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Golder Associates Inc.CONSULTING ENGINEERS

INTERIM REPORT NO. 3

BASELINE AIR SURVEYPRE-DESIGN INVESTIGATION TASK A-l

INDUSTRI-PLEX SITEWOBURN, MASSACHUSETTS

SDMS DocID 000230848

Prepared for:

Industri-Plex Site Remedial Trust800 North Lindbergh Boulevard

St. Louis, Missouri

DISTRIBUTION:

8 Copies - Industri-Plex Site Remedial Trust6 Copies - U.S. Environmental Protection Agency1 Copy - Massachusetts Dept. of Environmental Protection1 Copy - NUS Corporation2 Copies - Golder Associates Inc.

December 1990 Project No.: 893-6255

GOLDER ASSOCIATES INC. « 20000 HORIZON WAY. SUITE 500, MT. LAUREL. NEW JERSEY 08054 • TELEPHONE (609) 273 1110 • FACSIMILE (609) 273-0778

OFFICES IN UNITED STATES • CANADA • UNITED KINGDOM • SWEDEN • GERMANY • ITALY • AUSTRALIA

Colder Associates Inc.CONSULTING ENGINEERS

December 14, 1990 Project No. 893-6255

United States Environmental Protection AgencyWaste Management DivisionJ.F.K. Federal Building, HRS-CAN-3Boston, MA 02203-2211

Attn: Joseph DeColaRemedial Project Manager

RE: INDUSTRI-PLEX SITE, BASELINE AIR SURVEY,INTERIM REPORT NO. 3

Gentlemen:

On behalf of the Industri-Plex Site Remedial Trust, we aresubmitting the attached Interim Report No. 3 for Pre-DesignInvestigation Task A-l, Baseline Air Survey. These data,along with data from future sampling rounds, are intendedto document the baseline air quality at the site prior toinitiation of Remedial Action.

If you have any questions, please contact us.

Very truly yours,

INC.

James W. Voss, PrincipalProject Director

RMG/JWV/bjtC:A-1CL

Attachments

cc: J. Naparstek, MDEPA. Ostrofsky, NUSD.L. Baumgartner, ISRTW.L. Smull, ISRT (w/o attachments)

GOLDER ASSOCIATES INC. • 20000 HORIZON WAY. SUITE 500. MT. LAUREL. NEW JERSEY 08054 • TELEPHONE (609) 273 1 110 • FACSIMILE (609) 273-0778

OFFICES IN UNITED STATES • CANADA • UNITED KINGDOM • SWEDEN • GERMANY • ITALY • AUSTRALIA

December 1990_________________-1-_____________893-6255

1.0 INTRODUCTION

1.1 ObjectivesOne of the requirements of the Consent Decree for theIndustri-Plex Site Pre-Design Investigation, as stated inthe Remedial Design/Action Plan (RDAP), is to conduct:

"a baseline investigation to establish aneffective air monitoring program and todetermine acceptable on-site and off-site airquality standards for hazardous volatilecompounds and/or other odorous compounds anddust relative to planned grading, consolidation,excavation, dredging, groundwater treatment andcapping activities."

A baseline air survey is being conducted under Pre-DesignInvestigation Task A-l to document the baseline conditionsrelative to potential types of emissions expected duringremedial action. Specifically, the air survey addressesAir Data Need No. 3 given on page 107 of the Pre-DesignWork Plan. Target Compound List volatile organiccompounds (TCL VOCs) constitute the hazardous volatilecompounds, and reduced sulfur compounds (includinghydrogen sulfide and methyl mercaptan) constitute themajor odorous compounds. The concentration of dust (aswell as the concentrations of arsenic, lead, and chromiumin dust) will also be determined.

Four rounds of air sampling are planned. This interimreport presents the methods and results for the thirdround of air sampling conducted in November 1990. Thefourth quarter sampling results will be included, alongwith all previous quarterly data and proposed air qualitystandards, in the Task A-l Interim Final Report.

Colder Associates

December 1990______________-2-___________893-6255

1.2 History and Source AreasPertinent site history regarding air quality and theresults of previous investigations are given in Section3.5.3.1 and Appendix A of the Pre-Design Work Plan. TheRecord of Decision (ROD) states that repeated complaintshave been received from local citizens in the past,especially southeast of the site, with respect tooffensive odors generated by the hide piles. Thesecomplaints have been associated with former sitedevelopment activities and rain storms. Increased odorsduring storms are believed to be largely due to exposureof fresh areas of the hide piles to the atmosphere afterslumping of the unstable slopes, and due to increasedemissions as a result of pressure gradients induced bylower barometric pressure during storms events.

The hide piles are a source of odors at the site. Thecomposition of the hide pile gas was determined during theRemedial Investigation, and the odorous areas andcompounds at the site were identified by soil gassampling/laboratory analysis and use of an odor panel.The East Hide Pile was determined to be the dominant odorsource. The odorous compounds were determined to bemainly hydrogen sulfide, which occurred at concentrationsof 5,600 to 21,000 ppm within the East Hide Pile.Hydrogen sulfide was not detectable above ground usingportable monitoring equipment. Methyl roercaptan wasdetected in East Hide Pile gas at concentrations rangingup to 150 ppm. Other mercaptan compounds were alsodetected at individual concentrations of up to 180 ppm.Benzene and toluene were detected in East Hide Pile gas at1 to 11 ppm. Additional compositional data for the EastHide Pile gas are being collected under Pre-DesignInvestigation Task A-2. The East Hide Pile remediation

Colder Associates

December 1990_______________-3-____________893-6255

will include a gas collection layer and a gas treatmentplant.

Benzene and toluene could also potentially be emitted fromthe groundwater treatment plant which will be installed inorder to remediate Hazardous Substances in groundwater.Dust, and metals in dust, might be introduced into the airduring site grading and capping activities that willremediate Hazardous Substances in soil.

Colder Associates

December 1990_______________-4-____________893-6255

2.0. FIELD METHODS

Sampling locations were selected based upon the results ofair dispersion modeling using regional meteorological dataconducted during the Remedial Investigation/FeasibilityStudy (RI/FS) and the historical locations of odorcomplaints. Sample locations were given in Figure 47 ofthe Pre-Design Work Plan. Some of the sampling pointswere slightly relocated based upon a field inspection byMr. Bob Glazier (Golder Associates Task Leader) and Mr.Arnie Ostrofsky (NUS Project Manager). The revisedlocations are given in Figure 1 of this report along withthe location numbers used in the laboratory report. Thefield duplicate of location 5 was designated locationnumber 13. The trip blank for the dust filter cassetteswas numbered 14, the spike cassette was numbered 15. Thetrip blank and spiked Summa canisters were not assignedsample location numbers.

Air samples were collected in accordance with theprocedures given in Section 5.1 and Attachment 1 of thePre-Design Investigation Field Sampling Plan (FSP).Samples were collected during a 24-hour period on November5-6 1990. Samples were not collected at location 12 dueto repeated vandalism or disturbance on previous samplingevents, and the lack of a suitable nearby public place asa replacement sampling location.

The sampler inlets were positioned at least three feetabove average grade by either placing them on top of largeisolated boulders (locations 2, 6, 7, and 8) or suspendingthem from low tree branches (locations l, 3, 4, 5, and 11)such that other nearby branches did not obstruct thesampler inlet ports. The sampler at location 10 wassuspended from the top of unused playground equipment inthe middle of an open field. At location 9, the samplers

Golder Associates

December 1990_______________-5-______;_____893-6255

were positioned on top of a overhang above the schooldoorway on the side of the school facing the Industri-PlexSite. The school principal previously indicated thatclassroom windows must be shut at times due to odors fromthe site.

All sampler inlets were facing into the wind at the startof sampling. A duplicate sample was collected for allanalyses at location 5, and a trip blank canister andfilter cassette accompanied the samplers on the round tripfrom lab to site and back to the lab. A Summa canisterspiked with the reduced sulfur analyses (hydrogen sulfide,me thy liner cap tan, dimethylsulfide, and dimethyldisulfide)was shipped to the site on the first day of sampling andback to the laboratory with the samples the following day.The spiked canister was analyzed last by the laboratory. .

TCL VOCs, methane, and reduced sulfur compounds werecollected in 15-liter Summa passivated canisters. Thevacuum flow regulators were calibrated to approximately 8milliliters per minute by the laboratory and the flowrate/vacuum pressure was recorded by the laboratory on thecanister chain-of-custody record prior to shipping. Thevacuum pressure was checked and recorded in the fieldprior to and after sampling. Upon receipt by thelaboratory, the vacuum pressure and vacuum flow regulatorcalibration were checked and recorded. Theseverifications are documented on the canister chain of-custody forms (given in the lab report in Appendix A) andin Table 1. Sampling was initiated by removing the inletvalve dust cover and opening the valve. The valve wasclosed and the inlet dust cover replaced approximately 24hours later. Chain of custody documentation was completedand the samples were sealed in shipping containers and

Colder Associates

December 1990_______________-6-____________893-6255

sent by overnight courier to Enseco's Air Toxicslaboratory in El Monte, California.

Dust was collected on filter cassette cartridges using anSKC Model 224-PCXR7 programmable personal sampling pump.The pump was set to a flow rate of 2 liters per minutejust prior to sampling using a rotameter which had beencalibrated to a primary standard (1000-ml film typeflowmeter). Correction of the flow rate to standard dryair conditions (760 mm Hg, 298 K [25 degrees Celsius], 0percent relative humidity) results in a flow rate of2028.6 ml/min using the time-weighted-average conditionsgiven in Section 6 below. The pump was programmed toalternately pump for one minute then shut down for twominutes such that approximately 977 liters of air wassampled over a period of 24-hours. Two separate pumpswere used to collect field duplicate dust samples atlocation 5. Twenty four hours after the start ofsampling, the pumps shut down, the inlet caps werereplaced on the cassettes, and they were shipped underchain of custody to Radian Corporation in ResearchTriangle Park, North Carolina by overnight courier. Theflow rate of each pump was checked after sampling. Theflow checks for the dust sampling pumps are documented inTable 1 and Appendix B. The final flow rate of all dustsampling pumps was within 12 percent of the original flowrate (see Table 1 and Appendix B).

.All samplers deployed on November 5, 1990, appeared to beintact and did not show evidence of tampering. The vacuumpressure of all Summa canisters were checked upon receiptat the laboratory and were within 2 inches of mercury ofthe value recorded in the field, except for the canistersat locations 10 and 11 which were within 4 inches ofmercury of the reading at the end of sampling (see Table 1

Colder Associates

December 1990_________________-7-_____________893-6255

and lab report in Appendix A). The flow rate of allvacuum flow regulators was within 7 percent of theoriginal flow rate, except for the canister at location 7,which was within 24 percent. The dust pumps at locations5 and 8 had prematurely discontinued sampling after 1212minutes and 1321 minutes respectively (out of a plannedtotal sampling period of 1440 minutes [24 hours]). Thepumping program (one minute on, two minutes off cycle) forthe dust pump at location 8 was not functioning properly.Therefore the pump sampled continuously for a period of1321 minutes (22 hours).

Colder Associates

December 1990_______________-8-____________893-6255

3.0 IAB METHODSSumma canister samples were received by Enseco on November7, 1990. Dust cassette samples were received by RadianCorporation on November 7, 1990. Samples were analyzed inaccordance with the procedures and analytical methodsgiven in the FSP and the QAPjP.

