ector drums odessa, ector county, texas … drums odessa, ector county, texas data validation report...
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ECTOR DRUMS ODESSA, ECTOR COUNTY, TEXAS
DATA VALIDATION REPORT Date: June 11, 2015 Laboratory: Xenco Laboratories, Odessa, Texas Laboratory Project #: 508216 Data Validation Performed By: Lisa Graczyk, CSS-Dynamac Dynamac Work Order #: S101-21J This data validation report has been prepared by CSS-Dynamac. This report documents the data validation for seven soil samples and three waste liquid samples collected for the Ector Drums Site that were analyzed for the following parameters and U.S. Environmental Protection Agency methods:
Volatile Organic Compounds (VOC) by SW-846 Method 8260B Semivolatile Organic Carbons (SVOC) by SW-846 Method 8270C Polychlorinated biphenyls (PCB) by SW-846 Method 8082 Pesticides by SW-846 Method 8081A Total Petroleum Hydrocarbons (TPH) by Texas1005 Metals by SW-846 Method 6010B Mercury by SW-846 Method 7471A and 7470A Cyanide by SW-846 Method 9012B Flashpoint by SW-846 Method 1010
A level II data package was requested from Xenco Laboratories. The data validation was conducted in general accordance with the EPA “Contract Laboratory Program National Functional Guidance for Superfund Organic Methods Data Review” dated August 2014 and “Contract Laboratory Program National Functional Guidelines for Inorganic Superfund Data Review” dated August 2014. The Attachment contains the results summary sheets with the hand-written qualifiers applied during data validation.
001069
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 VOCs BY SW-846 METHOD 8260B 1. Samples
The following table summarizes the samples for which this data validation is being conducted.
Samples Lab ID Matrix Date Collected
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/27/2015 ED-S02 508216-002 Soil 5/19/2015 5/26/2015 ED-S03 508216-003 Soil 5/19/2015 5/26/2015 ED-S04 508216-004 Soil 5/20/2015 5/27/2015 ED-S05 508216-005 Soil 5/20/2015 5/26/2015 ED-S06 508216-006 Soil 5/20/2015 5/27/2015 ED-S07 508216-007 Soil 5/20/2015 5/27/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/26/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/26/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/28/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 14 days from sample collection.
3. Blanks
Method blanks were analyzed with the VOC analyses. The method blanks were free of target compound contamination above the reporting limits.
4. Surrogate Results
The surrogate recovery results were within the laboratory-established quality control (QC) limits except for as follows. In a few instances, one of the four surrogates were slightly outside the QC limits in the samples. No qualifications are required in these instances. The exceptions were for samples ED-SO6 and ED-S07. In these samples, two to three surrogates were detected high, above the QC limits. Detected VOCs in these two samples were flagged “J” as estimated due to potential matrix interferences.
001070
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 5. Laboratory Control Sample (LCS) Results
The LCS and LCS duplicate recoveries and relative percent differences (RPD) were within laboratory QC limits except for a few compounds in which the LCS was detected slightly high, above the QC limit. Because these compounds were not detected in the samples, no qualification was required.
6. Matrix Spike (MS) and Matrix Spike Duplicate (MSD) Results
A site-specific MS and MSD were analyzed using samples ED-S02 and ED-S07 as the spiked samples. Several of the recoveries were outside QC limits indicating matrix interferences with these samples.
For sample ED-S02, the MS and MSD recoveries were significantly outside QC limits. In this sample, all results were flagged. The quantitation limits for non-detect results were flagged “UJ” and the detected results were flagged “J” as estimated.
For sample ED-S07 MS/and MSD, if the MS/MSD recovery was low (indicating a low bias), detected results were flagged “J” and the quantitation limits for non-detected results were flagged “UJ” as estimated. If the MS/MSD recovery was high (indicating a high bias), detected results were flagged “J” as estimated in the parent sample.
7. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. Both samples only had toluene detected in them. However, the toluene concentration was much higher in the field duplicate resulting in an RPD of 139 between the two results. There appears to be sample heterogeneity associated with VOCs in the soil samples.
8. Overall Assessment
The VOC data are acceptable for use as qualified based on the information received.
001071
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 SVOCs BY SW-846 METHOD 8270C 1. Samples
The following table summarizes the samples for which this data validation is being conducted.
Samples Lab ID Matrix Date Collected
Date Prepared
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/26/2015 5/27/2015 ED-S02 508216-002 Soil 5/19/2015 5/26/2015 5/27/2015 ED-S03 508216-003 Soil 5/19/2015 5/26/2015 5/27/2015 ED-S04 508216-004 Soil 5/20/2015 5/26/2015 5/27/2015 ED-S05 508216-005 Soil 5/20/2015 5/26/2015 5/27/2015 ED-S06 508216-006 Soil 5/20/2015 5/26/2015 5/27/2015 ED-S07 508216-007 Soil 5/20/2015 5/26/2015 5/27/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/26/2015 5/27/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/26/2015 5/27/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/26/2015 5/27/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 14 days from sample collection to extraction and 40 days from extraction to analysis.
3. Blanks
Method blanks were analyzed with the SVOC analyses. The method blanks were free of target compound contamination above the reporting limits.
4. Surrogate Results
The surrogate recoveries were within the laboratory-established QC limits except for as follows. In some instances, one or two surrogates were slightly outside QC limits. No qualifications are required in these instances. In sample ED-WL08, three of the surrogates (non-phenolic SVOCs) were detected low, below the recovery QC limits. The quantitation limits for non-phenolic compounds in sample ED-WL08, were flagged “UJ” as estimated due to potential matrix interferences.
001072
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
In sample ED-WL09, three of the surrogates (non-phenolic and phenolic SVOCs) were detected low, below the recovery QC limits. In sample ED-WL09, the quantitation limits for non-detected SVOCs were flagged “UJ” and detected results were flagged “J” as estimated due to potential matrix interferences.
5. LCS Results
The percent recoveries and RPDs for the LCS and LCS duplicate results were within the laboratory-established QC limits. Note that one compound in one of the two LCSs was detected slightly below the QC limit. No qualification was applied for this minor discrepancy.
6. MS and MSD Results
A site-specific MS and MSD were not analyzed with this work order; therefore matrix interferences could not be evaluated using the MS/MSD.
7. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. Both samples contained no detections of SVOCs indicating good correlation between the samples.
8. Overall Assessment
The SVOC data are acceptable for use as qualified based on the information received.
001073
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
PCBs BY SW-846 METHOD 8082 1. Samples
The following table summarizes the samples for which this data validation was conducted.
Samples Lab ID Matrix Date Collected
Date Prepared
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/22/2015 5/28/2015 ED-S02 508216-002 Soil 5/19/2015 5/22/2015 5/28/2015 ED-S03 508216-003 Soil 5/19/2015 5/22/2015 5/28/2015 ED-S04 508216-004 Soil 5/20/2015 5/22/2015 5/28/2015 ED-S05 508216-005 Soil 5/20/2015 5/22/2015 5/28/2015 ED-S06 508216-006 Soil 5/20/2015 5/22/2015 5/28/2015 ED-S07 508216-007 Soil 5/20/2015 5/22/2015 5/28/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/26/2015 5/28/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/26/2015 5/28/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/26/2015 5/28/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 14 days from sample collection to extraction and 40 days from extraction to analysis.
3. Blanks
Method blanks were analyzed with the PCB analyses and were free of target compound contamination above the reporting limit.
4. Surrogates
The surrogate recoveries were within QC limits except for as follows. In the following samples, the surrogates were detected high above the QC limit indicating potential matrix interference: ED-S04 and ED-WL09. Because the recoveries indicate a high bias and there were no detections of PCBs in the samples, no qualification is required.
5. LCS Results
The LCS and LCS duplicate recoveries and RPDs were within the laboratory-established QC limits.
001074
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 6. MS and MSD Results
A site-specific MS and MSD were not analyzed.
7. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. Both samples contained no detections of PCBs indicating good correlation between the samples.
8. Overall Assessment
The PCB data are acceptable for use based on the information received.
PESTICIDES BY SW-846 METHOD 8081A 1. Samples
The following table summarizes the samples for which this data validation was conducted.
Samples Lab ID Matrix Date Collected
Date Prepared
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/22/2015 5/26/2015 ED-S02 508216-002 Soil 5/19/2015 5/22/2015 5/26/2015 ED-S03 508216-003 Soil 5/19/2015 5/22/2015 5/26/2015 ED-S04 508216-004 Soil 5/20/2015 5/22/2015 5/26/2015 ED-S05 508216-005 Soil 5/20/2015 5/22/2015 5/26/2015 ED-S06 508216-006 Soil 5/20/2015 5/22/2015 5/26/2015 ED-S07 508216-007 Soil 5/20/2015 5/22/2015 5/26/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/26/2015 5/27/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/26/2015 5/27/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/26/2015 5/27/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 14 days from sample collection to extraction and 40 days from extraction to analysis.
001075
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 3. Blanks
Method blanks were analyzed with the pesticide analyses. The method blanks were free of target compound contamination above the reporting limits.
4. Surrogates
The surrogate recoveries were within QC limits.
5. LCS Results
The LCS and LCS duplicate recoveries and RPDs were within the laboratory-established QC limits except for as follows.
For one LCS duplicate, the RPD for Endrin Aldehyde exceeded the QC limit. Because this compound was not detected in the samples, no qualification was required.
6. MS and MSD Results
A site-specific MS and MSD were not analyzed.
7. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. Both samples contained no detections of pesticides indicating good correlation between the samples.
8. Overall Assessment
The pesticide data are acceptable for use based on the information received.
001076
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
TPH BY TEXAS METHOD 1005 1. Samples
The following table summarizes the samples for which this data validation was conducted.
Samples Lab ID Matrix Date Collected
Date Prepared
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/21/2015 5/21/2015 ED-S02 508216-002 Soil 5/19/2015 5/21/2015 5/21/2015 ED-S03 508216-003 Soil 5/19/2015 5/21/2015 5/21/2015 ED-S04 508216-004 Soil 5/20/2015 5/21/2015 5/21/2015 ED-S05 508216-005 Soil 5/20/2015 5/21/2015 5/22/2015 ED-S06 508216-006 Soil 5/20/2015 5/21/2015 5/22/2015 ED-S07 508216-007 Soil 5/20/2015 5/21/2015 5/22/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/21/2015 5/22/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/21/2015 5/22/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/21/2015 5/22/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 14 days from sample collection to extraction and 40 days from extraction to analysis.
