fishbeck, thompson, carr & huber · 2016. 6. 11. · phase i remedial design additional studies...
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fishbeck, thompson, carr & huberengineers • scientists * architects
000003
PHASE I
REMEDIAL DESIGN
ADDITIONAL STUDIES REPORT
FOR
ELECTRO-VOICE, INC.Buchanan, Michigan
PHASE I
REMEDIAL DESIGN
ADDITIONAL STUDIES REPORT
FOR
ELECTRO-VOICE, INC.Buchanan, Michigan
April 1995Project No. F93307D
1995
Prepared by:
FISHBECK, THOMPSON, CARR & HUBER, INC.6090 East Fulton, P.O. Box 211
Ada, Michigan 49301-0211(616) 676-2666
7402 Westshire Drive, Suite 110Lansing, Michigan 48917-9764
(517) 627-1141
TABLE OF CONTENTS
1.0 INTRODUCTION . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11.1 Background . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 11.2 Work Plan Scope and Organization . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21.3 Geology and Hydrogeology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 21.4 Nature and Extent of Lagoon Area Soils Contamination . . . . . . . . . . . . . . . . 4
2.0 ADDITIONAL STUDIES WORK . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62.1 Lower Aquifer Investigation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6
2.1.1 Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 62.1.2 Soil Boring and Sampling Methodology . . . . . . . . . . . . . . . . . . . . . 7
2.2. Quarterly Groundwater Sampling . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 72.3 Lagoon Area Soils - Extent of Contamination Investigation . . . . . . . . . . . . . . 8
2.3.1 Purpose . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 82.3.2 Methodology . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 92.3.3 Background Calculations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 112.3.4 Results . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 122.3.5 Holding Times . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 14
3.0 DISCUSSION AND CONCLUSIONS . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 293.1 Lower Aquifer Investigation . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 293.2 Lagoon Area Soils - Extent of Contamination Investigation . . . . . . . . . . . . . . 293.3 Summary of Remediation Activities . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 31
4.0 REFERENCES . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 32
List of Tables
Table 2-1 • Background Soil Calculations . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 13Table 2-2 • Summary of Soil Sampling Results from Lagoon Investigation . . . . . . . . . . . . 15
List of Figures
Figure 1-1 * Location MapFigure 2-1 • Soil Boring Location MapFigure 2-2 • Soil Sampling MapFigure 2-3 • Lagoon Area Soil Analysis Decision Flow ChartFigure 2-4 • Depth of Soil Contamination MapFigure 3-1 • Cap Subgrade/Excavation Contours
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TABLE OF CONTENTS (continued)
List of Appendices
Appendix 2-A • Soil Boring Log for Lower Aquifer InvestigationAppendix 2-B • FTC&H Field Standard Operating ProceduresAppendix 2-C • Summary of Soil CharacteristicsAppendix 2-D • Laboratory Analytical Results for Lagoon Investigation Soil Samples
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1.0 INTRODUCTION
1.1 Background
I Electro-Voice, Inc. (EV) is a sound equipment manufacturer. Activities at the plant includeadministration, assembly, die casting, machining, painting, electroplating, research, and development.The plant is located in southwestern Michigan at the southern limit of the City of Buchanan, BerrienCounty, approximately six miles west of Niles, Michigan (Figure 1-1). The EV property isapproximately 11.5 acres in size and is located within the northwest quarter of Section 36, T7N, R18W.
In February 1983, EV was placed on the Michigan and the National Priority Lists. An Administrative
w Order by Consent (U.S. Environmental Protection Agency [U.S. EPA] Docket No. V-W-87-C-023) toconduct a remedial investigation (RI) and feasibility study (FS) was entered into by EV and the U.S. EPAon October 8, 1987. The results of the RI were presented in a report titled, Final Remedial InvestigationReport for Electro-Voice, Inc., dated August 1990, and prepared by Fishbeck, Thompson, Carr, &Huber, Inc. (FTC&H). The results of the FS were presented in a report titled, Feasibility Study Report,Electro-Voice, Inc. Site, dated September 10, 1991, and prepared for the U.S. EPA by CH2M Hill,
A Record of Decision for the First Operable Unit (ROD) (onsite remediation) was signed by the U.S.EPA Regional Administrator on June 23, 1992. The Operable Unit Consent Decree and Statement of
\ Work for the Remedial Design and Remedial Action for the First Operable Unit at the Electro-Voice Sitewas filed with the U.S. District Court on September 20, 1993. The Consent Decree/Statement of Work
} (SOW) divided the remedial design/remedial action (RD/RA) work into two phases: Phase I addressesthe former lagoon area soils investigation, including the extent of contamination investigation, the
installation and maintenance of a hazardous waste cap, lower aquifer investigation, and off-property.• groundwater monitoring; Phase II includes the installation and operation of a groundwater remediation
system, the installation and operation of a dry-well area soils remediation system, and the associated1 performance monitoring. On October 4, 1993, EV received authorization from the U.S. EPA to proceed
with the Phase I RD/RA work, as set forth in the Consent Decree/SOW.j
The major components of the RA for the first operable unit ROD for the EV site were discussed in the
Phase I Remedial Design Work Plan for Electro-Voice, Inc., prepared by FTC&H (February 1994).Greater detail regarding each component is also provided in the Consent Decree/SOW for the first
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operable unit (Appendix B of the Operable Unit Consent Decree). This report presents the results of thePhase I RD Additional Studies.
1.2 Work Plan Scope and Organization
The Consent Decree/SOW requires that two work plans be prepared as part of the Phase I work. Thefirst (SOW - Task II) was the Phase I RD Work Plan, which provided the overall management strategy
for performing the Phase I RD for the first operable unit at the EV site. The Phase I RD Work Planaddressed the additional studies for the lower aquifer investigation and the lagoon area soils - extent ofcontamination investigation, and the RD of the hazardous waste cap elements required in the ConsentDecree/SOW. Also included in the Phase I RD Work Plan, by reference, was the off-propertygroundwater monitoring program. Several additional elements were included, namely the site-specificHealth and Safety Plan, a Sampling and Analysis Plan, a site-specific Quality Assurance Project Plan(QAPP), a project schedule, a project organization plan, and a reporting summary, to complete thePhase I RD Work Plan. The Phase I RD Work Plan was prepared by FTC&H, and submitted to the U.S.EPA on November 30, 1993. The Phase I RD Work Plan was approved by the U.S. EPA on March 7,1994.
The second work plan (SOW - Task III) document to be prepared is the Phase I RA Work Plan, which
addresses the implementation of the Phase I RA. The Phase I RA Work Plan will be prepared after U.S.EPA approval of the final design submittal.
1.3 Geology and Hydrogeology
A summary of the geology and hydrogeology at the EV site follows. Further details on the geologic and
hydrogeologic setting may be found in the Electro-Voice Remedial Investigation/Feasibility Study WorkPlans (FTC&H, 1988), Phase II - Field Data, Volume I of III, Electro-Voice Rl/FS (FTC&H, 1989), andin the Final Remedial Investigation Report for Electro-Voice (FTC&H, 1990).
The local geology consists of unconsolidated glacial drift deposits underlain by the Late Devonian age
Antrim Shale Formation. The glacial drift consists of two primary units; an upper outwash sand andgravel unit, and a lower clay-rich till unit. The upper outwash unit is characterized as light-to-darkbrown, fine-to-coarse-grained, loose sand with varying gravel and pebble content. A general coarsening
downward sequence has been observed, with occasional silty sands and clayey zones in the upper horizon,
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grading to discrete and alternating intervals of fine, medium, and coarse sand with depth (FTC&H,
1990). The lower portion of the outwash sand and gravel unit comprises an areally extensive unconfmedaquifer. This unconfmed aquifer ranges in thickness from approximately 50 feet at the EV site toapproximately 10 feet near McCoy Creek to the north (FTC&H, 1980).
A blue-gray to gray-brown, clay-rich till unit underlies the upper aquifer or outwash unit. The till unit
is characterized as a very stiff, blue gray to gray-brown clay with minor sand and gravel. This clay-richconfining layer was encountered in all the investigative borings at the EV site that penetrated the aquifer,and was marked by drilling refusal at these locations. However, some of the borings did penetrate intothe till as much as 25 feet. The top of the clay-rich confining layer was found at elevations ranging from630 to 670 feet mean sea level (msl). The thickness of the till unit was not determined during the RI.However, regional well logs indicate the till unit ranges from 3 to 90 feet in thickness (FTC&H, 1990).
The thickness of the unconsolidated glacial deposits overlying the bedrock in Berrien County generallyranges from 101 to 200 feet (Western Michigan University [WMU], 1981). The glacial drift depositsat the EV site are estimated to be 150 to 180 feet thick (FTC&H, 1990).
The Late Devonian age Antrim Shale Formation consists of black shale. The elevation of the top of thebedrock surface ranges from 550 to 600 feet above msl (WMU, 1981). The elevation of the easternportion of the EV site is approximately 740 feet above msl. Hence, the depth to the Antrim Shale isestimated to be 140 to 190 feet below ground level (bgl). One residential well record (Well 36-53
[FTC&H, 1989]) describes a blue shale at a depth of 173 feet bgl. Presumably, this could be the AntrimShale. However, the exact location of this well could not be determined. The thickness of the Antrim
Shale is estimated to be between 50 to 100 feet (WMU, 1981). The Antrim Shale is underlain bylimestones of the Middle Devonian age Traverse and Detroit Group, and by evaporites of the LateSilurian age Salina Group (WMU, 1981). These bedrock formations are very dense, relatively
impermeable, and have no potential for groundwater supply.
The groundwater flow direction in the upper outwash aquifer is primarily northwesterly at the EV site.The direction trends to north-northeasterly in the central portion of the study area, and trendsnorthwesterly again at the northern portion of the study area near the McCoy Creek discharge boundary
(FTC&H, 1990).
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The depth to the water-table surface varies within the study area. The water-table surface isapproximately 30 feet bgl in the former lagoon area and decreases in depth to approximately 10 feet bglnear McCoy Creek. The water-table surface is as deep as 60 feet bgl in the south and central portion ofthe study area (FTC&H, 1990).
1.4 Nature and Extent of Lagoon Area Soils Contamination
The former dry well and the former plating waste lagoons were identified in the RI/FS as contaminantsource locations for the EV site. The Phase I RD Work Plan for the first operable unit addressed thecleanup/closure of the former lagoons. Information regarding other areas is provided in the Electro-VoiceRemedial Investigation/Feasibility Study Work Plans, dated July 1988, and the Final RemedialInvestigation Report for Electro-Voice, dated August 1990.
In 1952, EV constructed two bentonite-clay-lined lagoons, north and south, for disposal of liquid wastefrom the electroplating operation at the plant. The two lagoons were connected in series by an overflowpipe. EV discharged metal-plating waste to the north lagoon from 1952 to 1962. Use of these lagoonswas discontinued in 1962 after a new wastewater treatment facility was installed at the site (FTC&H,1990).
In September 1980, the north lagoon and its contents were removed. This included the removal of 9,500gallons of water, approximately 19,600 gallons of sludge, and 40 cubic yards of clay liner. Thesematerials were disposed of offsite. The area was then filled with clean soil (FTC&H, 1990). The southlagoon was not considered to be contaminated and was, therefore, filled with clean soil and contouredto match the natural surface topography of the area. Lagoon closure activity was performed inaccordance with Michigan's Hazardous Waste Management Act (Public Act 64 of 1979) and itsAdministrative Rules. The waste was listed on industrial waste disposal manifest forms, and approvedfor transportation and disposal by the Michigan Department of Natural Resources (MDNR) (FTC&H,1990).
Documentation related to the site history concluded that the soils contamination was confined primarilyto the immediate lagoon area. Subsequent surface soil sampling downslope and outside of the formerlagoon areas indicated elevated metal concentrations in the surface soils. It is believed that thesurrounding surficial soils were contaminated due to runoff and previous lagoon closure activities, suchas bulldozing contaminated soils to the edge of the lagoons, and the subsequent sediment transport ofthese soils. The horizontal and vertical extent of metals contamination in these soils were determined aspart of the Phase I RD.
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PROJECT NO.93307D
1-1
2.0 ADDITIONAL STUDIES WORK
The additional studies for the Phase I work included a lower aquifer investigation and a lagoon area soils- extent of contamination investigation. The purpose and methodology for each investigation is presentedbelow. Off-property groundwater sampling is ongoing as part of the Phase I work.
2.1 Lower Aquifer Investigation
2.1.1 Purpose
The purpose of the lower aquifer investigation was to determine whether a lower aquifer was present inthe vicinity of the EV site. This was done by loci ting a deep boring near MW-9D. The originalscreened auger boring near the location of MW-9D was completed to 93.5 feet bgl. The boring for theinstallation of monitor well MW-9D was completed to 74.5 feet bgl. The intent of this investigation was
to sample below the depth of the previous borings to determine if a lower aquifer was present. If such
an aquifer did exist, a groundwater monitor well would be installed to determine if any site-related
contamination had been released to this aquifer.
The thickness of the upper aquifer at the site was estimated to be 50 feet (FTC&H, 1990). A clay-til!unit underlies this aquifer. A double-cased soil boring was to be drilled 15 feet into the clay-till unit nearonsite monitor wells MW-9S and MW-9D, an area that directly underlies groundwater contamination ofthe upper aquifer (Figure 2-1). Contaminants historically detected in MW-9S and MW-9D include thevolatile organic compounds (VOCs) 1,1-dichloroethane, 1,2-dichloroethene (total), and vinyl chloride.If clay was present below approximately 90 feet, three soil samples of the clay til!, collected at intervalsof 5, 10, and 15 feet into the clay till, were to be submitted for laboratory analysis of VOCs.
If a water-bearing unit 5 feet or more in thickness and capable of yielding a substantial quantity of
groundwater to a monitor well was encountered, one or more groundwater samples would be collectedand analyzed for VOCs in lieu of analyzing the clay sampies. If the water-bearing unit was less than 10feet thick, a groundwater monitor well would be installed at the top of the unit and sampled for VOCs
analyses. If the water-bearing unit was greater than 10 feet thick, vertical groundwater profile samplingfor VOC analysis would be performed at 10-foot intervals through the thickness of this lower water-bearing unit. The proposed methodologies for the soil boring, soil sampling, vertical groundwater profile
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sampling, monitor well installation, and groundwater sampling were provided in the Phase I RD WorkPlan.
2.1.2 Soil Boring and Sampling Methodology
The soil boring, LAB-1, was performed on May 11 and 12, 1994, by Stearns Drilling Company ofDutton, Michigan using 8V4-inch inside-diameter hollow-stem augers. Drilling proceeded to 89 feet bgl,where a clay-till was encountered. A split-spoon sample collected at 89 to 91 feet bgl contained a stiff
silty clay. The drilling continued to 93 feet bgl to set the outer steel casing. However, a hard
clay/bedrock surface was encountered at 93 feet bgl. A split-spoon was collected from 92 to 92.2 feetbgl. The collected sample appeared to be predominantly "slough" from the overlying strata. However,reddish brown clay and some shale fragments were present in the tip of the spoon. The augers weresubsequently cleaned to clear the "slough" and a second spoon was driven to collect another sample from92 feet bgl. The blow counts for the second split-spoon were 200 counts for \ inch of spoon driven; the
augers were at refusal. The tip of the spoon contained a hard red-brown clay with fragments of reddish-brown shale.
It was determined that this lower reddish-brown strata was the top of the underlying bedrock shale, andthat a lower aquifer, or water-bearing zone, was not present. This conclusion was based on the extremelyhigh drilling pressure, the high blow counts (200 counts for \ inch of recovery), the presence of shale
fragments in the split-spoon and on the drill bit, and the reddish-brown color of the shale fragments whichwas indicative of the local underlying weathered shale formation. The decision was made to abandon andgrout the boring following discussions with the U.S. EPA. The boring log for LAB-1 is included inAppendix 2-A.
2.2. Quarterly Groundwater Sampling
Quarterly off-property groundwater sampling continued in accordance with the U.S. EPA approved
Electro-Voice, Inc., Groundwater Monitoring Plan for U.S. Environmental Protection Agency (FTC&H,November 1992). The first sampling event under the Phase I RD/RA was conducted in April 1994.Quarterly sampling was conducted in June and September 1994. The annual groundwater sampling wasconducted in January 1995. The sampling will continue on a quarterly basis until the second operable
unit ROD is effective or until the U.S. EPA, in conjunction with MDNR, determines that monitoring is
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no longer necessary. The results of the groundwater analyses have been forwarded to the U.S. EPA and
MDNR as they are received.
2.3 Lagoon Area Soils - Extent of Contamination Investigation
2.3.1 Purpose
The purpose of the lagoon area investigation was to determine the horizontal and vertical extent of soilsthat required capping/excavation outside of the proposed former lagoons cap area. Previous limited soilsampling for specific metals downslope and outside the proposed lagoon cap area was conducted by EVprior to the preparation of the Phase I RD Work Plan. The sampling indicated that surficial soils, 1 to2 feet bgl, were contaminated and most likely would equire excavation and placement beneath the cap.
Two types of soil sampling could have been used to determine the extent of the lagoon area soils to beexcavated; cleanup verification sampling prior to excavation or post-excavation cleanup verificationsampling. The former method, sampling prior to excavation, was chosen as the more efficient way toevaluate the lateral and horizontal extent of contaminated soils. Potential consequences of performingcleanup verification sampling after excavation include:
Delays in capping the contaminated material while waiting to sample and for laboratoryturnaround of the verification samples. This would expose contaminated soil to wind andsurface water erosion.
Time and costs associated with contractor mobilization/demobilization due to failure to
determine the full extent of contamination, including multiple delays for additional rounds of
sampling and laboratory analysis.
Delays caused by cap redesign due to additional soils being placed under the cap.
The analytical results from the soil sampling were used to determine which soils had been impacted fromlagoon area contaminants. The impacted soils would then be remediated with the former lagoon areas.The soil sampling and statistical analysis of the analytical results were conducted in accordance with theMDNR Cleanup Verification Guidance Document (MDNR Guidance Document), dated November 1991.
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2.3.2 Methodology
The area of investigation was initially estimated to cover approximately 97,000 square feet (Figure 2-2).
According to the MDNR Guidance Document, this acreage is considered a medium-sized site. Hence,the grid interval for stationing was calculated using the following equation:
Where: GI = grid interval (feet)A = area to be gridded (square feet)
Based on this calculation, a grid interval of 44 feet wj > required for the soil sampling. The grid layout
for 67 initial investigative soil sampling locations was surveyed and staked to establish the horizontallocation and elevation prior to soil sampling. The 44-foot grid interval used was actually a greaterdensity than could have been used. Additional soil sampling locations were added laterally beyond theoriginal area of investigation, resulting in a larger area of concern. Using the larger area in the above
formula would have resulted in a wider grid spacing. However, to maintain consistency with the originalsampling grid spacing, the 44-foot interval was used for the additional soil sampling points. Theinvestigated area of concern, with a superimposed grid interval of 44 feet, is shown in Figure 2-2. Soilsamples were initially collected at depth intervals of 0 to 1, 1 to 2, 2 to 3, 3 to 4, and 4 to 5 feet bgl ateach grid node. Background soil samples were also collected at five locations, as shown in Figure 2-2.
The background soil samples were collected from each soil horizon encountered while augering from a
depth of 0 to 5 feet bgl. The first round of soil sampling at each of the grid nodes, LSB-1 thoughLSB-72, and at each depth interval (0 to 1 foot bgl through 4 to 5 feet bgl) was conducted by FTC&H
personnel from April 25 to May 11, 1994.
The soil samples were obtained using a closed head, stainless-steel hand auger in accordance withFTC&H Standard Operating Procedure (SOP) #F6-4.1 (Appendix 2-B). The soil samples were identified
using the sample labeling criteria provided in the Phase I RD Work Plan QAPP. The soil samples were
collected in the appropriate bottles, packed in ice, and transported to the laboratory under chain-of-custody procedures (SOP #F3-2 in Appendix 2-B). The analytical methods, sample packaging, bottles,
and hold times were specified in the Phase I RD Work Plan QAPP. The hand auger was decontaminatedbetween samples by washing with a trisodium phosphate solution, rinsing with deionized water, andallowing to air dry. Decontamination fluids were containerized for later disposal. Field locations and
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other pertinent notes were recorded in the field notebook per SOP #F3-1 (Appendix 2-B). Soilcharacteristics of the samples are summarized in Appendix 2-C.
The Michigan Environmental Response Act (MERA) allows soils to be remediated to background
contaminant levels, Type A Default levels, or to a level which will pass an acceptable leaching test. Thecalculation of background soil contaminant values is discussed in Section 2.3.3 Background Calculations.The Type A Default levels in soil are provided in the MDNR MERA Operational Memorandum No. 15,Default Type A Cleanup Criteria. The soil samples can also be leached by a leaching test which isapproved by MDNR MERA Operational Memorandum No. 12, Alternate Leaching Tests. The results
of the leaching tests are then compared to the appropriate groundwater criteria for evaluation purposes.
Any one, or a combination, of these criteria may be used to establish acceptable contaminant levels ata site or for individual samples.
Based on these analytical alternatives and to establish a methodical procedure, the soil samples weresubmitted for laboratory analysis using a phased approach. The phased analytical approach for theinvestigative soil samples is shown in the logic diagram in Figure 2-3. Initially, soil samples weresubmitted for laboratory analysis of the indicator analytes cyanide, cadmium, and chromium. Further
analyses were conducted based on the analytical results of these indicator analytes. If the indicatoranalyte concentrations in a soil sample were below their respective State of Michigan, Act 307 Type ADefault levels, the soil sample was analyzed for the remainder of the metals of concern. The metals ofconcern were arsenic, barium, copper, lead, nickel, and zinc. If the concentrations of the metals of
concern were below their respective Type A Default levels, the soil sample was considered clean.
If one or more of the indicator analyte concentrations was above its respective Type A Default
concentration, a leaching test for the analyte(s), the Synthetic Precipitation Leaching Procedure (SPLP),
was performed. The SPLP is approved for metals analyses per the MDNR MERA OperationalMemorandum No. 12, Alternate Leaching Tests. The soil sample was submitted for either total metalor SPLP analysis of the metals of concern (arsenic, barium, copper, lead, nickel, and zinc) if theindicator analyte concentrations from the SPLP were below their respective cleanup criteria. The soilsample was considered clean if the concentrations of the metals of concern were below the cleanupcriteria, or if the concentrations of the metals of concern from the SPLP were below the cleanup criteria.
At any point in the comparison process (i.e., at any "no" point on Figure 2-3), the sample could beconsidered contaminated if the results were above the appropriate cleanup criteria.
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2.3.3 Background Calculations
The Phase I RD Work Plan was written so that the metal and cyanide concentrations in the soil samples
could be compared to either the Type A Default criteria, or the respective background concentrations inthe soil to determine if the soils were clean or contaminated. The leachate concentrations from the soilsamples could also be compared to the appropriate cleanup criteria to determine if the soil samples wereclean or contaminated. To establish background concentrations, the background soil samples, LSB-68,LSB-69, LSB-70, LSB-71, and LSB-72, were submitted for laboratory analysis of total arsenic, barium,cadmium, chromium, copper, cyanide, lead, nickel, and zinc. The background analyte concentrationswere calculated following the statistical methods presented in the MDNR Guidance Document (Table 2-1).