It was not possible to spike the Summa canisters with bothsulfur containing compounds and TCL VOCs because theywould react with each other. Therefore, because theodorous sulfur compounds are of greatest concern at thesite, the canisters were only spiked with the sulfurcompounds.

Laboratory Control Samples and Duplicate Control Sampleswere analyzed with each batch of samples from the site.

Colder Associates

December 1990_________________-9-_______;______893-6255

4.0 LAB RESULTSThe results of the analyses are presented in Appendix Aand summarized in Tables 2 and 3. Methane and reducedsulfur compounds were not detected in any of the samples.The following TCL VOCs were detected (maximumconcentrations detected in parentheses):trichlorofluoromethane (78 ppbv); l,l,2-trichloro-l,2,2-trifluoroethane (5.9 ppbv); 2-butanone (19 ppbv); 1,1,1-trichloroethane (3 ppbv); and toluene (23 ppbv). None ofthe above compounds were detected in the trip blank.Total dust measurements range from less than 10 to 267micrograms per cubic meter. However, the field blankcontained 100 ug of dust. The metals arsenic, lead, andchromium were not detected in any samples except for thesample from location 10 which contained 0.35 ug/m3,chromium. The reporting limits for arsenic, chromium, andlead were approximately 0.8 ug/m3, 0.1 ug/m3, and l.oug/m3, respectively.

Colder Associates

pecember 1990______________-10-__________893-6255

5.0 ASSESSMENT OF DATA USABILITYThere are no hold times for these analyses, but it wasplanned to analyze as many of the sensitive compounds aspossible within 72 hours of receipt by the lab. Sensitiveanalyses include TCL VOCs and reduced sulfur compounds.All of the twelve TCL VOC and sulfur compound samples wereanalyzed within 72 hours of receipt by the lab. Themethane analysis was conducted within 7 days after receiptby the lab. The sulfur compound stability studydocumented in the lab report indicates that sulfurcompounds might have been slightly affected by storage.However, no sample storage effects were noted on spikedcanisters stored for a period of seven days during thefirst round of sampling. Any corrections to the data willbe assessed when all four rounds of spike sample stabilitydata are available. There are no project-specific data tosupport such a conclusion for the TCL VOCs, but stabilitystudies have been performed for select TCL VOCs, and thesewill be included with the final report.

The Laboratory Control Samples (LCS) and Duplicate ControlSamples (DCS) for the TCL VOCs, reduced sulfur compounds,methane, and metals in dust (except lead) were within thecontrol limits, indicating that laboratory precision andaccuracy were acceptable. Reproducibility of the SummaCanister field duplicate is acceptable. All analyses inthe field duplicate pair were less than the methoddetection limit except for trichlorofluoromethane (Freon-11) which was detected in the sample from location 5, butnot in the duplicate sample designated location 13. Oneof the dust pumps in the field duplicate pair shut downprematurely, so there are no comparable field duplicatedata for dust.

Colder Associates

December 1990_______________-11-___________893-6255

As discussed above, spike recoveries were within controllimits for dimethylsulfide and dimethyldisulfide, butspike recoveries for hydrogen sulfide (26 percent) andmethylmercaptan (58 percent) were not within the specifiedcontrol limits. As discussed above, any corrections tothe data will be assessed when all four rounds of spikestability data are available.

The total dust measurement data are presented in Table 3.The data have been corrected by the laboratory for massloss in the blank filters (by adding the mass loss in theblanks) and for the actual volume of air sampled, whichvaried slightly at each location.

Data were reported for all samples. However, a sample wasnot collected at location 12 due to repeated tampering andvandalism. The overall data set is considered to becomplete. Data are reported in standard units and weredetermined using accepted procedures. Therefore, the dataare considered to be precise, accurate, comparable,complete, and representative of the conditions at the timeof sampling.

Colder Associates

December 1990_______________-12-___________893-6255

6.0 METEOROLOGICAL DATAMeteorological data, including wind speed and direction,relative humidity, temperature, and barometric pressurewere recorded by the site weather station during sampling.The data are presented in Appendix C.

The average temperature, barometric pressure, and humidityduring the sampling period were 59.41 degrees Fahrenheit(15.23 degrees centigrade), 29.92 inches of mercury (759.9mm Kg), and 74.02 percent (vapor pressure of water=9.59 mmHg), respectively. At the beginning of sampling (11:24),the dominant wind direction was from the west-northwestand the average wind speed was approximately 5 miles perhour (mph)• The wind speed/direction fluctuatedthroughout the sampling period but was from the east atthe end of sampling.

Colder Associates

December 1990______________-13-_____,______893-6255

7.0 DATA REDUCTION

The concentration data for methane, reduced sulfurcompounds, and TCL VOCs are reported by the laboratory inparts per million and parts per billion by volume (ppmv,ppbv) and therefore do not need to be corrected tostandard pressure and temperature. Relative humiditycorrections result in changes of less than 1 percent inthe results and have not been applied to the data becausethe accepted precision of the method can cause results todiffer by up to 20 percent. Data for dust have alreadybeen corrected to standard conditions by correcting theflow rate of the sampling pumps to standard conditions.

Colder Associates

December 1990________________-14-____________893-62S5

8.0 SUMMARYThe third round of air samples under Pre-Design Task A-lwere collected in accordance with the Pre-Design Work Planand Field Sampling Plan. All samples were analyzed inaccordance with the procedures given in the Field SamplingPlan. No reduced sulfur compounds or methane weredetected at any of the sample locations. The only TargetCompound List VOCs detected include trichlorofluoromethane(Freon 11); 1,1,2-trichloro-1,2,2-trifluoroethane (Freon113); 2-butanone (MEK); 1,1,1-trichloroethane; andtoluene. None of these compounds were detected in thetrip blank. The range in total dust concentrations wasless than 10 to 267 micrograms per cubic meter. Validdata were collected for all analyses at all locationsexcept location 12, which was not sampled. Location 12 isnot considered to be critical, and the data do not need tobe replaced. The dust data at sample locations 5 and 8 donot represent a full 24-hour time weighted average becausethe sampling pumps shut down prematurely. The dust dataat location 8 are for a 22-hour time weighted average, andsampled a larger volume of air than the other samplers dueto pump programming difficulties.

Colder Associates

TABLE 1SAMPLER CALIBRATION CHECKS

Sampler Flow Rate (ml/min) Vacuum Pressure(a)Type___Location Initial Final_____Lab___FieldSummaCanister

12345678910111213 (b)

7.17.37.27.37.37.17.57.57.37.37.2NA7.3

6.76.96.78.07.37.15.77.07.56.97.3NA6.8

30/1230/1430/1630/1530/1230/1530/1530/1430/1230/1330/13NA

30/15

30/1230/1530/1830/1630/1230/1530/1530/1630/1430/1730/16NA

30/16

Dust Pump(d) 1 572 573 574 575 576 577 578 579 5710 5711 5712 NA13(b) 5714(c) NA

5750605661575758605758NA56NA

NANANANANANANANANANANANANANA

NANANANANANANANANANANANANANA

Notes:(a) Readings given in inches of mercury. Data include

initial/final readings for each canister custodian (fieldand lab).

(b) Field duplicate of location 5.(c) Trip blank.(d) Flow rate values for dust pumps are original rotameter?: readings and have not been converted to ml/min.

Colder Associates

TABLE 2SUMMARY OF VOLATILE TARGET COMPOUND

LIST ANALYTES DETECTED DURING NOVEMBER 5-6, 1990

Concentration DetectionAnalyte Location (ppbv) Limit (ppbv)

Trichlorofluoromethane(Freon 11)

1457891011

218.07.2682.9781015

1

1,1,2-Trichloro-l,2,2-trifluoromethane(Freon 113) 1 5.9 2

1,1,l^Trichloroethane 9 3.0 2

2-Butanone (MEK) 10 19 3

Toluene 9 23 310 6.4

Note: See laboratory report in Appendix A for listing of compoundswhich were not detected and their respective detectionlimits.

Colder Associates

TABLE 3

TOTAL DUST MEASUREMENTS DURING NOVEMBER 5-6, 1990

Location

m

m

mvieldHankmMatrixipikemMatrix^pike

MethodBlank

m ——————Notes

m

-

l23456789101113

14

15

16

20

a.

b.

c.

d.

Pump ug dustPeriod collected(minutes)

477478480465404465475

1321 b480469480

f 470

0

0

0

0

ND aND20ND17050ND2026060ND70

100

ND

20

ND

ND - Not detected, detection limit=and 10 ug/m3 for dust concetration.

Sampler ran

Calculation

Calculation

continuously

: Minutes X Flow rate106 ml/m3

: ug of dust collected

Samplevolume

O ^i

.9676

.9697

.9737

.9433

.8196

.9433

.96362.6798.9737.9514.9737.9534

0

0

0

0

10 ug for ug

(2028.6)

= Dust Cone.

DustCone(ug/m3) d

NDND0.02ND13953.0ND

7.4626763.0 eND

73.4

NAg

NA

NA

NA

dust collected,

(ug/m3)": Vol sampled (m3)

e. Chromium =0.35 ug/m3

f. Field duplicate of location 5.

g. NA=Not Applicable.

Colder Associates

ODOR SOURCE AREASAMPLE LOCATIONAPPROXIMATE SITE BOUNDARY

WIND ROSE DIAGRAMBOSTON, MA

JOB NO. 893-6255DRAWN LASCHECKED

SCALE AS SHOWNOATE 07/06/00DWG NO MA01-096

AIR SAMPLE LOCATIONS

Colder Associates INDUSTRI-PLEX SITE REMEDIAL TRUSTFIGURE

APPENDIX A

LABORATORY REPORTS

ENSECO - AIR TOXICS LABORATORY REPORT

f Enseco —A Corning Company

rrrrrrrrrTTTTTTTT

Enseco - Air Toxics Laboratory9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

November 30, 1990

COLDER ASSOCIATES20000 Horizon Way, Ste. 500Mt. Laurel, NJ 08054ATTN: MR. BOB GLAZIER

ANALYSIS NO.: A9031101-001/014ANALYSES: Sulfur Compounds(GARB 16), Methane (SCAQMD Method25.2), Volatile Organics by GCMS -EPA TO14DATE SAMPLED: 24 hour compositesamples taken on 11/06/90DATE SAMPLE REC'D: 11/07/90

PROJECT: INDUSTRIPLEX

Enclosed with this letter is the report on the chemical and physicalanalyses on the samples from ANALYSIS NO: A9031101-001/014 as shown above.

The samples were received by Enseco - Air Toxics Laboratory, intact andand with the chain-of-custody record attached.

Please note that ND means not detected at the detection limit expressed.

