for: saipan wtp - commonwealth utilities · 2017-09-26 · analytical report for: saipan wtp . asl...

ANALYTICAL REPORT

For: Saipan WTP

ASL Report #: P1092 Project ID: 156197.00.SAIPAN Attn: Kerry Meyer/DEN

Authorized and Released By:

Laboratory Project Manager Kathy McKinley (541) 758-0235 ext.23144 February 03, 2015

All analyses performed by CH2M HILL are clearly indicated. Any subcontracted analyses are included as appended reports as received from the subcontracted

laboratory. The results included in this report only relate to the samples listed on the following Sample Cross-Reference page. This report shall not be

reproduced except in full, without the written approval of the laboratory.

Any unusual difficulties encountered during the analysis of your samples are discussed in the attached case narratives.

Accredited in accordance with NELAP: Oregon (100022) Louisiana (05031)

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ASL Report #: P1092

Sample Receipt Comments We certify that the test results meet all NELAP requirements. Some analyses were performed by an outside laboratory and their report will follow.

Sample Cross-Reference

ASL Sample ID Client Sample ID

Date/Time Collected

Date Received

P109201 Siapan - Talafofo 01/20/15 15:30 01/20/15 P109202 Siapan - Tanapag1 01/20/15 15:30 01/20/15 P109203 Siapan - Tanapag2 01/20/15 15:30 01/20/15 P109204 Siapan - Airport 01/20/15 15:30 01/20/15

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GC/MS VOLATILES ANALYSIS

Lab Name: ASL SDG#:

Project #:

CH2M HILL ASL

156197.00.SAIPAN

P1092

Project: Saipan WTP

CASE NARRATIVE

1100 NE Circle Blvd., Suite 300

Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

With the exceptions noted as flags, footnotes, or detailed in the section below; standard operating procedures were

followed in the analysis of the samples and no problems were encountered or anomalies observed.

Calculations are performed before rounding to minimize errors in calculated values.

All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise

detailed in the section below, or in the sample receipt documentation.

All laboratory quality control samples were within established control limits, with any exceptions noted below, or in the

associated QC summary forms.

Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of the method. For diluted

samples, the reporting limits are adjusted for the dilution required.

Method(s):E524.2: SW5030

MB150203-14:52-P1092-V of 41

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Matrix: Water

Lab Sample ID: P109204Client Sample ID:

Date Received: 01/20/15

Date AnalyzedAnalyte UnitsQualifier

CH2M HILL Applied Sciences Laboratory (ASL)

