Upload File

fb control proceso 2013 07

102
QUIMPAC S.A. LF-MFA01-001 Versión : 0 Fecha: 10/08/09 CONTROL QUIMICO DE PROCESO 01 07 13 ATAQUE Y PURIFICACION DIA MES AÑO SUPERVISOR LABORATORISTA H DFR - 01 DP - 02 E - 01 DP - 06 E - 02 DP - 03 DP - 16 DA-01 DA-03 OBSEVACIONES O REATAQUE DEFLUORINACION B A R HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCL A gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl % OPTIMO 35.0 9.0 700 33.0 2.0 175 33.0 2.0 124 45 38 2600 19.0 12.0 1200 19.0 11.0 1200 15 60 800 MAX. 40.0 11 1000 36.2 2.6 220 35 2.2 150 364 55 45.3 3500 22 18 1600 30 25.6 15.0 1500 20 70 1200 1.5 - - 100.0 -- -- MIN. 30.0 8.0 400 29.1 0 80 29.1 0 80 233 29.1 20.0 1200 12.1 5.0 400 14 12.1 5.0 500 10 50 400 2.0 - 50.0 344.0 30.0 Juan Lazo Ameli Pachas 7:00 36.2 12.0 33.7 2.6 31.2 1.8 96 325 41.2 68.6 33.4 28.3 25.2 17.9 20.0 55.7 8:00 34.1 11.7 33.0 1.5 30.5 2.1 102 299 19.0 65.7 9:00 36.9 12.0 34.1 5.1 32.0 1.8 110 291 20.6 65.0 10:00 35.1 14.2 33.0 4.4 33.0 2.8 140 236 43.4 66.1 18.8 58.0 11:00 32.3 12.8 32.0 2.1 32.0 2.1 140 229 35.5 69.4 20.9 55.1 12:00 32.7 12.4 28.8 1.8 32.0 1.8 128 250 17.4 55.5 13:00 32.7 11.8 32.0 1.8 32.3 1.8 114 283 18.8 56.2 14:00 32.3 10.2 29.8 1.1 28.4 1.5 108 263 16.3 51.1 JOSE AGUILAR LUIS MARIN 15:00 33.7 9.9 31.6 0.7 30.2 0.7 126 240 41.9 54.8 29.3 22.5 25.2 19.0 17.8 65.3 16:00 35.1 11.7 33.3 2.2 30.2 1.1 93 325 8.9 82.7 17:00 29.1 9.1 28.8 1.8 30.2 1.8 82 368 34.8 69.4 7.1 51.8 18:00 25.9 9.1 24.9 0.0 29.5 1.8 82 360 11.4 45.6 19:00 32.0 10.4 30.2 2.2 29.5 1.5 80 369 41.2 65.7 17.0 20.1 18.5 21.9 16.7 55.8 20:00 32.3 10.4 31.2 2.2 29.5 1.5 82 360 16.3 58.8 21:00 33.3 11.7 30.2 1.1 29.5 1.5 80 369 14.9 73.3 22:00 34.8 12.8 33.3 3.6 29.5 1.8 80 369 17.4 57.3 CARLOS HERNANDEZ EDGARD SAAVEDRA 23:00 35.5 9.9 33.0 0.4 31.2 1.8 114 274 44.0 73.0 22.7 29.2 19.9 25.2 19.5 60.6 0:00 35.1 10.2 34.1 1.8 31.2 1.5 116 269 19.2 58.8 1:00 36.9 11.0 35.5 2.2 31.6 1.8 110 287 20.6 62.8 2:00 36.2 11.0 35.1 1.8 32.0 1.8 102 314 44.0 62.4 20.6 60.6 3:00 37.3 11.7 35.9 1.1 33.0 1.5 110 300 19.5 61.0 4:00 36.6 11.7 35.9 1.8 33.0 1.5 100 330 19.9 60.6 5:00 36.6 11.7 35.5 1.8 33.0 1.8 110 300 41.5 62.8 22.4 22.6 21.7 21.2 19.9 61.7 6:00 36.9 12.0 35.5 3.3 33.0 2.2 96 344 19.5 64.6 PROM 34.2 11.3 32.5 2.0 31.1 1.7 104 306 40.8 65.8 25.0 24.5 0 22.1 21.0 17.5 60.2 MAX 37.3 14.2 35.9 5.1 33.0 2.8 140 369 44.0 73.0 33.4 29.2 0 25.2 25.2 20.9 82.7 MIN 25.9 9.1 24.9 0.0 28.4 0.7 80 229 34.8 54.8 17.0 20.1 0 18.5 17.9 7.1 45.6 P2O5 P2O5 P2O5 P2O5 P2O5 P2O5 P2O5 P2O5

Upload: macu1820

Post on 18-Aug-2015

224 views

Category:

Documents


3 download

Report

DESCRIPTION

Control quimico de un proceso. Data para el proceso

TRANSCRIPT

QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 01 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,-an La./A0e1i !achas'00 3%.! "!.0 33. !.% 3".! ".$ 9% 3!5 #".! %$.% 33.# !$.3 !5.! ".9 !0.0 55.$'00 3#." "". 33.0 ".5 30.5 !." "0! !99 "9.0 %5.9'00 3%.9 "!.0 3#." 5." 3!.0 ".$ ""0 !9" !0.% %5.0"0'00 35." "#.! 33.0 #.# 33.0 !.$ "#0 !3% #3.# %%." "$.$ 5$.0""'00 3!.3 "!.$ 3!.0 !." 3!.0 !." "#0 !!9 35.5 %9.# !0.9 55.""!'00 3!. "!.# !$.$ ".$ 3!.0 ".$ "!$ !50 ".# 55.5"3'00 3!. "".$ 3!.0 ".$ 3!.3 ".$ ""# !$3 "$.$ 5%.!"#'00 3!.3 "0.! !9.$ "." !$.# ".5 "0$ !%3 "%.3 5".",O"

A2UILARLUI" MARIN"5'00 33. 9.9 3".% 0. 30.! 0. "!% !#0 #".9 5#.$ !9.3 !!.5 !5.! "9.0 ".$ %5.3"%'00 35." "". 33.3 !.! 30.! "." 93 3!5 $.9 $!."'00 !9." 9." !$.$ ".$ 30.! ".$ $! 3%$ 3#.$ %9.# ." 5".$"$'00 !5.9 9." !#.9 0.0 !9.5 ".$ $! 3%0 "".# #5.%"9'00 3!.0 "0.# 30.! !.! !9.5 ".5 $0 3%9 #".! %5. ".0 !0." "$.5 !".9 "%. 55.$!0'00 3!.3 "0.# 3".! !.! !9.5 ".5 $! 3%0 "%.3 5$.$!"'00 33.3 "". 30.! "." !9.5 ".5 $0 3%9 "#.9 3.3!!'00 3#.$ "!.$ 33.3 3.% !9.5 ".$ $0 3%9 ".# 5.3CARLO" 3

RNAND

4

D2ARD "AAV

DRA!3'00 35.5 9.9 33.0 0.# 3".! ".$ ""# !# ##.0 3.0 !!. !9.! "9.9 !5.! "9.5 %0.%0'00 35." "0.! 3#." ".$ 3".! ".5 ""% !%9 "9.! 5$.$"'00 3%.9 "".0 35.5 !.! 3".% ".$ ""0 !$ !0.% %!.$!'00 3%.! "".0 35." ".$ 3!.0 ".$ "0! 3"# ##.0 %!.# !0.% %0.%3'00 3.3 "". 35.9 "." 33.0 ".5 ""0 300 "9.5 %".0#'00 3%.% "". 35.9 ".$ 33.0 ".5 "00 330 "9.9 %0.%5'00 3%.% "". 35.5 ".$ 33.0 ".$ ""0 300 #".5 %!.$ !!.# !!.% !". !".! "9.9 %".%'00 3%.9 "!.0 35.5 3.3 33.0 !.! 9% 3## "9.5 %#.%!ROM3#.! "".3 3!.5 !.0 3"." ". "0# 30% #0.$ %5.$ !5.0 !#.5 0 !!." !".0 ".5 %0.!MA5 3.3 "#.! 35.9 5." 33.0 !.$ "#0 3%9 ##.0 3.0 33.# !9.! 0 !5.! !5.! !0.9 $!.MIN !5.9 9." !#.9 0.0 !$.# 0. $0 !!9 3#.$ 5#.$ ".0 !0." 0 "$.5 ".9 ." #5.%P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 01 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,-an La./A0e1i !achas'00 9.% ".$ ".# ".$$'00 9.9 !." ".$ ".$9'00 $.5 ".$ !." !.""0'00 $.5 ".$ ".$ !." E-0#( #" )E-05( ""*$""'00 "#.9 3.% ".$ ".$"!'00 "!.$ #.% ".$ !.$"3'00 9.9 3.! !." !.""#'00 .5 #.3 3.! 3.!,O"

A2UILARLUI" MARIN"5'00 $.5 ".$ !." !.""%'00 "0. ".$ ".# ".#"'00 "". !." ".$ ".$"$'00 $.9 3.% ".# ".#"9'00 "".0 ".$ !.5 !.5!0'00 9.9 !." ".$ !."!"'00 .5 3.! ".$ ".$!!'00 9.9 !.5 !." !."CARLO" 3

RNAND

4

D2ARD "AAV

DRA!3'00 ".$ %.# !.5 !.50'00 9.! #.3 !.5 !.5"'00 "%.0 #.3 3.! 3.!!'00 "".0 5. !.$ !.$3'00 9.! !.$ !." !."#'00 9.! !.5 !." !."5'00 9.9 !.$ !." !."%'00 "5.3 #.% !." !."!ROM"0. 3." !." !.!MA5 ".$ %.# 3.! 3.!MIN .5 ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 01 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,-an La./A0e1i !achas'00$'00 0.00 0.00 0.00 "9.09 $0.9" 0.00 0.00 0.00 9.#0 90.%0 ".!% 3!".00 "."% "$.#! !$.!% 0.%5 0."# 0.#0 $0.00 $0 ".3$ "9."% !9.3! 0.%5 0."# 0.#! "0$.0 ""0 ".90 "$.3! !$.0! 0.%5 0."% 0.## "0$ ""09'00"0'00""'00"!'00"3'00 ".0$ "$."" !.!% 0.%% 0."% 0.#! $0.00 $0 ".!" ".9 !%.$5 0.%% 0."% 0.## "05 ""0 ".30 "$.#% !.$! 0.%% 0."$ 0.#0 "0$ ""0"#'00,O"

A2UILARLUI" MARIN"5'00"%'00 0."% 3.5$ !.9" "#.3" 9.0# 0.05 ".!3 !.#" .$5 $$.#% 0.9% "$.3# !.#5 0.% 0." 0.# $0.00 $0 ".3% "$.% !.#" 0.%$ 0." 0.# "05 ""0 ".5# "$.%9 !.#5 0.%$ 0."% 0.#% "03 ""0"'00"$'00"9'00!0'00!"'00 "$."0 !.# 0.%5 0."! 0.39 $0.00 $0 ".$% !.#5 0.%5 "0! ""0 "$."5 !.$" 0.%5 "0# ""0!!'00CARLO" 3

RNAND

4

D2ARD "AAV

DRA!3'000'00 . . . "9.#0 $0.%0 "."0 "$.$0 !$.00 0.% 0."# 0.## 9.00 $0 ".90 "$.%0 !.0 0.% 0."# 0.#" "0% ""0 ".%0 "$.#0 !.%0 0.% 0."# 0.#% ""0 ""0"'00!'003'00#'00 ".00 "9.00 !.90 0.%$ 0.0" 0.#" $0.00 $0 ".%0 "$.$0 !.$0 0.%$ 0."3 0.## "0$ ""0 ".%0 "$.0 !.%0 0.%$ 0."! 0.## ""0 ""05'00%'00!ROM 0." ".$ ".5 ".% $0.! 0.0 0.% ".! $.% $9.5 ".3 3!".0 ".0% "$.#% !. 0.%% 0."! 0.#! 9.$3 $0 ".#9 "$.50 !.% 0.% 0."5 0.## 333 ""0 ".59 "$.#5 !.! 0.% 0."5 0.## "0 ""0MA5 0.! 3.% !.9 "9.# $0.9 0." ".! !.# 9.# 90.% ".3 3!".0 "."% "9.00 !$.!% 0.%$ 0." 0.# $0.00 $0 ".90 "9."% !9.3! 0.%$ 0." 0.# 333 ""0 ".90 "$.0 !$.0! 0.%$ 0."$ 0.#% ""0 ""0MIN 0.0 0.0 0.0 "#.3 9.0 0.0 0.0 0.0 .9 $$.5 ".3 3!".0 0.9% "$."0 !.!% 0.%5 0.0" 0.39 9.00 $0 ".!" ".9 !%.$5 0.%5 0."3 0.#" 333 ""0 ".30 "$."5 !.#5 0.%5 0."! 0.#0 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0' 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,/se A6-i1arA0e1i !achas'00 33. "0.% 3!.0 "." 3!.0 "." "00 3!0 #!.% %!.# !9.$ !$.5 !".3 !#." "$.$ 55.5$'00 33.0 "". 30.! ".5 !9.$ !." "0! !9! ".$ %!."9'00 33. "0.% 3".% ".$ 30.! ".$ "05 !$$ #!.% %0.! "$.0 %3.9"0'00 33. "!.$ 3!.0 !.% 3".% !." ""0 !$ !".3 %".3""'00 3#." "". 3!.0 !.! 3!.0 !." "00 3!0 "9.9 5$.#"!'00 33. "". 3!.3 !.! 3".3 !." 9$ 3"9 #3.3 %%." !".3 %0.%"3'00 3#." "!.0 3!.0 !.! 30.! !." "00 30! !0.! %0.!"#'00 3#.$ "". 3!.3 "." 3!.0 "." 9% 333 #".9 %5.3 !.3 !%.0 !".! !0.$ !0.! %".3,UAN LA4OLUI" MARIN"5'00 35.5 "". 3#.$ !.! 33.3 ".$ 90 30 "9.5 %3.5 !".3 !. !!. !.0 !!.% %.9"%'00 35.5 "".# 3!.3 ".$ 33. ".$ 9! 3%% !".3 %0.!"'00 33.3 "".0 33.3 !.! 33.3 ".$ 90 30 3$.9 %!. ".$ 5%.%"$'00 33.3 "".0 3!.0 !.! 33.3 !.! $! #0% "$.5 5$.#"9'00 33. "".# 33.3 !.! 33.3 !.! $9 3# "$.$ 5$.#!0'00 3#.# "!.$ 3#.# ".$ 3!. !.! 90 3%3 #9.3 #.$ !!.0 !".9 !0.% !5.% "9.! 5$.#!"'00 3%.! "". 35.5 !.! 3!. !.! $% 3$0 ##.! %5. !". %0.!!!'00 35.5 "!.$ 35.5 3.% 3!. !.! $# 3$9 "9.9 %0.!CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 33. "3." 33.# !.% 3!.0 !. ""0 !9" 5.9 5$.# !3.# "9.3 !!.# !!.% !%30 !".0 5%.90'00 35." "!.$ 33.# ".$ 33.0 !.% 9$ 33 !". 5.3"'00 3%.! "".3 35." !.! 3#." ".$ 90 39 #9. %9.0 !0.9 5%.9!'00 3#.$ "". 33.# ".$ 33.0 !.! $$ 35 !0.! 59.93'00 35." "".3 3#.$ ".$ 33.# ".$ $! #0 5%.# 0.$ !0.% 5%.!#'00 3#.$ "". 33.0 "." 3!. ".$ "" !9 50." %5.0 "$." %".05'00 3#.# "".3 33. ".$ 3!.3 "." "00 3!3 53.% %!.# !#." !".! !!.# !".! "9.! 5$.#%'00 35." "". 3#." ".$ 3!.0 ".$ ""$ !" !0.! 5%.!!ROM3#.5 "". 33.! !.0 3!.# ".9 9 339 #5.# %5." !#. !#." 0 !".$ !3.% !%30 !0.0 59.#MA5 3%.! "3." 35.5 3.% 3#." !. ""$ #0 5.9 #.$ !9.$ !$.5 0 !!. !.0 !%30 !!.% %.9MIN 33.0 "0.% 30.! "." !9.$ "." $! !" "9.5 5$.# !".3 "9.3 0 !0.% !0.$ !%30 ".$ 55.5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0' 0# 1$!RCI!ITACION % LAVADO DIAMES !"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,/se A6-i1arA0e1i !achas'00 $.9 !." ".$ ".$$'00 $.9 ".$ ".$ ".$9'00 9.% !." ".$ ".$"0'00 $.5 ".$ ".5 ".5 E-0#( #" )E-05( ""*%""'00 "!.0 !.% !." ".$"!'00 "0.% !.$ !." !.""3'00 9.! !.$ !." !.""#'00 9.! !." !." !.",UAN LA4OLUI" MARIN"5'00 "9.! !." ".$ ".$"%'00 9.9 3.% ".$ ".$"'00 9.# !.$ ".$ ".$"$'00 9.9 !.$ !.5 !.""9'00 9.9 !.5 !." ".$!0'00 "". !." ".$ ".$!"'00 9.9 !." ".$ ".$!!'00 9.% !." ".$ ".$CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 "0.3 ".$ ".# ".#0'00 9.9 ".$ ".# ".#"'00 "".0 !." ".$ ".$!'00 9.! !." !." ".$3'00 "0.3 !." ".$ ".$#'00 $.9 !." ".$ ".$5'00 9.9 ".$ ".$ ".$%'00 "0. !." !." ".$!ROM"0.3 !.3 ".9 ".$MA5 "9.! 3.% !.5 !."MIN $.5 ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 0' 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,/se A6-i1arA0e1i !achas'00$'00 0.00 0.00 0.00 !0.5" 9.#9 0.03 "."0 !.%0 %.95 $9.3! "."% 3#0 !.0 ".3$ !$."9 0.%! 0."# 0.#! "0$ ""0 ".!5 ".#! !.9$ 0.%! 0."# 0.## ""0 ""09'00"0'00""'00"!'00"3'00 ".9$ "."9 !.$! 0.%! 0."3 0.#0 "0$ ""0 ".0$ ".3 !$.05 0.%! 0."! 0.#0 ""0 ""3"#'00,UAN LA4OLUI" MARIN"5'00"%'00 * * * !0."$ 9.$! * * * "5.$9 $#."" ".!" #39 ".#5 "$."! !.$5 0.%5 0."3 0.3 "0# ""0 ".3% ".$% !.#5 0.%5 0."3 0.3$ "0 ""0"'00"$'00"9'00!0'00!"'00 "."! "$.0# !.9% 0.%5 0."0 0.3 $ $0 ".3# ".55 !.#5 0.%# 0."" 0.3 "05 ""0 ".#! "$."# !.$9 0.%5 0."0 0.3% "09 ""0!!'00CARLO" 3