REVIEWED PROVED

g|| The Report Cover Letter Is an Integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

I

r Enseco - Air Toxics Laboratory

A Coming Company

9537 Telstar Avenue, Suite 118 • El Monte, CA 91731(818) 442-8400 • FAX: (818) 442-3758r

rCOLDER ASSOCIATESr 20000 Horizon Way, Ste. 500Mt. Laurel, NJ 08054ATTN: MR. BOB GLAZIERr

r

LABORATORY REPORT

ANALYSIS NO. : A9031101-001/007ANALYSES: Sulfur CompoundsDATE SAMPLED: 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90SAMPLE TYPE: AirQC BATCH NO.: GC401-9011081

(CARB 16)

Sulfur Compoundsrr

Sample Identification

P 1P/A-1/001/000/3/3/6 A-069

r lP/A-1/002/000/3/3/6 A-071

1P/A-1/003/000/3/3/6 A-095

|» 1P/A-1/004/000/3/3/6 A-067

1P/A-1/005/000/3/3/6 A-068

P 1P/A-1/006/000/3/3/6 A-074

1P/A-1/007/000/3/3/6 A-077

I

rrrr

Resultsppm (vol/vol)

Hydrogen Methyl DimethylSulfide Mercaptan Sulfide

ND (0.02) ND (0.02) ND (0 .02)

ND (0 .02) ND (0.02) ND (0 .02)

ND (0 .02) ND (0 .02 ) ND (0 .02)

ND (0 .02) ND (0 .02 ) ND (0 .02)

ND (0.02) ND (0.02) ND (0.02)

ND (0 .02 ) ND (0 .02 ) ND (0 .02 )

ND (0 .02 ) ND (0 .02 ) ND (0 .02 )

DimethylDisulfide

ND (0 .02)

ND (0 .02)

ND (0 .02)

ND (0 .02)

ND (0.02)

ND (0 .02)

ND (0.0:2)

'A The Report Cover Letter Is an integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

^Enseco —,A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT


ANALYSIS NO.: A9031101-008/013ANALYSES: Sulfur Compounds (GARB 16)DATE SAMPLED: 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90SAMPLE TYPE: AirQC BATCH NO.: GC401-9011081

Sulfur Compounds

Resultsppm (vol/vol)

HydrogenSample Identification Sulfide

1P/A-1/008/000/3/3/6 A-078 ND (0.02)

1P/A-1/009/000/3/3/6 A-072 ND (0.02)

1P/A-1/010/000/3/3/6 A-073 ND (0.02)

1P/A-1/011/000/3/3/6 A-079 ND (0.02)

1P/A-1/013/000/3/3/6 A-075 ND (0.02)

1P/A-1/014/000/3/3/6 A-096 ND (0.02)

MethylMercaptan

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

DimethylSulfide

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

DimethylDisulfide

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

ND (0.02)

The Report Cover Letter Is an Integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse ol the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authoriration is

&/Enseco —A Coming Company

Enseco - Ait Toxics Laboratory9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

GOLDER ASSOCIATES20000 Horizon Way, Ste. 500

mMt. Laurel, NJ 08054ATTN: MR. BOB GLAZIER

rrrrrrrrrrrrr

ANALYSIS NO.: A9031101ANALYSES: Sulfur Compounds (CARB 16)DATE SAMPLED: 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90SAMPLE TYPE: AirQC BATCH NO.: GC401-9011081

Compounds

Hydrogen SulfideMethyl MercaptanDimethyl Sulfide

Limit

QC SUMMARYSulfur Compounds

LaboratoryControl Sample

% Recovery

9599103

80 - 115

DuplicateControl Sample% Recovery

8999104

80 - 115

RPD

701

20

i The Report Cover Letter to an integral part of this reportThis report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

ri^Enseco -A Coming Company


(818) 442-8400 • FAX: (818) 442-3758

Sulfur Compound Stability Study

A 15L Summa passivated stainless steel canister was spikedwith a measured volume of a standard gas mixture (Scott SpecialtyGas) containing four sulfur compounds (HoS, methyl mercaptan,dimethyl sulfide, and dimethyl disulfide). A known volume ofhydrocarbon free air was added to the canister to simulate anambient air matrix. The canister used for this study was identicalto those used for the Industriplex project sampled 11/06/90 at 13sample locations and identified by Enseco analysis IA9031101-001/013.(The canisters were manufactured by the same supplier, and were fromthe same lot).

The spiked canister was analyzed on 11/05/90. The canisterwas sent to the Industriplex site on 11/05/90. The canister wassent back to the laboratory on 11/06/90 and received by Enseco AirToxics Laboratory on 11/07/90. The spiked canister was analyzed on11/09/90. The results are summarized below:

Concentration (ppmv)

Hydrogen Methyl Dimethyl DimethylDate Sulfide Mercaptan Sulfide Disulfide

*11/05/90 1.1 1.2. 1.1 1.111/05/90 0.85 0.78 1.1 1.411/09/90 0.22 0.45 1.2 1.3

* Preparation date and theoretical concentration of spiked canister.

The Report Cover Letter Is an Integral part ol this reportThis report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted (or the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

1

r Enseco - Air Toxics Laboratory9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

r

— •*- L.1 O^VAJA Corning Company

LABORATORY REPORTf —— ... ., ,„.._


|B Mt. Laurel, NJ 080541 ATTN: MR. BOB GLAZIER1

rrr

SAMPLE IDENTIFICATION

f 1P/A-1/001/000/3/3/6 A-0691P/A-1/002/000/3/3/6 A-071r lP/A-1/003/000/3/3/6 A-095

1P/A-1/004/000/3/3/6 A-0671P/A-1/005/000/3/3/6 A-068

f 1P/A-1/006/000/3/3/6 A-074

1P/A-1/007/000/3/3/6 A-077r iP/A-1/008/000/3/3/6 A-0781P/A-1/009/000/3/3/6 A-072

— 1P/A-1/010/000/3/3/6 A-073r 1P/A-1/011/000/3/3/6 A-079

rrrrr

ANALYSIS NO.: A903110 1-001/011ANALYSES: Methane (SCAQMD Method 25.2)DATE SAMPLED: 24 hour composite samplestaken from 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/12/90SAMPLE TYPE: AirQC BATCH NO. : GC101-9011081

METHANE

SAMPLING TIME RESULTS11/06/90 (Composite) ppm

120011301320

124011551500

150014201535

12551335

(vol/vol)

ND(8)ND(8)ND(8)

ND(8)N D ( 8 )ND(8)

ND(8)ND(8)ND(8)

ND(8)ND(8)

;

g| The Report Cover Letter to an integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted lor the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

fe>Enseco —A Corning Company

___Enseco - Air Toxics Laboratory___9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A903110101-013/01520000 Horizon Way, Ste. 500 ANALYSES: Methane (SCAQMD Method 25.2)Mt. Laurel, NJ 08054 DATE SAMPLED: 24 hour composite samplesATTN: MR. BOB GLAZIER taken from 11/06/90

DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/13/90SAMPLE TYPE: AirQC BATCH NO.: GC101-9011081

METHANE

SAMPLING TIME RESULTSSAMPLE IDENTIFICATION 11/06/90 (Composite^ ppm fvol/voU

1P/A-1/013/000/3/3/6 A-075 1155 ND(8)1P/A-1/014/000/3/3/6 A-096 1530 ND(8)1P/A-1/015/000/3/3/6 A-076 1500 ND(8)

The Report Cover Letter is an Integral part ol this reportThis report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

r A Coming Company

TTTTTTTTTTTTTTTT1


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT


ANALYSIS NO.: A9031101ANALYSES: Methane (SCAQMD 25.2)DATE SAMPLED: 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/12/90, 11/13/90SAMPLE TYPE: AirQC BATCH NO.: GC101-9011081

Compounds

Methane

Limit

QC SUMMARYMethane

LaboratoryControl Sample% Recovery

96

80 - 120

DuplicateControl Sample

% Recovery

95

80 - 120

RPD

20

f* The Report Cover Letter is an integral part of this reportThis report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted (or the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

^Enseco —iA Coming Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-00120000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMSMt. Laurel, NJ 08054 EPA TO14ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90

DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90

Sample ID: 1P/A-1/001/000/3/3/6 SAMPLE TYPE: AirA-069 QC BATCH NO.: MS201-9011081

Volatile Organics by GCMS - EPA TO14

Results DetectionParameter ppb(v/v) Limit

Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.5l,2,-Dichloro-l/l/2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluorome thane———————————————Freon 11——— 21 1cis-l,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 5.9 2Acetone———————————————————————————————————————— ND 10Methylene Chloride ND 4trans-l,2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— ND 3Chloroform ND 21,1,1,-Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene—————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene————————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane——————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone—————————————————————————— ND 3

cont...

The Report Cover Letter Is an Integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

Enseco - Air Toxics Laboratory

A Coming Company

9537 Telstar Avenue, Suite 118 • El Monte, CA 91731(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT


• Mt. Laurel, NJ 08054ATTN: MR. BOB GLAZIER

"sample ID: 1P/A-1/001/000/3/3/6A-069

Volatile Oraanics

iParameter

F trans-1 , 3-Dichloropropene1,1,2-Trichloroe thane ——————— •Tetrachloroethene

r2-Hexanone ———————————————— -Dibromochlorome thane1 , 2-Dibromoethane ———————————r Chlorobenzene

Total XylenesStyrene ———————————————————r Bromoform1,1,2, 2-Tetrachloroethane ————Benzyl Chloride

1,3, 5-Trimethylbenzene1,2, 4-Trimethylbenzene ———————

m 1,3-Dichlorobenzene1,4-Dichlorobenzene —————————1 , 2-Dichlorobenzene1,2 , 4-Trichlorobenzene ———————

•» Hexachlorobutadiene

F"

•

1

ANALYSIS NO.: A9031101-001ANALYSES: Volatile Organics by GCMS -EPA TO 14DATE SAMPLED: 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90SAMPLE TYPE: AirQC BATCH NO.: MS201-9011081

bv GCMS - EPA TO 14

Results Detectionppb ( v/ v ) Limit

————————————— ND 3ND 3

ND 3. ————————————— ND 5

ND 3

ND 2.5___ ______ ___ Mn 9 R

ND 5

ND 2

ND 2—————————————— ND 4

ND 2.5

ND 3. ————————————— ND 4

ND 5

ND 5

ill The Report Cover Letter Is an Integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

i^Enseco-A Coming Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

GOLDER ASSOCIATES ANALYSIS NO.: A9031101-00220000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMSMt. Laurel, NJ 08054 EPA T014ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90





Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.51,2,-Dichloro-l,!,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane—————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— ND 1cis-l,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone—————————————————————————————————————— ND 10Methylene Chloride ND 4trans-l/2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate——————————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone—————————————————————————————————————— ND 3Chloroform ND 21, 1,1, -Trichloroethane——————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene—————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene——————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane——————————————————————————— ND 2cis-l/3-Dichloropropene ND 34-Methyl-2-Pentanone————————————————————————————— ND 3

cont...

The Report Cover Letter Is an Integral part ol this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

;-l/Enseco —iA Corning Company

rirrrrf


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-00220000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMSMt. Laurel, NJ 08054 EPA T014ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90



Volatile Organics bv GCMS - EPA TO14

rrrrr••*•m

g

Parameter

trans-1, 3-Dichloropropene1,1, 2-Trichloroethane ————————————Tetrachloroethene2-Hexanone —————————————————————Dibroraochlorome thane1 , 2-Dibromoethane ———————————————Chlorobenzene

Total XylenesStyrene ———————————————————————Bromoform1,1,2, 2-Tetrachloroethane —————————Benzyl Chloride4 -Ethyl Toluene ——————————————————1,3, 5-Trimethylbenzene1,2, 4-Trimethylbenzene ———————————1 , 3-Dichlorobenzene1 , 4-Dichlorobenzene —————————————1 , 2 -Dichloro benzene1,2, 4-Trichlorobenzene ———————————Hexachlorobutadiene

Resultsppb(v/v)

ND———————— ND

ND———————— ND

ND————————— ND

ND

ND

ND———————— ND

ND————————— ND

ND————————— ND

ND

ND————————— ND

ND

DetectionLimit

33335322.52.55724242.5334575

if| The Report Cover Letter Is an integral part o( this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse ol the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

A Coming Company

Enseco - Air Toxics Laboratory___9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Oroanics by GCMS - EPA TO14


Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.5l,2,-Dichloro-l,l,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— ND 1cis-l,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone————————————————————————————————————— ND 10Methylene Chloride ND 4trans-l,2-Dichloroethene——————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— ND 3Chloroform ND 21,1,1,-Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene———————————————————————————————————•—— ND 31,2-Dichloroethane ND 2Trichloroethene——————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane—————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone——————————————————————————— ND 3

cont...