3. Blanks
Method blanks were analyzed with the TPH analyses. The method blanks were free of target compound contamination above the reporting limits.
4. Surrogates
The surrogate recoveries were within QC limits.
5. LCS Results
The LCS and LCS duplicate recoveries and RPDs were within the laboratory-established QC limits.
001077
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
6. MS and MSD Results
A site-specific MS and MSD were not analyzed. For the MS that was analyzed (using a sample from another project), the recoveries were within QC limits.
7. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. The RPDs were calculated for detected TPHs and ranged from 22 to 49 percent which is acceptable.
8. Overall Assessment
The TPH data are acceptable for use based on the information received.
001078
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 METALS BY SW-846 METHOD 6010B 1. Samples
The following table summarizes the samples for which this data validation is being conducted.
Samples Lab ID Matrix Date Collected
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/28/2015 ED-S02 508216-002 Soil 5/19/2015 5/28/2015 ED-S03 508216-003 Soil 5/19/2015 5/28/2015 ED-S04 508216-004 Soil 5/20/2015 5/28/2015 ED-S05 508216-005 Soil 5/20/2015 5/28/2015 ED-S06 508216-006 Soil 5/20/2015 5/28/2015 ED-S07 508216-007 Soil 5/20/2015 5/28/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/28/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/28/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/28/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 180 days from sample collection to analysis.
3. Blank Results
Method blanks were analyzed with the metals analysis. The blanks were free of target analyte contamination above the reporting limits.
4. LCS Results
The LCS and LCS duplicate recoveries and RPDs were within the laboratory-established QC limits for target analytes.
5. MS and MSD Results
An MS and MSD were analyzed using sample ED-S01 as the spiked sample. The percent recoveries and RPDs were within QC limits except for as follows.
In some instances of QC limit exceedance, the sample concentration was more than four times the spiked amount. In these instances, no qualification was required.
001079
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
The following compounds were detected low in the MS and/or MSD: antimony, barium, chromium, lead, magnesium, manganese, nickel, and zinc. The quantitation limits for non-detected results were flagged “UJ” and the detected results were flagged “J” as estimated due to apparent matrix interference.
6. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. The RPDs were calculated for detected metals and ranged from 0 to 21 percent which is acceptable.
7. Overall Assessment
The metals data are acceptable for use as qualified based on the information received.
MERCURY BY SW-846 METHOD 7471A and 7470A 1. Samples
The following table summarizes the samples for which this data validation is being conducted.
Samples Lab ID Matrix Date Collected
Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/27/2015 ED-S02 508216-002 Soil 5/19/2015 5/27/2015 ED-S03 508216-003 Soil 5/19/2015 5/27/2015 ED-S04 508216-004 Soil 5/20/2015 5/27/2015 ED-S05 508216-005 Soil 5/20/2015 5/27/2015 ED-S06 508216-006 Soil 5/20/2015 5/27/2015 ED-S07 508216-007 Soil 5/20/2015 5/27/2015 ED-WL08 508216-008 Liquid 5/20/2015 5/27/2015 ED-WL09 508216-009 Liquid 5/20/2015 5/27/2015 ED-WL10 508216-010 Liquid 5/20/2015 5/27/2015
2. Holding Times
The samples were analyzed within the required holding time limit of 28 days from sample collection to analysis.
001080
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 3. Blank Results
Method blanks were analyzed with the mercury analyses and were free of target analyte contamination above the reporting limits.
4. LCS Results
The LCS and LCS duplicate recoveries and RPDs were within the laboratory-established QC limits for target analytes.
5. MS and MSD Results
An MS and MSD were analyzed using sample ED-S01 as the spiked sample. The percent recoveries were low indicating matrix interference. In sample ED-SO1, the mercury result was flagged “J” as estimated.
6. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. The RPD was calculated to be 42 percent which is acceptable.
7. Overall Assessment
The mercury data are acceptable for use as qualified based on the information received.
001081
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216 GENERAL CHEMISTRY PARAMETERS (Flashpoint by 1010 and Cyanide by 9012B) 1. Samples
The following table summarizes the samples for which this data validation is being conducted.
Samples Lab ID Matrix Date Collected Date Analyzed
ED-S01 508216-001 Soil 5/19/2015 5/27/2015 – 5/28/2015 ED-S02 508216-002 Soil 5/19/2015 5/27/2015 – 5/28/2015
ED-S03 508216-003 Soil 5/19/2015 5/27/2015 – 5/28/2015
ED-S04 508216-004 Soil 5/20/2015 5/27/2015 – 5/28/2015
ED-S05 508216-005 Soil 5/20/2015 5/27/2015 – 5/28/2015
ED-S06 508216-006 Soil 5/20/2015 5/27/2015 – 5/28/2015
ED-S07 508216-007 Soil 5/20/2015 5/27/2015 – 5/28/2015
ED-WL08 508216-008 Liquid 5/20/2015 5/26/2015 – 5/28/2015
ED-WL09 508216-009 Liquid 5/20/2015 5/26/2015 – 5/28/2015
ED-WL10 508216-010 Liquid 5/20/2015 5/26/2015 – 5/28/2015
2. Holding Times
The method states that flashpoint should be analyzed as soon as possible. The samples were analyzed for flashpoint 6-8 days after collection. No qualifications were applied. For cyanide, the holding time limits are acceptable.
3. LCS Results
The percent recoveries and RPDs for the LCSs and LCS duplicates were within QC limits. 4. Method Blank Results
Method blanks were analyzed with the cyanide analyses. The method blanks were free of contamination.
5. MS and MSD Results
An MS and MSD were analyzed with the cyanide analysis using sample ED-S01 as the spiked sample. The percent recoveries and RPDs were acceptable. The RPD for the MS was slightly low; however, no qualification was applied for this minor discrepancy.
001082
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
6. Field Duplicate Results
Sample ED-S07 is a field duplicate of sample ED-S05. All general chemistry parameters contained no detections indicating good correlation between the samples.
7. Overall Assessment
The general chemistry data are acceptable for use based on the information received.
001083
Data Validation Report Ector Drums Site Xenco Laboratories Laboratory Project #: 508216
ATTACHMENT
XENCO LABORATORIES RESULTS SUMMARY WITH QUALIFIERS
001084
Certificate of Analys1::. ..Jummary 508216 Dynamac Corporation, Richardson, TX
(
Project Id: Project Name: A6KS
Contact: Lisa Graczyk
Project Location: ~
Labfd: 508216-001
Fiddfd: ED-SOI Analysis Requested
Deptlt:
Matrix: SOIL
Sampled: May-19-15 00:00
Flash Point (Cq SW-846 1010 Extracted:
SUB: TX104704215 Analyud: May-27-15 09:15
Umts/RL: DcgF RL
Flash Point >180 75.0
Mercury by SW 7471A Exlracted: May-27-15 15:00
SUB: TX104704215 Analyud: May-27-15 20:33
UniWRL: mg'lcg RL
Mercury ::r 0. 114 0.0237
TM anal)1xal rq><>rt, oad 1bc-.. dala pacbc< • r<po:mm.. Im bcea .-le ilr your admtvc and coofidmbal uoc. ne ~ ....i rcmJu apt<StCd -,i-1 lhz> oml)tJcol r<por< r<p<"""'1 ll>< -J""cJn<Dl oeXENCO ~ XENCO Lobo-.ics assumes no raporu!Dolity ond motes no •-anar.I)' to die co:! use or die dlla ilcttby pmcn<ed. Om liability iJ 6mi1ed k> cbe amount iM""Oiccd for tbi1 • vrt order UDless oCbcrwisc: a.grc:ed lo ia •Titirig.