The mean background concentration (Xb) and background variance (Sb) were calculated for each analytewithin each soil horizon. Three soil horizons were encountered at the background soil sampling location;
a silty clay, a clayey sand to clayey silt, and a sand to silty sand. The background coefficient of variance(CV) was also calculated for each analyte and each soil horizon to evaluate the data distribution. Thebackground value or maximum allowable limit for each analyte within each soil horizon was calculatedfor each analyte with a CV less than 1.00. The background value equaled the sum of the meanbackground concentration for each analyte plus three times the standard deviation for that analyte (Xb 4-3Sb). The results of the background soil sampling analyses are presented in Table 2-1.
The background metal and cyanide values were calculated to evaluate whether the local metal and cyanideconcentrations in the soil were higher than the Type A Default values. Higher background values wouldprovide more latitude in evaluating whether a sample was clean or contaminated. In general, the localmetal and cyanide values, based on three analyzed soil samples, were lower than the referenced Type A
Default values. Hence, four soil samples (n = 4), as required by the MDNR Guidance Document, were
not analyzed for each of the soil horizons. The Type A Default cleanup criteria and the leachateconcentrations were used instead to evaluate the soils investigative data.
Background concentrations of arsenic, chromium, and lead in the silty clay horizon (n = 4) were greaterthan the Type A Default values. These data (arsenic, chromium, and lead concentrations in the silty clayhorizon) were not used to evaluate whether the investigative soil samples were clean or contaminated
because the respective soil horizons were not always comparable. Furthermore, it was easier to applythe Type A Default criteria uniformly to the investigative soil samples, rather than matching the analytes
in each investigative soil horizon with the respective analyte and comparable background soil horizon.
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2.3.4 Results
Investigative soil samples, LSB-1 through LSB-67, and background soil samples, LSB-68 through
LSB-72, were collected in a single sampling event from April 25 to May 11, 1994. Based on the
analytical results of the investigative soil samples, three additional soil sampling rounds to collect soil
samples at deeper depths and at new sampling locations were performed. The rationale and background
for each additional soil sampling round are discussed below.
Soil samples from the 4- to 5-foot bgl interval from LSB-1 to LSB-67 were submitted first for the analysis
of cadmium, cyanide, and total chromium (indicator metals). The results of these analyses aresummarized in Table 2-2. Cadmium, total cyanide, and chromium concentrations above the Type ADefault soil levels were detected in some of the sample.' from the 4- to 5-foot bgl interval. These samplesincluded LSB-2, LSB-5, LSB-8, LSB-9, LSB-13, LSB-14, LSB-18, LSB-28. LSB-32, and LSB-38.
Therefore, additional samples from the 6.5- to 7.5-, and the 9- to 10-foot interval bgl were obtained atthese locations during a second round of sampling. Soil samples from the 9- to 10-foot bgl interval were
then submitted for analysis of the indicator metals.
In addition, three new soil sampling locations, LSB-73, LSB-74, and LSB-75, were located 33 feet northof LSB-1, LSB-2, and LSB-3, respectively (Figure 2-2) to funher define the lateral extent of the lagooncontaminants. The land begins to slope up near these borings. Hence, a spacing of 44 feet would haveplaced the borings too far up the hill, and beyond the impact of surface runoff from the lagoons. These
new soil sampling locations were sampled at depths of 0 to 1, 1 to 2, 2 to 3, 3 to 4, 4 to 5, 6.5 to 7.5,and 9 to 10 feet bgl. Soil samples from the 4- to 5-foot bgl interval were initially submitted for theindicator metal analyses. This second round of soil sampling was conducted between June 21 and 23,
1994.
A tentative western boundary for the lagoon cap was established based on the analytical results of the soil
samples from the 4- to 5-foot bgl interval. This tentative boundary coincided with the north-south soil
grid line beginning at LSB-81, and extending south to LSB-54, then angling southeast to LSB-66. The
samples selected for laboratory analyses were west, or outside of the tentative cap boundary. Soil
samples from the 0- to 1-foot bgl interval and west of the proposed lagoon cap extent were submitted forthe indicator analyses after receipt of the analytical results from the 4- to 5-foot bgl interval. Cadmium,total cyanide, and/or chromium concentrations above the Type A Default levels were detected in someof the soil samples from the 0- to 1-foot bgl interval. These samples included LSB-I, LSB-3, LSB-4,
04/14/95 ' - 11 -
LSB-7, LSB-10, LSB-19, LSB-20, LSB-22, LSB-23, LSB-44, LSB-64, LSB-65, and LSB-67. Therefore,14 new soil sampling locations, LSB-76 to LSB-89, were sampled at depths of 0 to 1, 1 to 2, 2 to 3, 3to 4, and 4 to 5 feet bgl (Figure 2-2) during the third round of soil sampling. Soil samples from the 0-
to 1-foot bgl interval were submitted for the indicator metal analyses. These new locations were used
to further define the lateral extent of the lagoon contaminants.
Cadmium, total cyanide, and/or chromium concentrations above the Type A Default soil levels weredetected in samples from the 9- to 10-foot bgl interval at locations LSB-5, LSB-8, LSB-13, LSB-28, andLSB-38. Deeper soil samples were obtained by hand augering to the 14- to 15-foot bgl interval forLSB-28 and LSB-38, and to the 16-to 17-foot bgl interval for LSB-5, LSB-8, and LSB-13. These soil
samples were submitted for the indicator metals analyses. This third round of soil sampling wasperformed July 25 though 29, 1994.
It was not possible to hand auger soil borings LSB-82 through LSB-85 north of the lagoon area, as bricks,cement blocks, and other near-surface debris were encountered. These soil borings and additional soil
borings LSB-90 through LSB-93 (Figure 2-2), were performed during the fourth round of soil samplingon November 16 and 17, 1994, using a backhoe to remove the near-surface debris. The soil sampleimmediately below the surface debris, at the native soil horizon, was submitted for total arsenic and leadanalyses, and the SPLP analyses of barium, cadmium, chromium, copper, cyanide, nickel, and zinc.
Many of the soil samples from the 4- to 5-foot bgl interval were submitted initially for laboratory SPLP
analyses of the remaining metals of concern, specifically, arsenic, barium, copper, lead, nickel, and zinc,rather than total metals analyses of the metals of concerns. Selected soil samples from the 9- to 10-footbgl interval and deeper sampling depths were also submitted for the SPLP analyses of the metals ofconcern rather than total metal analyses.
The following rationale was used for submitting the soil samples for SPLP analyses of the metals ofconcern rather than for total metals analyses. Five soil samples were submitted during the early stageof the investigation for total metals analyses of the metals of concern, specifically, arsenic, barium,
copper, lead, nickel, and zinc. Three soil samples were chosen from locations with high indicator metalconcentrations (LSB-20, LSB-32, and LSB-51), and several soil samples were chosen from locations with
indicator metal concentrations below the Type A Default concentrations (LSB-27 and LSB-58). The totalmetal concentrations for the metals of concern ranged from below the Type A Default concentrations to
above the Type A Default concentrations. Comparison of total indicator metal concentrations with SPLP
04/14/95 - 12 - froh
results showed the SPLP analyses to be a better measure of soils exceeding State of Michigan cleanupcriteria. Based on these analyses, the remaining soil samples were submitted for SPLP analyses of the
metals of concern rather than for total metals analyses to speed the investigative process. This revisedapproach was made in consultation with the respective regulatory agencies.
The soil analytical results are summarized in Table 2-2, and the laboratory sheets with the analytical
results are provided in Appendix 2-D. The depth and extent of contamination, based on any metal of
concern or cyanide exceeding the cleanup criteria in the soil samples, is shown in Figure 2-4. Thefollowing assumptions were used to generate Figure 2-4. First, the extent of contamination in areaswhich will be under the cap is not shown. Second, locations where contamination is not believed to bedue to the lagoons are not shown. These include soil sampling locations LSB-67 and LSB-89 on the southend of the site, and soil sampling locations LSB-4, LSB-7, LSB-73, LSB-74, LSB-75, LSB-76, LSB-78,and LSB-80 at the northwest end of the site. The rationale for not including these locations in the extent
of contamination is discussed in Section 3.2 Lagoon Area Soils - Extent of Contamination Investigation.
Third, the debris area north of the cap (soil sampling locations LSB-82 through LSB-85, and LSB-90
through LSB-93) is not included as the soils beneath the bricks and concrete were clean.
2.3.5 Holding Times
Some of the soil samples were held more than six months before laboratory analysis due to the sequential
nature of the soil sample submission and the performance of additional sampling rounds. The U.S. EPA
expressed concern over this issue and commented that analytical results from soil samples exceeding the"six months hold time" should be considered "biased low."
In general, there are no holding times for either the metals of concern or cyanide in the soil samples.
Sometimes the holding time for metals in water samples, six months, is followed for soil samples.However, the metals of concern are chemical elements which may be bound in the soil as oxides,sulfides, hydroxides, or other complexes. The complexes holding the element in the soil may breakdown
or change with time. However, the metal itself will still remain within the soil. This is different from
VOCs or other organic compounds which can volatilize from and/or breakdown into different compoundswithin the sample. In the case of organic compounds, analyses of a sample beyond its holding time,
compared to one within its holding time, can produce very different results because of these processes.However, soil samples are digested prior to metal analysis to breakdown the complexes holding the metal
elements and to release these metals into solution. Therefore, metals present in the soil sample when it
04/14/95 - 13 -
froh
was collected will still be there when the soil is analyzed regardless of the holding time. Hence, it is notnecessary to consider metal analyses conducted beyond the "six months hold time" as "biased low."
Cyanide in the soil samples is also relatively immobile. The cyanide is believed to be tightly bonded to
copper, zinc, and nickel or other metals in the soil. Because of the relatively high metal concentrations
in the soil, any free cyanide ions would probably complex with the metals in the soils. Any free
hydrogen cyanide, which is very volatile, would have migrated from the soils vadose zone prior to samplecollection. The total cyanide analysis for soils is designed to breakdown the soils' metal - cyanidecomplexes, and to release HCN, which can be detected and measured. Therefore, as with the metals,cyanide present in the soil sample when it was collected will still be there when the soil is analyzedseveral months past the holding time. It is not necessary to consider cyanide analyses conducted severalmonths beyond a "six months hold time" as "biased k A-."
04/14/95 - 14- froh
o
£
TABLE 2-1^ Background Soil Calculations ^__
Results reported in micrograms per kilogramsSand/Silty Sand
Analyte
ArsenicBariumCadmiumChromiumCopperCyanideLeadNickelZinc
Type ADefault Value
5,80075,000
1,20018,00032,000
39021,00020,00047,000
LSB-68(4.5-5')
—~
669,100
~ND
------
LSB-69(2-3')2,100
27,00041
5,2006,400
ND6,1006,300
26,000
LSB-70(7.5-8')
„,__
398,300
~150-~-
LSB-71(2-3')2,700
48,00082
7,4007,400
ND11,0009,400
34,000
LSB-72(3-4')
4,10030,000
3511,00013,000
3509,000
13,00043,000
Mean
2,96735,000
538,2008,933
1008,7009,567
34,333
Std. Dev.
8389,274
181,9132,904
1382,0122,7386,944
Mean +3SD
5,48162,821
10713,93917,647
51414,73517,78055,166
Clayey Silt
Analyte
ArsenicBariumCadmiumChromiumCopperCyanideLeadNickelZinc
Type ADefault Value
5,80075,000
1,20018,00032,000
39021,00020,00047,000
LSB-68(0-1')3,700
59,000280
11,00011,000
ND20,00011,00059,000
LSB-69(o-r>2,600
48,000280
6,0008,100
ND19,0007,100
40,000
LSB-70(0-1 ')2,800
49,000200
7,0008,000
ND15,0008,400
36,000
LSB-71(3-4')5,600
59,00070
15,00016,000
ND15,00020,00067,000
Mean
3,67553,750
2089,750
10,7750
17,25011,62550,500
Std. Dev.
1,1865,262
863,5623,248
02,2785,035
12,894
Mean +3SD
7,23369,536
46520,43620,520
024,08326,73089,181
Siltv ClayAnalyte
ArsenicBariumCadmiumChromiumCopperCyanideLeadNickelZinc
Type ADefault Value
5,80075,000
1,20018,00032,000
39021,00020,00047,000
LSB-68(2-3')4,000
50,00064
12,00013,000
ND7,800
13,00040,000
LSB-70(3-4')2,600
94,000220
11,0008,100
ND8,300
13,00040,000
LSB-72(1-2')3,800
89,000190
12,0008,800
21017,00014,00056,000
Mean
3,46777,667
15811,6679,967
7011,03313,33345,333
Std. Dev.
61819,669
68471
2,16499
4,224471
7542
Mean +3SD
5,321136,675
36113,08116,458
36723,70514,74867,961
CV
0.180.250.430.040.221.410.380.040.17
ND = Not Detected 3SD = Three Standard Deviations— M«f A n., i,^(i CV = Coefficient of Variance
CV
0.320.100.410.370.30
00.130.430.26
CV
0.280.260.350.230.331.380.230.290.20
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
2vo
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals; passed if nol shaded.
's/l
en5T£.ouio^*o^^l
1
ONi
t~~h""ijy\h— J*
DcpiliCd £tt Cl
1 530.',^.4j76q 8.5002345 510 250 12,00071017
Cd CH Cr1 i.4QQ 450 14,0002345 270 160 9,00071017
Cd Ctt Cti2345 71,000, ; ;^460, , 2iOCO7 ; $2,0$' 290 ?4^S^:
1017 20,000 - '^570- /t^OOO
Cd CM Ctl i^tffl 7JQ 22JJQQ2345 U U 12,0007
1017
LSB-Ol LSB-02A s B j C i i N i E b Z n C d C M C l A s E a C u M i
U 1,100 U U U 30 8.900 U 18,000 U 1.200 U U
2.000 U 9.100 U 620 U U
LSB-03 LSB-04A s B a C u N i E b Z n C d C M Q A s B a C u ^ i
U 1.400 U U U 40 2,100 460 18,000^ ,-'iff| 760 U U
U 430 U U U U 360 U 1 1 .000 L 1.200 U U
LSB-05 LSB-06A s E a C u t l i E b Z D C d C M C i A s f i a C u M i
• 15,000 i ,580" ; -^Oot)"
/ 1.200 20 U I 60 1,7QQ U 13.000 (/ 980 U U
0 710 U U U 20
LSB-07 LSB-08A s E a C u K i E b Z n C d C N C r A s E a C u K i
(/ 450 U U , & 90
i 1.000 U U 1 30 5,800 150 ' 57,000 U 1.200 U U
21,000 680 28,000 U 540 U U25.000 250 9,700 / MOO 20 U
i • ————————————————
DepthEb Zn
1234
U 40 51
U 40 1017
Eb Zu3 20 1
234
[/ 20 57!017
Eb Zn1234
U 20 511017
Eb Zni234
V JO 57
tf 50 10.? 110 17
'
TABLE 2-2 ^_Summary of Soil Sampling Results from Lagoon Investigation
Regular Font - samples analyzed initially for total metals. Reported as ug'kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metafs; passed if not shaded.^~ Dopih LSB-09 LSB-107 0 C s l C N C i A i B a C u M i E b Z i l C U C N C r A s B a<. ' 5J3QQ 20Q 18,000 U 1,000<s> 2a 38 4w 5 . 36X86 i7oV$3RtiBB u 590 u v v 20 410 iso 1 1,000 u 2300 ?
\oUi 10 1.800 U 1 1 .000 U 380 U U U 30^ 17
LSB-ll LSB-12C d C M C t A s B a C u M i E b Z o C d C M C i A s B a
1 600 240 9.100 V 690 V U U 50 ^H4,600 ' •°'l "'/:':'27,OQli'23
i 4— 5 220 U 10.000 U 640 U U U U USQ V 22JJQQ U 980
11017
i-sn-13 I.SB uC d C M C i A s B a C u N i E b Z n C U C N C i A s U a
l2345 , ;•; '24,606 I.OW^^M.OOO U 490 U U U 30 170 U 43.000 U 1.000710 '- l^jjBISB''**"'"''^^0? U 610 U U U 30 120 U 24.000 » J5017 .•..'•^^^pvJMtf: 11,000 2 /.Of» 20 U '£,, 140
LSB-15 LSB-I6C d C N C r A s B a C u M i E b Z a C d C M C i A s B a
1 220 U 7,200 2 530 U U U 30 330 270 7,300 (/ 5002
H"5 4^S 5 U U 4,100 110 U 8.600 U 610
<T 7MT-. 10N-> ,7
DepthCu Mi Eb Zn
f t/ y #> i234
u u u u s11017
Cu Mi Eb Znl234
(/ W U 40 571017
CD Mi Eb Zni234
V U U 80 51
U U U 10 1017
Cu Mi Eb Zn(/ U U 10 1
234
U U (1 10 511017
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
9a
ioU)o
Depch
2345710
1234
.5710
2345710
12345710
LSB-17
Italicized Font - samples analyzed initially for SPUP. Reported as ug/l.Shaded values are above Type B criteria
Underlined parameters were analyzed for total metals; passed if not shaded
LSB-18Cd CM Ci As Ba Cu
18,000 1,800 '"39,000
I.6QQ ilfl 18,000 / 7,400
LSB-19
60
Cd CM Cr As Ba
790 42Q JI.QQQ U
240 U 2JJJQQ U
940
1.100
Cu Ml Eb In
U U U
10 U U
30
Depth
123457
70 10
LSB-20
Cd CM &120 : 5\flba' 6,300
As Ba Cu Mi Eb Zn Cd CM' zirT6bo i'
& As Ba4,500
U U 5,900 3,000 400 U U 5,600 U 170 U 8.500 U 500
Cu Mi Eb Zn100,086"". 37,000"*" '51,000 410,000
U V U 20
LSB-21 LSB-22
Cd CM Ci As Ba Cu Hi Cb Zn CdHJQQ
CM Cc11,000
ASU
Ba600 U U 2 20
3 .900 250 18,000 630 U 40 230 260 9,100
LSB-23 LSB-24
Cd CM Ci2.400 1.300 14,000
65 U 11,000
AsV 620
CuU
Mi[7
Zn40
Cd360
45
34
CK320
Ci8,000
14,000
10,000
AS(7
Ba590
Cu MiU U
ttU
Zn60
2345710
2345710
2345710
O
5D
{_/!
?
1.o
TABLE 2-2 -._-Summary of Soil Sampling Results from Lagoon Investigation
Depth
234571015
1
234571015
1214571015
23457
10
Regular Font - samples analyzed initially for lotal metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
LSB-25
110
110
67
Cd
J.3QQ
Cd
14,000
Italicized Font - samples analyzed initially for SPLP. Reported as ug/lShaded values are above Type B criteria.
Underlined parameters were analyzed for total melals; passed if not shaded.
LSB-26Cd190
CN260
Ci10,000' '
As Ba7/0
CuU U
Eb Za60
Cd780
CN41Q
Ci12,000
ASU
Ba1.000
Cu NiU
Eb ZD30
6.900 110 570
LSB-27 LSB-28
U 7,100
U 6.800 (/ 640 U U U 3,80b
4.9002 6 0 i l Q :4QQ 14.000
1,300
1.700470
LSB-29Cr
58Q 16.000
L'.i
470
Mi 2JI Cr fia
10
LSB-31
40 270 U 4,600 V 310
LSB-32
Cr As
380 iV
N i Q j Z n C d C N C r A s B a
167,000 5,500 ;/250;OOb 2,200 50,000
1,200 220 ••;'" 64 300
2010
Cu
Cu Ni Eb
10
Cd190
CNU
Cr11,000
As4,400
DJ52,000
Cu14,000
Ni13.000
Eb17,000
Zn5JJQQ
Cd CN Cr AS Ba Cu Ni Eb Zu
40
19020
Zn
66,060 ; 110,060 990,000
Depth
234571015
234571015
1234571015
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
(—) Regular Font - samples analyzed initially for total metals. Reported as ug/kg.^ Shaded values are above Type A criteria.j^ Underlined parameters were leached; passed if nol shaded.
a
Depth
45710
2,300 270
LSB-33
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals; passed if not shaded.
LSB-34CN Ci As Ba24 IOO^y^-3, 480
Cu30
Ni ^ Eb ZD190
Cd CN Ci58 70
270
ASU
BaJ/0
Cu Ni20 U'
Za!40
Depth
2345710
LSB-35 LSB-36
o
Cd CN430 U
92 150
Cr As Ba Cu6,700 U 450 10
14,000
Ni Eb Zn CdU U U 120
61
CM240
U
C[12,000
6,500
ASU
U
Ba530
610
CuU
U
Niu
U
Eb ZnU 60
U U
123457
LSB-37 LSB-38
234571015
Cd Cfcl Ci As Ba Cu
95 MQ 13.000 U 250 U
Ni E b Z n
U 20
C d C M C l A s f i a
340 15,000TSSt 13,000
',,4 1,600U 490
Cu Mi
20 UU U
Eb Zu123457
130 10[/ 15
LSB-39 LSB-40C d C N Q A s
440 280 8,800 U 530 U
C d C M C i A s
3 20 1?,0«) 9,2iO(J</ ;32.000
Ba Cu Hi Eb Zn
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
Italicized Font - samples analyzed initially for SPLP. Reported as ug/).Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals; passed if not shaded.
O
Ui
Depth
1234571015
LSB-41 I.SB-42C d C N C r A s B a C u N i E b Z n C d C M C i A s
390 U 7,600
£11 Mi tt 2nDepth
234571015
LSB-43 LSB-44
to
Cd CM Ci Ai Ba Cu
1.900 'r2',SOO 12,000
C d C N C i A s
81 U 13.000
Ba Cu Ni Eb in12345710
LSB-45 LSB-46
2345710
Cdno
CN180
Q12,000
ASU
Ba970
CuU
MiV
EbV
ZQ40
Cd310
CM4QQ
Ci7,600
AsU
Ba710
Cua
Miu
Ebu
Zn60
120 U 9,000 L 820 U U V 20 110 U 9,200 U 260 10 U U 10
2345710
LSB-47 LSB-48
23457
10
Cd CM Ci As130,8)0 2,300 76.000
E a C i i t i i E b Z n C i l C N C i A s
2.200. 150 12,000 U 660 U U 40 800 220 9,800 U 250
Cu Ki Eb Zn
U U U U
12345710
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
O
£
.s.OLMWOvBLfl
NJ
Depth
12345710
23457If)
12345710
12345710
Regular Font - samples analyzed initially for total metats. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed rf not shaded.
LSB-49
Italicized Font - samples analyzed initially for SPLP. Reported as ugfl.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals; passed if not shaded.
LSB-50Cd CM Cc As Ba Cu
210 U 3,900 U 240 U U U U !<f&?
LSB-51
Cd CM Ci As Ba
8,300
LSB-52Cd CM Ci As Ba Cu N i E b Z n Cd CN Ci As
. 32,006 v •"-.; 9,'«6b; 220:000 i .300 6,900 ••74,1606.'. . 43,000 11 .coo '^ilSfobtiJ 530 200 24.000
USB-53 LSB-54
82 U 7.800 U 320 U U U 10
LSB-53
75 -"" 9,lJi» 7,200
39 160 5,800 U 560
LSB-56C d C N C i A s B a C u
1.8QQ 430 24.000 U 300 U U U U 980 190 6,400 U 430
Cu Mi
U U U
C d C M C r A s B a C u M i E b
U U U
la
Cd150 u
Ci8,100
As(/ 1,000
Cuu
Miu
Eb Zn Cd CN Cr As Ba Cu Mi Eb Zu
Dcpih
2345710
12345710
23457
U 10
Zn12345710
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
O£:£^O^-/l
CD-.8Q-O
u3O^o^HI/1
t
OJ1
r>i
Reg
Depth
1
2
34
57
10
1
234
5
7
10
12
34
57
10
1
2
3
457
10
ular Font • samples analyzed initially for total metals. Reported as ug/kgShaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
LSB-57
Cd CM Ci As Ba Cii250 U 6.200 U 1.300 U
44 U 11,000 U 440 U
LSB-59
Cd CN Ci As fia Cii32.000 31800 74,000
530 170 9,700 (7 580 U
610 270 13.000
LSB-61
Cd CN Ci As Ea Cii210 390 8,900 U 1. 100 U
39 220 5,200 U 620 U
LSB-63
Cd CN & As Ba Cu,190,0136 ::f4>OS. 180.000
-W2iw::- *t^*y&$to3.JQQ 390 13.000 U 430 U
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for tolal metals; passed if not shaded.