The Report Cover Letter Is an Integral part ol this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted (or the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

^Enseco —A Coming Company

rrrrrrrrrrrrrrrrr


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

GOLDER ASSOCIATES ANALYSIS NO.: A9031101-00320000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMSMt. Laurel, NJ 08054 EPA TO14ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90





Toluene——————————————————————————————— ND 3trans-l,3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone—————————————————————————————— ND 5Dibromochlororaethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene——————————————————————————— ND 2.5Total Xylenes ND 5Styrene———————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane————————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene————————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene—————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene———————————————————— ND 7Hexachlorobutadiene ND 5

IlK The Report Cover Letter Is an Integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

A Coming Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Oraanics bv GCMS - EPA TO 14


Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.5l^j-Dichloro-ljl^^-Tetrafluoroethane—Preon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane—————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— 8.0 1c is-1,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 101,lf2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone—————————————————————————————————————— ND 10Methylene Chloride ND 4trans-l,2-Dichloroethene——————————————————————— ND 4lf1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone—————————————————————————————————————— ND 3Chloroform ND 21,1,1, -Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene—————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene——————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane——————————————————————————— ND 2cis-1,3-Dichloropropene ND 34-Methyl-2-Pentanone—————————————————————————— ND 3

cont...

The Report Cover Letter to an integral part of this report.This report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusiveuse of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

^Enseco -A Corning Company

rrrrrrrrrrr


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




r

Volatile Orcranics bv GCMS - EPA TO 14


Toluene—————————————————————————————————— ND 3trans-l,3-Dichloropropene ND 31,1,2-Trichloroethane——————————————————— ND 3Tetrachloroethene ND 32-Hexanone————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene——————————————————————————— ND 2.5Total Xylenes ND 5Styrene———————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane————————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene————————————————————————— ND 41,3,5-Triraethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

t The Report Cover Letter Is an Integral part of this report,report pertains only to the samples investigated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusive

use of the client to whom it is addressed. Any reproduction of this report or use of this Laboratory's name for advertising or publicity purposes without authorization is prohibited.

^Enseco —A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-00520000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS -Mt. Laurel, NJ 08054 EPA T014ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90



Volatile Orcranics by GCMS - EPA TO 14


Dichlorodifluorome thane——————————————Freon 12——— ND 2Chloromethane ND 2.5l,2,-Dichloro-l,l,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromoraethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— 7.2 1cis-lf2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l/l^-Trichloro-l^^-Trifluoroethane Freon 113 ND 2Acetone————————————————————————————————————— ND 10Methylene Chloride ND 4trans-1,2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate————————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone—————————————————————————————————— ND 3 ,Chloroform ND 21,1,1 r -Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene——————————————————————————-———— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane——————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone——————————————————————————— ND 3

cont...

TThe Report Cover Letter Is an Integral part of this report.

This reoort oertains only to the samples investiqated and does not necessarily apply to other apparently identical or similar materials. This report is submitted (or the exclusive

A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Oroanics by GCMS - EPA T014


Toluene—————————————————————————————————— ND 3trans-l,3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene———————————————————————————— ND 2.5Total Xylenes ND 5Styrene—————————————————————————————— ND 7Bromoform ND 2l,l,2f 2-Tetrachloroethane———————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter Is an Integral part of this report.Ana* nnt nofoccarilv annlv «o nthor annarontlu iripntiral nr similar materials This rpnort is submitted for Itlfi exclusive

A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Oraanics by GCMS - EPA TO14


Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.5l,2,-Dichloro-l,l,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane—————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— ND 1cis-1,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone—————————————————————————————————————— ND 10Methylene Chloride ND 4trans-1,2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate—————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— ND 3Chloroform ND 21,1,1,-Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene————————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichlorome thane——————————————————————————— ND 2cis-1,3-Dichloropropene ND 34-Methyl-2-Pentanone——————————————————————————— ND 3

cont...

TThe Report Cover Letter I* an Integral part o( this report.

oniu in the samnles invfistioated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusive



(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-00620000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMSMt. Laurel, NJ 08054 EPA TO 14ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90





Toluene——————————————————————————————— ND 3trans-l,3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone——————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene——————————————————————————— ND 2.5Total Xylenes ND 5Styrene——————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane————————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene—————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene———————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter Is an Integral part of this report



(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-00720000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS -Mt. Laurel, NJ 08054 EPA TO 14ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90





Dichlorodifluorome thane——————————————Freon 12——— ND 2Chloromethane ND 2.51,2,-Dichloro-l,1,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluorome thane———————————————Freon 11——— 68 1cis-l,2-Dichloroethene ND 2Carbon Disulfide——————•——————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone————————————————————————————————————— ND 10Methylene Chloride ND 4trans-l/2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate——————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— ND 3 .Chloroform ND 2 "1,1,1, -Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene——————————————————————————————— ND 2.5lf2-Dichloropropane ND 8Bromodichloromethane—————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone——————————————————————————— ND 3

cont... «

The Report Cover Letter to an Integral part ot this report.nniu tn tho <samnlp.<! invfistioated and does not necessarily apply to other apparently identical or similar materials. This report is submitted for the exclusi'

%>Enseco —,A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT






Toluene—————————————————————————————————— ND 3trans-l/3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene———————————————————————————— ND 2.5Total Xylenes ND 5Styrene——————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane——————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene—————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter Is an Integral part of this report.

A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT






Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.51,2,-Dichloro-l,1,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane—————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— 2.9 1cis-l,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 101,1,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone———————————————————————————————————————— ND 10Methylene Chloride ND 4trans-l,2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— ND 3Chloroform ND 2 *j»1,1,1, -Trichloroethane————————————————————————— ND 2 |Carbon Tetrachloride ND 2Benzene————————————————————————————————————— ND 3 m1,2-Dichloroethane ND 2 TTrichloroethene—————————————————————————————— ND 2.5 '1,2-Dichloropropane ND 8Bromodichloromethane—————————————————————————— ND 2 *fcis-l,3-Dichloropropene ND 3 |4-Methyl-2-Pentanone——————————————————————————— ND 3

cont... w

1The Report Cover Letter Is an Integral part of this report.

jnat nnt nprp-;<;ariiv anolv to other aooarentlv identical or similar materials. This report is submitted for the exclusive

^Enseco-A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT






Toluene——————————————————————————————— ND 3trans-l/3-Dichloropropene ND 3lf 1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone——————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane———————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene——————————————————————————— ND 2.5Total Xylenes ND 5Styrene———————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane————————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene———————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene—————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene———————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter Is an Integral part of thto report.

A Corning Company

___Enseco - Air Toxics Laboratory_____9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Oroanics by GCMS - EPA TO14j>


Dichlorodifluoromethane—————————————Freon 12—— ND 2Chloromethane ND 2.51,2,-Dichloro-l,l,2f2-Tetra£luoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— 78 1cis-1,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone—————————t——.——————————-——————————- ND 10Methylene Chloride ND 4trans-1,2-Dichloroethene——————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone—————————————————————————————————— ND 3 »Chloroform llD 21,1,1,-Trichloroethane————————————————————————— 3.0 2Carbon Tetrachloride ND 2Benzene—————————————————————————————————————— ND 31,2-Difchloroethane ND 2Trichloroethene——————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane—————————————————————————— ND 2cis-l,3-Dichloropropene r ND 34-Methyl-2-Pentanone————————————————————.—-———— ND 3

cont...

r

The Report Cover Letter Is an integral part of this report.Ana* nnt npwwariiv anniv to other aooarentlv identical or simitar materials. This report is submitted for the exclusive

t^Enseco-A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Ororanics by GCMS - EPA TO 14


Toluene———————————————————————————————— 23 3trans-l,3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane———————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene———————————————————————————— ND 2.5Total Xylenes ND 5Styrene—————————————————————————————— ND 7Bromoform ND 21,1,2,2 -Tetrachloroethane———————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene—————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter 1$ an Integral part of this report.



(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-01020000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS -Mt. Laurel, NJ 08054 EPA TO14ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90





Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.51,2,-Dichloro-1,1,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— 10 1cis-l,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 101,1,2-Trichloro-1,2,2-Trifluoroethane Freon 113 ND 2Acetone————————<———————————————————————————— ND 10Methylene Chloride ND 4trans-l,2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— 19 3 v,Chloroform ND 21,1,1,-Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene—————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane—————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone——————————————————————————— ND 3

cont... i

The Report Cover Letter is an Integral part ol this report- - ; • . . .__• . , ._ _.i—„—„,„„«„ Montirai nr similar materials This reoort is submitted for the exclusi

%Enseco-A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT






Toluene———————————————————————————————— 6.4 3trans-l/3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone——————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene————————————————————————————— ND 2.5Total Xylenes ND 5Styrene——————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane————————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 3 :1.3-Dichlorobenzene ND 31.4-Dichlorobenzene————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter to an Integral part of this report.

^Enseoo —A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-01120000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS - ,_,Mt. Laurel, NJ 08054 EPA T014 JATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90 '



Volatile Orcranics by GCMS - EPA T014


Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.51,2,-Dichloro-1,1,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorof luoromethane———————————————Freon 11——— 15 1cis-l,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 101,1,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone——————————————————————————————————— ND 10Methylene Chloride ND 4trans-l,2-Dichloroethene——————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate——————————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone—————————————————————————————————— ND 3 -.Chloroform ND 21,1,1,-Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene—————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene————————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane——————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone————————————————————————————— ND 3

cont...

The Report Cover Letter is an Integral part of this report. ............ —i.. ,„ ^n.nr -,„„„„„)!„ iHoniirai nr similar materials. This reoort is submitted for the exclimiv

A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Orcranics bv GCMS - EPA TO 14


Toluene—————————————————————————————————— ND 3trans-l,3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone——————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane———————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene————————————————————————————— ND 2.5Total Xylenes ND 5Styrene——————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane———————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene———————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter is an Integral part of this report.- i__. _-» -—_,...•> .•;!.. «^l,, «« rtm«, ^—nmntltr iHonli^ol r,r ojr^itor motnriak ThtQ rpnnrt ic cithmittpH fnr ihp

A Corning Company


(818) 442-8400 « FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A9031101-01220000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS - !

Mt. Laurel, NJ 08054 EPA T014 j""ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90 I

DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90 p


Volatile Oraanics by GCMS - EPA TO14 - '

Results Detection "PParameter ppb(v/v) Limit |

Dichlorodifluoromethane——————————————Freon 12——— ND 2Chloromethane ND 2.5l,2,-Dichloro-l,l,2,2-Tetrafluoroethane—Freon 114—— ND 2Vinyl Chloride ND 2.5Bromomethane————————————————————————————————— ND 3Chloroethane ND 5Trichlorofluoromethane———————————————Freon 11——— ND 1cis-1,2-Dichloroethene ND 2Carbon Disulfide—————————————————————————————— ND 10l,l,2-Trichloro-l,2,2-Trifluoroethane Freon 113 ND 2Acetone—————————————————————————————————————— ND 10Methylene Chloride ND 4trans-1,2-Dichloroethene———————————————————————— ND 41,1-Dichloroethane ND 2.5Vinyl Acetate———————————————————————————————— ND 2.51,1-Dichloroethene ND 22-Butanone——————————————————————————————————— ND 3Chloroform ND 21,1,1, -Trichloroethane————————————————————————— ND 2Carbon Tetrachloride ND 2Benzene————————————————————————————————————— ND 31,2-Dichloroethane ND 2Trichloroethene————————————————————————————————— ND 2.51,2-Dichloropropane ND 8Bromodichloromethane—————————————————————————— ND 2cis-l,3-Dichloropropene ND 34-Methyl-2-Pentanone——————————————————————————— ND 3

cont...

The Report Cover Letter Is an Integral part of this reportj— „„, noroccariiu anniv to other aooarently identical or similar materials. This report is submitted for the exclusi

A Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT




Volatile Oroanics by GCMS - EPA TO 14


Toluene—————————————————————————————————— ND 3trans-1,3-Dichloropropene ND 31,1,2-Trichloroethane———————————————————— ND 3Tetrachloroethene ND 32-Hexanone—————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane———————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene———————————————————————————— ND 2.5Total Xylenes ND 5Styrene—————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane————————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 3 :1.3-Dichlorobenzene ND 31.4-Dichlorobenzene—————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Utter Is an Integral part of this report,JA«*- r*rt* r«nin<<f nrili* i^nltf *^ *i*Knr •mnirnntU I lHrtr»tif«al nr pinrtilaf moional^ 1 Hl

Enseco - Air Toxics Laboratory

f^/


LABORATORY REPORT

GOLDER ASSOCIATES20000 Horizon Way, Ste. 500Mt. Laurel, NJ 08054ATTN: MR. BOB GLAZIER

Sample ID: 1P/A-1/014/000/3/3/6A-096

Volatile Organics

Parameter

Y\ { f^ \\ 1 f* Tf*f\f^ 4 f 1 n f^ Y*/"M!HP^+" V^ 71 T^/^

ANALYSIS NO.: A9031101-013ANALYSES: Volatile OrganicsEPA TO 14DATE SAMPLED: 11/06/90DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/09/90SAMPLE TYPE: AirQC BATCH NO.: MS201-9011091

by GCMS - EPA

Chloromethane1,2, -Dichloro-1 , 1,2 , 2 -Tetraf luoroethane — FreonVinyl Chloride

ChloroethaneTrichlorofluoromethane ——————cis-l,2-Dichloroethene

1, 1,2-Trichloro-l, 2, 2-Trif luoroethane Freon

Methylene Chloridetrans-l,2-Dichloroethene —————1 , 1-Dichloroethane

1 , 1-Dichloroethene2-Butanone ———————————————— •Chloroform1 1 1 ^*PY"* "1 Vl 1 /^T'/^O'f* Vl 7% Yl A

Carbon TetrachlorideT^ ft in rm *"* ** *"^

1 , 2-Dichloroethane

1 , 2-DichloropropaneBromodichloromethane ———————— •cis-l,3-Dichloropropene4 -Methyl-2 -Pentanone ————————— -

T014

Resultsppb(v/v)

12 ——— NDND

114 —— NDND

ND11 ——— ND

ND—————— ND

113 ND—————— ND

ND

ND—————— ND

ND

ND—————— ND

ND—————— ND

ND—————— ND

ND—————— ND

ND—————— ND

COl

*a 4. f-1 nc^w^^LL,\ IbCXXJ ~A Corning Company

'

i

'by GCMS - .

•

———— 1Detection !Limit 1

o toi2.5 |22.5 «

I "1 -2

102

10 «•442.5 M2.52r- -223 K22.5

1 •33

it ... "•

The Report Cover Letter Is an Integral part oi this report.-------—>i..:j— l ;--'-'<-'""iior motoriaU Thi<s rpnnrt issnhmitted forthe exclm'

l^Enseoo—iA Corning Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT






Toluene——————————————————————————————— ND 3trans-l/3-Dichloropropene ND 31,1,2-Trichloroethane——————————————————— ND 3Tetrachloroethene ND 32-Hexanone—————————————————————————————— ND 5Dibromochloromethane ND 31,2-Dibromoethane——————————————————————— ND 2Chlorobenzene ND 2.5Ethylbenzene——————————————————————————— ND 2.5Total Xylenes ND 5Styrene———————————————————————————————— ND 7Bromoform ND 21,1,2,2-Tetrachloroethane———————————————— ND 4Benzyl Chloride ND 24-Ethyl Toluene——————————————————————————— ND 41,3,5-Trimethylbenzene ND 2.51,2,4-Trimethylbenzene——————————————————— ND 31.3-Dichlorobenzene ND 31.4-Dichlorobenzene————————————————————— ND 41,2-Dichlorobenzene ND 51,2,4-Trichlorobenzene——————————————————— ND 7Hexachlorobutadiene ND 5

The Report Cover Letter Is an Integral part of this report.

A Coming Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A903110120000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS -Mt. Laurel, NJ 08054 EPA T014ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90

DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/08/90SAMPLE TYPE: AirQC BATCH NO.: MS201-9011081

T

QC SUMMARYVolatile Organics by GCMS

EPA TO 14

Laboratory Duplicate IControl Sample Control Sample

Compounds % Recovery % Recovery RPD •*

Methylene Chloride 106 105 11,1 Dichloroethene 107 107 1 *Trichloroethene 102 102 1 |Toluene 100 100 0 '1,1,2,2-Tetrachlorethane 100 104 4 - ..

Limits 80 - 115 80 - 115 20

The Report Cover Letter Is an integral part ol this report' ' - • « - _ , _ _ _ — „*!., ifinnt't^&t r>f fimilor motusialc- Th»*> fftnnrt ic cjihmiHo/4 Irtr t

^Enseco-A Coming Company


(818) 442-8400 • FAX: (818) 442-3758

LABORATORY REPORT

COLDER ASSOCIATES ANALYSIS NO.: A903110120000 Horizon Way, Ste. 500 ANALYSES: Volatile Organics by GCMS -Mt. Laurel, NJ 08054 EPA T014ATTN: MR. BOB GLAZIER DATE SAMPLED: 11/06/90

DATE SAMPLE REC'D: 11/07/90DATE ANALYZED: 11/09/90SAMPLE TYPE: AirQC BATCH NO.: MS201-9011091

QC SUMMARYVolatile Organics by GCMS

EPA TO14

Laboratory DuplicateControl Sample Control Sample

Compounds % Recovery % Recovery RPD

Methylene Chloride 97 105 81,1 Dichloroethene 100 105 5Trichloroethene 106 105 1Toluene 112 112 11,1,2,2-Tetrachlorethane 112 115 3

Limits 80 - 115 80 - 115 20

The Report Cover Letter Is an Integral part of this report

110) -013 EnseooCanister Chain of Custody and

Field Data Record 5(Grab Samples)

Client

Canister Serial » A ~

Page of

Date Cleaned o

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CDFR1Enseco, Inc. - Air Toxics Laboratory

9537 Tetstar Avenue, iiuile 118 • El Monte. CA 91731(818)442-8400 • FAX: (818) 442-3758

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CDFR1Enseco, Inc. - Air Toxics Laboratory

9537 Telsfar Avenue, Suite 118 • Hi Monle. CA 91731(818) 442-8400 • FAX: (818) 442-3758

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CFDREnseco, Inc. - Air Toxics Laboratory

9537 Telstar Avenue. Suite 118 • El Monte, CA 91731(818)442-8400 • FAX: (818) 442-3758

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9537 Telstar Avenue, Suite 118 • El Monte, CA 91731(818)442-8400 • FAX: (818) 442-3758


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9537 Telstar Avenue, Suite 118 • El Monte. CA 91731(818)442-8400 • FAX: (818) 442-3758

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Enseco, Inc. - Air Toxics Laboratory9537 Telstar Avenue, Suite 118 • El Monte, CA 91731

(818)442-8400 • FAX: (818) 442-3758


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Enscco, Inc. - Air Toxics Laboratory9537 Telstar Avenue, Suite 118 « El Motile, CA 91731

(818) 442-8400 • FAX: (818) 442-3758

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(818)442-8400 • FAX: (818) 442-3758

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(818) 442-8400 • FAX: (818) 442-3758

^Enseco •™6

A CORNING Company

Q % coin \q| l»n GnA 92641JHD 2810 Bunsen Ave.. Unit A Ventura. CA 930037(805) 650-0548D 232S Skyway Or., Unit K. Santa Maria. CA 93455, (805) 922-2776X 9537 Telstar Ave., Unit 118, El Monte, CA 91731, (818) 442-8400D Mobile Labs, (800) ENSECO-8

OEr.llSTQnY RECORD| rLab

CLIENTADDRESS ^01000

CONTRACT / PURCHASE ORDER / QUOTE ft

Sample No. /Identification Date Time

Lab SampleNumber

PROJECT MANAGER

/4v</<t ANALYSES

LIQ. AIR SOLIDCondition/

REMARKS

— 01})

X<.•> 3

WO -co'i-OS?

A-ony-007

4-07* X -co 3V X" -06?

A-fi-73 x- x -o/oSAMPLERS: (Signature)

Relinquished bv: (Signature) 0

Received by: (Signature)


Date Time

Date Time

The delivery of samples and the signature on this chainof custody form constitutes authorization to perform theanalyses specified above under the Enseco Terms andConditions, unless a contract or purchase order has beenexecuted and is cited above.

Relinquished by: (Signature) Date Time Received for Laboratory by: Date RECEIVED Time Date ACCEPTED Time

Method of Shipment:

Special Instructions:

T ~7Z

COC^

SAMPLE DISPOSITION:1. Storage time requested:. .days(Samples will be stored for 30 days without additional charges;thereafter storage charges will be billed at the published rates.)2. Sample to be returned to client: Y (?S)(Enseco will dispose of unreturned samples at no extra charge.Disposal will be by incineration wherever possible; otherwise, asappropriate, according to legal requirements.)

DISTRIBUTION: White with report, Yellow to Enseco, Pink to Courier, Gold to Sample Control

EnsecoA CORNING Company

Q 7440 Lincoln Way, Garden Grove, CA 92641, (714) 898-6370Q 2810 Bunssn Ave., Unit A Ventura. CA 93003, (80S) 650-0546D 2325 Skyway Or., Unit K, Santa Maria. CA 93455, (805) 922-2778» 9537 Telstar Ave., Unit 118, El Monte, CA 91731, (818) 442-8400O Mobile Labs, (800) ENSECO-8

Date.

CHAIN OF CUSTODY RECORD

r?=_0L__Page_

Lab Number.

CLIENT PROJECT MANAGER

ADDRESSANALYSES

PHONE NUMBER

PROJECT NAME

CONTRACT / PURCHASE ORDER / QUOTE #SITE CONTACT

Sample No. /Identification Date Time

Lab SampleNumber

SAMPLE TYPE

LIQ. AIR SOLID

No. ofCon-

tainersSample Condition/

REMARKS

Mo X

\ttfr\f WlQ X?