508216-002
ED-S02
SOIL
May-19-15 00:00
May-27-15 10:45
DegF RL >180 75.0
May-27-15 15:00
May-27-15 20:39
mgllcg RL 0.1 13 0.0203
Houslon - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 10 of 107
Date Receh·ed in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MA Y -15
Project Mana2er: 508216-003 508216-004
ED-S03 ED-S04
SOIL SOIL
May-19-15 00:00 May-19- 15 00:00
May-27-15 11:30 May-27-1512:15
DegF RL Deg F RL >180 75.0 >180 15.0
May-27-15 15:00 May-27-15 15:00
May-27-15 20:41 May-27-15 20:43
mgllcg llL mg/leg RL 0.467 0.0261 0.0653 0.0195
Final 1.000
Kelsey Brooks ----508216-005
ED-SOS
SOIL
May-19-15 00:00
May-27-15 13:00
DegF RL >180 75.0
May-27-15 15:00
May-27-15 20:49
mgllcg RL 0.0-477 0.0226
Kelsey Brooks Project Manager
508216-006
ED-S06
SOIL
May-19-15 00:00
May-27-15 13:45
Deg F RL >180 75.0
May-27-15 15:00
May-27-15 20:51
mgllcg RL 0.0657 0.0211
001085
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
Organochlorine Pesticides by EPA8081A
SUB: TX104704215May-26-15 14:00 May-26-15 14:18 May-26-15 14:55 May-26-15 15:13 May-26-15 15:32 May-26-15 15:50
ug/kg Units/RL: ug/kg ug/kg ug/kg ug/kg
May-22-15 12:15Extracted: May-22-15 12:24 May-22-15 12:33 May-22-15 12:36 May-22-15 12:39 May-22-15 12:42
Analysis Requested
508216-001Lab Id:
Field Id: ED-SO1
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 4.10 103 103
4,4-DDD 4,4-DDE 4,4-DDT Aldrin Alpha-BHC Alpha-Chlordane Beta-BHC Delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone Gamma-BHC (Lindane) Gamma-Chlordane Heptachlor Heptachlor Epoxide Methoxychlor Chlordane Toxaphene
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 7.56 189 189
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
0.939
23.5 23.5
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 7.51 188 188
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 4.14 103 103
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 7.74 193 193
508216-002
ED-SO2
SOIL
May-19-15 00:00
508216-003
ED-SO3
SOIL
May-19-15 00:00
508216-004
ED-SO4
SOIL
May-19-15 00:00
508216-005
ED-SO5
SOIL
May-19-15 00:00
508216-006
ED-SO6
SOIL
May-19-15 00:00
RL RL RL RL RL RL
Analyzed:
ug/kg
Page 11 of 107 Final 1.000
001086
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
PCBs by EPA 8082SUB: TX104704215
Percent Moisture
May-28-15 11:08
May-22-15 17:30
May-28-15 11:25
May-22-15 17:30
May-28-15 12:15
May-22-15 17:30
May-28-15 12:32
May-22-15 17:30
May-28-15 12:49
May-22-15 17:30
May-28-15 13:05
May-22-15 17:30
ug/kg
%
Units/RL:
Units/RL:
ug/kg
%
ug/kg
%
ug/kg
%
ug/kg
%
May-22-15 12:15Extracted:
Extracted:
May-22-15 12:24 May-22-15 12:33 May-22-15 12:36 May-22-15 12:39 May-22-15 12:42
Analysis Requested
508216-001Lab Id:
Field Id: ED-SO1
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDND
18.9
103 103 103 103 103 103 103
1.00
PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260
Percent Moisture
NDNDNDNDNDNDND
11.9
378 378 378 378 378 378 378
1.00
NDNDNDNDNDNDND
29.0
46.9 46.9 46.9 46.9 46.9 46.9 46.9
1.00
NDNDNDNDNDNDND
11.4
188 188 188 188 188 188 188
1.00
NDNDNDNDNDNDND
19.5
103 103 103 103 103 103 103
1.00
NDNDNDNDNDNDND
14.0
193 193 193 193 193 193 193
1.00
508216-002
ED-SO2
SOIL
May-19-15 00:00
508216-003
ED-SO3
SOIL
May-19-15 00:00
508216-004
ED-SO4
SOIL
May-19-15 00:00
508216-005
ED-SO5
SOIL
May-19-15 00:00
508216-006
ED-SO6
SOIL
May-19-15 00:00
RL
RL
RL
RL
RL
RL
RL
RL
RL
RL
RL
RL
Analyzed:
Analyzed:
ug/kg
%
Page 12 of 107 Final 1.000
001087
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
SVOAs by EPA 8270CSUB: TX104704215 May-27-15 15:34 May-27-15 15:59 May-27-15 16:24 May-27-15 16:50 May-27-15 17:15 May-27-15 17:41
mg/kg Units/RL: mg/kg mg/kg mg/kg mg/kg
May-26-15 16:45Extracted: May-26-15 16:48 May-26-15 16:51 May-26-15 16:54 May-26-15 16:57 May-26-15 17:00
Analysis Requested
508216-001Lab Id:
Field Id: ED-SO1
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 4.10 2.05 2.05 2.05 2.05 2.05 2.05 4.10 2.05 2.05 4.10 4.10 4.10 2.05 2.05 4.10 2.05
1,2,4-Trichlorobenzene 1,2-Dichlorobenzene 1,3-Dichlorobenzene 1,4-Dichlorobenzene 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol 2,4-Dichlorophenol 2,4-Dimethylphenol 2,4-Dinitrophenol 2,4-Dinitrotoluene 2,6-Dinitrotoluene 2-Chloronaphthalene 2-Chlorophenol 2-Methylnaphthalene 2-methylphenol 2-Nitroaniline 2-Nitrophenol 3&4-Methylphenol 3,3-Dichlorobenzidine 3-Nitroaniline 4,6-dinitro-2-methyl phenol 4-Bromophenyl-phenylether 4-chloro-3-methylphenol 4-Chloroaniline 4-Chlorophenyl Phenyl Ether
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 3.78 1.89 1.89 1.89 1.89 1.89 1.89 3.78 1.89 1.89 3.78 3.78 3.78 1.89 1.89 3.78 1.89
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 4.69 2.35 2.35 2.35 2.35 2.35 2.35 4.69 2.35 2.35 4.69 4.69 4.69 2.35 2.35 4.69 2.35
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
7.82 NDNDNDND
1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 3.75 1.88 1.88 1.88 1.88 1.88 1.88 3.75 1.88 1.88 3.75 3.75 3.75 1.88 1.88 3.75 1.88
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 4.14 2.07 2.07 2.07 2.07 2.07 2.07 4.14 2.07 2.07 4.14 4.14 4.14 2.07 2.07 4.14 2.07
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 3.87 1.93 1.93 1.93 1.93 1.93 1.93 3.87 1.93 1.93 3.87 3.87 3.87 1.93 1.93 3.87 1.93
508216-002
ED-SO2
SOIL
May-19-15 00:00
508216-003
ED-SO3
SOIL
May-19-15 00:00
508216-004
ED-SO4
SOIL
May-19-15 00:00
508216-005
ED-SO5
SOIL
May-19-15 00:00
508216-006
ED-SO6
SOIL
May-19-15 00:00
RL RL RL RL RL RL
Analyzed:
mg/kg
Page 13 of 107 Final 1.000
001088
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
SVOAs by EPA 8270CSUB: TX104704215 May-27-15 15:34 May-27-15 15:59 May-27-15 16:24 May-27-15 16:50 May-27-15 17:15 May-27-15 17:41
mg/kg Units/RL: mg/kg mg/kg mg/kg mg/kg
May-26-15 16:45Extracted: May-26-15 16:48 May-26-15 16:51 May-26-15 16:54 May-26-15 16:57 May-26-15 17:00
Analysis Requested
508216-001Lab Id:
Field Id: ED-SO1
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
4.10 4.10 2.05 2.05 4.10 2.05 2.05 2.05 2.05 2.05 2.05 12.3 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05
4-Nitroaniline 4-Nitrophenol Acenaphthene Acenaphthylene Aniline (Phenylamine, Aminobenzene) Anthracene Benzo(a)anthracene Benzo(a)pyrene Benzo(b)fluoranthene Benzo(g,h,i)perylene Benzo(k)fluoranthene Benzoic Acid Benzyl Butyl Phthalate bis(2-chloroethoxy) methane bis(2-chloroethyl) ether bis(2-chloroisopropyl) ether bis(2-ethylhexyl) phthalate Chrysene Dibenz(a,h)Anthracene Dibenzofuran Diethyl Phthalate Dimethyl Phthalate di-n-Butyl Phthalate di-n-Octyl Phthalate Fluoranthene
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
10.6 NDNDNDNDNDNDNDND
3.78 3.78 1.89 1.89 3.78 1.89 1.89 1.89 1.89 1.89 1.89 11.3 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
2.90 NDNDNDNDNDNDNDND
4.69 4.69 2.35 2.35 4.69 2.35 2.35 2.35 2.35 2.35 2.35 14.1 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
3.75 3.75 1.88 1.88 3.75 1.88 1.88 1.88 1.88 1.88 1.88 11.3 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
4.14 4.14 2.07 2.07 4.14 2.07 2.07 2.07 2.07 2.07 2.07 12.4 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
3.87 3.87 1.93 1.93 3.87 1.93 1.93 1.93 1.93 1.93 1.93 11.6 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93
508216-002
ED-SO2
SOIL
May-19-15 00:00
508216-003
ED-SO3
SOIL
May-19-15 00:00
508216-004
ED-SO4
SOIL
May-19-15 00:00
508216-005
ED-SO5
SOIL
May-19-15 00:00
508216-006
ED-SO6
SOIL
May-19-15 00:00
RL RL RL RL RL RL
Analyzed:
mg/kg
Page 14 of 107 Final 1.000
001089
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
SVOAs by EPA 8270CSUB: TX104704215
TPH by Texas1005
May-27-15 15:34
May-21-15 22:46
May-27-15 15:59
May-21-15 23:07
May-27-15 16:24
May-21-15 23:30
May-27-15 16:50
May-21-15 23:53
May-27-15 17:15
May-22-15 00:14
May-27-15 17:41
May-22-15 08:27
mg/kg
mg/kg
Units/RL:
Units/RL:
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
mg/kg
May-26-15 16:45
May-21-15 14:00
Extracted:
Extracted:
May-26-15 16:48
May-21-15 14:00
May-26-15 16:51
May-21-15 14:00
May-26-15 16:54
May-21-15 14:00
May-26-15 16:57
May-21-15 14:00
May-26-15 17:00
May-21-15 14:00
Analysis Requested
508216-001Lab Id:
Field Id: ED-SO1
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND3950
332 4280
2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 2.05 4.10 2.05 4.10 2.05 4.10
30.7 30.7 30.7 30.7
Fluorene Hexachlorobenzene Hexachlorobutadiene Hexachlorocyclopentadiene Hexachloroethane Indeno(1,2,3-c,d)Pyrene Isophorone Naphthalene Nitrobenzene N-Nitrosodi-n-Propylamine N-Nitrosodiphenylamine Pentachlorophenol Phenanthrene Phenol Pyrene Pyridine
C6-C12 Gasoline Range Hydrocarbons C12-C28 Diesel Range Hydrocarbons C28-C35 Oil Range Hydrocarbons Total TPH 1005
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
529 27100
2070 29700
1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 1.89 3.78 1.89 3.78 1.89 3.78
283 283 283 283
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND650
40.5 691
2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 2.35 4.69 2.35 4.69 2.35 4.69
35.2 35.2 35.2 35.2
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND33700
2510 36200
1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 1.88 3.75 1.88 3.75 1.88 3.75
282 282 282 282
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND2220
123 2340
2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 2.07 4.14 2.07 4.14 2.07 4.14
31.0 31.0 31.0 31.0
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
ND6910
634 7540
1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 1.93 3.87 1.93 3.87 1.93 3.87
145 145 145 145
508216-002
ED-SO2
SOIL
May-19-15 00:00
508216-003
ED-SO3
SOIL
May-19-15 00:00
508216-004
ED-SO4
SOIL
May-19-15 00:00
508216-005
ED-SO5
SOIL
May-19-15 00:00
508216-006
ED-SO6
SOIL
May-19-15 00:00
RL
RL
RL
RL
RL
RL
RL
RL
RL
RL
RL
RL
Analyzed:
Analyzed:
mg/kg
mg/kg
Page 15 of 107 Final 1.000
001090
Project Id:
Certificate of AnalysC .Jummary 508216 Dynamac Corporation, Richardson, TX
Project Name: A6KS
(
Contact: Lisa Graczyk
Project Location:
Date Receirni in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MA Y-1 S
-Labld: 508216-001
Analysis Requested Field Id: ED-SOI
Depth:
Matrix: SOIL
Sampled: May-19-15 00:00
Total Metals by EPA 6010B Extracted: May-27-15 13:30
SUB: TX104704215 Analyud: May-28-15 00:42
Units/RL: mg/kg RL
Aluminum 6570 22.0
Antimony i)I ND 2.20
Arsenic 7.05 2-20 -Barium J 266 LIO
Beryllium 0.807 0.440
Cadmium ND 1.10
Calcium 136000 22.0
Chromium J 103 1.10
Cobalt 4 .10 1.10
Copper 17.8 2.20
Iron 8380 22.0
Lead ::r 178 2-20
Magnesium :r 2940 44.0
Mang;mese ""t- 386 2.20
Nie Ice I -:J' 48.9 1.10
Potassium 1480 55.0
Selenium ND 3.30
Silver ND 3.30
Sodium 126 55.0
Thallium ND 2.20
Vanadium 18.5 9.91
Zinc :r 301 3.30
n;. aaalybcal rqiort. and thc: CDbrc datl ~it rq>me11ts, has bcao mode ror >""' oclusrw and <OAlidcamJ-. T1ic ~ad rcsu1u opn:ncd ........,_.din mal)1Xal rcpoct """""''die bcstjadcmmtof XENCO ~ )(El,"C() lobonlorics ........ DO rc>pOl!Sibildy and makes DO -1)' to tk aid l1SC of tbe dlJa bcreby pm<DtN. Our tiabiltty is limited lo the - itwoicod roe lhis wort: order onless ~ agn:cd to ia .. Tiling.
