email regarding monthly progress report - july 2017 · 2019-10-15 · 7-17 west lake lf ou-1 mo...

From: Paul RosascoTo: Jump, Christine; Juett, Lynn; "Seabaugh, Ryan"; Mahler, TomCc: McGahren, John; Feingold, Stephanie R.; "Guariglia, Dale"; "Beck, Bill (LG)"; Sklenar, Scott E:(GenCo-Nuc);

"Lintecum, Sarah E. (LG)"; Merrigan, Jessie; Dupre, Phillip R (ENRD); Steve Miller; "Warren, Victoria"; Fanning,Erin; Dan Feezor; "Mike Bollenbacher"; [email protected]

Subject: West Lake OU-1 Monthly Progress Report - July 2017Date: Thursday, August 10, 2017 1:17:03 PMAttachments: 1707090_d.pdf

ATLSTDEDD_1707090.xls1706454_d.pdfATLSTDEDD_1706454.xls1706146_d.pdfATLSTDEDD_1706146.xls17061062.pdf17061062EDD.XLS1705139R.XLS1706028.xls1707070.xls7-17 West Lake LF OU-1 Mo Progress Report.pdf7-17 West Lake LF OU-1 Mo Progress Report.pdf

Ms. Jump,The monthly status report for OU-1 is attached.

Laboratory Analytical Reports

Air Monitoring

The lab reports and the electronic data deliverables (EDDs) for the EuroFins Air Toxics Ltd labreports 1706146, 1706454, and 1707090 are attached. No reports of results for air monitoringsamples were received from Eberline Laboratory during this period.Stormwater

The lab report and associated EDDs for TekLab report 17061062 are attached. The EDDs for theEberline stormwater sample lab reports numbers 1705139R, 1706028, and 1707070 are alsoattached. The full reports can be download using the following links:https://db.tt/PkT9lqLqNy

https://db.tt/Crf2hvcEZI

https://db.tt/Jquqlspmwt

Stormwater Memorandum

The Feezor Engineering, Inc. memorandum regarding stormwater monitoring and inspectionactivities conducted during July 2017 can be downloaded from the following link:

https://db.tt/Y7psu9RPa8

Please contact us if you have any questions.Thank-you, Paul.Paul V. Rosasco P.E.Engineering Management Support, Inc.25923 Gateway DriveGolden, CO 80401
mailto:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]:[email protected]://db.tt/PkT9lqLqNyhttps://db.tt/Crf2hvcEZIhttps://db.tt/Jquqlspmwthttps://db.tt/Y7psu9RPa8

7/21/2017Ms. Cecilia GreeneAuxier & Associates, Inc.9821 Cogdill Road, Suite 1

Knoxville TN 37932

Project Name: Project #:

Dear Ms. Cecilia Greene

The following report includes the data for the above referenced project for sample(s) received on 7/7/2017 at Air Toxics Ltd.

The data and associated QC analyzed by Passive S.E. RAD130/SKC are compliant with the project requirements or laboratory criteria with the exception of the deviations noted in the attached case narrative.

Thank you for choosing Eurofins Air Toxics Inc. for your air analysis needs. Eurofins Air Toxics Inc. is committed to providing accurate data of the highest quality. Please feel freeto contact the Project Manager: Kelly Buettner at 916-985-1000 if you have any questions regarding the data in this report.

Regards,

Kelly Buettner

Project Manager

Workorder #: 1707090

Page 1 of 17

Ms. Cecilia GreeneAuxier & Associates, Inc.9821 Cogdill Road, Suite 1Knoxville, TN 37932

WORK ORDER #: 1707090

CLIENT: BILL TO:

PHONE:


865-675-3669

865-675-367707/07/2017

DATE COMPLETED: 07/20/2017

P.O. #

PROJECT #

Work Order Summary

FAX:

DATE RECEIVED:CONTACT: Kelly Buettner

NAMEFRACTION # TEST01A 1 Passive S.E. RAD130/SKC02A 5 Passive S.E. RAD130/SKC03A 7 Passive S.E. RAD130/SKC04A 8 Passive S.E. RAD130/SKC05A 12 Passive S.E. RAD130/SKC06A DUP Passive S.E. RAD130/SKC07A TB Passive S.E. RAD130/SKC08A Lab Blank Passive S.E. RAD130/SKC09A LCS Passive S.E. RAD130/SKC09AA LCSD Passive S.E. RAD130/SKC

CERTIFIED BY:

Technical Director

DATE:

180 BLUE RAVINE ROAD, SUITE B FOLSOM, CA - 95630(916) 985-1000 . (800) 985-5955 . FAX (916) 985-1020

07/20/17

Page 2 of 17

This report shall not be reproduced, except in full, without the written approval of Eurofins Air Toxics, Inc.

LABORATORY NARRATIVERAD130 Passive SE by Mod EPA TO-17

Auxier & Associates, Inc.Workorder# 1707090

Seven Radiello 130 (Solvent) samples were received on July 07, 2017. The laboratory analyzed the charcoal sorbent bed of the passive sampler following modified method EPA TO-17. The VOCs were chemically extracted using carbon disulfide and an aliquot of the extract was injected into a GC/MS for identification and quantification of volatile organic compounds (VOCs).

The mass of each target compound adsorbed by the sampler was converted to units of concentration using the sample deployment time and the sampling rate for each VOC. If sampling rates werecalculated by the lab or the manufacturer, the concentration result has been flagged as an estimated value. Results are not corrected for desorption efficiency.

The reference method used for this procedure is EPA TO-17, which describes the collection of VOCs in ambient air using sorbents and analysis by GC/MS. Because TO-17 describes active sample collection using a pump and thermal desorption as the preparation step, several modifications are required. Modifications to TO-17 are listed in the table below:

Requirement ATL ModificationsTO-17Sample Collection Pump pulls measured

air volume through sorbent tube

VOCs in air adsorbed onto sorbent bed passively through diffusion

Receiving Notes

There were no receiving discrepancies.

The uptake rates were corrected based on average field temperatures if provided. In the absence of field temperatures, the uptake rates determined at 25 deg C were used.

To calculate ug/m3 concentrations in the Lab Blank and Trip Blank, a sampling duration of 20280 minutes was applied. The assumed temperature used for the uptake rate is listed on the data page. If the field temperatures were provided, the rate was adjusted in the same manner as the field samples.