SampleResultRL

Siapan - Airport

Analysis Method

Client Information Lab Information

Project Name: Saipan WTPSample Date: 01/20/15Sample Time: 15:30

Type: CompositeReport Revision No.: 0

CAS#

GC/MS Volatiles

Dilution Factor: 1

DL

01/23/15ug/LDichlorodifluoromethane 0.15 U0.50 E524.275-71-8 0.15

01/23/15ug/LChloromethane 0.15 U0.50 E524.274-87-3 0.15

01/23/15ug/LVinyl Chloride 0.15 U0.50 E524.275-01-4 0.15

01/23/15ug/LBromomethane 0.20 U0.50 E524.274-83-9 0.20

01/23/15ug/LChloroethane 0.15 U0.50 E524.275-00-3 0.15

01/23/15ug/LTrichlorofluoromethane 0.15 U0.50 E524.275-69-4 0.15

01/23/15ug/LAcetone 16.65.00 E524.267-64-1 1.00

01/23/15ug/L1,1-Dichloroethene 0.15 U0.50 E524.275-35-4 0.15

01/23/15ug/LMethylene chloride 0.22 J0.50 E524.275-09-2 0.15

01/23/15ug/Ltrans-1,2-Dichloroethene 0.15 U0.50 E524.2156-60-5 0.15

01/23/15ug/LMethyl tert-butyl ether (MTBE) 0.15 U0.50 E524.21634-04-4 0.15

01/23/15ug/L1,1-Dichloroethane 0.15 U0.50 E524.275-34-3 0.15

01/23/15ug/L2-Butanone (MEK) 2.00 U5.00 E524.278-93-3 2.00

01/23/15ug/Lcis-1,2-Dichloroethene 0.15 U0.50 E524.2156-59-2 0.15

01/23/15ug/LBromochloromethane 0.15 U0.50 E524.274-97-5 0.15

01/23/15ug/LChloroform 0.15 U0.50 E524.267-66-3 0.15

01/23/15ug/L2,2-Dichloropropane 0.15 U0.50 E524.2594-20-7 0.15


01/23/15ug/L1,1,1-Trichloroethane 0.15 U0.50 E524.271-55-6 0.15

01/23/15ug/L1,1-Dichloropropene 0.15 U0.50 E524.2563-58-6 0.15

01/23/15ug/LCarbon tetrachloride 0.15 U0.50 E524.256-23-5 0.15

01/23/15ug/LBenzene 0.15 U0.50 E524.271-43-2 0.15

01/23/15ug/LDibromomethane 0.15 U0.50 E524.274-95-3 0.15


01/23/15ug/LTrichloroethene (TCE) 0.15 U0.50 E524.279-01-6 0.15

01/23/15ug/LBromodichloromethane 0.15 U0.50 E524.275-27-4 0.15

01/23/15ug/Lcis-1,3-Dichloropropene 0.15 U0.50 E524.210061-01-5 0.15

01/23/15ug/L4-Methyl-2-pentanone (MIBK) 0.50 U2.00 E524.2108-10-1 0.50

01/23/15ug/Ltrans-1,3-Dichloropropene 0.15 U0.50 E524.210061-02-6 0.15


01/23/15ug/LToluene 0.23 J0.50 E524.2108-88-3 0.15


01/23/15ug/LDibromochloromethane 0.15 U0.50 E524.2124-48-1 0.15

01/23/15ug/L1,2-Dibromoethane (EDB) 0.15 U0.50 E524.2106-93-4 0.15

01/23/15ug/LTetrachloroethene (PCE) 0.15 U0.50 E524.2127-18-4 0.15

01/23/15ug/L1-Chlorohexane 0.15 U0.50 E524.2544-10-5 0.15

01/23/15ug/L1,1,1,2-Tetrachloroethane 0.15 U0.50 E524.2630-20-6 0.15

01/23/15ug/LChlorobenzene 0.15 U0.50 E524.2108-90-7 0.15

01/23/15ug/LEthylbenzene 0.18 J0.50 E524.2100-41-4 0.15

01/23/15ug/Lm,p-Xylene 0.93 J1.00 E524.2108-38-3/1 0.30

01/23/15ug/LBromoform 0.15 U0.50 E524.275-25-2 0.15

01/23/15ug/LStyrene 0.15 U0.50 E524.2100-42-5 0.15


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

MB150203-14:52-P1092-V

U=Not detected at specified detection limit

J=Estimated value below reporting limit

E=Estimated value above calibration range

*=See case narrative

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Matrix: Water

Lab Sample ID: P109204Client Sample ID:




SampleResultRL

Siapan - Airport

Analysis Method



Type: CompositeReport Revision No.: 0

CAS#

GC/MS Volatiles

Dilution Factor: 1

DL


01/23/15ug/Lo-Xylene 0.27 J0.50 E524.295-47-6 0.15

01/23/15ug/L1,2,3-Trichloropropane 0.15 U0.50 E524.296-18-4 0.15

01/23/15ug/LIsopropylbenzene 0.15 U0.50 E524.298-82-8 0.15

01/23/15ug/LBromobenzene 0.15 U0.50 E524.2108-86-1 0.15

01/23/15ug/Ln-Propylbenzene 0.15 U0.50 E524.2103-65-1 0.15

01/23/15ug/L2-Chlorotoluene 0.15 U0.50 E524.295-49-8 0.15


01/23/15ug/L1,3,5-Trimethylbenzene 0.15 U0.50 E524.2108-67-8 0.15

01/23/15ug/Ltert-Butylbenzene 0.15 U0.50 E524.298-06-6 0.15


01/23/15ug/Lsec-Butylbenzene 0.15 U0.50 E524.2135-98-8 0.15

01/23/15ug/L1,3-Dichlorobenzene 0.15 U0.50 E524.2541-73-1 0.15


01/23/15ug/Lp-Isopropyltoluene 0.15 U0.50 E524.299-87-6 0.15


01/23/15ug/Ln-Butylbenzene 0.15 U0.50 E524.2104-51-8 0.15

01/23/15ug/L1,2-Dibromo-3-chloropropane 0.15 U0.50 E524.296-12-8 0.15

01/23/15ug/L1,2,4-Trichlorobenzene 0.15 U0.50 E524.2120-82-1 0.15

01/23/15ug/LNaphthalene 0.26 J0.50 E524.291-20-3 0.15

01/23/15ug/LHexachlorobutadiene 0.15 U0.50 E524.287-68-3 0.15


Dibromofluoromethane

% Recovery Control Limits Qualifier

99 70-130

1,2-Dichloroethane-d4 105 70-130

Toluene-d8 97 70-1304-Bromofluorobenzene 99 70-130

Surrogate


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

MB150203-14:52-P1092-V





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Matrix: Water

Lab Sample ID: WB1-0123Client Sample ID:

Date Received: N/A



SampleResultRL

WB1-0123

Analysis Method


Project Name: Saipan WTPSample Date: N/ASample Time: N/A

Type: QCReport Revision No.: 0

CAS#

GC/MS Volatiles

Dilution Factor: 1

DL

01/23/15ug/LDichlorodifluoromethane 0.15 U0.50 E524.275-71-8 0.15

01/23/15ug/LChloromethane 0.15 U0.50 E524.274-87-3 0.15

01/23/15ug/LVinyl Chloride 0.15 U0.50 E524.275-01-4 0.15

01/23/15ug/LBromomethane 0.20 U0.50 E524.274-83-9 0.20

01/23/15ug/LChloroethane 0.15 U0.50 E524.275-00-3 0.15

01/23/15ug/LTrichlorofluoromethane 0.15 U0.50 E524.275-69-4 0.15

01/23/15ug/LAcetone 1.00 U5.00 E524.267-64-1 1.00

01/23/15ug/L1,1-Dichloroethene 0.15 U0.50 E524.275-35-4 0.15

01/23/15ug/LMethylene chloride 0.15 U0.50 E524.275-09-2 0.15

01/23/15ug/Ltrans-1,2-Dichloroethene 0.15 U0.50 E524.2156-60-5 0.15

01/23/15ug/LMethyl tert-butyl ether (MTBE) 0.15 U0.50 E524.21634-04-4 0.15


01/23/15ug/L2-Butanone (MEK) 2.00 U5.00 E524.278-93-3 2.00

01/23/15ug/Lcis-1,2-Dichloroethene 0.15 U0.50 E524.2156-59-2 0.15

01/23/15ug/LBromochloromethane 0.15 U0.50 E524.274-97-5 0.15

01/23/15ug/LChloroform 0.15 U0.50 E524.267-66-3 0.15




01/23/15ug/L1,1-Dichloropropene 0.15 U0.50 E524.2563-58-6 0.15

01/23/15ug/LCarbon tetrachloride 0.15 U0.50 E524.256-23-5 0.15

01/23/15ug/LBenzene 0.15 U0.50 E524.271-43-2 0.15

01/23/15ug/LDibromomethane 0.15 U0.50 E524.274-95-3 0.15


01/23/15ug/LTrichloroethene (TCE) 0.15 U0.50 E524.279-01-6 0.15

01/23/15ug/LBromodichloromethane 0.15 U0.50 E524.275-27-4 0.15

01/23/15ug/Lcis-1,3-Dichloropropene 0.15 U0.50 E524.210061-01-5 0.15

01/23/15ug/L4-Methyl-2-pentanone (MIBK) 0.50 U2.00 E524.2108-10-1 0.50

01/23/15ug/Ltrans-1,3-Dichloropropene 0.15 U0.50 E524.210061-02-6 0.15


01/23/15ug/LToluene 0.15 U0.50 E524.2108-88-3 0.15


01/23/15ug/LDibromochloromethane 0.15 U0.50 E524.2124-48-1 0.15

01/23/15ug/L1,2-Dibromoethane (EDB) 0.15 U0.50 E524.2106-93-4 0.15

01/23/15ug/LTetrachloroethene (PCE) 0.15 U0.50 E524.2127-18-4 0.15

01/23/15ug/L1-Chlorohexane 0.15 U0.50 E524.2544-10-5 0.15


01/23/15ug/LChlorobenzene 0.15 U0.50 E524.2108-90-7 0.15

01/23/15ug/LEthylbenzene 0.15 U0.50 E524.2100-41-4 0.15

01/23/15ug/Lm,p-Xylene 0.30 U1.00 E524.2108-38-3/1 0.30

01/23/15ug/LBromoform 0.15 U0.50 E524.275-25-2 0.15

01/23/15ug/LStyrene 0.15 U0.50 E524.2100-42-5 0.15


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

MB150203-14:52-P1092-V





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Matrix: Water

Lab Sample ID: WB1-0123Client Sample ID:

Date Received: N/A



SampleResultRL

WB1-0123

Analysis Method



Type: QCReport Revision No.: 0

CAS#

GC/MS Volatiles

Dilution Factor: 1

DL


01/23/15ug/Lo-Xylene 0.15 U0.50 E524.295-47-6 0.15

01/23/15ug/L1,2,3-Trichloropropane 0.15 U0.50 E524.296-18-4 0.15

01/23/15ug/LIsopropylbenzene 0.15 U0.50 E524.298-82-8 0.15

01/23/15ug/LBromobenzene 0.15 U0.50 E524.2108-86-1 0.15

01/23/15ug/Ln-Propylbenzene 0.15 U0.50 E524.2103-65-1 0.15




01/23/15ug/Ltert-Butylbenzene 0.15 U0.50 E524.298-06-6 0.15


01/23/15ug/Lsec-Butylbenzene 0.15 U0.50 E524.2135-98-8 0.15



01/23/15ug/Lp-Isopropyltoluene 0.15 U0.50 E524.299-87-6 0.15


01/23/15ug/Ln-Butylbenzene 0.15 U0.50 E524.2104-51-8 0.15

01/23/15ug/L1,2-Dibromo-3-chloropropane 0.15 U0.50 E524.296-12-8 0.15


01/23/15ug/LNaphthalene 0.15 U0.50 E524.291-20-3 0.15

01/23/15ug/LHexachlorobutadiene 0.15 U0.50 E524.287-68-3 0.15




100 70-130



Surrogate


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

MB150203-14:52-P1092-V





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Matrix: Water

LCS ID: BS1W0123

Date AnalyzedAnalyte Units %Recovery


SampleResult

SpikeAmount

Analysis Method


Project Name: Saipan WTP Report Revision No.: 0

CAS#

GC/MS Volatiles

Dilution Factor: 1Type: QC

01/23/15ug/LDichlorodifluoromethane 20.2 10120.0 E524.275-71-8

01/23/15ug/LChloromethane 20.0 10020.0 E524.274-87-3

01/23/15ug/LVinyl Chloride 16.6 8320.0 E524.275-01-4

01/23/15ug/LBromomethane 19.5 9720.0 E524.274-83-9

01/23/15ug/LChloroethane 18.3 9220.0 E524.275-00-3

01/23/15ug/LTrichlorofluoromethane 21.6 10820.0 E524.275-69-4

01/23/15ug/LAcetone 20.2 10120.0 E524.267-64-1

01/23/15ug/L1,1-Dichloroethene 17.1 8620.0 E524.275-35-4

01/23/15ug/LMethylene chloride 18.1 9120.0 E524.275-09-2

01/23/15ug/Ltrans-1,2-Dichloroethene 18.9 9520.0 E524.2156-60-5

01/23/15ug/LMethyl tert-butyl ether (MTBE) 17.7 8920.0 E524.21634-04-4

01/23/15ug/L1,1-Dichloroethane 18.5 9320.0 E524.275-34-3

01/23/15ug/L2-Butanone (MEK) 20.9 10520.0 E524.278-93-3

01/23/15ug/Lcis-1,2-Dichloroethene 18.8 9420.0 E524.2156-59-2

01/23/15ug/LBromochloromethane 18.5 9320.0 E524.274-97-5

01/23/15ug/LChloroform 19.7 9820.0 E524.267-66-3

01/23/15ug/L2,2-Dichloropropane 21.7 10820.0 E524.2594-20-7

01/23/15ug/L1,2-Dichloroethane 21.0 10520.0 E524.2107-06-2

01/23/15ug/L1,1,1-Trichloroethane 21.8 10920.0 E524.271-55-6

01/23/15ug/L1,1-Dichloropropene 19.3 9720.0 E524.2563-58-6

01/23/15ug/LCarbon tetrachloride 24.0 12020.0 E524.256-23-5

01/23/15ug/LBenzene 18.6 9320.0 E524.271-43-2

01/23/15ug/LDibromomethane 18.6 9320.0 E524.274-95-3


01/23/15ug/LTrichloroethene (TCE) 19.6 9820.0 E524.279-01-6

01/23/15ug/LBromodichloromethane 20.4 10220.0 E524.275-27-4

01/23/15ug/Lcis-1,3-Dichloropropene 21.1 10620.0 E524.210061-01-5

01/23/15ug/L4-Methyl-2-pentanone (MIBK) 20.1 10020.0 E524.2108-10-1

01/23/15ug/Ltrans-1,3-Dichloropropene 20.5 10320.0 E524.210061-02-6