-~
508216-002 508216-003
ED-S02 ED-S03
SOlL SOIL
May- 19- 15 00:00 May-19-15 00:00
May-27-15 13:30 May-27-15 13:30
May-28-15 01 :30 May-28-15 01:37
mg/kg RL mg/kg RL
1590 21.8 5710 26.1
ND 2. 18 4.92 2.61
2.56 2 .18 7.51 2-61
137 1.09 363 1.30
ND 0.436 0.766 0.522
ND 1.09 ND L30
121000 21.8 91900 26. I
7.45 1.09 460 L30
1.52 1.09 21.l 1.30
6.68 2. 18 178 2.GI
3200 21.8 ~700E 26. I
15.0 2.18 476 2 .61
944 43.6 1880 52.2
99.3 2.18 15900 2.61
2.82 1.09 56. 1 1.30
363 54.6 1760 65.2
'ND 3.27 5 .25 3.91
ND 3.27 ND 3.91
81.9 54.6 3200 65.2
ND 2. 18 ND 2.61
ND 9.82 38.4 11.7
7S.S 3.27 825 3.91
Houslon - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 16 of 107
P ' M K l B ks ro1ect ana2er: e sey roo
508216-004
ED-S04
SOLL
May-19-15 00:00
May-27-15 13:30
May-28-15 01 :44
mg/kg RL
2560 22.6
ND 2.26
ND 2.26
151 1.13
ND 0.451
2.10 1.13
80100 22.6
57.0 1.13
2.65 1.13
13.9 2.26
6040 22.6
169 2.26
1190 45.1
108 2.26
79.0 1.13
684 56.4
ND 3.39
ND 3.39
503 56.4
ND 2.26
ND 10.2
159 3.39
Final 1.000
5082 16-005
ED-SOS
SOIL
Ma)·-19-15 00:00
May-27-15 13:30
May-28-15 01:5 1
mg/kg RL
4220 23.9
ND 2.39
3.20 2.39
312 1. 19
ND 0.478
ND 1.19
17-IOO 23.9
11.0 1.19
2.08 1.19
7.94 2.39
4690 23.9
35.7 2.39
1480 47.8
59.8 2.39
13.1 1.19
1190 59.7
ND 3.58
ND 3.58
1020 59.7
ND 2.39
ND 10.8
164 3.58
Kelsey Brooks Project Manager
--508216-006
ED-S06
SOIL
May-19-15 00:00
May-27-15 13:30
May-28- I 5 0 1 :57
mg/kg RL
3380 21.1
ND 2.11
2.55 2 .11
200 1.06
ND 0.423
ND 1.06
66200 21.1
8.70 1.06
1.59 1.06
5.71 2.11
3860 21.1
21.2 2 .11
1230 42.3
44.5 2.11
5.90 1.06
989 52.8
ND 3.17
ND 3.17
515 52.8
ND 2 .11
ND 9.51
168 3.17
001091
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
Total and Amenable Cyanide by SW-846 9012B
SUB: TX104704215May-28-15 14:16 May-28-15 14:20 May-28-15 14:22 May-28-15 14:23 May-28-15 14:25 May-28-15 14:13
mg/kg Units/RL: mg/kg mg/kg mg/kg mg/kg
May-27-15 17:48Extracted: May-27-15 17:48 May-27-15 17:48 May-27-15 17:48 May-27-15 17:48 May-27-15 17:48
Analysis Requested
508216-001Lab Id:
Field Id: ED-SO1
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
ND 0.588 Cyanide, Total ND 0.566 1.59 0.588 ND 0.588 ND 0.577 ND 0.566
508216-002
ED-SO2
SOIL
May-19-15 00:00
508216-003
ED-SO3
SOIL
May-19-15 00:00
508216-004
ED-SO4
SOIL
May-19-15 00:00
508216-005
ED-SO5
SOIL
May-19-15 00:00
508216-006
ED-SO6
SOIL
May-19-15 00:00
RL RL RL RL RL RL
Analyzed:
mg/kg
Page 17 of 107 Final 1.000
001092
Certificate of Analysh. ... ummary 508216 Dynamac Corporation, Richardson, TX
(
Project Id: Project Name: A6KS
Contact: Lisa Graczyk Project Location:
Analysis Requested
VOAs by SW-846 82608 SUB: TX104704215
Benzene
Bromobenzene
Bromochloromethanc
Bromodichloromethane
Brornofonn
Methyl bromide
tert-Butylbenzene
Scc-Butylbenzene
n-Butylbenze:ne
Qirbon Tetrachloride
Cblorobenzenc
Cbloroethane
Cblorofonn
Methyl Chloride
2-Chlorotoluene
4-Chlorotoluene
p-Cymene (p-Isopropyltoluene)
1,2-Dibromo-3-Chloropropane
Dibromochloromethanc
1,2-Dibromoethane
Methylene bromide
1,2-Dichlorobenzene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
DichlorodiOuoromethane
Lab Id: 508216--001
Field Id: ED-SOI
Depth:
f'tfatr.ix: SOIL
Sampled: May-19-15 00:00
Extracted.· May-27-15 16:04
Analyzed: May-27-15 16:47
Units/RL: mg/kg RL
ND 0.00632
ND 0.()0632
ND 0.110632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.0126
ND 0.00632
ND 0.0126
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
is analytical n:port, and thr cn<U. d3ta ~ ii rcpre=IS, hos bca> made IOr )""' cxclusi•-. ii.Id coafidenaial use.. 111 Th x Our
c ~tions .. d =ulb c.~~t ILi< ...!)""'1 ttpo<t r<f>'..- lh.c: bcsljDdgmml ofXENCTJ Labo-n<s. e;co Ubon?orie< ....,.,.,. no r<Spo"'ihllity and iml:ei: no ""'""''Y ro lbe end use or me dala herd>y Jl«Selll«I.
liability is limited to the amow-..1 i.n\'Oiocd b ~i:S •'OC'k: order a.nJcu othCNiijC .agrud t> io 'Ariting.
508216-002
ED-S02
SOLL
May-19-15 00:00
May-26-15 13:10
May-26-15 13:30
mg/leg RL
/ 1~ND 0.00567
lfj' ND 0.00567
1J1 ND 0.00567
U1 ND 0.00567
' r "(ND 0.00567
j;f' ND 0.00567
U~ND 0.00567
U5 ND 0.00567
T 0.0216 0.00567
YrlND 0.00567
I ND 0.00567
ND 0.0113
ND 0.00567
ND 0.0113
ND 0.00567
,1 ND 0.00567 -____, 0.0138 0.00567
11 \' ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
\/ND 0.00567
Howton - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 18 of 107
Date Received in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MA Y -15
508216-003
ED-S03
SOIL
May-19-15 00:00
May-26-15 13:20
May-26-15 17:50
mg/leg RL ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.0141
ND 0.00703
ND 0.0141
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.0070J
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ro1ect anager: e sey roo s P. M K l B k
508216-004 508216-005 508216-006
ED-S04 ED-SOS ED-S06
SOlL SOIL SOlL
May-19-15 00:00 May-19-15 00:00 May-19-15 00:00
May-27-15 I 6:06 May-26-15 13:24 May-27-15 16:08
May-27-15 18:04 May-26-15 18:42 May-27-15 18:55
mg/kg RL mg/leg RL mglkg RL
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.110621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 .ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.0114 ND 0.0124 ND 0.0116
ND 0.00568 )1,1) 0.00621 ND 0.00582
ND 0.0114 ND 0.0124 ND 0.0116
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.1)()621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
~-1~ Final 1.000
Kelsey Brooks Project Manager
001093
Certificate of Analy -.. _,ummary 508216 Dynamac Corporation, Richardson, TX
(
Project Id: Project Name: A6KS
Contact: Lisa Graczyk
Project Location:
---
Analysis Requested
VOAs by SW-846 8260B SUB: TX104704215
1,2-Dichlorocthanc
I , 1-Dichloruclhane
trans-1,2-dicbloroethylene
cis-1,.2-Dichloroethylenc
I, 1-Dichloroelbene
2,2-Dichloropropane
1.3-Dichloropropane
1.2-Dichloropropanc
trans-1,3-dichloropropene
I , 1-Dichloropropcne
cis-1,3-Dichloropropcne
Etbylbenune
Hexachlorobutadienc
lsopropylbenzene
Methylene Chloride
MTBE
Naphthalene
o-Propylbenzene
Styrene
1, 1, I ,2-Te1rachloroelhane
I , l ,2,2-Te1rachloroetbanc
Tetrachloroethylenc
Toluene
1,2.3-Trichlorobenzene
1,2,4-Trichlorobenzene
-~ ~
Lab Id: 508216-001
Fiebl Id: ED-SOI
Depth:
Matrix: SOIL
Sampled: May-19-15 00:00
Extracted: May-27-15 16:04
Ana/yud: May-27-15 16:47
Units/Rl: mg/l<g RL ND 0.00632
ND 0.00632 -
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.0253
ND 0.00632
ND 0.0126
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
ND 0.00632
s ....fytlcol r<pOrt. -S the m'1t< dlla ~it reprcscalS, h1s been i-'< li:lr yoar cnhnm Uld COllfidelohal.,,. 11:J Tic XEN
~-1rcsalt1o;,,..,...,.t"""""'°"11hi1 -1)..X.I n:portn:prcocn11hc i.c.t.....,_ ofXelCO ~ 'CO Ubor>toncs UIUIDCS no rcspaosibtlil) and maltcs ao ,._ IG lhc C..S..,. af lhc dlla h<ttby prncnltd.
