestNo

PQL

0050

00050

0500 1005020

05000050

TestCode

TestNo

PQL

00050

050

6010WJT

6010W_T Units mg/L

SW60IOB

SPK value SPKRefVai

6010\V_T Units mg/L

SW6010B

SPK value SPKRefVai

1 01 0

20 01 0

20 0

20 020 005 0

6010W_T Units mg/L

SW6010B


1 0446

20 1490

Test Method: SW 6010B-Total 'l

Pi ep Date

Analysis Date

4/23/02

4/24/02


Piep Date

Analysis Date

4/23/02

4/24/02


107 85108 85104 85112 85106 85106 85

985 85110 85

Piep Date

Analysis Date

115 0115 0115 0115 0115 0115 0115 0115 0

4/23/02

4/24/02

%R£C LowLimit HighLimit RPD Ref Val

101 75150 75

125 0125 0

Run ID SUB-1616

SeqNo 29974

%RPD RPDLimit Qual

1

Run ID SUB-1616

SeqNo 29973

%RPD RPDLimit Qual

000

100000

Run ID SUB-1616

SeqNo 29975

%RPD RPDLimit Qual

00 C

4Qualifiers: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked

Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovety limits

J - T his (.onceilliation is consideied an estimate due to LCS failuie


Page 6 of 28

Date: 16-May-02



Analyte

Bai mm

Sodium


Analyte

Aluminum

Barium

Calcium

Iron

Magnesium

Potassium

Sodium

Vanadium


SampType MSU

Batch ID R_793

Result

1 4521490

Samp I ype DUP

Batch ID R_793

Result

NDNDNDNDNDNDNDND

I estCode

TestNo

PQL

00050

050

TestCode

TestNo

PQL

0050

00050

0 500 1005020

05000050

fioiowjrSW6010B

SPK value

120

6010W_T

SW6010B

SPK value

00000000

6010W_T

Units mg/L

SPK Ref Val

0446

1490

Units mg/L

SPKRefVai

000

00000

Test Method : S W 60 1 OB-Total

%REC

1010

%REC

000

00000

Piep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

Piep Date

Analysis Date

4/23/02

4/24/02

LowLimit HighLimit

00000000

00000000

RPD Ref Val

00

RPD Ref Val

00000000

Run ID SUB-1616

SeqNo 29976

%RPD RPDLimit Qual

00

Run ID SUB-1616

SeqNo 29972

%RPD RPDLimit Qual

00000000

Qualifici s: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked


J - This concentialion is consideied an estimate due to LCS fa i lu ie

B - Analyte detected in the associated Method Blank '

Page 7 of 28

Date: 16-May-02


Sample ID MB-R1615

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium

Silvei

Thallium

Zinc

Sample ID LCS-R1615

Analyte

Antimony

Aisenic

Beiylhum

Cadmium

Chiomium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium


SampType MBLK

Batch ID R_R1615

Result

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

SampType LCS

Batch ID R_R1615

Result

0 05628

0 09946

009871

005657

0053390054180052610 05243005574005439

0 1082

6020W_D


TestNo SW6020


OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I OO O O I O

0 00040

O O O I O


TestNo SW6020


O O O I O 005 0

O O O I O 01 0

O O O I O 01 0

O O O I O 005 0

O O O I O 005 0

O O O I O 005 0

O O O I O 005 0

O O O I O 005 0

O O O I O 005 0

O O O I O 005 0

O O O I O 01 0


Prep Date



Prep Date



113 85 115 0

995 85 115 0

987 85 115 0

113 85 115 0

107 85 115 0

108 85 115 0

105 85 115 0

105 85 115 0

111 85 115 0

109 85 115 0

108 85 115 0

Run ID SUB-1615

SeqNo 29928

%RPD RPDLimit Qual

i

,

1

Run ID SUB-1615

SeqNo 29927

%RPD RPDLimit Qual

0

0

0

0000000

o


Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits



Page 8 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project:

Sample ID

Analyte

Silver

Thallium

Zinc

Sample ID

Analyte

Antimony

Arsenic

Beiylhum

Cadmium

Chromium

Cobalt

Coppei

LeadManganese

Nickel

Selenium

Silvei

Thal l ium

Zinc

Sample ID

Analyte

AntimonyAisenic

Beryllium

Qualifiers

DGH-3F

LCS-R1615 SampType LCS

Batch ID R_R1615

Result

0 111005628

005417

L02043 10-003 A SampType MS

Batch ID R_R1615

Result

0 04629

0 14620 140200442

00634

0 05759

006179

0046913 573

0 06069

0 12980 1021

005421

0223

R0204242-003AMS SampType MS

Batch ID R_R1615

Result

0 046290 1462

0 1402

: ND - Not Detected at the Repoitmg Limit

Jl - MS 01 MSD outside accepance l imi ts

TestCode

TestNo

PQL

O O O I O

0 00040

OOOIO

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O0 00040

O O O I O

lestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

6020W_D

SW6020

SPK value

01005005

6020W_D

SW6020

SPK value

005

0 10 1

0050050050050050050050 10 1

005005

6020W_D

SW6020

SPK value

0050 10 1

6020W_D

Units mg/L

SPKRefVai

0

00

Units mg/L

SPKRefVai

000135

00376

00

0 00384

0 00277

0 00489

04014

0 00706

0 0059600

0 104

Units mg/L

SPKRefVai

000135

00376

0

ANALYTICAL QC SUMMARY REPORT!