RNAND

4FRANCO MA%3UA!3'000'00 0.!5 !.#9 !.3 "#."! $0.#" * * * !".3# $.%% ".!% #!" "."5 "$.0" !.$% 0.%5 0."! 0.39 9 $0 ".!! ".%3 !.%5 0.%# 0."! 0.#0 "00 ""0 ".39 "$."5 !.$5 0.%5 0."" 0.#0 "0% ""0"'00!'003'00#'005'00 "."0 "$.3" !.5% 0.%% 0."3 0.#0 $" $0 "."$ ".9$ !.%" 0.%5 0."3 0.39 "0" ""0 ".!0 "$.#" !.%9 0.%% 0."! 0.#0 "0 ""0%'00!ROM 0." ".! ".# "$.3 9.9 0.0 "." !.% "#. $#.0 ".! #00.0 "."! "$."! !.9 0.%5 0."! 0.39 9.33 $0 ".5# ".%# !.% 0.%# 0."3 0.39 333 ""0 ".!$ ".$9 !.$! 0.%# 0."! 0.#0 "0$ ""0.5MA5 0.3 !.5 !. !0.5 $0.# 0.0 "." !.% !".3 $9.3 ".3 #39.0 "."5 "$.3" !.9% 0.%% 0."3 0.#0 $".00 $0 !.0 "$."! !$."9 0.%5 0."# 0.#! 333 ""0 ".#! "$.#" !$.05 0.%% 0."# 0.## ""0 ""3MIN 0.0 0.0 0.0 "#." 9.5 0.0 "." !.% .0 $. ".! 3#0.0 "."0 "$.0" !.5% 0.%5 0."0 0.3 $.00 $0 "."$ "."9 !.#5 0.%! 0."" 0.3 333 ""0 ".0$ ".3 !.#5 0.%! 0."0 0.3% 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0$ 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,ULIO ARIA"LUI" MARIN'00 3#.$ "".0 3#.$ 0.# 3!.3 "." "0$ !99 5$.% 53.3 !5.% "5. !#.9 ".5 !". 5#.$$'00 3#.$ "".0 33.3 ".$ 3!.3 ".$ 93 3# 53.3 %9.0 !0.! %0.!9'00 35.5 "!.# 3#.$ 3.% 3!.3 !.! 90 359 #9.0 %.5 "9.9 %0.!"0'00 3#.$ "". 35." 3.! 3!.0 !.$ $% 3! ##. %.5 "9.5 5.""'00 3#.$ "". 3!.0 ".$ 3!.0 !.! $0 #00 !0.! 5%.%"!'00 3#.$ "". 33. !.! 3!.0 !.! $0 #00 "9.! %0.!"3'00 35." "". 33. !.% 3!.0 !.! $# 3$" #%.9 %5.0 "$.5 %!.""#'00 33. "". 3!. !.! 3!.0 !.! $9 3%0 "9.! 5$.#,UAN LA4O

D2ARD "AAV

DRA"5'00 3%.9 "".0 35.5 3. 33.# ".5 $$ 3$0 50.$ 5$.# !!. "9.0 !#." "$.3 !0.9 59.9"%'00 35.5 "".0 3#." 0. 3!.0 ".5 $# 3$" !0.9 5$.#"'00 35." "". 3#.# !.! 3!.0 ".$ ""0 !9" #9. %!.$ "9.5 %0.!"$'00 35.5 "". 3#." ".$ 3!.0 ".$ 90 35% !".3 %!.$"9'00 33.0 "".0 3".% 0. 3".! ".5 $% 3%3 3#.$ 3.0 "%.0 3".0 ".$ !3.0 "$.5 5#.$!0'00 3".% "0.! 3".! !.% 3".! ".$ 90 3# #%.! #.5 "%. 5.!"'00 33.0 "0.% 3!.0 ".$ 3".! ".$ 9% 3!5 "%. 59.9!!'00 3!.0 "0.! !9." 0.0 !9." ".5 90 3!3 #9. %0.! !!.0 "$.3 "9.0 5#.0CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 3!. "".0 3".! ".5 30.! "." 90 33% #.9 %3.9 !$.$ 30.3 !!.# !".9 30$0 !0.! 5#.$0'00 33.0 "".3 3!. ".5 30.! ".5 $0 3$ "9.9 5."'00 3#.# "". 33.# ".5 3".! ".5 $5 3% #.! %5.0 !!.# 59.9!'00 3#.$ "". 33. ".$ 3!. ".5 90 3%3 !0.9 5$.#3'00#'005'00%'00!ROM3#.3 "".3 33.! ".9 3". ".$ $9 35% #$.! %!.$ !3.3 !#.0 0 !!.! "9.$ 30$0 "9.$ 5$.#MA5 3%.9 "!.# 35.5 3. 33.# !.$ ""0 #00 5$.% 3.0 !$.$ 3".0 0 !#.9 !3.0 30$0 !!.# %!.$MIN 3".% "0.! !9." 0.0 !9." "." $0 !9" 3#.$ #.5 "%.0 "5. 0 ".$ ".5 30$0 "%. 5#.0P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0$ 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,ULIO ARIA"LUI" MARIN'00 "!.$ 3.% ".$ ".$$'00 "!.# 5.# !." ".$9'00 "0. 3.! !.5 !.5"0'00 "".# !.5 ".$ ".$""'00 "".0 !." ".# ".$"!'00 "".0 !." ".$ ".$"3'00 "". !.5 ".$ ".$"#'00 9.! !." ".$ ".$,UAN LA4O

D2ARD "AAV

DRA"5'00 "".# ".$ ".$ ".$"%'00 "!." #.% ".# ".#"'00 "0.3 #.3 !." !.""$'00 "0. !.$ !." !.""9'00 9.% 3.% !." !."!0'00 "0.3 !." !." !."!"'00 "0. !.5 ".# ".#!!'00 "".# !.5 ".# ".#CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 9.% !." ".# ".#0'00 "0. !." ".$ ".#"'00 "".# !." ".$ ".$!'00 "0.3 !.5 !." ".$3'00#'005'00%'00!ROM"0.9 !.$ ".$ ".$MA5 "!.$ 5.# !.5 !.5MIN 9.! ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 0$ 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,ULIO ARIA"LUI" MARIN'00$'00 0.0 !.5! !.39 "#.5 $0.! * * * "5.$ $#.!! ".!% #$9 0.$3 "$.%0 !9." 0.%# 0."0 0.39 $0.00 $0 ".!0 "$.#0 !$.$9 0.%# 0."0 0.3% "0# ""0 ".33 ".$9 !.9" 0.%# 0."" 0.#0 "0! ""09'00"0'00""'00"!'00"3'00 0.90 "9.#" !9.00 0.% 0."! 0.3% $0.00 $0 ".35 "$.9" !$."" 0.% 0."! 0.39 "0$ ""0 ".33 "$.%5 !.$3 0.% 0."3 0.3 "09 ""0"#'00,UAN LA4O

D2ARD "AAV

DRA"5'00"%'00 . . . "9.00 $".00 . . . !0.50 9.50 ".3! 5#" 0.$0 "$.$0 !$.00 0.% 0."! 0.#0 $0.00 $0 ".#0 "$.#0 !.%0 0.% 0."! 0.3% "0% ""0 ".0 "$.%0 !.0 0.% 0."3 0.3% "0% ""0"'00"$'00"9'00!0'00 "$.50 !.$0 0.% 0."" 0.#0 ".%0 "$.#0 !.0 0.%% 0."! 0.#"!"'00!!'00CARLO" 3

RNAND

4FRANCO MA%3UA!3'000'00 0.0$ ".$# !.!$ "!.$" $!.99 * * * "9."# $0.$% ".!# #09 ".#" "$.#5 !.$3 0.%% 0."! 0.#0 "0$ ""0 ".$" "$.5" !.$9 0.%% 0."3 0.#0 "0% ""0"'00!'003'00#'005'00%'00!ROM 0." !.! !.3 "5.5 $".# 0.0 0.0 0.0 "$.5 $".5 ".3 #9. 0.$# "$.9# !$.! 0.%% 0."" 0.3$ $0.00 $0 ".3# "$.53 !$.05 0.%% 0."" 0.3$ 333 ""0 ".55 "$.#" !.$" 0.%% 0."! 0.39 "0% ""0MA5 0." !.5 !.# "9.0 $3.0 0.0 0.0 0.0 !0.5 $#.! ".3 5#".0 0.90 "9.#" !9." 0.% 0."! 0.#0 $0.00 $0 ".#" "$.9" !$.$9 0.% 0."! 0.#0 333 ""0 ".$" "$.%5 !.9" 0.% 0."3 0.#" "09 ""0MIN 0." ".$ !.3 "!.$ $0.3 0.0 0.0 0.0 "5.$ 9.5 ".! #09.0 0.$0 "$.%0 !$.00 0.%# 0."0 0.3% $0.00 $0 ".!0 "$.#0 !.%0 0.%# 0."0 0.3% 333 ""0 ".33 ".$9 !.0 0.%# 0."" 0.3% 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0) 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,O"

A2UILARLUI" MARIN'00$'009'00"0'00""'00"!'00"3'00 "3." #3.#"#'00 !5.9 9.9 !#.9 ".5 !%.% ".5 %9 3$% 33. %.5 "9.5 #0.! "5.3 "". "#.! #3.",UAN LA4O

D2ARD "AAV

DRA"5'00 30.9 "!.0 30.5 !.% !$.0 0. %% #!# 35.5 %3.9 ".0 !0." !0.! !".9 "$." 5$.#"%'00 3".! "0.! !9.5 "." !9.5 "." 0 #!" ".$ 5!.%"'00 3".% "".0 !9.5 "." !9.5 "." 0 #!" ".$ 59.5"$'00 3!.0 "".0 30.5 ".$ !9.5 ".5 $0 3%9 ".$ %0.!"9'00 33.# "!.0 3!.0 "." !9.5 ".5 $% 3#3 #5.$ %5. !0.! "$.3 !0.% !0.$ "$." %#.%!0'00 33.0 "".0 3!.0 ".5 !9.$ ".5 $ 3$! "$." %0.!!"'00 33.0 "0.! 3".! "." 30.5 ".5 $% 355 "$.$ 59.5!!'00 33.0 "0.! 3!.0 ".5 3".! ".5 $0 390 !0.! 5$.0CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 3!.3 "".0 3".! ".5 !9.$ ".5 90 33" #".! %".3 !5.! !3.0 !".3 !".5 !0.% 55.$0'00 33.0 "".3 3!.0 ".$ 30.5 ".5 $$ 3# !0.! %".0"'00 33.0 "". 3!.3 ".$ 3".! ".5 90 3# ##.0 %0.! "$.5 5.!'00 3#.# "". 33.# !.! 30.! ".$ $% 35" #5." %$.% ".$ 59.93'00 3#.$ "".3 33.0 ".$ 3".! !.! $0 390 "9.9 5$.##'00 35.0 "". 33. ".$ 3!. ".$ $$ 3! "$.$ 59.95'00 3%.5 "".0 33. ".$ 3!.0 ".$ $! 390 #!.% 5$.# !$.# !!.% !". "9.3 "$.5 %0.!%'00!ROM3!. ""." 3".3 ".% 30." ".5 $" 3% #"." %#.9 !!." !#.$ 0 "9.$ "9.0 "$." 5.!MA5 3%.5 "!.0 33. !.% 3!. !.! 90 #!# #5.$ %.5 !$.# #0.! 0 !". !".9 !0.% %#.%MIN !5.9 9.9 !#.9 "." !%.% 0. %% 33" 33. 5$.# ".0 "$.3 0 "5.3 "". "3." #3."P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0) 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,O"