Analytical Notes

Ten qualifiers may have been used on the data analysis sheets and indicate as follows: B - Compound present in laboratory blank greater than reporting limit (background subtraction not performed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - Compound analyzed for but not detected above the reporting limit. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence.

Definition of Data Qualifying Flags

Page 3 of 17

C - Estimated concentration due to calculated sampling rate CN - See case narrative explanation.

File extensions may have been used on the data analysis sheets and indicates as follows: a-File was requantified b-File was quantified by a second column and detector r1-File was requantified for the purpose of reissue

Page 4 of 17

VOCS BY PASSIVE SAMPLER - GC/MSSummary of Detected Compounds

Client Sample ID: 1

Lab ID#: 1707090-01A

(ug/m3)(ug)(ug/m3)(ug)CompoundAmountAmountRpt. LimitRpt. Limit

0.10 0.099 0.10 0.101,2,4-Trimethylbenzene

0.10 0.062 0.32 0.202-Butanone (Methyl Ethyl Ketone)

0.20 0.13 0.23 0.15Acetone

0.10 0.074 0.38 0.28Carbon Tetrachloride

0.10 0.066 0.10 0.066Chloroform

0.10 0.073 0.12 0.089Ethyl Benzene

0.10 0.085 0.20 0.17Heptane

0.10 0.075 0.35 0.26Hexane

0.10 0.067 0.71 0.47Toluene

0.10 0.084 0.26 0.22Tetrachloroethene

0.10 0.070 0.34 0.24m,p-Xylene

0.10 0.076 0.12 0.093o-Xylene

Client Sample ID: 5

Lab ID#: 1707090-02A




0.20 0.13 0.26 0.17Acetone


0.10 0.066 0.13 0.087Chloroform

0.10 0.091 0.10 0.092Cyclohexane

0.10 0.073 0.14 0.10Ethyl Benzene

0.10 0.085 0.17 0.15Heptane

0.10 0.075 0.44 0.33Hexane

0.10 0.067 0.94 0.62Toluene

0.10 0.070 0.42 0.29m,p-Xylene

0.10 0.076 0.15 0.12o-Xylene

Client Sample ID: 7

Lab ID#: 1707090-03A

Page 5 of 17


Client Sample ID: 7

Lab ID#: 1707090-03A




0.20 0.13 0.23 0.15Acetone


0.10 0.091 0.10 0.095Cyclohexane

0.40 0.25 0.65 0.41Ethyl Acetate

0.10 0.073 0.18 0.13Ethyl Benzene

0.10 0.085 0.21 0.18Heptane

0.10 0.075 0.33 0.25Hexane

0.10 0.067 1.3 0.86Toluene


0.10 0.070 0.57 0.40m,p-Xylene

0.10 0.076 0.20 0.15o-Xylene

Client Sample ID: 8

Lab ID#: 1707090-04A




0.20 0.13 0.20 0.13Acetone


0.10 0.066 0.11 0.074Chloroform

0.10 0.073 0.12 0.088Ethyl Benzene

0.10 0.085 0.16 0.14Heptane

0.10 0.075 0.33 0.24Hexane

0.10 0.067 0.71 0.48Toluene

0.10 0.070 0.35 0.25m,p-Xylene

0.10 0.076 0.13 0.097o-Xylene

Client Sample ID: 12

Lab ID#: 1707090-05A

Page 6 of 17



Lab ID#: 1707090-05A





0.10 0.072 0.12 0.089Ethyl Benzene

0.10 0.085 0.15 0.13Heptane

0.10 0.075 0.31 0.23Hexane

0.10 0.067 0.72 0.48Toluene

0.10 0.070 0.37 0.26m,p-Xylene

0.10 0.076 0.13 0.10o-Xylene

Client Sample ID: DUP

Lab ID#: 1707090-06A




0.10 0.073 0.11 0.080Ethyl Benzene

0.10 0.085 0.20 0.17Heptane

0.10 0.075 0.23 0.17Hexane

0.10 0.067 0.63 0.42Toluene


0.10 0.070 0.30 0.21m,p-Xylene

0.10 0.076 0.10 0.080o-Xylene

Client Sample ID: TB

Lab ID#: 1707090-07ANo Detections Were Found.

Page 7 of 17

Client Sample ID: 1Lab ID#: 1707090-01A

VOCS BY PASSIVE SAMPLER - GC/MS

c071908simFile Name:Dil. Factor: 1.00

Date of Collection: 7/5/17 7:37:00 AMDate of Analysis: 7/19/17 10:12 AMDate of Extraction: 7/19/17


0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 0.10 0.101,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.062 0.32 0.202-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.23 0.15Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 0.38 0.28Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 0.10 0.066Chloroform0.10 0.091 Not Detected Not DetectedCyclohexane1.0 0.48 Not Detected Not DetectedEthanol

0.40 0.25 Not Detected Not DetectedEthyl Acetate0.10 0.073 0.12 0.089Ethyl Benzene0.10 0.085 0.20 0.17Heptane0.10 0.075 0.35 0.26Hexane0.10 0.076 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.087 Not Detected Not DetectedPropylbenzene0.10 0.081 Not Detected Not DetectedStyrene0.10 0.067 0.71 0.47Toluene0.10 0.084 0.26 0.22Tetrachloroethene0.10 0.072 Not Detected Not DetectedTrichloroethene0.10 0.070 0.34 0.24m,p-Xylene0.10 0.076 0.12 0.093o-Xylene

Temperature = 77.0F , duration time = 20244 minutes.Container Type: Radiello 130 (Solvent)

Limits%RecoverySurrogatesMethod

104 70-130Toluene-d8

Page 8 of 17






0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 0.13 0.131,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.062 0.28 0.182-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.26 0.17Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 0.35 0.26Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 0.13 0.087Chloroform0.10 0.091 0.10 0.092Cyclohexane1.0 0.48 Not Detected Not DetectedEthanol

0.40 0.25 Not Detected Not DetectedEthyl Acetate0.10 0.073 0.14 0.10Ethyl Benzene0.10 0.085 0.17 0.15Heptane0.10 0.075 0.44 0.33Hexane0.10 0.076 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.087 Not Detected Not DetectedPropylbenzene0.10 0.081 Not Detected Not DetectedStyrene0.10 0.067 0.94 0.62Toluene0.10 0.084 Not Detected Not DetectedTetrachloroethene0.10 0.072 Not Detected Not DetectedTrichloroethene0.10 0.070 0.42 0.29m,p-Xylene0.10 0.076 0.15 0.12o-Xylene