%REC

111113108

%REC

899109140

884119110114

93 8-882

107124102108238

%REC

899109

140

Piep Date


LowLimit HighLimit

858585

Piep Date

Analysis Date

115

115115

4/24/02

LowLimit HighLimit

75

75757575757575757575757575

Piep Date

Analysis Date

125125125125125125125125125125125125125125

4/24/02

LowLimit HighLimit

757575

125125125


LCS acceptable

J - This cuncentiation is consideied an estimate due to LCS

R - RPD outside accepted

fai lu ie

RPD Ref Val

000

RPD Ref Val

0

0000000000000

RPD Ref Val

000

Run ID SUB-1615

SeqNo 29927

%RPD RPDLimit Qual

000

Run ID SUB-1615

SeqNo 29929

%RPD RPDLimit Qual

0

00 Jl000000 C00000 Jl

Run ID SUB-1615

SeqNo 30046

%RPD RPDLimil Qual

000 II


lecoveiy limits Page 9 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project: DG1I-3F


Analyte

Cadmium

Chiomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

Sample ID L02043 10-003 A

Analyte

Antimony

Aisemc

Beryllium

Cadmium

Chiomium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium

Silver

Thallium

Zinc

SampType MS

Batch ID R_R1615

Result

00442

006340 05759

006179

004691

3573

0 06069

0 12980 1021

0 05421

0223

SampType MSD

Batch ID R_R1615

Result

0 05058

0 1459

0 142300441

0 0623700572

005881

004616

3 581

006051

0 12740 101

005398

0 1804

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

OOOIO

O O O I O

O O O I O

0 00040

O O O I O

TestCode

TestNo

PQL

O O O I O

OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

0 00040

O O O I O

6020W_D

SW6020

SPK value

005005005005005005005

0 10 1

005

005

6020W_D

SW6020

SPK value

0050 10 1

005005005005005005005

0 10 1

005005

6020W_D

Units mg/L



Pi ep Date


SPK Ref Val

0000384

0 00277

0 00489

04014

0 00706

0 00596

00

0 104

Units mg/L

%REC

884

119110114

93 8-882107124102108238

LowLimit

757575757575

7575757575

HighLimit

125125125125125125125125125125125

RPD Ref Val

00000000000

Pi ep Date


SPKRefVai

000135

00376

00

000384

0 00277

0 00489

04014

0 00706

0 00596

00

0 104

%REC

985

108142

882117109

108923866

107121101108153


00000000000000

Run ID SUB-1615

SeqNo 30046

%RPD RPDLimit Qual

000000 C00000 Jl

Run ID SUB-1615

SeqNo 29930

%RPD RPDLimit Qual

000 Jl000000 C

00000 Jl


II - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted iccoveiy limits

J - 1 his concentiation is consideied an estimate due to LCS failuie


Page 10 of 28

Date: 16-May-02



Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

CopperLead

Manganese

Nickel

SeleniumSilver

ThalliumZinc


Analyte

Antimony

Aisemc

Beiylhum

Cadmium

Chiomium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium


Samplype MSD

Batch ID R_R1615

Result

0 05058

0 1459

0 142300441

0 06237

00572

005881

004616

3581006051

0 12740 101

0 053980 1804

SampType DUP

Batch ID R_R1615

Result

ND003632

NDND

0 00466

0 00294

0 00568

ND4 07

0 00724

ND

TestCode

TestNo

PQL

O O O I O

OOOIO

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

0 00040O O O I O

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I O

OOOIO

O O O I O

O O O I OO O O I O

O O O I O

O O O I O

O O O I O

6020\Y_D

SW6020

SPK value

005

0 10 1

005005005005005005005010 1

005005

6020W_D

SW6020

SPK value

0

000000000

0

6020W_D

Units mg/L

SPKRefVai

000135

00376

0

00 00384

0 00277

0 00489

04014

0 00706

0 00596

00

0 104

Units mg/L

SPKRefVai

00000

00000

0


Pi ep Date



985

108142

882117

109108

923-866107121101108153

Piep Date



0 0 00 0 00 0 00 0 00 0 0

0 0 00 0 00 0 00 0 00 0 00 0 0

RPD Ref Val

0

0000000000000

RPD Ref Val

00000000000

Run ID SUB-1615

SeqNo 30047

%RPD RPDLimit Qual

000 Jl

000000 C

1

00000 Jl

Run ID SUB-1615 ]