LSB-58 Depth
Ni Eb Zn Cd CN Ci As fia C u N i E b Z nU 6 40 180 U 5.100 1,500 27,000 5,800 6,400 9,300 33.000 1
259 180 12.000 3
4U U 20 58 U 6,900 5
7
10
LSB-60
Ni Eb Zn C d C M C i A s Ba Cu Ni Eb Za12
U V 40 3
41800 220 9.700 U 450 U U U 20 5
7
10
LSB-62
N i E b Z D C d C M C r A s f i a C u N i E b Z nW 4 70 1.000 150 11.000 // 550 U U U 120 1
2
34
U U 20 34 130 4,100 5
7
10
LSB-64
M i E b Z a C d C M C i A s E a C u M i E b Z n920 52Q 8.900 U 630 U V U 50 \
234
U U 20 61 U 8,800 U 340 U If U U 5
1
10
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
*.Ui
s.o
o
to
&
Depth
12345710
2345710
12345710
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
LSB-65
Italicized Font • samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals; passed if not shaded.
LSB-66 DepthC d C H C r i s E a C u N i E b Z n C d C N & A s B a
8JQQ 220 9.300 U 290 U U U 10
170 U 1 1 .000 1 ,200 230 13,000
LSB-67 LSB-68 (B)C d C N C t A s f i a C u M i E b Z n C d C N Q A s H a
2.QQQ 8.10 8,700 U 1.300 U U •'">•'; fe^; 60 280 U 1 1,000 3,700 59.000
240 U 6,100 64 U 12.000 4.000 50,000
43 140 8,700 U $90 V U U U 66 U 9, 100
LSB-69 (B) LSB-70 (B)Cd CN Ci As Ik QJ Ni Eb Zn Cd CN Ci As &a
280 U 6,000 2,600 48,000 8,100 7.100 19,000 40.000 200 U 7,000 2.800 49,000
41 U 5,200 2,100 27,000 6,400 6,300 6.100 26,000220 U 11.000 2,600 *fa'$to
39 150 8.300
LSB-71 (B) LSB-72 (B)Cd CN Cr As Ba Cii N i E b Z n Cd CN Ci As Ba
190 210 12.000 3,800^:.''*f89,(KiO82 U 7,400 2,700 48,000 7,400 9,400 1 1 ,000 34.00070 U 15,000 5,600 59,000 16.000 20,000 15,000 •'''"• *$j$!fy . 35 350 11,000 4.100 30,000
Cu Hi Eb Zo12345710
£11 Ni Eb Zn11.000 11.000 20.000' -M.Oflb 1
213.000 13.000 7,800 40.000 3
45710
Cu Ni Eb Zn8,000 8.400 15.000 36,000 1
23
8.100 13.000 8,300 40.000 45710
£u Ni ED Znl
8.800 14.000 17.000'. ;!36,Qi60 23
13.000 13,000 9.000 43.000 45710
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
£5
o>
i.o
Depth
12345710
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
LSB-73Cd
100
210
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals; passed if not shaded.
LSB-74CM Ci As
i/'",r'*T:2'
150 16,000
U 8.800
Ba890
360
CuU
MiV\
Eb Zn100
CdU.
330
250
CNU.
210
U
atf!
13,000
8,500
AS Ba•'':$2t 530
U I.4OO
£uU
Mii / i
Znso
70
Depth
2345710
KJ120
110
LSB-75 LSB-76
Cd460
CN220
Ci9,400 M{
As.'*«•*
Da*W
CuU
HiU
£bU
ZnM
Cd370
CH320
Q8.400 |V
.. Al- Ba500
CuU
HiU
Eb(/
Zn40
U 17,000
U 6.500
490 10 U 480
2345710
t.SK-77 1 -SB-78Cd
740CN370
Ci11,000
As Ba380
CuU
MiU
EbU
USO
Cd240
CN140
Ci9,300
As Ba490
CuU
HiU
Eb(/
ZL40
360 20 U 810 30
12345710
LSB-79 1 -SB-80
Cd3.800
CM4QQ
Ci12,000
AsU 550
450
Cu[/
Niu
Eb(/
ZuJO
Cd540
CM200
Ci9,200
As Bai'f'i 520
U 750
CuU
Mi£/
EbU
ZnU
20
234
5710
TABLE 2-2Summary or Soil Sampling Results from Lagoon Investigation
£>L/l
aoUi
Pepth__
12345710
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria.
Underlined parameters were leached; passed if not shaded.
LSB-81
Cd170
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria
Underlined parameters were analyzed for total metals; passed if not shaded.
LSB-82
CMU
Ci8,100
AsU
Ba560
CuU
MiU
EbU
Zn30
C d C N C i A s Ba
0-3 U U 3,700 1.400
Cu
10
Ni Eb
7,200
Zn
60
Depth
345710
NJ
234
57
910
LSB-83 LSB-84
C d C N C r A s B a C i i N i E b Z n C d C M C i A s B a C u N i E b
U U U 3,800 770 /O [/ 10,000 40U U U 3,900 770 U U 11,000
Zn
70
123457910
12
3457
10
LSB-85 LSB-86
Cd CM Ci As Ea £u Mi Eb Zn Cd290
CM54J3
Ci7,000
Asu
Qa630
Cu(/
Miu
Eb(;
Zn50
U 1,900 J20 7,800
260 40
12345710
345710
LSB-87 L.SB-8Cd
200CM4JQ
Ci8.600
Asa
Ba400
CU til Eb ZD20
£43.000
CMZ5Q
Ci9.600
AsU
BJI670
Cu(/
MiU
Ebw
Za20
250 30 490
TABLE 2-2Summary of Soil Sampling Results from Lagoon Investigation
Regular Font - samples analyzed initially for total metals. Reported as ug/kg.Shaded values are above Type A criteria,
Underlined parameters were leached; passed if not shaded.
Italicized Font - samples analyzed initially for SPLP. Reported as ug/l.Shaded values are above Type B criteria.
Underlined parameters were analyzed for total metals: passed tf not shaded.
8.OtyiOJO
Depth
2345710
LSB-89 LSB-90Cd
440CM5J5Q
CL8,300
AsU
fiaA/00
Cu.t/
Zn Cd CN Cr Di Mi
6.QQO /, 200 13,000
Depth
2345710
LSB-91 LSB-92
NJ
12
345710
f l a C i i N i E b
4,200 350 U U 14,000
Z n C d C K C r A s
U U U 2,300
Cu Hi Eb
U U 8,900
2345710
LSB-93
1
23456710
Cd CM C i A s B a C u N i B
[/ 4,400 940 6.700
Zn
/O
MDNR Criteria: Cd-CN-Cr-As-Ba-Cu-N i -Pb-Zn-
Soil Type A1,200 ug/kg
390 tig/kg18,000 ug/kg5,800 ug/kg
75,000 ug/kg32.000 ug/kg20,000 ug/kg21,000 ug/kg47,000 ug/kg
SPLP Leachate Type B3.5 ug/lISO ug/l120 ug/l
0.02 ug/l2,400 ug/l1,300 ug/l
530 ug/l4 ug/l
2,300 ug/l
Note: The blank spaces indicate that a sample was either collectedand analyzed, or not collected. Analytical results for thesoil samples submitted for laboratory analysis are shownin this table.
>Tl
SYLVAN ST
CECIL ST.
K1Y
o>
roOo
NOR
ELECTRO-VOICE, INC.BUCHANAN, MICHIGAN
PHASE I RDADDITIONAL STUDIES REPORT
fishbeck, thompson, carr & huberengineers • scientists • architects
Ada • LansingMichigan
INITIAL! ESTIMATED EXTENTOR IMF ACTED SOILS(FEBRLARY 1994)
PROPERTY BOUNDARY
LEGEND# INVESTIGATIVE SOIL SAMPLE LOCATION(S> BACKGROUND SOIL SAMPLE LOCATION
SOIL SAMPLING MAP
SUBMIT SAMPLE FORANALYSIS OF INDICATOR
ANALYTES
Compare toBackground and Type
A Default Levels
CONTAMINATED SAMPLE
LAGOON AREA SOIL ANALYSIS
DECISION FLOWCHART
Analyze for Metals ofConcern
Bolow Background orTyp« A Default Lovub
7
CONTAMINATED SAMPLE
CLEANSAMPLE
CLEANSAMPLE
CLEANSAMPLE
CLEANSAMPLE
O J3(/] ""rt
.So «
43W
• iHM-H
-91Q
O
-oo563
ilUJ_jLd
OO.Ulo:
Q (/)ct: uj_ Q
3UJ (—oo tn
otro
PROJECT NO,
93307D
2-3
ro ELECTRO-VOICE, INC.BUCHANAN, MICHIGAN
PHASE I RDADDITIONAL STUDIES REPORT
ftoh fishbeck, thompson, carr & huberengineers • scientists • architects
Ada • LansingMichigan
3.0 DISCUSSION AND CONCLUSIONS
3.1 Lower Aquifer Investigation
The investigation determined that a lower aquifer, or water-bearing zone, was not present at the site basedon the boring located near MW-9D. At a depth of 92 feet bgl, a hard reddish-brown strata, the top of
the underlying bedrock shale, was encountered. The boring was abandoned and grouted followingdiscussions with and approval by the U.S. EPA. No further investigation of the lower aquifer was
conducted.
3.2 Lagoon Area Soils - Extent of Contamination Investigation
The lateral and vertical extent of contamination, based on the soil sampling results, is shown in Figure2-4. The extent of the lagoon cap, excavation areas, and the excavation cross sections are detailed in the
Basis of Design for Electro-Voice, Inc., prepared by FTC&H and dated February 1995.
The horizontal distribution of metals in the soil coincide with the natural drainage pattern or slope of theland. It appears that contaminants migrated with runoff from the lagoon area and flowed downslope(west-northwest) to the elevationally lowest area. Lateral migration of contaminants appears to berestricted by the natural drainage pattern or sidewalls of the drainage pathway.
Generally, the lateral extent or perimeter of contamination (outside of the area to be capped) was defined
by the 0- to 1-foot bgl interval meeting the appropriate cleanup criteria. It was observed that if the topsoils were clean, the underlying soil layers were also clean. This observation was supported by a numberof locations, including LSB-3, LSB-10, LSB-11, LSB-16, and LSB-26. In addition, a number of
locations had a top soil sample with elevated metal/cyanide concentrations and a lower sample(s) withmetal/cyanide concentrations which met the relevant cleanup criteria. Examples include LSB-6, LSB-17,
and LSB-20.
The reason for this pattern appears to be the contaminants' mode of transport. It appears that the lagoonareas are generally the source of the elevated metal/cyanide concentrations and that these contaminants
are transported by surface water runoff from the lagoons. This would generally produce the highestlevels of contamination in the surface layer(s) of soil, and contaminant concentrations would be expected
to decrease with depth because of the affinity of metals to bind to soil. This distribution of contaminants
04/14/95 (Revised 05/30/95) - 2 8 - P i
iron
is observed in the area influenced by surface runoff, wherein Type A Default levels are exceeded in the0- to 1-foot bgl interval, but met at lower intervals in the soil horizon.
Relatively high levels of metal/cyanide contamination were concentrated along the axis of the drainage
pathway. These elevated metal/cyanide concentrations extended to depths of 15 feet or more. The soils
in the area of borings LSB-5, LSB-8, and LSB-13 will be excavated to the groundwater surface and theexcavated soils will be placed under the lagoon cap.
Two anomalous areas with slightly elevated lead and arsenic concentrations in the surface soils (0- to 1-foot bgl) were identified, one at the south end of the site and the other at the northwest end of the site.At the south end of the site, soil sampling locations LSB-67 and LSB-89 had elevated lead concentrationsin the 0- to 1-foot bgl interval, as determined by both the total metal and SPLP analyses. These two soil
sampling locations are topographically upgradient of the lagoons and the drainage pathway. Therefore,the lagoons are not believed to be the source of the elevated lead concentrations. However, both pointslie in a drainage pathway which leads from the adjacent road (Carrol! Street) and other offsite property.Therefore, it appears that the source of the elevated lead concentrations may be road runoff from thenearby street or runoff from the areas.
Several soil sampling locations in the northwest corner of the site had slightly elevated lead or arsenic
concentrations in the 0- to 1-foot bgl interval. Samples from locations LSB-7, LSB-73, and LSB-74 had
lead concentrations above the relevant cleanup criteria, as determined by total lead and SPLP analyses.Samples from locations LSB-4, LSB-75, LSB-76, LSB-78, and LSB-80 had arsenic concentrations abovethe relevant cleanup criteria, as determined by total arsenic and SPLP analyses.
The source of contamination in the soil samples from these anomalous areas, however, does not appearto be the lagoons. These soil samples were obtained near the low area which receives and collects surfacewater runoff from nonsite areas such as roads and backyards, in addition to surface water runoff from
the lagoons. These soil sampling locations are also the furthest from the lagoon area. Therefore,elevated arsenic and lead concentrations in the drainage pathway soils between the lagoon and the low
area would be expected if these contaminants were transported by surface water runoff from the lagoonarea. However, this distribution of arsenic and lead is not observed. For example, the highest arsenic
concentrations were detected at locations LSB-75, LSB-76, LSB-78, and LSB-80. However, the highestconcentrations of the indicator metals or contaminants of concern were not detected at these locations.Cadmium, cyanide, and chromium concentrations above the cleanup levels were detected at locations
04/14/95 (Revised 05/30/95) - 29 -
LSB-5, LSB-8, and LSB-13 in the drainage pathway. However, arsenic concentrations at these same
locations were below the cleanup levels. Concentrations of all the indicator and contaminants of concern,
except arsenic, in the surface (0- to 1-foot bgl) sample at location LSB-20 were above the cleanup levels.Lastly, all of the indicator and contaminants of concern, except arsenic and barium, were detected at
concentrations above the cleanup levels at locations LSB-32 and LSB-51. These latter two locations are
in the former lagoon area which will be capped. Similarly, the distribution of lead does not fit the
distribution pattern of the other contaminants.
Furthermore, some of the soil sampling locations with elevated arsenic or lead concentrations are
topographically higher than the low area (approximately 3 to 5 feet higher). It is unlikely that runoff
from the lagoons would flow to these higher areas, or that water would pond to a sufficient depth in the
low area to reach these elevations. The soils in this area are permeable and no signs of such ponding
were noted in the low area. It is believed, based on the above, that the arsenic and lead contaminants
of concern are coming from an upgradient offsite source, and flowing downhill by surface water runoff
to the same lowland area in which runoff water from the lagoons collects.
3.3 Summary of Remediation Activities
The purpose of this section is to summarize the remediation activities in the area of and downgradient
of the lagoons. Greater detail and engineering drawings are provided in the Basis of Design Report for
Electro-Voice, Inc., prepared by FTC&H and dated February 1995.
The remediation activities include excavation of contaminated soils and capping of contaminated soils
(Figure 3-1). Contaminated soils downgradient of the cap will be excavated and placed in the area to be
capped. Locations LSB-5, LSB-8, and LSB-13 will be excavated to the groundwater surface. Other soil
locations will be excavated to depths as indicated in the Basis of Design report.
The cap will extend from LSB-25 west to LSB-19, turn south to LSB-58, and angle southeast from LSB-
58 along LSB-62, and LSB-65 to LSB-67. At LSB-67, the cap will extend east to the top of the bank
and will follow the edge of the bank north to LSB-25 (Figure 3-1).
04/14/95 (Revised 05/30/95) - 30 -
SDMS ADMINISTRATIVE RECORDIMAGERY INSERT FORM
SITE NAME
DOC ID #DESCRIPTION
OF ITEM(S)REASON WHY
UNSCANNABLEDATE OFITEM(S)
NO. OF ITEMSPHASE
O.U.LOCATION
ELECTROVOICE INC91460
MAP
X ILLEGIBLE or FORMATOVERSIZED
NONE
1X Remedial Removal Deletion Docket
Volume 1 of 2Original X Update # 7
Box# 3 Folder # 1
COMMENTS
4.0 REFERENCES
FTC&H, Electro-Voice, Buchanan, Michigan, Remedial Investigation/Feasibility Study Work Plans, Ada,Michigan, July 1988.
FTC&H, Phase II - Field Dam, Volume I of III, Electro-Voice RI/FS Buchanan, Michigan, Ada,Michigan, December 1989.
FTC&H, Final Remedial Investigation Report for Electro-Voice, Inc. Buchanan, Michigan, Ada,Michigan, August 1990.
FTC&H, Electro-Voice, Inc. Groundwater Monitoring Plan for U.S. Environmental Protection Agency,Ada, Michigan, November 1992.
FTC&H, Final Phase I Remedial Design Work Plan for Electro-Voice, Inc., Buchanan, Michigan, Ada,Michigan, February 1994.
FTC&H, Basis of Design Report for Electro-Voice, Inc., Buchanan, Michigan, Ada, Michigan, February1995.
U.S. Environmental Protection Agency, Declaration for the Record of Decision, June 23, 1992.
U.S. Environmental Protection Agency, Consent Decree for the Electro-Voice Superfund Site,September 20, 1993.
Western Michigan University, Hydrogeologic Atlas of Michigan, Western Michigan University,
Department of Geology, Kalamazoo, Michigan, in conjunction with the U.S. Environmental Protection
Agency, Underground Injection Control Program, 35 Plates, 1981.
04/14/95 - 31 -
APPENDIX 2-A
SOIL BORING LOG FOR LOWER AQUIFER INVESTIGATION
ftohfishbeck, thompaoru carr & huber
engineers • scientists • architectsAda • Lansing
Project Name: Electro-Voice/Phase I RD Aquifer InvestigationSite Location: Buchanan. Michigan__________________Contractor: Stearns Drilling Comnanv__________Rig Type: CME 950_____________________
LAB-Iof
Boring/Well No:.Page: 1___ ____Start Date: May 11. 1994Finish Date:.Project No.:_
Mav 12. 1994F93307B
Borehole Diameter 11-12"Casing: Diameter! —
I n t e r v a l : - -
Screen:
Total Length Installed:.Material: _____Diameter: _____Interval: ______
Slot Size:^_ gged bv: Matthew A. Baltusis - FTC&HGeophysical Logs: ____________Development Method: _________Notes: Adjacent to MW-9S and MW-9D.
Driller/Helper: Jim/Dennis/RichDrilling Method: Hollow-stem augerTotal Depth Drilled:_J&lGravel Pack: Type:_
Seal:
Grout:
TOC Elevation:Ground Elevation:.
Interval*:.Type: -Interval*:,
Interval*:.
Static Water Level: —Static Water Level: --
Date:.Date:.Date:.Date-
SampleTypeand
NumberRec.(ft)
Blowsper 6"
Depth
_ 3-89' See well log MW-9D for lilhologic description.Sample Description/Comments
ScreeningResults
InstrumentUsed
20_
30_
kDepth below ground level'"Legend: SS = Split Spoon; ST = Shelby Tube/Pocket Penetrometer; SL — Sectional Liner; N = Standard Penetration Resistance
frohfishbeck, thompson, carr & huber
engineers * scientists • architectsAda • Lanslng
Project Name: Electro-Voice/Phase I RD Aquifer Investigation
Boring/Well No:.Page:_2_____
LAB-1of
Start Date: Mav 11. 1994Finish Date:.Project No.:_
Mav 12. 1994F93307B
SampleTypeand
Number
SS
SS
Rec.(ftl
1.1
<0.1
Blowaper 6"
13291216
200 for0.5"
Depth(bgl)*
40
50
60
70
80
90
—
-
-
-
-_
_
_
Sample Description/Comments
*
SO-65' CLAY per drilling characteristics.
'ILL at 85' per drilling characteristics.
8*89' Drilling pressure increased.9-91':0.9' of GRAVEL (50-70%), fine, subrounded; SAND (30-40%), fine to medium.0.2' of SILT (<70%); CLAY (>3056); moist, medium brown-red, stiff.subrounded to rounded; wet, light gray, poorly sorted. "Slough" from above.
IEDROCK at 92' consisting of SHALE, very weathered, moderateiy stiff, medium red-rown matrix with fragments of mon; competent SHALE.
End of boring at 92'.
ScreeningResult!
InstrumentUsed
*Depth below ground level"'Legend: SS = Split Spoon; ST - Shelby Tube/Pocket Penetrometer; SL = Sectional Liner; N = Standard Penetration Resistance
APPENDIX 2-B
FTC&H FIELD STANDARD OPERATING PROCEDURES
FISHBECK, THOMPSON CARR & HUBER, INC.STANDARD OPERATING PROCEDURE
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 1 of 1 1Version 2.0Date: 4/7/94
Scope: The following SOP is to be used as a guideline when recording activities on any jobsiteoutside of the FTC&H offices. The primary purpose of recording data in the fieldnotebook and on the field data sheets is to create a record by which anyone canreconstruct the field activity without reliance on the recorder's memory. The fieldnotebook and field data sheets will become part of the final evidence file.
Equipment: Field Notebook for Site ActivityCalculatorWaterproof Ink PenWatch (for time of day)Field Data Sheets
Procedure:
1. All information pertinent to the field activity or sampling event must be recorded in a fieldnotebook on field data sheets using the waterproof ink pen. If the ink pen does not function atthe time of entry, note the malfunction as reason for using some other method (i.e., pencil, etc.).At a minimum, entries in the field notes must include the following:
a. Date.b. Time of each entry (24-hour clock).c. FTC&H personnel on jobsite.d. Objective/purpose for activity.e. Name, address and telephone number of field contact.f. References, such as maps or photographs of the study site.g. Field observations.h. Weather conditions, if known, or estimate.i. Describe any field methods to be used for the site activities, reference additional SOPs, if
possible.j. Personnel and equipment decontamination procedures,k. Signatures of personnel responsible for observations.
2. For sampling efforts, specific details for each sample will be recorded on designated field datasheets within the field notebook. However, in addition to the items listed above, the followinginformation will be included in the field notes portion of the notebook.
a. Type and number of samples to be collected.b. Sample location and identification number.c. Sampling method (reference SOP numbers) particularly deviations from the work plan or the
SOP listed.d. Page number reference for sample documentation sheet,e. Sample handling, packaging, labeling and shipping information, including destination.
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3~1Page 2 of 1 1Version 2.0Date: 4/7/94
3. The field notes portion of the notebook should be completed in a sequential, chronological order.No blank pages should be found within the daily notes section of the notebook. Data changesor errors within the field notebook should be corrected by placing a single line through the data,followed by the recorders initials, followed by the correction.
4. The field notebook should be kept in a secure place during the field activities (i.e. in hand,within visual site, locked in field vehicle, etc,). Upon completion of the activity, the fieldnotebook should be checked for completeness. A copy of the completed notebook will then bemade. The copy of the notebook will be stored as part of the FTC&H project files. The originalfield notebook will become part of the final evidence file.