(JOuL -ft

A -070 A<rf-

SAMPLERS: (Signature)

Relinquished by: (Signature)



Date Time(730

Date Time

The delivery of samples and the signature on this chainof custody form constitutes authorization to perform theanalyses specified above under the Enseco Terms andConditions, unless a contract or purchase order has beenexecuted and is cited above.

Relinquished by: (Signature) Date Time Received for Laboratory by:

4Date RECEIVED Time Date ACCEPTED Time

Method of Shipment:

Special Instructions:

SAMPLE DISPOSITION:1. Storage time requested:. .days(Samples will be stored for 30 days without additional charges;thereafter storage charges will be billed at the published rates.)2. Sample to be returned to client: Y Qy(Enseco will dispose of unreturned samples at no extra charge.Disposal will be by incineration wherever possible; otherwise, asappropriate, according to legal requirements.)

DISTRIBUTION: White with report, Yellow to Enseco, Pink to Courier, Gold to Sample ControlV i f f f f f

RADIAN CORPORATION LABORATORY REPORT

DUST SAMPLE LOCATION NUMBER AS GIVENIN RADIAN CORPORATION LABORATORY REPORT

DUST CASSETTESAMPLE LOCATION NO. SAMPLE IDENTIFICATION NUMBER

*

1 #03-212 03-223 03-234 03-245 03-256 03-267 03-278 03-289 03-2910 03-3011 03-3113 (field duplicate) 03-3314 (field blank) 03-3215 (spike) 03-34, 03-35

Colder Associates

RADIANRadian Work Order PC-11-026

Analytical Report12/07/90

Colder Associates, Inc.

Colder Associates, Inc.Colder Associates, Inc.20000 Horizon Way, Suite 500t(T Laurel. NJ 08054Bob Claiier

Customer Uork Identification Industri-PlexPurchase Order Number -

123^

Contents:

Analytical Data SumnarySample HistoryCcxmems SummaryNotes and Definitions

Radian Analytical Services900 Perimeter ParkHorrisville, NC 27S60

919-481-0212

Client Services Coordinator: JSGIB

Certified by

RADIANAnalytic*! Data Sumary Page: 2

1 Colder Associates, Inc.Radian Work Order: PO-11-026

MethodslCP 25 element «can (1) : ;listtlCP List - Inductri Plex

Sanple 10: *03-21 W3-22 W3-23 *03-24

factor: 0.00001 0.00001 0.00001 0.00001Results in: total aq total »a total mg total mg

OU 02A 03A 04AMatrix: filter filter filter filter

ArsenicChromiumLead

Result Oet. Unit Result Ott. Limit Result Oct. limit Result Det. LimitNO HHH M> flip "0 0.0008 ND 0 0008NO liiit ND pJool NO 0.0001 NO Milwo b.0010 NO 0.0010 NO IIP NO ill!

NO Not detected at specified detection Unit

(1) For a detailed description of flags and technical term in this report refer to Appendix A in this report.

RADIAN

Colder Associates, Inc.Radian Work Order: PO-11-026

Analytical Data Summary Page: 3

Method: ICP 25 element scan (1)List:lC»> List - Industri Plex

Sample ID: #03-25 «03-26 *03-27 #03-28

Factor: 0.00001 0.00001 0.00001 0.00001Results in: total «8 total ng total mg total mg

05A 06A 07* 08*Hatrix: filter filter filter filter

ArsenicChromiumLead

I, ————————————— : ———————————

Result Det. UnitND O-it'OQQBND 1 oboiND O^OOI 0

Result Det. LimitND fipND «;OQ01ND tfiisjo

Result Det. LinitND orooosND 0:0001NO 6.0010

Result Det. LimitND 0.0008ND 0.0001ND 0.0010

———————————————————— ,|

NO Not detected at specified detection Knit

(1) For a detailed description of flags and technical terns in this report refer to Appendix A in this report.

RADIANAnalytical Data Summary Page: 4


Method: I CP 25 element scan (1) :ListilCP List !• Industri Plex

Sanple ID: #03-29 #03-30 #03-31 #03-33

factor: 0.00001 0.00001 0.00001 0.00001Results in: , total tig total mg total ng total mg

09A 10A 11A 12AMatrix: filter filter filter filter

ArsenicChromiumlead

Result Oet. Limit Result Det. Limit Result Oct. Limit Result Oet. limitM<::-:-s--:-*--» £>*•*•:•:•::>:•:-:• >»:•:;:•:::•:•::>:*:: >:••".>-•:-:;-:.:-:.:

NO 0.0008 ND 0.0008 NO 0.0008 NO 0.0008*:**« *Wv*S<: *:¥;•>*:-::« ::;*i~i-:X«NO fi||00j 0.00035 a ojowi NO |i|op01 NO p;;oogr

NO bloBio ND Iffii NO JHofb NO |ttid

NO Mot detected at specified detection Unit 8 Est. result less than 5 times detection limit

(1) For • detailed description of flags and technical terns in this report refer to Appendix A in this report.

RADIAN

1 Colder Associates, inc.Radian Work Order: PO-11-026

1

Analytical Data Sumary Page: S

•tethod:ICP 25 element «can (1) . ... . . 'XYi'>:.:: •"•.:•'...,-List:lCP List - Industri Plex

Sample IB: #03-32 (FIELD W3-34 (MATRI- *03-35 (HATR1- METHOD BLANK- BUNK) X SPUE) » SPIKE DUP)

Factor: 0.00001 0 0 0.00001Results in: total mo X rec X rec total mg

ISA UA ISA 20*Matrix: filter filter filter fitter

ArsenicChromiumLead

Result Oct. Limit Result Oct. Limit Result Det. Limit Result Det. Limit» 111 «.2 fill 78.6 HI NO IPND pfOMt «7.2 81.5 NO 6 JND filbolii 17.0 19.6 ND WX

NO Not detected at specified detection limit

(1) For a detailed description of flags and technical terms in this report refer to Appendix A in this report.

RADIAN


Analytical Data Summary Page:6

Kethod/Analyte

Matrix

#03-21

01AIR

: Sample Identifications

#03-22 #03-23

02AIR

03AIR

NIOSN Method 0500Total Dust

Result

NO

Det. Limit

WX*Xi*-Z3total ing OiCIO i

Result

NO

Det. Limitx;:->:j««.:-:-»a<K;

total mg q31|0;f|j

Result

.02 a

Get. Limit

total «9 |*fjb!1

MO Not detected at specified detection (tnit a Est. result less than 5 times detection limit

(1) for a detailed description of flags »nd technical terns in this report refer to the glossary.

RADIANAnalytical Data Sunmary Page:?


. •• . '•' :: ••'•'•'•.• • • ' ' ' ' '. ' : .: . -:v-~:;: /•. -< •.:;»•':' :;.;iiv , .. '. •-•: .. .Sample Identifications .-:. . . .Method/ Ana lyte :

#03-24 «03-25 #03-26

<K 05 06Matrix : AIR AIR AIR

KIOSK Method 0500Total Oust

Result Det. Limit Result Oct. Linit Result Get. limit

NO total ng OfSlfSi .17 total mg O dlflBl .05 total mg blb ulll

NO Not detected at specif ied detection Unit

<1) For • detailed description of flags and technical terms in this report refer to the glossary.

RADIAN


Analytical Data Summary Page:8

Method/Ana lyte

Matrix

*03-27

orAIR

Sample Identifications

#03-28 *03-29

AIR0VAIR

NIOSH Method 0500Total Oust

Result

NO

Det. Limit Result Oet. Limit Result

total lag i .02 8 total ma 016:

Det. Limit

SfiX£?.*.:f.fy,total mg 0.010;

NO Mot detected at specified detection limit a Est. result less than 5 times detection limit

(1) For • detailed description of flags and technical tents in this report refer to the glossary.

RADIANC O H V O M A T I O M

Colder Associates, Inc. : :

Radian Work Order: PO-11-026

Analytical Data Suimary Page:9

Method/Analyte

Matrix

#03-30

10AIR

Sample Identifications

#03-31 #03-33

11AIR

12AIR

HIOSH Method 0500Total Dust

Result Oct. Unit

.06 total i

Result Det. Limit

NO total no d!blb11

Result

.07

Oct. Limit

NO Not detected at specified detection Unit

<1) For (detailed description of flags and technical terns In this report refer to the glossary.

RADIAN


Analytical Data Summary Page: 10

NIOSH

Kethod/Analyte#03-32 (FIELDBLANK)13

Matrix AIR

Result Oet. LimitMethod 0500

Total Oust .10 total mo o!«ll

NO Not detected at specif ied detection limit

Sanple Identifications

•03-34 (MATRI- #03-35 <MATRI-X SPIKE) X SPIKE DUP)14 15AIR AIR

Result Oet. Limit Result Oct. Limit

NO total KO b OloSS; .02 a total mg 0.010 V

a Est. result less than S times detection limit. • • . • • .• . - . .

<1) For a detailed description of flags and technical terns in this report refer to the glossary.

RADIAN


Analytical Date Summary Page:11

MethocVAnalyte

Hatrix

Saitple Identifications

MEIHOC BUNK

20AIR

NIOSH Method 0500Total Oust

Result

NO

Oct. Limit

total «ig

NO Not detected at cpecified detection Unit

(1) For a detailed description of flags and technical tens in this report refer to the glossary.

RADIANSample History Page:12

Colder Associates, Inc.Kadian Work Order: PC-11-026

S ;'?:; : '--' Sample Identifications and Dates ' • :- -V:-.:',.:•'• : .' '": ..' ' . .;'• ••'•-•" • • ' . ' - • • • • ' : : • ' ' ' - . • •

Sample ID #03-21 #03-22 #03-23 #03-24 #03-25 #03-26

Date Sampled 11/06/90 11/06/90 11/06/90 11/06/90 11/06/90 11/06/90Date Received 11/07/90 11/07/90 11/07/90 11/07/90 11/07/90 11/07/90Matrix filter- filter filter filter filter filterV 01 02 °3 .- « 05 06

II10SN Method 0500PreparedAnalyzedAnalystFile IDBlank IDInstrumentReport as'

ICP 25 element scanPreparedAnalyzedAnalystfile IDBlank 10InstrumentReport as

11/12/9011/13/90UK

MH201received

11/19/9011/28/90JOl11026011102620ICP#1received

11/12/9011/13/90LKK

MH20Treceived

11/19/9011/28/90JOL11026021102620ICP#1received

11/12/9011/13/90UK

HH20Treceived

11/19/9011/28/90JOL110260311026201CP#1received

11/12/9011/13/90UK

HH201received

11/19/9011/28/90JOL11026041102620]CP*1received

11/12/9011/13/90UK

HH20Treceived

11/19/9011/28/90JDL110260511026201CP#1received

11/12/9011/13/90IKK

HH20Treceived

11/19/9011/28/90JDL11026061102620ICP#1received

RADIANSanple History Page:13


_-:: --'-';"::;i;:.:-t;:-:v->'vv- •".•-•"• .-• Sample Identifications «nd Dates _ . . ;-.•. -• " ..." •- - : ' - ' ' -"-: '-.-'•- • " • - • • . . " . - - ' ' ' ' . . - "

;:." - - - : - . . -

Sanpl« IB i '•03-27 #03-28 #03-29 *03-30 *03-31 #03-33

Date Sanpled 11/06/90 11/06/90 11/06/90 11/06/90 11/06/90 11/06/90Date Received 11/07/90 11/07/90 11/07/90 11/07/90 11/07/90 11/07/90•tatrlx filter filter filter filter filter filter

07 08 09 10 11 12

MIOSH Method 0500PreparedAnalyzedAnalystFile IDBlank IDInstrunentReport as

ICP 25 element scanPreparedAnalyzedAnalystFile IDBlank IDInstrunentReport as

11/12/9011/13/90LKK

MH20Treceived

11/19/9011/28/90JOL11026071102620ICP#1received

11/12/9011/13/90IKK

MH20Treceived

11/19/9011/28/90JOL11026081102620ICP#1received

11/12/9011/13/90LICK

MK20Treceived

11/19/9011/28/90JOL11026091102620ICP#1received

11/12/9011/13/90IKK

MH20Treceived

11/19/9011/28/90JOL110261011026201CP*1received

11/12/9011/13/90LKK

MH20Treceived

11/19/9011/28/90JOL11026111102620ICP«1received

11/12/9011/13/90LKK

HH20Treceived

11/19/9011/28/90JOL110261211026201CP*1received

RADIANSanple History Page:U

Colder Associates, Inc.R»dian Uork Order: PO-11-026

•':^lf^:''--f v.' :::."':;::::: : v;:^:i:: ;S«Mple Identlfieitions end 0«t« : :. ; - -'.....• . . . . . < , - . - ' : -:.•'..;• • . . . ; . . :• --: • '-' . •'";•.' ''.-'. •' '.'-•-'•• ' •-.--' -. -' - •: • .':'••.''- : ' . ;• ---:-.' -..-.- . .- • -'. • •- ' • ' • - ; .