A2UILARLUI" MARIN'00$'009'00"0'00""'00"!'00"3'00"#'00 9.9 3.% ".# ".#,UAN LA4O

D2ARD "AAV

DRA"5'00 "#.9 #.3 3.% 3.9"%'00 "!.$ 3.9 !." !.""'00 "3.5 !.$ !." !.""$'00 "0.3 !.5 ".$ ".$"9'00 9.9 !." ".$ ".$!0'00 "0.3 !." ".$ ".$!"'00 "!." 3.% ".$ ".$!!'00 "0.3 !.$ !." !."CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 $.! ".$ ".$ ".$0'00 "0.3 ".$ ".# ".#"'00 "".0 !." ".$ ".#!'00 "!.$ !.5 ".$ ".$3'00 "".# !.$ !." ".$#'00 "". 3.! !." !."5'00 "3.$ 3.% !.5 !."%'00!ROM"".5 !.$ !.0 !.0MA5 "#.9 #.3 3.% 3.9MIN $.! ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 0) 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,O"

A2UILARLUI" MARIN'00$'00 0.0$ ".!3 ".50 "".0! $%." * * * !0."0 9.90 ".3! 5!09'00"0'00""'00"!'00"3'00"#'00,UAN LA4O

D2ARD "AAV

DRA"5'00"%'00 . . . "9."0 $0.90 . . . !0."0 9.90 ".!9 50""'00 ".%0 "$.%0 !.90 0.% 0."! 0.#0 "09 ""0 ".0 "$.0 !.90 0.% 0."! 0.## "0$ ""0"$'00"9'00!0'00!"'00 ".#0 "$.#0 !.90 0.%% 0."" 0.3% "0% ""0 ".90 "$."0 !.0 0.%5 0."! 0.#5 "0% ""0!!'00CARLO" 3

RNAND

4FRANCO MA%3UA!3'000'00 0."$ !.%! !.$0 "!.$" $".59 * * * !".#$ $.5! ".!5 #!$ "." ".95 !.$% 0.%# 0."3 0.3$ 9$.00 ""0 ".$" "$.!" !.$# 0.%5 0."! 0.39 "00 ""0"'00!'003'00#'005'00 ".5" "$.#9 !.$$ 0.%% 0."" 0.39 "05 ""0 ".#" "$.5# !.9$ 0.%% 0."! 0.#0 "05 ""0%'00!ROM 0." ".9 !.! "#.3 $!.9 0.0 0.0 0.0 !0.% 9.# ".3 #$3.0 0.00 0.00 0.00 0.00 ".5% "$.3% !.$9 0.%% 0."! 0.3$ 333 ""0 "." "$.39 !.$% 0.%% 0."! 0.#! "05 ""0MA5 0.! !.% !.$ "9." $%.! 0.0 0.0 0.0 !".5 9.9 ".3 5!0.0 0.00 0.00 0.00 0.00 "." "$.%0 !.90 0.% 0."3 0.#0 333 ""0 ".90 "$.0 !.9$ 0.% 0."! 0.#5 "0$ ""0MIN 0." ".! ".5 "".0 $0.9 0.0 0.0 0.0 !0." $.5 ".3 #!$.0 0.00 0.00 0.00 0.00 ".#0 ".95 !.$% 0.%# 0."" 0.3% 9$.00 ""0 ".#" "$."0 !.0 0.%5 0."! 0.39 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0+ 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,O"

A2UILARLUI" MARIN'00$'009'00"0'00""'00 30.! "".0 30.! !.$ !9." !.! "!3 !3 #!.% %9.# !9.$ 3#. ".# !".! "#.! #$.!"!'00 !5.% "0. !5.% !." !$.$ !.! 90 3!0 "$.5 ##.5"3'00 !.3 "0.# !%.3 ".5 !$.0 ".5 $% 3!% "$.5 #9.!"#'00 33.3 "".0 30.! 0. !$.# ".5 $5 33# #3.3 %0.! "9.5 %!.",UAN LA4O

D2ARD "AAV

DRA"5'00 3.0 "". 35." ".5 30.! 0.0 %$ ### 5"." ".! !!.0 "9.3 !3.# "9.3 !0.% 5."%'00 3#.$ "!.0 3#." ".$ 3".% 0.# %0 5! !0.! 5$.#"'00 3#.# "!.0 3#." #.0 3".% ".$ $% 3% #.9 %!.# "9.! %0.%"$'00 33. "!.# 33.0 !.! 3".% !.! $$ 359 "9.! 59.5"9'00 3#.# "". 33.0 ".$ 3".% ".$ ""# ! !0.! 59.9!0'00 3#.$ "!.0 3#.# ".$ 3!.0 ".$ 90 35% #3. 5$.0 !!.# "9. !3.# "$.3 "$.$ %!."!"'00 3#." "". 33.0 ".$ 3!.0 ".$ "0! 3"# "$.$ %0.%!!'00 33. "". 3!.0 ".5 3!.0 ".$ 9% 333 ##.# %0.% "$." 59."CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 33.0 "". 3!.0 ".$ 3".% ".$ 90 35" ##. 3.0 !#.9 35.0 !3." !5.! 3!$0 ".0 5.30'00 33. "". 3!. ".$ 3".! ".$ $$ 355 ".# 5%.9"'00 33.0 "".3 3!.3 ".$ 30.9 ".$ 95 3!5 "%. 5.3!'00 33. "". 33.0 ".$ 3!.0 ".$ 90 35% 5!.! %.! ".0 5.3'00 3#.# "".3 3!. ".$ 3!.0 ".$ 9# 3#0 ".# 5.3#'00 3!. "0.% 3!.0 ".$ 3".% ".$ ""9 !%% 53.3 %0.! !#.9 !%.# !". !0.$ "$.$ 53.35'00 33. "". 3!. ".$ 3".! ".$ "!0 !%0 "9.! 5$.0%'00 33.0 "".0 3!. ".5 3!.0 ".5 95 33 5!.9 %!.$ !0.% 5$.#!ROM33.0 "".5 3!." ".9 3".0 ". 9# 339 #.% %#.5 !#.$ !.0 0 !".$ !".0 3!$0 "$.5 5%.9MA5 3.0 "!.# 35." #.0 3!.0 !.! "!3 5! 53.3 3.0 !9.$ 35.0 0 !3.# !5.! 3!$0 !0.% %!."MIN !5.% "0.# !5.% 0. !$.0 0.0 %0 !3 #!.% 5$.0 !!.0 "9.3 0 ".# "$.3 3!$0 "#.! ##.5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0+ 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,O"

A2UILARLUI" MARIN'00$'009'00"0'00""'00 "0.# ." 0.% 3.%"!'00 "0.# 3.! !.5 !.!"3'00 "0.# ".$ !.! !.!"#'00 "".0 ".$ ".$ ".$,UAN LA4O

D2ARD "AAV

DRA"5'00 9.9 !.5 ".$ ".$"%'00 "".0 !.$ !." !.""'00 9.9 !." ".$ ".$"$'00 "!.# 3.! !." !.""9'00 "".0 !.$ !." !."!0'00 "0.3 ".$ ".$ ".$!"'00 9.9 !.5 ".$ ".$!!'00 "".# !.$ ".$ ".$CARLO" 3

RNAND

4FRANCO MA%3UA!3'00 9.% ".$ ".$ ".$0'00 "0.3 !." ".$ ".#"'00 9.% !." ".$ ".$!'00 "0.3 !.5 ".$ ".$3'00 "0. ".$ ".$ ".##'00 "0.3 !." ".$ ".$5'00 "".# !.$ !." ".$%'00 $.9 3.! !." !."!ROM"0.5 !.% ".9 !.0MA5 "!.# ." !.5 3.%MIN $.9 ".$ 0.% ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 0+ 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,O"

A2UILARLUI" MARIN'00$'00 0."! !."! ".9% "!.!0 $3.%0 ".39 "$.00 !.3% 0.%% 0."! 0.#" "0# ""09'00"0'00""'00"!'00"3'00"#'00,UAN LA4O

D2ARD "AAV

DRA"5'00"%'00 . . . "$.90 $"."0 . . . !0.90 9."0 ".! #3 "."0 "$.30 !.$0 0.%% 0."# 0.#0 $ $0 ".$0 ".$0 !.0 0.%# 0."3 0.#" ""0 ""0 ".90 "$." !.$0 0.% 0."# 0.3% "0$ ""0"'00"$'00"9'00!0'00 0.0 "$.50 !.$0 0.% 0."! 0.#0 ".#0 "$.0 !.90 0.% 0."0 0.#0 ".0 "$.#0 !.0 0.%% 0."0 0.3%!"'00!!'00CARLO" 3

RNAND

4FRANCO MA%3UA!3'000'00 0."% !.% !.$# "!.9! $".3! * * * "$.%3 $".3 ".!# #!$ "."0 "$."0 !.$" 0.%5 0."! 0.#0 9 $0 ".3$ ".$" !.$% 0.%# 0."" 0.#" "00 ""0 ".#$ "$.!3 !.$ 0.%% 0."! 0.#" "03 ""0"'00!'003'00#'005'00 ".00 "$.5" !.9# 0.%% 0."3 0.39 $" $0 ".!" ".9" !.#5 0.%5 0."! 0.39 "00 ""0 ".30 "$.33 !.$% 0.%% 0."! 0.39 "0# ""0%'00!ROM 0." !.# !.# "#. $!.0 0.0 0.0 0.0 "9.$ $0.! ".3 #50.5 0.9$ "$.35 !.$# 0.%% 0."3 0.#0 9.33 $0 ".#5 "$.0% !.3 0.%5 0."! 0.#0 333 ""0 ".55 "$.33 !.0 0.%% 0."! 0.39 "05 ""0MA5 0.! !.$ !.$ "$.9 $3.% 0.0 0.0 0.0 !0.9 $".# ".3 #3.0 "."0 "$.5" !.9# 0.% 0."# 0.#0 $".00 $0 ".$0 "$.0 !.90 0.% 0."3 0.#" 333 ""0 ".90 "$." !.$% 0.% 0."# 0.#" "0$ ""0MIN 0." !." !.0 "!.! $"." 0.0 0.0 0.0 "$.% 9." ".! #!$.0 0.0 "$."0 !.$0 0.%5 0."! 0.39 $.00 $0 ".!" ".$0 !.#5 0.%# 0."0 0.39 333 ""0 ".30 "$.00 !.3% 0.%% 0."0 0.3% 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0( 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,ULIO ARIA"LUI" MARIN'00 33. "0. 33. ".5 30.! ".5 ""$ !5% 5$.% %0.! !3.$ "9. !!.# "9.3 !0.% 5#.$$'00 35.9 "0. 3#.$ ".$ 30.! ".5 9% 3"5 5#.0 3.# !0.! 5$.#9'00 35.5 "".# 35.5 !.! 3!.0 ".5 90 35% 5$.9 %5.0 ".0 55.5"0'00 35.5 "0. 3#.% ".$ 3!. ".$ $! 399 "9.5 %0.!""'00 3.3 "".# 35.5 ".$ 33.3 ".5 $0 #"% !".3 5$.#"!'00 3.3 "".0 3%.! !.! 33. ".5 $5 39% #3.3 5"." !5.% "#.% !5.% ".! !!.0 5%.% 0.% $.9 3."3'00 39." "!.$ 3$.9 !.! 3#.# !.! $! #!0 5".$ 3.# !!. %0.!"#'00 39." "!.$ 3$.# !.! 33. !.! $9 39 !!. %0.!,O"

A2UILARLUI" MARIN"5'00 3%.! "". 3#.# !.% 3#.$ ".$ 90 3$ #%.9 %3.9 !!. !".9 !!.# !".5 !".3 5$.#"%'00 3.3 "". 33. "." 3#.$ ".$ "!! !$5 !".3 5%.9"'00 35.5 "!.$ 33. !.! 33. ".$ "0$ 3"! #%.9 3.# !0.% %0.!"$'00 35.5 "!.$ 35.5 !.! 33. !.! $9 39 #9.0 %9.# "9.9 5$.#"9'00 35.5 "". 3#.# !.! 33.3 ".$ $$ 3$ "9.9 5$.#!0'00 35.9 "". 3#.$ !.! 33.3 ".$ $0 #"% #".9 %.5 !0.% !#.5 "9.5 !3. "9.! 59.5!"'00 35.5 "". 3#.# ".$ 33.3 ".5 $! #0% "$.5 %0.!!!'00 35.5 "". 3#.$ ".5 33.3 ".5 $% 3$ "$.5 5$.#,UAN LA4O

D2ARD "AAV

DRA!3'00 3%.% "". 35.9 0. 33. 0. $% 39! #%.9 %9.# !0.9 "$.3 !3." "$.3 !0.! %!."0'00 3.% "!.# 3%.! ".5 33. "." $# #0" !0.9 5$.0"'00 3%.% "!.0 35.5 ".$ 33. ".5 $0 #!" #%.! %3.5 "9.! 59.5!'00 35.9 "".3 35." !.! 33.0 ".$ $% 3$# !0.! 5$.#3'00 35.5 "".3 3#.# ".$ 33.0 ".$ "0# 3" !0.! 59."#'00 35.5 "".0 3#.$ !.! 33.0 ".$ "0! 3!# #9.3 5%.% !5.! "9.3 !#.5 "%.# !0.9 5$.$5'00 35.9 "".0 3#.# ".5 3!.0 ".$ "00 3!0 !0.! 5$.#%'00 35.5 "".0 35." ".$ 3!.0 ".$ "0% 30! "9.! %5.!ROM3%.! "".% 35.! ".9 33." ". 9! 3%# #9.5 %5.% !3." "9. 0 !!.9 "9.# !0.3 5$.9 0.% $.9 3.MA5 39." "!.$ 3$.9 !.% 3#.$ !.! "!! #!" 5$.9 3.# !5.% !#.5 0 !5.% !3. !!. %5. 0.% $.9 3.MIN 33. "0. 33. 0. 30.! 0. $0 !5% #".9 5"." !0.% "#.% 0 "9.5 "%.# ".0 5#.$ 0.% $.9 3.P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0( 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 9.0 ".0 9.5 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." %.0 0 9.0 0,ULIO ARIA"LUI" MARIN'00 ." !." !.5 3.! $.0 0.00 9.3 0.00$'00 $.9 ".$ ".5 ".5 $.$0 0.00 9.05 0.009'00 $.5 ".$ ".5 ".5 $.# 0.00 9.05 0.00"0'00 "0.# 3.! ".5 ".5 $.9 0.00 9."0 0.00""'00 9.! 3.9 !." !." $.# 0.00 9."9 0.00"!'00 $.9 3.% ".$ ".$ $.$" 0.00 9."! 0.00"3'00 $.5 !.$ !.5 3.! $.#$ 0.00"#'00 $.9 !.5 ".$ ".$ $." 0.00 9.35 0.00,O"

A2UILARLUI" MARIN"5'00 $.9 !.5 ".$ ".$ $.$" 0.00"%'00 $.9 !.$ ".$ ".$ $.$$ 0.00 9.3$ 0.00"'00 $.! !.5 ".$ ".$ $.#! 0.00"$'00 9.9 !." ".$ ".$ $.#$ 0.00 9."0 0.00"9'00 $.$ ".$ ".5 ".$ $. 0.00 9.#" 0.00!0'00 .$ ".$ ".5 ".5 $.9 0.00!"'00 $.5 !." ".5 ".5 $.%5 0.00 9.!9 0.00!!'00 $.5 !." ".5 ".5 $.9# 0.00,UAN LA4O

