fecha de reporte: 2018-10-15 página: revisión:...
TRANSCRIPT
Destino Final:
Observaciones:
LA TIJERA, LOS REYES MICH
Aleatorio
EUA Y EU
La muestra se recibió en condiciones para su análisis.
2906-01 SECTOR 1
Estado: Michoacán Código postal: 60330
Ext. 133
60330
[email protected], [email protected],
Información de Facturación
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Fruits-Giddings SA de CV
Km. 1 Carretera los Reyes- Jacona Sn
Michoacán
Razón social:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
2018-10-15 Página: 1 de 7 Revisión: AR271-TS-61
Empresa:
Correo electrónico:
Fecha de reporte:
SUN BELLE MÉXICO S.A. DE C.V.
Dirección: Km 1 Carr. los Reyes-Jacona S/N Ciudad o Localidad: Los Reyes
Solicitante: ALFREDO OSEGUERA DÍAZ
[email protected], [email protected],
Teléfono: 3545427328
Información del Cliente
Domicilio Fiscal:
Estado:
RFC: SBM040520QN6
Ciudad o Localidad: Los Reyes
Código postal:
Analisis Multiresidual de Pesticidas
Nombre común:
Libro de registro:
Rubus Ulmifoli
oct-18P-18-24827No. Reg. de Muestra:
Fecha de recepción:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Nombre científico: Variedad:
Fecha de Término:Fecha de inicio: 2018-10-11
Información de la Muestra
Zarzamora
Ext. SD Correo electrónico:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Telefono: 3545420170
2018-10-15
Menos de 1.5kg
SD
Tupy|Otras
2018-10-11
Parte analizada:
Productor:
Lugar de muestreo:
Uso comercial:
Fruto
NEFTALI ARMANDO GONZALEZ
VAZQUEZ
Fecha de muestreo: 10/09/2018
SD
SD
Estado de la muestra:
Lugar de cosecha:
Método de muestreo:
Destino Comercial:
Cantidad recibida:
Registro SAGARPA:
RFC de Bodega:
Aduana:Mercado Nacional y Extranjero
Congelado
DIRECCION: LOS REYES,
MICHOACÁN
Humano
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace
responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
B B
B B
B B
B B
B B
B BB BB B
B B
B BB BB BB BB B
B B
B BB BB BB BB BB BB B
B B
B BB BB BB BB B
B B
B B
B B
B B
B V
B B
B B
B BB BB B
B B
B BB B
B B
B B
B B
B B
B B
B B
B BB BB BB B
B B
B B
B BB BB BB BB BB BB B
1.5 0.5
- - - -
- - - -
- -
- - - -
0.1 0.7
- - - -
0.01 0.1
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
0.01 - -
- - - -
- -
0.01 0.05
- - - -
0.05 0.1
0.01 - -
0.01 0.01
- - - -
- -
0.01 - -
- - - -
0.01 - -
0.01 0.7
0.01 2
0.01 - -
0.02 1
0.2 0.5
3 1
0.5
0.5 2
0.05 0.1
0.05 0.05
- - - -
- - - -
1
0.01 - -
0.01 - -
0.01 0.05
0.01 0.4
0.01 1
0.05 0.1
- - - -
- - - -
- -
0.01 0.5
0.01 0.05
0.01 0.3
0.1 - -
0.01 1
0.02 0.02
0.01 - -
- - - -
0.5
THIOPHANATE
METHYL/
BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
0.01 - -
0.01 0.05
0.05
0.01 0.1
0.01 0.05
1 0.7
- - - -
0.01
0.01
0.01
0.02
0.01
- -
- -
5
0.01 0.1
- - - -
0.01 5
0.05 - -
0.01 - -
0.01 - -
- - - -
0.01 - -
0.01 0.02
0.01 - -
0.01 0.5
0.01 0.01
0.01 0.01
0.01 0.01
0.01 0.01
0.05
1 1
2 0.3
0.01 0.02
0.02 1
0.01 0.05
0.02 0.02
0.02 0.02
0.02 0.02
0.05
0.01 0.02
Chlordimeform - - 0.01
- - < LCL
Chloroneb GC/MSMS
0.05 < LCL
SD
CA EU
< LCL
0.01 < LCL
- - < LCL
- - < LCL
0.05
0.01 0.1 - - < LCL
- - - - 0.01 0.1 - - < LCL
Chlorobenzilate GC/MSMS
Fecha de reporte: 2018-10-15
Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
Reg. Sagarpa:
No. Reg. Lab.:
Cantidad obtenida en mg/kg
(ppm)MX US JP CA CHN
Cantidad obtenida en mg/kg
(ppm)Analito Analito
Analizado
mediante
equipo
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
AR271-TS-61Revisión:
Cliente:
Productor:
Cromatograma GC:
SUN BELLE MÉXICO S.A. DE C.V.
NEFTALI ARMANDO GONZALEZ
VAZQUEZ
P-18-24827 10-11-2018.D
P-18-24827
US JP
2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1
Uso autorizado
LMR (ppm)
MX US JP CA CHN
0.1 0.1 < LCL Chlordane- a GC/MSMS 0.1 0.1 0.02 0.1 0.02
EU KOR EU KOR
0.1 0.05 0.02
3,4 Dichloroaniline GC/MSMSLINURON
METABOLITE
LINURON
METABOLITE
LINURON
METABOLITE
LINURON
METABOLITELINURON METABOLITE < LCL
2,6 Dichlorobenzonitrilo GC/MSMS - - - - - -
2,3 dihydro-2,2dimethylbenzofuran 7-
olGC/MSMS - - - - - - - - - - < LCL- - - -
- - - -
LINURON
METABOLITELINURON METABOLITE
Acetamiprid LC/MSMS 1.6 1.6 2 4 2 < LCL
Acephate LC/MSMS - - - - 0.01
- - - - < LCL
Abamectin LC/MSMS 0.2 0.2 0.01 0.2 - - < LCL
3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -
0.08
Aldicarb LC/MSMS - - - - 0.01 0.1 0.02 < LCL
Alachlor LC/MSMS - - - -
0.1 - - < LCL
Acrinathrin GC/MSMS - - - - 2 0.1 - - < LCL
Acetochlor LC/MSMS - - - - 0.01
Aldrin GC/MSMS 0.05 0.05
- -- -GC/MSMSAmetryn
0.05
0.1 0.02 < LCL
Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 0.02 < LCL
Aldicarb sulfone LC/MSMS - - - - 0.01
0.01 0.01
0.01 0.05
0.01 - -
Azamethiphos LC/MSMS - - - - 0.01
0.1 - - < LCL
Atrazine-2-hydroxy LC/MSMS - - - - - - - - - - < LCL
Atrazine GC/MSMS - - - - 0.05 - -
- - - -
0.01 - -
Azoxystrobin GC/MSMS 5 5 5 5 - - < LCL
Azinphos-methyl GC/MSMS - - - - 0.01
Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - - < LCL0.02 - -
0.05 0.3
5 1
Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - - < LCL
Bendiocarb LC/MSMS - - - - 0.01
- - - - < LCL
Benalaxyl GC/MSMS - - - - 0.05 0.1 - - < LCL
Baycarb LC/MSMS - - - - - - - - - -
0.05
BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL
BHC lindane alpha GC/MSMS 0.5 0.5 0.3
0.1 - - < LCL
Benzoximate LC/MSMS - - - - 0.01 0.1 - - < LCL
Bensulide LC/MSMS - - - - 0.01
Bifenox GC/MSMS - - - - 0.01 0.1 - - < LCL
Bifenazate LC/MSMS 5 5 7
0.1 - - < LCL
BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - - < LCL
BHC lindane delta GC/MSMS 0.5 0.5 0.3
7 7
0.01
Boscalid LC/MSMS 10 10 10 6 - - < LCL
Bolstar GC/MSMS - - - - - -
< LCL
Bitertanol LC/MSMS - - - - 0.05 0.1 - - < LCL
Bifenthrin GC/MSMS 1 1 1
0.01 1
- - - -
10
Bromopropylate GC/MSMS - - - - 2
Bromophos methyl GC/MSMS - - - - - - - - - - < LCL
Bromacil GC/MSMS - - - - 0.01
Buprofezin GC/MSMS - - - - 0.01 0.1 - - < LCL
Bupirimate LC/MSMS - - - - 0.01
Bromuconazole* LC/MSMS - - - - 0.01 0.1 - - < LCL
1.5 - -
0.05 1
1 1
0.1
Chlorfenvinphos LC/MSMS - - - -
LC/MSMS - - - - 0.01
- - < LCL
5 7 < LCL
0.1 - - < LCL
0.1 - - < LCL
2 1 < LCL
0.1 - - < LCL
0.1
0.05
0.01 1
0.1 - - < LCL
0.1 - - < LCL
0.1 - - < LCL
0.1 - - < LCL
- -
0.1
Chlorfenapyr GC/MSMS - - - -
0.1
0.5 < LCL
- - - - < LCL
Coumaphos GC/MSMS - - - - - - 0.1
GC/MSMS - -
- - - - 0.01
0.1 - - < LCL
Chlormequat LC/MSMS - - - - 0.05 0.1 - - < LCL
Chloridazon (Pyrazon) LC/MSMS - - - - 0.01
0.1
- - 0.01 0.1 - - < LCL
Clomazone* LC/MSMS - - - - 0.02
- - - - < LCL
Chlorthiophos GC/MSMS - - - - - - - - - - < LCL
Chlortal dimethyl GC/MSMS
< LCL- -0.1 3 1
0.01 0.05
- - - -
Cyantraniliprole* LC/MSMS - - - - 0.01 0.1 - - < LCL
0.1 - - < LCL
Cyhalothrin (Isomero Lambda
y gamma)**GC/MSMS - - - - 0.5 0.01 0.2 < LCL
Cyfluthrin GC/MSMS - - - - 0.02
0.02 - - < LCL
Cycloate LC/MSMS - - - - 0.01 0.1 - - < LCL
Cyazofamid LC/MSMS - - - - 0.01
0.1 - - < LCL
Cyprodinil GC/MSMS 10 10 10 10 - - < LCL
Cyproconazole LC/MSMS - - - - 0.5
4 - - < LCL
Cypermethrin a (Zeta-
Cypermethrin)**GC/MSMS 0.8 0.8 0.5 0.1 - - 0.013
Cymoxanil LC/MSMS 4 4 4
- - - - < LCL
DDE-o,p GC/MSMS - - - - - - - - - - < LCL
DDD-p,p GC/MSMS - - - - - -
0.1 - - < LCL
DDD-o,p GC/MSMS - - - - - - - - - - < LCL
Cyromazine LC/MSMS - - - - 0.01
- - - - < LCL
DEET (Diethyl-m-toluamide,
N,N-)GC/MSMS - - - - - - - - - - < LCL
DDT-p,p GC/MSMS - - - - - -
- - - - < LCL
DDT-o,p GC/MSMS - - - - - - - - - - < LCL
DDE-p,p GC/MSMS - - - - - -
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE< LCL
Demeton S GC/MSMS - - - - 0.4
0.1 - - < LCL
Demeton O GC/MSMS - - - - - - - - - - < LCL
Deltamethrin GC/MSMS - - 0.1
0.1 0.02 < LCL
Demeton-s-methyl-sulfone
- - - - < LCLDialifos LC/MSMS - - - - - -
0.1 - - < LCL
Desmetryn GC/MSMS - - - - - - - - - - < LCL
Desmedipham LC/MSMS - - - - 0.01
- - - -
- - < LCL
Captan GC/MSMS 25 25 0.01 0.1 - - < LCL Diazinon GC/MSMS 0.75 0.75 0.1 0.1 0.1 < LCL
Carbaryl GC/MSMS 12 12 10 10 - - - - - -
0.01 0.120 5
0.01
0.2 < LCL
Carbetamide LC/MSMS - - - - 0.01 0.1 - - < LCL Diclobutrazol* LC/MSMS - - - - - - - - - - < LCL
Carbendazim LC/MSMSTHIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
TRAZAS
- - < LCL
Carboxin LC/MSMS - - - - 0.01 0.1 - - < LCL Dicrotophos LC/MSMS - - - - 0.01 0.1 - - < LCL
Carbofuran GC/MSMS - - - - 0.3 0.1 0.02 < LCL Diclofop methyl
0.05
0.02 < LCL
Chinometionate GC/MSMS - - - - 0.01 0.1 - - < LCL Diethofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL
Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL Dieldrin
0.01 2
Butocarboxim*
- - 0.01 0.1 - - < LCL
Chlorbromuron LC/MSMS - - - - - - - - - - < LCL Difenoxuron LC/MSMS - - - - - - - - - - < LCL
Chlorantraniliprole LC/MSMS 1.8 1.8 2 0.9 1 < LCL Difenoconazole
Butylate GC/MSMS - - - - 0.01 0.1 - - < LCL
Buturon LC/MSMS - - - - - -
Butocarboxim-sulfoxide LC/MSMS - - - - 0.01
- - - - < LCL
0.1 - - < LCL
0.1
- -- - - -
- -
GC/MSMS 0.05
GC/MSMS - -
GC/MSMS - -
< LCL Dichloran GC/MSMS - -
LC/MSMSOXYDEMETON
METHYL
METABOLITE
LC/MSMS
0.05 0.05 0.1
Dichlorvos
- - 0.01 0.1
- - 0.1 0.1
- - - - - -
- -
- -
0.02
< LCL- -
< LCL- -0.1
0.1 - - < LCL
Chlorsulfuron LC/MSMS - - - - 0.01
- -
0.01
LC/MSMSAminocarb
Chlorfluazuron LC/MSMS - - - - 2
0.01
0.1 0.05 < LCL
Ametoctradin LC/MSMS - - - - 0.01 0.1 Chlorpyrifos methyl GC/MSMS - - - - 0.05
Chlorpyrifos GC/MSMS - - - - 1
Chlorpropham GC/MSMS - - - - 0.01
< LCL
- -- -
0.1 - - < LCL
0.1 - - < LCL
0.1 - - < LCL
0.1 - - < LCL
Chloroxuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Chlorotoluron LC/MSMS - - - - 0.01
- - < LCL
- -- -
LC/MSMS - -
Página:
Muestra:
Huerto:
Cromatograma LC:
2 de 7
Zarzamora
LA TIJERA, LOS REYES MICH
P-18-24827 10-14-2018.d
0.02- -- -LC/MSMSClodinafop-propargyl
- - - - < LCL
Chlorothalonil GC/MSMS - - - - 10 0.1 - - < LCL
Chloropropylate GC/MSMS - - - - - -
KOR CHN
Crimidine LC/MSMS - - - - - - - - - - < LCL
Cyanazine LC/MSMS - - - - 0.01 0.1 - - < LCL
MX
0.01- -- -LC/MSMSClofentezine
- -0.1
- - < LCL
0.1 - - < LCL
Cloquintocet-mexyl
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto.
Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
B BB BB BB BB BR BB BB BB BB BB BB BB BB B
B B
B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B B
B B
B B
B B
B BB B
B B
B BB B
B B
B B
B B
B B
B B
B BB B
0.05
0.5 0.5
30 30
0.02
0.01 0.3
- -
0.02 0.02
0.01 1
- -
0.01 0.01
0.01
- -
0.01 0.05
0.01
0.05
0.01 0.3MALATHION
METABOLITE
MALATHION
METABOLITE
0.02 0.5
0.05 5
0.01 0.1
- - - -
0.01 0.05
4 3
0.02 1
0.01 1
0.1 - -
- -
- -
5 0.04
0.05
0.05
0.5 1
0.05 2
0.01 3
0.05 - -
- -
0.01 - -
0.01 - -
0.01 0.3
0.01 - -
- - - -
0.03 3
0.01 0.05
- - - -
- -
0.01 0.05
0.01 0.02
0.01
0.01 0.2
0.01
0.01
5
0.05
0.05
0.013
0.01
0.01
0.01
- -
0.05
0.02
0.1
0.02
0.02
0.01
0.01
0.01
0.02
0.01 0.3
0.01 0.05
0.05 0.5
0.01
0.01
0.01
0.01
0.01 0.5
0.01 - -
0.01 - -
0.7 0.5
- - - -
0.01 0.02
0.01 2
0.02 0.1
0.02 0.2
0.01 0.5
0.05 0.5
5 2
0.01 - -
- - - -
15 15
0.01 0.05
0.01 5
0.01 5
- - - -
0.02 0.02
- - - -
0.01 0.01
1 1
0.01 0.3
0.01 0.2
0.01 0.03
0.05 0.2
0.05 0.2
0.05 0.2
0.01 0.01
0.05 0.5
0.02 - -
- - - -
0.01 1
0.01 1
0.01 - -
0.01 0.05
0.01 0.1
0.01 0.1
0.01 1
0.01 - -
0.01 - -
KOR EU KOR
0.01 - -
- - - -
- - - -
0.01 - -
0.01 0.01
0.01 1
0.05 1
1
- -
5
0.05
0.3
- -0.7
CHN MX US JP CA
Revisión: AR271-TS-61
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Resultados de AnálisisSe han detectado residuos de pesticidas prohibidos
Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm) Cantidad obtenida en
mg/kg (ppm)Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
Reg. Sagarpa: SD
No. Reg. Lab.:
CHN
Fecha de reporte:
Cantidad obtenida en
mg/kg (ppm)MX US JP CA
Cliente: P-18-24827
Productor:
Cromatograma GC:
SUN BELLE MÉXICO S.A. DE
C.V.
NEFTALI ARMANDO
GONZALEZ VAZQUEZ
EU
< LCL
Dimefuron LC/MSMS - - - - - - - - - - < LCL Fluchloralin
LC/MSMS - - - - 0.01 0.1 - -Diflufenican LC/MSMS - - - - 0.01 0.1 - - < LCL Flubendiamide
< LCL
Dimethachlor LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenacet
GC/MSMS 5 5 5 7 - -
< LCL
Dimepax GC/MSMS - - - - - - - - - - < LCL Fludioxonil
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Dimethoate GC/MSMS - - - - 1 0.1 - - 0.251 Fluometuron
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Dimethenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flufenoxuron
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Diniconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoroglycofen-ethyl
LC/MSMS - - - - 0.01 0.1 - -< LCL
Dimethomorph LC/MSMS - - - - 0.01 0.1 - - < LCL Fluopicolide
LC/MSMS - - - - 0.02 0.1 - -
< LCL
Dioxathion GC/MSMS - - - - 0.01 0.1 - - < LCL Flurtamone
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Dinotefuran LC/MSMS - - - - 0.01 0.1 - - < LCL Fluoxastrobin
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Disulfoton GC/MSMS - - - - 0.05 0.1 - - < LCL Flutriafol
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Diphenamid LC/MSMS - - - - 0.01 0.1 - - < LCL Flusilazole
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Diuron (Karmex)* LC/MSMS 0.1 0.1 0.05 0.1 - - < LCL Folpet
GC/MSMS - - - - - - - - - -
< LCL
Disulfoton-sulfone LC/MSMS - - - - 0.05 0.1 - - < LCL Fluvalinate
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Dyfonate GC/MSMS - - - - 0.01 0.1 0.01 < LCL Formetanate
LC/MSMS - - - - 0.1 0.1 - -
< LCL
Dodemorph LC/MSMS - - - - 0.01 0.1 - - < LCL Forchlorfenuron
GC/MSMS - - - - 0.01 25 - -
< LCL
Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - - < LCL Furathiocarb
LC/MSMS - - - - 0.01 0.1 - -
< LCLLC/MSMS - - - - - - - - - -
Fuberidazole< LCL- -0.10.01- -- -LC/MSMSEdifenphos
< LCL
Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL Haloxyfop-methyl
GC/MSMS 0.1 0.1 0.02 0.1 0.02
< LCL
Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - - < LCL g Chlordan
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Endosulfan sulfate GC/MSMS - - - - 0.5 0.1 - - < LCL Heptachlor
LC/MSMS - - - - 0.05 0.1 - -
0.010.10.010.050.05GC/MSMS < LCL
0.05
0.01
< LCL
Epoxiconazole LC/MSMS - - - - 0.01 0.1 - - < LCL Heptenophos
GC/MSMS 0.05 0.05 0.01 0.1 0.01< LCL Heptachlor exo-epoxide (isomer 0.01
- -
< LCL
Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - - < LCL Hexaconazole
GC/MSMS 0.05 0.05 0.01 0.1 - -
< LCL
Esfenvalerate + Fenvalerate* (**) GC/MSMS 1 1 1 0.1 0.2 < LCL Hexachlorobenzene
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Ethiofencarb LC/MSMS - - - - 0.01 0.1 - - < LCL Hexythiazox
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Ethalfluralin GC/MSMS - - - - 0.01 0.1 - - < LCL Hexazinone
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Ethirimol LC/MSMS - - - - - - - - - - < LCL Imazapyr
LC/MSMS - - - - 0.02 0.1 - -
< LCL
Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - - < LCL Imazalil
LC/MSMS 1 1 0.01 1.5 - -
< LCL
Ethylan GC/MSMS - - - - - - - - - - < LCL Imidacloprid
LC/MSMS - - - - 0.05 0.1 - -
< LCL
Ethoprop GC/MSMS - - - - 0.01 0.1 0.02 < LCL Imazaquin
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Etofenprox GC/MSMS 5 5 0.01 0.1 - - < LCL Indoxacarb
GC/MSMS - - - - 0.1 0.1 - -
< LCL
Etion GC/MSMS - - - - 0.3 0.1 - - < LCL Imidan
LC/MSMS 2.5 2.5 4 2.5 - -
< LCL
Famoxadone LC/MSMS 10 10 10 10 - - < LCL Iprovalicarb
GC/MSMS 25 25 12 25 - -
< LCL
Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - - < LCL Iprodione
GC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenarimol LC/MSMS - - - - 1 0.1 - - < LCL Isazophos
LC/MSMS - - - - - - - - - -
< LCL
Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02 < LCL Irgarol
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenbuconazol LC/MSMS - - - - 0.01 0.1 - - < LCL Isoprocarb
LC/MSMS - - - - 0.01 0.1 0.01
< LCL
Fenazaquin LC/MSMS - - - - 0.01 0.1 - - < LCL Isofenphos
LC/MSMS - - - - 0.01 0.1 0.01
< LCL
Fenchlorphos GC/MSMS - - - - 0.01 0.1 - - < LCL Isoxaflutole
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - - < LCL Isoproturon
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenhexamid LC/MSMS 20 20 15 20 15 < LCL Kresoxim-methyl
GC/MSMS - - - - 3 3 - -
< LCL
Fenfuram LC/MSMS - - - - - - - - - - < LCL Kelthane***
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenoxaprop-ethyl LC/MSMS - - - - 0.1 0.1 - - < LCL Linuron
LC/MSMS - - - - 0.3 0.1 - -
< LCL
Fenitrothion GC/MSMS - - - - 0.8 0.1 0.5 < LCL Lenacil
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenpropathrin GC/MSMS 12 12 5 12 5 < LCL Malaoxon
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenoxycarb LC/MSMS - - - - 0.05 0.1 - - < LCL Lufenuron
LC/MSMS - - - - 0.2 0.1 - -
< LCL
Fenpropimorph LC/MSMS - - - - 0.05 0.1 - - < LCL Mancozeb
GC/MSMS 8 8 8 8 - -
< LCL
Fenpropidin LC/MSMS - - - - 0.01 0.1 - - < LCL Malathion
LC/MSMSMALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
Fenson GC/MSMS - - - - - - - - - - < LCL Mebendazole
LC/MSMS - - - - 0.01 0.1 - -
< LCL
Fenpyroximate LC/MSMS - - - - 0.01 0.1 - - < LCL Mandipropamid
LC/MSMS - - - - 5 0.1 5
Fenthion GC/MSMS - - - - 0.01 0.1 0.05 < LCL Mepanipyrim
LC/MSMS - - - - 0.01 0.1 - -
< LCL- - 0.01 0.1 - -0.01 0.2
Fensulfothion GC/MSMS - - - - 0.01 0.1 - - < LCL Mecarbam
0.1Methamidophos
Methabenzthiazuron
0.005 0.05
0.01 - -
- - - -
0.01 0.1 - -
- - - - - -
0.01 - -
< LCL Metconazole - - 0.01 0.1LC/MSMS
0.03 0.5
Fipronil GC/MSMS - - - - 0.01 0.1 0.02 < LCL Metamitron
GC/MSMS 0.7 0.7 0.2 0.1 - -
< LCL
- - < LCLMetalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)Fenuron LC/MSMS - - - - - -
LC/MSMS - - - - 0.2 0.1 0.05
< LCL
Fluazifop-butyl LC/MSMS - - - - 0.01 0.1 - - < LCL Methidathion
LC/MSMS - - - - 0.01 0.1 0.05Flonicamid LC/MSMS - -
< LCL
- - 0.01 0.1 - - < LCL
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LC/MSMS - -Flamprop methyl LC/MSMS - - - - 0.01 0.1 - - < LCL Metazachlor
LC/MSMS - -
2018-10-15
LC/MSMS - -
Endrin GC/MSMS - - - - 0.01 0.1 0.05
Flazasulfuron LC/MSMS - - - - 0.1 0.1 - - < LCL
- -
< LCL
Flamprop-isopropyl LC/MSMS - - - - - - - - - - - -
0.05
CHNKOR
< LCLLC/MSMS - - - - 0.01 0.1 - -
< LCL
- - 0.01 0.1 - -- -
0.4
- -
US JP CA EUMX
< LCL
< LCL
< LCLLC/MSMS - - - - - - - - - -
< LCL
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del
resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tacha duras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B B
B BB B
B B
B B
B B
B B
R B
B B
B B
B BB BB BB BB BB BB BB BB B
B B
B
B
B
B
B
BBBBBBBBBBBB
0.02 - -
0.01 - -
0.01 - -
- - - -
0.1 1
0.01 0.25
0.01 0.05
0.05 0.1
0.5
0.05 0.05
0.01 - -
0.01 - -
0.01 - -
3 0.5
3 3
0.01 1
0.5 1
0.01 0.05
0.01 - -
0.01 2
- - - -
- - 0.05
0.01 0.05
4 1
0.01 0.02
0.01 1
0.01 - -
0.05 1
0.01 2
0.01 2
- - - -
- - - -
- - - -
0.05 5
0.01 - -
0.01 0.5
- - - -
0.01 0.05
0.01 0.05
0.01 0.05
0.01 5
0.01 0.2
0.3
0.01 0.2
0.1 0.2
0.05 2
0.05 0.05
QUINTOCENE
(PENTACHLORONIT
ROBENZENE)META
BOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
- - - -
0.02 0.01
0.01 - -
- - - -
0.01 14
0.01 0.5
0.01 0.2
0.05 0.1
0.01 0.05
0.01 - -
- - - -
0.01 5
< LCL
Pentachloroanisol GC/MSMS - - - - - - - - - - < LCL
Pencycuron LC/MSMS - - - - 0.01 0.1 - - < LCL
< LCL
Pendimethalin
- - - - 0.01 0.1 - - < LCL
Simazine GC/MSMS 0.2 0.2 0.2 0.1 - - < LCL
LC/MSMS
LC/MSMS 0.1 0.1 0.05 0.1 - -
S-Metolachlor
LC/MSMS
< LCL
Simetryn
0.1 0.1 0.01 0.1 - -
Sethoxydim* LC/MSMS 5 5 1 5 - - < LCL
Profenofos GC/MSMS - - - - 0.01 0.1 - - < LCL
Profluoralin GC/MSMS - - - - - - - - - - < LCL
Promecarb GC/MSMS - - - - - - - -
Prometon GC/MSMS
Fecha de reporte: 2018-10-15 Revisión: AR271-TS-61
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Reg. Sagarpa: SD
No. Reg. Lab.:Cliente:
Productor:
Cromatograma GC:
SUN BELLE MÉXICO S.A. DE C.V.