5. Specific examples of the field data sheets forms are as follows:
a. Field Notes (Page 3)b. Groundwater Sample Documentation (Page 4)c. Soil Boring Forms (Page 5)d. Soil Sample Documentation (Page 6)e. Surface Water Sample Documentation (Page 7)f. Sediment Sample Documentation (Page 8)g. Hydraulic Conductivity Test Data (Page 9)h. Step-Drawdown Test Data (Page 10)i. Aquifer Test - Pumping Well (Page 11)
froh
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 3 of 11Version 2.0Date: 4/7/94
FIELD NOTES
Project Name:_
Project No.:
Project Site Location:, Date:
frc>h
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP #F3-1Page 4 of 1 1Version 2.0Date: 4/7/94
Site:
GROUNDWATER SAMPLE DOCUMENTATION
Proj-^i No.:_ Date:Sampling Station:Weather Conditions:Physical Location:Static Water Level:Method: Wet Tape
I.D. Numbers:
Electric Tape Drop Buzzer
Arrival Time:
Lock Key No.;Total Depth:
Other:Physical Condition of Well:__Pump Decon Time/Procedure: _Purging Data:
Bailer/Pump Type and Suiting:.Calculation of one well volume: V =* 0.17 rl v = ________r = radius of well in inches Three well volumes1 = column of water in Feel Purge Rate:
Presampling Data: Initial Purge Water Description:Clock Time Total Volume Purged
________ Start Purging
0.17 (
gallons
Snecirlc Conductance % Difference of Conductivity
Begin Sampling:__________Final Sample Water Description:Field Filtration Method, if used:Field Parameter Measurements:
pH (S.U.):____________Turbidity: ____________
Finish Sampling:
Temperature (°C):Eh:
Specific Conductance (/tmhos/cm):Dissolved Oxygen:_______
Sample Containers:Time of Measurements:
Bottle Tvml
"mlmi
"mi
Glass or PlusCicClass or PlasticGlass or PlasticGlass or Plastic
Filtered PreservativeY«s or No None, HN03. NaOH, H2S04
Yes or No None, HN03, NaOH. H,SO4
Yes or No None, HN03, NaOH, H2SO4
Yes or No None, HNO^, NaOH, H,S04
Reference numbers for any serialized documents on which the sample(s) is listed (sample labels, air bill numbers,chain-of-custody, etc.):_____________________________________________________
Any Deviation from Plan/Notes:
Sample Personnel:Name
froh
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 5 of 11Version 2.0Date: 4/7/94
fef
fohbcck. thompson, cacr & HUKT
Ad* • Li mint
Project Name:,Site Location:,,Contractor__Rig Type:___Borehole Diameter___Casing: Diameter.
Interval:_
Screen:
Total Length Installed:.Material:________Diameter________Interval'_________Material:________Slot Size:________
Logged by:______Geophysical Logs:__Development Method:.Notes:__________
Boring/Well No:_Page:_______ of.Start Date:______Finish Date:_____Project No.:_____
Driller/Helper___Drilling Method:__Total Depth Drilled:.Gravel Pack: Type:.
Seal:
Grout
Interval*:.Type:——Interval*:.Type:___Interval*'
TOC Elevation:__Ground Elevation:,.Static Water Level:,Static Water Level:.
Date:.Date:.Date:.Date:.
Sampl*Typ«ud
NumberR.C.(ft)
Blovip«r 8"
D«pthSample D«teription/Commenti
ScrMdinjRuuJU
Initrumtnt
'Depth b«lo» [round Itvoi"L«c«nd: 33 = Split Spoon; ST s Sh«lby Tub./Poek« P«n*tn>m*lir; 3L = 3«tion»l LLnir; N = Sl»nd»rd P.n.tntion
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 6 of 11Version 2.0Date: 4/7/94
SOIL SAMPLE DOCUMENTATION
Site:
Sampling Station:_
Date: _____ Time:Weather Conditions:
Sample Identification Number:.
Physical Location:________
Sampling Equipment and Procedures, if deviation from plan:
Sample Description (Type, Quantity, Appearance, Analysis Performed):
Sample Containers:
___ 500 ml Amber glass, with no preservation___ 1,000 ml Plastic, with HNOs___ 250 ml Plastic, with no preservation
___ 40 ml Glass vials, with no preservation
Field Compositing Method, if deviation from plan:_
Decontamination Procedures, if deviation from plan:
Reference numbers for any serialized document!) on which the sample(s) is listed
(sample labels, air bill numbers, chain-of-custody, etc.):
Photographic Information:
Notes:
Sample Personnel:Name: Signatures:
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 7 of 11Version 2.0Date: 4/7/94
SURFACE WATER SAMPLE DOCUMENTATION
Sampling Slarinn:
Date: Time:
Sample Identification Number:
Physical Location:
Sampling Equipment and Procedure!
Weather Conditions:
. if deviation from plan:
Sample Description (Type. Quantity, Appearance, Analysis Performed):
Sample Containers:__ 1,000 ml Plastic, with no preservation__ 1,000 ml Plastic, with Ultrex__ 1.000 ml Plastic, with HjSO.__ 500 ml Plastic, with NaOH
__ 500 ml Amber glass, with HjSO,__ 40 ml Glass vials, with no preservation__ 1.000 ml Amber glass, with no preservations__ 1,000 ml glass, with HjSO,
Field Filtration Method, if used:
Decontamination Procedures, if deviation from plan:_
Reference number? for any serialized document* on which the uinplefs) is luted (sample labels, air bill numbers, chain-of-cusiody, eta);
Photographic Information:_______
Final Field Parameters Measurements:
Temperature (*C):______________________Specific Conductance {^mhos/cm):________________
Corrected Specific Conductance 0»tnhos/cm):____..„,-•-_pH (S.U.):_________Time of Measurements:.
Notes:
Sample Personnel:
Signaturea
froh
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 8 of 1 1Version 2.0Date: 4/7/94
SEDIMENT SAMPLE DOCUMENTATION
Site:
Sampling Station:,Date: Time:
Weather Conditions:
Sample Identification Number:,
Physical Location:________Sampling Equipment and Procedures, if deviation from plan:
Sample Description (Type, Quantity, Appearance, Analysis Performed):
Sample Containers:____ 500 ml Amber glass, with no preservation
____ 1,000 ml Plastic, with no preservation____ 250 ml Plastic, with no preservation____ 40 ml Glass vials, with no preeervation
Field Compositing Method, if deviation from plan:_
Decontamination Procedures, if deviation from plan:
Reference numben for any serialized documents on which the sample (a) is listed
(sample labels, air bill numbers, chain-of-custody, etc.):
Photographic Information:
Notes:
Sample Personnel:Name: Signatures:
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 9 of 11Version 2.0Date: 4/7/94
HYDRAULIC CONDUCTIVITY TEST DATA
Site:_______
Sample Station:,Date:_______ Time: Weather Conditions:Sample Identification No.:_ Physical Location:,Equipment and Procedures, if deviation from plan:.
Hermit Data:Unit Serial No.:___________Transducer XD Setting:________
Test Data: Insert Rod
Test No.:__________ Step No,:,Length of Rod Used:__________
Test Data: Remove RodTest No.:__________ Step No.;_
Transducer Scale Factor;feet Reference Setting:
Start Time: End Time:
feet Diameter of Rod Used:
Start Time: . End Time:
Length of Rod Used;, feet Diameter of Rod Used:Decontamination Procedures, if deviation from plan:
inch
inch
Reference numbers of any serialized documents on which the samples) is listed (sample labels, air bill numbers,chain-of-custody, etc.):_________________________________________________________
Photographic Information:
Well Details:Static Water Level:.Screen Material:
_ feet Total Depth:______ feet Total Water Column Length:Slot Size:_____ Screen Length:_____ feet Screen Diameter,
Gravel Pack Material:__Total Aquifer Thickness:,Notes:__________
Gravel Pack Length:. feet Gravel Pack Diameter.
Sample Personnel:Name:
_feetinchinchfeet
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 10 of 11Version 2.0Date: 4/7/94
STEP-DRAWDOWN TEST DATA
Project Name:_
Date:Project Task No.
Elevation of Measuring Points:_
Well No.: Method of Drawdown Measurement:Static Water Level Elevation:
Method of Pumping Rate Measurement:,
Observer:_________________
Remarks/Additional Well Information:
ClockTime
ElapaedTime
PumpingRate fQ) Hold Read DTW Drawdown fs) Q/S
FIELD NOTEBOOK AND FIELD DATA SHEETSSOP#F3-1Page 11 of 11Version 2.0Date: 4/7/94
AQUIFER TEST - PUMPING WELL
Project Name:_
Project No.:__
Well No.:
SWL Measuring Method:.
Pump Setting:_______
Pump Size:__________
Observer (Initials/Name):____________Other Observation Well (I.D. and Distance:.
Project Task No.:.
Date:
Casing Length:__
Casing Diameter:_
TOG Elevation:_
SWL Elevation:_
Ground Elevation:
Remarks: (i.e., discharge location, discharge/recharge boundary locations, etc.)
MinutesClock FromTime Start Hold Read
Drawdownor Pumping
Recovery Rate
FISHBECK, THOMPSON, CARR & HUBER, INC.STANDARD OPERATING PROCEDURE
CHAIN-OF-CUSTODYSOP #F3-2Page 1 of 8Version 1.4Date: 4/7/94
Scope: The following SOP outlines the requirements that provide the ability to trace possessionand handling of samples from time of collection through transportation to the laboratoryfor analysis and final reporting of the data.
Equipment: Sample TagsCustody SealsChain-of-Custody RecordSample-Analysis Request SheetWaterproof Ink Pen
Definition:
Samples are considered to be in a person's custody if they are:
1. In a person's physical possession.2. In view of a person after taking possession.3. Secured by that person so that no one can tamper with it, or secured by that person in an area
that is restricted to authorized personnel.
Procedure:
1. Sample tags are necessary to prevent misidentification of samples. An example of a completedsample tag is included on Page 4. Sample tags should include at least the following information:
a. Project number.b. Name of collector.c. Date and time of collection.d. Sample identification.e. Preservatives used.f. Filtration used.g. Any notes that may affect the analysis.h. Analysis to be completed.
Tags should be securely affixed to sample containers prior to or at the time of collection.
2. All sampling activity will be recorded in two places in the field notes. In the sequential portionof the field notes, the following information will be recorded:
a. Sample location and number.b. Type and number of samples.c. Reference to page number of Sample Documentation Sheet for the particular sample
location.
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CHAIN-OF-CUSTODYSOP #F3-2Page 2 of 8Version 1.4Date: 4/7/94
9.
The second location for recording sampling activity is on the Sample Documentation Sheet.All numbers referencing chain-of-custody documents are also recorded at this location.
Upon completion of sample collection, a chain-of-custody record will be completed and willaccompany the sample-shipment container (cooler) to the laboratory. If more than onesample-shipment container is used, a separate chain-of-custody form should be completedfor each container. An example of a completed chain-of-custody form is included on Page 5.
The chain-of-custody record will include the following information:
a. Client name.b. FTC&H project name and number.c. Sampling site location.d. Sample identification or description.e. Date and time (24-hour clock) of collection.f. Type of sample; i.e., investigative, duplicate, blank, trip blank, etc.g. Signature of collector.h. Signature of persons involved in the chain of possession.
The chain-of-custody form is to be completed with a waterproof ink pen.
The completed Chain-of-Custody Record and a Sample-Analysis Request sheet (referenceSOP #F3-3) will be placed in a waterproof container (zip-lock plastic bag) and placed insidethe sample-shipment container.
Using bubble packing or styrofoam sheets, securely wrap samples and arrange in the shippingcooler in such a way as to minimize the chance for breakage during shipment. Place a layerof blue ice packs over the samples and wrap cooler securely with strapping tape if shipmentby common carrier.
A Chain-of-Custody Seal is used to seal sample-shipment containers which are ready to betransported by means other than the FTC&H sampling team. An example of a completedChain-of-Custody Seal is included on Page 6. The seals should contain the followinginformation:
a. Project name.b. Project number.c. Date sealed.d. Signature of sampler who last relinquished samples.
The seal is to be completed with a waterproof ink pen.
Samples should be delivered to the laboratory for analysis as soon as possible. The samplesmust be delivered to the person in the laboratory authorized to receive samples (samplecustodian).
CHAIN-OF-CUSTODYSOP #F3-2Page 3 of 8Version 1.4Date: 4/7/94
10. There are three routes through which samples reach the laboratory, including:
a. FTC&H personnel who collected samples delivers them to the analytical laboratorydirectly.
b. FTC&H personnel who collected samples delivers them to the FTC&H offices and asecond FTC&H personnel delivers them to the analytical laboratory.
c. FTC&H personnel delivers samples to a common carrier; i.e., UPS, Federal Express,etc., to be shipped to the analytical laboratory. In this case, the Bill of Lading or airbillpackage tracking number becomes part of the chain-of-custody documentation.
11. The relinquish/received portion of the chain-of-custody form has been included on Page 7,illustrating the described situations. A completed sample Federal Express shipping label isincluded on Page 8, illustrating the portions of the form to be filled out by samplingpersonnel. The areas to be completed by the sampling personnel include sections I, 2, 3, 4,and 5. The airbill package tracking number is found in the upper right hand corner and isto be recorded on the Chain-of-Custody form and Sample Documentation Sheet in the fieldnotebook.
The actual chain-of-custody document contains three separate copies. These will bedistributed as follows:
Pink Copy - kept by FTC&H sampling personnel and retained in the project file.
Yellow Copy - retained by analytical laboratory for their records.
White Copy - returned to FTC&H project personnel with the analysis data package andretained in the project file.
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CHAIN- OF- CUSTOD YSOP #F3-2Page 4 of 8Version 1.4Date: 4/7/94
PROIFHT NO. V°HC
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CHAIN-OF-CUSTODYSOP #F3-2Page 5 of 8Version 1,4Date: 4/7/94
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CHAIN-OF-CUSTODYSOP #F3-2Page 6 of 8Version 1.4Date: 4/7/94
CUSTODY SEAL PROJECT NO. OATC
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SOP #F3-2CHAIN-OF-CUSTODY Page 7 of 8
Version 1.4Date: 4/7/94
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CHAIN-OF-CUSTODYSOP #F3-2Page 8 of 8Version 1.4Date: 4/7/94
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FISHBECK, THOMPSON, CARR & HUBER, INC.STANDARD OPERATING PROCEDURE
SAMPLE ANALYSIS REQUEST SHEETSOP #F3-3Page 1 of 2Version 1.2Date: 12/19/94
Scope: The purpose of this SOP is to provide uniformity in the completion of a SampleAnalysis Request Sheet (Analytical Work Request). The purpose of the Sample AnalysisRequest Sheet is to clearly and accurately apprise the laboratory of all informationpertinent to the analytical work requested.
Procedure:
1. The Sample Analysis Request Sheet (Analytical Work Request) will be filled out as completelyas possible before samples are given to a laboratory for analysis. A copy of this form has beenincluded on Page 2.
2. The following lists the necessary information needed to be completed by either the ProjectManager or the Project Engineer/Scientist:
a. Who is to receive the final laboratory report?b. Who is to receive the invoice?c. Client name.d. Client address.e. Client telephone number, including area code.f. Client contact person.g. Date samples are submitted.h. Date results are needed.i. FTC&H Project number.j. FTC&H Project Manager or Project Engineer/Scientist.k. Analytical parameters requested.1. Initials of person approving request and date.
3. The FTC&H field personnel who actually collect the samples will provide the followinginformation:
a. Name(s) of person collecting sample(s).b. Date of sample collection,c. Time of sample collection if only one sample.d. Sample(s) description identification.
4. The Sample Analysis Request Sheet must include all of'the above listed information beforesamples are brought to the laboratory for analysis. Samples will not be received by FTC&HAnalytical Services without a completed Sample Analysis Request Sheet. The only informationthat will be completed by laboratory personnel is the initials of the person approving the work.
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S-
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A<filrf<;<f;
Request Apprc
Work Approve
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Project Fn£inwr/Sflpntlsl:
ved By:
n* By
Final Report: FTC&II |Client 1
Invoice: I'TC&H |Client 1
———————————————————————
————— 1GENERAL CHEMISTRY PARAMETERS
Acidily ChlorideAlkal ini ty , Bicarbonate COD
1 Alkalinity, Carbonate ColorAlkalinity. Total Cyanide, ABOD Cyanide, FBromide Cyanide, T
METALS Please specify T = Total or D « Dissolved; S
Fluoride N, Nitrite Phosphorus. T Specific Cond.Hardness Oil & Grease Solids, T Specific Grav. IIMBAS pH Solids, TD Sulfate JN. Ammonia Phenols. R Solids. TS Sulfide IN, T.Kjeldahl Phosphorus, D Solids, V TPHN, Nitrate Phosphorus. O Solids, VS TOC |
- Standard Lab DL or A - Act 307 DL
Aluminum Beryllium Chromium, H Gold Manganese PalladiumAntimony Boron Chromium, T Iron Mercury PlatinumArsenic Cadmium Cobalt Lead Molybdenum PotassiumBarium Calcium Copper Magnesium Nickel Selenium
| ORGANIC ANALYSES
EPA 601 Purgeable Halocarbons EPA 624 PurgeablesEPA 602 Purgeable Aromalics EPA 625 BN SVOCsEPA 608 Pesl/PCBs EPA 625 Acid SVOCs
Turbidity
Silver ZincSodium I!ThalliumVanadium ||
MDNR Scan 1 EPA 8010 Purgeable Halocarbons EPA 8240 PurgeablesMDNR Scan 2 EPA 8020 Purgeabte Aromatics EPA 8270 ON SVOCsMDNR Scan 3 EPA 8310 Polynuclear Aromatics EPA 8270 Acid SVOCs |jMDNR Scan 8 EPA 8080 Pest/PCBs |
1 WASTE CHARACTERIZATION ANALYSES Please specify
SPLP/Metals (As Ba Cd Cr+6 Cr Cu HE Pb Se Ag Zn]TCLP/Metals |As Ba Cd Cr+6 Cr Cu Hg Pb Se Ag Zn]ASTM D3987-85/SVOCsEP Tox/Metals [As Ba Cd Cr*6 Cr Cu Hg Pb Se Ag Zn]
1
DL: S = Sld lab DL or A = Act 307 DL
SPLP/VOCs SPLP/SVOCsTCLP/VOCs TCLP/SVOCs
SPLP/CNSPLP/S" ||
ASTM D3987-85/CN ASTM D3987~85/S~ Flash Point ||Cyanide, R EP Tox/SVOCs
Sulfide, RPaint Filler Test
SAM
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FISHBECK, THOMPSON, CARR & HUBER, INCSTANDARD OPERATING PROCEDURE
SOIL SAMPLING BY HAND-AUGER METHODSOP#F6-4.1Page 1 of 2Version J . IDate: 11/16/93
Scope: The following SOP is to be used to acquire soil samples from the surface to a depthof approximately five feet.
Equipment: Closed head 31-inch hand augerClosed head 2{-inch hand augerExtension rods"T" Handles4-foot-long piece of 4-inch inner-diarneter polyvinyl chloride (PVC) pipeClean paper towelingSpray bottle of trisodium phosphate (TSP) solutionSpray bottle of deionized, organic free waterOne large disposable aluminum pan for EACH site to be sampledTongue depressorsAppropriate number and type of sample containers and labels
Procedure:
Remove top layer of litter and debris from area to be sampled. With tip of the 3±-inch auger, startsmall hole in soil. Place auger tip into hole and hold auger steady. As auger moves into soil,slowly and carefully rotate the auger to keep it loose in the borehole. This will allow for easyremoval upon completion of drilling. When auger has reached a depth of 1-foot below groundlevel (bgl), stop turning. Leave auger standing in borehole unti l ready to take sample.
When ready to obtain sample, remove auger. Using a tongue depressor, scrape top 1 to 2 inchesof soil from auger and discard. Collect sample material into a disposable aluminum pan. Mix thesoil matrix completely. Place soil into appropriate sample containers.
Label the sample containers clearly and accurately. Complete chain-of-custody documents andrecord activities in field notebook. Store samples in cooler with ice during sampling andtransportation periods.
Decontaminate equipment between samples by washing with a TSP solution and rinsing withdeionized water. Dry equipment with clean paper towel or allow to air dry before further use.
Following collection of 1 -foot bgl sample, place PVC casing in hole and push down to 1 -foot bgl.Carefully remove any remaining soil cuttings from inside casing to prevent mixing of soils fromdifferent depth intervals.
Place 21-inch auger inside casing and auger to 2 feet bgl. Remove auger from borehole, leavingPVC casing in place. Scrape top 1 to 2 inches and bottom 1 to 2 inches of soil from auger anddiscard. Collect sample as previously described.
SOIL SAMPLING BY HAND-AUGER METHODSOP #F6-4.1Page 2 of 2Version I.IDate: 11/16/93
After sample collection, auger to 2 feet bgl using 3i-inch auger. At 2 feet bgl, remove 3i-inchauger and push PVC casing to depth of 2 feet bgl. Carefully remove any remaining soil cuttingsfrom inside PVC casing. Place 2i--inch auger inside PVC casing and auger to 3 feet bgl. Repeatsoil sample collection by continuing auger/casing process un t i l final depth is reached.
Prepare a boring log record of the soil types and thickness encountered for each location. Thisboring log will be used in the preparation of any reports for the site.
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APPENDIX 2-C
SUMMARY OF SOIL CHARACTERISTICS
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Summary of Soil CharacteristicsElectro- Voice, Inc.
Depth123456789
9.51017
Depth123456789
9.510
11.514
14.517
LSB-1Clayey Sandy SiltClayey SiltClayey SiltClayey SiltClayey Silt
LSB-7Clayey SiltClayey SiltClayey SiltSilty Clay
LSB-2Clayey SiltClayey SiltClayey SiltClayey Silty SandClayey Silty SandClayey Silty SandClayey Sandy GravelClayey Sandy GravelClayey Sandy GravelClayey Sandy GravelSand
LSB-8Clayey SiltClayey SiltClayey SiltSilty ClaySilty ClaySandSandSandSandSandSandGravelly SandSandClaySilty Sand
LSB-3Clayey SiltClayey SiltClayey Silty SandClayey Silty SandSilty Gravelly Sand
LSB-9Clayey SiltClayey SiltClayey Silty SandClayey Silty SandSilty Gravelly SandSilty Gravelly SandGravelly Silty SandGravelly Silty SandGravelly Silty SandGravelly Silty SandGravelly Silty Sand
LSB-4Clayey Silty SandClayey SiltClayey SiltClayey SandClayey Sand
i
LSB-10Clayey SiltSilty ClayGravelly Clayey SandClayey Silty SandClayey Silty Sand
LSB-5Clayey SiltSandy Clayey SiltClayey Gravelly SandClayey Gravelly SandClayey Gravelly SandClayey Gravelly SandClayey Sandy GravelClayey Sandy GravelGravelGravelSandSand
LSB-1 1Sandy SiltSandy SiltSandy SiltSilty SandClayey Gravelly Sand
LSB-6Clayey SiltClayey Silty SandClayey Silty SandClayey Silty SandSilty Sand
r LSB-1 2Clayey Silt^ayey SiltSilty ClaySilty ClayClayey Sand
Summary of Soil CharacteristicsElectro-Voice, Inc.