Page 9 of 17






0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 0.17 0.171,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.062 0.27 0.172-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.23 0.15Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 0.38 0.28Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 Not Detected Not DetectedChloroform0.10 0.091 0.10 0.095Cyclohexane1.0 0.48 Not Detected Not DetectedEthanol

0.40 0.25 0.65 0.41Ethyl Acetate0.10 0.073 0.18 0.13Ethyl Benzene0.10 0.085 0.21 0.18Heptane0.10 0.075 0.33 0.25Hexane0.10 0.076 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.087 Not Detected Not DetectedPropylbenzene0.10 0.081 Not Detected Not DetectedStyrene0.10 0.067 1.3 0.86Toluene0.10 0.084 0.10 0.086Tetrachloroethene0.10 0.072 Not Detected Not DetectedTrichloroethene0.10 0.070 0.57 0.40m,p-Xylene0.10 0.076 0.20 0.15o-Xylene




Page 10 of 17











Page 11 of 17






0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 0.12 0.121,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.062 0.21 0.132-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 Not Detected Not DetectedAcetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 0.36 0.26Carbon Tetrachloride0.10 0.072 Not Detected Not DetectedChlorobenzene0.10 0.066 Not Detected Not DetectedChloroform0.10 0.091 Not Detected Not DetectedCyclohexane1.0 0.48 Not Detected Not DetectedEthanol





Page 12 of 17

Client Sample ID: DUPLab ID#: 1707090-06A



Date of Collection: 7/5/17 7:37:00 AMDate of Analysis: 7/19/17 12:17 PMDate of Extraction: 7/19/17


0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 Not Detected Not Detected1,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.062 0.24 0.152-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 Not Detected Not DetectedAcetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 0.33 0.24Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 Not Detected Not DetectedChloroform0.10 0.091 Not Detected Not DetectedCyclohexane1.0 0.48 Not Detected Not DetectedEthanol





Page 13 of 17

Client Sample ID: TBLab ID#: 1707090-07A



Date of Collection: NA Date of Analysis: 7/19/17 09:47 AMDate of Extraction: 7/19/17


0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 Not Detected Not Detected1,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.062 Not Detected Not Detected2-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 Not Detected Not DetectedAcetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 Not Detected Not DetectedCarbon Tetrachloride0.10 0.072 Not Detected Not DetectedChlorobenzene0.10 0.066 Not Detected Not DetectedChloroform0.10 0.091 Not Detected Not DetectedCyclohexane1.0 0.48 Not Detected Not DetectedEthanol

0.40 0.25 Not Detected Not DetectedEthyl Acetate0.10 0.072 Not Detected Not DetectedEthyl Benzene0.10 0.085 Not Detected Not DetectedHeptane0.10 0.075 Not Detected Not DetectedHexane0.10 0.076 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.086 Not Detected Not DetectedPropylbenzene0.10 0.081 Not Detected Not DetectedStyrene0.10 0.067 Not Detected Not DetectedToluene0.10 0.084 Not Detected Not DetectedTetrachloroethene0.10 0.071 Not Detected Not DetectedTrichloroethene0.10 0.070 Not Detected Not Detectedm,p-Xylene0.10 0.076 Not Detected Not Detectedo-Xylene




Page 14 of 17

Client Sample ID: Lab BlankLab ID#: 1707090-08A










Page 15 of 17

Client Sample ID: LCSLab ID#: 1707090-09A




Limits%RecoveryCompoundMethod

103 70-1301,1,1-Trichloroethane94 70-1301,2-Dichloroethane94 70-1301,2,4-Trimethylbenzene74 50-1101,4-Dichlorobenzene89 70-1302-Butanone (Methyl Ethyl Ketone)99 70-1304-Methyl-2-pentanone87 70-130Acetone

102 70-130Benzene100 70-130Carbon Tetrachloride87 70-130Chlorobenzene

102 70-130Chloroform97 70-130Cyclohexane55 50-130Ethanol99 70-130Ethyl Acetate93 70-130Ethyl Benzene94 70-130Heptane

101 70-130Hexane101 70-130Methyl tert-butyl ether20 5-80Naphthalene82 70-130Propylbenzene66 20-100Styrene97 70-130Toluene98 70-130Tetrachloroethene

100 70-130Trichloroethene92 70-130m,p-Xylene99 70-130o-Xylene

Container Type: NA - Not Applicable



Page 16 of 17

Client Sample ID: LCSDLab ID#: 1707090-09AA





112 70-1301,1,1-Trichloroethane100 70-1301,2-Dichloroethane90 70-1301,2,4-Trimethylbenzene74 50-1101,4-Dichlorobenzene96 70-1302-Butanone (Methyl Ethyl Ketone)

102 70-1304-Methyl-2-pentanone89 70-130Acetone

100 70-130Benzene109 70-130Carbon Tetrachloride87 70-130Chlorobenzene96 70-130Chloroform

108 70-130Cyclohexane55 50-130Ethanol

101 70-130Ethyl Acetate93 70-130Ethyl Benzene98 70-130Heptane92 70-130Hexane

119 70-130Methyl tert-butyl ether19 5-80Naphthalene81 70-130Propylbenzene64 20-100Styrene98 70-130Toluene98 70-130Tetrachloroethene

101 70-130Trichloroethene93 70-130m,p-Xylene96 70-130o-Xylene




Page 17 of 17


Knoxville TN 37932

Project Name: WEST LAKE LANDFILLProject #:





Regards,

Kelly Buettner

Project Manager


Page 1 of 17



CLIENT: BILL TO:

PHONE:


865-675-3669

865-675-367706/23/2017


P.O. #

PROJECT # WEST LAKE LANDFILL

Work Order Summary

FAX:

DATE RECEIVED: CONTACT: Kelly Buettner

NAMEFRACTION # TEST01A 1 Passive S.E. RAD130/SKC02A 5 Passive S.E. RAD130/SKC03A 7 Passive S.E. RAD130/SKC04A 8 Passive S.E. RAD130/SKC05A 12 Passive S.E. RAD130/SKC06A DUP Passive S.E. RAD130/SKC07A TB Passive S.E. RAD130/SKC08A Lab Blank Passive S.E. RAD130/SKC09A LCS Passive S.E. RAD130/SKC09AA LCSD Passive S.E. RAD130/SKC

CERTIFIED BY:

Technical Director

DATE:


06/28/17

Page 2 of 17




Seven Radiello 130 (Solvent) samples were received on June 23, 2017. The laboratory analyzed thecharcoal sorbent bed of the passive sampler following modified method EPA TO-17. The VOCs were chemically extracted using carbon disulfide and an aliquot of the extract was injected into a GC/MS for identification and quantification of volatile organic compounds (VOCs).