NEFTALI ARMANDO GONZALEZ
VAZQUEZ
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Se han detectado residuos de pesticidas prohibidos
Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm) Cantidad obtenida en
mg/kg (ppm)Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
CHN
Cantidad obtenida
en mg/kg (ppm)MX US JP CA CHN MX US JP CAEU KOR EU KOR
Methiocarb GC/MSMS - - - - 0.05 0.1 - - < LCL Picoxystrobin
Methiocarb sulfoxide GC/MSMS - - - - 0.05 0.1 - - < LCL Piperonyl Butoxide
Methiocarb sulfone GC/MSMS - - - -
0.2 0.05
0.2 0.05
0.2 0.05
< LCL
0.1
LC/MSMS - - - - - - - -0.05 0.1 - - < LCL Piperalin
LC/MSMS - - - - 0.01
8 8LC/MSMS 8 8
0.01 1
- -
LC/MSMS - - - - 0.01 0.1
LC/MSMS - - - - 0.01 0.1
LC/MSMS
LC/MSMS - - - -
Methoxychlor GC/MSMS - - - - 7 0.1 - - < LCL
Metobromuron LC/MSMS
< LCL
Pirimiphos-ethyl
Primisulfuron-methyl
Piperophos
Methoprotryne LC/MSMS
0.2
- - - - - - - - - - < LCL Pirimicarb
Methomyl LC/MSMS - - - - 1 0.1
< LCLPirimiphos-methyl
- - - - 0.01 0.1
Methoxyfenozide LC/MSMS 6 6 0.01 6 - -
- - - - 0.01 0.1 - -
LC/MSMS
Metolcarb LC/MSMS - - - - 0.01 0.1 - - < LCL
< LCL< LCL
Metolachlor LC/MSMS - - - - 0.01 0.1 - - < LCL Prochloraz LC/MSMS - - - - 0.05 0.1 - - < LCL
Procymidone GC/MSMS - - - - 1.5 0.1
Metrafenone LC/MSMS - - - - 0.01 0.1 - - < LCL
Metoxuron LC/MSMS - - - - - - - - - - < LCL
Metosulam LC/MSMS - - - - 0.01 0.1 - - < LCL
Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL
Metsulfuron-methyl* LC/MSMS - - - - 0.01 0.1 - - < LCL
Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL0.1 0.05
0.01 - -
0.01 0.5
Monocrotophos LC/MSMS - - - - 0.01 0.1 0.03 < LCL
Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL
Mexacarbate LC/MSMS - - - - - - - - - - < LCL- - - -
0.01 - -
0.01 0.2
Myclobutanil GC/MSMS 2 2 1 2 - - < LCL
Monuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 - -
0.01 - -
1 1
Neburon LC/MSMS - - - - - - - - - - < LCL
Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL
N-2,4-Dimethylphenyl formamide
(2,4-DMPF)LC/MSMS - - - - - - - - - - < LCL- - - -
0.1 0.05
- - - -
Norflurazon LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL
Nitrapyrin GC/MSMS - - - - 0.01 0.1 - - < LCL
Nicosulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.3
0.01 0.2
0.01 0.1
Omethoate LC/MSMSDIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE0.226
Ofurace LC/MSMS - - - - - - - - - - < LCL
Novaluron* LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 1
- - - -
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL
Ovex GC/MSMS - - - - - - - - - - < LCL
op Dicofol*** GC/MSMS - - - - 3 3 - - < LCL0.02 1
- - - -
0.01 1
Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1 - - < LCL
Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL
Oxamyl LC/MSMS - - - - 0.01 0.1 - - < LCL0.01 0.5
0.01 - -
0.05 0.05
Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL
Paraoxon LC/MSMS - - - - - - - - - - < LCL
Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL0.5 0.05
- - - -
- - - -
GC/MSMS - - - - 0.02 0.1 - - < LCL
Parathion GC/MSMS - - - - 0.5 0.1 0.01 < LCL
Penconazol LC/MSMS - - - - 0.2 0.1 - - < LCL
Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL
0.05
< LCL
Permethrin GC/MSMS - - - - 1 0.1 1 < LCL
Pentachloroaniline GC/MSMS
QUINTOCENE
(PENTACHLORO
NITROBENZENE
)METABOLITE
QUINTOCENE
(PENTACHLORON
ITROBENZENE)M
ETABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE)
METABOLITE
QUINTOCENE
(PENTACHLORO
NITROBENZENE)
METABOLITE
QUINTOCENE
(PENTACHLORON
ITROBENZENE)M
ETABOLITE
Phenmedipham LC/MSMS - - - - 0.01 0.1 - -
Pentachlorophenol GC/MSMS - - - - 0.01 0.1 - - < LCL
Pentachloronitrobenzene
Phorate GC/MSMS - - - - 0.05 0.024 0.01 < LCL
Phenyl valerate GC/MSMS - - - - - - - - - - < LCL
Phenthoate LC/MSMS - - - - 0.01 0.1 - - < LCL
- - - - 0.01 0.1 - - < LCL
Phorate-sulfoxide LC/MSMS - - - - 0.05 0.024 0.01 < LCL
Phorate-sulfone LC/MSMS - - - - 0.05 0.024 0.01 < LCL
Picolinafen LC/MSMS - - - - 0.01 0.1 - - < LCL
- - - - - - - - - - < LCL
Phoxim LC/MSMS - - - - 0.02 0.1 0.05 < LCL
Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05 < LCL
Propachlor LC/MSMS - - - - 0.01 0.1
Phosalone LC/MSMS
Propamocarb LC/MSMS - - - - 0.05 0.1 - - < LCL
Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL
Pronamide LC/MSMS - - - - - - - - - - < LCL
0.01 0.05
- - - -
0.02 - -
0.01 0.1
- -
< LCL
- -
- -
- -
< LCL
< LCL
Propetamphos LC/MSMS - - - - 0.01 0.1 - - < LCL
Propanil LC/MSMS - - - - 0.1 0.1 - - < LCL
Propargite (Omite) LC/MSMS - - - - 0.01 0.1 - - < LCL
- -
0.01 0.1 - - < LCL
- - < LCL
0.1 0.1 - -
- - 0.5 0.1
< LCL
< LCL
- -
1
< LCL- -
< LCL
- - < LCL
- - < LCL
0.01 0.05
0.01 7
0.01 - -
0.01 - -
0.01
0.01 0.1 - -
- -
Resultados de análisis
Propazin GC/MSMS - - - - 0.01 0.1 - - < LCL
< LCL
Propiconazole GC/MSMS 1 1 0.05 1 - - < LCL
Propoxur LC/MSMS - - - - 1 0.1
Propyzamide LC/MSMS 0.05 0.05
- - 0.01 0.1 - -
Pyrimethanil
Pyriproxyfen
Quinalphos
Quinoxyfen
Prosulfocarb LC/MSMS - - - - 0.01 0.1 - -
- - - - 0.01 0.1 - -
- - - - 0.01 0.1 - -
4 4 3 3.5 - -
- - - -
Quizalofop-ethyl
Rimsulfuron
Rotenone
Sebuthylazine
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
GC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
GC/MSMS
Prosulfuron
Pymetrozine
Pyraclostrobin
Pyrazophos
Pyridaben
- - - - 0.05 0.1 - -
15 15 10 15 - -
1 1 0.01 0.1 - -
- - 0.01 0.1 - -
0.1 - -
15 15
0.05 1
0.01 0.01
0.05 0.05
- - - - - - - - - -
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
0.01 0.01 0.01 0.01 - -
- -
- - - - 0.02
- - - - 0.01 0.1 - -
KOR
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El re sultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del
resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166 -1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
BB BBBBBBBBBBBBBBBBBBBBBBBB
B
BBBBBBBBBBBBBBBBBBBBBBBBBBB
BB- - < LCLVinclozolin GC/MSMS - - - - 5 0.1 0.01 5
Vamidothion LC/MSMS - - - - 0.01 0.1 0.01 0.05 - -
< LCL
Trimidal LC/MSMS - - - - - - - - - - - - - - < LCL
< LCL
Terbumeton LC/MSMS
Terbacil GC/MSMS
Teflubenzuron LC/MSMS
Thiacloprid LC/MSMS
Tetramethrin LC/MSMS
Thiabendazole LC/MSMS
0.35 0.35
- -
Thidiazuron
Tetrahydrophthalimide, cis-1,2,3,6-(THPI) GC/MSMS
GC/MSMS
LC/MSMS
GC/MSMS
< LCL
Terbuthylazine
GC/MSMS
GC/MSMS
GC/MSMS
Terrazole
Tetradifon
Tetrachlorvinphos, E-isomer
Terbutryn
Terbuthylazine-desethyl
LC/MSMS
Thiamethoxam LC/MSMS
< LCL
- -
- - - - 0.01 - -0.1
0.1
0.01
0.01
- -
- - < LCL0.20.01
1
0.01
1 < LCL
3 - -
< LCL
- - - - - - < LCL
- - - - - - - -- -
< LCL- -
0.1
- - - - 0.01 0.05 - - < LCL
- - - -
0.01
Tebuthiuron LC/MSMS
1 1 1
- -
- -
< LCL
- - < LCL
- - - - 0.01 0.1
- -
0.05 - - < LCL
- -
- -
- - - -
- -
Spirodiclofen
Productor: NEFTALI ARMANDO GONZALEZ VAZQUEZ Huerto: LA TIJERA, LOS REYES MICH Reg. Sagarpa: SD
Cliente:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
US JP KOR CHNCA
Cantidad obtenida
en mg/kg (ppm)
Cromatograma LC:
EU
Fecha de reporte: 2018-10-15 Página: 5 de 7 Revisión:
SUN BELLE MÉXICO S.A. DE C.V. Muestra: Zarzamora No. Reg. Lab.: P-18-24827
AR271-TS-61
LC/MSMS
- - - - 0.01 0.2
- - - - 0.01 1
0.8 0.8 0.7 0.05
Spinosad A LC/MSMS
MX
1
0.5
0.5
Sumithrin GC/MSMS
- - < LCL
Sulfentrazone LC/MSMS
Spiroxamine LC/MSMS - - < LCL
0.15 0.15 0.05 - - - - < LCL
- - - - 0.01
Spirotetramat LC/MSMS
Spiromesifen LC/MSMS
0.1
Sulfotep LC/MSMS
Sulfosulfuron LC/MSMS
< LCL
- - < LCL
- - - - 0.01 - - 0.01 < LCL
- - - - 0.01 - -
Sulfoxaflor LC/MSMS
0.1
0.1
Tebufenozide LC/MSMS
Tebuconazole GC/MSMS
- -
- - - - 0.01 0.1 - -
0.5
0.053 3 3 1 - -
- - - - 0.01 0.5
- - - - 0.01
- - - - 0.01 - - - - < LCL
- - - - 2 0.5
0.1
0.05
0.01
< LCL
- - - - 0.01 1 - - < LCL
- - - -
CAPTAN METABOLITE
0.01
0.01
- -
0.1
0.1
- -
- -
0.2 0.2 0.1
- - - -
- -
0.01
- -
< LCL
- - 1 10.01
CAPTAN
METABOLITE
CAPTAN
METABOLITE
< LCL
< LCL
- -
0.01 0.05 - - < LCL0.1LC/MSMSThifensulfuron-methyl 0.01- -
- - - -
Triforine LC/MSMS - - - - 0.01 0.1 0.01 0.5
Triflusulfuron-methyl LC/MSMS - - - - 0.01 0.1 0.01
- -
- - - - 0.01 0.1
- - 3
- - 0.01
CAPTAN METABOLITE CAPTAN METABOLITE
0.5 1 - - < LCL
- - - - 5 0.70.1
0.5
- -
Tebutam LC/MSMS
Tebufenpyrad GC/MSMS
0.1
CAPTAN METABOLITECAPTAN
METABOLITE
< LCL
- -
- -
0.1
0.1
0.1
< LCL
0.1
0.1
0.1
0.1
< LCL- - - - 0.01 - - - -
< LCL1
1.5 1 < LCL
Se han detectado residuos de pesticidas prohibidos
US JP CA EU KOR
- -
P-18-24827 10-14-2018.d MX
Resultados de análisis
CHNCromatograma GC: P-18-24827 10-11-2018.D
Spinetoram J LC/MSMS
Analito
Analizado
mediante
equipo
Uso autorizado
LMR (ppm)
< LCL
< LCL
< LCL
- -
0.02
0.02
0.1
0.01
0.01
0.01
0.01
0.01
0.1 0.01
0.15
0.1
- -
0.5
0.01 1
0.02
- -
0.1
2
0.01 0.05 - - < LCL
Thiocyclam hydrogen oxalate GC/MSMS - - - - 3 0.1 0.01 1 - - < LCL
Thiobencarb LC/MSMS - - - - 0.01 0.1
< LCL
Thionazin LC/MSMS - - - - - - - - - - - - - - < LCL
Thiodicarb LC/MSMS - - - - 1 0.1 0.01 1 - -
< LCL
Tokution GC/MSMS - - - - - - - - - - - - - - < LCL
Thiophanate-methyl LC/MSMS - - - - 3 6 0.1 2 - -
< LCL
Triadimefon GC/MSMS - - - - 0.1 0.1 0.01 0.05 - - < LCL
Tolyfluanid GC/MSMS - - - - 5 0.1 0.02 2 5
< LCL
Triasulfuron LC/MSMS - - - - 0.01 0.1 0.05 - - - - < LCL
Triadimenol GC/MSMS - - - - 0.5 0.1 0.01 0.5 - -
< LCL
Tribenuron-methyl LC/MSMS - - - - 0.01 0.1 0.01 - - - - < LCL
Triazophos GC/MSMS - - - - 0.01 0.1 0.01 0.05 - -
0.05 0.2 < LCL
Trichloronate GC/MSMS - - - - - - - - - - - - - - < LCL
Trichlorfon LC/MSMS - - 0.5 0.1 0.01
< LCL
Tricyclazole GC/MSMS - - - - 0.02 0.1 0.01 0.05 - - < LCL
Triclocarban LC/MSMS - - - - - - - - - - - - - -
< LCL
Trifloxystrobin LC/MSMS - - - - 0.01 0.1 3 0.7 - - < LCL
Trietazine LC/MSMS - - - - - - - - - - - - - -
< LCL
Triflumuron LC/MSMS - - - - 0.02 0.1 0.05 0.5 - - < LCL
Triflumizole LC/MSMS - - - - 0.01 0.1 0.1 2 - -
< LCLTrifluralin GC/MSMS - - - - 0.05 0.1 0.01 0.05 - -
Atención: Análisis Técnicos S.A. de C.V no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V, por lo cual no se hace responsable de la representatividad del resultado para el total del producto.
Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto. Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Autoriza Lic. Carlos Sepúlveda Ibarra
Director General
*Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado. Las bandas de colores son de apoyo visual basadas en los LMRs de México y no representan un resultado. 1Límite Máximo de Residuos (LMR) expresados en ppm para cada país indicado en código ISO 3166-1 alfa-3. LCL = Lowest Calibration Level (Nivel Mínimo de Calibración) ppm = Partes por millón = mg/kg GC/MSMS =Cromatografía de Gases/Masas/Masas LC/MSMS = Cromatografía de Líquidos/MasasMasas Trazas/Traces = < 0.010 ppm.
Vamidothion 0.005
Malaoxon 0.005 Pentachloroaniline 0.010 Spinosad A 0.005
Lenacil 0.005 Penconazol 0.005 Simetryn 0.005
Kresoxim-methyl 0.005 Parathion methyl 0.010 Simazine 0.010
Vinclozolin 0.010
Triflusulfuron-methyl 0.005
Kelthane*** 0.010 Parathion 0.010 Sethoxydim* 0.010 Trimidal 0.005
Lufenuron 0.005 Pendimethalin 0.005 Spinetoram J 0.005
Isofenphos 0.005 Oxyfluorfen 0.010 Quizalofop-ethyl 0.005
Mancozeb 0.005 Pentachloronitrobenzene 0.010 Spiromesifen 0.005
Malathion 0.010 Pentachloroanisol 0.010 Spirodiclofen 0.005
Mebendazole 0.005 Permethrin 0.010 Spiroxamine 0.005
Mandipropamid 0.005 Pentachlorophenol 0.010 Spirotetramat 0.005
Mepanipyrim 0.010 Phenthoate 0.005 Sulfosulfuron 0.005Mecarbam 0.005 Phenmedipham 0.005 Sulfentrazone 0.005
Metamitron 0.005 Phorate 0.010 Sulfoxaflor 0.005
Metalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)0.010 Phenyl valerate 0.010 Sulfotep 0.005
0.005
Metconazole 0.005 Phorate-sulfoxide 0.005 Tebuconazole 0.010
Metazachlor 0.005 Phorate-sulfone 0.005 Sumithrin 0.020
Lowest Calibration Level (Nivel Mínimo de Calibración) por analitoAnalito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)
Methidathion 0.005 Phoxim 0.010 Tebutam 0.005
Methamidophos 0.005 Phosphamidon 0.005 Tebufenpyrad 0.010
Methabenzthiazuron 0.005 Phosalone 0.010 Tebufenozide
Fecha de reporte: 2018-10-15 Página: 6 de 7 Revisión:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
AR271-TS-61
Analito LCL (ppm)
Endosulfan I (alpha isomer) 0.010
2,3 dihydro-2,2dimethylbenzofuran 0.020 Butocarboxim-sulfoxide 0.005 Cyproconazole 0.005 Endosulfan II (beta isomer) 0.010
2, 4-D Methyl ester 0.010 Butocarboxim* 0.010Cypermethrin a (Zeta-
Cypermethrin)**0.010
Endosulfan sulfate 0.010
3,4 Dichloroaniline 0.010 Butylate 0.020 Cyromazine 0.005 Endrin 0.0102,6 Dichlorobenzonitrilo 0.010 Buturon 0.005 Cyprodinil 0.010
Epoxiconazole 0.005
Abamectin 0.005 Carbaryl 0.010 DDD-p,p 0.010 Esfenvalerate + Fenvalerate* (**) 0.0103-Hydroxy carbofuran 0.005 Captan 0.010 DDD-o,p 0.010
Etaconazole (Etaconazole I y II) 0.010
Acetamiprid 0.005 Carbetamide 0.005 DDE-p,p 0.010 Ethalfluralin 0.010Acephate 0.005 Carbendazim 0.005 DDE-o,p 0.010
Ethiofencarb 0.005
Acrinathrin 0.020 Carboxin 0.005 DDT-p,p 0.010 Ethiofencarb-sulfone 0.005Acetochlor 0.005 Carbofuran 0.010 DDT-o,p 0.010
Ethirimol 0.005
Aldicarb 0.005 Chinometionate 0.010 Deltamethrin 0.010 Ethoprop 0.010Alachlor 0.005 Carfentrazone ethyl 0.005 DEET (Diethyl-m-toluamide, N,N-) 0.010
Ethylan 0.010
Aldicarb-sulfoxide (Aldoxicarb) 0.005 Chlorbromuron 0.005 Demeton S 0.010 Etion 0.010Aldicarb sulfone 0.005 Chlorantraniliprole 0.005 Demeton O 0.010
Etofenprox 0.010
Ametoctradin 0.005 Chlordimeform 0.010 Desmedipham 0.005 Etoxazole 0.005Aldrin 0.010 Chlordane- a 0.010 Demeton-s-methyl-sulfone 0.005
Famoxadone 0.010
Aminocarb 0.005 Chlorfenvinphos 0.005 Dialifos 0.005 Fenamiphos 0.005Ametryn 0.010 Chlorfenapyr 0.010 Desmetryn 0.010
Fenarimol 0.005
Atrazine-2-hydroxy 0.005 Chloridazon (Pyrazon) 0.005 Dichloran 0.010 Fenazaquin 0.005Atrazine 0.010 Chlorfluazuron 0.005 Diazinon 0.010
Fenbuconazol 0.005
Azinphos-ethyl 0.005 Chlorobenzilate 0.010 Diclobutrazol* 0.010 Fenbutatin oxide* 0.010Azamethiphos 0.005 Chlormequat 0.005 Dichlorvos 0.010
Fenchlorphos 0.010