SeqNo 29926

%RPD RPDLimit Qual

00

000000000



J - This concenUation is consideied an estimate due to LCS failuie

B - Analyte detected in the associated Method Blank i

Page 11 of 28

Date: 16-May-02



Analyte

Silver

Thallium

Zinc

Sample ID R0204242-003ADUP

Analyte

Antimony

Aisemc

Beiylhum

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silver

Thal l ium

Zinc


SampType DUP

Batch ID R_R1615

Result

ND

ND

0 108

SampType DUP

Batch ID R_R1615

Result

ND

0 03632

ND

ND

0 00466

0 00294

0 00568

ND407

0 00724

ND

ND

ND

0 108

TestCode

TestNo

PQL

O O O I O

0 00040

O O O I O

TestCode

TestNo

PQL

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I O

O O O I OO O O I O

O O O I OO O O I O

O O O I O

0 00040

O O O I O

6020W_D

SW6020

SPK value

0

0

0

6020W_D

SW6020

SPK value

0

0

0

0

0

0

0

0

0

0

0

0

0

0

6020W_D

Units mg/L

SPKRefVai

0

0

0

Units mg/L

SPKRefVai

0

0

0

0

0

0

0

0

0

0

0

0

0

0


%REC

0

0

0

%REC

0

0

0

0

0

0

0

0

0

0

0

0

0

0

Piep Date


LowLimit HighLimit

0

0

0

Pi ep Date

Analysis Date

0

0

0

4/24/02

LowLimit HighLimit

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

0

RPD Ref Val

0

0

0

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

0

0

0

Run ID SUB-1615

SeqNo 29926

%RPU RPDLimit Qual

0

0

0

Run ID SUB-1615

SeqNo 30043

%RPD RPDLimit Qual

00000000000000



J - This concenuaijon is consideied an estimate due lo LCS failuie


Page 12 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project:

Sample ID

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chromium

Cobalt

Copper

LeadManganese

Nickel

Selenium

SilverThallium

Zinc

Sample ID

Analyte

Antimony

Arsenic

Beryllium

Cadmium

Chiomium

Cobalt

Coppei

Lead

Manganese

Nickel

Selenium

Qualif icis

DGH-3F

MB-795 SampType MBLK

Batch ID R_795

Result

NDNDNDNDNDNDNDNDNDNDNDNDNDND

LCS-795 SampType LCS

Batch ID R_795

Result

0 05695

009415

0 1524

00519

00537

0 05475

00567

00545

00494

00554

00956

ND - Not Detected at the Repoitmg Limit

Jl - MS 01 MSD outside accepance limits

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

LCS acceptable

J - This coucentialion is cons,ideied an estimate due to LCS

ANALYTICAL QC SUMMARY REPORT6020W_T Test Method: SW 6020-Total

6020W_T Units mg/L Piep Date 4/23/02 Run ID SUB-1627

SW6020 Analysis Date 4/24/02 SeqNo 29953

SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

1

6020WJT Units mg/L Piep Date 4/23/02 Run ID SUB-1627

SW6020 Analysis Date 4/24/02 SeqNo 29952

SPK value SPKRefVai %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

005 0 114 85 115 0 00 1 0 942 85 115 0 001 0 152 85 115 0 0

005 0 104 85 115 0 0

005 0 107 85 115 0 0005 0 110 85 115 0 0005 0 113 85 115 0 0005 0 109 85 115 0 0

005 0 988 85 115 0 0005 0 111 85 115 0 0

0 1 0 956 85 115 0 0

C - Unspiked sample >5 times the amount spiked B - Analyte detected in the associated Method Blank

R - RPD outside accepted recovery limits Page 13 of 28

failuie Date: 16-May-02


Sample ID LCS-795

Analyte

Silver

Thall ium

Zinc


Analyte

Antimony

Arsenic

Beiylhum

Cadmium

Chromium

Cobalt

Copper

Lead

Manganese

Nickel

Selenium

Silvei

Thall ium

Zinc


Analyte

Antimony

Arsenic

Beiylhum


SampType LCS

Batch ID RJ795

Result

0 1364

00547

0 04785

SampType MS

Batch ID RJ795

Result

00629

0 1046

0 1637

0 05525

0 05645

0059

006515

0 05685

00643

0 062550 1049

0 1384

0 06405

0 1304

SampType MSD

Batch ID R_795

Result

0 05965

00966

0 1534

TestCode

TestNo

6020W_T

SW6020

PQL SPK value

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

00050

00050

00050

0005000050

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

0 1

005

005

6020WJT

SW6020

SPK value

005

0 1

0 1

005

005

005

005

005

005

005

0 1

0 1

005

005

6020W_T

SW6020

SPK value

005

0 1

0 1

6020WJT

Units mg/L

SPKRefVai

000

Units mg/L

SPKRefVai

0

0

0

0

00055

0

0 00675

0

00105

00

0

0

008105

Units mg/L

SPK Ref Va!