The mass of each target compound adsorbed by the sampler was converted to units of concentration using the sample deployment time and the sampling rate for each VOC. If sampling rates were calculated by the lab or the manufacturer, the concentration result has been flagged as an estimated value. Results are not corrected for desorption efficiency.





Receiving Notes

There were no receiving discrepancies.



Analytical Notes

Ten qualifiers may have been used on the data analysis sheets and indicate as follows: B - Compound present in laboratory blank greater than reporting limit (background subtraction not performed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits. U - Compound analyzed for but not detected above the reporting limit. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence.


Page 3 of 17

C - Estimated concentration due to calculated sampling rate CN - See case narrative explanation.


Page 4 of 17


Client Sample ID: 1

Lab ID#: 1706454-01A




0.20 0.13 0.22 0.14Acetone


0.10 0.074 0.12 0.091Ethyl Benzene

0.10 0.087 0.26 0.23Heptane

0.10 0.076 0.28 0.21Hexane

0.10 0.068 0.76 0.52Toluene


0.10 0.072 0.32 0.23m,p-Xylene

0.10 0.078 0.10 0.081o-Xylene

Client Sample ID: 5

Lab ID#: 1706454-02A




0.20 0.13 0.21 0.14Acetone


0.40 0.26 0.51 0.33Ethyl Acetate

0.10 0.074 0.17 0.12Ethyl Benzene

0.10 0.087 0.24 0.21Heptane

0.10 0.077 0.40 0.30Hexane

0.10 0.068 1.1 0.74Toluene

0.10 0.072 0.50 0.36m,p-Xylene

0.10 0.078 0.15 0.12o-Xylene

Client Sample ID: 7

Lab ID#: 1706454-03A



Page 5 of 17


Client Sample ID: 7

Lab ID#: 1706454-03A0.10 0.064 0.32 0.202-Butanone (Methyl Ethyl Ketone)

0.20 0.13 0.28 0.18Acetone


0.10 0.094 0.16 0.15Cyclohexane

0.40 0.26 1.3 0.87Ethyl Acetate

0.10 0.074 0.36 0.27Ethyl Benzene

0.10 0.087 0.32 0.28Heptane

0.10 0.077 0.45 0.35Hexane

0.10 0.068 1.9 1.3Toluene


0.10 0.072 1.2 0.90m,p-Xylene

0.10 0.078 0.35 0.27o-Xylene

Client Sample ID: 8

Lab ID#: 1706454-04A




0.10 0.087 0.14 0.12Heptane

0.10 0.077 0.29 0.22Hexane

0.10 0.068 0.65 0.44Toluene

0.10 0.072 0.25 0.18m,p-Xylene


Lab ID#: 1706454-05A





0.10 0.074 0.17 0.13Ethyl Benzene

0.10 0.087 0.22 0.19Heptane

0.10 0.077 0.47 0.36Hexane

Page 6 of 17



Lab ID#: 1706454-05A0.10 0.068 0.91 0.62Toluene

0.10 0.072 0.48 0.35m,p-Xylene

0.10 0.078 0.15 0.12o-Xylene

Client Sample ID: DUP

Lab ID#: 1706454-06A




0.20 0.15 0.31 0.234-Methyl-2-pentanone

0.20 0.13 0.23 0.15Acetone


0.10 0.094 0.11 0.10Cyclohexane

0.10 0.074 0.16 0.12Ethyl Benzene

0.10 0.087 0.21 0.18Heptane

0.10 0.077 0.42 0.32Hexane

0.10 0.068 0.87 0.59Toluene

0.10 0.072 0.46 0.34m,p-Xylene

0.10 0.078 0.16 0.12o-Xylene



Page 7 of 17






0.10 0.081 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.066 Not Detected Not Detected1,2-Dichloroethane0.10 0.10 0.12 0.121,2,4-Trimethylbenzene0.10 0.099 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.064 0.28 0.182-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.22 0.14Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.075 0.55 0.41Carbon Tetrachloride0.10 0.074 Not Detected Not DetectedChlorobenzene0.10 0.067 Not Detected Not DetectedChloroform0.10 0.093 Not Detected Not DetectedCyclohexane1.0 0.49 Not Detected Not DetectedEthanol





Page 8 of 17







0.40 0.26 0.51 0.33Ethyl Acetate0.10 0.074 0.17 0.12Ethyl Benzene0.10 0.087 0.24 0.21Heptane0.10 0.077 0.40 0.30Hexane0.10 0.078 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.089 Not Detected Not DetectedPropylbenzene0.10 0.083 Not Detected Not DetectedStyrene0.10 0.068 1.1 0.74Toluene0.10 0.086 Not Detected Not DetectedTetrachloroethene0.10 0.073 Not Detected Not DetectedTrichloroethene0.10 0.072 0.50 0.36m,p-Xylene0.10 0.078 0.15 0.12o-Xylene




Page 9 of 17






0.10 0.082 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.066 Not Detected Not Detected1,2-Dichloroethane0.10 0.10 0.28 0.281,2,4-Trimethylbenzene0.10 0.099 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.064 0.32 0.202-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.28 0.18Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.075 0.45 0.34Carbon Tetrachloride0.10 0.074 Not Detected Not DetectedChlorobenzene0.10 0.067 Not Detected Not DetectedChloroform0.10 0.094 0.16 0.15Cyclohexane1.0 0.50 Not Detected Not DetectedEthanol





Page 10 of 17






0.10 0.082 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.066 Not Detected Not Detected1,2-Dichloroethane0.10 0.10 Not Detected Not Detected1,2,4-Trimethylbenzene0.10 0.099 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.064 0.22 0.142-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 Not Detected Not DetectedAcetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.075 0.40 0.30Carbon Tetrachloride0.10 0.074 Not Detected Not DetectedChlorobenzene0.10 0.067 Not Detected Not DetectedChloroform0.10 0.094 Not Detected Not DetectedCyclohexane1.0 0.50 Not Detected Not DetectedEthanol

