edible oil and biodiesel refining - biodiesel expansion - biodiesel reactors
TRANSCRIPT
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 1/11
Crude Oil Refining - Step 1
De-gumming Process / Removing of impurities and gums
Crude Oil Refining - Step 2Neutralizations Process / removing of FFA
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 2/11
Continuous Transesterification Process
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 3/11
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 4/11
Semi - Continuos -Batch
Transesterification Process
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 5/11
IKA Plants & Turnkey Systems
Highly sophisticated designs , using IKA dispersing and mixing equipment.
IKA - Process has been renowned the world over for many years as a
manufacture of high-shear mixing and dispersing machines.
IKA – Engineering provides the capability to design and fabricate complete
turnkey systems incorporating the IKA High-Shear technology.
As a result, IKA plant programs are created to precess ion with engineering
expertise.
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 6/11
Batch Agitation vs. Batch High-Shear
Conventional batch agitation for the transesterification process takes between 2 – 4 hour
per batch to convert the feedstock, methanol, and catalyst to methyl ester and glycerin.Precise des igned batch high-shear m ixer (not batch shear-pump mixer) accelerates the
conventional batch mixing process down to 10 - 30 minutes depending of quality of refined
oil, temperature, pressure and amount of methanol.
For mixing tanks above 1000 Gal. a recirculation process with in-line mixer is
recommended ins tead of top-entry mixer. Multiple sets of rotor and stator combined in one
machine can adopt the process in max. two passes. High-shear mixers with up to tree
sets of rotor/stator and flow-rates up to 1,500 GPM are available. In addition, these mixers
can operate with tanks after tanks.
Batch Process vs. Inline Process
Continuous flow processing is favored by larger
facilities. Continuous flow facilities usual ly process
at high temperatures and with Ultra-Shear to
shorten the process ing time and ensure highest
quality. The equipment (e.g. biodiesel reactor,
inline - high s hear, centrifugal separators) for
continuous flow processing does not usually
require a lot of space, and it can be scaled-up to
provide increased capacity without taking a
corresponding increase of space.
Current manufacturing
status
The leading oil refining
manufactures have adopted
the more cost effective in-line
ultra shear process. The
same manufactures are
adopting this process within
the new in-line
transesterification process .
More and more Bio-diesel
producer realizing that theconventional batch agitation
process is to time consuming
and expensive.
Biodiesel Process Systems
KA® is a global company that manufactures in Wilmington, NC. IKA provides a complete
line of batch, in-line high-shear mixing process equipment, and biodiesel reactors for a
variety of applications in the Bio-Diesel, Ethanol and Petroleum-Oil industry, such as de-
gumm ing, neutralization, bleaching, transesterification, esterification, water washing, wet-
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 7/11
grinding of cellulose sol id, catalyst reactions, and fuel-blending
The comprehensive IKA program emphasizes on s cale up
from Laboratory to Processingplants, with applications for ultra-shear and high-shear
mixing, dispers ing, homogenizing, grinding, emuls ifying, and particle s ize reduction IKA
has a fully equipped testing facility for testing, and als o has trial machines available for on-
site testing in Wilmington, NC
1 GPM primary and secondary
transesterification system (left)1,500 GPM multiple stage biodiesel reactor
(below)
Proven Technology for Biodiesel Production! Features of the BR
Continuous capacity of 1 gpm,or optional 2 gpm
Capacity is suitable for pilotplants or production
Ultra High Shear mixertechnology - used in reactionsfor over 50 years
Two stage transesterification
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 8/11
process ensures 100%conversion to M.E. & Glycerin
Accurately meters thefeedstock, methanol andcatalyst with precision gearpumps and high accuracy massflow meters
Connect the inlets to supplytanks, and outlets to theseparation process, and startproducing biodiesel !
A Complete Line of IKA Systems are Available for Transesterification, as
well as Degumming, Neutralization and Water Wash.BIOREAX System Capacities
BR 2000/04 BR 2000/05 BR 2000/10 BR 2000/20 BR 2000/30 BR 2000/40 BR 2000/50
2 gpm 10 gpm 40 gpm 100 gpm 180 gpm 300 gpm 550
BIOREAX Technical Specifications BR 2000/04
System Type: Transesterification
Capacity: 1 or 2 gpm
Classification: Class I, Div I, Grp D
High Shear Mixers (2): IKA LP 2000/04
Number of Stages: 3
Wetted materials: Stainless Steel
HP (each): 3
Sealing: Lip seal
Pumps (6): Rotary Gear
Wetted materials: Stainless Steel
Sealing: Mag Drive
Flow Meters (6): Coriolis / Mass Flow
Wetted materials: Stainless Steel
Piping: Seamless Tubing
Material: Stainless Steel
Base Frame: Two piece, stackable
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 9/11
Material: Stainless Steel
Controls: Optional
Type: Automatic or Manual
Enclosure: NEMA 12
Pricing
BR 2000/4-T, Two Stage Transesterification, 1 gpm................... $109,000
Control Package for BR 2000/4, Fully Automatic........................... $49,000
Special Show Pricing Valid Through April 1, 2008
Options
:BR 2000/4-T, Two Stage Transesterification, 2 gpm.................... On Request
Crude Oil Refining - Degumming and Neutralization ..................... On Request
Washing Process – Two Stage Water Wash.................................. On Request
Control Package Options: Manual, Refining, Wash, etc............... On Request
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 10/11
7/27/2019 Edible Oil and Biodiesel Refining - Biodiesel Expansion - Biodiesel Reactors
http://slidepdf.com/reader/full/edible-oil-and-biodiesel-refining-biodiesel-expansion-biodiesel-reactors 11/11