Depth
123456789
9.510121417
Depth123456789
9.51017
LSB-13Clayey SiltClayey SiltClayey SiltClayey SiltClayey SiltClayey SiltClayey SandClayey SandClayey SandSilty SandSiity SandSandGravelly SandSand
LSB-19SandSandSandSandGravelly Sand
LSB-14
Silty SandSilty SandSilty SandSandy SiltSilty SandSilty SandSilty SandSilty SandSilty SandSilty SandSilty Sand
LSB-20Silty SandClayey Silty SandClayey Silty SandSandSand
LSB-15
SandSandSandSandSand
LSB-21Silty ClaySilty ClaySilty ClaySilty ClaySilty Clay
LSB-16
Silty ClaySandy ClaySandy ClayClayey Gravelly SandClayey Gravelly Sand
LSB-22Silty SandClayey SandClayey SandClayey SandClayey Sand
LSB-17
Silty ClaySilty ClaySilty Sandy ClaySilty Sandy ClayClayey Sand
LSB-23Sandy SiltClayey SandClayey SandClayey SandSandy Clay
LSB-18
Clayey SiltClayey SiltClayey Sandy SiltClayey Sandy SiltClayey Sandy SiltClayey Sandy SiltClayey Sandy SiltClayey Sandy SiltSilty Gravelly SandSilty Gravelly SandSilty Gravely Sand
LSB-24Silty SandClayey SiltClayey SiltClayey SiltSilty Sand
Summary of Soil Characteristics -—Electro-Voice, Inc.
Depth12345678910
11.513.5
15Depth
12
34567891017
LSB-25
Clayey Sandy SiltClayey Sandy SiltSilty SandSilty SandSand and Gravel
LSB-31
Clayey SiltClayey SiltClayey SiltClayey SiltClayey Sandy Silt
LSB-26
Silty ClayGravelly SandGravelly SandGravelly SandGravelly Sand
LSB-32
Silty SandClayey SiltClayey SiltClayey SiltClayey SiltClayey SiltClayey SiltClayey SiltSilty SandSilty Clay
LSB-27
Silty ClaySilty ClayGravelly SandGravelly SandGravelly Sand
LSB-33
Sandy SiltSandy SiltClayey Sandy SiltSandy SiltSandy Silt
LSB-28
Silty Clayey SandSilty Clayey SandSandy Clayey SiltSilty ClaySilty ClaySilty ClaySilty ClayClayey SandClayey SandClayey SandSandSilty ClayClayey Silty Sand
LSB-34
Sandy SiltClayey Sandy SiltClayey SiltSilty ClaySilty Sandy Clay
LSB-29
Sandy Silty ClaySandSandSandSand
LSB-35
Silty Gravelly SandSilty ClaySilty ClaySilty ClaySilty Gravelly Sand
LSB-30
Silty SandSilty SandSilty Gravelly SandSilty Gravelly SandSilty Gravelly Sand
LSB-36
Silty ClayClayey SiltSandy SiltSand and GravelSand and Gravel
Summary of Soil CharacteristicsElectro -Voice, Inc.
Depth
1234567
8910
12.517
Depth
12
34
5
67891017
LSB-37Silty SandSilty SandSilty SandClayey SiltClayey Silt
LSB-43
Silty SandSilty SandSilty SandSilty SandClayey Silty Sand
LSB-38
Clayey SiltClayey SiltClayey Sandy SiltClayey Silty SandClayey Silty SandClayey Silty SandSilty ClaySilty ClaySilty ClayClayey SandSandGravelly Sand
LSB-44
Silty SandSilty SandSilty SandSilty SandSandy Silty Clay
LSB-39
Silty SandSilty SandSilty Gravelly SandSandy GravelSandy Gravel
LSB-45
Clayey SiltClayey Sandy SiltSilty Sand and GravelSandSand
LSB-40
Sandy SiltClayey SiltSilty SandSilty ClaySandy Gravel
LSB-46
Clayey SiltSilty SandClayey SiltSilty SandSilty Sand
LSB-41
Silty Sand and GravelSilty SandSilty SandSilty SandSilty Sand
LSB-47
Clayey Silty SandSilty SandSilty SandyClayey Sandy SiltClayey Sandy Silt
LSB-42
Silty SandSilty SandSilty ClayClayey Silty SandSandy Silt
LSB-48
Silty SandSilty SandSilty SandSilty SandSilty Sand
^^ Summary of Soil Characteristics —Electro-Voice, Inc.
Depth123456789
9.51017
Depth
123456789
9.51017
LSB-49
SandSandSandSand and GravelSand
LSB-55
Silty SandSilty SandSilty SandSilty SandSandy Silt
LSB-50
Silty ClaySilty ClaySand and GravelSand and GravelSand and Gravel
LSB-56
Silty SandSandSandSandSand
LSB-51
Silty SandSilty SandSilty SandSilty SandSilty Sand
LSB-57
Silty SandSilty SandSilty ClaySilty ClayClayey Silty Sand and Gravel
LSB-52
Silty SandSilty SandSilty SandSilty SandSilty Sand
LSB-58
Silty SandSilty ClaySand and GravelSand and GravelSand
LSB-53
Clayey SiltClayey Sandy SiltSandSandSand and Gravel
LSB-59
Silty SandSilty SandSandy SiltClayey Sandy SiltSilty Sandy Clay
LSB-54
Silty SandSilty SandSilty SandSilty SandSilty SandSandSandGravelGravelSandSand
LSB-60
Silty SandSand and GravelSilty SandSandSilty Sand
Summary of Soil CharacteristicsElectro-Voice, Inc.
Depth
1234
5
6789
9.51017
DepthI234567
89
9.51017
LSB-61
Sandy SiltSilty SandSilty SandSilty SandSilty Sand
LSB-67
Silty SandSilty SandClayey Silty SandSandy Silty ClayClayey Sandy Silt
LSB-62
Clayey Sandy SiltSandSandSandSand
LSB-68
Clayey SiltSilty ClaySilty ClayClayey Silty SandSilty Sand
LSB-63
Silty Gravelly SandSand and GravelSilty Gravelly SandSandy SiltClayey Sandy Silt
LSB-69
Clayey SiltClayey SiltSandSandSilty Clay
LSB-64
Clayey Sandy SiltSilty SandClayey Sandy SiltClayey Sandy SiltSilty Sand
LSB-70
Clayey SiltClayey SiltSilty ClaySilty ClaySilty ClaySilty ClaySilty ClaySilty Sand
LSB-65
Gravelly Silty SandGravelly Silty SandClayey Sandy SiltClayey Sandy SiltSilty Clay
LSB-71Silty SandSilty SandSilty SandClayey SiltClayey Sand
LSB-66
Silty SandSilty SandSilty SandSilty SandClayey Silty Sand
LSB-72
Gravelly Silty SandSilty ClaySilty ClaySilty SandSilty ClayClayey Sand
"^ Summary of Soil Characteristics — 'Electro -Voice, Inc.
Depth
123456789
9.51017
Depth
1234567
891017
LSB-73
Silty SandSandy SiltSandy SiltSandy SiltClayey SiltClayey SiltSilty Gravelly SandSilty Gravelly SandSilty Gravelly SandSilty Gravelly SandSilty Gravelly Sand
LSB-79
Silty SandSilty SandSilty SandSilty SandSilty Sand
LSB-74
Sandy SiltSandy SiltSandy SiltClayey SiltClayey SiltClayey SiltSilty Gravelly SandSilty Gravelly SandSilty Gravelly SandSilty Gravelly Sand
LSB-80
Clayey Silty SandClayey Silty SandClayey Silty SandClayey Sand/GravelClayey Sand/Gravel
LSB-75
Sandy SiltSandy SiltSandy SiltClayey SiltClayey SiltClayey SiltSilty Gravelly SandSilty Gravelly SandSilty Gravelly SandSilty Gravelly SandSilty Gravelly Sand
LSB-81
Silty SandSilty SandSilty SandSilty SandSilty Sand
LSB-76
Clayey Silty SandClayey Silty SandClayey Silty SandSilty SandSilty Sand
LSB-82
DebrisDebrisDebrisDebrisDebrisDebrisSilty Clayey SandSilty Clayey SandSandSand
LSB-77
Silty SandSilty SandSilty SandSilty SandSilty Sand
LSB-83
DebrisDebrisDebrisDebrisDebrisDebrisSandy ClaySilty SandGravelly SandGravel and Sand
LSB-78
Clayey Silty SandClayey Silty SandGravelly SandGravelly SandGravelly Sand
LSB-84
DebrisDebrisDebrisDebrisDebrisDebrisDebrisDebrisSilty Clayey SandSilty Clayey Sand
oto
Summary of Soil CharacteristicsElectro- Voice, Inc.
Depth
12345678910
Depth1234567
8910
LSB-85
DebrisDebrisDebrisSilty Clayey SandSilty Clayey SandSilty SandSilty SandSilty Clayey SandSandSand
LSB-90DebrisDebrisDebrisDebrisSilty SandSilty SandSandSandSandSand
LSB-86
Silty SandSitty SandSilty SandSilty SandSilty Sand
LSB-91DebrisDebrisDebrisDebrisGravelly SandGravelly SandSandSandSandSand
LSB-87
Silty SandSilty SandSilty SandSilty SandSand
LSB-92
DebrisDebrisDebrisDebrisGravelly SandSandSandSandSandSand
LSB-88
Silty SandSilty SandSilty SandSilty SandSilty Sand
LSB-93DebrisDebrisDebrisDebrisDebrisClayey Silty SandSilty SandSilty SandSandGravelly Sand
LSB-89Silty SandSilty SandSilty SandSilty SandSilty Sand
APPENDIX 2-D
LABORATORY ANALYTICAL RESULTS FOR
LAGOON INVESTIGATION SOIL SAMPLES
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-1 (0 - l')I04/27/94F93307C, COC No: 6814
Report Date: 06/24/94Lab Number: 940600306Date Received: 06/08/94Client ID: 60688
003
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
5304.78.5
86.4
ug/kgmg/kging/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-1 (4 - 5')I04/27/94F93307C, COC No: 9366
Report Date: 05/13/94Lab Number: 940400675Date Received: 04/29/94Client ID: 60688
002-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
5100.2512
80.3
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900289Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-1 (4 --5')I04/27/94F93307C, COC No: 6878
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U1.10.01 U0.02 U
1 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-2 (4 - 5') I04/26/94F93307C, COG No: 9117
014
Report Date: 11/02/94Lab Number: 94100467Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.7
Units
s. u.
Electro-Voice Report Date: 05/13/94600 Cecil Street Lab Number: 940400676Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-2 (4 - 5')I04/26/94F93307C, COG No: 9366
'• Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
89000.14 U18
85.6
ug/kgmg/kgmg/kg%
003
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900290Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr.' Ron Graham
Sample ID: SPLP/LSB-2 (4 - 5') I04/26/94F93307C, COC No: 6878
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
Arsenic 1 U ug/1Barium 1.2 ™g/lCopper 0.01 U mg/1Nickel 0.02 U mg/1Lead 1 U ug/1Zinc 0.04 rog/1
00?
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100455Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-2 (4 - 5')I04/26/94F93307C, COC No: 9117
Results reported with "U" flag indicate the parameter was analyzed- for but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
0.7
Units
ug/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-2 (9 - 10')I06/22/94F93307C, COG No: 9101
Report Date: 07/13/94Lab Number: 940601031Date Received: 06/24/94Client ID: 60688
012-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
20000.14 U9.190.9
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-2 (9 - 10')Duplicate06/22/94F93307C, COG No: 9102
Report Date: 07/13/94Lab Number: 940601032Date Received: 06/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
j CadmiumCyanide, T.
i Chromium, T.j Solids, Total
14000.14 U7.0
90.8
ug/kgmg/kgmg/kg
013
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-2 (9 - 10')I06/22/94F93307C, COC No: 6861
Report Date: 07/25/94Lab Number: 940700344Date Received: 07/15/94Client ID: 60688
coz
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
0.9
Units
ug/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-2 (9 - 10') I] 06/22/94> F93307C, COC No: 6861
012.
Report Date: 07/20/94Lab Number: 940700354Date Received: 07/15/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit,
Parameter
I pH
Result
7.5
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-2 (9 - 10')06/22/94F93307C, COC No: 6876
002
Report Date: 10/04/94Lab Number: 940900275Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.620.01 U0.02 U
1 U0.04
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-3 (0 - l')I04/26/94F93307C, COC No: 6814
Report Date: 06/24/94Lab Number: 940600307Date Received: 06/08/94Client ID: 60688
004-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium/ T.Solids, Total
34000.45
1483 .8
ug/kgmg/kgmg/Jcg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-3 (0 - I7)I04/26/94F93307C, COC No: 6861
005
Report Date: 07/25/94Lab Number: 940700345Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
1.0
Units
ug/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-3 (0 - l')I04/26/94F93307C, COC No: 6861
Report Date: 07/20/94Lab Number: 940700355Date Received: 07/15/94Client ID: 60688
013
• Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.0
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-3 (0 - l')I04/26/94F93307C, COC No: 9396
Report Date: 10/28/94Lab Number: 94100247Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U1.4
0.005 U0.01 U0.02 U
5 U0.04
ug/1mg/1mg/1mg/1mg/1ug/1mg/1
004
Electro-Voice Report Date: 05/13/94600 Cecil Street Lab Number: 940400677Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-3 (4 - 5')I04/26/94F93307C, COC No: 9366
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2700.169.0
91.7
ug/kgmg/kgmg/kg
OO'
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-3 (4 - 5') I04/26/94F93307C, COC No: 6878
Report Date: 10/04/94Lab Nuinber: 940900291Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.430.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
005
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600308Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-4 (0 - l')I04/26/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
71000.4618
80.6
ug/kgmg/Jcgmg/kg%
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-4 (0 - l')I04/26/94F93307C, COG No: 6861
Report Date: 07/29/94Lab Number: 940700346Date Received: 07/15/94Client ID: 60688
004
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, Total
0.40.005 U
ug/1mg/1
014
Electro-Voice Report Date: 07/20/94600 Cecil Street Lab Number: 940700356Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-4 (0 - l')I04/26/94F93307C, COC No: 6861
'; Results reported with "U" flag indicate the parameter was analyzed* for but not detected in the sample above the detection limit.
Parameter
pH
Result
7.4
Units
s.u.
003
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100259Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-4 (0 - l')I04/26/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
ArsenicBariumCopperNickelLeadZinc
Result
30.760.01 U0.02 U
30.02
Units
ug/1mg/1mg/1mg/1ug/1mg/1
Attention: Mr, Ron Graham
Sample ID: LSB-4 (0 - 1')I/Soil04/26/94F93307C, COC No: 9414
002-
Electro-Voice600 Cecil StreetBuchanan MI 49107
Report Date: 11/23/94Lab Number: 941100284Date Received: 11/15/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
780081.2
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100383Buchanan MI 49107 Date Received: 10/20/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-4, 4-5'04/26/94F93307C, COC No: 9400
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
550087.2
Electro-Voice Report Date: 05/13/94600 Cecil Street Lab Number: 940400679Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-5 (4 - 5')I04/26/94F93307C, COG No: 9366
_ •• Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
710000.4628
85.8
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-5 (4 - 5') I04/26/94F93307C, COC No: 6878
Report Date: 10/04/94Lab Number: 940900293Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
11.20.020.02 U
10.06
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-5 (6.5 - 7.5')I06/22/94F93307C, COC No: 9101
Report Date: 07/13/94Lab Number: 940601030Date Received: 06/24/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
520000.29
2887
ug/kgmg/kgrag/kg
007
Electro-Voice Report Date: 08/30/94600 Cecil Street Lab Number: 940800079Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-5 (16 - 17')07/26/94F93307C, COG No: 9272
* Results reported with "U11 flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T;Solids, Total
200000.5719
91.7
ug/kgmg/kgmg/kg
Oil
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900284Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-5 (16 - 17')07/26/94F93307C, COC No: 6876
* Results reported with "U" flag- indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.710.01 U0.02 U
1 U0.02
ug/lmg/lmg/1mg/lug/1mg/l
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-6 (0 - l')I04/26/94F93307C, COC No: 6862
Report Date: 08/02/94Lab Number: 940700332Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
150000.58
226.2
82.3
ug/kgmg/kgmg/kgs.u.
007
Electro-Voice Report Date: 05/13/94600 Cecil Street Lab Number: 940400680Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-6 (4 - 5')I04/26/94F93307C, COC No: 9366
, Rssults reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
17000.15 U
1386.1
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-6 (4 - 5')I04/26/94F93307C, COG No: 6811
003
Report Date: 06/24/94Lab Number: 940600341Date Received: 06/09/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
0.2 U
Units
ug/i
007
Report Date: 10/04/94Lab Number: 940900294Date Received: 09/19/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-6 (4 - 5')I04/26/94F93307C, COC No: 6878
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.980.01 U0.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
39000.7822
86.2
ug/kgmg/kgmg/kg
001?
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600309Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-7 (0 - l')I04/26/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-7 (0 - l')l04/26/94F93307C, COG No: 6861
005
Report Date: 07/29/94Lab Number: 940700347Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cyanide, Total
Result
0.005 U
Units
mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-7 (0 - I7)I04/26/94F93307C, COG No: 6861
Report Date: 07/20/94Lab Number: 940700357Date Received: 07/15/94Client ID: 60688
015
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.1
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-7 (0 - I')*04/26/94F93307C, COC No: 9396
Report Date: 10/31/94Lab Number: 94100238Date Received: 10/17/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumChromium, T.CopperNickelLeadZinc
2 U0.450.4 U
0.02 U0.01 U0.02 U19
0.09
ug/1mg/1ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-7 (0 - 1')I/Soil07/28/94F93307C, COC No: 9414
01!
Report Date: 11/30/94Lab Number: 941100293Date Received: 11/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
mg/kgLeadSolids, Total
95065.4
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-7 (4 - 5') I04/26/94F93307C, COG No: 9366
Report Date: 05/13/94Lab Number: 940400681Date Received: 04/29/94Client ID: 60688
• Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
190 U0.15 U12
84.5
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Hr. Ron Graham
Sample ID: SPLP/LSB-7 (4 - 57)I04/26/94F93307C, COC No: 6878
Report Date: 10/04/94Lab Number: 940900295Date Received: 09/19/94Client ID: 60688
* Results reported with "D" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLead2inc
11.00.01 U0.02 U
10.03
ug/1mg/1mg/1mg/1ug/1mg/1
00;
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900301Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-13 (4 - 5') I04/27/94F93307C, COC No: 6879
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.490.01 U0.02 U
1 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
00:,
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-13 (9 - 10')06/22/94F93307C, COG No: 6876
Report Date: 10/04/94Lab Number: 940900278Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.610.01 U0.02 U
1 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-12 (4 - 5') I04/27/94F93307C, COC No: 6811
005
Report Date: 06/24/94Lab Number: 940600343Date Received: 06/09/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumChromium, T.
0.2 U0.02 U
ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-12 (4 - 5')I04/27/94F93307C, COC No: 6878
Report Date: 10/04/94Lab Number: 940900300Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.980.01 U0.02 U
1 U0.04
ug/lmg/lmg/1mg/lug/lmg/l
014
Electro-Voice Report Date: 05/18/94600 Cecil Street Lab Number: 940400687Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-13 (4 - 5')I04/27/94F93307C, COC No: 9367
Results reported with "U" flag indicate the parameter was analyzed-" for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
240001.985
76 .4
ug/kgmg/Jcgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-13 (9 - 10') I06/22/94F93307C, COC No: 9101
Report Date: 07/13/94Lab Number: 940601028Date Received: 06/24/94Client ID: 60688
009
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
120000.66
2087.6
ug/kgmg/kgmg/kg
ooj
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100384Buchanan MI 49107 Date Received: 10/20/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-7, 4-5'04/26/94F93307C, COC No: 9400
Results reported with "U" flag indicate the parameter was analyzed- for but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicSolids, Total
300085.2
ug/kg%
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-8 (4 - 5')I04/26/94F93307C, COG No: 9366
Report Date: 05/13/94Lab Number: 940400682Date Received: 04/29/94Client ID: 60688
009
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result units
CadmiumCyanide, T.Chromium, T.Solids, Total
58000.1557
85.4
ug/kgmg/kgrag/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-8 (4 - 5'}I04/26/94F933Q7C, COC No: 6878
Report Date: 10/04/94Lab Number: 940900296Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U1.2
0.01 U0.02 U
1 U0,03
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-8 (9 - 10') I06/21/94F93307C, COC No: 9101
Report Date: 07/13/94Lab Number: 940601023Date Received: 06/24/94Client ID: 60688
004
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
210000.6828
88.4
ug/kgmg/kgmg/kg
003
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900276Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-8 (9 - 10')06/21/94F93307C, COG No: 6876
* Results reported with "U" flag indicate the parameter was analyzed~ for but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.540.01 U0.02 U
1 U0.05
ug/1rag/1mg/lmg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-8 (16 - 17')07/26/94F93307C, COG No: 9272
Report Date: 08/31/94Lab Number: 940800078Date Received: 08/04/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T,Chromium, T.Solids, Total
250000.259.7
91.2
ug/kgmg/kgmg/kg
012-
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900285Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-8 (16 - 17')07/26/94F93307C, COC No: 6876
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
11.1
0.020.02 U
30.11
ug/1mg/1mg/1mg/1ug/1mg/1
0\0
Electro-Voice Report Date: 05/13/94600 Cecil Street Lab Number: 940400683Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-9 (4 - 5')I04/26/94F93307C, COG No: 9366
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
360000.17
2586.1
ug/kging/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-9 (4 - 5') I04/26/94F93307C, COC No: 6878
oio
Report Date: 10/04/94Lab Number: 940900297Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.590.01 U0.02 U
1 U0.02
ug/1 ,mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 07/13/94600 Cecil Street Lab Number: 940601024Buchanan MI 49107 Date Received: 06/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-9 (9 - 10') I06/21/94F93307C, COG No: 9101
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
18000.14 U11
89.3
ug/kgmg/kgmg/kg
004
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900277Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-9 (9 - 10')06/21/94F93307C, COC No: 6876
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.380.01 U0.02 U
1 U0.03
ug/img/lmg/1mg/lug/1mg/l
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-9 (9 - 10'} I04/26/94F93307C, COG No: 9117
Report Date: 11/03/94Lab Number: 94100456Date Received: 10/24/94Client ID: 60688
003
* Results reported with "U" flag indicate the parameter was analysedfor but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
0.4 U
Units
ug/1
015
Electro-Voice Report Date: 11/02/94600 Cecil Street Lab Number: 94100468Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-9 (9 - 10')I04/26/94F93307C, COG No: 9117
..Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result
6.4
Units
s.u.PH
00'
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600310Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-10 (0 - l')I04/27/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
50000.70
1881.6
ug/kgmg/kgmg/kg
00k
Report Date: 07/25/94Lab Number: 940700348Date Received: 07/15/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-10 (0 - I7)I04/27/94F93307C, COC No: 6861
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
6.5
Units
ug/1
Electro-Voice Report Date: 07/20/94600 Cecil Street Lab Number: 940700358Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-10 (0 - l')I04/27/94F93307C, COG No: 6861
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.5
Units
s .u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-10 (0 - l')I04/27/94F93307C, COC No: 9396
Report Date: 10/31/94Lab Number: 94100244Date Received: 10/17/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedr but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalCopperNickelLeadZinc
2 U1.00.7
0.005 U0.01 U0.02 U
5 U0.03
ug/1mg/1ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 05/13/94600 Cecil Street Lab Number: 940400684Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-10 (4 - 5')I04/27/94F93307C, COC No: 9366
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
4100.15 U11
84.1
ug/kgmg/kgmg/kg
Oil
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-10 (4 - 5')I04/27/94F93307C, COC No: 6878
Report Date: 10/04/94Lab Number: 940900298Date Received: 09/19/94Client ID: 60688
* Results reported with "IT" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.280.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
6000.249.1
84.1
ug/kging/kging/kg
00?
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 9406003X1Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-11 (0 - l')I04/27/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
002-
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100258Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-11 (0 - l')I04/27/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.690.01 U0.02 U
2 U0.05
ug/1mg/1mg/1mg/1ug/1mg/1
014-
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100270Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-11 (0 - l')I04/27/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.2
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-11 (4 - 5')I04/27/94F93307C, COG No: 9366
Report Date: 05/18/94Lab Number: 940400685Date Received: 04/29/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, TSolids, T.