Sariple ID #03-32 (FIELD *03-34 OUTKI- «03-35 (MATRI- KETHOO BUNK8UMK) XSPltt) X Sf l« DUP)

0«t« Sanpled 11/06/90 11/06/90 11/06/90Date tecetved 11/07/90 11/07/90 11/07/90 11/07/90•tatrix filter filter -filter filter

;:. -,:,;' " • • .•,.;•« -. . ,i*">'". 15 ... . ' ";. 20' V ..'-.-.

NIOSH Method 0500PreparedAnalyzedAnalystFile ID•lank 10InstrunentReport as

ICP 2S element scanPreparedAnalyzedAnalystfile IDBlank IDInstrunentReport as

11/12/9011/13/90LKK

HH20Treceived

11/19/9011/28/90JOL11026131102620ICP*1received

11/12/9011/13/90UK

MN20Treceived

11/19/9011/28/90JOL11026U1102620ICPflreceived

11/12/9011/13/90LKK

HH2OT

received

11/19/9011/28/90JOL11026151102620ICPtlreceived

11/12/9011/13/90LKK

HH20Treceived

11/19/9011/28/90JOL1102620

ICP*1received

. :: : V " . - . ' • • - • • " Appendix A •, • : . . . : : ; - ; .

jConrnentc, Motes and Definitions

RADIANCO«*>Oli*TIOII

Colder Associates, IncRadi an Work Order : PO-11-026

Report Comments and Narrative Page: A-2

General CoomentsThe Chronfin and Lead values have been blank corrected.

The natrlx spike recoveries for lead are possibly low due tothe fusing of lead to the grassuare during the ashing steps.

RADIANNotes and Definitions Page: A-3

Colder Associates; inc.Radian Work Order:"M-11-026

8 ALL METHODS EXCEPT CLPThe results which are less than five times the method specifieddetection limit.EXPLANATIONUncertainty of the analysis will increase as the method detectionlimit Is approached. These results should be considered approximate.

NO ALL METHODS EXCEPT CLPThis flag Is used to denote analytes which are not detected at or•bove the specified detection limit.EXPLANATIONThe value to the right of the < synbol Is the method specifieddetection limit for the analyte.

RADIANNotes and Definitions Page: A-4

Colder Associates/ Inc. :;;i;Radian Work Order: M-11 -026

TERMS USED IN THIS REPORT:Analyte - A chemical for which a sanple Is to be analyzed. The analysis will meetEPA Method and OC specifications.

Compound - See Analyte.

Detection Limit - The Method specified detection Unit, which is the lower Unit ofquantitation specified by EPA for a Method. Radian staff regularly assess theirlaboratories' Method detection Units to verify that they Meet or are lower than thosespecified by EPA. Detection Units which are higher than Method limits are basedon experimental value* at the 99X confidence level. The detection Units for EPA CIP(Contract Laboratory Program) Methods are CROLs (contract required quantitationlimits) for organic* and CRDLs (contract required detection limits) for inorganics.Note, the detection limit May vary from that specified by CPA based on samplesize, dilution or cleanup. (Refer to Factor, below)

EPA Method - The EPA specified method used to perform an analysis. EPA has specifiedstandard Methods for analysts of environmental samples. Radian will perform Itsanalyses and accompanyina OC test* in confonwnce with EPA methods unless otherwise specified.

Factor - Default Method detection limits are based on analysis of clean water samples.A factor is required to calculate cample specific detection limits based on alternatematrices (soil or water), reporting wilts, use of clean*] procedures, or dilution of extracts/digestates. For example, extraction or digestion of 10 grans of soil in contrastto 1 liter of water will result in a factor of 100.

Matrix - The cample Material. Generally, It will be soil, water, air, oil, or solidwaste.

Radian Work Order - The unique Radian identification code assigned to the samples reported inthe analytical summary.___________________________________

Units - ug/t i :: micrograms per liter Xparts per billion);liquids/waterug/kg \Micrograins per kilogram (part* per billion); coilt/solidsug/H3 :,.; micrograns per cubic Meter; *ir samples •Mg/t y milligrams per liter (parts per Mill ion) .-liquids/water : : V•9/fcg Milligrams per kilogram (parts per nlll1on);s6ils/solids

' * i;~percent; usually used for^percent recovery of (C standardsUS/cm conductance unit; nicroSiemans/centiineter

: ::*t/hr•:.*!;»iU{Mterc per hour; rate of settlement of natter In water:*,:;: • ::vsirrU '*v ^turbidity iunlt; nepheiometric turbidity unit ;,;;:;;'-'O-"- ;v"\;..

CO ?: v . eofor unit; equal to 1 «e/l^ of chloroplatinate salt

APPENDIX B

DUST PUMP FIELD CALIBRATIONAND

SAMPLING DOCUMENTATION

PRE-DESIGN INVESTIGATIONINDUSTRI-PLEX SITE

WGBURN, MASSACHUSETTS

FLOW PUMP FIELD DATA FORM

PROJECT NO.: 893-6255

LOCATION NO.: | SAMPLER NAME:

LOCATION DESCRIPTION [Address]: u/,uf of /^ B--J /£y/.u 4 ?*»<#& fa tf jiJ

DATE STARTED: U ISh<> ________ TIME STARTED:

DATE COMPLETED: n/D/?° TIME COMPLETED;

PUMP SERIAL NO. : >5T/ 6 3 ~7"£> RECORDED TARE OF FILTER:

INITIAL ROTAMETER READING:

FINAL ROTAMETER READING: > "7

REQUIRED FLOW RATE (al/ttin) :

INTERMITTENT PUMPING REQUIRED: * YES _____ NO

PUMP PROGRAMMING:

1. DELAYED START [Time started - min.]

2. SAMPLE PERIOD [Total time - min.]:

3. PUMP PERIOD [Total time - min.]:

WEATHER: AWo-,-' dad** " n**>

OBSERVATIONS: &r

— |

C:FPFDFORM

Colder Associates


WOBURN, MASSACHUSETTS



LOCATION NO.:________^__________ SAMPLER NAME:

LOCATION DESCRIPTION [Address]: /u»-A of febf /k4 P,l

DATE STARTED: ii/5/^ TIME STARTED: // ~ Y

DATE COMPLETED: /'/ b/ ' TIME COMPLETED: •'

PUMP SERIAL NO. : 3'*O ^ <— RECORDED TARE OF FILTER:.

INITIAL ROTAMETER READING: _

FINAL ROTAMETER READING:

REQUIRED FLOW RATE (ml/min) : *Loo£

INTERMITTENT PUMPING REQUIRED: _£__ YES _____ NO

PUMP PROGRAMMING:

1. DELAYED START [Time started - min.]: °____

2. SAMPLE PERIOD [Total time - min.]: _

3. PUMP PERIOD [Total time - min.]: _

WEATHER:

r\ efe*r

OBSERVATIONS:

C:FPFDFORM

Colder Associates




PROJECT NO. : 893-6255

LOCATION NO. SAMPLER NAME;

LOCATION DESCRIPTION [Address]:

DATE STARTED: J]

DATE COMPLETED:

»o

TIME STARTED:

TIME COMPLETED; C3

PUMP SERIAL KO.: RECORDED TARE OF FILTER:



REQUIRED FLOW RATE (ml/ain):

INTERMITTENT PUMPING REQUIRED: YES

PUMP PROGRAMMING:

1. DELAYED START [Time started - min.]:

2. SAMPLE PERIOD [Total time - Bin.3:


WEATHER: *{<?"£''

OBSERVATIONS:

NO

C:FPFDFORM

Colder Associates





LOCATION NO.:_____^____________ SAMPLER NAME;

LOCATION DESCRIPTION [Address]: /U</' corner<*f site.-_________

DATE STARTED: " l^fac _____ TIME STARTED: / *~^L'

DATE COMPLETED: / / / f e / 7 0 TIME COMPLETED;

(r)PUMP SERIAL NO.: 5/4jTc/_i ( J RECORDED TARE OF FILTER

INITIAL ROTAMETER READING: _ S7__


REQUIRED FLOW RATE (ml/Bin):

INTERMITTENT PUMPING REQUIRED: __X__ YES _____ NO

PUMP PROGRAMMING:

1. DELAYED START [Time started - min.]: °_______

2. SAMPLE PERIOD [Total time - min.]: /Wo


WEATHER:

jj %Afl\

OBSERVATIONS:

•j ^ * J/-jo/'/hv//y C

C:FPFDFORM

Colder Associates





LOCATION N O . : * > _ S A M P L E R NAME:/?.-*

LOCATION DESCRIPTION [Address]: J^f <=*><•)- &f e^s^ fa<&.

DATE STARTED: i« islÔ TIME STARTED: _______lilLlQn 11 (/<"DATE COMPLETED: ///Q/7^ TIME COMPLETED; //Y-*

PUMP SERIAL NO.: $'/£S'2-? RECORDED TARE OF FILTER:.

INITIAL ROTAMETER READING: _


REQUIRED FLOW RATE (ml/min):

INTERMITTENT PUMPING REQUIRED: _ .__ YES _____ NO

PUMP PROGRAMMING:

1. DELAYED START (Time started - lain.]: <?____*

2. SAMPLE PERIOD [Total time - min.]: _


WEATHER:

OBSERVATIONS: Ôllêc/ 0f«s$iM<, /

C:FPFDFORM

Colder Assodates





LOCATION NO.:


SAMPLER NAME:

. . tfV &J t!f(^^>-<{._ .