0

0

0


%REC

136

109

957

%REC

126

105

164

110

102

118

117

114

108

125

105

138

128

987

%REC

119

966

153

Piep Date

Analysis Date

4/23/02

4/24/02

I owLimit HighLimit

85

85

85

Piep Date

Analysis Date

115

115

115

4/23/02

4/24/02

LowLimit HighLimit

75

75

75

75

75

75

75

75

75

75

75

75

75

75

Piep Date

Analysis Date

125

125

125

125

125

125

125

125

125

125

125

125

125

125

4/23/02

4/24/02

LowLimit HighLimit

RPD Ref Val

0

0

0

RPD Ref Val

0

0

0

0

0

0

0

0

0

0

0

0

0

0

RPD Ref Val

0

0

0

Run ID SUB-1627

SeqNo 29952

%RPD RPDLimit Qual

0

0

0

Run ID SUB-1627

SeqNo 29954

%RPD RPDLimit Qual

0

0

0 Jl

0

0

0

0

0

0

00

0 Jl

0 Jl

0

Run ID SUB-1627

SeqNo 29955

%RPD RPD! milt Qual

0

0

0 Jl i



J - This concentiation is consideied an estimate due to LCS i a i l u i e


Page 14 of 28

Date: 16-May-02



Analyte

Cadmium

Chiomium

Cobalt

Copper

Lead

ManganeseNickel

Selenium

Silver

ThalliumZinc


Analyte

Antimony

Arsenic

Beiylhum

Cadmium

Chromium

Cobalt

Copper

Lead

ManganeseNickel

Selenium

Silver

ThalliumZinc


SampType MSD

Batch ID R_795

Result

00516

0 05325

0 055250 06085

00528

0 05925

0 05675

0 10260 130800593

0 1252

SampType DUP

Batch ID RJ795

Result

NDNDND

NDND

ND00061

ND

00094

ND

NDNDND

0 07405

TestCode

TestNo

PQL

00050

00050

0005000050

00050

0005000050

00050

00050

00050

00050

TestCode

TestNo

PQL

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

00050

6020WJT

SW6020

SPK value

005005

005005005005005

0 101

005005

6020W_T

SW6020

SPK value

000000

000

00000

6020WJT

Units mg/L

SPKRefVai

000055

00 00675

000105

0000

008105

Units mg/L

SPKRefVai

000000

00000000


Prep Date

Analysis Date

4/23/02

4/24/02


103955110108106

975114103131119

884

Piep Date

Analysis Date

4/23/02

4/24/02


0 00 00 0

0 00 0

0 00 00 00 00 00 0

0 00 00 0

000

00

0000000

00

RPD Ref Val

00000000000

RPD Ref Val

00000000000

0

00

Run ID SUB-1627

SeqNo 29955

%RPD RPDLimit Qual

000000000 Jl

00

Run ID SUB-1627

SeqNo 29951

%RPD RPDLimit Qual

000

00000000000

r»noi;r,o^c. Kin _ M^t riMprip/i M il-ip R^nmimo 1 irmt P - 1 IncmVprl camnle >S timps thp amnimi snikpri R - Analvte detected in the associated Method Blank

Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted lecovery limits

J - Tins conccnuation is consideied an estimate due to LCS failuie

Page 15 of 28

Date: 16-May-02


-J.-t

8260 W

ANALYTICAL QC SUMMARY REPORTTest Method: SW8260B

Sample ID Method Blank 02 SampType MBLK

Analyte

Batch ID R2684

Result

TestCode 8260_W Units ug/L

TestNo SW8260B


Prep Date




SeqNo 20642

%RPD RPDLimit Qual

1,1,2-Ti ichlorotnfluoioethaneMTBEAcetoneBenzeneBromobenzeneBromochloro methaneBiomodichloiomethaneBromofoi mBiomomethane2-Butanonen-Butylbenzenesec-Butylbenzenetert-ButylbenzeneCarbon disulfideCarbon tctiachlondeChloiobenzeneChloioelhane2-Chloioethyl vinyl etheiChloioformChloiomethane2-Chloiotoluene4-ChloiotolueneDibi omochloromethane1,2-Dibi omo-3-chloi opi opane1,2-DibiomoethaneDibiomomethane1,2-Dichloiobcnzene1,3-Dichloiobenzcne1,4-Dichloi obenzene

Dichloi odi lluoi omethanc

ne NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDNDNDND

lane ND

NDNDND

NDND

ND

50502550505050505025505050505050

505050505050505050

50505050

50


Jl - MS or MSD outbide accepance limits LCS acceptable R - RPD outside accepted lecoveiy l imits

J - 1 Ins concentiation is consideied an estimate due to LCS failuie


Page 16 of 28

Date: 16-May-Q2



Analyte

1,1-Dichloi oethane

1 ,2-Dichloroethane1,1-Dichloi oethene

cis-l,2-Dichloroetheneti ans- 1 ,2-Dichloroethene1 ,2-Dichloi opropane1 ,3-Dichloropropane

2,2-Dichloi opropane1 ,1 -Dichloi opropenecis-l,3-Dichloropropenetrans-1 ,3-DichloropropeneEthylbenzeneHexachlorobutadiene

2-HexanonelodomethaneIsopropylbenzenep-Isopiopyltoluene

Methylene chlonde4-Methyl-2-pentanoneNaphthalene

n-PiopylbenzeneStyiene1,1,1 ,2-Teti achloi oethane

1 , 1 ,2,2-Teti achloi oethaneTeti achloi oethene

Toluene1 ,2,3-Tnchloiobenzene1 ,2,4-Tnchloiobenzene1,1,1-Tnchloi oethane1 ,1 ,2-1 richloroethane

Samplype MBLK

Batch ID R2684

Result

NDNDND

NDNDNDNDNDNDNDNDNDNDNDND

NDNDNDNDND

NDNDND

NDNDNDNDNDNDND

ANALYTICAL QC SUMMARY REPORT )

8260_W Test Method: SW8260B

TestCode 8260_W Units ug/L Prep Date Run ID L_VOAMS-2_020423A


PQL SPK value SPKRefVai %RLC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual

505050

50505050

5050505050502550

5050502510

5050505050505050505 0

Qualifiets: ND - Not Detected at the Repoiting Limit C - Unspiked sample >5 times the amount spiked