D2ARD "AAV

DRA!3'00 .5 !.$ !." !."0'00 $.9 !.5 !." !.""'00 $.9 !." ".$ ".$!'00 9.9 3.% ".$ ".$3'00 .$ !.5 ".# ".##'00 $.9 ".$ ".# ".#5'00 9.! ".$ ".# ".#%'00 9.9 !.$ ".$ ".$!ROM$.$ !.5 ".$ ".$ $.3 0.00 9.!! 0.00MA5 "0.# 3.9 !.5 3.! $.9 0.00 9.#" 0.00MIN ." ".$ ".# ".# $.#! 0.00 9.05 0.00P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 0( 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,ULIO ARIA"LUI" MARIN'00$'00 0."$ !.%# !.5 "!.! $!.3# . . . "9."! $0.$$ ".!% #9! "$."# !.#5 0.%% 0."! 0.39 $0.00 $0 ".9% !.5# 0.%5 0."! 0.3% "0# ""0 "$."! !.#5 0.%% 0."3 0.#0 "0% ""09'00"0'00""'00"!'00"3'00 0.9% "$.5! !.53 0.% 0."0 0.39 $".00 $0 ".!$ "$.99 !.#9 0.%9 0."0 0.#0 "0 ""0 ".3# "$.9# !.#3 0.%9 0."0 0.39 "09 ""0"#'00,O"

A2UILARLUI" MARIN"5'00"%'00 0.0$ ".9% !.#" "".5 $3.$0 * * * "."! $!.$$ ".!# #!3 0.$# "$.%! !$."! 0.%% 0."0 0.39 $0.00 $0 ".3# "$.#3 !.#5 0.% 0."0 0.3% "05 ""0 ".!$ "$.5! !.95 0.%% 0."0 0.3% "09 ""0"'00"$'00"9'00!0'00!"'00 0.9% "$.5" !.$9 0.%% 0."0 0.3 .00 $0 ".!$ "$.!3 !.5% 0.%% 0."0 0.3% "0 ""0 ".3" "$.#3 !.$9 0.%% 0."0 0.39 "0# ""0!!'00,UAN LA4O

D2ARD "AAV

DRA!3'000'00 . . . "$.$0 $".!0 . . . !0.00 $0.00 ".!% #$0 0.$0 "$.90 !.0 0.%$ 0."0 0.#0 $.00 $0 ".%0 "$.%0 !.%0 0.% 0."0 0.39 "0% ""0 ".%0 "$.0 !.%0 0.%$ 0."0 0.39 "0% ""0"'00!'003'00#'00 0.90 "$.$0 !.0 0.%$ 0."" 0.3$ %.00 $0 ".#0 "$.#0 !.%0 0.% 0."0 0.#0 "0% ""0 ".30 "$.!0 !.#0 0.%% 0."0 0.39 "0$ ""05'00%'00!ROM 0." !.3 !.5 "#.3 $!.# 0.0 0.0 0.0 "$. $".3 ".3 #%5.0 0.$9 "$.5$ !.3 0.% 0."" 0.39 $.% $0 ".3$ "$.## !.5# 0.% 0."0 0.3$ 333 ""0 ".3 "$.#9 !.%! 0.% 0."" 0.39 "0 ""0MA5 0.! !.% !.% "$.$ $3.$ 0.0 0.0 0.0 !0.0 $!.9 ".3 #9!.0 0.9% "$.90 !$."! 0.%$ 0."! 0.#0 $".00 $0 ".%0 "$.99 !.%0 0.%9 0."! 0.#0 333 ""0 ".%0 "$.9# !.95 0.%9 0."3 0.#0 "09 ""0MIN 0." !.0 !.# "".$ $".! 0.0 0.0 0.0 "." $0.0 ".! #!3.0 0.$0 "$."# !.#5 0.%% 0."0 0.3 %.00 $0 ".!$ ".9% !.#5 0.%5 0."0 0.3% 333 ""0 ".!$ "$."! !.#0 0.%% 0."0 0.3% 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0# 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0CARLO" 3

RNAND

4LUI" MARIN'00 35.5 9.9 33. ".5 3!.3 ".$ 9$ 330 #0.$ %9.# !0.% !3.0 !0.% !".9 "$.$ 5.3$'00 3#.$ "". 3#.# !.! 3!.0 ".$ 90 35% "$.5 59."9'00 35." "".0 33. ".5 3!.0 ".$ $% 3! "9.! %3.5"0'00 35." "!.# 35." ." 3!.0 ".$ $9 3%0 ##.$ %3. "9.! %0.!""'00 35.5 "". 3!.0 !.! 3!.3 !.! $$ 3% "9.! 5$.#"!'00 35." "". 3#.$ !.! 3!.3 !.! $0 #0# "9.! 5$.#"3'00 3#.$ "". 3#.$ !.% 3!.0 !.! $% 3! #%.9 %9.# "9.5 !!.3 "9.9 !".9 "9.5 5.3"#'00 3#.# "". 3!. ".5 3!.0 ".$ $! 390 "$.$ 5%.%,UAN LA4OLUI" MARIN"5'00 3#.# "".0 33. 3.! 3!.0 ".$ 93 3## #5.$ %0.! !0.! !".! "9.9 !".9 !"00 "$.5 5%.%"%'00 3#.$ "".0 33.3 3.9 3".% !.! $% 3% ".$ 5$.#"'00 3#.$ "". 3#.$ 3.! 3".% !.! 9! 3#3 !0.% 59.""$'00 3%.9 "3.9 35.5 3.9 3".% !.! $5 3! #".5 %9.# !".3 5$.#"9'00 3%.9 "!.# 35.9 !." 3!.0 !.! $0 #00 !!.# 5$.#!0'00 3.3 "!.# 35.9 ".$ 3!. !.! $% 3$0 3.3 %5.0 !5.! "9.0 !5.9 "9.3 !5.% 5$.#!"'00 3$.# "!.# 3%.9 ".$ 3!. !.! $9 3% !5.! 5$.#!!'00 39." "!.# 35.5 "." 33.3 !.! 90 30 !#.9 5$.#,O"

A2UILAR

D2ARD "AAV

DRA!3'00 3%.9 "". 35." 0.# 3#.$ ".$ "$0 "93 #0.$ ".! !#.9 !5.! !!.0 "9. !0.9 5$.#0'00 3%.% "". 3#.$ ".5 3#." ".5 "#! !#0 !0.9 5$.$"'00 3%.! "". 35.9 5.5 33. ".$ "0! 330 #.! %5.3 "9.5 %".3!'00 3%.% "". 35." ".$ 33. ".$ ""% !9" "9.9 %0.%3'00 3%.! "". 35.5 ".$ 33. ".$ ""# !9% "9.9 %0.%#'00 3#.$ "".0 33. ".$ 33. ".$ "00 33 #!.! %0.! !3.# !3.0 !!. !".! !0.% 5%.!5'00 35.5 "".0 3#.# ".$ 33. ".$ "0% 3"$ !0.! 5$.$%'00 35.5 "".3 3#." "." 3!.0 ".5 90 35% !0.% 5$.#!ROM35.9 "". 3#.% !.# 3!. ".9 9$ 3## #3.0 %%.0 !!.3 !!.3 0 !".$ !".0 !"00 !0.5 5$.$MA5 39." "3.9 3%.9 ." 3#.$ !.! "$0 #0# #.! ".! !5.! !5.! 0 !5.9 !".9 !"00 !5.% %3.5MIN 3#.# 9.9 3!.0 0.# 3".% ".5 $0 "93 3.3 %0.! "9.5 "9.0 0 "9.9 "9.3 !"00 ".$ 5%.!P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 0# 0# 1$!RCI!ITACION % LAVADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0CARLO" 3

RNAND

4LUI" MARIN'00 9.9 ".$ ".# ".#$'00 $.9 ".$ ".# ".#9'00 "0. !." ".# ".#"0'00 $.# !." ".# ".#""'00 "0. !.5 ".$ ".#"!'00 $.5 !." ".$ ".#"3'00 $.5 !." ".$ ".$"#'00 9.9 !.5 ".$ ".$,UAN LA4OLUI" MARIN"5'00 $.9 !.5 ".$ ".$"%'00 9.9 !.$ ".$ ".$"'00 9.% 5.# !.5 !.5"$'00 $.9 3.% 3.! !.5"9'00 $.! !.$ !.5 !."!0'00 ." ".$ "." ".$!"'00 .5 !." ".$ ".$!!'00 .$ !." ".$ ".5,O"

A2UILAR

D2ARD "AAV

DRA!3'00 $.! !.$ !." !."0'00 $.9 !.5 ".$ ".$"'00 ." !.5 ".$ ".$!'00 $.! !." ".$ ".$3'00 $.! !." ".$ ".$#'00 $.5 !.$ !." !."5'00 .$ !.5 !." !."%'00 %. !." ".$ ".$!ROM$. $.# !.5 ".9 ".$MA5 "0. 9.9 5.# 3.! !.5MIN %. ." ".$ "." ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 0# 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90CARLO" 3

RNAND

4LUI" MARIN'00$'00 * * * "$.93 $".0 * * * "5.!3 $#. ".!0 3%0 0.93 "$.3# !$.00 0.%% 0."0 0.#0 % $0 "."0 "$."! !.#5 0.%% 0."0 0.3% "03 ""0 ".30 "$.5" !.#5 0.% 0."0 0.3% "09 ""09'00"0'00""'00"!'00"3'00 0.$5 ".$9 !.#5 0.%5 0."" 0.3 9 $0 ".!# ".%5 !.#5 0.%# 0."0 0.3% "0% ""0 ".3$ "$."! !.9% 0.%5 0."# 0.3" ""0 ""0"#'00,UAN LA4OLUI" MARIN"5'00"%'00 * * * "9.!# $0.% * * * ".$5 $!."5 ".!5 #5 0.9# "$.00 !$.00 0.%# 0."0 0.39 $0 $0 ".3# ".$5 !.$# 0.%# 0."" 0.3$ "03 ""0 ".! ".55 !.#5 0.%# 0."" 0.3% "0 ""0"'00"$'00"9'00!0'00!"'00 "."0 "$.5# !.9% 0.%% 0."" 0.39 $ $0 ".!5 "$.!5 !."! 0.% 0."" 0.39 "05 ""0 ".30 "$.5# !.5% 0.% 0."! 0.3 "05 ""0!!'00,O"

A2UILAR

D2ARD "AAV

DRA!3'000'00 . . . "9.%0 $0.#0 . . . "$.!0 $".$0 ".!# #%0 ".00 "$.!0 !.90 0.%5 0."" 0.3% $0 $0 ".%0 "$."0 !.$0 0.%5 0."" 0.#0 "0# ""0 ".50 "$.30 !$.00 0.%5 0."" 0.3$ ""0 ""0"'00!'003'00#'00 ".#0 "$.%0 !$."0 0.%% 0."" 0.#0 $0 $0 ".0 "$.#0 !.$0 0.%% 0."! 0.#" "0% ""0 ".%0 "$.!0 !.0 0.%% 0."! 0.#0 "0% ""05'00%'00!ROM 0.0 0.0 0.0 "9.3 $0. 0.0 0.0 0.0 "." $!.9 ".! #!5. ".0# "$.!% !.90 0.%5 0."" 0.39 $.$3 $0 ".3 "$.0% !.5$ 0.%% 0."" 0.3$ 333 ""0 ".39 "$.!0 !.%9 0.%% 0."! 0.3% "0$ ""0MA5 0.0 0.0 0.0 "9.% $"." 0.0 0.0 0.0 "$.! $#.$ ".3 #%0.0 ".#0 "$.%0 !$."0 0.%% 0."" 0.#0 $0.00 $0 ".0 "$.#0 !.$# 0.% 0."! 0.#" 333 ""0 ".%0 "$.5# !$.00 0.% 0."# 0.#0 ""0 ""0MIN 0.0 0.0 0.0 "$.9 $0.# 0.0 0.0 0.0 "5.! $".$ ".! 3%0.0 0.$5 ".$9 !.#5 0.%# 0."0 0.3% %.00 $0 "."0 ".%5 !."! 0.%# 0."0 0.3% 333 ""0 ".! ".55 !.#5 0.%# 0."0 0.3" 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 08 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0C*3ernan7e.A*!achas'00 33. $.$ 30.5 0. !9." "." !%0 ""! #%.! %3." !0.! !!.% ".0 "9. !".3 #%.0$'00 33.# "0.% 3!.3 "." !9." ".5 !00 "#% "9.$ 5$.39'00 33.# "!.# 3!.3 !.% !$.# 0. "0% !%$ "9.! 5%.!"0'00""'00"!'00 3!.3 "!.0 3!.0 !.% !$.# ".$ ""0 !5$ #5.$ 3.# !".3 !.0 "9.! ".5 "$.% 5%.$"3'00 3".! "!.0 !9." 3. !$.# "." "0% !%$ #!.$ %3.5 "%. 5#.#"#'00 3".% 30.5 30.5 !.% !9.$ ".$ 9$ 30# "%. 50.#,UAN LA4O FRANCO MA%3UA "5'00"%'00 !$.# $.$ !%.% ".5 !%.3 !.! "! !0 #!.% 3.0 !!. !3.# !0.! "$.3 !33# "#.! #5.3"'00 3".! 9.5 !9.$ "." !$.# ".5 90 3"% #%.5 %$.3 "9.! 53.3"$'00 3#.$ "".0 33. !.! !9.5 ".$ $$ 335 39." $.# "9.5 55.""9'00 35." "". 33.0 !.! 30.! !.! 95 3"$ !".3 59.5!0'00 3%.! "3.5 3#.$ 3.3 30.! !.! $! 3%$ 39.$ ." !3." 5$.$!"'00 3#.$ "!.# 33.0 !.! 3".% 3.3 90 35" 30.! !.# !!. "9.3 !!. 5$.0!!'00 3%.% "!.0 3#.$ !.% 3!.0 !.! ""$ !" 3$.0 3.# !3." 59.5,O"

A2UILAR

D2ARD "AAV

DRA!3'00 3%.! "3." 35." 0.0 3#." "." !0% "%% #3.3 %5. "$.$ "%.# !!.# "%.$ !". 5$.00'00 3%.% "!.0 35.9 ".$ 33. "." "#0 !#" !". 5$.$"'00 3%.! "3.9 35.5 3. 33.0 ".$ 9% 3## #.9 ".9 !0.% 59.5!'00 35.9 "!.0 3#." ".5 33.0 ".$ ""% !$# !". 59.93'00 3#." "!.# 33.0 !.! 3!.0 ".$ "0# 30$ #%.! %". "$." 5$.0#'00 3".% "". 30.! "." 30.5 ".5 ""% !%3 "$." 5#.#5'00 33.0 "".0 3!.0 ".$ 30.! ".5 "0# !90 #$.3 %0.! !0.% ".9 !!. ".! "$." 5$.$%'00 3%.9 "3.9 3%.% 3.3 30.9 ".$ "0% !9! !".3 %#.!!ROM3#.0 "!.% 3!.% !." 30.# ". "!! !! #3.9 %9." !!.3 !!.5 0 !0. "5.5 !33# "9.$ 5%.3MA5 3%.9 30.5 3%.% 3. 3#." 3.3 !%0 3%$ #$.3 $.# 30.! !.# 0 !!. "9. !33# !3." %#.!MIN !$.# $.$ !%.% 0.0 !%.3 0. $! ""! 3$.0 %0.! "$.$ "%.# 0 ".0 ".5 !33# "#.! #5.3P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 08 0# 1$!RCI!ITACION % LAVADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0C*3ernan7e.A*!achas'00 %.0 ".$ ".# ".$$'00 %. ".$ ".# "."9'00 !.5 ".$ ".$"0'00""'00"!'00"3'00 $.9 !.5 ".$ ".$"#'00 "".0 %.0 !." ".$,UAN LA4O FRANCO MA%3UA "5'00"%'00 %.# 3.% !.$ !.5"'00 "!.$ 3.! !." ".$"$'00 "!." #.% !." ".$"9'00 9.9 3.! ".$ ".$!0'00 "".# !.5 ".$ ".$!"'00 "".0 3.! ".$ ".$!!'00 $.! 3.% !." ".$,O"