01/23/15ug/L1,1,2-Trichloroethane 19.4 9720.0 E524.279-00-5

01/23/15ug/LToluene 19.2 9620.0 E524.2108-88-3


01/23/15ug/LDibromochloromethane 20.1 10020.0 E524.2124-48-1

01/23/15ug/L1,2-Dibromoethane (EDB) 19.4 9720.0 E524.2106-93-4

01/23/15ug/LTetrachloroethene (PCE) 18.5 9320.0 E524.2127-18-4

01/23/15ug/L1-Chlorohexane 17.7 8820.0 E524.2544-10-5

01/23/15ug/L1,1,1,2-Tetrachloroethane 20.9 10520.0 E524.2630-20-6

01/23/15ug/LChlorobenzene 17.0 8520.0 E524.2108-90-7

01/23/15ug/LEthylbenzene 18.6 9320.0 E524.2100-41-4

01/23/15ug/Lm,p-Xylene 37.3 9340.0 E524.2108-38-3/1

01/23/15ug/LBromoform 23.0 11520.0 E524.275-25-2

01/23/15ug/LStyrene 18.8 9420.0 E524.2100-42-5


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

MB150203-14:52-P1092-V





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Matrix: Water

LCS ID: BS1W0123



SampleResult

SpikeAmount

Analysis Method


Project Name: Saipan WTP Report Revision No.: 0

CAS#

GC/MS Volatiles

Dilution Factor: 1Type: QC

01/23/15ug/L1,1,2,2-Tetrachloroethane 18.5 9220.0 E524.279-34-5

01/23/15ug/Lo-Xylene 17.7 8920.0 E524.295-47-6

01/23/15ug/L1,2,3-Trichloropropane 20.0 10020.0 E524.296-18-4

01/23/15ug/LIsopropylbenzene 17.9 9020.0 E524.298-82-8

01/23/15ug/LBromobenzene 18.4 9220.0 E524.2108-86-1

01/23/15ug/Ln-Propylbenzene 17.7 8820.0 E524.2103-65-1

01/23/15ug/L2-Chlorotoluene 17.9 9020.0 E524.295-49-8

01/23/15ug/L4-Chlorotoluene 17.8 8920.0 E524.2106-43-4

01/23/15ug/L1,3,5-Trimethylbenzene 20.0 10020.0 E524.2108-67-8

01/23/15ug/Ltert-Butylbenzene 18.0 9020.0 E524.298-06-6

01/23/15ug/L1,2,4-Trimethylbenzene 19.8 9920.0 E524.295-63-6

01/23/15ug/Lsec-Butylbenzene 17.7 8920.0 E524.2135-98-8

01/23/15ug/L1,3-Dichlorobenzene 17.5 8720.0 E524.2541-73-1


01/23/15ug/Lp-Isopropyltoluene 18.2 9120.0 E524.299-87-6


01/23/15ug/Ln-Butylbenzene 19.2 9620.0 E524.2104-51-8

01/23/15ug/L1,2-Dibromo-3-chloropropane 20.3 10220.0 E524.296-12-8

01/23/15ug/L1,2,4-Trichlorobenzene 18.5 9320.0 E524.2120-82-1

01/23/15ug/LNaphthalene 19.3 9720.0 E524.291-20-3

01/23/15ug/LHexachlorobutadiene 20.9 10520.0 E524.287-68-3

01/23/15ug/L1,2,3-Trichlorobenzene 19.2 9620.0 E524.287-61-6



100 70-130



Surrogate


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

MB150203-14:52-P1092-V





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GENERAL CHEMISTRY ANALYSIS

Lab Name: ASL SDG#:

Project #:

CH2M HILL ASL

156197.00.SAIPAN

P1092

Project: Saipan WTP

CASE NARRATIVE


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276










Method(s):E1664A, E1664B

Matrix Spike/Matrix Spike Duplicate(s):E1664A, E1664B: Insufficient sample amount provided to perform MS/MSD. LCS/LCSD were used tomeasure precision.

TP150129-10:57-P1092-W of 41

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Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Oil and GreaseResultRL

E1664A


Project Name: Saipan WTP

Type: See C.O.C.