J - This concentiation is considered an estimate due to LCS fa i lu ie


Page 17 of 28

Date: 16-May-02



Analyte

Trichloroethene

Trichlorofluoi ome thane

1 ,2,3-Ti ichloropropane

1 ,2,4-Ti imethy Ibenzene

1 ,3,5-Ti imethylbenzene

Vinyl acetate

Vinyl chloride

o-Xylene

m,p-Xylene

Surr Dibiomofluoiomethane

Surr Foluene-dS

SUIT 4-Bromofluorobenzene


Analyte

Acetone

Benzene

Biomofoirn

Bromomethane

Chloiobcnzene

Chloiolorm

Chloiomethane

Dichloi odi fluoi omethane

1,1-Dichloi oethane

1,1-Dicliloi oethene

1,2-Dichloiopiopane

Ethylbeiizcne

1 ,1 ,2,2-Tetrachloioethane

SampType MBLK

Batch ID R2684

Result

NDNDNDNDND

NDNDNDND

4804

5357

4476

SampType LCS

Batch ID R2684

Result

37814857

3986

7834

51 774996

6859

6665249

4887

49 165039

5234

TestCode

TestNo

PQL

505050

5050

50505010

505050

TestCode

TestNo

PQL

25505050505050

5050505050

50

8260_W

SW8260B

SPK value

505050

8260_W

SW8260B

SPK value

50505050505050

5050505050

50

8260_W

Units u-g/L



Prep Date


SPKRefVai

000

Units ug/L

%REC

96 1107

895

LowLimit

80808562

HighLimit

120119139

RPD Ref Val

0

00

Piep Date


SPKRefVai

00000

00

000000

%REC

75697 1797157104

999137133105

977983

101105

LowLimit

70707070708070

707080808070

HighLimit

130130130130130

120130

130130120120120130

RPD Ref Val

00000

00

000000


SeqNo 20642

%RPD RPDLimit

000

Qual


SeqNo 20645

%RPD RPDLimit

000000

0

000000

Qual

S

SS



J - This concent!ation is consideied an estimate due to LCS fai luie


Page 18 of 28

Date: 16-May-02



Analyte

Toluene

TrichloioetheneVinyl chlonde

SUIT Dibiomofluoromethane

Suir Toluene-dS

Sun 4-Bromofluorobcnzene

Sample ID L0204322-001A MS

Analyte

Acetone

BenzeneBromomethane

Chloiobenzene

Chlorome thane

Dichloi odifluoi omethane

1,1-Dichloi oethene

Toluene

Trichloioethene

Vinyl chlonde

Surr Dibi omofluoi omethane

Sun 1oluene-d8Sun 4-Bi omofluoi obenzcne

Sample ID L0204322-001 A MSD

Analyte

Acetone


SampType LCS

Batch ID R2684

Result

4647

47 1558 174495

5268

42 1

SampType MS

Batch ID R2684

Result

51 33

5436759

5366

8647

8365

58 15

5299

52 186921

4669

5546

4873

SampType MSD

Batch ID R2684

Result

4805

Quahfieis: ND - Not Detected at the Reporting Limit

Jl - MS 01 MSD outside accepance limits LCS

J - This cunccntiation is coiiiideied an estimate

TestCode 8260_W

TestNo SW8260B

PQL SPK value

50 5050 5050 5050 5050 5050 50

TestCode 8260_W

TestNo SW8260B

PQL SPK value

25 5050 5050 5050 5050 5050 5050 5050 5050 5050 5050 5050 5050 50

TestCode 8260_W

TestNo SW8260B

PQL SPK value

25 50

8260 W

Units u.g/L

SPKRefVai

00000

0

Units ug/L

SPK Ref Val

00000000

00000

Units ug/L

SPKRefVai

0

*


Piep Date


%RBC LowLimit HighLimit

92 9 80 12094 3 70 130116 80 120

89 9 80 120105 808 119

842 562 139

Piep Date



103 70 130109 70 130152 70 130107 70 130173 70 130167 70 130116 80 120106 80 120104 70 130138 80 120

934 926 108111 957 112

975 853 104

Piep Date


%REC LowLimit l l ighLimi t

96 1 70 130


acceptable R - RPD outside accepted

due to LCS fai luie

recoveiy limits

RPD Ref Val

000000

RPD Ref Val

0000000000000

RPD Ref Val

51 33

i


SeqNo 20645

%RPD RPDLimit Qual

000000 i


SeqNo 20643

%RPD RPDLimit Qual

000 S00 S0 S0

o00 S00o


SeqNo 20644

%RPD RPDLimit Qual

660 25

B - Analyte detected in the associated Method Blank '

Page 1 9 of 28

Date: 16-May-02\


Sample ID L0204322-001A MSD

Analyte

Benzene

Bromomethane

Chloiobenzene

Chloi omethane

Dichloiodifluoi omethane

1,1-Dichloi oethene

Toluene

Trichloioethene

Vinyl chlorideSun Dibiomofluoromethane

Surr Toluene-d8

Sun 4-Biomofluoiobenzene


SampType MSD

Batch ID R2684

Result

4938

67 13

4966

6853

7924

5277472147785748

4707

53 57

4505

TestCode

TestNo

PQL

50

50

50

50

50

50

50

50

50

50

50

50

8260_\Y

SW8260B

SPK value

50

50

50

50

50

50

50

50

50

50

50

50

8260_W

Units u.g/L

SPKRefVai

0

0

0

0

0

0

0

0

0

0

0

0


%REC

988

134

99.3

137

158

106

944

956

115

94 1

107

90 1

Piep Date


LowLimit HighLimit

70

70

70

70

70

80

80

70

80

926

957

853

130

130

130

130

130

120

120

130

120

108

112

104


SeqNo 20644

RPD Ref Val

5436

759

5366

8647

8365

58 15529952 18

6921

0

0

0

%RPD

960

123

774

231

5 4 1

97011 5

880

185

0

0

0

RPDLimit Qual

2525 S

25

25 S

25 S

2525

25

25

0

o0


Jl - MS or MSD outside accepance limits LCS acceptable R - RPD outside accepted iccovery limits