2200.14 U1088
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil streetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-11 (4 - 5') I04/27/94F93307C, COG No: 6878
Report Date: 10/04/94Lab Number: 940900299Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.640.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
007
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700333Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-12 (0 - l')l04/27/94F93307C, COC No: 6862
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
140000.46
277.3
80.9
ug/kgmg/kgmg/kgs.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-12 (4 - 5')I04/27/94F93307C, COG No: 9367
013
Report Date: 05/18/94Lab Number: 940400686Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, T.
17000.15 U22
83.6
ug/kgmg/kgmg/kg
Report Date: 08/30/94Lab Number: 940800077Date Received: 08/04/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-13 (16 - 17')07/26/94F93307C, COG No: 9272
4 * Results reported with "U" flag indicate the parameter was analyzedv for but not detected in the sample above the detection limit.
005
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
28000.8111
85.8
ug/kgmg/kgmg/kg
013
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-13 (16 -17')07/26/94F93307C, COG No: 6876
Report Date: 10/04/94Lab Number: 940900286Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
21.0
0.020.02 U
50.14
ug/1mg/1mg/1mg/1ug/1mg/1
-_J
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-14 (4 - 5') I04/27/94F93307C, COG No: 9367
015
Report Date: 05/18/94Lab Number: 940400688Date Received: 04/29/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedf for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, TSolids, T.
1700.14 U
4390.2
ug/kging/kgmg/kg
oc:
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-14 (4 - 5') I04/27/94F93307C, COC No: 6879
Report Date: 10/06/94Lab Number: 940900302Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U101 U02 U1 U
0.08
ug/1mg/1mg/1mg/1ug/1mg/1
004
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100457Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-14 (4 - 5')I04/27/94F93307C, COC No: 9117
v Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Chromium, T
Result
0.02 U
Units
mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-14 (4 - 5')I04/27/94F93307C, COG No: 9117
Report Date: 11/02/94Lab Number: 94100469Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.4
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-14 (9 - 10'} I06/22/94F93307C, COG No: 9101
Report Date: 07/13/94Lab Number: 940601029Date Received: 06/24/94Client ID: 60688
010
' Results reported with "U" flag indicate the parameter was analyzedbut not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1200.14 U24
90.9
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-14 (9 - 10')06/22/94F93307C, COC No: 6876
Report Date: 10/04/94Lab Number: 940900279Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.350.01 U0.02 U
1 U0.01
ug/lmg/lmg/1mg/lug/lmg/l
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-14 (9 - 10') I04/27/94F93307C, COC No: 9117
Report Date: 11/03/94Lab Number: 94100458Date Received: 10/24/94Client ID: 60688
005
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Chromium, T.
Result
0.02 U
Units
mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-14 (9 - 10')I04/27/94F93307C, COC No: 9117
Report Date: 11/02/94Lab Number: 94100470Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.8
Units
s.u.
009
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600312Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-15 (0 - l')I04/27/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2200.14 U7.2
91.3
ug/kgmg/kgmg/kg
003
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-15 (0 - l')I04/27/94F93307C, COG No: 9197
Report Date: 11/03/94Lab Number: 94100295Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.530.01 U0.02 U
2 U0.03
ug/lmg/1mg/1tng/lug/lmg/1
0<J7
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-15 (0 - l')I04/27/94F93307C, COG No: 9197
Report Date: 10/21/94Lab Number: 94100299Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result* •. •* v* «VB^H •
6.4
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-15 (4 - 5') I04/27/94F93307C, COG No: 9367
Report Date: 05/18/94Lab Number: 940400689Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, T.
68 U0.13 U4.194.1
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-15 (4 - 5')D04/27/94F93307C, COC No: 9367
Report Date: 05/18/94Lab Number: 940400694Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, T.
56 U0.163.6
94.3
ug/kging/kgmg/kg
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
3300.277.3
84.6
ug/kging/kgmg/kg
j_
010
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600313Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-16 (0 - I'}*04/28/94F93307C, COG No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-16 (0 - l')I04/28/94F93307C, COC No: 9397
Report Date: 10/31/94Lab Number: 94100260Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.500.01 U0.02 U
2 U0.01
ug/1mg/1mg/1mg/1ug/1mg/1
Parameter
pH
Result
7.3
Units
s . u .
OH*
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100272Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-16 (0 - l')I04/28/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
017
Electro-Voice Report Date: 05/18/94600 Cecil Street Lab Number: 940400690Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-16 (4 - 5')I04/27/94F93307C, COC No: 9367
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium , T .Solids, T.
1100.14 U8.6
88.3
ug/kgmg/kgmg/kg%
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-16 (4 - 5')I04/28/94F93307C, COC No: 6879
DCf
Report Date: 10/06/94Lab Number: 940900303Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.610.01 U0.02 U
1 U0.01
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-17 (0 - l')I04/28/94F93307C, COC No: 6862
Report Date: 08/02/94Lab Number: 940700334Date Received: 07/15/94Client ID: 60688
002
* Results reported with "IT" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
180001.8397.184.3
ug/kgmg/kgmg/kgs.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-17 (4 - 5') I04/27/94F93307C, COC No: 9367
Report Date: 05/18/94Lab Number: 940400691Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, T.
16000.41
1884.0
ug/kgmg/kgnig/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-17 (4 - 5')I04/28/94F93307C, COC No: 6811
octt
Report Date: 06/24/94Lab Number: 940600342Date Received: 06/09/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cadmium
Result
0.6
Units
ug/1
Report Date: 10/06/94Lab Number: 940900304Date Received: 09/19/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-17 (4 - 5') I04/28/94F93307C, COC No: 6879
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
11.40.01 U0.02 U
20.06
ug/lmg/lmg/lmg/lug/lmg/l
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-17, 4-5'04/26/94F93307C, COC No: 9400
Report Date: 10/31/94Lab Number: 94100385Date Received: 10/20/94Client ID: 60688
oof
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
390086.3
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/17 (4 - 5') I04/28/94F93307C, COC No: 9117
Report Date: 10/31/94Lab Number: 94100460Date Received: 10/24/94Client ID: 60688
007
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cyanide, Total
Result
0.013
Units
mg/1
Electro-Voice Report Date: 11/02/94600 Cecil Street Lab Number: 94100472Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-17 (4 - 5')I04/28/94F93307C, COC No: 9117
,* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
019
Parameter
PH
Result
6.7
Units
s.u.
019.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-18 (4 - 5')I04/27/94F93307C, COG No: 9367
Report Date: 05/3.8/94Lab Number: 940400692Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, TSolids, T.
7900.4341
87.0
ug/kgmg/kgmg/kg
00!*
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900305Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-18 (4 - 5')I04/27/94F93307C, COC No: 6879
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
19401 U
U0.0.0.02 U
1 U0.03
ug/lmg/lrag/1mg/lug/lmg/l
006
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100461Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/18 (4 - 5')I04/27/94F93307C, COG No: 9117
* Results reported with "U" flag indicate the parameter was analyzed .,for but not detected in the sample above the detection limit.
Parameter Result Units
Cyanide, Total 0.005 U mg/1Chromium, T. 0.02 U rog/1
020
Electro-Voice Report Date: 11/02/94600 Cecil Street Lab Number: 94100473Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-18 (4 - 5')I04/27/94F93307C, COC No: 9117
e Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.1
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-18 (9 - 10')I06/22/94F93307C, COC No: 9101
Report Date: 07/13/94Lab Number: 940601027Date Received: 06/24/94Client ID: 60688
00$
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2400.15 U
2185.2
ug/kgmg/kging/kg
001
Electro-Voice Report Date: 10/04/94600 Cecil Street . Lab Number: 940900280Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-18 (9 - 10')06/22/94F93307C, COG No: 6876
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected'in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U1.10.010.02 U
1 U0.07
ug/lmg/lmg/1mg/lug/1mg/l
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-18 (9 - 10')I04/27/94F93307C, COC No: 9117
Report Date: 11/03/94Lab Number: 94100459Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Chromium, T.
Result
0.02 U
Units
rag/1
01$
Electro-Voice Report Date: 11/02/94600 Cecil Street Lab Number: 94100471Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-18 (9 - 10')I04/27/94F93307C, COG No: 9117
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.3
Units
s.u.
on
Report Date: 06/24/94Lab Number: 940600314Date Received: 06/08/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-19 (0 - 1'JI04/27/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide , T .Chromium , T .Solids, Total
1205.06.393.8
ug/kgmg/kgmg/kg%
Electro-Voice Report Date: 05/18/94600 Cecil Street Lab Number: 940400693Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-19 (4 - 5')I04/27/94F93307C, COG No: 9367
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, TSolids, T.
49 U0.13 U5.996.3
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-19 (4 - 5')I04/27/94F93307C, COC No: 9555
Report Date: 01/05/95Lab Number: 941200533Date Received: 12/20/94Client ID: 60688
004
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result units
ArsenicLeadSolids, Total
30005.6
96.0
ug/kgmg/kg
005
Electro-Voice Report Date: 01/04/95600 Cecil Street Lab Number: 941200534Buchanan MI 49107 Date Received: 12/20/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-19 (4 - 5') I04/27/94F93307C, COC No: 9555
^ Results reported with "U11 flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCopperNickelZinc
0.400.01 U0.02 U0.01 U
mg/1mg/1mg/1mg/1
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600315Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-20 (0 - 1'JI05/04/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
12000021160
80.6
ug/kgmg/kgmg/kg
Report Date: 08/10/94Lab Number: 940700370Date Received: 07/19/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-20 (0-1)105/04/94F93307C
•* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
4500781003751410
ug/kgmg/kgmg/kgmg/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-20 (4 - 5')I05/04/94F93307C, COG No: 9370
Report Date: 05/26/94Lab Number: 940500173Date Received: 05/05/94Client ID: 60688
001*.
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
170p.14 U'8.588.8
ug/kgmg/kgmg/kg
002
** Electro-Voice.1 600 Cecil Streetm Buchanan MI 49107
Report Date: 11/18/94Lab Number: 94100479Date Received: 10/24/94Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-20 (4 - 5') I05/04/94F93307C, COG No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.500.01 U0.02 U
2 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-20 (4 - 5') I05/04/94F93307C, COC No: 9221
Report Date: 11/03/94Lab Number: 94100491Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.1
Units
s.u.
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500194Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-21 (4-5)105/04/94F93307C, COG No: 9371
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
39000.2518
71.3
ug/kgmg/kgmg/kg
otf
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-21 (4 - 5') I05/04/94F93307C, COG No: 9221
Report Date: 11/18/94Lab Number: 94100486Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCopperNickelLeadZinc
2 U0.630.4 U
0.01 U0.02 U
2 U0.04
ug/1mg/1ug/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date; 11/03/94600 Cecil Street Lab Number: 94100498Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-21 (4 - 5')I05/04/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.3
Units
s.u.
013
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600316Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-22 (0 - l')I05/04/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
20000.63
1179
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 07/29/94600 Cecil Street Lab Number: 940700349Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-22 (0 - I7)I05/04/94F93307C, COC No: 6861
f Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
007
• Parameter Result
0.005 U
Units
mg/1Cyanide, Total
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-22 (0 - 1'JI05/04/94F93307C, COC No: 6861
017
Report Date:. 07/20/94Lab Number: 940700359Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.8
Units
s.u.
oio
Electro-Voice Report Date: 11/18/94600 Cecil Street Lab Number: 94100487Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-22 (0 - l')I05/04/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCopperNickelLeadZinc
2 U0.600.4 U0.01 U0.02 U
20.02
ug/1mg/1ug/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-22 (0 - l')I05/04/94F93307C, COC No: 9221
Report Date: 11/03/94Lab Number: 94100499Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.3
Units* m V* "•* i
s.u.
009
Electro-Voice Report Date: 05/27/94600 Cecil Street Lab Number: 940500180Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-22 (4 - 5')I05/04/94F93307C, COC No: 9370
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2300.269.185.1
ug/kgmg/kgmg/kg
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids/ Total
24001.314
77.4
ug/kgmg/kgrag/kg
014-
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600317Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-23 (0 - l')I05/05/94F93307C, COC No: 6814
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Electro-Voice Report Date: 11/18/94600 Cecil Street Lab Number: 94100488Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-23 (0 - l')I05/05/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalCopperNickelLeadZinc
2 U0.620.4 U
0.005 U0.01 U0.02 U
50.04
ug/1mg/1ug/img/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr..Ron Graham
Sample ID: LSB-23 (0 - l')I05/05/94F93307C, COC No: 9221
Report Date: 11/03/94Lab Number: 94100500Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.3
Units
s.u.
0!
Electro-Voice Report Date: 05/27/94600 Cecil Street Lab Number: 940500182Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-23 (4 - 5'}I05/05/94F93307C, COC No: 9370
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
650.15 U
1185.9
ug/kgmg/kgmg/kg
Off
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600318Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-24 (0 - 1')*05/05/94F93307C, COC No: 6813
W* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
Cadmium 360 ug/kgCyanide, T. 0.32 mg/kgchromium, T. 8.0 mg/kgSolids, Total 84.7 %
003
Electro-Voice600 Cecil StreetBuchanan MI 49107
Report Date: 11/18/94Lab Number: 94100480Date Received: 10/24/94Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-24 (0 - l')I05/05/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.590.01 U0.02 U
2 U0.06
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-24 (0 - l')I05/05/94F93307C, COC No: 9221
Report Date: 11/03/94Lab Number: 94100492Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.9
Units
s.u.
017
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700343Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60683
Attention: Mr. Ron Graham
Sample ID: LSB-24 (2 - 3')I05/05/94F93307C, COG No: 6863
, * Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
450.15 U145.2
84.7
ug/kgmg/kgmg/kgs.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-24 (4 - 5') I05/05/94^F93307C, COG No: 9370
Report Date: 05/26/94Lab Number: 940500183Date Received: 05/05/94Client ID: 60688
012-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
340.14 U10
87.1
ug/kgmg/kgmg/kg
004
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600319Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-25 (0 - l')I05/05/94F93307C, COC No: 6813
* Results reported with "U11 flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.chromium, T.Solids, Total
1900.2610
85.2
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-25 (0 - l')I05/05/94F93307C, COC No: 9221
Report Date: 11/18/94Lab Number: 94100482Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.710.01 U0.02 U
50.06
ug/1mg/1mg/1mg/1ug/1mg/1
Oil
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-25 (0 - l')I05/05/94F93307C, COC No: 9221
Report Date: 11/03/94Lab Number: 94100494Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.9
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-25 (4 - 5')I05/05/94F93307C, COC No: 9370
Report Date: 05/27/94Lab Number: 940500184Date Received: 05/05/94Client ID: 60688
013
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide,. T.Chromium, T.Solids, Total
1100.14 U6.990.4
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-26 (0 - l')I05/02/94F93307C, COC No: 9397
017
Report Date: 10/20/94Lab Number: 94100273Date Received: 10/17/94Client ID: 60688
* Results reported with "U11 flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.6
Units•- . — —.*»«
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-26 (0 - I7) I05/02/94F93307C, COC No: 9555
Report Date: 12/30/94Lab Number: 941200535Date Received: 12/20/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Cyanide, Total
Result• 4VOV* A»M^«^»^B«B *
0.005 U
Units
mg/1
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600320Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-26 (0 - l')I05/02/94F93307C, COC No: 6813
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
COS
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
7800.4112
79.6
ug/kgmg/kgmg/kg
005
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100261Buchanan MI 49107 ' Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-26 (0 - l')I05/02/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U1.0
0.01 U0.02 U
30.03
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham4I Sample ID: SPLP/LSB-26 (4 - 5') I
05/02/94. F93307C, COC No: 6879
001
Report Date: 10/06/94Lab Number: 940900306Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.570.01 U0.02 U
1 U0.01
ug/lmg/lmg/1mg/lug/lmg/l
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1100.14 U8.3
83.2
ug/kgmg/kgmg/kg
007 '
Electro-Voice Report Date: 05/27/94600 Cecil Street Lab Number: 940500178Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-26 (4 - 5') I05/02/94F93307C, COC No: 9370
* Results reported with "U" flag, indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
E1ectro-Vo ice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-27 (0 - l')I05/02/94F93307C, COG No: 6813
Report Date: 06/24/94Lab Number: 940600321Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result
Cadmiumcyanide, T.Chromium, T.Solids, Total
1900.15 U11
84.8
Units
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-27 (0 - l'05/02/94F93307C
Report Date: 08/10/94Lab Number: 940700369Date Received: 07/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
44005214131750
ug/kgmg/kgmg/kgmg/kgmg/kgmg/kg
01?
Report Date: 10/20/94Lab Number: 94100274Date Received: 10/17/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-27 (0 - l')I05/02/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.1
Units
s.u.
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100262Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688V
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-27 (0 - 1'JI05/02/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.990.01 U0.02 U19
0.14
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-27 (0 - 1') I/Soil04/26/94F93307C, COC No: 9414
Report Date: 11/30/94Lab Number: 941100289Date Received: 11/15/94Client ID: 60688
007
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
LeadSolids, Total
1683.4
mg/kg%
014
Report Date: 08/02/94Lab Number: 940700340Date Received: 07/15/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-27 (2 - 3')I05/02/94F93307C, COG No: 6863
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
1100.14 U7.16.186.5
ug/kgmg/kgmg/kgs.u.%
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-27 (4-5)105/02/94F93307C, COC No: 9371
Report Date: 05/26/94Lab Number: 940500187Date Received: 05/05/94Client ID: 60688
Olfc
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
670.14 U6.8
90.5
ug/kgmg/kgmg/kg
oos
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900307Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-27 (4 - 5') I05/02/94F93307C, COC Ho: 6879
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.640.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
019
Electro-Voice Report Date: 05/27/94600 Cecil Street Lab Number: 940500186Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-28 (4-5)105/02/94F93307C, COC No: 9371
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
38000.6760
77.8
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900308Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-28 (4 - 5')I05/02/94F93307C, COC No: 6879
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U1.3
0.01 U0.02 U
1 U0.04
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-28 (9 - 10') I06/22/94F93307C, COC No: 9101
Report Date: 07/13/94Lab Number: 940601026Date Received: 06/24/94Client ID: 60688
007
•• Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
79000.2620
86.6
ug/kgmg/kgrag/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-28 (9 - 10')06/22/94F93307C, COC No: 6876
Report Date: 10/04/94Lab Number: 940900281Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
21.7
0.020.02 U
30.19
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 08/30/94600 Cecil Street Lab Number: 940800076Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-28 (14 - 15')07/26/94F93307C, COC No: 9272
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
49000.40
1487.8
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900287Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention:. Mr. Ron Graham
Sample ID: SPLP/LSB-28 (14-15')07/26/94F93307C, COC No: 6877
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBarium,CopperNickelLeadZinc
1 U0.470.010.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
009
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100462Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-28 (14 - 15')I05/02/94F93307C, COC No: 9117
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, Total
0.4 U0.006
ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-28 (14 - 15')I05/02/94F93307C, COG No: 9117
Report Date: 11/02/94Lab Number: 94100474Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.1
Units
s .u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-29 (4 - 5') I05/02/94F93307C, COC No: 9370
Report Date: 05/26/94Lab Number: 940500179Date Received: 05/05/94Client ID: 60688
00?
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
33000.5816
91.2
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-29 (4 - 5')D05/02/94F93307C, COG No: 9370
Report Date: 05/27/94Lab Number: 940500181Date Received: 05/05/94Client ID: 60688
010'
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
25000.259.3
89.5
ug/kgmg/kgmg/kg
0\\
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100464Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-29 (4 - 5')I05/02/94F93307C, COC No: 9117
_- Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalCopperNickelLeadZinc
2 U0.471.6
0.005 U0.010.02 U
2 U0.04
ug/1mg/1ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-29 (4 - 5')D05/02/94F933Q7C, COG No: 9118
Report Date: 11/18/94Lab Number: 94100510Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalCopperNickelLeadZinc
1 U0.380.4
0.005 U0.01 U0.02 U
2 U0.02
ug/1mg/1ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 11/02/94600 Cecil Street Lab Number: 94100476Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-29 (4 - 5')I05/02/94F93307C, COG No: 9117
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.6
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-29 (4 - 5')D05/02/94F93307C, COG No: 9118
Report Date: 11/16/94Lab Number: 94100518Date Received: 10/24/94Client ID: 60688
* Results reported with "IT" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.8
Units
s.u.
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500235Buchanan MI 49107 Date Received: 05/06/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-30 (4 - 5') I05/06/94F93307C, COC No: 9369
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2700.14 U4.6
90.8
ug/kgmg/kgmg/kg%
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-30 (4 - 5')I05/06/94F93307C, COC No: 9221
Report Date: 11/18/94Lab Number: 94100483Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.310.01 U0.02 U
2 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-30 (4 - 5') I05/06/94F93307C, COG No: 9221
Report Date: 11/03/94Lab Number: 94100495Date Received: 10/24/94Client ID: 60688
Otf
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.8
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-31 (4-5') I05/06/94F93307C, COC No: 9369
Report Date: 06/01/94Lab Number: 940500236Date Received: 05/06/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
140000.38
7479.2
ug/kging/kgmg/kg
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500231Buchanan MI 49107 Date Received: 05/06/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-32 (4 - 5') I05/05/94F93307C, COC No: 9369
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1670005.5250
77.5
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-32 (4 - 5')I05/05/94F93307C
Report Date: 08/10/94Lab Number: 940700371Date Received: 07/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
220050
- 20066110990
ug/kgmg/kgmg/kgmg/kgmg/kgmg/kg
Electro-Voice Report Date: 07/13/94600 Cecil Street Lab Number: 940601022Buchanan MI 49107 Date Received: 06/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-32 (9 - 10') I06/21/94F93307C, COC No: 9101
* Results reported with "U" flag indicate the parameter was analyzed,. for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
12000.22
6480.1
ug/kgmg/kgmg/kg
or
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-33 (0 - l')I05/05/94F93307C, COC No: 9221
Report Date: 11/18/94Lab Number: 94100489Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalChromium, T.CopperNickelLeadZinc
30.4841
0.0240.100.030.02 U
140.19
ug/1mg/1ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 11/16/94600 Cecil Street Lab Number: 94100501Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-33 (0 - l')I05/05/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
024
Parameter
PH
Result
7.4
Units* _ «•» «» » ^ •
s.u.
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500234Buchanan MI 49107 Date Received: 05/06/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-33 (4-5') I05/05/94F93307C, COG No: 9369
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
23000.2735
84.7
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-34 (4-5') I05/05/94F93307C, COG No: 9369
Report Date: 06/01/94Lab Number: 940500239Date Received: 05/06/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
13000.2730
83.9
ug/kgmg/kgmg/kg
OIC
Electro-Voice Report Date: 07/27/94600 Cecil Street Lab Number: 940700350Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-34 (4 - 5')I05/05/94F93307C, COC No: 6861
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Chromium, T.
Result
0.02 U
Units
mg/1
013
Electro-Voice Report Date: 11/18/94600 Cecil Street Lab Number: 94100490Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-34 (0 - l')I05/05/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalChromium, T.CopperNickelLeadZinc
2 U0.51
190.0580.070.020.02 U
70.14
ug/1mg/1ug/1mg/1mg/1mg/1mg/1ug/1mg/1
r
Electro-Voice Report Date: 11/16/94600 Cecil Street Lab Number: 94100502Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-34 (0 - l')I05/05/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result• ••••••••v**
7.4
units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-34 (4 - 5')I05/05/94F93307C, COG No: 6861
Report Date: 07/20/94Lab Number: 940700360Date Received: 07/15/94Client ID: 60688
018
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.2
Units
s.u.