Azoxystrobin 0.010 Chloropropylate 0.010 Dicrotophos 0.005 Fenfuram 0.005Azinphos-methyl 0.010 Chloroneb 0.010 Diclofop methyl 0.020
Fenhexamid 0.005
Benalaxyl 0.010 Chlorotoluron 0.005 Diethofencarb 0.005 Fenitrothion 0.020Baycarb 0.005 Chlorothalonil 0.010 Dieldrin 0.010
Fenoxaprop-ethyl 0.005
Bensulfuron-methyl 0.005 Chlorpropham 0.010 Difenoxuron 0.005 Fenoxycarb 0.005Bendiocarb 0.005 Chloroxuron 0.005 Difenoconazole 0.005
Fenpropathrin 0.010
Benzoximate 0.005 Chlorpyrifos methyl 0.010 Dimefuron 0.005 Fenpropidin 0.005Bensulide 0.005 Chlorpyrifos 0.010 Diflufenican 0.005
Fenpropimorph 0.005
BHC lindane beta 0.010 Chlortal dimethyl 0.010 Dimethachlor 0.005 Fenpyroximate 0.005BHC lindane alpha 0.010 Chlorsulfuron 0.005 Dimepax 0.010
Fenson 0.020
BHC lindane gamma 0.010 Clodinafop-propargyl 0.005 Dimethoate 0.010 Fensulfothion 0.010BHC lindane delta 0.010 Chlorthiophos 0.020 Dimethenamid 0.005
Fenthion 0.010
Bifenox 0.020 Clomazone* 0.005 Diniconazole 0.005 Fenuron 0.005Bifenazate 0.005 Clofentezine 0.005 Dimethomorph 0.005
Fipronil 0.020
Bitertanol 0.005 Dioxathion 0.010 Flamprop methyl 0.010Bifenthrin 0.010 Cloquintocet-mexyl 0.005 Dinotefuran 0.005
Flamprop-isopropyl 0.010Coumaphos 0.010
Boscalid 0.005 Disulfoton 0.010 Flazasulfuron 0.005Bolstar 0.010 Diphenamid 0.005Crimidine 0.005
Cyanazine 0.005
Flonicamid 0.010
Bromophos methyl 0.010 Cyazofamid 0.005 Diuron (Karmex)* 0.010 Fluazifop-butyl 0.005Bromacil 0.010 Cyantraniliprole* 0.010 Disulfoton-sulfone 0.005
Flubendiamide 0.010
Bromuconazole* 0.010 Cyfluthrin 0.010 Dyfonate 0.010 Fluchloralin 0.020Bromopropylate 0.010 Cycloate 0.005 Dodemorph 0.005
Fludioxonil 0.010
Buprofezin 0.010 Cymoxanil 0.005 Emamectin Benzoate 0.005 Flufenacet 0.005
Bupirimate 0.005Cyhalothrin (Isomero Lambda y
gamma)**0.010 Edifenphos 0.005
Analito LCL (ppm)
Flufenoxuron 0.005 Methomyl 0.005 Piperonyl Butoxide 0.005 Terbumeton 0.005
Analito LCL (ppm) Analito LCL (ppm) Analito LCL (ppm)
Terbuthylazine 0.010
Fluopicolide 0.005 Methoxychlor 0.010 Pirimicarb 0.005 Terbuthylazine-desethyl 0.005
Fluometuron 0.005 Methoprotryne 0.005 Piperophos 0.005
Terbutryn 0.010
Fluoxastrobin 0.005 Metobromuron 0.010 Pirimiphos-methyl 0.005 Terrazole 0.010
Fluoroglycofen-ethyl 0.005 Methoxyfenozide 0.005 Pirimiphos-ethyl 0.005
Tetrachlorvinphos, E-isomer 0.010
Flusilazole 0.005 Metolcarb 0.010 Prochloraz 0.005 Tetradifon 0.010
Flurtamone 0.005 Metolachlor 0.005 Primisulfuron-methyl 0.005
Tetrahydrophthalimide, cis-1,2,3,6-
(THPI)0.010
Fluvalinate 0.010 Metoxuron 0.005 Profenofos 0.010 Tetramethrin 0.005
Flutriafol 0.005 Metosulam 0.005 Procymidone 0.010
Thiabendazole 0.005
Forchlorfenuron 0.005 Metribuzin 0.010 Promecarb 0.010 Thiacloprid 0.005
Folpet 0.010 Metrafenone 0.005 Profluoralin 0.020
Thiamethoxam 0.005
Fuberidazole 0.005 Mevinphos 0.010 Prometryn 0.010 Thidiazuron 0.005
Formetanate 0.005 Metsulfuron-methyl* 0.005 Prometon 0.010
0.010
Furathiocarb 0.005 Mexacarbate 0.005 Pronamide 0.005
Thiocyclam hydrogen oxalate 0.010
Thifensulfuron-methyl 0.005
g Chlordan 0.010 Mirex 0.010
Haloxyfop-methyl 0.005 Monocrotophos 0.005 Propamocarb 0.005
Propachlor 0.005 Thiobencarb
Propetamphos 0.005
Heptenophos 0.005 Myclobutanil 0.010
Heptachlor 0.010 Monolinuron 0.005 Propanil 0.005
Heptachlor exo-epoxide (isomer B) 0.010 Monuron 0.005 Propargite (Omite)
Propazin
0.005
0.010
Hexachlorobenzene 0.010N-2,4-Dimethylphenyl formamide
(2,4-DMPF)0.010
Hexazinone 0.010 Neburon 0.005 Propoxur 0.005
Hexaconazole 0.005 Napropamide 0.005 Propiconazole 0.010
Imazalil 0.005 Nitrapyrin 0.010 Prosulfocarb 0.005
Hexythiazox 0.005 Nicosulfuron 0.005 Propyzamide 0.005
Imazaquin 0.005 Novaluron* 0.010 Pymetrozine 0.005
Imazapyr 0.005 Norflurazon 0.005 Prosulfuron 0.005
Imidan 0.010 Omethoate 0.005 Pyrazophos 0.005
Imidacloprid 0.005 Ofurace 0.005 Pyraclostrobin 0.005
Iprodione 0.010 Ovex 0.010 Pyrimethanil 0.005
Indoxacarb 0.010 op Dicofol*** 0.010 Pyridaben 0.005
Irgarol 0.005 Oxamyl 0.005 Quinalphos 0.005
Iprovalicarb 0.005 Oxadixyl 0.005 Pyriproxyfen 0.010
Isazophos 0.010 Oxydemeton-methyl 0.005 Quinoxyfen 0.005
Sebuthylazine 0.010
Isoproturon 0.005 Paraoxon 0.005 Rotenone 0.005
Isoprocarb 0.005 Paclobutrazol (Bonzi) 0.005 Rimsulfuron 0.005
Isoxaflutole 0.010 Paraoxon-methyl 0.005
Methiocarb sulfoxide 0.020 Piperalin 0.005 Terbacil 0.010
Linuron 0.005 Pencycuron 0.005 S-Metolachlor 0.005
Methiocarb sulfone 0.020 Picoxystrobin 0.005 Teflubenzuron 0.010
Methiocarb 0.010 Picolinafen 0.005 Tebuthiuron 0.005
Thiodicarb
Thionazin
Thiophanate-methyl
Tokution
Tolyfluanid
Triadimefon
Triadimenol
Triasulfuron
Triazophos
0.005
0.005
0.005
0.010
0.010
0.010
0.010
0.005
0.010
Tribenuron-methyl
Trichlorfon
Trichloronate
Triclocarban
0.005
0.005
0.010
0.010
Triflumizole 0.005
Trifloxystrobin 0.005
Trietazine 0.005
Tricyclazole 0.010
Triforine 0.010
Triflumuron 0.010
Trifluralin 0.010
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A.
de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
ppm = Partes por millón = mg/kg Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed ". No. de Documento SANCO/10684/2009. Punto 91
International Maximum Residue Level Database
http://www.mrldatabase.com/
EU Pesticides Database
http://ec.europa.eu/sanco_pesticides/public/index.cfm
Electronic Code of Federal Regulation
http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?
Health Canada
http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php
Normas Alimentarias FAO/OMS
http://www.codexalimentarius.net/pestres/data/pesticides/search.html
Positive List System for Agricultural Chemical Residues in Foods (Japón)
http://m5.ws001.squarestart.ne.jp/foundation/search.html
Información correspondiente a la página 2, página 3, página 4 y página 5
Información correspondiente a la página 5 y 6
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Referencias
Glosario
Trazas = < 0.010 ppm.
MX= México
US= Estados Unidos
JP= Japón
CA= Canadá
EU= Union Europea
KOR=Corea
CHN= China
GC/MSMS = Gases/Masas/Masas AGILENT 225/MS, 240/MS
LC/MSMS = Líquidos/Masas/Masas QQQ (AGILENT 6460)
LCL = Lowest Calibration Level (Nivel Mínimo de Calibración)
LMR = Límite Máximo de Residuos
ppm = Partes por millón = mg/Kg
SD = Sin dato
1. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y
semillas (incorporando extracción QuEChERS), por cromatografia de GASES/MASAS/MASAS ante el sistema ISO/IEC 17015:2005. 7890
2. El laboratorio Análisis Técnicos S.A. de C.V. se encuentra acreditado ante la EMA, en el Ensayo de determinación de residuos de pesticidas en frutas, legumbres, alimentos agrícolas y
semillas (incorporando extracción QuEChERS), por cromatografia de LÍQUIDOS/MASAS/MASAS ante el sistema ISO/IEC 17015:2005.
3. * = Analito no declarado en el alcance acreditado y/o autorizado que se obtiene por método acreditado y/o autorizado.
4. Uso autorizado del plaguicida en el país correspondiente indicado en código ISO 3166-1 alfa-2. Los LMR de cada país se indican en la misma tabla de resultados.
5. En caso de no haber sido detectado algun pesticida se observa una banda verde fuerte. En caso de haber detectado algun pesticida dentro de los límites permitidos se observa una banda
amarilla. En caso de haber detectado algun pesticida fuera de los límites permitidos se observará una banda roja. En caso de haber detectado algún pesticida prohibido se observará una
banda roja.
6. Las bandas de colores son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.
7. ** = Se toma el LMR de Isomero Lambda para la molécula Cyhalothrin (Isomero Gamma y Lambda) , para Cypermethrin a (Zeta-Cypermethrin) se toma el LMR de Zeta-Cypermethrin y
para el LMR de Esfenvalerate + Fenvalerate se toma el de Esfenvalerate.
8. 2 = Para Canadá se considera el default LMR de 0.1 ppm según el punto 5.2.1.4.2 Food and Drug Regulations de Canada Food Inspection Agency http://www.inspection.gc.ca/food/meat-
and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.
9. Las bandas de colores de cada molécula son de apoyo visual basadas en los LMRs de cada país y no representan un resultado.
10. **El LMR de Dicofol es la suma de Kelthane(Dicofol) y op Dicofol
1. En las tablas correspondientes se presenta el punto más bajo de la calibración (LCL).
2. Las tablas correspondientes NO REPRESENTAN UN RESULTADO. Son datos informativos de calidad.
3.Incertidumbre = 50 % según "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91
Límites Máximos de Residuos (LMR) para Zarzamora indicados en El Catálogo Oficial
de Plaguicidas de México 2004.
Límites Máximos de Residuos (LMR) para Zarzamora indicados en Enviromental
Protection Agency (EPA) Estados Unidos.
Límites Máximos de Residuos (LMR) para Zarzamora indicados en Electronic Code of
Federal Regulations, (e-CFR TM) Estados Unidos.
1. El cliente tiene cinco días naturales posteriores a la emisión de resultados**** para poder hacer alguna observación o reclamación al respecto, ya que en caso de no hacerlo en este
periodo de tiempo se considerará este informe como aceptado.
2. Las muestras podrán ser desechadas a los 5 días después de la emisión de resultados****, únicamente las muestras para análisis microbiológico serán desechadas 24 h después de ser
recibidas.
3. La información inscrita en el presente "Informe de resultados de análisis" se trata con estricto apego al aviso de privacidad de Análisis Técnicos S.A. de C.V. acatando a los artículos
tercero transitorio, 16 y 17 de la Ley Federa de Protección de Datos Personales en Posesión de los Particulares, con la finalidad de regular su tratamiento legítimo, controlado e informado, a
efecto de garantizar la privacidad y el derecho a la autodeterminación informativa de las personas.
4. Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas.
5. Análisis Técnicos S.A. de C.V. no se encuentra acreditado en muestreo.
6. Los LMR de los paises son un dato de referencia, solicitando revisar los sitios oficiales de cada país ya que pueden cambiar o modificarse.
7. El resultado representa la muestra que fue recibida en las instalaciones de Análisis Técnicos S.A. de C.V., por lo cual no se hace responsable de la representatividad del resultado para el
total del producto
8. Este formato de interpretación está protegido y registrado ante el Instituto Nacional del Derecho de Autor (INDAUTOR), así mismo, los logotipos y nombre de Agrolab y sus filiales se
encuentran registrados ante el Instituto Mexicano de la propiedad Industrial (IMPI). Se prohibe su reproducción total o parcial, para otro fin que no sea la interpretación de resultados, sin
previa autorización.
9. El presente informe de resultados no será válido si presenta raspaduras, tachaduras o enmendaduras.
10. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
11. El laboratorio Análisis Técnicos S.A. de C.V. no es responsable de la actualización de los LMR's ya que son considerados como un dato informativo. Es responsabilidad del usuario del
Informe revisar los sitios oficiales para LMR de cada país ya que la información puede cambiar o modificarse.
12. La detección del residuo del plaguicida por arriba del límite de cuantificación se reporta como ppm (mg//Kg) , por debajo del límite de cuantificación se reportar como <LCL ppm (mg/Kg)
y por debajo del LD se considera como no determinado.
****La emisión del resultados, contempla el informe final destinado a ser enviado al cliente (PDF). La entrega de resultados al cliente, se encuentra sujeta a confirmación de pago.
13.La regla de decisión no incluye la incertidumbre.
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Información adicional y complementaria
Información general
Fecha de reporte: 2018-10-15 7 de 7 Revisión:Página:
Final del informe
AR271-TS-61
Atención: Análisis Técnicos S.A. de C.V. no tiene la autoridad, ni la facultad para negar, aceptar o autorizar cortes o cosechas. El resultado representa la muestra que fue recibida en las instalaciones de
Análisis Técnicos S.A. de C.V. , por lo cual no se hace responsable de la representatividad del resultado para el total del producto. Análisis Técnicos S.A de C.V no se hace responsable por el destino comercial o final que se le de al producto.
Este formato de interpretación esta protegido y registrado ante el Instituto Mexicano de la Propiedad Intelectual. Se prohibe su reproducción total o parcial sin autorización. El presente informe de resultados no será valido si presenta raspaduras, tachaduras o enmendaduras.
Documento controlado ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Report Date: 2018-10-15 Page: 1 of 7 Revision AR272-TS-61
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Client Information
Applicant: ALFREDO OSEGUERA DÍAZ Company: SUN BELLE MÉXICO S.A. DE C.V.
[email protected], [email protected],
Address: Km 1 Carr. los Reyes-Jacona S/N City or Town: Los Reyes
State: Michoacán ZIP Code: 60330
Telephone: 3545427328 Ext. 133 E-mail:
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Billing Information
Corporate name: Fruits-Giddings SA de CV RFC SBM040520QN6
Address: Km. 1 Carretera los Reyes- Jacona Sn City or Town: Los Reyes
State: Michoacán ZIP Code: 60330
Sample Reg. No. P-18-24827 Registry Book: oct-18
Receipt Date: 2018-10-11 Start Date: Termination Day: 2018-10-152018-10-11
Sample Information
Telephone: 3545420170 Ext. SD E-mail:[email protected], [email protected],
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Pesticides Multiresidual Analysis
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Tupy|Otras
Analyzed part: Fruit Sample status: Frozen Less Than 1.5Kg
Variety:
Amount recieved:
Common Name: Blackberry Scientific Name: Rubus Ulmifoli
Sampling Place: DIRECCION: LOS REYES,
MICHOACÁNSampling Method: Random SDWarehouse RFC:
Producer:NEFTALI ARMANDO GONZALEZ
VAZQUEZHarvest Place: LA TIJERA, LOS REYES MICH SDSAGARPA Reg.:
Commercial use: Human Commercial Destination: National And Foreign Market
Sampling date: 10/09/2018
Sample received in conditions for analysis.