J - This concentiation is consideied an estimate due to LCS fai lu ie


Page 20 of 28

Date: l6-May-02


DGI1-3F ALK W

ANALYTICAL QC SUMMARY REPORTTest Method: SM2320 B

Sample ID MB-R2983

Analyte





Sample ID LCS-R2983

Analyte

SampType MBLK

Batch ID R2983

Result

NDNDNDND

SampType LCS

Batch ID R2983

Result


TestNo M2320 B


25252525


TestNo M2320B


Prep Date



Piep Date



Run ID L_APITR-1_020429A

SeqNo 22904

%RPD RPDLimit Qual

Run ID L_AT1TR-1_020429A

SeqNo 22903

%RPD RPDLimit Qual

Alkalinity, Total (As CaCO3) 144 25 125 115 80 120


Analyte


Sample ID L0204322-001BDUP

Analyte



Hydi oxide (As CaC03)

Alkal ini ty, Total (As CaCO3)

SampType LCSD

Batch ID R2983

Result

122

SampType DUP

Batch ID R2983

Result

ND74

ND74

TestCode

TestNo

PQL

25

TestCode

TestNo

PQL

25252525

ALK_W

M2320 B

SPK value

125

ALK_W

M2320 B

SPK value

0000

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

0000

%REC

976

%R£C

0

000

Prep Date


LowLimit HighLimit

80

Piep Date

Analysis Date

120

4/29/02

LowLimit HighLimit

0000

0

000

RPD Ref Val

144

RPD Ref Val

0750

75

Run ID L_ATITR-1

SeqNo 22906

_020429A

%RPD RPDLimit

165

Run ID L.AT1TR-1

SeqNo 22905

25

Qual

_020429A

%RPD RPDLimit

01 34

01 34

10101010

Qual

Qualifiers: ND - Not Delected at the Repoitmg Limit C - Unspiked sample >5 times the amount spiked


J - This conccniiation is consideied an estimate due to LCS fa i lu ie


Page 21 of 28

Date: l6-May-02


Project: DGH-3F COD

ANALYTICAL QC SUMMARY REPORTTest Method: SM5520 D

Sample ID MB-R2949

Analyte


Sample ID LCS-R2949

Analyte



Analyte



Analyte


Sample ID L0204310-001 BMSD

Analyte

SampType MBLK

Batch ID R2949

Result

ND

SampType LCS

Batch ID R2949

Result

533

SampType LCSD

Batch ID R2949

Result

503

SampType MS

Batch ID R2949

Result

554

SampType MSD

Batch ID R2949

Result

TestCode

TestNo

PQL

10

TestCode

TestNo

PQL

10

TestCode

TestNo

PQL

10

TestCode

TestNo

PQL

10

TestCode

TestNo

PQL

COD

M5220 C

SPK value

COD

M5220 C

SPK value

500

COD

M5220 C

SPK value

500

COD

M5220 C

SPK value

4625

COD

M5220 C

SPK value

Units mg/L

SPK Ref Val

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

75

Units mg/L

SPK Ret Val

Prep Date



Piep Date



107 80

Piep Date

Analysis Date

120 0

4/29/02


101 80

Piep Date

Analysis Date

%REC LowLimit Hi

104 70

Piep Date

Analysis Date

120 533

4/29/02

ghLimit RPD Ref Val

130 0

4/29/02


Run ID 1 _\VC_020429C

SeqNo 22627

%RPD RPDLimit

Run ID L_\VC_020429C

SeqNo 22626

%RPD RPDLimit

0

Run ID L_WC_020429C

SeqNo 22630

%RPD RPDLimit

579 15

Run ID I _WC_020429C

SeqNo 22628

%RPD RPDLimit

0

Run ID L_\VC_020429C

SeqNo 22629

%RPD RPDLimit

Qual ,

Qual

Qual

Qual

Qual

Chemical Oxygen Demand 546 10 4625 75 102 70 130 546 25


Jl - MS 01 MSD outside accepance limits LCS acceptable R-RPD outside accepted lecoveiy limits

/ - This concenUation is consideied an estimate due to LCS failuie


Page 22 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project: DGH-3F HG 7470 D