0
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-35 (0 - l')I05/05/94F93307C, COG No: 6813
Report Date: 06/24/94Lab Number: 940600322Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
4300.14 U6.7
89.2
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 11/18/94600 Cecil Street Lab Number: 94100481Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-35 (0 - l')I05/05/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.450.010.02 U
2 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-35 (0 - l')I05/05/94F93307C, COC No: 9221
Report Date: 11/03/94Lab Number: 94100493Date Received: 10/24/94Client ID: 60688
OlV
* Results reported with "0" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.7
Units
s.u.
004
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500233Buchanan MI 49107 Date Received: 05/06/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-35 (4 - 5') I05/05/94F93307C, COG No: 9369
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
920.1514
83.4
ug/kgmg/kgmg/kg
oo;
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600323Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-36 (0 - l')I05/03/94F93307C, COG No: 6813
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1200.2412
82.7
ug/kgmg/kgmg/kg
00!
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100263Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-36 (0 - I')!05/03/94F93307C, COG No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.530.01 U0.02 U
2 U0.06
ug/1rag/1rag/1ing/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-36 (0 - l')I05/03/94F93307C, COC No: 9397
Report Date: 10/20/94Lab Number: 94100275Date Received: 10/17/94Client ID: 60638
019
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.6
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-36 (4-5)105/03/94F93307C, COG No: 9371
Report Date: 05/27/94Lab Number: 940500189Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
610.14 U6.592.1
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-36 (4 - 5')I05/03/94F93307C, COC No: 6879
Report Date: 10/07/94Lab Number: 940900309Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.610.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 05/27/94600 Cecil Street Lab Number: 940500190Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-37 (4-5)105/03/94F93307C, COC No: 9371
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result
CadmiumCyanide, T.Chromium, T.Solids, Total
950.48
1383.4
Units
ug/kg
ing/kg
0
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-37 (4 - 5')I05/03/94F93307C, COG No: 6879
Report Date: 10/07/94Lab Number: 940900310Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.250.01 U0.02 U
1 U0.02
ug/lmg/1mg/1mg/1ug/lmg/1
013
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100466Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-37 (4 - 5')I05/03/94F93307C, COC No: 9117
^ Results reported with "U" flag indicate the parameter was analyzed^ for but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U0.320.005 U0.01 U0.02 U
2 U0.03
ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-37 (4 - 5')I05/03/94F93307C, COG No: 9117
Report Date: 11/03/94Lab Number: 94100478Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.1
Units
s. u.
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500193Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-38 (4 - 5)105/03/94F93307C, COG No: 9371
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
103000.4131
85.4
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-38 (9 - 10') I06/22/94F93307C, COG No: 9101
Report Date: 07/13/94Lab Number: 940601025Date Received: 06/24/94Client ID: 60688
oot?
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
47000.3415
80.8
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-38 (9 - 10')06/22/94F93307C, COC No: 6876
Report Date: 10/04/94Lab Number: 940900282Date Received: 09/19/94Client ID: 60688
oo<
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
41.6
0.020.02 U
40.13
ug/1mg/1mg/1mg/1ug/1mg/1
003 i
Electro-Voice Report Date: 08/30/94600 Cecil Street Lab Number: 940800075Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-38 (14 - 15')07/25/94F93307C, COC No: 9272
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
22000.7013
89.4
ug/kgmg/kging/kg
015
Electro-Voice Report Date: 10/04/94600 Cecil Street Lab Number: 940900288Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-38 (14 - 15')07/25/94F93307C, COG No: 6877
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.490.01 U0.02 U
1 U0.01 U
ug/lmg/1mg/1mg/1ug/lmg/1
OK)
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-38 (14 - 15')I05/03/94F93307C, COG No: 9117
Report Date: 11/03/94Lab Number: 94100463Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, Total
0.50.005 U
ug/1mg/1
C Electro-Voice Report Date: 11/02/94600 Cecil Street Lab Number: 94100475Buchanan MI 49107 Date Received: 10/24/94
H Client ID: 60688
Attention: Mr. Ron Graham
1^ Sample ID: LSB-38 (14 - 15') I• 05/03/94
F93307C, COC No: 9117
!;* Results reported with "U" flag indicate the parameter was analyzed
< ^ for but not detected in the sample above the detection limit.
Parameter Result Units
pH 7.3 s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-39 (4-5') I05/06/94F93307C, COC No: 9369
Report Date: 06/01/94Lab Number: 940500237Date Received: 05/06/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
4400.288.8
88.2
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 11/18/94600 Cecil Street Lab Number: 94100484Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-39 (4 - 5'} I ;05/06/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.530.01 U0.02 U
30.02
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-39 (4 - 5')I05/06/94F93307C, COG No: 9221
oft
Report Date: 11/03/94Lab Number: 94100496Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.7
Units
s.u.
009
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-40 (4 - 5') I05/06/94F93307C, COG No: 9369
Report Date: 06/01/94Lab Number: 940500238Date Received: 05/06/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
190009.232
92.2
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-41 (4-5')05/06/94F93307C, COC No: 9369
Report Date: 06/01/94Lab Number: 940500232Date Received: 05/06/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
3900.14 U7.6
89.0
ug/kgmg/kgmg/kg
013
Electro-Voice Report Date: 06/02/94600 Cecil Street • Lab Number: 940500307Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-42 (4 - 5') I05/09/94F93307C, COC No: 9373
Results reported with "U" flag indicate the parameter was analyzed^ for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
61001.389
86.1
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-43 (4 - 5')I05/09/94F93307C, COC No: 9373
Report Date: 06/02/94Lab Number: 940500305Date Received: 05/11/94Client ID: 60688
01V-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
19002.5
1285.0
ug/kging/kgmg/kg
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600324Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-44 (0 - l')I05/09/94F93307C, COC No: 6813
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide , T .Chromium, T.Solids, Total
610003.86686
ug/kgmg/kging/kg%
Electro-Voice Report Date: 06/02/94600 Cecil Street Lab Number: 940500309Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-44 (4 - 5') I05/09/94F93307C, COC No: 9374
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
015'
Parameter Result Units
CadmiumCyanide , T .Chromium, T.Solids, Total
810.15 U
1382.2
ug/kgmg/kgmg/kg%
Electro-Vo ice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-45 (0 - l')I05/03/94F93307C, COG No: 6813
Report Date: 06/24/94Lab Number: 940600325Date Received: 06/08/94Client ID: 60688
01C
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
rParameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1100.18
1283.3
ug/kgrag/kgmg/kg
_1_
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-45 (0 - l')I05/03/94F93307C, COC No: 9397
Report Date: 10/31/94Lab Number: 94100264Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.970.010.02
20.04
U
UUU
ug/1mg/lmg/1mg/1ug/1mg/1
010
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100276Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-45 (0 - l')I05/03/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.4
Units
s.u.
on!
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-45 (4 - 5)105/03/94F93307C, COG No: 9371
Report Date: 05/27/94Lab Number: 9405001S8Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1200.14 U
989.9
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-45 (4 - 5')D05/03/94F93307C, COG No: 9370
Report Date: 05/26/94Lab Number: 940500175Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1000.14 U9.289.4
ug/kgmg/kgmg/kg
004
012s
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-45 (4 - 5')I05/03/94F93307C, COG No: 6879
Report Date: 10/07/94Lab Number: 940900311Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
10.820.01 U0.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
00!)
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100386Buchanan MI 49107 Date Received: 10/20/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-45, 4-5'04/26/94F93307C, COC No: 9400
* Results reported with "U" flag indicate the parameter was analyzed., for but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
400089.7
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-46 (0 - l')I05/03/94F93307C, COC No: 6813
Report Date: 06/24/94Lab Number: 940600326Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
3100.407.682.1
ug/kgmg/kgmg/kg%
004-
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-46 (0 - l')I05/03/94F93307C, COC No: 9396
Report Date: 10/28/94Lab Number: 94100239Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U0.710.005 U0,01 U0.02 U
5 U0.06
ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-46 (0 - l')I05/03/94F93307C, COG No: 9396
Report Date: 10/20/94Lab Number: 94100249Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.8
Units
s.u.
014
Electro-Voice Report Date: 05/27/94600 Cecil Street Lab Number: 940500185Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-46 (4-5)105/03/94F93307C, COC No: 9371
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1100.14 U9.2
86.1
ug/kgmg/kgmg/kg
0\
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-46 (4 - 5') I05/03/94F93307C, COC No: 6879
Report Date: 10/07/94Lab Number: 940900312Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.260.010.02 U
1 U0.01
ug/1mg/1mg/1mg/1ug/1mg/1
009
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700335Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-47 (0 - l')I05/03/94F93307C, COC No: 6862
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
1300002.376
7.281.1
ug/kgmg/kgnig/kgs.u.
Electro-Vo ice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-47 (4 - 5)105/03/94F93307C, COG No: 9371
Report Date: 05/27/94Lab Number: 940500191Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
22000.15
1285.1
ug/kgmg/kgrag/kg
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100465Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-47 (4 - 5')I05/03/94F93307C, COC No: 9117
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCopperNickelLeadZinc
2 U0.660.50.01 U0.02 U
2 U0.04
ug/1mg/1ug/1mg/lmg/1ug/1mg/l
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-47 (4 - 5'} I05/03/94F93307C, COG No: 9117
Report Date: 11/03/94Lab Number: 94100477Date Received: 10/24/94Client ID: 60688
024
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.0
Units
s.u.
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500301Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-48 (4 - 5') I05/09/94F93307C, COC No: 9373
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.•Solids, Total
8000.229.889.0
ug/kgmg/kgmg/kg
007
DOS
Electro-Voice Report Date: 11/18/94600 Cecil Street Lab Number: 94100485Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-48 (4 - 5'} I05/09/94F93307C, COC No: 9221
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.250.01 U0.02 U
2 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-48 (4 - 5') I05/09/94F93307C, COG No: 9221
Report Date: 11/03/94Lab Number: 94100497Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.8
Units
s.u.
CO/
Report Date: 06/01/94Lab Number: 940500296Date Received: 05/11/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-49 (4 - 5') I05/09/94F93307C, COG No: 9373
* Results reported with "U" flag indicate the parameter was analyzedfor taut not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2100.14 U3.9
87.2
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-49 (4 - 5') I05/09/94F93307C, COC No: 9118
001
Report Date: 11/18/94Lab Number: 94100503Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.240.01 U0.02 U
2 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-49 (4-5)105/09/94F93307C, COC No: 9118
Report Date: 11/16/94Lab Number: 94100511Date Received: 10/24/94Client ID: 60688
010'
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
8.5
Units
s.u.
003
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500297Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-50 (4 - 5') I05/09/94F93307C, COG No: 9373
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
25000.558.3
95.5
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-51 (4 - 5')I05/09/94F933Q7C, COC No: 9373
Report Date: 06/02/94Lab Number: 940500304Date Received: 05/11/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
320009.8220
85.3
mg/kgmg/kg
007
Electro-Voice Report Date: 08/10/94600 Cecil Street Lab Number: 940700372Buchanan MI 49107 Date Received: 07/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-51 (4 - 5')I05/04/94F93307C
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
130069744311140
ug/kgmg/kgmg/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-52 (4 - 5') I05/09/94F93307C, COG No: 9374
Report Date: 06/02/94Lab Number: 940500308Date Received: 05/11/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor taut not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
5300.2024
89.2
ug/kgmg/kgmg/kg
009
Report Date: 07/27/94Lab Number: 940700351Date Received: 07/15/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-52 (4 - 5') I05/09/94F93307C, COC No: 6861
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Chromium, T.
Result
0.02 U
Units
mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-52 (4 - 5')I05/09/94F93307C, COC No: 6861
Report Date: 07/20/94Lab Number: 940700361Date Received: 07/15/94Client ID: 60688
019
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result
6.9
Units
s.u.
012-
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600327Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-53 (0 - I')*05/04/94F93307C, COG No: 6813
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide , T .Chromium, T.Solids, Total
1500.15 U8.183.3
ug/kgmg/kgmg/kg%
009
E1ectro-Vo ice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-53 (0 - l')I05/04/94F93307C, COC No: 9397
Report Date: 10/31/94Lab Number: 94100265Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U1.0
0.01 U0.02 U
40.04
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100277Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-53 (0 - l')I05/04/94F93307C, COG No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
6.5
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-53 (4-5)105/04/94F93307C, COC No: 9371
Report Date: 05/27/94Lab Number: 940500192Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium , T .Solids, Total
820.14 U7.8
91.5
ug/kgmg/kgmg/kg%
001
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-53 (4 - 5')I05/04/94F93307C, COC No: 6881
Report Date: 10/06/94Lab Number: 940900313Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.320.01 U0.02 U
1 U0.01
ug/1ntg/1mg/1mg/1ug/1mg/1
00'
Electro-Voice Report Date: 05/26/94600 Cecil Street Lab Number: 940500174Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-54 (4 - 5')I05/04/93F93307C, COC No: 9370
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
759.87.2
86.3
ug/kgmg/kgmg/kg
(902-
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-54 (9 - 10')07/25/94F93307C, COG No: 9272
Report Date: 08/30/94Lab Number: 940800074Date Received: 08/04/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
390.165.8
94.9
ug/kgmg/kgmg/kg
010
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-54 (9 - 10')07/25/94F93307C, COC No: 6876
Report Date: 10/04/94Lab Number: 940900283Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.560.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-55 (4 - 5') I05/10/94F93307C, COC No: 9373
Report Date: 06/01/94Lab Number: 940500302Date Received: 05/11/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
18000.4324
81.9
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-55 (4 - 5')I05/10/94F93307C, COG No: 9118
Report Date: 11/18/94Lab Number: 94100509Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalChromium, T.CopperNickelLeadZinc
1 U0.300.2 U
0.005 U0.02 U0.01 U0.02 U
2 U0.01 U
ug/1mg/1ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-55 (4 - 5') I05/10/94F93307C, COC No: 9118
Report Date: 11/16/94Lab Number: 94100517Date Received: 10/24/94Client ID: 60688
Olt
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.7
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-56 (4 - 5')I05/10/94F93307C, COG No: 9118
0
Report Date: 11/16/94Lab Number: 94100512Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.8
Units
s.u.
013
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-57 (0 - l')I05/04/94F93307C, COG No: 6813
Report Date: 06/24/94Lab Number: 940600328Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2500.15 U6.2
84.7
ug/kgmg/kgmg/kg%
010
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100266Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-57 (0 - 1'JI05/04/94F93307C, COG No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
Arsenic 2 U ug/1Barium 1.3 mg/1Copper 0.01 U mg/1Nickel 0.02 U mg/1Lead 6 ug/1Zinc 0.04 mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-57 (0 - l')I/Soil05/11/94F93307C, COC No: 9414
00?
Report Date: 11/30/94Lab Number: S41100290Date Received: 11/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
mg/kgLeadSolids, Total
1184.9
ow-
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-57 (0 - l')I05/04/94F93307C, COG No: 9397
Report Date: 10/20/94Lab Number: 94100278Date Received: 10/17/94Client ID: 60688
* Results reported with HU" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
5.8
Units
s.u.
Electro-Voice Report Date: 05/26/94600 Cecil Street Lab Number: 940500177Buchanan MI 49107 Date Received: 05/05/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-57 (4 - 5')I05/04/94F93307C, COC No: 9370
* Results reported with "IT" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
440.15 U11
84.5
ug/kgmg/kgmg/kg
C03
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-57 (4 - 5')I05/04/94F93307C, COG No: 6881
Report Date: 10/06/94Lab Number: 940900314Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.440.01 U0.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
014
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-58 (0 - 1'JI05/04/94F93307C, COC No: 6813
Report Date: 06/24/94Lab Number: 940600329Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1800.14 U5.1
87.2
ug/kgmg/kgmg/kg
00?
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-58 (0 - l'05/04/94F93307C
Report Date: 08/10/94Lab Number: 940700373Date Received: 07/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
150027
5,86.49,333
ug/kgmg/kgmg/kgmg/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-58 (0 - I7)I05/04/94F93307C, COC No: 9197
Report Date: 11/03/94Lab Number: 94100296Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.420.01 U0.02 U
2 U0.05
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-58 (0 - l')I05/04/94F93307C, COC No: 9197
06?
Report Date: 10/21/94Lab Number: 94100300Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
4.9
Units
s.u.
015
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700341Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-58 (2 - 3') I05/04/94F93307C, COG No: 6863
+ Results reported with "U" flag indicate the parameter was analyzed^ for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
590.1812
5.385.2
ug/kgmg/kgmg/kgs.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-58 (2 - 3')D05/04/94F93307C, COG No: 6863
Report Date: 08/02/94Lab Number: 940700342Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
620.15 U
105.3
85.9
ug/kging/kgmg/kgs.u.
00
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-58 (4 - 5')I05/04/94F93307C, COC No: 9370
Report Date: 05/26/94Lab Number: 940500176Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
580.14 U6.9
92.2
ug/kgmg/kgmg/kg
Olfi
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-59 (0 - l')I05/10/94F93307C, COG No: 6812
Report Date: 06/24/94Lab Number: 940600330Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
320003.874
90.0
ug/kgmg/kgmg/kg
010
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700336Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-59 (2 - 3') I05/10/94F93307C, COC No: 6862
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
5300.17
9.77.5
87.2
ug/kgmg/kgmg/kgs.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-59 (2 - 3')I05/10/94F93307C, COC No: 9118
Report Date: 11/18/94Lab Number: 94100505Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.580.01 U0.02 U
2 U0.04
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-59 (2 - 3') I05/10/94F93307C, COC No: 9118
Report Date: 11/16/94Lab Number: 94100513Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.3
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-59 (4 - 5') I05/10/94F93307C, COG No: 9374
Report Date: 06/02/94Lab Number: 940500310Date Received: 05/11/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
6100.27
1383.6
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 06/01/94600 Cecil Street Lab Number: 940500298Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-60 (4 - 5')I05/10/94F93307C, COC No: 9373
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
18000.229.7
89.3
ug/kgmg/kging/kg
004
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-60 (4 - 5')I05/10/94F93307C, COC No: 9118
005
Report Date: 11/18/94Lab Number: 94100506Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCopperNickelLeadZinc
2 U0.450.2
0.01 U0.02 U
2 U0.02
ug/1mg/1ug/1mg/1mg/1ug/1mg/1
•J
Electro-Voice Report Date: 11/16/94600 Cecil Street Lab Number: 94100514Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-60 (4 - 5')I05/10/94F93307C, COC No: 9118
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.9
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-61 (0 - l')I05/04/94F93307C, COG No: 6812
Report Date: 06/24/94Lab Number: 940600331Date Received: 06/08/94Client ID: 60688
OKi
* Results reported with "UM flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2100.398.984.3
ug/kgmg/kgmg/kg
oi\
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100267Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-61 (0 - l')I05/04/94F93307C, COC No: 9397
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
21.10.010.02
40-07
U
UU
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-61 (0 - l')I05/04/94F93307C, COC No: 9397
Report Date: 10/20/94Lab Number: 94100279Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.4
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-61 (4 - 5)1
F93307C, COC No: 9371
C24
Report Date: 06/01/94Lab Number: 940500195Date Received: 05/05/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
390.225.2
91.7
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-61 (4 - 5')I05/04/94F93307C, COC No: 6881
Report Date: 10/06/94Lab Number: 940900315Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.620.01 U0.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
017
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600332Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-62 (0 - l')I05/10/94F93307C, COC No: 6812
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
10000.15
1183.9
ug/kgmg/kgmg/kg
005
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-62 (0 - l')I05/10/94F93307C, COG No: 9197
Report Date: 11/03/94Lab Number: 94100297Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.550.01 U0.02 U
2 U0.12
ug/1mg/1mg/1mg/1ug/1mg/1
00k
Electro-Voice Report Date: 05/24/94600 Cecil Street Lab Number: 940400668Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-69 (2 - 3')I04/25/94F93307C, COC No: 9216
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, T.Chromium , T .CopperNickelLeadSolids, TotalZinc
21002741
0.14 U5.26.46.36.1
88.326
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
._i_
oc;
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-70 (0 - l')I04/25/94F93307C, COC No: 9216
Report Date: 05/24/94Lab Number: 940400669Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, T.Chromium, T.CopperNickelLeadSolids, TotalZinc
2800492000.14 U7.08.08.415
86.936
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
00?
Electro-Voice Report Date: 10/21/94600 Cecil Street Lab Number: 94100301Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-62 (0 - l')I05/10/94F93307C, COC No: 9197
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
5.2
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-62 (4 - 5') I05/10/94F93307C, COC No: 9373
Report Date: 06/01/94Lab Number: 940500299Date Received: 05/11/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
340.134.1
94.8
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-63 (0 - I'}*05/10/94F93307C, COC No: 6862
Report Date: 08/02/94Lab Number: 940700337Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide , T .Chromium , T .pHSolids, Total
1900004.81806.990
ug/kgmg/kgmg/kgs.u.%
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-63 (2 - 3')I05/10/94F93307C, COG No: 6862
Report Date: 08/02/94Lab Number: 940700338Date Received: 07/15/94Client ID: 60688
Oil
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
210005.3547.489.4
ug/kgmg/kgmg/kgs.u.%
012-
Electro-Voice Report Date: 06/02/94600 Cecil Street Lab Number: 940500306Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-63 (4 - 5')I05/10/94F93307C, COC No: 9373
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
31000.39
1382 .9
ug/kging/kging/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-63 (4 - 5') I05/10/94F93307C, COG No: 9118
Report Date: 11/18/94Lab Number: 94100507Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCopperNickelLeadZinc
1 U0.430.2 U0.01 U0.02 U
2 U0.02
ug/1mg/1ug/1mg/1mg/1ug/1mg/1
s
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-63 (4 - 5')I05/10/94F93307C, COG No: 9118
Report Date: 11/16/94Lab Number: 94100515Date Received: 10/24/94Client ID: 60688
014-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.7
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-64 (0 - l')I05/11/94F93307C, COC No: 6812
Report Date: 06/24/94Lab Number: 940600333Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
9200.528.9
82.1
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 10/28/94600 Cecil Street Lab Number: 94100241Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-64 (0 - l')I05/11/94F93307C, COC No: 9396
Results reported with "U" flag indicate the parameter was analyzeds for but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U0.630.005 U0.01 U0.02 U
5 U0.05
ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100251Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-64 (0 - l')I05/11/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
4.9
Units
s.u.
Electro-Voice Report Date: 06/02/94600 Cecil Street Lab Number: 940500311Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-64 (4 - 5') I05/11/94F93307C, COC No: 9374
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
610.15 U8.884.1
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-64 (4 - 5') I05/11/94F93307C, COC No: 6881
Report Date: 10/06/94Lab Number: 940900316Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.340.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
015
Electro-Voice Report Date: 11/16/94600 Cecil Street Lab Number: 94100516Buchanan MI 49107 Date Received: 10/24/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-65 (0 - l')I05/10/94F93307C, COC No: 9118
* Results reported with "XT" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.6
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49X07
Attention: Mr. Ron Graham
Sample ID: LSB-65 (4 - 5')I05/10/94F93307C, COG No: 9373
CO?
Report Date: 06/01/94Lab Number: 940500303Date Received: 05/11/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1700.15 U11
83.7
ug/kgmg/kgmg/kg
018
Electro-Voice Report Date: 06/02/94600 Cecil Street Lab Number: 940500312Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-66 (4- 5')I05/11/94F93307C, COC No: 9374
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
12000.23
1386.3
ug/kging/kgmg/kg
WO'
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-67 (0 - l')I05/11/94F93307C, COG No: 6812
Report Date: 06/24/94Lab Number: 940600335Date Received: 06/08/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
20000.818.7
89.8
ug/kgmg/kgmg/kg
010
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100245Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-67 (0 - l')I05/11/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalCopperNickelLeadZinc
2 U1.30.5
0.005 U0.01 U0.02 U16
0.06
ug/1mg/1ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr- Ron Graham
Sample ID: LSB-67 (0 - l')I05/11/94F93307C, COG No: 9396
Report Date: 10/20/94Lab Number: 94100255Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit*
Parameter
pH
Result
7.6
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-67 (0 - 1'} I/Soil07/28/94F93307C, COC No: 9414
Report Date: 11/30/94Lab Number: 941100294Date Received: '11/15/94Client ID: 60688
013-
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
mg/kgLeadi Solids, Total
10089.8
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-67 (2 - 37)I05/11/94F93307C, COG No: 6863
Report Date: 08/02/94Lab Number: 940700339Date Received: 07/15/94Client ID: 60688
013
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgCadmiumCyanide, T.Chromium, T.PHSolids, Total
2400.15 U6.17.4
83.7
mg/kgs.u.