°"'" balnbry r1 lmu1od IG the ....,.,.. m•'Goecd for this wartc anlcr ualcss a<hcnns<: agr=l to m "TitmJI.
508216-002
ED-S02
SOIL
May-19-15 00:00
May-26-15 13:10
May-26-15 13:30
mg/l<g RL
iJJ ND 0.00561
ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
ND 0.00567
l\'D 0.00567
ND 0.00567
ND 0.00567
\/ ro 0.00567
J 16.8 D 1.42
UJ ND 0.00567
:r 0.0295 0.00567
1F.L ND 0.0227
rJJ ND 0.00567
j" 0.0269 0.0113
J 0.142 0 .00567
IJJ ND 0.00567
ND 0.00567
]l,'l) 0 .00567
]l,'l) 0.00567
ND 0.00567
rm 0.00567
\V ND 0.00561
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 19 of 107
Date Receh·ed in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MA Y-15
508216-003
ED-S03
SOLL
May-19-15 00:00
May-26-1513:20
May-26-15 17:50
mgllcg RL
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0 00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.0281
ND 0.00703
ND 0.0141
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
ND 0.00703
Project Manafer : Kelsev Brooks -- -508216-004 508216-005 508216-006
ED-S04 ED-SOS ED-S06
SOlL SOIL SOIL
May-19-15 00:00 May-19-15 00:00 May-19-15 00:00
May-27-15 16:06 May-26-15 13:24 May-27-15 16:08
May-27-15 18:04 May-26-15 18:42 May-27-15 18:55
mg/kg RL mg/l<g RL mg/kg RL ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 rm 0.00621 ND 0.00581
ND 0.00568 l\'D 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 rm 0 .00621 ND 0.00582
ND 0.00568 ND 0 .00621 ND 0.00582
ND 0.00568 ND 0 .00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0 .00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.0227 ND 0.02411 ND 0.0233
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.0114 ND 0.0124 ND 0.0116
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
NU 0.00568 ]l,'l) 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 000582
ND 0.00568 ND 0.00621 ND 0.00582
0.0183 ~.00568 0.00621 0.00621 ND 0_00582
ND 0.00568 ND 0.00621 ND 0.00582
ND 0.00568 ND 0.00621 ND 0.00582
~.;,~ Final 1.000
Kelsey Brooks Project Manager
001094
Certificate of Analys( .Jummary 508216 Dynamac Corporation, Richardson, TX
(
Project Id: Project Name: A6KS
Contact: Lisa Graczyk
Pl"Oject Location:
- Lah/d: 5082 16-001
Analysis Requested Field Id: ED-SOI
Depth:
Matrix: SOIL
Sampled: May-19-15 00:00
VOAs by SW-846 8260B Extracted: May-27-1 5 16:04
SUB: TX10470421S Analyzed: May-27-15 16:47
Units/RL: mg/leg RL
I , 1,2-Trichloroethane ND 0.00632
I , I, 1-Trichloroelhane ND 0.00632
Trichlo1oethylcoe ND 0.00632
Trichloronuoromcthane ND 0.00632
1,2,3-Trichloropropane ND 0.00632
I ,2.4-Trimethylbeozeoe ND 0.00632
1,3.5-Trimethylbeoz.eoe ND 0.00632
Vinyl Chloride ND 0.00253
o-Xyleoe ND 0.00632
m,~Xylenes ND 0.0126
ThlS ....Ui11e11l rq><><t, and lhe C9lir< daia poc~ It repttKtl!S, M5 bcco IDldo for )VP eiclm., .. and coor.:knml me. Tbc: intci]Xd-tivm .-:I tcSUl.u 69ft:Si0.I datou,OOU. thiJ ~.J 1tpurfl lcprdc:nl d.c: bal juJ6ux:al uf XEP.."C'O ~ XENCO l.abonlorit'I wumcs no rcspoaSJbilll)' and maln no -ty to the md me oflhc d3la locr<:by -tcd. Our liabilioy is lamtcd to !he UOOlllll ion>ocod for Ibis"'°"' ord« 1111lcss otbctwisc agi«d IO io •mlmg.
- --508216-002
ED-S02
SOLL
~ia>·-19-1 5 00:00
May-2~15 13:10
May-2~15 13:30
mgilc:g RL
l.1 'f ND 0.00567
°11.'D 0.00567
°11.'D 0.00567
ND 0.00567
,v NU 0.00567
J 120D 5.70
.J l4.3 D 1.42
lf 1 ND 0.00227
I 48.0D 5.70
75.6 D 2.85
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Larin America - Odessa - Corpus Christi
Page 20 of 107
Date Received in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MAY-15 p
- ro"ect Mana~er: 508216-003 508216-004
ED-S03 ED·S04
SOLL SOIL
May-19-15 00:00 May-19-15 00:00
May-2~15 13:20 May-27-15 16:06
May-~15 17:50 May-27-15 18:04
mgllcg RL mg/leg RL
ND 000703 ND 0.00568
ND 0.00703 ND 0.00568
ND 0.00703 ND 0.00568
ND 0.00703 ND 0 00568
ND 0.00703 ND 0.00568
ND 0.00703 ND 0.00568
ND 0.00703 ND 0.00568
ND 0.00281 ND 0.00227
ND 0.00703 ND 0.00568
ND 0.0141 ND 0.0l 14
Final 1.000
e sey roo s Kl B k
508216-005
ED-SOS
SOIL
May-19-15 00:00
May-26-15 13:24
May-26-15 18:42
mg/leg RL °11.'D 0.00621
l\"D 0.00621
l\"D 0.00621
ND 0 .00621
ND 0.00621
ND 0.00621
ND 0.00621
ND OJI0248
ND 0.00621
ND 00124
Kelsey Brooks Project Manager
---508216--006
ED-S06
SOLL
May-19-15 00:00
May-27-15 16:08
May-27-15 18:55
mg/leg RL ND 0.00582
ND 0.00582
ND 0.00582
ND 0.00582
ND 0.00582
ND 0.00582
ND 0.00582
ND 0.00233
ND 0.00581
ND 0.01 16
001095
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
Flash Point (CC) SW-846 1010SUB: TX104704215
Mercury by EPA 7470ASUB: TX104704215
Mercury by SW 7471ASUB: TX104704215
May-27-15 14:30
May-27-15 20:53
May-26-15 12:15
May-27-15 19:54
May-26-15 13:00
May-27-15 19:55
May-26-15 13:45
May-27-15 19:57
Deg F
mg/kg
Units/RL:
Units/RL:
Units/RL:
Deg F
mg/L
Deg F
mg/L
Deg F
mg/L
May-27-15 15:00
Extracted:
Extracted:
Extracted:
May-27-15 12:10 May-27-15 12:10 May-27-15 12:10
Analysis Requested
508216-007Lab Id:
Field Id: ED-SO7
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
>180
0.0313
75.0
0.0212
Flash Point
Mercury
Mercury
>180
ND
75.0
0.00100
>180
0.00421
75.0
0.00100
>180
ND
75.0
0.0100
508216-008
ED-WL08
LIQUID
May-19-15 00:00
508216-009
ED-WLO9
LIQUID
May-19-15 00:00
508216-010
ED-WL10
LIQUID
May-19-15 00:00
RL
RL
RL
RL
RL
RL
RL
RL
Analyzed:
Analyzed:
Analyzed:
Page 21 of 107 Final 1.000
001096
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
Organochlorine Pesticides by EPA8081A
SUB: TX104704215May-26-15 16:09 May-27-15 11:24 May-27-15 11:42 May-27-15 12:00
ug/kg Units/RL: ug/L ug/L ug/L
May-22-15 12:45Extracted: May-26-15 16:18 May-26-15 16:21 May-26-15 16:24
Analysis Requested
508216-007Lab Id:
Field Id: ED-SO7
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 4.02 101 101
4,4-DDD 4,4-DDE 4,4-DDT Aldrin Alpha-BHC Alpha-Chlordane Beta-BHC Delta-BHC Dieldrin Endosulfan I Endosulfan II Endosulfan Sulfate Endrin Endrin Aldehyde Endrin Ketone Gamma-BHC (Lindane) Gamma-Chlordane Heptachlor Heptachlor Epoxide Methoxychlor Chlordane Toxaphene
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 25.0 25.0
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 25.0 25.0
NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND
1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 1.00 25.0 25.0
508216-008
ED-WL08
LIQUID
May-19-15 00:00
508216-009
ED-WLO9
LIQUID
May-19-15 00:00
508216-010
ED-WL10
LIQUID
May-19-15 00:00
RL RL RL RL
Analyzed:
Page 22 of 107 Final 1.000
001097
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
PCBs by EPA 8082SUB: TX104704215
Percent Moisture
May-28-15 13:22
May-22-15 17:30
May-28-15 14:30 May-28-15 14:46 May-28-15 15:03
ug/kg
%
Units/RL:
Units/RL:
ug/L
ug/L
ug/L
May-22-15 12:45Extracted:
Extracted:
May-26-15 16:18 May-26-15 16:21 May-26-15 16:24
Analysis Requested
508216-007Lab Id:
Field Id: ED-SO7
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
NDNDNDNDNDNDND
17.3
101 101 101 101 101 101 101
1.00
PCB-1016 PCB-1221 PCB-1232 PCB-1242 PCB-1248 PCB-1254 PCB-1260
Percent Moisture
NDNDNDNDNDNDND
2.50 2.50 2.50 2.50 2.50 2.50 2.50
NDNDNDNDNDNDND
2.50 2.50 2.50 2.50 2.50 2.50 2.50
NDNDNDNDNDNDND
2.50 2.50 2.50 2.50 2.50 2.50 2.50
508216-008
ED-WL08
LIQUID
May-19-15 00:00
508216-009
ED-WLO9
LIQUID
May-19-15 00:00