Sample ID MB-799

Analyte

Mercury

Samplype MBLK

Batch ID R_799

Result

ND

TestCode HG_7470_D Units mg/L

TestNo SW7470


0 00020

Piep Date

Analysis Date

4/24/02

4/24/02


Run ID SUB-1625

SeqNo 29941

%RPD RPDLimit Qual

Sample ID LCS-799

Analyte

Meicury


Analyte

Mercury


Analyte

Mercury


Analyte

SampType LCS

Batch ID R_799

Result

0 00499

SampType MS

Batch ID R_799

Result

000521

SampType MS

Batch ID R_799

Result

000521

SampType MSD

Batch ID R_799

Result

TestCode HG_7470_

TestNo SW7470

PQL SPK value

0 00020 0 005

TestCode HG_7470_

TestNo SW7470

PQL SPK value

0 00020 0 005

TestCode HG_7470_

TestNo SW7470

PQL SPK value

0 00020 0 005

TestCode HG_7470

TestNo SW7470

PQL SPK value

D Units mg/L

SPKRefVai

0

D Units mg/L

SPKRefVai

0

_D Units mg/L

SPKRefVai

0

_D Units mg/L

SPK Ref Val

Piep Date

Analysis Date

4/24/02

4/24/02


998 85

Prep Date

Analysis Date

115 0

4/24/02

4/24/02


104 85

Piep Date

Analysis Date

115 0

4/24/02

4/24/02


104 85

Piep Date

Analysis Date

115 0

4/24/02

4/24/02


Run ID SUB-1625

SeqNo 30057

%RPD RPDLimit

0

Run ID SUB-1625

SeqNo 29942

%RPD RPDLimit

0

Run ID SUB-1625

SeqNo 30059

%RPD RPDLimit

0

Run ID SUB-1625

SeqNo 29943

%RPD RPDLimit

Qual

Qual

Qual

Qual

Meicuiy 00051 0 00020 0005 102

Qualifiers: ND - Not Detected at the Repoitmg Limit C - Unspiked sample >5 tunes the amount spiked

Jl - MS 01 MSD outside accepance limits LCS acceptable R- RPD outside accepted iccoveiy limits

J - Tins conctntiation is consideied an estimate due to LCS fai lu ie


Page 23 of 28

Date: 16-May-02

CLIENT: RSSN

Work Order: L0204323Project: DGH-3F HG 7470 D



Analyte

SampType MSD

Batch ID R_799

Result

FestCode HGJ7470_D Units mg/L

FestNo SW7470


Prep Date 4/24/02



Run ID SUB-1625

SeqNo 30021

%RPD RPDLimit Qual

Mercuiy 00051 0 00020 0005 102





Page 24 of 28

Date: 16 May-02

CLIENT: RSSNWork Order: L0204323Project: DGH-3F HG 7470 T

ANALYTICAL QC SUMMARY REPORT iTest Method: SW 7470-TotaI

Sample ID MB-800

Analyte

SampType

Batch ID

MBLK

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Pi ep Date

Analysis Date

4/24/02

4/24/02

%REC LoviLmiit HighLimit RPD Ref Val

Run ID

SeqNo

SUB-1626

29947

%RPD RPDLimit Qual

Meicury ND 0 00020

Sample ID LCS-800

Analyte

Meicuiy


Analyte

Samp Type LCS

Batch ID R_800

Result

000518

SampType MS

Batch ID R_800

Result

TestCode HG_7470_T

TestNo SW7470

PQL SPK value

0 00020 0 005

TestCode HG_7470_T

TestNo SW7470

PQL SPK value

Units mg/L

SPKRefVai

0

Units mg/L

SPKRefVai

Piep Date

Analysis Date

4/24/02

4/24/02


104 85

Prep Date

Analysis Date

115 0

4/24/02

4/24/02


Run ID SUB-1626

SeqNo 29946

%RPD RPDLimit

0

Run ID SUB-1626

SeqNo 29948

%RPD RPDLimit

Qual

Qual

Mercury 000541 0 00020 0005 108 85 115


Analyte

SampType

Batch ID

MSD

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Piep Date

Analysis Date

4/24/02

4/24/02

Run ID

SeqNo

%REC LowLimit HighLimit RPD Ref Val %R

SUB-1626

29949

PD RPDI imit Qual

Meicuiy 0 00539 0 00020 0005 108


Analyte

SampType

Batch ID

DUP

R_800

Result

TestCode

TestNo

PQL

HG_7470_T

SW7470

SPK value

Units mg/L

SPKRefVai

Piep Date

Analysis Date

4/24/02

4/24/02

Run ID

SeqNo

%REC LowLimit HighLimit RPD Ret Val %R

SUB-1626

29945

PD RPDLimit Qual

Meicuiy ND 0 00020


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted recoveiy limits

J - This concentiation is consideied an estimate due to LCS f a i l u i e


Page 25 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project: DGH-3F NH3-N W


Test Method: SM4500-NH3 C

Sample ID MB-R2996

Analyte

SampType MBLK

Batch ID R2996

Result

FestCode NH3-N_W Units mg/L

TestNo M4500-NH3 C


Piep Date



Run ID L_WC_020430A i

SeqNo 23035|

%RPD RPDLimit Qual 1


Sample ID LCS-R2996

Analyte

SampType LCS

Batch ID R2996

Result


TestNo M4500-NH3 C


Piep Date



Run ID L WC 020430Aj

SeqNo 23034

%RPD RPDLimit Qual

Ammonia, as N 1008 030 101 839 117

Sample ID LCSD-R2996 SampType LCSD

Analyte

Batch ID R2996

Result


TestNo M4500-NH3 C


Piep Date



Run ID L_WC_020430A

SeqNo 23037

%RPD RPDLunit

|

1

Qual

Ammonia, as N 1 01 030 101 839 117 1 008 0 198 25


Analyte

SampType MS

Batch ID R2996

Result


TestNo M4500-NH3 C


Piep Date



Run ID L_WC_020430A 1

SeqNo 23036

%RPD RPDLimit Qual

Ammonia, as N 1 12 030 112 764 124


Jl - MS 01 MSD outside accepance limits LCS acceptable R RPD outside accepted lecoveiy limits