2906-01 SECTOR 1
Final Destination:
Observations:
SDCustoms House:
USA AND EU
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the
representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad IntelectualIts total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
B B
B B
B B
B B
B B
B BB BB B
B B
B BB BB BB BB B
B B
B BB BB BB BB BB BB B
B B
B BB BB BB BB B
B B
B B
B B
B B
B V
B B
B B
B BB BB B
B B
B BB B
B B
B B
B B
B B
B B
B B
B BB BB BB B
B B
B B
B BB BB BB BB BB BB B
KOR CHN
1.5 0.5
3 1
- - - -
- - - -
0.01 0.1
- - - -
0.01 0.05
- - - -
0.05 0.1
0.01 - -
0.01 0.01
0.01 2
- - - -
- - - -
- - - -
0.7
0.01 - -
0.02 1
- - - -
0.01 0.1
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL METABOLITE
0.01 - -
- - - -
0.2 0.5
0.01 0.5
0.5 2
0.05 0.1
0.05 0.05
- - - -
- - - -
- - - -
- -
0.01 1
0.01 - -
0.01 - -
0.01 0.05
- - - -
0.01 0.4
0.01 1
0.05 0.1
- - - -
- - - -
0.02 - -
3 1
0.01 0.05
- - - -
0.02
0.01 - -
0.01 0.5
0.01 0.05
0.01 0.3
0.1 - -
0.01 1
0.02 0.02
0.01 - -
20 5
0.01 0.5
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
0.01 - -
0.01 0.05
0.05 0.05
1 0.7
- - - -
0.01
- -
0.1
- - - -
10 5
0.01 0.1
- - - -
0.01 5
0.05 - -
1.5 - -
0.05 1
0.01 - -
0.01 0.5
0.01 0.01
0.01 0.01
0.01 0.01
0.01 0.01
7 7
0.01 0.05
1 1
0.01 1
- - - -
0.01 - -
0.02 - -
0.05 0.3
5 1
- - - -
0.05 0.05
0.01 0.02
0.01 0.02
0.01 0.05
0.02 0.02
0.02 0.02
0.02 0.02
0.01 0.01
0.01 0.05
0.01 - -
- - - -
0.05 - -
- - - -
- - - -
LINURON
METABOLITELINURON METABOLITE
- - - -
0.08 0.05
0.01 1
2 0.3
0.01 0.02
0.02 1
Report Date: 2018-10-15 Page: 2 of 7 Revision: AR272-TS-61
Chromatogram GC: P-18-24827 10-11-2018.D Chromatogram LC: P-18-24827 10-14-2018.d
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Analysis Results
Producer:NEFTALI ARMANDO GONZALEZ
VAZQUEZOrchard: LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD
Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-18-24827
US JPMX CA EU
JP CA CHN
2, 4-D Methyl ester GC/MSMS 0.2 0.2 0.1 0.1 0.1
US JP CA CHN MX US
Banned pesticides residues have been detected
Analyte Analyzed by
Authorized use
MRL (ppm) Obtained amount in mg/kg
(ppm)Analyte Analyzed by
Authorized use
MRL (ppm) Obtained amount in mg/kg
(ppm)MX EU KOR EU KOR
0.1 0.05
0.1 0.01 < LCL
2,6 Dichlorobenzonitrilo GC/MSMS - - - - - - - - - -
< LCL Chlordimeform GC/MSMS - - - - 0.01
0.1 0.02 < LCL
2,3 dihydro-2,2dimethylbenzofuran 7-ol GC/MSMS - - - - - - - - - -
< LCL Chlordane- a GC/MSMS 0.1 0.1 0.02
0.1 - - < LCL
3-Hydroxy carbofuran LC/MSMS - - - - - - - - - -
< LCL Chlorfenvinphos LC/MSMS - - - - 0.05
0.1 - - < LCL
3,4 Dichloroaniline GC/MSMS LINURON METABOLITELINURON
METABOLITE
LINURON
METABOLITE
LINURON
METABOLITELINURON METABOLITE
< LCL Chlorfenapyr GC/MSMS - - - - 0.01
0.1 - - < LCL
Acephate LC/MSMS - - - - 0.01 0.1 0.5
< LCL Chloridazon (Pyrazon) LC/MSMS - - - - 0.01
0.1 - - < LCL
Abamectin LC/MSMS 0.2 0.2 0.01 0.2 - -
< LCL Chlorfluazuron LC/MSMS - - - - 2
0.1 - - < LCL
Acetochlor LC/MSMS - - - - 0.01 0.1 - -
< LCL Chlorobenzilate GC/MSMS - - - - 0.01
0.1 - - < LCL
Acetamiprid LC/MSMS 1.6 1.6 2 4 2
< LCL Chlormequat LC/MSMS - - - - 0.05
- - - - < LCL
Alachlor LC/MSMS - - - - 0.01 0.1 - -
< LCL Chloropropylate GC/MSMS - - - - - -
0.1 - - < LCL
Acrinathrin GC/MSMS - - - - 2 0.1 - -
< LCL Chloroneb GC/MSMS - - - - 0.01
0.1 - - < LCL
Aldicarb sulfone LC/MSMS - - - - 0.01 0.1 0.02
< LCL Chlorotoluron LC/MSMS - - - - 0.01
0.1 - - < LCL
Aldicarb LC/MSMS - - - - 0.01 0.1 0.02
< LCL Chlorothalonil GC/MSMS - - - - 10
0.1 - - < LCL
Aldrin GC/MSMS 0.05 0.05 0.05 0.1 0.05
< LCL Chlorpropham GC/MSMS - - - - 0.01
0.1 - - < LCL
Aldicarb-sulfoxide (Aldoxicarb) LC/MSMS - - - - 0.01 0.1 0.02
< LCL Chloroxuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Ametryn GC/MSMS - - - - 0.01 0.1 - -
< LCL Chlorpyrifos methyl GC/MSMS - - - - 0.05
0.1 - - < LCL
Ametoctradin LC/MSMS - - - - 0.01 0.1 - -
< LCL Chlorpyrifos GC/MSMS - - - - 1
- - - - < LCL
Atrazine GC/MSMS - - - - 0.02 0.1 - -
< LCL Chlortal dimethyl GC/MSMS - - - - - -
0.1 - - < LCL
Aminocarb LC/MSMS - - - - - - - - - -
< LCL Chlorsulfuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Azamethiphos LC/MSMS - - - - 0.01 0.1 - -
< LCL Clodinafop-propargyl LC/MSMS - - - - 0.02
- - - - < LCL
Atrazine-2-hydroxy LC/MSMS - - - - - - - - - -
< LCL Chlorthiophos GC/MSMS - - - - - -
0.1 - - < LCL
Azinphos-methyl GC/MSMS - - - - 0.01 2 1
< LCL Clomazone* LC/MSMS - - - - 0.02
0.1 - - < LCL
Azinphos-ethyl LC/MSMS - - - - 0.01 0.1 - -
< LCL Clofentezine LC/MSMS - - - - 0.01
< LCL
0.1 - - < LCL
Azoxystrobin GC/MSMS 5 5 5 5 - -
< LCL Cloquintocet-mexyl LC/MSMS - - - - 0.01
Coumaphos GC/MSMS - - - - - - 0.1 0.05 < LCL0.01 - -
< LCLBenalaxyl GC/MSMS - - - - 0.05 0.1 - -
0.02 - -
Baycarb LC/MSMS - - - - - - - - - - < LCL Crimidine LC/MSMS - - - - - - - - - -
0.1 - -
- - - -
0.01 - -
0.01 < LCL
Bensulfuron-methyl LC/MSMS - - - - 0.01 0.1 - -
< LCL Cyantraniliprole* LC/MSMS - - - - 0.01Bendiocarb LC/MSMS - - - - 0.01 0.1 - - 0.7
0.01 2
0.1 - - < LCL
Benzoximate LC/MSMS - - - - 0.01 0.1 - -
< LCL Cycloate LC/MSMS - - - - 0.01
< LCL
Bensulide LC/MSMS - - - - 0.01 0.1 - -
< LCL Cyazofamid LC/MSMS - - - - 0.01
0.01 - -
0.01 0.2 < LCL
BHC lindane beta GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCLCyhalothrin (Isomero Lambda
y gamma)**GC/MSMS - - - - 0.5
0.1 - - < LCL
BHC lindane alpha GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCL Cyfluthrin GC/MSMS - - - - 0.02
0.1 - - 0.013
BHC lindane gamma GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCLCypermethrin a (Zeta-
Cypermethrin)**GC/MSMS 0.8 0.8 0.5
4 - - < LCL
BHC lindane delta GC/MSMS 0.5 0.5 0.3 0.1 - -
< LCL Cymoxanil LC/MSMS 4 4 4
10 - - < LCL
Bifenox GC/MSMS - - - - 0.01 0.1 - -
< LCL Cyprodinil GC/MSMS 10 10 10
0.1 - - < LCL
Bifenazate LC/MSMS 5 5 7 5 7
< LCL Cyproconazole LC/MSMS - - - - 0.5
- - - - < LCL
Bitertanol LC/MSMS - - - - 0.05 0.1 - -
< LCL DDD-o,p GC/MSMS - - - - - -
0.1 - - < LCL
Bifenthrin GC/MSMS 1 1 1 1 1
< LCL Cyromazine LC/MSMS - - - - 0.01
- - - - < LCL
Boscalid LC/MSMS 10 10 10 6 - -
< LCL DDE-o,p GC/MSMS - - - - - -
- - - - < LCL
Bolstar GC/MSMS - - - - - - - - - -
< LCL DDD-p,p GC/MSMS - - - - - -
- - - - < LCL
Bromophos methyl GC/MSMS - - - - - - - - - -
< LCL DDT-o,p GC/MSMS - - - - - -
- - - - < LCL
Bromacil GC/MSMS - - - - 0.01 0.1 - -
< LCL DDE-p,p GC/MSMS - - - - - -
- - - - < LCL
Bromuconazole* LC/MSMS - - - - 0.01 0.1 - -
< LCLDEET (Diethyl-m-toluamide,
N,N-)GC/MSMS - - - - - -
- - - - < LCL
Bromopropylate GC/MSMS - - - - 2 0.1 - -
< LCL DDT-p,p GC/MSMS - - - - - -
- - - - < LCL
Buprofezin GC/MSMS - - - - 0.01 0.1 - -
< LCL Demeton O GC/MSMS - - - - - -
0.1 - - < LCL
Bupirimate LC/MSMS - - - - 0.01 0.1 - -
< LCL Deltamethrin GC/MSMS - - - - 0.1
OXYDEMETON
METHYL
METABOLITE
< LCL
Butocarboxim-sulfoxide LC/MSMS - - - - 0.01 0.1 - -
< LCL Demeton-s-methyl-sulfone LC/MSMSOXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
OXYDEMETON
METHYL
METABOLITE
0.1 0.02 < LCL
Butocarboxim* LC/MSMS - - - - 0.01 0.1 - -
< LCL Demeton S GC/MSMS - - - - 0.4
0.01
0.1 - -
< LCL Desmetryn GC/MSMS - - - - - -
0.1 - - < LCL
Buturon LC/MSMS - - - - - - - - - -
< LCL Desmedipham LC/MSMS - - - - 0.01- -
- - - -
0.01 - -
12 12 10 10 - -
< LCL Diazinon GC/MSMS 0.75 0.75 0.1
- - - - < LCL
Captan GC/MSMS 25 25 0.01 0.1 - -
< LCL Dialifos LC/MSMS - - - - - -Butylate GC/MSMS - - - - 0.01
Carbetamide LC/MSMS - - - - 0.01 0.1 - -
TRACES Dichlorvos GC/MSMS - - - - 0.1
- - - - < LCL
Carbendazim LC/MSMSTHIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
THIOPHANATE
METHYL/ BENOMYL
METABOLITE
< LCL Dichloran GC/MSMS - - - - - -
< LCL
Carbaryl GC/MSMS
- - 0.01 0.1 - -
- - < LCL
Carboxin LC/MSMS - - - - 0.01 0.1 - -
< LCL Diclofop methyl GC/MSMS - - - - 0.01Carbofuran GC/MSMS - - - - 0.3 0.1 0.02 0.1
0.1 0.02 < LCL< LCL Dieldrin
1.8 2 0.9 1
0.05 0.05
0.1 - - < LCL
0.1 - - < LCL
Carfentrazone ethyl LC/MSMS 0.1 0.1 0.1 0.1 - -
< LCL Dicrotophos LC/MSMS - - - - 0.01
0.01 0.1
0.01 0.05Chinometionate GC/MSMS - -
< LCL Difenoxuron LC/MSMS - - - - - -
0.1 - - < LCL
< LCL Diethofencarb LC/MSMS - - - - 0.01
Chlorbromuron LC/MSMS - - - - - - - - - -
< LCL Difenoconazole LC/MSMS - - - - 0.01Chlorantraniliprole LC/MSMS 1.8
GC/MSMS 0.05
< LCL
Cyanazine LC/MSMS - - - - 0.01 0.1 - - < LCL
- - - - < LCL
- - - - < LCLDiclobutrazol* LC/MSMS - - - - - -
0.1 0.2 < LCL
0.1 0.1 < LCL
- - - - < LCL
OXYDEMETON
METHYL
METABOLITE
* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.
Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
B BB BB BB BB BR BB BB BB BB BB BB BB BB B
B B
B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B B
B B
B B
B B
B BB B
B B
B BB B
B B
B B
B B
B B
B B
B BB B
0.01 0.3MALATHION
METABOLITE
MALATHION
METABOLITE
0.02 0.5
0.02 0.01
0.05 5
0.01 0.1
- - - -
0.01 0.05
4 3
0.02 - -
0.1 - -
0.02 - -
0.02 0.4
0.01 0.02
0.01 0.3
0.01 1
0.01 1
0.1 - -
0.05 0.05
0.01 - -
0.02 0.02
0.02 1
0.01 - -
0.01 0.05
0.01 0.05
0.5 1
0.05 2
0.01 3
30 30
- - - -
0.01 0.01
0.05 - -
5 0.04
0.05 0.05
0.5 0.5
0.01 - -
- - - -
0.03 3
0.01 0.05
- - - -
0.01 - -
0.01 0.05
0.01 0.02
0.01 0.05
0.01 0.01
0.01 0.01
0.01 - -
0.01 - -
- - - -
0.01 - -
0.03 0.5
0.01 0.2
0.01 1
0.01 - -
5 5
0.05 0.05
0.05 0.3
0.01 - -3 0.7
0.01 - -
0.01 - -
0.01 - -
0.01 0.3
0.01 0.5
0.01 - -
0.01 - -
0.7 0.5
- - - -
0.01 0.02
- - - -
0.02 0.02
- - - -
0.01 0.01
1 1
0.01 0.3
0.01 2
0.01 0.2
- - - -
0.005 0.05
0.01 0.5
0.05 0.5
5 2
0.01 - -
- - - -
15 15
0.01 0.3
0.01 0.05
0.05 0.5
0.02 0.1
0.02 0.2
0.05 0.2
0.05 0.2
0.01 0.01
0.05 0.5
0.02 - -
- - - -
0.01 0.05
0.01 5
0.01 5
0.01 0.05
0.01 0.1
0.01 0.1
0.01 1
0.01 - -
0.01 - -
0.01 0.2
0.01 0.03
0.05 0.2
- - - -
- - - -
0.01 - -
0.01 0.01
0.01 1
0.05 1
0.01 1
0.01 1
0.01 - -
Report Date: 2018-10-15 Page: 3 of 7 Revision: AR272-TS-61
Chromatogram GC: P-18-24827 10-11-2018.D Chromatogram LC: P-18-24827 10-14-2018.d
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Analysis Results
Producer:NEFTALI ARMANDO
GONZALEZ VAZQUEZOrchard: LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD
Client:SUN BELLE MÉXICO S.A. DE
C.V.Sample: Blackberry Lab Reg. No.: P-18-24827
US JP CA EUMX
JP CA CHN
Diflufenican LC/MSMS - - - - 0.01 0.1 - -
US JP CA CHN MX US
Banned pesticides residues have been detected
AnalyteAnalyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)Analyte
Analyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)MX EU KOR EU KOR
0.01 - -
0.1 - - < LCL
Dimepax GC/MSMS - - - - - - - - - -
< LCL Fluchloralin GC/MSMS - - - - 0.01
0.1 - - < LCL
Dimefuron LC/MSMS - - - - - - - - - -
< LCL Flubendiamide LC/MSMS - - - - 0.01
0.1 - - < LCL
Dimethenamid LC/MSMS - - - - 0.01 0.1 - -
< LCL Flufenacet LC/MSMS - - - - 0.01
7 - - < LCL
Dimethachlor LC/MSMS - - - - 0.01 0.1 - -
< LCL Fludioxonil GC/MSMS 5 5 5
0.1 - - < LCL
Dimethomorph LC/MSMS - - - - 0.01 0.1 - -
0.251 Fluometuron LC/MSMS - - - - 0.02
0.1 - - < LCL
Dimethoate GC/MSMS - - - - 1 0.1 - -
< LCL Flufenoxuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Dinotefuran LC/MSMS - - - - 0.01 0.1 - -
< LCL Fluoroglycofen-ethyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Diniconazole LC/MSMS - - - - 0.01 0.1 - -
< LCL Fluopicolide LC/MSMS - - - - 0.01
0.1 - - < LCL
Diphenamid LC/MSMS - - - - 0.01 0.1 - -
< LCL Flurtamone LC/MSMS - - - - 0.01
0.1 - - < LCL
Dioxathion GC/MSMS - - - - 0.01 0.1 - -
< LCL Fluoxastrobin LC/MSMS - - - - 0.01
0.1 - - < LCL
Disulfoton-sulfone LC/MSMS - - - - 0.05 0.1 - -
< LCL Flutriafol LC/MSMS - - - - 0.01
0.1 - - < LCL
Disulfoton GC/MSMS - - - - 0.05 0.1 - -
< LCL Flusilazole LC/MSMS - - - - 0.01
25 - - < LCL
Dodemorph LC/MSMS - - - - 0.01 0.1 - -
< LCL Folpet GC/MSMS - - - - 0.01
- - - - < LCL
Diuron (Karmex)* LC/MSMS 0.1 0.1 0.05 0.1 - -
< LCL Fluvalinate GC/MSMS - - - - - -
- - - - < LCL
Edifenphos LC/MSMS - - - - 0.01 0.1 - -
< LCL Formetanate LC/MSMS - - - - - -
0.1 - - < LCL
Dyfonate GC/MSMS - - - - 0.01 0.1 0.01
< LCL Forchlorfenuron LC/MSMS - - - - 0.1
0.1 - - < LCL
Endosulfan I (alpha isomer) GC/MSMS - - - - 0.5 0.1 - -
< LCL Furathiocarb LC/MSMS - - - - 0.01
0.1 - - < LCL
Emamectin Benzoate LC/MSMS - - - - 0.1 0.1 - -
< LCL Fuberidazole LC/MSMS - - - - 0.01
0.1 - - < LCL
Endosulfan sulfate GC/MSMS - - - - 0.5 0.1 - -
< LCL Haloxyfop-methyl LC/MSMS - - - - 0.05
0.1 0.02 < LCL
Endosulfan II (beta isomer) GC/MSMS - - - - 0.5 0.1 - -
< LCL g Chlordan GC/MSMS 0.1 0.1 0.02
0.1 0.01 < LCL
Epoxiconazole LC/MSMS - - - - 0.01 0.1 - -
< LCL Heptachlor exo-epoxide (isomer GC/MSMS 0.05 0.05 0.01
0.1 0.01 < LCL
Endrin GC/MSMS - - - - 0.01 0.1 0.05
< LCL Heptachlor GC/MSMS 0.05 0.05 0.01
0.1 - - < LCL
Etaconazole (Etaconazole I y II) LC/MSMS - - - - - - - - - -
< LCL Hexachlorobenzene GC/MSMS 0.05 0.05 0.01
0.1 - - < LCL
Esfenvalerate + Fenvalerate* (**) GC/MSMS 1 1 1 0.1 0.2
< LCL Heptenophos LC/MSMS - - - - 0.01
0.1 - - < LCL
Ethiofencarb LC/MSMS - - - - 0.01 0.1 - -
< LCL Hexazinone GC/MSMS - - - - 0.01
0.1 - - < LCL
Ethalfluralin GC/MSMS - - - - 0.01 0.1 - -
< LCL Hexaconazole LC/MSMS - - - - 0.01
0.1 - - < LCL
Ethirimol LC/MSMS - - - - - - - - - -
< LCL Imazalil LC/MSMS - - - - 0.02
1.5 - - < LCL
Ethiofencarb-sulfone LC/MSMS - - - - 0.01 0.1 - -
< LCL Hexythiazox LC/MSMS 1 1 0.01
0.1 - - < LCL
Ethylan GC/MSMS - - - - - - - - - -
< LCL Imazaquin LC/MSMS - - - - 0.05
0.1 - - < LCL
Ethoprop GC/MSMS - - - - 0.01 0.1 0.02
< LCL Imazapyr LC/MSMS - - - - 0.01
0.1 - - < LCL
Etofenprox GC/MSMS 5 5 0.01 0.1 - -
< LCL Imidan GC/MSMS - - - - 0.1
2.5 - - < LCL
Etion GC/MSMS - - - - 0.3 0.1 - -
< LCL Imidacloprid LC/MSMS 2.5 2.5 4
25 - - < LCL
Famoxadone LC/MSMS 10 10 10 10 - -
< LCL Iprodione GC/MSMS 25 25 12
0.1 - - < LCL
Etoxazole LC/MSMS 1.5 1.5 0.01 1.5 - -
< LCL Indoxacarb GC/MSMS - - - - 0.01
- - - - < LCL
Fenarimol LC/MSMS - - - - 1 0.1 - -
< LCL Irgarol LC/MSMS - - - - - -
0.1 - - < LCL
Fenamiphos LC/MSMS - - - - 0.02 0.1 0.02
< LCL Iprovalicarb LC/MSMS - - - - 0.01
0.1 0.01 < LCL
Fenbuconazol LC/MSMS - - - - 0.01 0.1 - -
< LCL Isofenphos LC/MSMS - - - - 0.01
0.1 0.01 < LCL
Fenazaquin LC/MSMS - - - - 0.01 0.1 - -
< LCL Isazophos LC/MSMS - - - - 0.01
0.1 - - < LCL
Fenchlorphos GC/MSMS - - - - 0.01 0.1 - -
< LCL Isoproturon LC/MSMS - - - - 0.01
0.1 - - < LCL
Fenbutatin oxide* LC/MSMS - - - - 1 0.1 - -
< LCL Isoprocarb LC/MSMS - - - - 0.01
3 - - < LCL
Fenhexamid LC/MSMS 20 20 15 20 15
< LCL Kelthane*** GC/MSMS - - - - 3
0.1 - - < LCL
Fenfuram LC/MSMS - - - - - - - - - -
< LCL Isoxaflutole LC/MSMS - - - - 0.01
0.1 - - < LCL
Fenoxaprop-ethyl LC/MSMS - - - - 0.1 0.1 - -
< LCL Lenacil LC/MSMS - - - - 0.3
0.1 - - < LCL
Fenitrothion GC/MSMS - - - - 0.8 0.1 0.5
< LCL Kresoxim-methyl LC/MSMS - - - - 0.01
0.1 - - < LCL
Fenpropathrin GC/MSMS 12 12 5 12 5
< LCL Lufenuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Fenoxycarb LC/MSMS - - - - 0.05 0.1 - -
< LCL Linuron LC/MSMS - - - - 0.2
8 - - < LCL
Fenpropimorph LC/MSMS - - - - 0.05 0.1 - -
< LCL Malathion GC/MSMS 8 8 8
MALATHION
METABOLITE
MALATHION
METABOLITE< LCL
Fenpropidin LC/MSMS - - - - 0.01 0.1 - -
< LCL Malaoxon LC/MSMSMALATHION
METABOLITE
MALATHION
METABOLITE
MALATHION
METABOLITE
0.1 - - < LCL
Fenson GC/MSMS - - - - - - - - - -
< LCL Mandipropamid LC/MSMS - - - - 0.01
0.1 5 < LCL
Fenpyroximate LC/MSMS - - - - 0.01 0.1 - -
< LCL Mancozeb LC/MSMS - - - - 5
0.1 - - < LCL
Fenthion GC/MSMS - - - - 0.01 0.1 0.05
< LCL Mecarbam LC/MSMS - - - - 0.01
- - - - < LCL
Fensulfothion GC/MSMS - - - - 0.01 0.1 - -
< LCL Mebendazole LC/MSMS - - - - - -
0.1 - - < LCL
Fipronil GC/MSMS - - - - 0.01 0.1 0.02
< LCLMetalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)GC/MSMS 0.7 0.7 0.2
0.1 - - < LCL
Fenuron LC/MSMS - - - - - - - - - -
< LCL Mepanipyrim LC/MSMS - - - - 0.01
0.1 - - < LCL
Flamprop-isopropyl LC/MSMS - - - - - - - - - -
< LCL Metazachlor LC/MSMS - - - - 0.01
0.1 - - < LCL
Flamprop methyl LC/MSMS - - - - 0.01 0.1 - -
< LCL Metamitron LC/MSMS - - - - 0.01
LC/MSMS - - - - 0.01 0.1 - -
< LCL Methabenzthiazuron LC/MSMS - - - - 0.01
0.1 - - < LCL
Flazasulfuron LC/MSMS - - - - 0.1 0.1 - -
< LCL Metconazole LC/MSMS - - - - 0.01
0.01 0.05
0.01 0.1
CHNKOR
0.1 0.05 < LCL< LCL Methidathion LC/MSMS - - - - 0.2
0.1 0.05 < LCL
Fluazifop-butyl LC/MSMS - - - - 0.01 0.1 - -
< LCL Methamidophos LC/MSMS - - - - 0.01
0.1 - - < LCL
Flonicamid
*Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it´s not responsible for the
representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
B BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB BB B
B B
B B
B BB B
B B
B B
B B
B B
R B
B B
B B
B BB BB BB BB BB BB BB BB B
B B
B
B
B
B
B
BBBBBBBBBBBB
0.02 - -
0.05 0.1
0.05 1
0.01 0.01
0.05 0.05
0.01 - -
0.01 - -
- - - -
0.1 1
0.01 0.25
0.01 0.05
0.01 0.05
0.01 7
0.01 - -
0.01 - -
0.01 0.5
0.05 0.05
0.01 - -
0.01 - -
0.01 - -
0.01 2
0.01 2
- - - -
- - - -
- - - -
0.01 0.05
- - - -
0.02 - -
0.01 0.1
0.01 - -
0.05 5
0.01 - -
0.01 0.5
- - - -
0.01 0.05
0.01 0.05
0.01 0.05
0.01 5
- - - -
0.05 0.3
0.01 0.2
0.1 0.2
0.05 2
0.05 0.05
QUINTOCENE
(PENTACHLORONITR
OBENZENE)METABOL
ITE
QUINTOCENE
(PENTACHLORON
ITROBENZENE)M
ETABOLITE
- - - -
0.02 0.01
- - - -
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
0.02 1
- - - -
0.01 1
0.01 0.5
0.01 - -
0.05 0.05
0.5 0.05
0.01 - -
1 1
- - - -
0.1 0.05
- - - -
0.01 0.3
0.01 0.2
0.01 0.1
0.01 1
0.01 0.05
0.01 - -
- - - -
0.01 5
0.1 0.05
0.01 - -
0.01 0.5
- - - -
0.01 - -
EU KOR EU KOR
0.2 0.05
0.2 0.05
0.2 0.05
0.01 1
- - - -
0.01 14
0.01 0.5
0.01 2
- - - -
- - 0.05
0.01 0.05
4 1
0.01 0.02
0.01 1
Pencycuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Penconazol LC/MSMS - - - - 0.2
LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD
US JP CA EU
Piperalin
Banned pesticides residues have been detected
AnalyteAnalyzed
by
Authorized use
MRL (ppm)
MX JP CA CHN
0.2
7 0.1 - -
- - - -
0.2 0.1 - -
0.01< LCL Pirimiphos-ethyl
0.1< LCL Pirimicarb 1
- -
< LCL Primisulfuron-methyl
- -
- -
- - < LCL
0.03
Sethoxydim* LC/MSMS 5 5 1 5 - -
Simazine GC/MSMS
0.1 - -
Analysis Results
AnalyteAnalyzed
by
Authorized use
MRL (ppm) Obtained amount in
mg/kg (ppm)CA CHN
LC/MSMS 6 6 0.01
Methiocarb sulfone GC/MSMS - - - - 0.05
Methoprotryne LC/MSMS - - - - - -
Methomyl LC/MSMS - - - -
Methiocarb sulfoxide GC/MSMS
Methoxyfenozide
Methoxychlor GC/MSMS - - - -
- -
< LCL Picoxystrobin
Report Date: 2018-10-15 Page: 4 of 7 Revision: AR272-TS-61
P-18-24827SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.:Client:
Producer:NEFTALI ARMANDO GONZALEZ
VAZQUEZOrchard:
US JP MX US
Chromatogram GC: P-18-24827 10-11-2018.D Chromatogram LC:
Obtained amount in
mg/kg (ppm)
P-18-24827 10-14-2018.d MXAgrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
- - - -
LC/MSMS - - - - 0.01 < LCL
8 < LCL
0.1
- -LC/MSMS 8 8 8
- -
Methiocarb GC/MSMS - - - - 0.05 0.1 - -
- - < LCL- -< LCL
0.1 - -
LC/MSMS - -0.1
- - - - 0.05 0.1 - -
0.011 LC/MSMS - - - -0.1 0.2
< LCL Piperonyl Butoxide
< LCL Piperophos < LCL
< LCLLC/MSMS - - - - 0.1< LCL Pirimiphos-methyl6
0.1 - - < LCLLC/MSMS - - - - 0.01
Metolachlor LC/MSMS 0.1- - - - 0.01 0.1 - -
0.01 0.2
0.05 0.1
0.01 - -
0.05 1
Metolcarb LC/MSMS - - - - 0.01 0.1 - -
< LCL Prochloraz < LCLLC/MSMS - -
< LCLLC/MSMS - - - - 0.5
Metobromuron LC/MSMS - - - - 0.01 0.1 - -
0.1 - - < LCLLC/MSMS - - - -
< LCL Procymidone
0.1
0.1
- - 0.05
- - < LCLGC/MSMS - - - - 1.5
< LCL Profluoralin
< LCL Promecarb
< LCL
Metoxuron LC/MSMS - - - - - - - - - -
< LCL Profenofos GC/MSMS - - - - 0.01
- - - - < LCLGC/MSMS - - - - - -
Metosulam LC/MSMS - - - - 0.01 0.1 - -
Metribuzin GC/MSMS - - - - 0.01 0.1 - - < LCL
GC/MSMS - - - - - -
- - < LCL
Metrafenone LC/MSMS - - - - 0.01 0.1 - -
Mexacarbate LC/MSMS - - - - - - - -
Mevinphos GC/MSMS - - - - 0.01 0.1 - - < LCL
Metsulfuron-methyl* LC/MSMS - - - - 0.01 0.1
< LCL
Monolinuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Monocrotophos LC/MSMS - - - - 0.01 0.1
Mirex GC/MSMS - - - - 0.01 0.1 0.01 < LCL
0.01 0.2
0.01 - -
- - < LCL
Napropamide LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL
N-2,4-Dimethylphenyl formamide
(2,4-DMPF)LC/MSMS - - - - - - - -
- - < LCL
Myclobutanil GC/MSMS 2 2 1 2 - - < LCL
Monuron LC/MSMS - - - - 0.01 0.1
- - < LCL
Norflurazon LC/MSMS 0.1 0.1 0.1 0.1 - - < LCL
Nitrapyrin GC/MSMS - - - - 0.01 0.1
- - < LCL
Nicosulfuron LC/MSMS - - - - 0.01 0.1 - - < LCL
Neburon LC/MSMS - - - - - - - -
DIMETHOATE
METABOLITE0.226
op Dicofol*** GC/MSMS - - - - 3 3 - - < LCL
Omethoate LC/MSMSDIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
DIMETHOATE
METABOLITE
- - < LCL
Ofurace LC/MSMS - - - - - - - - - - < LCL
Novaluron* LC/MSMS - - - - 0.01 0.1
< LCL
Oxydemeton-methyl LC/MSMS - - - - 0.02 0.1 - - < LCL
Oxamyl LC/MSMS - - - - 0.01 0.1
- - < LCL
Oxadixyl LC/MSMS - - - - 1 0.1 - - < LCL
Ovex GC/MSMS - - - - - - - -
Paraoxon-methyl LC/MSMS - - - - - - - - - - < LCL
Paraoxon LC/MSMS - - - - - - - -
- - < LCL
Paclobutrazol (Bonzi) LC/MSMS - - - - 0.01 0.1 - - < LCL
Oxyfluorfen GC/MSMS 0.05 0.05 0.01 0.1
- - - -
GC/MSMS - - - - - - - - - -
0.01 < LCL
Parathion methyl GC/MSMS - - - - 0.2 0.1 0.02 < LCL
Parathion GC/MSMS - - - - 0.5 0.1
- - < LCLPendimethalin LC/MSMS 0.1 0.1 0.05 0.1
- - < LCL
Permethrin GC/MSMS - - - - 1 0.1 1 < LCL
Pentachlorophenol GC/MSMS - - - - 0.01 0.1
0.1
Pentachloronitrobenzene GC/MSMS - - - - 0.02 0.1 - - < LCL
Pentachloroaniline GC/MSMS
QUINTOCENE
(PENTACHLORON
ITROBENZENE)M
ETABOLITE
QUINTOCENE
(PENTACHLORONIT
ROBENZENE)META
BOLITE
QUINTOCENE
(PENTACHLORONI
TROBENZENE)MET
ABOLITE
QUINTOCENE
(PENTACHLORONI
TROBENZENE)MET
ABOLITE
QUINTOCENE
(PENTACHLORONIT
ROBENZENE)META
BOLITE
< LCL
Pentachloroanisol
Phorate GC/MSMS - - - - 0.05 0.024 0.01 < LCL
Phenyl valerate GC/MSMS - - - - - - - -
- - < LCL
Phenthoate LC/MSMS - - - - 0.01 0.1 - - < LCL
Phenmedipham LC/MSMS - - - - 0.01 0.1
Phosphamidon LC/MSMS - - - - 0.01 0.1 0.05 < LCL
Phosalone LC/MSMS - - - - 0.01 0.1
0.01 < LCL
Phorate-sulfoxide LC/MSMS - - - - 0.05 0.024 0.01 < LCL
Phorate-sulfone LC/MSMS - - - - 0.05 0.024
0.01 0.2
Picolinafen LC/MSMS - - - - 0.01 0.1 - - < LCL
Phoxim LC/MSMS - - - - 0.02 0.1 0.01 0.05
0.01 - -
- - - - < LCL
Prometon GC/MSMS - - - - - - - - - - < LCL
0.05 < LCL
- - < LCL
- - < LCL
< LCL
- - < LCL
- - < LCL
- -
Propachlor LC/MSMS - - - - 0.01 0.1 - - < LCL
Propamocarb LC/MSMS - - - - 0.05 0.1 - - < LCL
Prometryn GC/MSMS - - - - 0.01 0.1 - - < LCL
Pronamide LC/MSMS - - - - - - - - - - < LCL
Propazin GC/MSMS - - - - 0.01 0.1 - - < LCL
Propetamphos LC/MSMS - - - - 0.01 0.1 - - < LCL
Propanil LC/MSMS - - - - 0.1 0.1 - - < LCL
Propargite (Omite) LC/MSMS - - - - 0.01 0.1 - - < LCL
Propiconazole GC/MSMS 1 1 0.05 1 - - < LCL
Propoxur LC/MSMS - - - - 1 0.1 - - < LCL
Propyzamide LC/MSMS 0.05 0.05 0.01 0.1 - -
1 1 0.01 0.1 - -
- - - - 0.01 0.1
< LCL
Prosulfocarb LC/MSMS - - - - 0.01 0.1 - - < LCL
- -
- - - - 0.01 0.1 - -
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
4
Rotenone
Sebuthylazine
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
GC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
LC/MSMS
GC/MSMS
Prosulfuron
Pymetrozine
Pyraclostrobin
Pyrazophos
Pyridaben
Pyrimethanil
Pyriproxyfen
Quinalphos
Quinoxyfen
Quizalofop-ethyl
Rimsulfuron
4 3 3.5 - -
- - - - 0.01 0.1 - -
- - - - 0.01 0.1 - -
15 15 10 15 - -
3 0.5
3 3
0.01 1
0.5 1
15 15
< LCL
< LCL
< LCL
< LCL
< LCL
< LCL
0.01 0.01 0.01 0.01 - -
- -
- - - - 0.02 0.1 - -
- - 0.01 0.1 - -
- - - - 0.01 0.1 - -
- - - - 0.05 0.1 - -
S-Metolachlor LC/MSMS 0.1 0.1 0.01 0.1 - - < LCL
- - - - - - - - - -
< LCL
< LCL
0.2
LC/MSMS - - - - 0.01 0.1 - - < LCLSimetryn
CHNKOR
* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166-1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it́ s not responsible for the representation of the result for the total
product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
BBBBBBBBBBBBBBBBBBBBBBBBB
B
BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBVinclozolin GC/MSMS - - - - 5 0.1 0.01 5
Vamidothion LC/MSMS - - - - 0.01 0.1 0.01 0.05 - -
< LCL
Trimidal LC/MSMS - - - - - - - - - - - - - - < LCL
Triforine LC/MSMS - - - - 0.01 0.1 0.01 0.5
< LCL
< LCL
< LCL
1.5
0.02
Spinetoram J LC/MSMS 0.8 0.8 0.7 0.05 - - < LCL0.5 1
1
Spirodiclofen LC/MSMS - - - - 0.01 1 - -
Spinosad A LC/MSMS 1 1 1 10.5
0.1
Report Date: 2018-10-15 Page: 5 de 7 Revision: AR272-TS-61
Chromatogram GC: P-18-24827 10-11-2018.D Chromatogram LC: P-18-24827 10-14-2018.d
Producer: NEFTALI ARMANDO GONZALEZ VAZQUEZ Orchard: LA TIJERA, LOS REYES MICH SAGARPA Reg.: SD
Client: SUN BELLE MÉXICO S.A. DE C.V. Sample: Blackberry Lab Reg. No.: P-18-24827
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
MX US JP CA EU KOR
CA EU
Analysis ResultsBanned pesticides residues have been detected
CHN
Analyte Analyzed by
Authorized use
LMR (ppm)Obtained
amount in
mg/kg (ppm)MX US JP KOR CHN
- - < LCL
Spiromesifen LC/MSMS - - - - 0.01 10.1
2
0.02
0.1
- - < LCL
Spirotetramat LC/MSMS - - - - 0.01 0.2
- - < LCL
Sulfentrazone LC/MSMS 0.15 0.15 0.05 - - - - < LCL
Spiroxamine LC/MSMS - - - - 0.01 - -0.1
0.15
0.01
0.01
- - < LCL
Sulfotep LC/MSMS - - - - 0.01 - - 0.01 < LCL
Sulfosulfuron LC/MSMS - - - - 0.01 - -0.1
0.1
0.01
0.01
- - < LCL
Sumithrin GC/MSMS - - - - 0.01 0.1 - - < LCL
Sulfoxaflor LC/MSMS - - - - 0.01 0.50.1
0.1
0.01
0.02
- - < LCL
Tebufenozide LC/MSMS 3 3 3 1 - - < LCL
Tebuconazole GC/MSMS - - - - 0.01 0.50.1
0.1
0.5
0.05
Tebuthiuron LC/MSMS - - - - 0.01 - - - - < LCL
- - < LCL
Tebutam LC/MSMS - - - - 0.01 - - - - < LCL
Tebufenpyrad GC/MSMS - - - - 2 0.5
- - < LCL
Terbacil GC/MSMS 0.2 0.2 0.1 - - - - < LCL
Teflubenzuron LC/MSMS - - - - 0.01 1
0.01
- - < LCL
Terbuthylazine GC/MSMS - - - - 0.01 0.1 - - < LCL
Terbumeton LC/MSMS - - - - - - - -
0.05
- -- -
0.1
- - < LCL
Terbutryn GC/MSMS - - - - 0.01 0.05 - - < LCL
Terbuthylazine-desethyl LC/MSMS - - - - - - - -- -
0.01
- -
0.1
- - < LCL
Tetrachlorvinphos, E-isomer GC/MSMS - - - - 0.01 - - - - < LCL
Terrazole GC/MSMS - - - - - - - -- -
0.1
- -
0.01
- - < LCL
Tetrahydrophthalimide, cis-1,2,3,6-(THPI) GC/MSMS CAPTAN METABOLITE CAPTAN METABOLITE CAPTAN METABOLITE CAPTAN METABOLITE CAPTAN METABOLITE < LCL
Tetradifon GC/MSMS - - - - 1 10.1
CAPTAN METABOLITE
0.01
CAPTAN METABOLITE
- - < LCL
Thiabendazole LC/MSMS - - - - 3 3 - - < LCL
Tetramethrin LC/MSMS - - - - 0.01 - -0.1
0.1
0.01
0.01
1 < LCL
Thiamethoxam LC/MSMS 0.35 0.35 0.5 1 - - < LCL
Thiacloprid LC/MSMS - - - - 5 0.70.1
0.5
1
0.01
0.1 0.01 0.05
- - < LCL
Thifensulfuron-methyl LC/MSMS - - - - 0.01 0.05 - - < LCL
Thidiazuron LC/MSMS - - - - 0.01 0.20.1
0.1
0.01
0.01
< LCL
- -
- -
Triflusulfuron-methyl LC/MSMS - - - - 0.01 0.1 0.01 - - - -
Trifluralin GC/MSMS - - - - 0.05 < LCL
< LCL
- - < LCL
0.05
0.01
0.01
0.01
0.1
0.1
0.1
0.1
0.1
< LCL
Thiobencarb LC/MSMS - - - - 0.01 0.1 0.01 0.05 - -
Thiocyclam hydrogen oxalate GC/MSMS - - - - 3 0.1 0.01 1 - -
< LCL
Thionazin LC/MSMS - - - - - - - - - - - - - - < LCL
Thiodicarb LC/MSMS - - - - 1 0.1 0.01 1 - -
< LCL
Tokution GC/MSMS - - - - - - - - - - - - - - < LCL
Thiophanate-methyl LC/MSMS - - - - 3 6 0.1 2 - -
< LCL
Triadimefon GC/MSMS - - - - 0.1 0.1 0.01 0.05 - - < LCL
Tolyfluanid GC/MSMS - - - - 5 0.1 0.02 2 5
< LCL
Triasulfuron LC/MSMS - - - - 0.01 0.1 0.05 - - - - < LCL
Triadimenol GC/MSMS - - - - 0.5 0.1 0.01 0.5 - -
< LCL
Tribenuron-methyl LC/MSMS - - - - 0.01 0.1 0.01 - - - - < LCL
Triazophos GC/MSMS - - - - 0.01 0.1 0.01 0.05 - -
< LCL
Trichloronate GC/MSMS - - - - - - - - - - - - - - < LCL
Trichlorfon LC/MSMS - - - - 0.5 0.1 0.01 0.05 0.2
< LCL
Tricyclazole GC/MSMS - - - - 0.02 0.1 0.01 0.05 - - < LCL
Triclocarban LC/MSMS - - - - - - - - - - - - - -
< LCL
Trifloxystrobin LC/MSMS - - - - 0.01 0.1 3 0.7 - - < LCL
Trietazine LC/MSMS - - - - - - - - - - - - - -
< LCL
Triflumuron LC/MSMS - - - - 0.02 0.1 0.05 0.5 - - < LCL
Triflumizole LC/MSMS - - - - 0.01 0.1 0.1 2 - -
* Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized. The colored bands are visual aids based on MRLs of Mexico and are not a result. 1Maximum Resuide Limits (MRL) expressed in ppm for every country using ISO 3166 -1 alfa-2. LCL = Lowest Calibration Level ppm = Parts per million = mg/kg GC/MSMS = Gass Chromatography /Mass/Mass LC/MSMS = Liquid Chromatography /MassMass Trazas/Traces = < 0.010 ppm.
Attention: Análisis Técnicos S.A. de C.V does not have the authority nor the faculty to deny, accept or authorize crops. The issued resu lt only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s not responsible for the representation of the result for the total product.
Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product. This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total o r partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or ame ndments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]
Authorizes Lic. Carlos Sepúlveda Ibarra
General Director
Triflumuron 0.010
Trifluralin 0.010
Lufenuron 0.005 Pendimethalin 0.005 Spinetoram J 0.005
0.005 Paraoxon 0.005 Rotenone 0.005
Isofenphos 0.005 Oxyfluorfen 0.010 Quizalofop-ethyl 0.005
Triflusulfuron-methyl 0.005
Triforine 0.010
Malathion 0.010 Pentachloroanisol 0.010 Spirodiclofen 0.005
Malaoxon 0.005 Pentachloroaniline 0.010 Spinosad A 0.005
Trimidal 0.005
Vamidothion 0.005
Vinclozolin 0.010
Mandipropamid 0.005 Pentachlorophenol 0.010 Spirotetramat 0.005
Mancozeb 0.005 Pentachloronitrobenzene 0.010 Spiromesifen 0.005
Mecarbam 0.005 Phenmedipham 0.005 Sulfentrazone 0.005
Mebendazole 0.005 Permethrin 0.010 Spiroxamine 0.005
Metalaxyl-M (Mefenoxam, R-
enantiomero de metalaxyl)0.010 Phenyl valerate 0.010 Sulfotep 0.005
Mepanipyrim 0.010 Phenthoate 0.005 Sulfosulfuron 0.005
Metazachlor 0.005 Phorate-sulfone 0.005 Sumithrin 0.020
Metamitron 0.005 Phorate 0.010 Sulfoxaflor 0.005
Methabenzthiazuron 0.005 Phosalone 0.010 Tebufenozide 0.005
Metconazole 0.005 Phorate-sulfoxide 0.005 Tebuconazole 0.010
Methidathion 0.005 Phoxim 0.010 Tebutam 0.005
Methamidophos 0.005 Phosphamidon 0.005 Tebufenpyrad 0.010
Triflumizole 0.005
Trifloxystrobin 0.005
Trietazine 0.005
Tricyclazole 0.010
Report Date 2018-10-15 Page 6 of 7 Revision: AR272-TS-61
Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab Agrolab
Lowest Calibration Level per analyteAnalyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)
Endosulfan I (alpha isomer) 0.010
2,3 dihydro-2,2dimethylbenzofuran 0.020 Butocarboxim-sulfoxide 0.005 Cyproconazole 0.005 Endosulfan II (beta isomer) 0.0102, 4-D Methyl ester 0.010 Butocarboxim* 0.010 Cypermethrin a (Zeta- 0.010
Endosulfan sulfate 0.010
3,4 Dichloroaniline 0.010 Butylate 0.020 Cyromazine 0.005 Endrin 0.0102,6 Dichlorobenzonitrilo 0.010 Buturon 0.005 Cyprodinil 0.010
Epoxiconazole 0.005
Abamectin 0.005 Carbaryl 0.010 DDD-p,p 0.010 Esfenvalerate + Fenvalerate* (**) 0.0103-Hydroxy carbofuran 0.005 Captan 0.010 DDD-o,p 0.010
Etaconazole (Etaconazole I y II) 0.010
Acetamiprid 0.005 Carbetamide 0.005 DDE-p,p 0.010 Ethalfluralin 0.010Acephate 0.005 Carbendazim 0.005 DDE-o,p 0.010
Ethiofencarb 0.005
Acrinathrin 0.020 Carboxin 0.005 DDT-p,p 0.010 Ethiofencarb-sulfone 0.005Acetochlor 0.005 Carbofuran 0.010 DDT-o,p 0.010
Ethirimol 0.005
Aldicarb 0.005 Chinometionate 0.010 Deltamethrin 0.010 Ethoprop 0.010Alachlor 0.005 Carfentrazone ethyl 0.005 DEET (Diethyl-m-toluamide, N,N-) 0.010
Ethylan 0.010
Aldicarb-sulfoxide (Aldoxicarb) 0.005 Chlorbromuron 0.005 Demeton S 0.010 Etion 0.010Aldicarb sulfone 0.005 Chlorantraniliprole 0.005 Demeton O 0.010
Etofenprox 0.010
Ametoctradin 0.005 Chlordimeform 0.010 Desmedipham 0.005 Etoxazole 0.005Aldrin 0.010 Chlordane- a 0.010 Demeton-s-methyl-sulfone 0.005
Famoxadone 0.010
Aminocarb 0.005 Chlorfenvinphos 0.005 Dialifos 0.005 Fenamiphos 0.005Ametryn 0.010 Chlorfenapyr 0.010 Desmetryn 0.010
Fenarimol 0.005
Atrazine-2-hydroxy 0.005 Chloridazon (Pyrazon) 0.005 Dichloran 0.010 Fenazaquin 0.005Atrazine 0.010 Chlorfluazuron 0.005 Diazinon 0.010
Fenbuconazol 0.005
Azinphos-ethyl 0.005 Chlorobenzilate 0.010 Diclobutrazol* 0.010 Fenbutatin oxide* 0.010Azamethiphos 0.005 Chlormequat 0.005 Dichlorvos 0.010
Fenchlorphos 0.010
Azoxystrobin 0.010 Chloropropylate 0.010 Dicrotophos 0.005 Fenfuram 0.005Azinphos-methyl 0.010 Chloroneb 0.010 Diclofop methyl 0.020
Fenhexamid 0.005
Benalaxyl 0.010 Chlorotoluron 0.005 Diethofencarb 0.005 Fenitrothion 0.020Baycarb 0.005 Chlorothalonil 0.010 Dieldrin 0.010
Fenoxaprop-ethyl 0.005
Bensulfuron-methyl 0.005 Chlorpropham 0.010 Difenoxuron 0.005 Fenoxycarb 0.005Bendiocarb 0.005 Chloroxuron 0.005 Difenoconazole 0.005
Fenpropathrin 0.010
Benzoximate 0.005 Chlorpyrifos methyl 0.010 Dimefuron 0.005 Fenpropidin 0.005Bensulide 0.005 Chlorpyrifos 0.010 Diflufenican 0.005
Fenpropimorph 0.005
BHC lindane beta 0.010 Chlortal dimethyl 0.010 Dimethachlor 0.005 Fenpyroximate 0.005BHC lindane alpha 0.010 Chlorsulfuron 0.005 Dimepax 0.010
Fenson 0.020
BHC lindane gamma 0.010 Clodinafop-propargyl 0.005 Dimethoate 0.010 Fensulfothion 0.010BHC lindane delta 0.010 Chlorthiophos 0.020 Dimethenamid 0.005
Fenthion 0.010
Bifenox 0.020 Clomazone* 0.005 Diniconazole 0.005 Fenuron 0.005Bifenazate 0.005 Clofentezine 0.005 Dimethomorph 0.005
Fipronil 0.020
Bitertanol 0.005 Dioxathion 0.010 Flamprop methyl 0.010Bifenthrin 0.010 Cloquintocet-mexyl 0.005 Dinotefuran 0.005
Flamprop-isopropyl 0.010Coumaphos 0.010
Boscalid 0.005 Disulfoton 0.010 Flazasulfuron 0.005Bolstar 0.010 Diphenamid 0.005Crimidine 0.005
Cyanazine 0.005Flonicamid 0.010
Bromophos methyl 0.010 Cyazofamid 0.005 Diuron (Karmex)* 0.010 Fluazifop-butyl 0.005Bromacil 0.010 Cyantraniliprole* 0.010 Disulfoton-sulfone 0.005
Flubendiamide 0.010Bromuconazole* 0.010 Cyfluthrin 0.010 Dyfonate 0.010 Fluchloralin 0.020Bromopropylate 0.010 Cycloate 0.005 Dodemorph 0.005
Fludioxonil 0.010
Buprofezin 0.010 Cymoxanil 0.005 Emamectin Benzoate 0.005 Flufenacet 0.005
Bupirimate 0.005Cyhalothrin (Isomero Lambda y
gamma)**0.010 Edifenphos 0.005
Analyte LCL (ppm)
Flufenoxuron 0.005 Methomyl 0.005 Piperonyl Butoxide 0.005 Terbumeton 0.005
Analyte LCL (ppm) Analyte LCL (ppm) Analyte LCL (ppm)
Terbuthylazine 0.010
Fluopicolide 0.005 Methoxychlor 0.010 Pirimicarb 0.005 Terbuthylazine-desethyl 0.005
Fluometuron 0.005 Methoprotryne 0.005 Piperophos 0.005
Terbutryn 0.010
Fluoxastrobin 0.005 Metobromuron 0.010 Pirimiphos-methyl 0.005 Terrazole 0.010
Fluoroglycofen-ethyl 0.005 Methoxyfenozide 0.005 Pirimiphos-ethyl 0.005
Tetrachlorvinphos, E-isomer 0.010
Flusilazole 0.005 Metolcarb 0.010 Prochloraz 0.005 Tetradifon 0.010
Flurtamone 0.005 Metolachlor 0.005 Primisulfuron-methyl 0.005
Tetrahydrophthalimide, cis-1,2,3,6-
(THPI)0.010
Fluvalinate 0.010 Metoxuron 0.005 Profenofos 0.010 Tetramethrin 0.005
Flutriafol 0.005 Metosulam 0.005 Procymidone 0.010
Thiabendazole 0.005
Forchlorfenuron 0.005 Metribuzin 0.010 Promecarb 0.010 Thiacloprid 0.005
Folpet 0.010 Metrafenone 0.005 Profluoralin 0.020
Thiocyclam hydrogen oxalate 0.010
Thiamethoxam 0.005
Fuberidazole 0.005 Mevinphos 0.010 Prometryn 0.010 Thidiazuron 0.005
Formetanate 0.005 Metsulfuron-methyl* 0.005 Prometon 0.010
Thifensulfuron-methyl 0.005
g Chlordan 0.010 Mirex 0.010 Propachlor 0.005 Thiobencarb 0.010
Furathiocarb 0.005 Mexacarbate 0.005 Pronamide 0.005
Heptachlor 0.010 Monolinuron 0.005 Propanil 0.005Haloxyfop-methyl 0.005 Monocrotophos 0.005 Propamocarb 0.005
0.005
0.010
Hexaconazole 0.005 Napropamide 0.005 Propiconazole 0.010
Hexachlorobenzene 0.010N-2,4-Dimethylphenyl formamide (2,4-
DMPF)0.010 Propetamphos 0.005
Heptenophos 0.005 Myclobutanil 0.010
Heptachlor exo-epoxide (isomer B) 0.010 Monuron 0.005 Propargite (Omite)
Propazin
Hexythiazox 0.005 Nicosulfuron 0.005 Propyzamide 0.005
Hexazinone 0.010 Neburon 0.005 Propoxur 0.005
Imazapyr 0.005 Norflurazon 0.005 Prosulfuron 0.005
Imazalil 0.005 Nitrapyrin 0.010 Prosulfocarb 0.005
Imidacloprid 0.005 Ofurace 0.005 Pyraclostrobin 0.005
Imazaquin 0.005 Novaluron* 0.010 Pymetrozine 0.005
Indoxacarb 0.010 op Dicofol*** 0.010 Pyridaben 0.005
Imidan 0.010 Omethoate 0.005 Pyrazophos 0.005
Iprovalicarb 0.005 Oxadixyl 0.005 Pyriproxyfen 0.010
Iprodione 0.010 Ovex 0.010 Pyrimethanil 0.005
Isazophos 0.010 Oxydemeton-methyl 0.005 Quinoxyfen 0.005
Irgarol 0.005 Oxamyl 0.005 Quinalphos 0.005
Methiocarb sulfoxide 0.020 Piperalin 0.005 Terbacil 0.010
Linuron 0.005 Pencycuron 0.005 S-Metolachlor 0.005
Methiocarb sulfone 0.020 Picoxystrobin 0.005 Teflubenzuron 0.010
Methiocarb 0.010 Picolinafen 0.005 Tebuthiuron 0.005
0.005
0.005
0.010
0.010
Thiodicarb
Thionazin
Thiophanate-methyl
Tokution
Lenacil 0.005 Penconazol 0.005 Simetryn 0.005
0.010
Kelthane*** 0.010 Parathion 0.010 Sethoxydim* 0.010
Triasulfuron
Triazophos
Kresoxim-methyl
0.005
0.005
0.005
0.010
0.010
0.010
0.010
0.005
0.010
Tolyfluanid
Triadimefon
Triadimenol
0.010
Isoxaflutole 0.010
Tribenuron-methyl
Trichlorfon
Trichloronate
Triclocarban
0.005 Parathion methyl 0.010
Isoprocarb 0.005 Paclobutrazol (Bonzi) 0.005 Rimsulfuron
Paraoxon-methyl 0.005 Sebuthylazine
Simazine
0.005
Isoproturon
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued res ult only affects the sample received at the facility of Análisis Técnicos S.A. de C.V, therefore it ´s
not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad Intelectual. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
ppm = Parts per million = mg/kg Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. Punto 91
Data corresponding to page 2, page 3, page 4 and page 5
Report Date: 2018-10-15 Page: 7 of 7 Revision AR272-TS-61
End of Report
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Additional and complementary information
General Information
1. The customer has five calendar days of issuance of the results**** in order to make any comment or complaint about it, because if not done within this time period will be considered this
report has been accepted.
2. Samples may be disposed within 5 days after the issue of results**** only samples for microbiological analysis shall be discarded 24 hours after being received
3. The information recorded in this "Report test results" is treated with strict adherence to privacy notice Análisis Técnicos S.A. de C.V complying with Articles third transient, 16 and 17 of Law
Protection Federation Personal Data Held by Private Parties, in order to regulate their treatment legitimate, controlled and reported, in order to ensure privacy and the right to self-determination
informative individuals.
4.Análisis Técnicos S.A. de C.V not have the authority, or the right to deny, accept or approve cuts or harvests.
5. Análisis Técnicos S.A. de C.V. is not accredited in sampling.
6. MRLs of the countries are a reference data, requesting check the official sites of each country and that can be changed or modified.
7. The result represents the sample that was received on the premises of Análisis Técnicos S.A. de C.V , which is not responsible for the representation of the result for the total product
8. This form of interpretation is protected and registered with the Instituto Nacional del Derecho de Autor (INDAUTOR), likewise, logos and Agrolab name and its subsidiaries are registered with
the Instituto Mexicano de la Propiedad Intelectual (IMPI). Reproduction is prohibited in whole or in part, for any purpose other than the interpretation of results, without permission.
9. This report is not valid if you have scratches, erasures or amendments.
10. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
11. Análisis Técnicos S.A. de C.V. It is not responsible for updating the MRL's because they are considered as a piece of information. It is your responsibility to review the report LMR official
sites for each country since the information can be changed or modified.
12. The detection of the pesticide residue above the quantification limit is reported as ppm (mg / kg), below the limit of quantification reported as <LCL ppm (mg / kg) and below the LD is
considered as undetermined.
13.The decision rule does not include uncertainty.
**** The issuance of the results includes the final report in PDF format. Delivering results to the client, is subject to confirmation of payment.
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References
International Maximum Residue Level Database
http://www.mrldatabase.com/
EU Pesticides Database
http://ec.europa.eu/sanco_pesticides/public/index.cfm
Electronic Code of Federal Regulation
http://ecfr.gpoaccess.gov/cgi/t/text/text-idx?
Health Canada
http://pr-rp.hc-sc.gc.ca/mrl-lrm/index-eng.php
Normas Alimentarias FAO/OMS
http://www.codexalimentarius.net/pestres/data/pesticides/search.html
Positive List System for Agricultural Chemical Residues in Foods (Japón)
http://m5.ws001.squarestart.ne.jp/foundation/search.html
1. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating
QuEChERS extraction), by GASS CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.
2. The laboratory Análisis Técnicos S.A. de C.V. is accredited before EMA, in the test of determination of residues of pesticides in fruits, vegetables, agricultural food and seeds (incorporating
QuEChERS extraction), by LIQUID CHROMATOGRAPHY / MASS / MASS to the ISO / IEC 17015:2005.
3. * = Analyte not declared in the scope accredited and / or licensed accredited obtained by method and / or authorized.
4.Authorized use of the pesticide in the relevant country code specified in ISO 3166-1 alpha-2. RML for each country are indicated in the same results table.
5. If no pesticide was detected a green band is shown. If a pesticide was detected within the allowed limits a yellow band is shown. If a pesticide was detected outside of the allowed limits a red
band is shown. If a forbidden pesticide was detected a red band is shown.
6. The colored bands are visual aids based on MRLs of each country and are not a result.
7. ** = The MRL of Isomero Lambda is taken for the molecule Cyhalothrin (Isomero Gamma and Lambda), for Cypermethrin a (Zeta-Cypermethrin) the MRL for Zeta-Cypermethrin is taken and
for the MRL for Esfenvalerate + Fenvalerate, the one for Esfenvalerate is taken.
8. 2 =For Canada the MRL of 0.1 ppm default is considered according to the point 5.2.1.4.2 Food and Drug Regulations of the Canada Food Inspection Agency
http://www.inspection.gc.ca/food/meat-and-poultry-products/manual-of-procedures/chapter-5/eng/1395150894222/1395150895519?chap=2.
9. *** = Dicofol MRL is the sum of p, p-dicofol and o, p-dicofol.
10. The color bands of each molecule are visual support based on the MRLs of each country and do not represent a result.
Information corresponding to page 5 and 6
1. In the corresponding table it´s represented the lower calibration poing (LCL).
2.The correspondig table is NOT A RESULT. It represents quality information data.
3. Uncertainty = 50 % according to "Method validation and quality control procedures for pesticide residues analysis in food and feed". No. de Documento SANCO/10684/2009. point 91
Glosario
GC/MSMS = Gass/Mass/Mass AGILENT 225/MS, 240/MS
LC/MSMS = Liquid/Mass/Mass QQQ (AGILENT 6460)
LCL = Lowest Calibration Level
MRL = Maximum Resuide Limits
ppm = Parts per million = mg/Kg
SD = No Data
Traces = < 0.010 ppm.
MX= Mexico
US= United States
JP= Japan
CA= Canada
EU= European Union
KOR= Korea
CHN= China
Maximum Residue Limits (MRLs) for Blackberry listed in The Official Catalog of Mexico
Pesticide 2004.
Maximum Residue Limits (MRLs) for Blackberry indicated in Environmental Protection
Agency (EPA) United States.
Maximum Residue Limits (MRLs) for Blackberry indicated in Electronic Code of Federal
Regulations (e-CFR TM) United States.
Attention: Análisis Técnicos S.A. de C.V. does not have the authority nor the faculty to deny, accept or authorize crops. The issued result only affects the sample received at the facility of Análisis Técnicos S.A.
de C.V, therefore it´s not responsible for the representation of the result for the total product. Análisis Técnicos S.A. de C.V. is not responsible for the commercial or final destination of the product.
This form of interpretation is protected and registered with the Instituto Mexicano de la Propiedad. Its total or partial reproduction without authorization is prohibited. This report will not be valid if you have scratches, erasures or amendments.
Controlled document ISO/IEC 17025:2005
Análisis Técnicos S.A. de C.V. | Km 7, Carretera Pachuca - Actopan, Pachuca, Hidalgo, México, C.P. 42088 | Teléfono: 771 713 28 01 | Fax: 771 713 82 55 | [email protected]