508216-010
ED-WL10
LIQUID
May-19-15 00:00
RL
RL
RL RL RL
Analyzed:
Analyzed:
Page 23 of 107 Final 1.000
001098
Project Id:
Contact: Lisa Graczyk
Project Location:
A nalysis Requested
SVOAs by EPA 8270C SUB: TX10470421S
1,2,4-Trichlorobenzene
1,2-Dichlorobcnzene
l,3-Dichlorobcozene
1,4-Dichlorobcnzenc
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dichlorophcnol
2,4-Dimcthylphcnol
2,4-Dinitrophcnol
2,4-Dinitrotoluene
2,6-Dinitrotolucne
2-Cbloronaphtbalene
2-Chlorophcnol
2-Methylnaphthalene
2-methylphcnol
2-Nitroaniline
2-Nitrophcnol
3&4-Metbylphenol
3,3-Dichlorobcnzidine
3-Nitroaniline
4,6-dinitro-2-methyl phenol
4-Bromophenyl-phenylether
<k:hloro-3-methylpbenol
4-Chloroaniline
4-Chlorophenyl Phenyl Ether
Certificate of Analy[ J ummary 508216
Lab Id:
Field Id:
Depth:
Matrix:
Sampled:
Extracted:
Analyzed:
Units/RL:
Dynamac Corporation, Richardson, TX Project Name: A6KS
Date Received in Lab:
-- -- ---508216-007 508216-008
ED-S07 ED-WL08
SOIL LIQUID
May-19-15 00:00 May-19-15 00:00
May-26- 15 17:03 May-26-15 15:54
May-27-15 18:06 May-27-15 18:31
mg/kg RL mg/L RL
ND .1.00 L:J1'TI 0.125
ND 1.00 ND 0.12S
ND 1.00 ND 0.12S
ND 1.00 ' / ND 0.125
ND 1.00 ND O.llS
ND 1.00 ND O. l lS
ND 1.00 ND 0. 125
ND 1.00 KD O.llS
ND 2.01 ND O.lSO
ND 1.00 # I~ ND 0.125
ND 1.00 /)J _ND 0.125
ND 1.00 V-' ND 0.llS
ND 1.00 _ND 0 .125
ND 1.00 ll1 ND 0 .125
ND 1.00 ND 0 .125
ND 2.01 lf1 ND 0 .250
ND 1.00 ND O. llS
ND 1.00 0;151 O. llS
ND 2.01 UJ ND 0.2SO
ND 2.01 ND 0 .250
ND 2.01 ND 0 .250
ND 1.00 UJ ND 0 .12S
ND 1.00 _ND 0 .12S
ND 2.01 VJ ,ND 0.250
ND 1.00 /JJ ND 0 .125
---508216-009
ED-WL09
LIQUID
May-19-1 5 00:00
May-26-15 15:57
May-27-15 18:57
mg/L RL
1fJ ND 0.250
ND 0..2SO
ND 0..250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0..250
ND 0.500
ND 0250
ND 0.250
ND 0.250
ND 0.2SO
ND 0 .2.SO
ND 0.2SO
ND 0.500
ND 0.250
ND 0.250
ND 0.500
ND o.soo ND o.soo ND 0.250
ND 0.250
. ND 0.500
~7 ND 0.250
ro1ect 1 anas?.er:
Report Date:
p M 508216-010
ED-WLIO
LIQUID
May-19-15 00:00
May-26-15 16:00
May-27-1 5 19:22
mg/L RL ND O.lSO
ND 0.250
ND 0.250
ND 0250
ND 0.250
ND 0.250
ND 0.250
ND 0250
ND 0.500
ND 0.250
ND 0.2SO
ND 0.2SO
ND 0.250
ND 0.2SO
ND 0.2SO
ND 0.500
ND O.lSO
ND 0.250
ND o.soo ND o.soo ND 0.500
ND O.lSO
ND 0.250
ND 0.500
ND 0.250
Wed May-'20-15 05 :00 pm
29-MAY- 15
C SC)' roo K I B ks
(
is anaJytical r<poct, ond die eo1ite dlla pocbge • r<prcocmlS. has bom mode for>""' ucJusn-e ud 0011fidcnli3l UK.
--ioM ond ...Wrs cxp«n<d ~· diis amlytical ._,. ropr<SCDI Ille: bcot jadgma>t of XnlCO l..abonloncs. ·co Ubon:orics ummcs no ._,;biliiy and mm..., wonaory,. th< end - o>flhc dara bcr<by ~-boMily "limned ID the-m"°iccd a Ibis wotkonler 8'llcss otkrwisc ..,...i ID• wribng.
1li 1lic XEN Ow I,, ~~~ Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 24 of 107 Final 1.000
Kelsey Brooks Project Manager
-
001099
Certificate of Analys( Jummary 508216 (
Project Id:
Dynamac Corporation, Richardson, TX Project Name: A6KS
Contact: Lisa Graczyk
Project Location:
- - - - -~ --- -Lab Id: 508216-007
Analysis Requested Field Id: ED-S07
Dept It:
Matrix: SOIL
Sampled: May- l 9- l 5 00:00
SVOAs by EPA 8270C Extracted: May-26-15 17:03
SUB: TX10470421S Analyud: May-27-15 18:06
Units/RL: mg/leg RL 4-Nitroaniline ND 2.01
4-Nilrnphcool ND 2.01
Acenapbthcnc ND LOO
Acenaphlhylenc ND LOO
Aniline (Phenylamine, Aminobenzene) ND 2.01
Anlhracenc ND LOO
Benzo(a)anlhracenc ND 1.00
Benzo(a)pyrcne ND 1.00
Bcnzo(b )Ouoranthenc ND 1.00
Bcnzo(g.h ,i)perylene ND 1.00
Bcnzo(lc)Ouoranthcnc ND 1.00
Bcnzoic Acid ND 6.03
Bcnzyl Butyl Phthalate ND 1.00
bis(2<hloroethoxy) methane ND 1.00
bis(2<hloroethyl) ether ND LOO
bis(2-chloroisopropyl) ether ND LOO
bis(2-cthylhexyl) phlhalatc ND LOO
Chrysenc ND LOO
D ibenz( a,h )Anthraccne ND LOO
Dibenz.ofuran ND 1.00
Diethyl Phthalate ND LOO
Dimethyl Pblhalate ND 1.00
di-a-Butyl Phlhalate ND 1.00
di-n-Octyi Pblhalate ND 1.00
Fluoranthenc ND 1.00 ·
- ..J}1'Cal report. and dJc ftll~ cbta pocbi-c ii r<pr<S<DIS. bas been mode Ii:><)- eWmn'< and <X>Dlidtnbal US< This The XES Our
U>l<lp«UIN>DS and ...W" dl>f""'1 tb<.....,..,..t doD -Jy<K..I RpUCI rcprncn1 11>< bcst jadcmcat of XENCO l..obonlories. ·co l.aboral<lrics a5SWD<5 no mponstb~tty ll!ld ....m no"'~'>'"' lhoo end use of die dooa hereby -ed. lllbillty ii limited lo the. amoanJ in\Viccd fOr ch.1t •'Ork Order anlcu otbcrwisc .agreed to 1a '4Ti1ing.
---508216-008
ED-Wl.08
LIQUID
May-19-1 5 00:00
May-26-15 15:54
May-27-15 18:31
mg/I.. RL
uJ ND 0.250
)\1) 0.2SO
IJJ ND 0.125
ND 0.125
ND 0.250
ND 0.125
ND 0.125
ND 0.1 25
ND 0.125
ND 0.125
ND 0.125
ND 0.150
ND 0.125
ND 0.125
ND 0.125
ND 0.125
ND 0.125
ND 0.125
KD 0.125
ND 0.125
ND 0.125
ND 0.125
ND 0.125
i ' ND 0.125
t ND 0 125
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 25of107
Date Receind in Lab: Wed May-20-15 05:00 pm
Report Date: 29-~{A Y-15
---508216-009
ED-WL09
LIQUID
May-19-15 00:00
May-26-15 15:57
May-27-15 18:57
mlllL RL
1JJ ND 0500
ND o.soo ND 0.250
ND 0.250
ND 0.500
ND 0.250
ND 0.250
ND 0.250
ND 0.150
ND 0250
\/ ND 0.250
l.96 I.SO
ir1 ND 0.250
ND 0.250
I ND 0.250
~ ND 0.250
) 0.258 0.250
1/J ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
\ / ND 0.250
"'
P. M Kl B k ro1ect anaeer: e sey roo s ----508216-010
ED-WLIO
LIQUID
May-19-15 00:00
May-26-15 16:00
May-27-15 19:22
mg/I.. RL
ND 0.500
ND 0.500
ND 0.250
ND 0.250
ND O.SOO
ND 0.250
ND 0.250
ND 0.250
ND 0.150
~ 0.250
ND 0.250
ND 1.50
ND 0.250
ND 0.250
ND 0.250
ND 0.250
9-38 D 1.25
~ 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
4~~ Final 1.000
Kelsey Brooks Project Manager
001100
Certificate of Analysi. .. ., ummary 508216 Dynamac Corporation, Richardson, TX
Project Id:
Contact: Lisa Graczyk Project Location:
Project Name: A6KS Date Receh·ed in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MA Y -15
-- - --- - ~ Pro·ect Man~er· Kelsey Brooks --- -
lab Id: 508216-007 508216--008
Analysis Requested Field Id: ED-S07 ED-WL08
Depth:
Matrix: SOIL LIQUID
Sampled: May-19-15 00:00 May-19-15 00:00
SVOAs by EPA 8270C Extracted: May-26-15 17:03 May-26-15 15:54
SUB: TX10470421S Anal)'ud: May-27-15 18:06 May-27-15 18:31
Units/RL: mg/kg RL mg/L RL
Fluon:nc ND 1.00 ID I'm 0.125
Hc:i<achlorobenzene ND 1.00 ND 0.125
Heicachlorobutadicne ND 1.00 ND 0.125
Hcicach.lorocyclopenladicnc ND 1.00 ND 0.125
Hcuchloroethanc ND 1.00 ND 0.125
lndeno( 1.2,3-c,d)Pyrcne ND 1.00 NU 0.125
lsophoronc ND 1.00 ND 0.125
Naphthalene ND 1.00 ND 0.125
Nitrobenzcne ]\'I) 1.00 ND 0.125
N-Nitrosodi-n-Propylamine ND 1.00 1'1> 0.125
N-Nilrosodiphcnylaminc ND 1.00 \/ ]\'I) 0.125
Pcntachlorophcnol ND 2.01 ND 0.250
Phcnanthrene ND 1.00 UJ ND 0.125
Phenol ND 2.01 )l.534 0.250
Pyn:ne ND 1.00 lr1 ND 0 125
Pyridine NO 2.01 TJ"1 NO 0.250
TPH by TexaslOOS Extracted: May-21-15 14:00 May-21-15 14:00
Anal)'l.t'd: May-22-15 01:00 May-22-15 00:33
UnilSIRL: mg/kg RL mglL RL
C6-C 12 Gasoline Range Hydrocarbons ND 30.I 46.3 15.0
C l2-C28 Diesel Range Hydrocarbons 2760 30.1 1150 15.0
C28-C35 Oil Range Hydrocarbons I 186 30.1 NO 15.0
Total TPH JOOS 2950 30. I 1200 15.0
This aal)tl<al rq>OCt, and me~ dm ~ • ~ IMts b<cn mode for your culus"< ud con6dcDtlal o« 11w: _....._ ..! ooult. ~ ~ dm -1)u.I rq>0<1 rq>t<OCOI the bcstJwlpncal of XENCO l..abonroncs.
