ebsd(electronbackscattereddiffraction
TRANSCRIPT
Layout 1Equipment & Consumables
Left: EBSD pattern for cartridge brass, Cu - 30% Zn - PQI: 221 ± 8.6. Right:Microstructure of wrought Cu - 30% Zn etched with equal parts hydrogen peroxide (3%) and ammonium hydroxide.
TABLE OF CONTENTS EBSD PreparationMethod byMaterial
Equipment ........................................................................................................................................................................................................................................................Page 3
1 Cutting 10-2415-400 Delta® AbrasiMet®W/Hood Switch
10-2165-400 Delta® AbrasiMet® Recirc System
10-2170 Sliding Vise, AbrasiMet®, Left Hand
10-2171 Sliding Vise, AbrasiMet®, Right Hand
2 Mounting 20-1415 SimpliMet® 1000 Mounting Press
20-2402 Mold Assembly 14″ ID, 60mmOD
3 Semi-Automated 49-1780 EcoMet® 4000 Grinder/Polisher
Grinding/Polishing 60-1970 AutoMet® 2000 Power Head
49-1777 All Platens (4 needed)
60-5282 Specimen Holder, Barrel, 14″ x 10
60-2413 Loading Plate, 8″ and 12″ 60-9000 Drive Adapter
4 Final Polish 67-1635-250 VibroMet® 2 Vibratory Polisher
67-1527 Specimen Holder, 14″,VibroMet® (2 sets needed)
67-1529 SpecimenWeights,VibroMet® (2 sets needed)
5 Microscope to 0760-0100 ViewMet™ Inverted Lab Microscope
Inspect Quality of
Preparation
3
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-120-100
10″ (254mm) 30-5125-120-100
12″ (305mm) 15-5112-120-100
8″ (203mm) 30-5118-180-100
10″ (254mm) 30-5125-180-100
12″ (305mm) 15-5112-120-100
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-240-100
12″ (305mm) 30-5121-240-100
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-320-100
12″ (305mm) 30-5112-320-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
8″ (203mm) 40-7518
10″ (254mm) 40-7520
12″ (305mm) 40-7522
8″ (203mm) 40-7518
10″ (254mm) 40-7520
12″ (305mm) 40-7522
8″ (203mm) 40-8318
10″ (254mm) 40-8320
12″ (305mm) 40-8322
1 CarbiMet® Discs
(PSA) Grinding Paper
CarbiMet® Abrasive Discs
STEEL PREPARATIONMETHODS FOR EBSD & NANO INDENTATION WITH CONSUMABLE PART NUMBERS
VibroMet® 2
4
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
ChemoMet® I)
Holder Only
120-150 Contra
120-150 Contra
120-150 Contra
120-150 Contra
ALUMINUM 5 STEP PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
40-6370-006
5
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
ChemoMet® I)
Holder Only
120-150 Contra
120-150 Contra
120-150 Contra
ALUMINUM 4 STEP PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
VibroMet® 2
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME
Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/ Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
ChemoMet® I)
Holder Only
100-150 Contra
100-150 Contra
100-150 Contra
80-120 Contra
10
7
5
3
60
COBALT & IT’S ALLOYS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
40-6370-006
7
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
Holder Only
COPPER & BRASS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
40-6370-006
8
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-120-100
10″ (254mm) 30-5125-3-120-100
12″ (305mm) 30-5112-120-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
IRON ALLOYS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
63-6377-006
9
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
Holder Only
120-150 Contra
120-150 Contra
120-150 Contra
NI BASED ALLOYS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
63-6377-006
10
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-3-320-100
12″ (305mm) 30-5112-320-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
40-6370-006
11
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-3-320-100
12″ (305mm) 30-5112-320-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
MasterMet® Colloidal Silica
40-6370-006
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME
Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/ Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-320-100
12″ (305mm) 15-5112-320-100
8″ (203mm) 30-5118-400-100
10″ (254mm) 30-5125-400-100
12″ (305mm) 15-5112-400-100
8″ (203mm) 30-5118-600-100
10″ (254mm) 30-5125-600-100
12″ (305mm) 30-5121-600-100
VibroMet® 2
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME
Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/ Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-240-100
12″ (305mm) 15-5112-240-100
VibroMet® 2
BUEHLER LTD. –Worldwide Headquarters 41Waukegan Road • P.O. Box 1 • Lake Bluff, Illinois 60044-1699 USA Tel: 847/295-6500 • Fax: 847/295-7979 • Sales: 1/800/BUEHLER • 1/800/283-4537 Web Site: http://www.buehler.com • Email: [email protected]
BUEHLER GMBH - European andMESA Headquarters In der Steele 2 • 40599 Düsseldorf • Postfach 16 03 55 • 40566 Düsseldorf Telefon: (49) 211 974100 • Telefax: (49) 211 9741079 Web Site: http://www.buehler-met.de • Email: [email protected]
BUEHLER FRANCE Téléphone: 0800 89 73 71 • Télécopie: 0800 88 05 27 Web Site: http://www.buehler.fr • Email: [email protected]
BUEHLER UNITED KINGDOM Telephone: 0800 707 6273 • Fax: 0800 707 6274 Web Site: http://www.buehler.co.uk • Email: [email protected]
BUEHLER CANADA 10 Carlow Court, Unit #2 •Whitby,Ontario L1N 9T7 Telephone: (905) 430-4684 • Fax: (905) 430-4647 Sales Telephone: 1-800-268-3593 Email: [email protected]
Left: EBSD pattern for cartridge brass, Cu - 30% Zn - PQI: 221 ± 8.6. Right:Microstructure of wrought Cu - 30% Zn etched with equal parts hydrogen peroxide (3%) and ammonium hydroxide.