A2UILAR

D2ARD "AAV

DRA!3'00 "0.3 3.! !." !."0'00 9.% 3.! !." !.""'00 "0.3 !.5 ".$ ".$!'00 "0.3 !.$ ".$ ".$3'00 9.9 !.5 ".$ ".$#'00 9.! !.5 ".$ ".$5'00 9.! !." ".$ ".$%'00 9.! ".$ ".$ ".$!ROM%.# "0.0 3.0 ".9 ".$MA5 %. "!.$ %.0 !.$ !.5MIN %.0 %.# ".$ ".# "."P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 08 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90C*3ernan7e.A*!achas'00$'00 0.00 0.00 0.00 "9.#$ $0.5! 0.00 0.00 0.00 ".9 $!.03 ".!% 3$".00 ".!% "$.%0 !$."$ 0.%% 0."3 0.#0 $0 $0 ".$0 "$.55 !.$ 0.% 0."# 0.#! "05 ""0 ".30 "$.! !.$5 0.%% 0."! 0.#! ""0 ""39'00"0'00""'00"!'00"3'00 0.9$ "$.!5 !$.5" 0.%# 0."! 0.3$ $0 $0 ".30 "$.05 !$.!% 0.%# 0."3 0.#0 "05 ""0 ".5% "$.!3 !$.3% 0.%# 0."3 0.#0 ""0 ""3"#'00,UAN LA4O FRANCO MA%3UA "5'00"%'00 0.3# !.93 !.9" "!.3 $".#5 * * * !#.## 5.5% ".! #5! ".!! "$."" !$."0 0.%# 0."% 0.#0 9 $0 ".#0 ".$% !.$" 0.%# 0."3 0.#! 9$ ""0 ".3$ "$.0! !.5% 0.%5 0."% 0.39 "00 ""0"'00"$'00"9'00!0'00!"'00 "."0 "$.#$ !.$$ 0.%% 0."3 0.39 $" $0 ".!$ ".9$ !.%$ 0.%5 0."3 0.39 "00 ""0 ".!9 "$.%" !.$$ 0.% 0."# 0.#0 "0% ""0!!'00,O"

A2UILAR

D2ARD "AAV

DRA!3'000'00 . . . "$."0 $".90 . . . !!."0 .90 ".!% #%0.00 ".00 "$.#0 !.90 0.%% 0."% 0.#" $ $0 ".%0 "$.%0 !$."0 0.%% 0."% 0.#0 "00 ""0 ".50 "$."0 !.%0 0.%% 0."% 0.## "0% ""0"'00!'003'00#'00 "."0 "$.30 !$.00 0.%5 0."$ 0.#0 $0 $0 ".90 "$.30 !$."0 0.%5 0."$ 0.#! "00 ""0 ".0 "$.00 !.#0 0.%% 0."$ 0.#" "0$ ""05'00%'00!ROM 0.! ".5 ".5 "%. $".3 0.0 0.0 0.0 !".5 $.5 ".3 #3".0 "."" "$.3% !$."0 0.%5 0."5 0.#0 9.% $0 ".55 "$.!! !.9% 0.%5 0."5 0.#" 333 ""0 ".#% "$.!" !.$ 0.%% 0."5 0.#" "0 """MA5 0.3 !.9 !.9 "9.5 $".9 0.0 0.0 0.0 !#.# $!.0 ".3 #%0.0 ".!% "$.%0 !$.5" 0.%% 0."$ 0.#" $".00 $0 ".90 "$.%0 !$.!% 0.% 0."$ 0.#! 333 ""0 ".0 "$.%" !$.3% 0.% 0."$ 0.## ""0 ""3MIN 0.0 0.0 0.0 "!.# $0.5 0.0 0.0 0.0 "$.0 5.% ".3 3$".0 0.9$ "$."" !.$$ 0.%# 0."! 0.3$ $.00 $0 ".!$ ".$% !.%$ 0.%# 0."3 0.39 9$.00 ""0 ".!9 "$.00 !.#0 0.%# 0."! 0.39 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 09 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0C*3ernan7e.A*!achas'00 33. "3.5 3!.0 !.% 30.! ".$ "#0 !"% #".5 ".5 !3.# !".5 !!.3 "$.3 "9.5 55.$$'00 3#." "".0 33.0 !." 3".! ".$ "%! "93 #!.3 0.# "$.$ 5$.09'00 3!.0 "3.5 3".% !.$ 30.5 !." "30 !35 ".$ 5#.$"0'00 33.0 "!.0 3".! 3. !9.5 !.% "!$ !30 50.$ 5!.! !!. !!.% !".3 "9. ".$ 5#.$""'00 3!.3 "3.5 3".! !." !9.5 ".$ "00 !95 "$." 55.5"!'00 3!.0 "3." 30.9 !." !9.5 ".$ 9% 30 "$.5 55.5"3'00 3!.3 "!.# 3".! ".$ !9.5 ".$ 9! 3!" #$." 55.$ "$.5 5%.#"#'00 3#.# "!.# 3!.3 !.5 30.! ".$ 9! 3!$ "$.$ 5.,UAN LA4O FRANCO MA%3UA "5'00 33.# "!.0 33.0 !.% !9." !.% 9$ !9 #3.% %.5 "$.$ ".! !!. "5.0 !"00 ".$ %0.%"%'00 3#.# "!.0 33.0 !.! 30.! !.% ""0 !5 ".9 59.5"'00 3#.$ "". 33.# ".$ 3".% !.! 9! 3#3 5!.9 5$.0 "9.! 5$.0"$'00 3%.! "". 3#.# !.% 3!.0 ".$ "!0 !% 5!.9 5".$ "$.9 %!.""9'00 3#.$ "!.0 33.# ".$ 3!.0 !.! 9$ 3! #5.# 5. ".9 %0.%!0'00 35.5 "".0 33. 0.# 33.0 "." "!5 !%# "$.5 %!."!"'00 3#.$ "".3 33.0 ".$ 3!. 0.# 95 3## #%.5 %!." !#.5 "9. ".$ ".5 "9.! %0.!!!'00 3#.# "". 33.# ".$ 3!.0 ".5 ""! !$% !0.9 5.,O"

A2UILARLUI" MARIN!3'00 3.3 "".0 3.3 !.% 3#.# ".5 ""0 3"3 #.! %!." !".3 "9.3 !3.# "!.$ "9.9 %%.#0'00 35.9 "".0 35.5 ".5 33. ".5 9% 35" "$.$ 5$.#"'00 3.3 "!.$ 3#.$ 3.! 3!. ".$ 90 3%3 #".9 %$.0 "9.! %!.$!'00 3#.$ "". 33. 3.! 33. !.! $! #"" ##. %9.# "$.$ 5%.%3'00 3#.$ "".0 3#.$ !." 33. !.! $$ 3$3 "$.$ 5$.##'00 35." "".0 33.3 0.0 33.3 ".$ $% 3$ ##.# %0.! !0.% ".5 !0.% "$.% "$.5 %0.!5'00 3*#*# "!.# 33. ".$ 33.3 ".$ $9 3# "9.9 59."%'00 35.5 "". 3#.$ ".$ 33.3 ".$ 90 30 "9.! %0.!!ROM3#.5 "!.0 33.3 !." 3". ".9 "05 3"! #%.3 %!." !".9 "9.% 0 !".# ".0 !"00 "$.$ 5$.$MA5 3.3 "3.5 3.3 3. 3#.# !.% "%! #"" 5!.9 ".5 !#.5 !!.% 0 !3.# "9. !"00 !0.9 %%.#MIN 3!.0 "".0 30.9 0.0 !9." 0.# $! "93 #".5 5".$ "$.$ ".! 0 ".$ "!.$ !"00 ".$ 5#.$P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 09 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." 9.! 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 9.0 ".0 9.5 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." %.0 0 9.0 0C*3ernan7e.A*!achas'00 $.9 !." ".# ".$ $.0! 0.00$'00 9.! !." ".$ ".$ $."% 0.009'00 9.5 !." ".# ".$ .9$ 0.00 9."0 0.00"0'00 "".0 !.$ !." ".$ $."0 0.00 9.!3 0.00""'00 9.9 !.5 ".$ ".$ 9.00 0.00 9.0$ 0.00"!'00 9.9 !.5 ".$ !." $.9$ 0.00 9."9 0.00"3'00 9.9 !.5 !." !." $.$% 0.00"#'00 "".# 3.% !.5 !." $.90 0.00 9."0 0.00,UAN LA4O FRANCO MA%3UA "5'00 9.! !.5 !." !." $.#3 0.00 9.## 0.00"%'00 "".0 !." !." ".$ $.!" 0.00 9.0% 0.00"'00 $.5 !." ".$ ".$ $.95 0.00 9.3" 0.00"$'00 9.9 ".$ ".$ ".$ $.!9 0.00 9.3! 0.00"9'00 "".0 !." ".$ ".$ $.#! 0.00 9."" 0.00!0'00 $.9 3.% ".$ ".$ $."0 0.00 9.30 0.00!"'00 9.9 3.! !." ".$ $.!# 0.00 9."5 0.00!!'00 "0.3 3.! !." !." $.3% 0.00 9.!# 0.00,O"

A2UILARLUI" MARIN!3'00 "".0 3.% ".$ !." $.5$ 0.000'00 9.9 3.% ".$ ".$ $.#0 0.00"'00 .$ !." !." ".$ $.!" 0.00 9.#% 0.00!'00 9.% !.5 ".$ ".$ $.3$ 0.00 9.!0 0.003'00 9.9 !.5 ".$ ".$ $.%5 0.00 9.## 0.00#'00 9.9 !.5 ".$ ".$ $.#5 0.00 9.! 0.005'00 $.5 !.$ ".$ ".$ $.35 0.00 9."5 0.00%'00 9.9 !.5 ".$ ".$ $.% 0.00 9.0 0.0!ROM9.$ !.% ".9 ".9 $.#5 0.00 9.!! 0.00MA5 "".# 3.% !.5 !." 9.00 0.00 9.#% 0.00MIN .$ ".$ ".# ".$ .9$ 0.00 9.0% 0.00P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 09 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90C*3ernan7e.A*!achas'00$'00 0.00 0.00 0.00 ".9" $!.09 0.00 0.00 0.00 !0.03 9.9 ".!$ #3$ ".9! ".9! !$.05 0.%# 0."$ 0.39 $0.00 $0 3.3" ".95 !.$! 0.%5 0."% 0.#0 "00 "00 ".!" "$.!% !$.# 0.%# 0." 0.#0 ""3 ""09'00"0'00""'00"!'00"3'00 0.00 0.00 0.00 !!.%3 .3 ".!# 39 ".30 "$.0! !.$9 0.%5 0."% 0.3$ $0 $0 "$."9 !$."% 0.%5 0."# 0.#0 "05 "05 ".3$ "$.0# !$.#0 0.%# 0."% 0.#0 ""3 ""0"#'00,UAN LA4O FRANCO MA%3UA "5'00"%'00 0.!% !.0! !."3 "!."" $3.#$ ".!$ "$.%! !.$$ 0.% 0." 0.#! 9 $0 ".## ".9! !.%$ 0.%5 0."% 0.#3 "00 ""0 ".30 "$.!# !.%$ 0.%% 0."$ 0.#! "0% ""0"'00 * * * !!.0% .9# ".!5 ##$"$'00"9'00!0'00!"'00 ".!! "$.%% !.$% 0.% 0."5 0.#0 $" $0 ".5$ "$.00 !.$$ 0.%5 0."5 0.39 "00 ""0 ".3! "$.#$ !. 0.% 0."% 0.39 "05 ""0!!'00,O"

A2UILARLUI" MARIN!3'000'00 0."$ !."! ".9% "".5 $3.99 * * * "9.#" $0.59 ".!! #!".00 0.9% "$.5" !.9% 0.%% 0."# 0.#5 $0.00 $0 ".!! "$.#" !.$5 0.%% 0."# 0.3% "0 ""0"'00!'003'00#'005'00 "."! "$.! !.$9 0.%% 0."! 0.#0 $0.00 $0 ".!% "$.3 !.% 0.%% 0."! 0.39 "0! ""0 ".3# "$.!! !.#5 0.%% 0."! 0.39 "0% ""0%'00!ROM 0." ".# ".# "3.9 $3.! 0.0 0.0 0.0 !".0 9.0 ".! #!%.0 ".30 "$.33 !.9! 0.%% 0."5 0.#" $0.00 $0 ".90 "$.09 !.$% 0.%5 0."5 0.#0 333 "0 ".30 "$.!$ !.9# 0.%5 0."% 0.39 "0$ ""0MA5 0.3 !." !." ".9 $#.0 0.0 0.0 0.0 !!.% $0.% ".3 ##$.0 ".9! "$.%% !$.05 0.% 0."$ 0.#5 $".00 $0 3.3" "$.3 !$."% 0.%% 0."% 0.#3 333 ""0 ".3$ "$.#$ !$.# 0.% 0."$ 0.#! ""3 ""0MIN 0.0 0.0 0.0 "".$ $!." 0.0 0.0 0.0 "9.# .# ".! 39.0 0.9% ".9! !.$% 0.%# 0."! 0.3$ 9.00 $0 ".!% ".9! !.%$ 0.%5 0."! 0.39 333 "00 ".!" "$.0# !.#5 0.%# 0."! 0.3% 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 10 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0 CARLO" 3

RNAND

4 FRANCO MA%3UA '00 3#.$ "!.$ 33.# !.% 33.0 !.! 9$ 33 #.9 %3." !!.# !3.0 "9.9 "9.0 "9.! 5%.%$'00 35.5 "!.0 33. ".$ 3!. !.! "00 3! !0.% 5$.99'00 3#.# "". 33. !.9 33.0 ".$ 95 3# 50.$ %$.% !".3 55.""0'00 3#.$ "". 33.0 !.! 35. !.% 9$ 3%# !0.% 5$.$""'00 35." "". 3#.$ ".$ 3!.0 !.! $5 3% 5".5 5$.# "9.5 5.3"!'00 3#.$ "".3 33.0 !.! 3!. ".$ 90 3%3 !0.% 5.3"3'00 33.0 "". 3!. !.! 3!.0 !.! $$ 3%# #9. %!." !#.% "$.3 !0.% "%.$ "9.! 5#.#"#'00 33.# "".0 33.0 ".$ 3!. !.! "00 3! !0.% 5.,-an La./A0e18 !achas"5'00"%'00"'00"$'00 "%. #$.9"9'00 33. $.! 3".% 3.% 30.! 3.3 !00 "5" "$.% 3.$!0'00 3!.3 $.0 3".! 3.3 30.! !.% "%0 "$9 39." 5".5 !3.$ "9. "$.$ "%.$ ".$ #5.%!"'00 33. 9.5 3".% 3.% !9.5 3.3 "$0 "%# "$." #$.9!!'00 3".# "0.% !$.# "." !.3 !." "%! "%9 "5.% %0.%,O"