J -1 his conccntialion is consideied an estimate due to LCS failuie


Page 26 of 28

Date: !6-May-Q2

CLIENT: RSSNWork Order: L0204323Project: DGII-3F SULF W

ANALYTICAL QC SUMMARY REPORTTest Method: SM4500-S D


Analyte

Sulfide

Batch ID R2855

Result

ND


TestNo M4500-S D


0030

Prep Date Run ID LjSPEC-2_020426A


%REC LowLimit HighLimit RPD Ret Val %RPD RPDLimit Qual

Sample ID LCS-R2855

Analyte

Sulfide

SampType LCS TestCode SULF_W Units mg/L Piep Date Run ID L_SPEC-2_020426A

Batch ID R2855 TestNo M4500-S D Analysis Date 4/26/02 SeqNo 21794


0107 0030 0107 0 100 80 120 0 0


Analyte

Sulfide


Analyte

SampType LCSD

Batch ID R2855

Result

0 111

SampType MS

Batch ID R2855

Result

TestCode

TestNo

PQL

0030

TestCode

TestNo

PQL

SULF_W Units mg/L

M4500-S D

SPK value SPKRefVai

0 107 0

SULF_W Units mg/L

M4500-S D

SPK value SPKRefVai

Piep Date



104 80 120 0 107

Piep Date




SeqNo 21796

%RPD RPDLimit

367 25

Qual


SeqNo 21797

%RPD RPDLimit Qual

Sulfide 0 114 0030 0107 0 107 70 130 0

Sample ID L0204310-001BMSD

Analyte

SampType MSD

Batch ID R2855

Result


TestNo M4500-SD


Piep Date




SeqNo 21798

%RPD RPDLimit Qual

Sulfide 0 109 0030 0 107 102 70 130 0 114 4 4 8 25


Jl - MS 01 MSD outside accepance limits LCS acceptable R - RPD outside accepted tecoveiy limits

J - 1 his concent!ation is consideied an estimate due to LCS failuie


Page 2 7 of 28

Date: 16-May-02

CLIENT: RSSNWork Order: L0204323Project: DGH-3F TDS W

ANALYTICAL QC SUMMARY REPORTTest Method: SM2540 C

Sample ID MB-R2814

Analyte

SampType

Batch ID

MBLK

R2814

Result

TestCode

TestNo

PQL

TDS_W

E160.1

SPK value

Units mg/L

SPKRefVai

Prep Date

Analysis Date

%REC LowLimit Hi

4/24/02

ghLimit RPD Ref Val

Run ID

SeqNo

L_\VC_0204241

21508i

%RPD RPDLimit Qual

Total Dissolved Solids ND 150

Sample ID LCS-R2814

Analyte


SampType LCS TestCode TDS_W Units mg/L Prep Date Run ID L_\VC_020424I '

Batch ID R2814 TestNo E160.1 Analysis Date 4/24/02 SeqNo 21507


967 150 1000 0 967 80 120 0 0

Sample ID L0204356-003EDUP SampType DUP

Analyte

Batch ID R2814

Result


TestNo E160.1


Prep Date



Run ID L_WC_020424I

SeqNo 21509

%RPD RPDLimit1

Qual '

Total Dissolved Solids 346 150 367 589 25

Qualifiei s: ND - Not Detected at the Reporting Limit C - Unspiked sample >5 times the amount spiked




Page 28 of 28

Date: 16-May-02



CHAIN OF CUSTODY NEL Work Order: £-O'LO<~(

Project Name

Phoenix Division • 3201 So 35th Street, Suite B6 • Phoenix, Arizona 85034602-437-0099 • Fax 602-437-2225 • 888-238-2514

Company Attention

Address

Phone Numb ax Number

Billing Address Expected Due Date/v

Requested Turnaround1 5-day 2-day 1 -day Othe

Time/DateSampled Customer Sample Identification

NE.LIdentification

urchase Order Number

Project Number

Sampled By

Analysis

X

JLY 7%

Q( Y

D fflt£ X

Custody Seal intact? YCondition

Box#1 DW Drinking Water SD SolidWW Waste Water AQ AqueousOI_ Oil/Organic Uquid A Air

Box #2 A HC!B HNO3

C H2SO4

D NaOH

E Ice OnlyF Other_G Not Preserved

Relinquished by (Ppnt) Date/Time Received by (Print) (Signature) Date/Time \

'

The liability of NEL Laboratories Inc is limited strictly to the price of sample analysis for those samples received in good condition by NEL NEL is not responsible for loss damage resampling costs and/or qualified data related to samples not received in good conditionIncluding adequate sample volume and number of containers Customer signature of this CoC constitutes a purchase order for NEL to perform work and constitutes acceptance of all NEL Standard Terms and Conditions Signature also constitutes acceptanceof NEL Standard List Prices for all services ordered here on, except those specified otherwise via an NEL Quotation for Testing Services in effect at the time of sample receipt NEL turnaround times are measured in regular working days Samples received at thelaboratory after 16 30 will be considered received on the next working day Commitment of laboratory to the requested turnaround time wilt be confirmed via Sample Confirmation transmitted to the fax number provided above

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