TABLE OF CONTENTS EBSD PreparationMethod byMaterial
Equipment ........................................................................................................................................................................................................................................................Page 3
1 Cutting 10-2415-400 Delta® AbrasiMet®W/Hood Switch
10-2165-400 Delta® AbrasiMet® Recirc System
10-2170 Sliding Vise, AbrasiMet®, Left Hand
10-2171 Sliding Vise, AbrasiMet®, Right Hand
2 Mounting 20-1415 SimpliMet® 1000 Mounting Press
20-2402 Mold Assembly 14″ ID, 60mmOD
3 Semi-Automated 49-1780 EcoMet® 4000 Grinder/Polisher
Grinding/Polishing 60-1970 AutoMet® 2000 Power Head
49-1777 All Platens (4 needed)
60-5282 Specimen Holder, Barrel, 14″ x 10
60-2413 Loading Plate, 8″ and 12″ 60-9000 Drive Adapter
4 Final Polish 67-1635-250 VibroMet® 2 Vibratory Polisher
67-1527 Specimen Holder, 14″,VibroMet® (2 sets needed)
67-1529 SpecimenWeights,VibroMet® (2 sets needed)
5 Microscope to 0760-0100 ViewMet™ Inverted Lab Microscope
Inspect Quality of
Preparation
3
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-120-100
10″ (254mm) 30-5125-120-100
12″ (305mm) 15-5112-120-100
8″ (203mm) 30-5118-180-100
10″ (254mm) 30-5125-180-100
12″ (305mm) 15-5112-120-100
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-240-100
12″ (305mm) 30-5121-240-100
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-320-100
12″ (305mm) 30-5112-320-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
8″ (203mm) 40-7518
10″ (254mm) 40-7520
12″ (305mm) 40-7522
8″ (203mm) 40-7518
10″ (254mm) 40-7520
12″ (305mm) 40-7522
8″ (203mm) 40-8318
10″ (254mm) 40-8320
12″ (305mm) 40-8322
1 CarbiMet® Discs
(PSA) Grinding Paper
CarbiMet® Abrasive Discs
STEEL PREPARATIONMETHODS FOR EBSD & NANO INDENTATION WITH CONSUMABLE PART NUMBERS
VibroMet® 2
4
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
ChemoMet® I)
Holder Only
120-150 Contra
120-150 Contra
120-150 Contra
120-150 Contra
ALUMINUM 5 STEP PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
40-6370-006
5
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
ChemoMet® I)
Holder Only
120-150 Contra
120-150 Contra
120-150 Contra
ALUMINUM 4 STEP PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
VibroMet® 2
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME
Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/ Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
ChemoMet® I)
Holder Only
100-150 Contra
100-150 Contra
100-150 Contra
80-120 Contra
10
7
5
3
60
COBALT & IT’S ALLOYS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
40-6370-006
7
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
Holder Only
COPPER & BRASS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
40-6370-006
8
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-120-100
10″ (254mm) 30-5125-3-120-100
12″ (305mm) 30-5112-120-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
IRON ALLOYS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
63-6377-006
9
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-3-240-100
12″ (305mm) 30-5112-240-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
Holder Only
120-150 Contra
120-150 Contra
120-150 Contra
NI BASED ALLOYS PREPARATIONMETHOD FOR EBSD & NANO INDENTATION WITH CONSUMABLES PART NUMBERS
63-6377-006
10
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-3-320-100
12″ (305mm) 30-5112-320-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
40-6370-006
11
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/
Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-3-320-100
12″ (305mm) 30-5112-320-100
8″ (203mm) 40-7448
10″ (254mm) 40-7450
12″ (305mm) 40-7452
MasterMet® Colloidal Silica
40-6370-006
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME
Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/ Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-320-100
10″ (254mm) 30-5125-320-100
12″ (305mm) 15-5112-320-100
8″ (203mm) 30-5118-400-100
10″ (254mm) 30-5125-400-100
12″ (305mm) 15-5112-400-100
8″ (203mm) 30-5118-600-100
10″ (254mm) 30-5125-600-100
12″ (305mm) 30-5121-600-100
VibroMet® 2
ABRASIVE & POLISHING DISCS ABRASIVE TYPE LOAD SPEED TIME
Step Consumable Platen Catalog Abrasive Abrasive Catalog Lbs. (N) RPM/ Grinder/Polisher Type Surface Size No. Type Size No. Per Sample Direction Minutes
8″ (203mm) 30-5118-240-100
10″ (254mm) 30-5125-240-100
12″ (305mm) 15-5112-240-100
VibroMet® 2
BUEHLER LTD. –Worldwide Headquarters 41Waukegan Road • P.O. Box 1 • Lake Bluff, Illinois 60044-1699 USA Tel: 847/295-6500 • Fax: 847/295-7979 • Sales: 1/800/BUEHLER • 1/800/283-4537 Web Site: http://www.buehler.com • Email: [email protected]
BUEHLER GMBH - European andMESA Headquarters In der Steele 2 • 40599 Düsseldorf • Postfach 16 03 55 • 40566 Düsseldorf Telefon: (49) 211 974100 • Telefax: (49) 211 9741079 Web Site: http://www.buehler-met.de • Email: [email protected]
BUEHLER FRANCE Téléphone: 0800 89 73 71 • Télécopie: 0800 88 05 27 Web Site: http://www.buehler.fr • Email: [email protected]
BUEHLER UNITED KINGDOM Telephone: 0800 707 6273 • Fax: 0800 707 6274 Web Site: http://www.buehler.co.uk • Email: [email protected]
BUEHLER CANADA 10 Carlow Court, Unit #2 •Whitby,Ontario L1N 9T7 Telephone: (905) 430-4684 • Fax: (905) 430-4647 Sales Telephone: 1-800-268-3593 Email: [email protected]