A2UILAR

D2ARD "AAV

DRA!3'00 35.9 "".3 35.5 3. 33.0 3.3 !9% """ "9.! %!."0'00"'00 33.0 3. "## !!9!'003'00#'005'00%'00!ROM3#." "0.9 3!. !.5 3".9 !.5 "35 !3 #.$ %0. !3.% !0.3 0 "9.$ ".5 "9." 5%.9MA5 35.9 "!.$ 35.5 3. 35. 3. !9% 3% 5".5 %$.% !#.% !3.0 0 !0.% "9.0 !".3 3.$MIN 3".# $.0 !$.# "." !.3 ".$ $5 """ 39." 5".5 !!.# "$.3 0 "$.$ "%.$ "5.% #5.%P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 10 0# 1$!RCI!ITACION % LAVADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0 CARLO" 3

RNAND

4 FRANCO MA%3UA '00 9.! ".$ ".# ".#$'00 "0.3 !.5 ".# ".#9'00 "".# 3.! !." ".$"0'00 9.! 3.% !." !."""'00 "0. 3.% !.5 !.""!'00 "0.3 !.$ !." !.""3'00 "0. 3.! !." !.""#'00 "!.# !.$ !." !.",-an La./A0e18 !achas"5'00"%'00"'00"$'00"9'00 "#.$ 5.! !.$ !.$!0'00 "3." #.% !.$ !.$!"'00 "!.# 3.% !.5 !.5!!'00 "0.% 3.! !." !.",O"

A2UILAR

D2ARD "AAV

DRA!3'00 "!.# 3.% !.$ !.$0'00 "0. 3.! !." !.""'00 "#.! !.$ !.5 !.5!'00 "". 3.! ".$ ".$3'00 "!.# 3.% !." !."#'005'00%'00!ROM"!.5 "0.5 3.3 !.! !.!MA5 "#.$ "!.# 5.! !.$ !.$MIN "0.% 9.! ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 10 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 CARLO" 3

RNAND

4 FRANCO MA%3UA '00$'00 0.0$ ".55 ". "".$! $#.$ * * * "%.3! $3.%$ ".!# #0# "."$ "$.%# !.33 0.%$ 0."3 0.#" 9 $0 ".!! "$.$3 !.$ 0.%$ 0."3 0.#! "0" ""09'00"0'00""'00"!'00"3'00 ".!! "$.3" !.#3 0.% 0."3 0.#0 $0 $0 ".30 "$.5" !.5 0.% 0."! 0.#0 "0 ""0 ".!$ "$.%" !.$# 0.% 0."3 0.#" "0% ""0"#'00,-an La./A0e18 !achas"5'00"%'00"'00"$'00"9'00!0'00 * * * "%.5# $3.#% * * * ".#0 $!.%0 ".!0 3%0.00 ".!" "$.5" !$.5# 0.%5 0."# 0.#0 $0.00 $0 ".!" "$.#! !$.#! 0.%5 0."% 0.#0 "0$ ""0 "."0 "$.5! !$.5# 0.%5 0." 0.#! "0% ""0!"'00!!'00,O"

A2UILAR

D2ARD "AAV

DRA!3'000'00 ".%0 "$.$0 !.0 0.%$ 0.!! 0.## $.00 $0 ".90 "$.#0 !.50 0.% 0.!" 0.#! "0$ ""0 !."0 "$.%0 !.0 0.% 0.!" 0.#0 "0% ""0"'00!'003'00#'00 ".%0 "$.%0 !.%0 0.% ".#0 "$.0 !.50 0.%$5'00%'00!ROM 0." ".% ".$ "#.! $#." 0.0 0.0 0.0 "%.9 $3." ".! 3$!.0 ".30 "$.5 !.5 0.% 0."% 0.#" 9.!5 $0 ".50 "$.#$ !.$! 0.%% 0."% 0.#" 333 ""0 ".#! "$.%5 !.$9 0.% 0."% 0.#" "05 ""0MA5 0." ".% ".$ "%.5 $#.$ 0.0 0.0 0.0 ".# $3. ".! #0#.0 ".%0 "$.$0 !$.5# 0.%$ 0.!! 0.## $0.00 $0 ".90 "$.%0 !$.#! 0.% 0.!" 0.#! 333 ""0 !."0 "$.$3 !$.5# 0.%$ 0.!" 0.#! "0% ""0MIN 0." ".% ".$ "".$ $3.5 0.0 0.0 0.0 "%.3 $!.% ".! 3%0.0 "."$ "$.3" !.33 0.%5 0."3 0.#0 $.00 $0 ".!" "$.#0 !.50 0.%5 0."! 0.#0 333 ""0 "."0 "$.5! !.50 0.%5 0."3 0.#0 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 11 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0'00$'009'00"0'00""'00"!'00"3'00"#'00"5'00"%'00"'00"$'00"9'00!0'00!"'00!!'00!3'000'00"'00!'003'00#'005'00%'00!ROM0 0MA5 0 0MIN 0 0P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 11 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0'00$'009'00"0'00""'00"!'00"3'00"#'00"5'00"%'00"'00"$'00"9'00!0'00!"'00!!'00!3'000'00"'00!'003'00#'005'00%'00!ROMMA5MINP!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 11 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90'00$'009'00"0'00""'00"!'00"3'00"#'00"5'00"%'00"'00"$'00"9'00!0'00!"'00!!'00!3'000'00"'00!'003'00#'005'00%'00!ROM 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0MA5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0MIN 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00 0.00C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1' 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ #$*) $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 (0*' 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0 CARLO" 3

RNAND

4 FRANCO MA%3UA '00 !0.9 "".0 !0.! "." "%. !.! !0 %! !0.9 5".5 ." "#.% %.# "3.9 3.% 5%.%$'00 !. "0.% !5.! ".$ !0.9 !.! "3 "!" #.3 5.09'00 !$.$ "".0 !%.% ".$ !!.# ".$ "50 "#9 !$.9 0." 5. 5$.#"0'00 !5.9 "0.% !5.! "." !3.# ".5 ""0 !"3 5.3 5#.0""'00 !9.$ "". !$.# !.! !#.9 ".5 90 ! 5. %5."!'00 30.! "".0 !9.5 ".$ !%.3 !.! 9! !$% #.% 5%.%"3'00 30.5 "3." !$.$ !.% !%.% ".$ "!$ !0$ !. 5$.# "#.9 9.9 .5 "0.! %.0 55.$"#'00 !9.$ "!.$ !$." 3. !%.3 !.% "$0 "#% !3." %0.! $.5 %!.$CARLO" 3

RNAND

4LUI" MARIN"5'00 30.! "". 30.! 0.# ""0 !.0 0.# "0 "59 !.0 %0.! "0.3 9." "0.3 9." 95# $.9 5%.% $%0"%'00 30.! "0. !$.$ ".5 !5.9 ".$ ""0 !35 $.9 %".0"'00 3".% "". 30.9 !.$ !%.% ".$ "09 !## .$ %!.""$'00 3!.3 "0.% 30.9 ".5 !$.# ".$ $0 355 33.3 5!.9 9.% %!.""9'00 33. "".0 30.9 ".5 !$.$ ".$ $! 35" 9.% %".!!0'00 3#.# "". 3!. ".5 !9." ".5 3 399 35.5 53.3 "!.# "3." "0. "!.# "0.3 %5.!"'00 33. "".# 3!. ".5 !9.$ ".$ $ 3$! "0.3 5$.#!!'00 3!.3 "0.% 30.! ".5 30.! ".$ ! #"9 39." %.5 "".# 5.,O"

A2UILAR

D2ARD "AAV

DRA!3'00 3#.# "0.% 3#." !.! 3".! "." $0 390 #".9 5!.9 "%.0 "3.9 "5.3 "".0 "!.# %%.$0'00 3#.# "". 3#." !.! 3".% ".5 90 35" "3." 5$.$"'00 3!.0 "".0 3".% 0. 3".% ".5 $0 395 ##.0 %!." "3." 59.9!'00 3!. "".0 3!.0 ".$ 3".! ".$ $! 3$0 "3." 5$.$3'00#'00 3!. "".0 3!.0 !.% 3".! ".$ %% #3 "!.$ %".05'00 33.0 9.9 3".! "." 30.! "." $0 3$ #5.# 59.9 "#.! "#.% "#.% "".0 "".# %".0%'00 33.0 "0.% 3!.0 ".5 30.! ".5 ""% !%0 "!.# 59.9!ROM3"." "".! !9.$ ".$ ""0 !.# ". """ !$$ 33.3 59.0 "!.5 "!.5 0 "0.$ "".3 95# 9." 59.9 $%0MA5 3#.# "3." 3#." 3. ""0 3".% !.% !0 #3 #5.# 0." "%.0 "#.% 0 "5.3 "3.9 95# "3." %%.$ $%0MIN !0.9 9.9 !0.! 0.# ""0 "%. 0.# %% %! !0.9 5".5 ." 9." 0 %.# 9." 95# 3.% 5#.0 $%0P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1' 0# 1$!RCI!ITACION % LAVADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0 CARLO" 3

RNAND

4 FRANCO MA%3UA '00 %. "." 0. 0.$'00 9.! !." "." "."9'00 "0.3 !.5 ".$ ".$"0'00 "5.% 5. !.5 !."""'00 "3.5 3.9 !.5 !.""!'00 "0. 3.! !.$ !.""3'00 9.% !.$ !." !.""#'00 .$ !." ".$ ".$CARLO" 3

RNAND

4LUI" MARIN"5'00 "0. !.$ "." ".""%'00 9.% !." "." ".""'00 "!.# !." "." 0."$'00 "0.# !." ".# ".#"9'00 "".# !.$ ".# ".#!0'00 "!.$ 3.! ".$ ".#!"'00 9.9 3.% !." !."!!'00 9.% 3.% !.5 !.",O"

A2UILAR

D2ARD "AAV

DRA!3'00 "". 3.% !.5 !.50'00 "0.3 #.% !." !.""'00 9.9 #.3 ".$ !.$!'00 9.9 3.! ".$ ".$3'00#'00 "0.3 !.5 ".$ ".$5'00 $.! !.5 !.5 !.5%'00 9.9 !.$ ".$ ".$!ROM"0.5 3.0 ".$ ".$MA5 "5.% 5. !.$ !.$MIN %. "." 0. 0.P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 1' 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 CARLO" 3

RNAND

4 FRANCO MA%3UA '00$'009'00 * * * !#.$ 5.!! ".!% #3%.00"0'00""'00"!'00"3'00"#'00CARLO" 3

RNAND

4LUI" MARIN"5'00"%'00 * * * !%.#" 3.59 ".39 5%!.00 ".$5 !$."! 0.%3 0.!! 0.3% $" $0 ".5! !.9% 0.%3 0.!0 0.39 "0! ""0 ".%3 !.$5 0.%3 0.!0 0.#3 "03 ""0"'00"$'00"9'00!0'00!"'00 0.$5 ".9% !.#5 0.%5 0."$ 0.3$0 ".!5 ".$5 !.%! 0.%5 0.!0 0.3% 9% ""0 ".3% "$.!5 !.#5 0.%% 0."$ 0.39 "0$ ""0!!'00,O"

A2UILAR

D2ARD "AAV

DRA!3'000'00 0.90 "$.$0 !.90 0.% 0."% 0.3% $ $0 ".%0 "$.#0 !.%0 0.% 0."% 0.#" "0# ""0 ".#0 "$.0 !.0 0.%$ 0."% 0.#0 "0% "09"'00!'003'00#'00 0.$0 "$.%0 !.%0 0.% 0."" 0.39 $ $0 ".#0 "$.$0 !.0 0.%$ 0."" 0.#0 "0% ""0 ".90 "$.#0 !.50 0.% 0."" 0.3% "0% ""05'00%'00!ROM 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 !5.% #.# ".3 #99.0 0.$5 "$.30 !. 0.%% 0." 0.3 $.50 $0 ".#! "$."# !.! 0.%5 0." 0.39 333 ""0 ".55 "$.!5 !.%3 0.%% 0."% 0.#0 "0% "09.$MA5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 !%.# 5.! ".# 5%!.0 0.90 "$.$0 !$."! 0.% 0.!! 0.39 $".00 $0 ".%0 "$.$0 !.9% 0.%$ 0.!0 0.#" 333 ""0 ".90 "$.0 !.$5 0.%$ 0.!0 0.#3 "0$ ""0MIN 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 !#.$ 3.% ".3 #3%.0 0.$0 ".$5 !.#5 0.%3 0."" 0.3% .00 $0 ".!5 ".5! !.%0 0.%3 0."" 0.3% 9%.00 ""0 ".3% ".%3 !.#5 0.%3 0."" 0.3% 333 "09C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1$ 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,ULIO ARIA"FRANCO MA%3UA '00 33.# "".0 33. !.9 30.9 ".5 9! 33% #0.$ %0.% ".# "9.3 "#.! "#.% "%5% "3.5 %0.!$'00 33.0 "".3 3!. ".$ !9.$ !.! 90 33" "#.! 59."9'00 33.# "".3 33.0 ".$ 30.! ".$ $$ 3#3 ##.0 %9. "#.% 59.9"0'00 3#.$ "".3 33. !.! 3!.0 ".$ ""! !$% "#.! %!."""'00 35." "".0 3#.$ ".$ 3!. !.! ""# !$ "#.% %".3"!'00 35.5 "".3 3#.# ".$ 33.0 ".$ "00 330 "#.9 %0.!"3'00 3#.$ "0.% 3!.0 ".$ 3".% ".$ 93 3#0 #9.0 5%.% "9.0 "%.0 "#.% "%.# "3.$ 53.3"#'00 33.0 "".0 3!. !.! 3!.0 ".$ $9 3%0 55.# %3." "#.% %".0,UAN LA4O