0.40 0.26 Not Detected Not DetectedEthyl Acetate0.10 0.074 Not Detected Not DetectedEthyl Benzene0.10 0.087 0.14 0.12Heptane0.10 0.077 0.29 0.22Hexane0.10 0.078 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.089 Not Detected Not DetectedPropylbenzene0.10 0.083 Not Detected Not DetectedStyrene0.10 0.068 0.65 0.44Toluene0.10 0.086 Not Detected Not DetectedTetrachloroethene0.10 0.073 Not Detected Not DetectedTrichloroethene0.10 0.072 0.25 0.18m,p-Xylene0.10 0.078 Not Detected Not Detectedo-Xylene




Page 11 of 17






0.10 0.082 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.066 Not Detected Not Detected1,2-Dichloroethane0.10 0.10 0.18 0.181,2,4-Trimethylbenzene0.10 0.099 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.064 0.18 0.112-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 Not Detected Not DetectedAcetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.076 0.48 0.36Carbon Tetrachloride0.10 0.074 Not Detected Not DetectedChlorobenzene0.10 0.068 Not Detected Not DetectedChloroform0.10 0.094 Not Detected Not DetectedCyclohexane1.0 0.50 Not Detected Not DetectedEthanol





Page 12 of 17

Client Sample ID: DUPLab ID#: 1706454-06A





0.10 0.082 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.066 Not Detected Not Detected1,2-Dichloroethane0.10 0.10 0.16 0.161,2,4-Trimethylbenzene0.10 0.099 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.064 0.30 0.192-Butanone (Methyl Ethyl Ketone)0.20 0.15 0.31 0.234-Methyl-2-pentanone0.20 0.13 0.23 0.15Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.076 0.41 0.31Carbon Tetrachloride0.10 0.074 Not Detected Not DetectedChlorobenzene0.10 0.068 Not Detected Not DetectedChloroform0.10 0.094 0.11 0.10Cyclohexane1.0 0.50 Not Detected Not DetectedEthanol





Page 13 of 17




Date of Collection: NA Date of Analysis: 6/26/17 07:16 PMDate of Extraction: 6/26/17







Page 14 of 17











Page 15 of 17






125 70-1301,1,1-Trichloroethane116 70-1301,2-Dichloroethane96 70-1301,2,4-Trimethylbenzene87 50-1101,4-Dichlorobenzene110 70-1302-Butanone (Methyl Ethyl Ketone)110 70-1304-Methyl-2-pentanone110 70-130Acetone102 70-130Benzene124 70-130Carbon Tetrachloride102 70-130Chlorobenzene108 70-130Chloroform122 70-130Cyclohexane76 50-130Ethanol114 70-130Ethyl Acetate110 70-130Ethyl Benzene118 70-130Heptane101 70-130Hexane124 70-130Methyl tert-butyl ether17 5-80Naphthalene101 70-130Propylbenzene72 20-100Styrene107 70-130Toluene113 70-130Tetrachloroethene119 70-130Trichloroethene105 70-130m,p-Xylene99 70-130o-Xylene




Page 16 of 17






122 70-1301,1,1-Trichloroethane112 70-1301,2-Dichloroethane98 70-1301,2,4-Trimethylbenzene89 50-1101,4-Dichlorobenzene106 70-1302-Butanone (Methyl Ethyl Ketone)110 70-1304-Methyl-2-pentanone103 70-130Acetone100 70-130Benzene123 70-130Carbon Tetrachloride105 70-130Chlorobenzene105 70-130Chloroform122 70-130Cyclohexane69 50-130Ethanol110 70-130Ethyl Acetate112 70-130Ethyl Benzene119 70-130Heptane96 70-130Hexane120 70-130Methyl tert-butyl ether17 5-80Naphthalene105 70-130Propylbenzene73 20-100Styrene109 70-130Toluene115 70-130Tetrachloroethene119 70-130Trichloroethene107 70-130m,p-Xylene99 70-130o-Xylene




Page 17 of 17


Knoxville TN 37932

Project Name: West Lake LandfillProject #:





Regards,

Kelly Buettner

Project Manager


Page 1 of 17



CLIENT: BILL TO:

PHONE:


865-675-3669

865-675-367706/08/2017


P.O. #

PROJECT # West Lake Landfill

Work Order Summary

FAX:

DATE RECEIVED: CONTACT: Kelly Buettner

NAMEFRACTION # TEST01A 1 Passive S.E. RAD130/SKC02A 5 Passive S.E. RAD130/SKC03A 7 Passive S.E. RAD130/SKC04A 8 Passive S.E. RAD130/SKC05A 12 Passive S.E. RAD130/SKC06A Dup Passive S.E. RAD130/SKC07A TB Passive S.E. RAD130/SKC08A Lab Blank Passive S.E. RAD130/SKC09A LCS Passive S.E. RAD130/SKC09AA LCSD Passive S.E. RAD130/SKC

CERTIFIED BY:

Technical Director

DATE:


06/22/17

Page 2 of 17




Seven Radiello 130 (Solvent) samples were received on June 08, 2017. The laboratory analyzed thecharcoal sorbent bed of the passive sampler following modified method EPA TO-17. The VOCs were chemically extracted using carbon disulfide and an aliquot of the extract was injected into a GC/MS for identification and quantification of volatile organic compounds (VOCs).

The mass of each target compound adsorbed by the sampler was converted to units of concentration using the sample deployment time and the sampling rate for each VOC. If sampling rates were calculated by the lab or the manufacturer, the concentration result has been flagged as an estimated value. Results are not corrected for desorption efficiency.





Receiving Notes



All Quality Control Limit exceedances and affected sample results are noted by flags. Each flag isdefined at the bottom of this Case Narrative and on each Sample Result Summary page.

Analytical Notes

Ten qualifiers may have been used on the data analysis sheets and indicate as follows: B - Compound present in laboratory blank greater than reporting limit (background subtraction not performed). J - Estimated value. E - Exceeds instrument calibration range. S - Saturated peak. Q - Exceeds quality control limits.


Page 3 of 17

U - Compound analyzed for but not detected above the reporting limit. UJ- Non-detected compound associated with low bias in the CCV N - The identification is based on presumptive evidence. C - Estimated concentration due to calculated sampling rate CN - See case narrative explanation.