Report Revision No.: 0

General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:

DLLab Sample IDDilutionFactor

P109204 01/28/155.3 U5.3Siapan - Airport 1 N/A

WB1-0128 01/28/155.0 U5.0WB1-0128 1 N/A


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

TP150129-10:57-P1092-W

U=Not detected at specified detection limitJ=Estimated value below reporting limit



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LCS IDDate

Analyzed


SampleResult

SpikeAmount



General Chemistry

Lab Batch ID: P1092

AnalyteAnalysisMethodUnits % Recovery

Matrix: Water

Project Name: Saipan WTPType: QC

Oil and Grease 01/28/1517.4BS1W0128 E1664Amg/L20.0 87


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

TP150129-10:57-P1092-W





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METALS ANALYSIS

Lab Name: ASL SDG#:

Project #:

CH2M HILL ASL

156197.00.SAIPAN

P1092

Project: Saipan WTP

CASE NARRATIVE


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276










Method(s):E200.7: E200.2, FLDFLTE200.8: FLDFLT, E200.2

EB150203-13:23-P1092-M of 41

Draft

Matrix: Water

P109201


Date AnalyzedAnalyte UnitsQual


ResultRL

Siapan - Talafofo



Type: Composite

Report Revision No: 0

Metals

DilutionFactor DL

Lab Sample ID:Client Sample ID:

AnalysisMethod

PrepMethod

01/27/15ug/LIron 54.9 J100 E200.71 10.0 E200.2

02/03/15ug/LManganese 2.580.50 E200.81 0.025 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

EB150203-13:23-P1092-M




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Matrix: Water

P109201F




ResultRL

Siapan - Talafofo



Type: Composite


Dissolved Metals

DilutionFactor DL


AnalysisMethod

PrepMethod

01/27/15ug/LCalcium 40900500 E200.71 200 FLDFLT

01/27/15ug/LIron 29.4 J100 E200.71 10.0 FLDFLT

01/27/15ug/LMagnesium 6230500 E200.71 50.0 FLDFLT

01/21/15ug/LManganese 1.010.50 E200.81 0.025 FLDFLT


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

P109202




ResultRL

Siapan - Tanapag1



Type: Composite


Metals

DilutionFactor DL


AnalysisMethod

PrepMethod

01/27/15ug/LIron 259100 E200.71 10.0 E200.2

02/03/15ug/LManganese 45.20.50 E200.81 0.025 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

P109202F




ResultRL

Siapan - Tanapag1



Type: Composite


Dissolved Metals

DilutionFactor DL


AnalysisMethod

PrepMethod






Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

P109203




ResultRL

Siapan - Tanapag2



Type: Composite


Metals

DilutionFactor DL


AnalysisMethod

PrepMethod

01/27/15ug/LIron 452100 E200.71 10.0 E200.2

02/03/15ug/LManganese 28.30.50 E200.81 0.025 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

P109203F




ResultRL

Siapan - Tanapag2



Type: Composite


Dissolved Metals

DilutionFactor DL


AnalysisMethod

PrepMethod






Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

EB150203-13:23-P1092-M




of 41

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Matrix: Water

P109204




ResultRL

Siapan - Airport



Type: Composite


Metals

DilutionFactor DL


AnalysisMethod

PrepMethod

01/27/15ug/LIron 50.9 J100 E200.71 10.0 E200.2

02/03/15ug/LManganese 11.50.50 E200.81 0.025 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

P109204F




ResultRL

Siapan - Airport



Type: Composite


Dissolved Metals

DilutionFactor DL


AnalysisMethod

PrepMethod


01/27/15ug/LIron 10.0 U100 E200.71 10.0 FLDFLT


01/21/15ug/LManganese 0.34 J0.50 E200.81 0.025 FLDFLT


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

WB1-0127

Date Received: N/A



ResultRL



Type: QC


Metals

DilutionFactor DL

Method Blank ID:

AnalysisMethod

PrepMethod

01/27/15ug/LIron 10.0 U100 E200.71 10.0 E200.2

02/03/15ug/LManganese 0.025 U0.50 E200.81 0.025 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

EB150203-13:23-P1092-M




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Matrix: Water

WB10-0121

Date Received: N/A



ResultRL



Type: QC


Dissolved Metals

DilutionFactor DL

Method Blank ID:

AnalysisMethod

PrepMethod

01/21/15ug/LManganese 0.065 J0.50 E200.81 0.025 FLDFLT


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

WB10-0127

Date Received: N/A



ResultRL



Type: QC


Metals

DilutionFactor DL

Method Blank ID:

AnalysisMethod

PrepMethod

01/27/15ug/LCalcium 200 U500 E200.71 200 E200.2

01/27/15ug/LIron 10.0 U100 E200.71 10.0 E200.2

01/27/15ug/LMagnesium 50.0 U500 E200.71 50.0 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

Blank Spike ID: BS10W0121



SpikeAmount

AnalysisMethod


Project Name: Saipan WTP Report Revision No: 0

Metals

Result

Type: QC Dilution Factor: 1

PrepMethod

01/21/15ug/LManganese 19.8 9920.0 E200.8 FLDFLT


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water




SpikeAmount

AnalysisMethod



Metals

Result


PrepMethod

01/27/15ug/LCalcium 1020 1021000 E200.7 E200.2

01/27/15ug/LIron 1110 1111000 E200.7 E200.2

01/27/15ug/LMagnesium 948 951000 E200.7 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water




SpikeAmount

AnalysisMethod



Metals

Result


PrepMethod

01/27/15ug/LIron 549 110500 E200.7 E200.2

02/03/15ug/LManganese 51.3 10350.0 E200.8 E200.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Lab Name: ASL SDG#:

Project #:

CH2M HILL ASL

156197.00.SAIPAN

P1092

Project: Saipan WTP

CASE NARRATIVE


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276










Method(s):E350.1E300.0ASM2540CE310.1SM5910B

BS150202-12:04-P1092-W of 41

Draft

Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Alkalinity, Bicarbonate as CaCO3ResultRL

E310.1



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/21/151405.0Siapan - Talafofo 1 N/A

P109202 01/21/152105.0Siapan - Tanapag1 1 N/A


P109204 01/21/1558.55.0Siapan - Airport 1 N/A

WB1-0121 01/21/155.0 U5.0WB1-0121 1 N/A


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Alkalinity, Carbonate as CaCO3ResultRL

E310.1



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/21/155.0 U5.0Siapan - Talafofo 1 N/A

P109202 01/21/155.0 U5.0Siapan - Tanapag1 1 N/A

P109203 01/21/155.0 U5.0Siapan - Tanapag2 1 N/A

P109204 01/21/155.0 U5.0Siapan - Airport 1 N/A

WB1-0121 01/21/155.0 U5.0WB1-0121 1 N/A


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

BS150202-12:04-P1092-W




of 41

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Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Alkalinity, Total as CaCO3ResultRL

E310.1



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/21/151405.0Siapan - Talafofo 1 N/A



P109204 01/21/1558.55.0Siapan - Airport 1 N/A

WB1-0121 01/21/155.0 U5.0WB1-0121 1 N/A


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Ammonia-NResultRL

E350.1



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/27/150.020 U0.10Siapan - Talafofo 1 0.020

P109202 01/27/150.020 U0.10Siapan - Tanapag1 1 0.020

P109203 01/27/150.020 U0.10Siapan - Tanapag2 1 0.020

P109204 01/27/150.020 U0.10Siapan - Airport 1 0.020

WB1-0127 01/27/150.020 U0.10WB1-0127 1 0.020


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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of 41

Draft

Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


SulfateResultRL

E300.0A



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/23/155.970.20Siapan - Talafofo 1 0.022

P109202 01/26/1518.80.40Siapan - Tanapag1 2 0.043

P109203 01/24/1513.02.00Siapan - Tanapag2 10 0.22

P109204 01/24/150.022 U0.20Siapan - Airport 1 0.022

WB1-0123 01/23/150.022 U0.20WB1-0123 1 0.022

WB1-0126 01/26/150.022 U0.20WB1-0126 1 0.022

WB2-0123 01/23/150.022 U0.20WB2-0123 1 0.022


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Total Dissolved Solids (TDS)ResultRL

SM2540C



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/23/1526625.0Siapan - Talafofo 1 4.2

P109202 01/23/1533925.0Siapan - Tanapag1 1 4.2

P109203 01/23/1535325.0Siapan - Tanapag2 1 4.2

P109204 01/23/1591.025.0Siapan - Airport 1 4.2

WB1-0123 01/23/154.2 U25.0WB1-0123 1 4.2


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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of 41

Draft

Matrix: Water

Client Sample ID


Date Analyzed

cm-1

Qualifier


UV254ResultRL

SM5910B



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 01/21/15 10:480.0370.0090Siapan - Talafofo 1 0.0018