D2ARD "AAV

DRA"5'00 3%.% "".3 35.9 %.! 3".% ".$ "0% !9$ #5.$ %0.! "%.0 "3.5 ".# "3.5 "%.0 %3.""%'00 3%.% "".0 35." ".5 3!.0 !.% "!% !5# "%.0 59.9"'00 33.0 9.5 3".% 0.# 3".% ".$ ""0 !$ "%.0 50.0"$'00 35." "".0 3#.# ".$ 3!.0 ".$ "0! 3"# ".# %3.""9'00 3#." "!.# 33. !.! 3".! ".$ ""# !# 3.3 %".3 "#.! "!.$ "9.5 "!.$ ".# %".0!0'00 3#.$ "!.0 3. ".$ 3".% ".$ "00 3"% ".$ 5$.$!"'00 3#.$ "".0 33.0 ".5 3".! ".$ "0! 30% #!.% %!.# ".# 59.9!!'00 33.0 9.9 30.! 0.0 3".! ".5 ""0 !$# "%. 5".",UAN LA4OLUI" MARIN!3'00 3#.$ "".0 3.3 !.! 30.! 0.# $9 339 5".$ #!.0 "$.$ "".0 "$." "3." "%.0 5%.%0'00 33.3 "5.3 3!.0 5.# 30.! ".5 9% 3"5 #!.% $.# ".# 5%.%"'00!'00 33.3 "3.5 3!.3 5." !9.5 ".$ "%! "$! "#.! #%.3'00 3!.0 "".# !%.% 0.0 !9." !.! !"0 "39 "#.! %!."#'00 3#.# "0. 30.9 0.# 30.! ".$ !00 "5" #5." 3.# ".# !#." "%.3 !%.3 "%.0 %0.!5'00 3#.# "!.$ 30.! "." 30.! ".5 ""$ !5% 5"." 3.# "5.% %!."%'00 3#.# "". 3!. ".$ 30.! ".5 $9 339 "%.! %0.!!ROM3#.! "".# 30." !." 3"." ".$ ""# !90 #%.0 %3. "." "%." 0 "%. "%." "%5% "5.% 5$.%MA5 3%.% "5.3 35.9 %.! 33.0 !.% !"0 3%0 55.# $.# "9.0 !#." 0 "9.5 !%.3 "%5% ".$ %3."MIN 3!.0 9.5 3.3 0.0 !9." 0.# $$ "39 3.3 #!.0 "#.! "".0 0 "#.! "!.$ "%5% "3.5 #%.P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1$ 0# 1$!RCI!ITACION % LAVADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,ULIO ARIA"FRANCO MA%3UA '00 "#.9 3.! ".$ ".$$'00 $.5 #.% !." ".$9'00 9.! 3.! ".$ ".$"0'00 "0. !." ".$ ".$""'00 "0. !.$ ".$ ".$"!'00 $.! 3.3 !." ".$"3'00 "0.3 !." ".$ ".#"#'00 "0. !.5 ".$ ".$,UAN LA4O

D2ARD "AAV

DRA"5'00 9.! !.5 !.5 !.5"%'00 "#.! 5.0 !." !.""'00 .5 !.$ ".$ ".$"$'00 9.! ".$ ".$ ".$"9'00 $.5 !.$ ".# ".#!0'00 9.! !.$ !." !."!"'00 $.! !.5 ".$ ".$!!'00 .$ !.5 ".$ ".$,UAN LA4OLUI" MARIN!3'00 ." !." ".$ ".$0'00 "0. !.$ ".$ ".$"'00!'00 9.% !.$ ".$ ".$3'00 "0.# !.$ !." !."#'00 $.9 !." ".# ".$5'00 "!.# !.$ ".$ ".$%'00 9.9 3.% ".$ ".$!ROM9.$ !.$ ".9 ".$MA5 "#.9 5.0 !.5 !.5MIN ." ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 1$ 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,ULIO ARIA"FRANCO MA%3UA '00$'00 * * * "$.9! $".0$ ".!% ##$ "."0 "$.# !$.%9 0.%# 0."3 0.3$ 9 $0 ".30 ".$# !.%$ 0.%# 0."# 0.3$ "0 ""0 ".!$ "$.0! !$.0! 0.%# 0."# 0.3$ "0% ""09'00"0'00""'00"!'00"3'00 ".!! "$.33 !.%" 0.%% 0."# 0.3$ $0 $0 ".! "$.00 !.5$ 0.%5 0."3 0.39 "05 ""0 "."$ "$.35 !.$% 0.%% 0."3 0.39 "0$ ""0"#'00,UAN LA4O

D2ARD "AAV

DRA"5'00"%'00 . . . ".00 $3.00 ".3! 50 "."0 "$.%0 !.90 0.% 0."! 0.#0 $ $0 ".$0 "$."0 !.50 0.%% 0."! 0.#! "0$ ""0 ".%0 "$.#0 !.%0 0.% 0."! 0.#" ""0 ""0"'00"$'00"9'00!0'00 ".00 "$.#0 !.$0 0.%% 0."! 0.#0 % $0 ".#0 "$.30 !.00 0.%$ "0% ""0 ".30 "$.#0 !.0 0.%% 0."! 0.#0 ""0 ""0!"'00!!'00,UAN LA4OLUI" MARIN!3'000'00 * * * "$.5% $".## ".!$ 5"%.00 0.$5 "$.5" !.#5 0.% 0."# 0.39 $0 $0 ".9% "$.!# !.5% 0.%% 0."! 0.## "0$ ""0"'00!'003'00#'005'00 0.9" "$.55 !.9% 0.%% 0."$ 0.3$ $0.00 $0 ".3# "$.3# !.$ 0.%% 0.!" 0.3 "0# ""0 ".#5 "$.39 !.$% 0.%% 0."$ 0.39 "05 ""0%'00!ROM 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "$.! $".$ ".3 5"".3 ".03 "$.#$ !.90 0.%% 0."# 0.39 $.$3 $0 ".#! "$."! !.5" 0.%% 0."5 0.39 333 ""0 ".#% "$.30 !. 0.%% 0."# 0.#0 "0$ ""0MA5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "$.9 $3.0 ".3 50.0 ".!! "$.%0 !$.%9 0.% 0."$ 0.#0 $0.00 $0 ".$0 "$.3# !.$ 0.%$ 0.!" 0.#! 333 ""0 ".9% "$.#0 !$.0! 0.% 0."$ 0.## ""0 ""0MIN 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 ".0 $"." ".3 ##$.0 0.$5 "$.33 !.#5 0.%# 0."! 0.3$ %.00 $0 ".! ".$# !.00 0.%# 0."! 0.3 333 ""0 "."$ "$.0! !.5% 0.%# 0."! 0.3$ 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1) 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,O"

A2UILARFRANCO MA%3UA'00 33.0 "!.# 30.9 3. !9.$ ".$ "5" "9 #.% %9.0 "9.5 !0.$ "%.0 !3.# !"00 "%.0 5$.$$'00 33. "!.0 3!.0 !.! 30.9 !.% "3$ !!# "%.! 59.#9'00 3!. "". 30.9 ".$ 30.! !.! "00 30! #%.5 !.% "%.0 5%.%"0'00 3#. "". 3!. 3.3 3!.0 !.! "#% !"9 5"." %!.$ "#.9 55.5""'00 33.# "".0 3!.3 "." 30.9 !.% "%$ "$# ".0 5%.9"!'00 3!.9 "".3 3".! "." 30.! ".5 ""$ !5% ##.0 %!." "%.0 5#.0"3'00 33.# "".3 3!.3 ".$ 30.! "." "05 !$$ 50.# %!.$ "%.! 5%.9"#'00 33. "".0 3!.0 3.3 3".! ".$ "00 3"! "%. 5$.$CARLO" 3

RNAND

4FRANCO MA%3UA"5'00 !9.5 "". !$.$ "." !$.0 !.! "!# !!% ##. %9.# !#.9 !3.0 "$.$ "5.3 "$!0 "#.! 53."%'00 !$.# "0.% !$.0 0. !. "." 99 !$0 "#.9 55.5"'00 !9.$ 9.5 !$.# ".5 !.0 "." $9 303 5#. 5$.# ".$ ##.9"$'00 !9.5 9.9 !$.# ".$ !.3 ".5 $0 3#" "%.3 %0.!"9'00 30.5 9.5 30.! ".$ !. ".$ 90 30$ "$." 5%.%!0'00 3".% 9.5 30.! "." !$.$ ".$ 95 303 5#.3 3.0 "9.! 5!.9!"'00 33.0 "". 3!.3 ".$ 30.! "." $5 355 ".0 5$.$!!'00 3#.# "!.# 3#." ".$ 30.9 ".$ 9$ 3"5 ".# %".0,UAN LA4OLUI" MARIN!3'00 3!.0 "". 3".% ".$ 30.9 ".5 $% 359 #5.$ 5%.% "#.% $.0 ".0 "#.! "#.! #$.!0'00 30.! "".# 30.! ".$ 30.! ".$ $! 3%$ "#.! %0.!"'00 3!. "".0 3!.0 3.% 30.! ".$ $9 339 #$.3 %3.9 "%.3 %3.9!'00 3!. "". 3!. ".$ 3".% !.% "39 !! "%.3 %0.!3'00 3#.# "". 3#.# !.! 3!.0 ".$ 9$ 3! ".$ 5$.##'00 3!.3 "". 3!.3 !.$ 3!.0 !.! ""! !$% "$." 55.55'00 3#.# "". 33. ".$ 3!.3 !.! "!0 !%9 #.9 #5.% !0.! "".0 "$.5 ".! ".0 %0.!%'00 3#.$ "".# 33. ".5 3!.3 !.! 9! 35" #$.3 %".! ".$ %0.!!ROM3!.# "".! 3".5 !.0 30.! ".$ "09 !$9 #$.% %3." "9.$ "5. 0 ".% ".5 "9%0 "%.5 5.0MA5 3#.$ "!.# 3#.# 3. 3!.3 !.% "%$ 3%$ 5#. 3.0 !#.9 !3.0 0 "$.$ !3.# !"00 "9.! %3.9MIN !$.# 9.5 !$.0 0. !.0 "." $0 "$# ##.0 #5.% "#.% $.0 0 "%.0 "#.! "$!0 "#.! ##.9P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1) 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,O"

A2UILARFRANCO MA%3UA'00 "0.3 !.$ !." !."$'00 9.! !.$ !." ".$9'00 $.9 !.$ ".$ ".$"0'00 9.! 3.% !." !."""'00 "3. 3.9 !." ".$"!'00 9.! 3.! !." ".$"3'00 $.9 !.$ !." ".$"#'00 "".# 5. !." ".$CARLO" 3

RNAND

4FRANCO MA%3UA"5'00 "". #.3 !.5 !.""%'00 9.! !.5 !.5 !.5"'00 $.9 !.$ !." !.""$'00 9.! ".$ ".$ ".$"9'00 9.9 !.5 ".$ ".#!0'00 9.! !.$ ".$ ".#!"'00 $.9 !.$ !." ".$!!'00 9.% !.5 !." !.",UAN LA4OLUI" MARIN!3'00 9.9 !." ".$ ".#0'00 $.5 !." ".# ".#"'00 "0. !.5 ".# ".# #.$$ 0.5" %.#! 0.09!'00 "0.# !.$ ".$ ".$3'00 "". !.$ ".$ ".$#'00 "0. !.$ ".$ ".$5'00 "!.# !.$ ".5 ".5%'00 "0.% 3.% ".$ ".$!ROM"0." 3.0 ".9 ".$ #.9 0.5 %.#! 0.09MA5 "3. 5. !.5 !.5 #.9 0.5 %.#! 0.09MIN $.5 ".$ ".# ".# #.9 0.5 %.#! 0.09P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 1) 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,O"

A2UILARFRANCO MA%3UA'00$'00 * * * "5.53 $#.# ".!$ #!$ ".0" "$.% !.$5 0.% 0.!0 0.#" 9.00 $0 ".$" "$.#" !.%$ 0.% 0.!0 0.#0 "00 ""09'00"0'00""'00"!'00"3'00 ".0" "$.5! !.$$ 0.%% 0."9 0.#0 $0.00 $0 ".!0 "$.3! !.95 0.%% 0."9 0.#! "05 ""0 ".!$ "$.3 !.5% 0.% 0.!0 0.#! "0# ""0"#'00CARLO" 3

RNAND

4FRANCO MA%3UA"5'00"%'00 * * * "3.9! $%.0$ ".!# 3!$ "."$ "$.5! !.5% 0.% 0."$ 0.#0 "0# ""0 ".!5 "$.%$ !.$% 0.% 0."$ 0.#0 "03 ""0"'00"$'00"9'00!0'00!"'00 "."3 "$.#9 !.$% 0.%% 0."# 0.#0 "03 ""0 "."$ "$.55 !.$ 0.% 0."3 0.39 "0# ""0!!'00,UAN LA4OLUI" MARIN!3'000'00 * * * "5.%9 $#.3" ".3# "$.5" !.$5 0.%% 0."" 0.3$ "0# ""0 ".!5 "$.#3 !.$ 0.%% 0."" 0.3$ "05 ""0"'00!'003'00#'005'00 0.$% "$.3 !.%3 0.%% 0."# 0.#" $0.00 $0 ".!$ "$."! !.#" 0.%% 0."# 0.39 "0% ""0 ".! "$.# !.$5 0.%% 0."# 0.3 "0$ ""0%'00!ROM 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "5.0 $5.0 ".3 3$.0 0.9% "$.5! !.9 0.% 0."$ 0.#" 9.% $0 ".!3 "$.39 !.3 0.%% 0."5 0.#0 333 ""0 ".3# "$.#9 !.5 0.% 0."% 0.39 "0# ""0MA5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "5. $%." ".3 #!$.0 ".0" "$.% !.$$ 0.% 0.!0 0.#" $0.00 $0 ".3# "$.5! !.95 0.% 0."9 0.#! 333 ""0 ".$" "$.%$ !.$% 0.% 0.!0 0.#! "0$ ""0MIN 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "3.9 $#.3 ".! 3!$.0 0.$% "$.3 !.%3 0.%% 0."# 0.#0 9.00 $0 "."3 "$."! !.#" 0.%% 0."" 0.3$ 333 ""0 "."$ "$.3 !.5% 0.%% 0."" 0.3 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1+ 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,O"

A2UILARFRANCO MA%3UA'00 33.0 "!.0 3!. 3.3 30.9 !.9 ""! !% #!.9 %5. !". "9.3 "$." ".! ""! ".# 5$.$$'00 33.# "". 3!.3 !.! 30.! 3.3 "!0 !5! "$." 59.59'00 3#." "".0 3!. ".5 30.5 !.! "5! !0" #3.0 %%." "$." 55.$"0'00 35.5 "".3 33.0 3.3 3!. ".$ "3 !39 #$.0 %3.9 "%. 59.5""'00"!'00"3'00"#'00CARLO" 3