XB;CO ~ _, ""._sibilny and makes oo wvnn1y to me end""" of me dm hereby prcs<nlOd. Our liatnbry K limited to the amoont in,.'Oiocd fur ch.ii won: onlc:r unlc:.ss othmrisc: agrcc:d ro in wrinft,g.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 26 of 107
508216-009
ED-WL09
LIQUID
May-19-15 00:00
May-26-15 15:57
May-27-15 18:57
mgfL RL
11-f ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0 250
ND 0.250
ND 0.500
ND 0.1.50
ND 0.500
NO 0.250
. JND 0.500
M:i(-21-15 14:00
May-22-15 00:56
mg/L RL
27.7 15.0
775 15.0
NO 15.0
803 15.0
508216-010
ED-WLIO
LIQUID
May-19-15 00:00
May-26-15 16:00
May-27-15 19:22
mgfL RL ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.250
ND 0.500
ND 0.250
l\'D 0.500
ND 0.250
ND 0.500
May-21-15 14:00
May-22-15 01:17
mg/L RL 19.0 15.0
1160 15.0
ND 15.0
1180 15.0
Final 1.000
Kelsey Brooks Project Manager
(
-
001101
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
Total Metals by EPA 6010BSUB: TX104704215 May-28-15 02:04 May-28-15 17:21 May-28-15 17:28 May-28-15 17:35
mg/kg Units/RL: mg/L mg/L mg/L
May-27-15 13:30Extracted: May-28-15 09:30 May-28-15 09:30 May-28-15 09:30
Analysis Requested
508216-007Lab Id:
Field Id: ED-SO7
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
4680 ND
3.52 358 NDND
21400
11.8 2.36 7.94
5360 42.4
1640 71.0 12.6
1310 NDND
1120 NDND
156
22.4 2.24 2.24 1.12 0.448
1.12 22.4 1.12 1.12 2.24 22.4 2.24 44.8 2.24 1.12 56.0 3.36 3.36 56.0 2.24 10.1 3.36
Aluminum Antimony Arsenic Barium Beryllium Cadmium Calcium Chromium Cobalt Copper Iron Lead Magnesium Manganese Nickel Potassium Selenium Silver Sodium Thallium Vanadium Zinc
NDNDNDNDNDND
23.0 ND
0.113
NDNDND
4.49 0.302
13.4 211 NDND
4560 NDND
1.06
2.00 0.200
0.200
0.100
0.0400
0.100
2.00 0.100
0.100
0.200
2.00 0.150
4.00 0.200
0.100
5.00 0.300
0.300
5.00 0.200
0.900
0.300
16.4 ND
0.237
1.79 NDND
373 0.567
0.184
3.90 192
0.704
73.9 1.63 3.65 306 NDND
4370 NDND
50.9
2.00 0.200
0.200
0.100
0.0400
0.100
2.00 0.100
0.100
0.200
2.00 0.150
4.00 0.200
0.100
5.00 0.300
0.300
5.00 0.200
0.900
0.300
66.5 ND
0.759
1.22 NDND
2020 0.678
230 ND
197 2.25 91.2 5.12 17.2
3380 NDND
5540 NDND
71.0
5.00 0.500
0.500
0.250
0.100
0.250
5.00 0.250
0.250
0.500
5.00 0.375
10.0 0.500
0.250
12.5 0.750
0.750
12.5 0.500
2.25 0.750
508216-008
ED-WL08
LIQUID
May-19-15 00:00
508216-009
ED-WLO9
LIQUID
May-19-15 00:00
508216-010
ED-WL10
LIQUID
May-19-15 00:00
RL RL RL RL
Analyzed:
Page 27 of 107 Final 1.000
001102
Project Id:
Dynamac Corporation, Richardson, TX
Lisa GraczykContact:Project Location:
Wed May-20-15 05:00 pm 29-MAY-15Kelsey Brooks
Date Received in Lab:Report Date:
Project Manager:
Project Name: A6KS
This analytical report, and the entire data package it represents, has been made for your exclusive and confidential use.The interpretations and results expressed throughout this analytical report represent the best judgment of XENCO Laboratories.XENCO Laboratories assumes no responsibility and makes no warranty to the end use of the data hereby presented.Our liability is limited to the amount invoiced for this work order unless otherwise agreed to in writing.
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi________________________________
Project ManagerKelsey Brooks
Certificate of Analysis Summary 508216
Total and Amenable Cyanide by SW-846 9012B
SUB: TX104704215May-28-15 14:14 May-28-15 13:46 May-28-15 13:48 May-28-15 13:49
mg/kg Units/RL: mg/L mg/L mg/L
May-27-15 17:48Extracted: May-27-15 17:48 May-27-15 17:48 May-27-15 17:48
Analysis Requested
508216-007Lab Id:
Field Id: ED-SO7
SOIL
May-19-15 00:00
Depth:
Matrix:
Sampled:
ND 0.588 Cyanide, Total 0.0524 0.00500 0.0395 0.0250 0.0665 0.0250
508216-008
ED-WL08
LIQUID
May-19-15 00:00
508216-009
ED-WLO9
LIQUID
May-19-15 00:00
508216-010
ED-WL10
LIQUID
May-19-15 00:00
RL RL RL RL
Analyzed:
Page 28 of 107 Final 1.000
001103
Project Jd:
Contact: Lisa Graczyk
Project LoCJ1tlon:
- -
A11alysis Requested
VOAs by SW-846 8260B SUB: TX104704215
Benzene
Bromobcnzenc
Bromocbloromethaoe
Bromodicl1loromethane
Bromofonn
Methyl bromide
ten-Butyl benzene
Scc-Butylbenzcne
n-Butylbcn.tenc
Carbon Tetrachloride
Chlorobenzcnc
Cbloroctbane
Chloroform
Methyl Chloride
2-Chlorotoluene
4-Chlorotoluene
p-Cymcnc (p-lsopropyltoluenc)
1,2-Dibromo-3-Chloropropanc
Dibromochloromcthanc
1,2-Dibromocthane
Methylene bromide
1.2-Dichlorobenzene
1,3-Dichlorobcnzene
1,4-Diehlorobcnzcne
Dichlorodifluoromcthanc
.~
Certificate ot Analys ~ _,ummary 508216 Dynamac Corporation, Richardson, TX
Lab Id:
Field Id:
Depth:
Matrix:
S amp/Ld:
Extra~ted:
Analyzed:
Uni/s/RL:
Project Name: A6KS Date Receh·ed in Lab:
Report Date: p . M ana er: --- -- --- -- -~
ro1ect 508216-007 508216·008 508216-009 508216-010
ED-S07 ED-WLOS ED·WL09 ED-WLIO
SOIL LIQUID LIQUID LIQUID
May-19-15 00:00 May-19-15 00:00 May-19-15 00:00 May-19-15 00:00
May-27-15 14:42 May-26-15 17:22 May-26-15 17:22 May-28-15 14:00
May-27-15 14:59 May-26-15 18:00 May-26-15 18:26 May-28-15 14:32
mg/kg RL mg/L RL mg/L RL mg/kg RL ND 0.00604 ND o.osoo ND 0.12S ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND 0.0500 ND 0.125 ND 0.500
NO 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND o.soo ND 0.00604 ND o.osoo ND 0.125 ND o.soo
ilT ND 0.00604 ND o.osoo ND 0.125 ND 0.500 ..... ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.0121 ND 0 100 ND 0.2SO ND 1.00
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.0121 ND 0.100 ND 0.2SO ND 1.00 ND 0.00604 ND o.osoo ND 0. 125 ND o.soo ND 0.00604 ND 0.0500 ND 0.125 ND 0.500
ND 0.00604 ND 0.0500 ND 0.125 ND o.soo ND 0.00604 ND 0.0500 ND 0.125 ND 0.500
ND 0.00604 ND 00500 ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND 0.0500 ND 0. 125 ND 0.500
ND 0.00604 ND 0.0500 ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND 0.500
ND 0.00604 ND o.osoo ND 0.125 ND o.soo ND 0.00604 ND o.osoo ND 0.125 ND 0.500
Wed May-20-15 05:00 pm
29-MAY-15
c scy roo s --KI B k
(
-
is analytical report. and chc cn1in: data packlae it represents. Ms b«:n made for your exclusive 1od confidential use. iokrprctationi end rc~ults cxprc«cd throu.&hout thi1 analytical report rcprcseot the best judjJncnt of XENCO LaboratQrict. CO Laboratoric1 usumes no tt1pooS1bility and makes no wamnty to the end - of the dal• hen:by pmcnted. Jiabiliry iJ hm..IC!d to chc amowu in'f'Oacc:d for this "'"Ork order unless othc1wi.Jc •J"'!Cd 1o U) wnhn1
Th The XEN Ow / ~-1~ Houston - Dallas - San Antonio - Atlanlll - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 29 of 107 Final 1.000
Kelsey Brooks Project Manager
001104
Project Id:
Contact: Lisa Graczyk
Project Location:
-Analysis Requested
VOAs by SW-846 8260B SUB: TX104704215
1,2-Dichlorocthanc
1,1-Dicbloroethanc
ttans-1,2-dichlorocthylene
cis-1,2-Dichloroethylene
I, 1-Dichloroclhcne
2,2-Dichloropropane
1,3-Dichloropropane
1,2-Dichloropropanc
trans-1 ,3-dichloropropcnc
I, 1-Dichloropropene
cis-1,3-Dichloropropene
Ethyl benzene
Hexachlorobul.adicnc
lsopropylbenzene
Methylene Chloride
MTBE
Naphthalene
n-Propylbcnzcnc
StyTcne
1, I, 1,2-Tetrachloroetbaac
l, I ,2,2-Tetracbloroetbaae
Tetracblorocthylcnc
Toluene
1,2,3-Tricblorobenzene
1,2,4-Trichlorobcnzeae
Certificate of AnalysC .Jummary 508216 Dyoamac Corporation, Richardson, TX
Project Name: A6KS
--- ·- --- - ·-Lab Id: 508216-007 508216-008