DATE STARTED:

DATE COMPLETED:

PUMP SERIAL NO. :

" TIME STARTED: /

TIME COMPLETED:

RECORDED TARE OF FILTER:



REQUIRED FLOW RATE (ml/Bin):

INTERMITTENT PUMPING REQUIRED: YES NO

PUMP PROGRAMMING:



3. PUMP PERIOD [Total tine - nin.]:

WEATHER:

h,

OBSERVATIONS: .A <S

C:FPFDFORM

Colder Associates





LOCATION NO.: ~1 SAMPLER NAME:/?


DATE STARTED:

DATE COMPLETED:

carter

TIME STARTED:

PUMP SERIAL NO. : STI&3 3 /



TIME COMPLETED; /S&y

RECORDED TARE OF FILTER;

S~7

REQUIRED FLOW RATE (al/min) :

INTERMITTENT PUMPING REQUIRED: X YES NO

PUMP PROGRAMMING:

1. DELAYED START [Tine started - min.]



WEATHER:

OBSERVATIONS:

C:FPFDFORM

Colder Associates





LOCATION NO.: ________ 8 _________ SAMPLER NAME:

LOCATION DESCRIPTION [Address]: a-f /

DATE STARTED: U lslalO TIME STARTED: / V

DATE COMPLETED: " I^H^ TIME COMPLETED: I j

PUMP SERIAL NO. : S~l(=3 ffff RECORDED TARE OF FILTER:



REQUIRED FLOW RATE (nl/nin):

INTERMITTENT PUMPING REQUIRED: * YES _____ NO

PUMP PROGRAMMING:

1. DELAYED START [Tine started - nin.]: G

2. SAMPLE PERIOD [Total tine - nin.]: __

3. PUMP PERIOD [Total tine - nin.]: __

WEATHER:»

OBSERVATIONS:

y>

C:FPFDFORM

Colder Associates





LOCATION NO.:________j_________ SAMPLER NAME:.

LOCATION DESCRIPTION [Address]: />W^

DATE STARTED: '' /5" flp TIME STARTED: /S^S"

DATE COMPLETED: ^ Hn^ TIME COMPLETED: ^

PUMP SERIAL NO.: ~" «?o /1 RECORDED TARE OF FILTER:.

INITIAL ROTAMETER READING: _ £~7



INTERMITTENT PUMPING REQUIRED: X YES _____ NO

PUMP PROGRAMMING:

1. DELAYED START [Time started - min.]: °____2. SAMPLE PERIOD [Total time - min.]: _


WEATHER:

Jfa

OBSERVATIONS: o",* fivcxr #+ r<\ of •zttrtrflhg ,vcxr #+5 J

C:FPFDFORM

Colder Associates





LOCATION NO.: SAMPLER NAME; lU


DATE STARTED:

DATE COMPLETED:

TIME STARTED:

TIME COMPLETED: ( 2*O

PUMP SERIAL NO. : RECORDED TARE OF FILTER;





PUMP PROGRAMMING:




WEATHER:

}v*(..*——— r

OBSERVATIONS:

C:FPFDFORM

Colder Atsodates





LOCATION NO.: SAMPLER NAMEt&X


DATE STARTED: _

DATE COMPLETED: '

<£

TIME STARTED: _____

TIME COMPLETED: /33

PUMP SERIAL NO.: <&&31 £~




REQUIRED FLOW RATE (ml/Bin) :

INTERMITTENT PUMPING REQUIRED: _x YES

PUMP PROGRAMMING:

1. DELAYED START [Time started - min.]

2. SAMPLE PERIOD [Total tine - min.]:

3. PUMP PERIOD [Total time - nin.]:

WEATHER:

•

OBSERVATIONS:

C:FPFDFORM

NO

O

Colder Associates





LOCATION NO.: SAMPLER NAME; ./£./.


DATE STARTED:

DATE COMPLETED:

PUMP SERIAL NO.

\\\5\ciO

/ 1/6/fO

TIME STARTED:

TIME COMPLETED:


INITIAL ROTAMETER READING




PUMP PROGRAMMING:




HEATHER:

°

OBSERVATIONS: w ^ of //t

/^ i%T) *

C:FPFDFORM

Colder Assodates

APPENDIX C

METEOROLOGICAL DATA

INDUSTRI-PLEX SITE WOBURN, MAWEATHER STATION DATA 1 1/05 - 1 1/06 1990

iiffliiii |::ivy}|lllliiiillii nliiiiii '•siiiji :;iiilii B

1990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990

308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308

0153045

100115130145200215230245300315330345400415430445500515530545600615630645700715730745800815830845900

0.6791.8680.7250.5691.1191.9440.9221.1641.527

1.022.5991.4781.4891.2981.7331.7092.0182.6362.1782.9283.65

3.0892.0331.7621.5992.4423.4743.7833.2712.9352.3211.9461.2912.669

2.322.8072.376

178.8207.6105.3171.2

91.181.4

98224.4192.4179.9167.4

185166.3185.6159.4153.5179.7170.6188.8162.9170.4165.6155.1139.1149.1157.1163.6169.8167.2

163152.9154.9131.1160.5168.5188.3192.3

58.8559.4958.9857.9357.5557.1156.8855.7755.2255.4656.5857.0956.1256.1756.0556.2756.0555.6355.8555.2656.9157.3257.1456.7656.2856.7557.7958.5558.4158.2257.5657.0357.4158.3659.6160.4861.88

100.599.3

103.2106.5106.5105.196.693.795.396.9

9795.596.396.997.497.598.299.199.2

101.3101.2101.3101.9102.2103.6103.6

102100.299.599.8

100.5101.6

10299,395.391.187.5

30.0330.0330.0330.0330.0330.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0230.0330.0230.0230.0230.01

30

INDUSTRI-PLEX SITE WOBURN, MAWEATHER STATION DATA 11/05 - 11/06 1990

^EARg

1990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990

308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308308

iliiililii

915930945

1000101510301045110011151130114512001215123012451300131513301345140014151430144515001515153015451600161516301645170017151730174518001815

liiAMlliiiiiii

2.8582.5233.3763.9015.0496.6186.0595.9525.3665.5896.904

7.56.5858.439.57

10.4511.7111.7711.5111.1312.2511.7612.3710.8310.449.2311.69.687.247.947.48

6.8896.9156.788.367.1

6.554

riililll

171.6189.2214.3235.3253.5

269257

259.5260.5

245247.6247.7242.9231.2233.1235.5

245236.4232.9235.3239.7248.5239.8247.8241.6247.9254.8

255261.4255.5257.3248.1248.9253.2259.6251.2255.1

ilKilll

62.2363.4464.3565.4667.2868.0668.8969.6970.270.1

7070.270.971.772.573.173.273.874.775.675.875.374.874.774.574.874.473.873.172.571.770.970.3

69.6769.2268.5768.04

iim&mliilliiilitiMiiiii

98.196.974.877.873.480.676.6

52.0751.0262.4371.670.970.7

64.1649.9643.7743.1542.9341.6

39.5936.8

35.8335.9636.8738.4

39.5537.1436.7952.5455.6385.186.174.169.275.277.1

66.91

3029.9929.9829.9729.9629.9529.9329.91

29.929.8829.8729.8629.8529.8329.81

29.829.7929.7829.7729.7629.7629.7629.7629.7629.7529.7529.7629.7629.7529.7529.7529.7629.7629.7729.7729.7729.78

INDUSTRI-PLEX SITE WOBURN, MAWEATHER STATION DATA 11/05 - 11/06 1990

1990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990

308308308308308308308308308308308308308308308308308308308308308308309309309309309309309309309309309309309309309

lllllBlllliiAVGiiilllllll11111111!

1830184519001915193019452000201520302045210021152130214522002215223022452300231523302345

0153045

100115130145200215230245300315330

6.4146.1075.2536.7467.13

5.9356.5246.0956.5677.587.99

6.9888.527.23

6.5446.2727.09

6.7686.4155.7584.6033.9622.723.56

5.8256.1826.4765.5446.3886.8556.6186.3776.5475.4933.8234.33

3.407

•iiffiliiii

251248.4240.6236.6240.6238.9242.2239.6241.8247.6248.3243.4236.9

237237.5245.7243.9239.2

240231.4216.5215.9221.1242.5240.7240.3239.2251.4261.2257.8261.3265.2263.1275.9287.5341.3350.7

67.6366.9466.2266.0265.8465.5865.3965.0364.5764.4364.2963.8663.8963.3763.0262.5362.2

61.7461.4561.0960.1859.6358.9958.7759.3759.7559.8559.7359.9960.0259.7959.5159.1158.5957.6657.2656.93

ijMMm1111111 mIIMI :;;yJiti): !i

55.557.8368.365.663.2

64.1665.0968.3566.1866.1664.6958.5757.7659.4665.9547.9748.0157.26

63.465.1369.7370.8

51.7164

71.370.2

69.8269.5869.38

6969.0969.6470.471.372.874.876.5

iiii§ill

29.7929.829.829.829.829.829.829.829.829.8

29.7929.7929.7929.7929.7929.7929.79

29.829.829.829.8

29.8129.8129.8229.8229.8229.8229.8329.8329.8229.8229.8329.8429.8529.8629.8729.88

INDUSTRI-PLEX SITE WOBURN, MAWEATHER STATION DATA 1 1/05 - 1 1/06 1990

s;:i:-:YEAii||

:• '•:'•::'' '•:'-:'-:':'-''<^-<''-''-<-'-<- •<•••'•-'•-'•:• • ; . . ' . ; • : .-;.;..;.;.;.;.;•:•:•:•:•:•:•:•:

1990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990199019901990

309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309309

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lilliilillIlllilllli;

345400415430445500515530545600615630645700715730745800815830845900915930945

100010151030104511001115113011451200121512301245

liillll

5.9079.698.22

6.1997.727.78

6.1126.3085.6636.9376.8916.5756.5478.458.928.968.097.118.728.068.058.517.867.7

8.947.46

5.4444.5945.1083.27

5.1045.5267.14

6.8417.356.648.04

1.62511.56

9.70.43

3.0426.0227.32

10.34359.74.628356.9355.92.1996.8473.084358.5358.3355.25.5436.67714.04

24.335.7716.8

18.5511.4614.3615.0828.5537.63

77.985.1

9187.595.481.285.6

56.6555.3554.4

53.6352.7451.7651.0750.6450.1750.0149.6349.3749.1248.9348.8

48.4347.9847.6447.5547.3347.1646.9447.0847.0247.0146.9146.8746.9747.0247.5447.9448.0547.7147.1546.4746.1845.77

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76.270.270.170.573.580.483.583.682.480.475.779.581.181.981.878.772.372.171.971.771.471.170.4

69.6668.2866.7766.7866.7765.8564.5365.2665.9766.5360.2360.6461.0461.63

29.8929.9129.9229.9229.9329.9429.9429.9529.9629.9629.9729.9829.9829.9929.99

3030.0230.0230.0330.0430.0530.0530.0530.0630.0630.0630.0630.0630.0630.0630.0630.0630.0530.0530.0530.0630.06

INDUSTRI-PLEX SITE WOBURN. MAWEATHER STATION DATA 1 1/05 - 1 1/06 1 990

1990199019901990

309309309309

lllili^•::::'/'-^^-'£^^'•^••^'•:'--'^^-:^'^^^\

1300131513301345

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7.137.36

5.6726.222

iiWilill:llillll: !(P;EG)l!t

82.777.976.279.2

:iilllil:;

45.3745.2345.1945.14

iiMmM

63.7872.775.673.7

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30.0630.0630.0630.06

golder associates inc. - us environmental protection · pdf file3*4o&i golder associates...

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