RNAND

4

D2ARD "AAV

DRA"5'00 35.9 "".0 3#.$ "." 33.# "." $$ 3$0 5#.0 5. !!.5 "%.# !".3 "3.5 "$." 5$.#"%'00 35.5 "0.! 3#.# ".5 3!.0 "." $% 3! ".$ %".3"'00 3%.% "".0 35.5 ".5 33. ".5 $0 #!" #.% %#.! ".$ %".3"$'00 3%.% "".0 35." ".$ 33. ".5 $% 39! "$." 59.9"9'00 3%.% "".0 35.5 ".$ 3#." ".$ $% 39 "9.9 %".!0'00 3%.% "".0 35.5 ".$ 3#." ".$ $% 39 #9. %9.# !!. ".! !0.9 "#.% "9.! %".3!"'00 3%.% "".0 35." ".$ 33. ".$ "0! 330 "9.9 5$.$!!'00 3.3 "". 3%.! 3.3 33. ".$ 9% 35" !0.% 5$.#,UAN LA4OLUI" MARIN!3'00 35.5 "0.% 33. !.! 33. !.! 9$ 3## ##. %9.# "$.$ !3. !0.% !0." !0.! 55."0'00 30.! 9.9 30.! ".5 33.3 !.! $ 3$3 "$." !9.!"'00 !$.# 9." !. "." 30.! ".5 $0 3$ "%.3 55.5!'00 3!.9 "0.% 3!.0 !.! 30.! ".$ $0 3$ ".$ %3.93'00 3.3 "#.! 3.3 5.# 3".% ".$ $! 3$5 #".9 %5. !".3 !".9 !!.0 !0.$ "$.$ %%.$#'00 3%.9 "!.$ 35." !.% 3!.0 !.! $% 3! "$.5 %!."5'00 3#.# "". 3#.# !.$ 3#.# !.% "%# !"0 #!.$ %!. "$.$ 59."%'00 3#.$ "0.% 33. !.% 33. !.! ""# !9% "$.$ %0.!!ROM3#.9 "".! 33.$ !.3 3!.% !.0 "0" 33$ #%." %5.0 !".# "9. 0 !0.% ".! ""! "$.5 5$.3MA5 3.3 "#.! 3.3 5.# 3#.# 3.3 "%# #!" 5#.0 %9.# !!. !3. 0 !!.0 !0.$ ""! !0.% %%.$MIN !$.# 9." !. "." 30.! "." $0 !0" #".9 5. "$.$ "%.# 0 "$." "3.5 ""! "%.3 !9.!P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1+ 0# 1$!RCI!ITACION % LAVADO DIAMES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,O"

A2UILARFRANCO MA%3UA'00 "!.$ 3.% !." ".$$'00 "0.3 3.9 !." !."9'00 9.% #.3 !." !.""0'00 %. ".$ ".$ ".$""'00"!'00"3'00"#'00CARLO" 3

RNAND

4

D2ARD "AAV

DRA"5'00 $.! !.5 !." !.""%'00 $.9 3.! !.5 !.5"'00 $.5 !.$ !.$ !.$"$'00 $.9 !.$ ".$ ".$"9'00 $.5 3.! !." ".$!0'00 $.9 3.! ".$ ".$!"'00 $.! !.$ ".$ ".$!!'00 . !." !." !.",UAN LA4OLUI" MARIN!3'00 $.! ".$ ".$ !."0'00 "#.! !." ".# ".#"'00 $.5 !.$ ".$ ".$!'00 9.% !." ".$ ".$3'00 9.9 !.5 ".$ ".$#'00 9.9 !.5 ".$ ".$5'00 9.9 !." !." ".$%'00 "0. !.5 ".$ ".$!ROM9.# !. !.0 ".9MA5 "#.! #.3 !.$ !.$MIN %. ".$ ".# ".#P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 1+ 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $# - ! !3 !3 !.3 !.3 !.3MA&. - - - - 90 - - - - 90 1*+ +00 $0 '( '( '*+ 19*0 '8*# 0*#0 0*18 0*+0 90 90 '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+ '*+ 19*0 '8*# 0*#0 0*18 0*+0 10+ 10+MIN. - - - - 80 - - - - 80 - - '+ 18*0 18*0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ #0 #0 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90 0*8 1#*8 '+*+ 0*(( 0*1' 0*1+ 90 90,O"

A2UILARFRANCO MA%3UA'00$'00 * * * "!.59 $.#" "."! 0.39 9 $0 "."# 0."$ 0.39 9 $0 ".!" 0." 0.#0 "00 ""09'00"0'00""'00"!'00"3'00"#'00CARLO" 3

RNAND

4

D2ARD "AAV

DRA"5'00"%'00 . . . "5.30 $#.0 ".!# ##0 ".00 "$.%0 !$.00 0.%% 0."# 0.#0 9 $0 ".$0 "$.30 !$.00 0.%5 0."# 0.3% "09 ""0 ".%0 "$.30 !$.00 0.%5 0."# 0.## "0% ""0"'00"$'00"9'00!0'00 ".00 "$.$0 !.0 0.%$ 0."" 0.#" ".%0 "$.%0 !.50 0.%$ 0."! 0.3$ ".#0 "$.#0 !.50 0.% 0."! 0.#0!"'00!!'00,UAN LA4OLUI" MARIN!3'000'00 * * * ".50 $!.50 ".! 53".00 0.$% "$.# !.$9 0.% 0."! 0.3$ $0.00 $0 ".3 "$.5# !.$% 0.% 0."! 0.3 "0# ""0"'00!'003'00#'005'00 0.9" "$.%9 !.$5 0.% 0."! 0.3 $0.00 $0 ".!$ "$.#3 !.%3 0.% 0."! 0.39 "0! ""0%'00!ROM 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "5." $#.9 ".3 #$5.5 0.9$ "$." !.$% 0.% 0."! 0.39 9.50 $0 ".## "$.# !.5 0.% 0."# 0.3$ 9$.50 "0!.5 ".#0 "$.35 !.5 0.%% 0."# 0.#" "03 ""0MA5 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 ".5 $.# ".3 53".0 "."! "$.$0 !$.00 0.%$ 0."# 0.#" $0.00 $0 ".$0 "$.%0 !$.00 0.%$ 0."$ 0.39 333 ""0 ".%0 "$.#0 !$.00 0.% 0." 0.## "0% ""0MIN 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0 "!.% $!.5 ".! ##0.0 0.$% "$.%0 !.0 0.%% 0."" 0.3 9.00 $0 "."# "$.30 !.50 0.%5 0."! 0.3% 9.00 $0 ".!" "$.30 !.50 0.%5 0."! 0.#0 333 ""0C0CO3C0CO3H!O H!O H!O H!O H!O H!OQUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-001Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1( 0# 1$ATAQU %!URIFICACION DIA MES AO"U!

RVI"ORLA&ORATORI"TAH DFR - 01 D! - 0'- 01 D! - 0(- 0' D! - 0$ D! - 1( DA-01 DA-0$O&"VACION"ORATAQU DFLUORINACION B AR HCl F HCl F HCl F I.C HCl F HCl F I.C HCl F HCl F pH HCl NAOH HCL HCLA gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm gpl gpl ppm - gpl gpl ppm gpl gpl ppm gpl gpl gpl gpl %OPTIMO 35.0 9.0 00 33.0 !.0 "5 33.0 !.0 "!# #5 3$ !%00 "9.0 "!.0 "!00 "9.0 "".0 "!00 "5 %0 $00MA&. )0*0 11 1000 $(*' '*( ''0 $+ '*' 1+0 $() ++ )+*$ $+00 '' 18 1(00 $0 '+*( 1+*0 1+00 '0 #0 1'00 1*+ - - 100*0 -- --MIN. $0*0 8*0 )00 '9*1 0 80 '9*1 0 80 '$$ '9*1 '0*0 1'00 1'*1 +*0 )00 1) 1'*1 +*0 +00 10 +0 )00 '*0 - +0*0 $))*0 $0*0,O"

A2UILAR

D2ARD "AAV

DRA'00 3#.# "".3 3#." !.9 33.0 !.! ""% !$# ##.# %$.% !0.% !0.$ !0.% 5$.0$'00 35." "".3 3#.# ".$ 33.0 !.! "0$ 30% !0.! %".39'00"0'00 50.0""'00 3#." "0.! 33.0 "." 33.0 !.! ""0 300 "9.5 59.5"!'00 39." "". 3%.% 0. 33. ".$ 9% 35" 50." %5. !0.! "5.3 !".3 !0.$ "9.! %3.9"3'00 3.3 "".0 3%.% ".$ 33. ".5 "00 33 "9.! 59.9"#'00 3.% "". 3%.% !.! 33. ".$ "9.! %!."CARLO" 3

RNAND

4FRANCO MA%3UA"5'00 35.5 "!.$ 3#.$ !.% 33. !.! "0$ 3"! #3.0 %.! !0.! "9. "9.9 !".5 "$.$ %".3"%'00 35.9 "!.# 3#." !.! 33.0 !.% "00 330 "$." 5%.9"'00 33. "3." 33.0 ".$ 3!. !.! 9$ 33# 3$.3 %.! ".0 59.9"$'00 35.9 "". 3#." ".$ 33. ".$ "5! !!! ".$ 59.""9'00 3#." "". 33.0 "." 3!. ".$ "35 !#! ".0 5%.9!0'00 33.0 "". 3!. ".5 3!.0 "." "!0 !% #.9 5".0 ".# 5%.9!"'00 3#.$ "".0 33.0 ".5 3!. ".5 99 330 55. %".3 "$." "9.0 !0.9 "%.$ ".# 5.!!'00 35.5 "".3 33. ".$ 3!.0 ".5 "!5 !5% "$." 5$.#,UAN LA4OLUI" MARIN!3'00 35.5 "0.% 35.5 3.% 3!.3 ".$ ""! !$$ #!.% 3.# ".# "9. !0.9 "5. ".# %0.!0'00 3#.# "". 3!. ".$ 3!.3 !.! "0! 3" ".# %0.!"'00 3#.# "". 3!.3 ".$ 3!.3 !.! 9! 35" ##.! %$.# "%. %0.!!'00 3#.# "".# 33. 3.% 3!.3 ".$ $ 3" ".0 5$.#3'00 3#.# "0.% 3!.0 "." 3!.3 ".$ $0 #0# ".# 5.#'00 35.5 "". 33. ".$ 3!.3 ".$ $! 39# ".$ 5$.#5'00 35.5 "!.# 3#.# 3.9 3!.3 ".5 $0 #0# #$.9 5%.% "9.5 "!.$ "$.5 ".5 ".$ 5$.#%'00 3!.3 "". 3!.3 ".$ 3!.0 ".$ $9 3%0 "%.0 59."!ROM35." "".% 33.9 !.0 3!.$ ".9 "0# 3!! #%." %#.# "9." ".3 0 !0.# "$.9 "$.0 5$.9MA5 39." "3." 3%.% 3.9 33. !.% "5! #0# 55. 3.# !0.! "9. 0 !".3 !".5 !0.% %3.9MIN 3!.3 "0.! 3!.0 0. 3!.0 "." $0 !!! 3$.3 5".0 ".# "!.$ 0 "$.5 "5. "%.0 50.0P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTA FOSFATO BICALCICO.LF-MFA01-00$Versin :0Fecha:10/08/09CONTROL QUIMICO D !ROC"O 1( 0# 1$!RCI!ITACION % LAVADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH- 0)- 0+- 0( D!-09O&"VACION"O 1 ' $ ) + ( # 8 9 10 11 1'R PH PH pH pH pH pHA gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gpl gplOPTIMO "!.0 #.0 !.0 !.0 3.5 ".0 5." 0.! %.0 0." %.0 0."MA&. "# %.0 #.0 3.5 #.0 !." 5.5 0.5 $.0 ".0 $.0 ".0MIN. $.5 3.0 ".5 ".5 3.0 0.5 5.0 0." 5.5 0 5.5 0,O"

A2UILAR

D2ARD "AAV

DRA'00 "0.3 !.$ !." !."$'00 $.5 3.% !.$ !.$9'00"0'00""'00 $.! !.5 !.5 !.$"!'00 "0.3 !.5 !.5 !.5"3'00 9.% 3.% ".$ ".$"#'00 $.! ".$ ".$ ".$CARLO" 3

RNAND

4FRANCO MA%3UA"5'00 .$ !." "." ".""%'00 "".# ".$ ".$ ".#"'00 "0.3 !.$ ".$ ".$"$'00 "0. 3.! !." ".$"9'00 9.% !.$ !." !."!0'00 "3.% !." ".$ ".$!"'00 "0.3 3.! !." ".$!!'00 $.5 !." !." !.",UAN LA4OLUI" MARIN!3'00 "0. !." ".$ ".$0'00 9.% !." ".$ ".$"'00 "%.0 !.5 ".# ".#!'00 $.5 3.% ".$ ".$3'00 $.9 ".$ ".5 ".$#'00 9.9 !." ".$ ".$5'00 "0.# !.5 ".$ ".$%'00 9.% !.5 ".$ ".$!ROM"0.0 !.% ".9 ".9MA5 "%.0 3.% !.$ !.$MIN .$ ".$ "." "."P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5P!O5QUIMPAC S.A.PLANTAFOSFATO BICALCICO.LF-MFA01-00'Versin : 0Fecha: 10/08/09CONTROL QUIMICO D !ROC"O 1( 0# 1$MOLINDA % "CADO DIA MES AO"U!

RVI"ORLA&ORATORI"TAH 2RANULOMTRIA 2RANULOMTRIA FILTRO" "CADOR ROTATORIO "CADOR FLA"3 01 FILTRO !RN"A 0'O&"VACION"O MOLINO &RADL% MOLINO D &OLA" ROT F! 01 F! 0' !RODUCTO !RODUCTO !RODUCTOR D+,- C.,/. P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SP P C0 P)C0 F Cl T SPA M"00 M"0 M!00 M3!5 M-3!5 M"00 M"0 M!00 M3!5 M-3!5 g1)// gpl % % % % % % % % 2C 2C % % % % % 2C 2C % % % % % 2C 2COPTIMO - - - - 8) - - - - $#


PROCESO DE CONTROL

Control Estadistico de Proceso

Control Proceso Administrativo

Sensores Control Proceso

Control Proceso s

Control Estadístico de Proceso y Capacidad Del Proceso

Product description DCV-FB – Flow balance control unit€¦ · DCV-FB – Flow balance control unit Product description DCV-FB_E08_PB20_eng 1(3) ... Size: XXX = 125, 160, 200, 250,

En proceso coloquio fb hacia la autoconsciencia

FB Control Instrumentation Range 2013

Control (proceso administrativo)

Proceso Administrativo - Control

Proceso de Control Administrativo

PLCopen Motion Control Function Block Reference …...2 FUNCTION DESCRIPTION 2.3 FB Operation 11 2 2.3 FB Operation Data communication method To control the devices connected with

proceso administrativo control

B Control de Proceso

Library description 12/2017 Axis Control Blocks for S7 ... · FB 30604 LAxisCtrl_ExtEncoder 2 48 FB 30605 LAxisCtrl_GetAxisStatusWord 0.4 12 FB 30606 LAxisCtrl_GetAxisWarningWord

Proceso administrativo, control

Control estadistico del proceso

proceso de control y Fuentes de control

Wireless remote control 10-channel ZW fb User manual for ... · Wireless remote control 10-channel ZW fb GB ... 3.0 User manual düwi wireless remote control art no 0 44 0 düwi wireless

Control Estadístico Del Proceso

FB Series - IDEC · 4 FB Series Plastic Control Boxes IP65 lightweight plastic enclosures for installing control units. • ø22mm control units can be installed. • Blank front

Control de proceso

ˇ˜ ˇ LEO FB - FLOWAIR · 2018-07-30 · fb | 5 ГАБАРИТЫ ТЕХНИЧЕСКИЕ ПАРАМЕТРЫ fb 10s fb 10v fb 10m fb 20s fb 20v fb 20m fb 30v fb 30m fb 25s fb 25v

Proceso administrativo- Control

Control Digital de Proceso

Control Proceso

Proceso control remoto

Control Organización Proceso Nde Control

Control En Proceso Administrativo

Fisher FB and FBG Control Valves Bulletin.pdf

PROCESO ADMINISTRATIVO: CONTROL

Proceso de control

VELOCE FB 10s - campagnolo.com · 47 ergopower™ fb control levers velocetm fb 10s ep6-vlxcfb r.h. complete control lever / comando dx completo ep6-vlxfbr l.h. complete control lever