Page 4 of 17


Client Sample ID: 1

Lab ID#: 1706146-01A




0.20 0.13 0.37 0.24Acetone


0.10 0.067 0.15 0.10Chloroform

0.10 0.074 0.22 0.16Ethyl Benzene

0.10 0.087 0.29 0.25Heptane

0.10 0.076 0.43 0.33Hexane

0.10 0.068 1.0 0.71Toluene


0.10 0.072 0.57 0.41m,p-Xylene

0.10 0.077 0.19 0.15o-Xylene

Client Sample ID: 5

Lab ID#: 1706146-02A




0.20 0.13 0.41 0.27Acetone

0.40 0.25 0.45 0.28Benzene


0.10 0.066 0.12 0.082Chloroform

0.10 0.092 0.14 0.12Cyclohexane

0.40 0.25 0.45 0.29Ethyl Acetate

0.10 0.073 0.21 0.15Ethyl Benzene

0.10 0.085 0.30 0.25Heptane

0.10 0.075 0.58 0.43Hexane

0.10 0.067 1.3 0.86Toluene


0.10 0.071 0.54 0.38m,p-Xylene

0.10 0.076 0.18 0.13o-Xylene

Page 5 of 17


Client Sample ID: 7

Lab ID#: 1706146-03A




0.20 0.13 0.40 0.26Acetone

0.40 0.25 0.42 0.26Benzene


0.10 0.066 0.14 0.096Chloroform

0.10 0.092 0.15 0.14Cyclohexane

0.40 0.26 1.0 0.66Ethyl Acetate

0.10 0.073 0.27 0.20Ethyl Benzene

0.10 0.086 0.36 0.31Heptane

0.10 0.075 0.69 0.52Hexane

0.10 0.067 1.6 1.1Toluene


0.10 0.071 0.77 0.55m,p-Xylene

0.10 0.077 0.25 0.19o-Xylene

Client Sample ID: 8

Lab ID#: 1706146-04A




0.20 0.13 0.28 0.18Acetone


0.10 0.073 0.16 0.12Ethyl Benzene

0.10 0.085 0.20 0.17Heptane

0.10 0.075 0.30 0.23Hexane

0.10 0.067 0.89 0.59Toluene

0.10 0.071 0.41 0.29m,p-Xylene

0.10 0.076 0.14 0.10o-Xylene

Page 6 of 17



Lab ID#: 1706146-05A




0.20 0.13 0.44 0.28Acetone


0.10 0.066 0.11 0.073Chloroform

0.10 0.092 0.11 0.10Cyclohexane

0.40 0.25 0.54 0.34Ethyl Acetate

0.10 0.073 0.18 0.13Ethyl Benzene

0.10 0.085 0.29 0.24Heptane

0.10 0.075 0.39 0.29Hexane

0.10 0.067 1.2 0.79Toluene

0.10 0.071 0.51 0.36m,p-Xylene

0.10 0.076 0.16 0.12o-Xylene

Client Sample ID: Dup

Lab ID#: 1706146-06A




0.20 0.13 0.31 0.20Acetone


0.10 0.073 0.18 0.13Ethyl Benzene

0.10 0.085 0.21 0.18Heptane

0.10 0.075 0.71 0.53Hexane

0.10 0.067 0.94 0.63Toluene

0.10 0.071 0.45 0.32m,p-Xylene

0.10 0.076 0.14 0.11o-Xylene



Page 7 of 17











Page 8 of 17






0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 0.18 0.181,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.063 0.41 0.262-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.41 0.27Acetone0.40 0.25 0.45 0.28Benzene0.10 0.074 0.43 0.32Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 0.12 0.082Chloroform0.10 0.092 0.14 0.12Cyclohexane1.0 0.48 Not Detected Not DetectedEthanol





Page 9 of 17






0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.065 Not Detected Not Detected1,2-Dichloroethane0.10 0.10 0.25 0.251,2,4-Trimethylbenzene0.10 0.098 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.063 0.34 0.212-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.40 0.26Acetone0.40 0.25 0.42 0.26Benzene0.10 0.074 0.37 0.28Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 0.14 0.096Chloroform0.10 0.092 0.15 0.14Cyclohexane1.0 0.49 Not Detected Not DetectedEthanol





Page 10 of 17











Page 11 of 17






0.10 0.080 Not Detected Not Detected1,1,1-Trichloroethane0.10 0.064 Not Detected Not Detected1,2-Dichloroethane0.10 0.099 0.15 0.151,2,4-Trimethylbenzene0.10 0.097 Not Detected Not Detected1,4-Dichlorobenzene0.10 0.063 0.32 0.202-Butanone (Methyl Ethyl Ketone)0.20 0.15 Not Detected Not Detected4-Methyl-2-pentanone0.20 0.13 0.44 0.28Acetone0.40 0.25 Not Detected Not DetectedBenzene0.10 0.074 0.38 0.28Carbon Tetrachloride0.10 0.073 Not Detected Not DetectedChlorobenzene0.10 0.066 0.11 0.073Chloroform0.10 0.092 0.11 0.10Cyclohexane1.0 0.48 Not Detected Not DetectedEthanol

0.40 0.25 0.54 0.34Ethyl Acetate0.10 0.073 0.18 0.13Ethyl Benzene0.10 0.085 0.29 0.24Heptane0.10 0.075 0.39 0.29Hexane0.10 0.076 Not Detected Not DetectedMethyl tert-butyl ether0.10 0.20 Not Detected Not DetectedNaphthalene0.10 0.087 Not Detected Not DetectedPropylbenzene0.10 0.081 Not Detected Not DetectedStyrene0.10 0.067 1.2 0.79Toluene0.10 0.084 Not Detected Not DetectedTetrachloroethene0.10 0.072 Not Detected Not DetectedTrichloroethene0.10 0.071 0.51 0.36m,p-Xylene0.10 0.076 0.16 0.12o-Xylene




Page 12 of 17

Client Sample ID: DupLab ID#: 1706146-06A










Page 13 of 17











Page 14 of 17











Page 15 of 17






111 70-1301,1,1-Trichloroethane102 70-1301,2-Dichloroethane96 70-1301,2,4-Trimethylbenzene86 50-1101,4-Dichlorobenzene97 70-1302-Butanone (Methyl Ethyl Ketone)120 70-1304-Methyl-2-pentanone77 70-130Acetone97 70-130Benzene112 70-130Carbon Tetrachloride110 70-130Chlorobenzene92 70-130Chloroform130 70-130Cyclohexane41 Q 50-130Ethanol99 70-130Ethyl Acetate106 70-130Ethyl Benzene114 70-130Heptane89 70-130Hexane113 70-130Methyl tert-butyl ether26 5-80Naphthalene114 70-130Propylbenzene79 20-100Styrene106 70-130Toluene106 70-130Tetrachloroethene109 70-130Trichloroethene103 70-130m,p-Xylene98 70-130o-Xylene