Field Id: ED-SO? ED-WL08
Depth:
,Uatrix: SOIL LIQUID
Sampled: May-19-15 00:00 May-19-15 OO·OO
Extracted: May-27-1 5 14:42 May-26-15 17:22
Analyzed: May-27-IS 14:59 May-26-15 18:00
Units/RL: mg/kg RL mg/L RL ND 0.00604 ND o.osoo ND 0.00604 ND o.osoo ND 0.00604 ND 0.0500
ND 0.00604 ND 0.0500
ND 0.00604 ND 0.0500
ND 0.00604 ND 0.0500
ND 0.00604 ND o.osoo ND 0.00604 ND o.osoo ND 0.00604 ND 0.0500
ND 0.00604 ND 0.0500
ND 0.00604 ND 0.0500
ND 0.00604 ND 00500
UJ ND 0.00604 ND 0.0500
IJj' ND 0.00604 ND 0.0500
ND 0.0242 ND 0.0500
ND 0.00604 ND 0.0500
tr T ND 0.0121 ND 0.100 - ND 000604 0.0866 o.osoo
ND 0.00604 ND 0.0500
ND 0.00604 ND o.osoo ND 0.00604 ND 0.0500
ND 0.00604 ND 0.0500
0.0348 .J 0.00604 0.311 o.osoo H IND 0.00604 ND o.osoo IJ-\"'ND 0.00604 ND 0.0500
Date Received in Lab: Wed May-20-15 .05:00 pm
Report Date: 29-MA Y-15
-- --__: __ ---Project Manager· Kelsey Brooks
-508216-009 508216-010
ED-WL09 ED-WLIO
LIQUID LIQUID
May-19-15 00:00 May-19-15 00:00
May-26-15 17:22 May-2R-IS 14:00
May-26- 1 S 18:26 May-28-IS 14:32
mg.IL RL mg/kg RL ND 0.125 ND 0.500
ND 0.1 25 ND 0.500
ND 0.125 ND o.soo ND 0.125 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND o.soo ND 0.1 25 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND 0.500
0.161 0.1 25 ND 0.500
ND 0.1 25 ND 0.500
ND 0.1 25 ND 0.500
ND 0.125 ND 2.00
ND 0.125 ND 0.500 0.2S4 0.250 ND 1.00 0.251 0.125 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND 0.500
ND 0.125 ND 0.500 0.430 0.125 3.04 0.500
ND 0.125 ND o.soo ND 0.125 ND 0.500
(
Th The XEN Our
is analytical ttport. and the entitt data p1ck11c it rcprescn1s, has been made ror your ex.elusive o.nd confidential use. interprcta1iooJ and ttsults c-xpres'IC<I throuahout thii analytical report rquucnt tbt bcstjudpne:nt orXENCO Labontturict 'CO Laboratori<t usumcs no rcspoo11bihiy and makes no warranl)I to the end me of the data hereby pteS<nted. liability i• lunltcd to the amount invviccd for !hit woric otdcr Wilm olhawisc: ag«d to 10 wntona ~1~
Houston - Dallas - San Antonio - Atlanta - Tampa - Boca Raton - Latin America - Odessa - Corpus Christi
Page 30 of 107 Final 1.000
Kelsey Brooks Project Manager
001105
Certificate of AnalysL ...;ummary 508216 Dynamac Corporation, Richardson, TX
Project Id: Project Name: A6KS
Contact: Lisa Graczyk
Project Location:
---
A11alysis Requested
VOAs by SW-846 82608 SUB: TX10470421S
I, 1,2-Tricbloroctbanc
1, I, I· Trichloroethane
Trichloroethylcoc
Trichloronuoromcthanc
1,2,3· Trichloroprop11ne
1.2,4-Trimelhylbenzcnc
1.3,5-Trimetbylbenunc
Vinyl Chloride
o-Xylcnc
m,p-Xylenes
---Lab Id:
Field Id:
Depth:
Matrix:
Sampled:
Extracted:
Analyt,ed:
Units/RL:
--- -508216-007
ED-S07
SOIL
May-19-15 00:00
May-27-15 14:42
May-27-15 14:59
mg/kg RL ND 0.00604
ND 000604
ND 0 00604
ND 0.00604
ND 0.00604
ND 0.00604
ND 0.00604
ND 0.00242
ND 0.00604
ND 0.0121
This analytical rcport. and lhe entire da11 pat.Oge it represents. has been made for your cxcluS1\'C and confiden1ial uSt. The inccrprc:ta1ioos and rcsultJ expressed throughout thi• anaJytica1 report rcprctcn! the bcs-tjudl"'ICnt ofX'ENCO Labont.tories. XENCO Laborat.>rin assumes no rnpocsibihry and nW<u no "'""""'Y to the end we oflhc dora h<r<by pr<SCntcd. Our li:lbihry is limited to the amou.n1 tn\.'Oiccd fur lh.1'1 •'Oft order unlcff olhmiruc 1grecd &om "'T1hng.
- --5082 16-008
ED-Wl-08
LIQUID
Muy-19-15 00:00
May-26-15 17:22
May-26-15 18:00
mg/L RL ND 0.0500
ND 0.0500
ND o.osoo ND 0.0500
ND 0.0500
0.455 0.0500
0.144 0.0500
ND 0.0200
0.0557 0.0500
0.117 0.100
Houston. Dallas - San Anlonio - Atlanta· Tampa • Boca Raton - Latin America - Odessa· Corpus Christi
Page 31of107
Date Received in Lab: Wed May-20-15 05:00 pm
Report Date: 29-MA Y-15
-- -5082 16-009
ED-Wl09
LIQUID
May-19-15 00:00
May-26-15 17:22
May-26-15 18:26
mg/L RL ND 0.125
ND 0.125
ND 0.125
ND 0. 125
ND 0. 125
1.48 0.125
0.452 0. 125
ND 0.0500
0.295 0. 125
0.658 0.250
Project Mana~: Kelsey Brooks -- ---508216-010
ED-WLIO
LIQUID
May-19-15 00:00
May-28-15 14:00
May-28-15 14:32
mg/kg RL ND 0.500
ND o.soo ND o.soo ND 0.500
ND o.soo 2.03 o.soo 0.552 0.500
ND 0.200
0.664 o.soo ND 1.00
Final 1.000
Kelsey Brooks Project Manager
001106
Houston - Dallas - San Antonio - Atlanta - Midland/Odessa - Tampa/Lakeland - Phoenix - Latin America
4143 Greenbriar Dr, Stafford, TX 774779701 Harry Hines Blvd , Dallas, TX 75220 5332 Blackberry Drive, San Antonio TX 78238 2505 North Falkenburg Rd, Tampa, FL 3361912600 West I-20 East, Odessa, TX 797656017 Financial Drive, Norcross, GA 300713725 E. Atlanta Ave, Phoenix, AZ 85040
Phone Fax(281) 240-4200 (281) 240-4280(214) 902 0300 (214) 351-9139(210) 509-3334 (210) 509-3335(813) 620-2000 (813) 620-2033(432) 563-1800 (432) 563-1713(770) 449-8800 (770) 449-5477(602) 437-0330
Recipient of the Prestigious Small Business Administration Award of Excellence in 1994.Certified and approved by numerous States and Agencies.
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Flagging Criteria
X In our quality control review of the data a QC deficiency was observed and flagged as noted. MS/MSD recoveries were found to be outside of the laboratory control limits due to possible matrix /chemical interference, or a concentration of target analyte high enough to affect the recovery of the spike concentration. This condition could also affect the relative percent difference in the MS/MSD.
B A target analyte or common laboratory contaminant was identified in the method blank. Its presence indicates possible field or laboratory contamination.
D The sample(s) were diluted due to targets detected over the highest point of the calibration curve, or due to matrix interference. Dilution factors are included in the final results. The result is from a diluted sample.
E The data exceeds the upper calibration limit; therefore, the concentration is reported as estimated.
F RPD exceeded lab control limits.
J The target analyte was positively identified below the quantitation limit and above the detection limit.
U Analyte was not detected.
L The LCS data for this analytical batch was reported below the laboratory control limits for this analyte. The department supervisor and QA Director reviewed data. The samples were either reanalyzed or flagged as estimated concentrations.
H The LCS data for this analytical batch was reported above the laboratory control limits. Supporting QC Data were reviewed by the Department Supervisor and QA Director. Data were determined to be valid for reporting.
K Sample analyzed outside of recommended hold time.
JN A combination of the "N" and the "J" qualifier. The analysis indicates that the analyte is "tentatively identified" and the associated numerical value may not be consistent with the amount actually present in the environmental sample.
** Surrogate recovered outside laboratory control limit.
BRL Below Reporting Limit.
RL Reporting Limit
MDL Method Detection Limit SDL Sample Detection Limit LOD Limit of Detection
PQL Practical Quantitation Limit MQL Method Quantitation Limit LOQ Limit of Quantitation
DL Method Detection Limit
NC Non-Calculable
+ NELAC certification not offered for this compound. * (Next to analyte name or method description) = Outside XENCO's scope of NELAC accreditation
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