P109202 01/21/15 10:490.0220.0090Siapan - Tanapag1 1 0.0018

P109203 01/21/15 10:500.0018 U0.0090Siapan - Tanapag2 1 0.0018

P109204 01/21/15 10:520.0950.0090Siapan - Airport 1 0.0018

WB1-0121 01/21/15 10:430.0018 U0.0090WB1-0121 1 0.0018


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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LCS IDDate

Analyzed


SampleResult

SpikeAmount



General Chemistry

Lab Batch ID: P1092


Matrix: Water


Alkalinity, Total as CaCO3 01/21/1551.2BS1W0121 E310.1mg/L47.6 108UV254 01/21/150.032BS1W0121 SM5910Bcm-10.028 113Sulfate 01/23/155.32BS1W0123 E300.0Amg/L5.00 106Sulfate 01/23/154.81BS2W0123 E300.0Amg/L5.00 96Total Dissolved Solids (TDS) 01/23/151010BS1W0123 SM2540Cmg/L1000 101Sulfate 01/26/155.13BS1W0126 E300.0Amg/L5.00 103Ammonia-N 01/27/151.17BS1W0127 E350.1mg/L1.09 107


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

BS150202-12:04-P1092-W





of 41

Draft


Lab Name: ASL SDG#:

Project #:

CH2M HILL ASL

156197.00.SAIPAN

P1092

Project: Saipan WTP

CASE NARRATIVE


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276










Method(s):E353.2

Matrix Spike/Matrix Spike Duplicate(s):E353.2: MSD recovery of Nitrate/Nitrite as N (110.9%) in Siapan - Talafofo did not meet acceptance criteriaof 90-110%.

KO150202-16:15-P1092-W of 41

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Matrix: Water

Client Sample ID


Date Analyzed

mg/L

Qualifier


Nitrate/Nitrite-NResultRL

E353.2



Type: See C.O.C.


General Chemistry

Lab Batch ID: P1092

Analysis Method:

Units:


P109201 02/02/150.0420.010Siapan - Talafofo 1 0.0028

P109202 02/02/150.0069 J0.010Siapan - Tanapag1 1 0.0028

P109203 02/02/150.0057 J0.010Siapan - Tanapag2 1 0.0028

P109204 02/02/150.0059 J0.010Siapan - Airport 1 0.0028

WB1-020215 02/02/150.0036 J0.010WB1-020215 1 0.0028


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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LCS IDDate

Analyzed


SampleResult

SpikeAmount



General Chemistry

Lab Batch ID: P1092


Matrix: Water


Nitrate/Nitrite-N 02/02/150.70BS1W0202 E353.2mg/L0.67 104


Corvallis, OR 97330

Tel 541-768-3120 Fax 541-752-0276

CH2M HILL ASL

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Sample Receipt Record

SDG ID: P1092

Client/Project: Saipan

Were custody seals intact and on the outside of the cooler?

10.4 °C

Was a Chain of Custody (CoC) Provided?

Was the CoC correctly filled out (If No, document below)

Did sample labels agree with COC? (If No, document below)

Did the CoC list a correct bottle count and the preservative types (No=Correct on CoC)

Were the sample containers in good condition (broken or leaking)?

Was enough sample volume provided for analysis? (If No, document below)

Containers supplied by ASL?

Any sample with < 1/2 holding time remaining? If so contact LPM

Samples have multi-phase? If yes, document on SRER

All water VOCs free of air bubbles? No, document on SRER

pH of all samples met criteria on receipt? If "No", preserve and document below.

Dissolved/Soluble metals filtered in the field?

Dissolved/Soluble metals have sediment in bottom of container? If so document below.

Reagent Volume Added24 hour pH check

Initials/Time

Resolution to Exception:

Temp OK? (<6C) Therm ID: TH173 Exp. 2/15

Preservation Adjustment

Did pH of all metals samples preserved upon receipt meet criteria 24 hours after preservation?

Shipping Record:

Packing Material:

Sample ID Initials/Time


Received By: KF

Radiological Screening for DoD

Client was notified on: Client contact:

Sample Exception Report (The following exceptions were noted)

Reagent Lot Number

Yes No N/A

On File COCHand Delivered

Yes No N/A

Ice Blue Ice Box

Yes No N/A

Hand Delivered

NoYes

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

Yes No N/A

DOC CONTROL ID: ASL593-0714 of 41

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for: saipan wtp - commonwealth utilities · 2017-09-26 · analytical report for: saipan wtp . asl...

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