Q = Exceeds Quality Control limits.Container Type: NA - Not Applicable



Page 16 of 17






98 70-1301,1,1-Trichloroethane93 70-1301,2-Dichloroethane105 70-1301,2,4-Trimethylbenzene96 50-1101,4-Dichlorobenzene86 70-1302-Butanone (Methyl Ethyl Ketone)116 70-1304-Methyl-2-pentanone69 Q 70-130Acetone102 70-130Benzene98 70-130Carbon Tetrachloride114 70-130Chlorobenzene101 70-130Chloroform111 70-130Cyclohexane38 Q 50-130Ethanol94 70-130Ethyl Acetate115 70-130Ethyl Benzene109 70-130Heptane101 70-130Hexane101 70-130Methyl tert-butyl ether27 5-80Naphthalene128 70-130Propylbenzene83 20-100Styrene105 70-130Toluene109 70-130Tetrachloroethene106 70-130Trichloroethene110 70-130m,p-Xylene101 70-130o-Xylene

Q = Exceeds Quality Control limits.Container Type: NA - Not Applicable



Page 17 of 17

http://www.teklabinc.com/

July 19, 2017

WorkOrder: 17061062West Lake NPDES AnalysisRE:

Dear Paul V. Rosasco, P.E.:

TEKLAB, INC received 3 samples on 6/15/2017 6:40:00 PM for the analysis presented in the following report.

Samples are analyzed on an as received basis unless otherwise requested and documented. The sample results contained in this report relate only to the requested analytes of interest as directed on the chain of custody. NELAP accredited fields of testing are indicated by the letters NELAP under the Certification column. Unless otherwise documented within this report, Teklab Inc. analyzes samples utilizing the most current methods in compliance with 40CFR. All tests are performed in the Collinsville, IL laboratory unless otherwise noted in the Case Narrative.

All quality control criteria applicable to the test methods employed for this project have been satisfactorily met and are in accordance with NELAP except where noted. The following report shall not be reproduced, except in full, without the written approval of Teklab, Inc.

If you have any questions regarding these tests results, please feel free to call.

Sincerely,

25923 Gateway DriveGolden, CO 80401

(303) 940-3426TEL:FAX:

Paul V. Rosasco, P.E.Engineering Management Support, Inc.

Emily PohlmanProject Manager(618)344-1004 ex [email protected]

Page 1 of 25

This reporting package includes the following:

Report Contents

Client Project: West Lake NPDES Analysis

Client: Engineering Management Support, Inc.

Report Date: 19-Jul-17

Work Order: 17061062


Cover Letter 1

Report Contents 2

Definitions 3

Case Narrative 4

Accreditations 5

Laboratory Results 6

Sample Summary 12

Dates Report 13

Quality Control Results 16

Receiving Check List 25

Chain of Custody Appended

Page 2 of 25

____TeklabHdrP

Definitions






Abbr DefinitionCCV Continuing calibration verification is a check of a standard to determine the state of calibration of an instrument between recalibration.

DF Dilution factor is the dilution performed during analysis only and does not take into account any dilutions made during sample preparation. The reported result is final and includes all dilutions factors.

DNI Did not ignite

DUP Laboratory duplicate is an aliquot of a sample taken from the same container under laboratory conditions for independent processing and analysis independently of the original aliquot.

ICV Initial calibration verification is a check of a standard to determine the state of calibration of an instrument before sample analysis is initiated.

IDPH IL Dept. of Public Health

LCS Laboratory control sample, spiked with verified known amounts of analytes, is analyzed exactly like a sample to establish intra-laboratory or analyst specific precision and bias or to assess the performance of all or a portion of the measurement system. The acceptable recovery range is in the QC Package (provided upon request).

LCSD Laboratory control sample duplicate is a replicate laboratory control sample that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).

MBLK Method blank is a sample of a matrix similar to the batch of associated sample (when available) that is free from the analytes of interest and is processed simultaneously with and under the same conditions as samples through all steps of the analytical procedures, and in which no target analytes or interferences should present at concentrations that impact the analytical results for sample analyses.

MDL Method detection limit means the minimum concentration of a substance that can be measured and reported with 99% confidence that the analyte concentration is greater than zero.

MS Matrix spike is an aliquot of matrix fortified (spiked) with known quantities of specific analytes that is subjected to the entire analytical procedures in order to determine the effect of the matrix on an approved test method’s recovery system. The acceptable recovery range is listed in the QC Package (provided upon request).

MSD Matrix spike duplicate means a replicate matrix spike that is prepared and analyzed in order to determine the precision of the approved test method. The acceptable recovery range is listed in the QC Package (provided upon request).

MW Molecular weight

ND Not Detected at the Reporting Limit

NELAP NELAP Accredited

PQL Practical quantitation limit means the lowest level that can be reliably achieved within specified limits of precision and accuracy during routine laboratory operation conditions. The acceptable recovery range is listed in the QC Package (provided upon request).

RL The reporting limit the lowest level that the data is displayed in the final report. The reporting limit may vary according to customer request or sample dilution. The reporting limit may not be less than the MDL.

RPD Relative percent difference is a calculated difference between two recoveries (ie. MS/MSD). The acceptable recovery limit is listed in the QC Package (provided upon request).

SPK The spike is a known mass of target analyte added to a blank sample or sub-sample; used to determine recovery deficiency or for other quality control purposes.

Surr Surrogates are compounds which are similar to the analytes of interest in chemical composition and behavior in the analytical process, but which are not normally found in environmental samples.

TIC Tentatively identified compound: Analytes tentatively identified in the sample by using a library search. Only results not in the calibration standard will be reported as tentatively identified compounds. Results for tentatively identified compounds that are not present in the calibration standard, but are assigned a specific chemical name based upon the library search, are calculated using total peak areas from reconstructed ion chromatograms and a response factor of one. The nearest Internal Standard is used for the calculation. The results of any TICs must be considered estimated, and are flagged with a "T". If the estimated result is above the calibration range it is flagged "ET"

TNTC Too numerous to count ( > 200 CFU )

Qualifiers# - Unknown hydrocarbon B - Analyte detected in associated Method Blank

E - Value above quantitation range H - Holding times exceeded

I - Associated internal standard was outside method criteria J - Analyte detected below quantitation limits

M - Manual Integration used to determine area response ND - Not Detected at the Reporting Limit

R - RPD outside accepted recovery limits S - Spike Recovery outside recovery limits

T - TIC(Tentatively identified compound) X - Value exceeds Maximum Contaminant Level

Page 3 of 25

Case Narrative






Cooler Receipt Temp: 3.42 °C

Field pH was provided by Feezor Engineering.