019
Electro-Voice Report Date: 06/02/94600 Cecil Street Lab Number: 940500313Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-67 (4 - 5')I05/11/94F93307C, COC No: 9374
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
Cadmium 43 ug/kgCyanide, T. 0.14 mg/kgChromium, T. 8.7 mg/kgSolids, Total 87.0 %
Report Date: 10/06/94Lab Number: 940900317Date Received: 09/19/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-67 (4 - 5')I05/11/94F93307C, COC No: 6881
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.590.01 U0.02 U
1 U0.01 U
ug/1rag/1mg/1mg/1ug/1mg/1
003
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-68 (0 - l')I04/25/94F93307C, COC No: 9216
Report Date: 05/24/94Lab Number: 940400665Date Received: 04/29/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium , T .CopperNickelLeadSolids, TotalZinc
370059280
0.15 U11111120
84.359
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
004
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-68 (2 - 3')I04/25/94F93307C, COC No: 9216
Report Date: 05/24/94Lab Number: 940400666Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium , T .CopperNickelLeadSolids, TotalZinc
40005064
0.15 U1213137.8
84.140
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
Electro-Voice Report Date: 06/02/94600 Cecil Street Lab Number: 940500315Buchanan MI 49107 Date Received: 05/11/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-68 (4.5 - 5')I05/11/94F93307C, COC No: 9374
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
Cadmium 66 ug/kgCyanide, T. 0.14 U mg/kgChromium, T. 9.1 mg/kgSolids, Total 90.2 %
GOiJ
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-69 (0 - l')I04/25/94F93307C, COC No: 9216
Report Date: 05/24/94Lab Number: 940400667Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium, T.CopperNickelLeadSolids, TotalZinc
260048280
0.15 U6.08.17.119
85.340
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-70 (7.5 - 8') I05/11/94F93307C, COC No: 9374
Report Date: 06/02/94Lab Number: 940500314Date Received: 05/11/94Client ID: 60688
Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
390.158.383.9
ug/kgmg/kgmg/kg
OOS i
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-70 (3 - 4')I04/25/94F93307C, COG No: 9216
Report Date: 05/24/94Lab Number: 940400670Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium , T .CopperNickelLeadSolids, TotalZinc
260094220
0.15 U118.1138.3
83.240
ug/kgmg/kgug/kgrag/kgmg/kgmg/kgmg/kgmg/kg%.mg/kg
009
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-71 (2 - 3') I04/25/94F93307C, COG No: 9216
Report Date: 05/24/94Lab Number: 940400671Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T ,Chromium , T .CopperNickelLeadSolids, TotalZinc
27004882
0.14 U7.47.49.411
86.934
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
oic
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-71 (3 - 4')I04/25/94F93307C, COG No: 9216
Report Date: 05/24/94Lab Number: 940400672Date Received: 04/29/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium , T .CopperNickelLeadSolids, TotalZinc
56005970
0.15 U15162015
83.467
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
01
Electro-Voice Report Date: 05/24/94600 Cecil Street Lab Number: 940400673Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-72 (1 - 2')I04/25/94F93307C, COC No: 9216
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium , T .CopperNickelLeadSolids, TotalZinc
380089190
0.21128.81417
83.256
ug/kgrag/ kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%ma/ka
012
Electro-Voice Report Date: 05/24/94600 Cecil Street Lab Number: 940400674Buchanan MI 49107 Date Received: 04/29/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-72 (3 - 4')I04/25/94F93307C, COG No: 9216
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide , T .Chromium, T.CopperNickelLeadSolids, TotalZinc
41003035
0.35111313
9.084.343
ug/kgmg/kgug/kgmg/kgmg/kgmg/kgmg/kgmg/kg%mg/kg
010
Report Date: 08/02/94Lab Number: 940700352Date Received: 07/15/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-73 (0 -l')I06/23/94F93307C, COC No: 6861
* Results reported with "U" flag indicate the parameter was analyzed• for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, TotalChromium, T.
0.2 U0.005 U0.02 U
ug/1mg/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-73 (0 - l')I06/23/94F93307C, COG No: 6861
Report Date: 07/20/94Lab Number: 940700362Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.1
UnitsP ••» m m~ w —— -
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Report Date: 08/19/94Lab Number: 940800105Date Received: 08/04/94Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-73 (0 - l')I06/23/94F93307C, COC No: 9277
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
019
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
6300.2910
86.9
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-73 (0 - l')I06/23/94F93307C, COG No: 9397
Report Date: 10/31/94Lab Number: 94100268Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.890.01 U0.02 U13
0.10
ug/1mg/1mg/1mg/1ug/1mg/1
c005
Electro-Voice Report Date: 11/30/94600 Cecil Street Lab Number: 941100291Buchanan MI 49107 Date Received: 11/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-73 (0 - 1')I/Soil07/27/94F93307C, COC No: 9414
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
mg/kgLeadSolids, Total
4288.2
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-73 (4 - 5')I06/23/94F93307C, COG No: 6862
OC'
Report Date: 08/02/94Lab Number: 940700329Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
1000.15166.4
84.4
ug/kgmg/kgmg/kgs.u.
007
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900318Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-73 (4 - 5')I06/23/94F93307C, COC No: 6881
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
13601 U
U0.0.0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-73 (9 -10')I06/23/94F93307C, COC No: 9102
Report Date: 07/13/94Lab Number: 940601033Date Received: 06/24/94Client ID: 60688
014
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2100.14 U8.889.6
ug/kgmg/kgmg/kg
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700353Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-74 (0 -l')I06/23/94F93307C, COC No: 6861
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, TotalChromium, T.
0.2 U0.005 U0.02 U
ug/1mg/1mg/1
J_
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-74 (0 - l')I06/23/94F93307C, COC No: 6861
Report Date: 07/20/94Lab Number: 940700363Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.2
Units
s.u.
VU)
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-74 (0 - l')I06/23/94F93307C, COC No: 9277
Report Date: 08/19/94Lab Number: 940800106Date Received: 08/04/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
6300.1610
93.6
ug/kgmg/kgmg/kg
013
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-74 (0 - l')I06/23/94F93307C, COC No: 9397
Report Date: 10/31/94Lab Number: 94100269Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.530.01 U0.02 U
50.05
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-74 (0 - l')I06/23/94F93307C, COC No: 9397
Report Date: 10/20/94Lab Number: 94100281Date Received: 10/17/94Client ID: 60688
02-5
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
8.0
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-74 (0 - 1')I/Soil06/23/94F93307C, COC No: 9414
Report Date: 11/30/94Lab Number: 941100292Date Received: 11/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
mg/kgLeadSolids, Total
7794.7
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-74 (4 - 5') I06/23/94F93307C, COC No: 6862
Report Date: 08/02/94Lab Number: 940700330Date Received: 07/15/94Client ID: 60688
004
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.pHSolids, Total
3300.21
137.5
82.8
ug/kgmg/kging/kgs.u.
008
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900319Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-74 (4 - 5')*06/23/94F93307C, COC No: 6881
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U1.4
0.01 U0.02 U
1 U0.07
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 07/13/94600 Cecil Street Lab Number: 940601034
» Buchanan MI 49107 Date Received: 06/24/94Client ID: 60688
! Attention: Mr. Ron Graham
i Sample ID: LSB-74 (9 - 10') I06/23/94F93307C, COC No: 9102
i, v Results reported with "U" flag indicate the parameter was analyzed
for but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2500.14 U8.590.1
ug/kgmg/kgmg/kg
oc
Electro-Voice600 Cecil streetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-75 (0 - l')I06/23/94F93307C, COG No: 6862
Report Date: 08/02/94Lab Number: 940700328Date Received: 07/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
4600.229.47.7
91.9
ug/kgmg/kgmg/kgs.u.
ooz
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100282Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-75 (0 - l')I06/23/94F93307C, COC No: 9398
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
40.400.01 U0.02 U
2 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
00$
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-75 (0 - l')I06/23/94F93307C, COC No: 9398
Report Date: 10/21/94Lab Number: 94100288Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.5
Units
s.u.
Electro-Voice Report Date: 06/24/94600 Cecil Street Lab Number: 940600334Buchanan MI 49107 Date Received: 06/08/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-65 (0 - l')I05/10/94F93307C, COC No: 6812
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
81000.229.390.7
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-65 (0 - l')I05/10/94F93307C, COC No: 9118
Report Date: 11/18/94Lab Number: 94100508Date Received: 10/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCopperNickelLeadZinc
1 U0.290.2 U0.01 U0.02 U
2 U0.01
ug/1mg/1ug/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 11/23/94600 Cecil Street Lab Number: 941100285Buchanan MI 49107 Date Received: 11/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-75 (0 - 1')I/Soil05/02/94F93307C, COC No: 9414
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
680091.7
Electro-Voice Report Date: 08/02/94600 Cecil Street Lab Number: 940700331Buchanan MI 49107 Date Received: 07/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-75 (4 - 5')I06/23/94F93307C, COC No: 6862
* Results reported with "U" flag indicate the parameter was analyEedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.PHSolids, Total
1200.15 U177.383.9
ug/kgmg/kgmg/kgs.u.
009
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-75 (4 - 5') I06/23/94F93307C, COC No: 6881
Report Date: 10/06/94Lab Number: 940900320Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.490.01 U0.02 U
1 U0.01
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-75 (9 -10')I06/23/94F93307C, COG No: 9102
Olk»
Report Date: 07/13/94Lab Number: 940601035Date Received: 06/24/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1100.14 U6.5
92.2
ug/kgmg/kging/kg
014-
Electro-Voice Report Date: 08/19/94600 Cecil Street Lab Number: 940800086Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-76 (0-1')07/28/94F93307C, COC No: 9275
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide , T.Chromium, T.Solids, Total
3700.328.484.4
ug/kgmg/kgmg/kg
003
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100283Buchahan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-76 (0 - l')I07/28/94F93307C, COC No: 9398
* Results reported with I!U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
Arse-nicBariumCopperNickelLeadZinc
60.500.01 U0.02 U
2 U0.04
ug/1mg/1mg/1mg/1ug/1mg/1
009
Electro-Voice Report Date: 10/21/94600 Cecil Street Lab Number: 94100289Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-76 (0 - l')I07/28/94F93307C, COC No: 9398
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
6.0
Units
s.u.
Electro-Voice Report Date: 11/23/94600 Cecil Street Lab Number: 941100286Buchanan MI 49107 Date Received: 11/15/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-76 (0 - 1')I/Soil05/04/94F93307C, COC No: 9414
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
1100085.3
) Electro-Voice*• 600 Cecil Street
Buchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-76 (4 - 5'}I07/26/94F93307C, COG No: 6881
010
Report Date: 10/06/94Lab Number: 940900321Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.480.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 08/19/94600 Cecil Street Lab Number: 940800090Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-77 (0-1')07/28/94F93307C, COC No: 9275
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
7400.3711
86.5
ug/kgmg/kgmg/kg
oof
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100284Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-77 (0 - 1'JI07/28/94F93307C, COC No: 9398
* Results reported with "U11 flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.330.01 U0.02 U
2 U0.05
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-77 (0 - l')I07/28/94F93307C, COG No: 9398
Report Date: 10/21/94Lab Number: 94100290Date Received: 10/17/94Client ID: 60688
010
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
4.9
Units
s.u.
Oil
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900322Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-77 (4 - 5')I07/28/94F93307C, COC No: 6881
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
13601 U
U000.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-78 (0-1')07/27/94F93307C, COC No: 9272
013'
Report Date: 08/19/94Lab Number: 940800085Date Received: 08/04/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2400.149.389.0
ug/kgmg/kgmg/kg
005
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100285Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-78 (0 - l')I07/28/94F93307C, COC No: 9398
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
110.490.01 U0.02 U
2 U0.04
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-78 (0 - l')I07/28/94F93307C, COG No: 9398
0
Report Date: 10/21/94Lab Number: 94100291Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
7.0
Units•» •* m »*»«
s.u.
00'
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-78 (0 - 1')I/Soil06/23/94F93307C, COC No: 9414
Report Date: 11/23/94Lab Number: 941100287Date Received: 11/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicSolids, Total
900088.5
ug/kg%
Oil
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900323Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-78 (4 - 5') I07/27/94F93307C, COC No: 6881
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.810.01 U0.02 U
1 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 08/19/94600 Cecil Street Lab Number: 940800089Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-79 (0 - 1')07/28/94F93307C, COC No: 9275
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
38000.40
1287.1
ug/kgmg/kgmg/kg
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-79 (0 - l')I07/28/94F93307C, COC No: 9398
Report Date: 10/21/94Lab Number: 94100292Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
5.4
Units
s.u.
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100286Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-79 (0 - l')I07/28/94F93307C, COC No: 9398
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
2 U0.580.01 U0.02 U
2 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
002-
Electro-Voice Report Date: 01/06/95600 Cecil Street Lab Number: 941200531Buchanan MI 49107 ' Date Received: 12/20/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-79 (0 - l')I07/28/94F93307C, COG No: 9555
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, Total
0.50.005 U
ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-79 (4 - 5') I07/28/94F93307C, COC No: 6881
Report Date: 10/06/94Lab Number: 940900324Date Received: 09/19/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.450.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 08/19/94600 Cecil Street Lab Number: 940800084Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-80 (0-1')07/27/94F93307C, COC No: 9272
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
5400.209.2
87.4
ug/kgmg/kgmg/kg
I
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100287Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-80 (0 - 1'JI07/28/94F93307C, COC No: 9398
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
50.520.01 U0.02 U
2 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
013
Electro-Voice Report Date: 10/21/94600 Cecil Street Lab Number: 94100293Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-80 (0 - l')I07/28/94F93307C, COC No: 9398
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
pH
Result
7.7
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-80 (0 - l')I/Soil06/23/94F93307C, COC No: 9414
001?
Report Date: 11/23/94Lab Number: 941100288Date Received: 11/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ug/kgArsenicSolids, Total
730087.2
OK
Report Date: 10/06/94Lab Number: 940900325Date Received: 09/19/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-80 (4 - 5')I
F93307C, COC No: 6882
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.750.01 U0.02 U
1 U0.02
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 08/19/94600 Cecil Street Lab Number: 940800087Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-81 (0 - 1')07/28/94F93307C, COC No: 9275
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1700.14 U8.1
90.8
ug/kging/kgmg/kg
Electro-Voice Report Date: 08/19/94600 Cecil Street Lab Number: 940800088Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-81 (0 - 1')Duplicate07/28/94F93307C, COC No: 9275
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
1800.14 U8.390.9
ug/kgmg/kgmg/kg
002.
Electro-Voice Report Date: 11/03/94600 Cecil Street Lab Number: 94100294Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-81 (0 - l')I07/28/94F93307C, COC No: 9197
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the samole above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
20.560.010.02
20.03
U
UUU
ug/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-81 (0 - l')I07/28/94F93307C, COG No: 9197
Report Date: 10/21/94Lab Number: 94100298Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
5.8
Units
s.u.
01-
Electro-Voice Report Date: 12/05/94600 Cecil Street Lab Number: 941100416Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60638
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-82 (6 - 7')11/17/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCadmiumCyanide, TotalChromium, T.CopperNickelZinc
1.40.3
0.005 U0.02 U0.010.02 U0.06
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
oco
Electro-Voice Report Date: 11/30/94600 Cecil Street Lab Number: 941100408Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-82 (6 - 7')11/17/94F93307C, COG No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicLeadSolids, Total
37007.286.4
ug/kgmg/kg
0!
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-83 (6 - 7')11/17/94F93307C, COC No: 9546
Report Date: 12/05/94Lab Number: 941100415Date Received: 11/18/94Client ID: 60638
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCadmiumCyanide, TotalChromium, T.CopperNickelZinc
0.770.2 U
0.005 U0.02 U0.010.02 U0.04
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-83 (6 - 7')11/17/94F93307C, COC No: 9546
Report Date: 11/30/94Lab Number: 941100407Date Received: 11/18/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result
ArsenicLeadSolids, Total
380010
85.0
Units
ug/kgmg/Xg
Report Date: 12/05/94Lab Number: 941100414Date Received: 11/18/94Client ID: 60688
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-84 (8 - 9')11/17/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Resul' Units
BariumCadmiumCyanide, TotalChromium, T.CopperNickelZinc
0.770.2 U
0.005 U0.02 U0.01 U0.02 U0.01
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-84 (8 - 9')11/17/94F93307C, COC No: 9546
Report Date: 11/30/94Lab Number: 941100406Date Received: 11/18/94Client ID: 60688
Parameter Result Units
ArsenicLeadSolids, Total
390011
87.2
ug/kgmg/kg
005
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
010
Electro-Voice Report Date: 12/05/94600 Cecil Street Lab Number: 941100413Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-85 (3-4')11/16/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCadmiumCyanide, TotalChromium, T.CopperNickelZinc
0.320.2 U
0.005 U0.02 U0.01 U0.02 U0.01 U
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
Electro-Voice Report Date: 11/30/94600 Cecil Street Lab Number: 941100405Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-85 (3 - 4')11/16/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicLeadSolids, Total
19007.8
83.1
ug/kgmg/kg
005
Electro-Voice Report Date: 08/30/94600 Cecil Street Lab Number: 940800080Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-86 (0 - 1')07/27/94F93307C, COC No: 9272
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
2900.54
7 . 088.2
ug/kging/kgmg/kg
005
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-86 (0 - l')I07/27/94F93307C, COC No: 9396
Report Date: 10/28/94Lab Number: 94100240Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U0.630.005 U0.01 U0.02 U
5 U0.05
Units
ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100250Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-86 (0 - l')I07/27/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
4.9
Units
s.u.
007
Electro-Voice Report Date: 10/28/94600 Cecil Street Lab Number: 94100242Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-87 (0 - l')I07/27/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U0.400.005 U0.01 U0.02 U
5 U0.20
ug/1mg/1mg/1mg/1mg/1ug/1mg/1
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100252Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-87 (0 - l')I07/27/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
PH
Result
4.7
Units
s.u.
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900327Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-87 (4 - 5')I07/27/94F93307C, COC No: 6882
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCopperNickelLeadZinc
1 U0.250.01 U0.02 U
1 U0.03
ug/1mg/1mg/1mg/1ug/1mg/1
010
Electro-Voice Report Date: 08/30/94600 Cecil Street Lab Number: 940800082Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-88 (0 - 1')07/27/94F93307C, COC No: 9272
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
30000.759.690.1
ug/kgmg/kgmg/kg
DO'S
Electro-Voice Report Date: 10/31/94600 Cecil Street Lab Number: 94100243Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-88 (0 - l')I07/27/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCadmiumCyanide, TotalCopperNickelLeadZinc
2 U0.670.4 U
0.005 U0.01 U0.02 U
5 U0.02
ug/lmg/lug/lmg/lmg/lmg/lug/lmg/l
Electro-Voice Report Date: 10/20/94600 Cecil Street Lab Number: 94100253Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-88 (0 - l')I07/27/94F93307C, COG No: 9396
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
ParameterWB*B^^^B*BB ^——^ •
pH
Result
7.3
Units
s.u.
0
Electro-Voice Report Date: 10/06/94600 Cecil Street Lab Number: 940900328Buchanan MI 49107 Date Received: 09/19/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-88 (4 - 5')I07/27/94F93307C, COC No: 6882
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result units
ArsenicBariumCopperNickelLeadZinc
1 U0.490.01 U0.02 U
1 U0.01 U
ug/1mg/1mg/1mg/1ug/1mg/1
009
Electro-Voice Report Date: 08/30/94600 Cecil Street Lab Number: 940800081Buchanan MI 49107 Date Received: 08/04/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-89 (0 - 1')07/27/94F93307C, COC No: 9272
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
CadmiumCyanide, T.Chromium, T.Solids, Total
4400.568.3
88.2
ug/kgmg/kging/kg
Electro-Voice Report Date: 10/28/94600 Cecil Street Lab Number: 94100246Buchanan MI 49107 Date Received: 10/17/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-89 (0 - l')I07/27/94F93307C, COC No: 9396
* Results reported with "U" flag indicate the parameter was analyzed'for but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicBariumCyanide, TotalCopperNickelLeadZinc
2 U1.1
0.005 U0.01 U0.02 U14
0.06
ug/1mg/1mg/1mg/img/1ug/1mg/1
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-89 (0 - l')I07/27/94F93307C, COC No: 9396
Report Date: 10/20/94Lab Number: 94100256Date Received: 10/17/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
ParameterVB ^H ^B «* *• HWB4
pH
Result
7.3
Units
s.u.
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: LSB-89 (0 - 1')I/Soil07/28/94F93307C, COC No: 9414
Report Date: 11/30/94Lab Number: 941100295Date Received: 11/15/94Client ID: 60688
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
mg/kgLeadSolids, Total
4488.4
Electro-Voice Report Date: 12/05/94600 Cecil Street Lab Number: 941100417Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-90 (4-5')11/17/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCadmiumCyanide , TotalChromium, T.CopperNickelZinc
1.20.2 U
0.005 U0.02 U0.01 U0.02 U0.03
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
Electro-Voice Report Date: 11/30/94600 Cecil Street Lab Number: 941100409Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-90 (4 - 5')11/17/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicLeadSolids, Total
600013
88.0
ug/kgmg/kg
003
Electro-Voice Report Date: 01/06/95600 Cecil Street Lab Number: 941200532Buchanan MI 49107 Date Received: 12/20/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-90 (4 - 5') I11/17/94F93307C, COC No: 9555
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter
Arsenic
ResultP. •• V* H W* <
2 U
Units
ug/1
01'
Electro-Voice600 Cecil StreetBuchanan MI 49107
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-91 (4 - 5')11/17/94F93307C, COC No: 9546
Report Date: 12/05/94Lab Number: 941100418Date Received: 11/18/94Client ID: 60638
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCadmiumCyanide, TotalChromium, T.CopperNickelZinc
0.350.2 U
0.005 U0.02 U0.01 U0.02 U0.01 U
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
00'
Electro-Voice Report Date: 11/30/94600 Cecil Street Lab Number: 941100410Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: LSB-91 (4 - 5')11/17/94F93307C, COC No: 9546
* Results reported with "Un flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicLeadSolids, Total
420014
90.1
ug/kgmg/kg
Electro-Voice Report Date: 12/05/94600 Cecil Street Lab Number: 941100419Buchanan MI 49107 Date Received: 11/18/94
Client ID: 60688
Attention: Mr. Ron Graham
Sample ID: SPLP/LSB-92 (4 - 5')11/17/94F93307C, COC No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
BariumCadmiumCyanide , TotalChromium , T .CocperNickelZinc
0.250.2 U
0.005 U0.02 U0.01 U0.02 U0.01 U
mg/1ug/1mg/1mg/1mg/1mg/1mg/1
Electro-Voice Report Date: 11/30/94600 Cecil Street Lab Number: 941100411Buchanan MI 49107 Date Received: 11/18/94
Client ID; 60688
Attention: Mr. Ron Graham
Sample ID: LSB-92 (4 - 5')11/17/94F93307C, COG No: 9546
* Results reported with "U" flag indicate the parameter was analyzedfor but not detected in the sample above the detection limit.
Parameter Result Units
ArsenicLeadSolids, Total
23008.993.9
ug/kgmg/kg