Uranium analysis was performed by Pace, PA. See attached report for results and QC.

Locations

___________________________________Collinsville

5445 Horseshoe Lake Road

Collinsville, IL 62234-7425

(618) 344-1004

(618) 344-1005

[email protected]

___________________________________Springfield

3920 Pintail Dr

Springfield, IL 62711-9415

(217) 698-1004

(217) 698-1005

[email protected]

___________________________________Kansas City

8421 Nieman Road

Lenexa, KS 66214

(913) 541-1998

(913) 541-1998

[email protected]

___________________________________Collinsville Air

5445 Horseshoe Lake Road

Collinsville, IL 62234-7425

(618) 344-1004

(618) 344-1005

[email protected]

___________________________________Chicago

1319 Butterfield Rd.

Downers Grove, IL 60515

(630) 324-6855

[email protected]

Page 4 of 25

____TeklabHdrP

Accreditations






NELAPState Cert # Exp Date LabDept

Illinois 100226 1/31/2018 CollinsvilleNELAPIEPA

Kansas E-10374 4/30/2018 CollinsvilleNELAPKDHE

Louisiana 166493 6/30/2018 CollinsvilleNELAPLDEQ

Louisiana 166578 6/30/2018 CollinsvilleNELAPLDEQ

Texas T104704515-12-1 7/31/2018 CollinsvilleNELAPTCEQ

Arkansas 88-0966 3/14/2018 CollinsvilleADEQ

Illinois 17584 5/31/2017 CollinsvilleIDPH

Indiana C-IL-06 1/31/2018 CollinsvilleISDH

Kentucky 98006 12/31/2017 CollinsvilleKDEP

Kentucky 0073 1/31/2018 CollinsvilleUST

Louisiana LA170027 12/31/2017 CollinsvilleLDPH

Missouri 930 1/31/2018 CollinsvilleMDNR

Missouri 00930 5/31/2017 CollinsvilleMDNR

Oklahoma 9978 8/31/2017 CollinsvilleODEQ

Page 5 of 25http://www.teklabinc.com/

TeklabHdrP

Laboratory Results






Analyses Result Units Date AnalyzedRL DFCertification Qual

Collection Date: 06/15/2017 8:49

Lab ID: 17061062-001 Client Sample ID: OU-1-001

Matrix: AQUEOUS

Batch

STANDARD METHOD 4500-H B FIELDpH 06/15/2017 8:491.00 17.93 R234055

EPA 1664AHexane Extractable Material J 06/20/2017 12:035 mg/L 14NELAP R234236

EPA 600 375.2 REV 2.0 1993 (TOTAL)Sulfate S 06/16/2017 16:22200 mg/L 20214NELAP R234083

MS and MSD did not recover within control limits. Result is verified by re-analysis at a dilution.

STANDARD METHODS 2540 DTotal Suspended Solids 06/20/2017 14:066 mg/L 136NELAP R234218

STANDARD METHODS 2540 FSolids, Settleable 06/16/2017 10:370.1 ml/L 10.1NELAP R234070

STANDARD METHODS 3500-CR BChromium, Hexavalent 06/15/2017 21:140.010 mg/L 2< 0.010NELAP R234036

Elevated reporting limit due to sample composition.

STANDARD METHODS 4500-CL E (TOTAL)Chloride 06/20/2017 17:0310 mg/L 258NELAP R234261

STANDARD METHODS 4500-NH3 H MODIFIED (TOTAL)Nitrogen, Ammonia (as N) S 06/19/2017 18:100.10 mg/L 10.15NELAP R234156

MS and/or MSD did not recover within control limits due to matrix interference.

STANDARD METHODS 5210 BBiochemical Oxygen Demand 06/16/2017 11:295 mg/L 117NELAP 131299

STANDARD METHODS 5220 D (TOTAL)Chemical Oxygen Demand 06/21/2017 11:1350 mg/L 1104NELAP R234246

TRIVALENT CHROMIUMTrivalent Chromium 06/15/2017 21:110.010 mg/L 2< 0.010 R234036

Elevated reporting limit due to sample composition.

EPA 600 245.1 R3.0 (TOTAL)Mercury 06/20/2017 8:260.00020 mg/L 1< 0.00020NELAP 131337

EPA 600 4.1.4, 200.7R4.4, METALS BY ICP (TOTAL)Aluminum 06/19/2017 18:170.0250 mg/L 10.448NELAP 131300Antimony 06/20/2017 17:230.0500 mg/L 1< 0.0500NELAP 131300Arsenic 06/19/2017 18:170.0250 mg/L 1< 0.0250NELAP 131300Beryllium 06/19/2017 18:170.0005 mg/L 1< 0.0005NELAP 131300Cadmium 06/19/2017 18:170.0020 mg/L 1< 0.0020NELAP 131300Cobalt J 06/19/2017 18:170.0050 mg/L 10.0038NELAP 131300Copper 06/19/2017 18:170.0050 mg/L 10.0122NELAP 131300Iron 06/19/2017 18:170.0200 mg/L 11.05NELAP 131300Magnesium 06/21/2017 11:270.0500 mg/L 122.6NELAP 131300Nickel 06/19/2017 18:170.0050 mg/L 10.0112NELAP 131300Selenium 06/19/2017 18:170.0400 mg/L 1< 0.0400NELAP 131300Silver 06/19/2017 18:170.0050 mg/L 1< 0.0050NELAP 131300Thallium 06/19/2017 18:170.0500 mg/L 1< 0.0500NELAP 131300Zinc 06/19/2017 18:170.0100 mg/L 10.0609NELAP 131300

STANDARD METHODS 2340 B, HARDNESS (TOTAL)Hardness, as ( CaCO3 ) 06/21/2017 0:001.00 mg/L 1375NELAP 131300

EPA 600 624 (MODIFIED), VOLATILE ORGANIC COMPOUNDS BY GC/MSBenzene 06/19/2017 14:542.0 µg/L 1NDNELAP 131405

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Laboratory Results






Analyses Result Units Date

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