Download - Golder Associates Inc. , Golder Associates - · PDF fileMEMORANDUM TO: Coakley Landfill Site Project QA Record FR: Jeffrey R. Hendel, Golder Associates Inc. Cq RE: Data Validation

Golder Associates Inc.

400 Commercial StreetManchester. NH USA 03101 -1113Telephone (603) 668-0880Fax (603) 668-1199

, GolderAssociates

TRANSMITTAL LETTER

To: Mr. Roger Duwart, HBORemedial Project ManagerNH/RI Superfund SectionU.S. EPA New EnglandJ.F.K. Federal BuildingBoston, MA 02203-2211

Date: December 11,1997Project No.: 963-6813

Copies to: Tal Hubbard - NHDES, Dan MacRitchie - City of Portsmouth,Pat Steerman - BFI, David S. Allen - City of Portsmouth,Tom Roy - Aries Engineering, Bea Hebert - PSNH

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Description

Validated Groundwater Quality Sampling Results,Third Quarter 1997, Coakley Landfill

Remarks:

Per: Michael Zarenski/lil

OFFICES IN AUSTRALIA, CANADA, GERMANY, HUNGARY, ITALY, SWEDEN, UNITED KINGDOM, UNITED STATES

WELL I.D. - SAMPLE ID CROSS REFERENCE FORM

COAKLEY LANDFILL

WELL I.D./QC I.D.

MW-5S

MW-5D

MW-2

MW-11

MW-8

MW-8 Field Dup

MW-9

MW-10

BP-4

OP-5

RP-1

GZ-105

FPC-5A

OP-2

SAMPLE I.D.

M5S997

M5D997

MW2997

W11997

MW8997

MW8FD1

MW9997

W10997

BP4997

OPS 997

RP1997

105997

C5A997

OP2997

LL\project\963-6813\wellid.doc Colder Associates

MEMORANDUM

TO: Coakley Landfill Site Project QA Record

FR: Jeffrey R. Hendel, Golder Associates Inc. Cq

RE: Data Validation Summary

November 1997

963-6813

1.0 INTRODUCTION

This memo presents the results of the data validation for the Coakley landfill Site Remedial Design Project. Thelaboratory submitted five separate reports, divided by sample collection date (SDGs). The packages containingthe monitoring well data consist of thirteen (13) primary groundwater samples, one field duplicate, one matrixspike/matrix spike duplicate (MS/MSD), one rinsate blank, and five trip blanks. All samples were analyzed forvolatile organics compounds (VOCs) utilizing SW-846 8260 and TAL Metals by USEPA 200 Seriesmethodologies. The trip blanks were analyzed for VOCs only. Accutest, of Marlborough, Maine analyzed allsamples. Following this memo includes data qualification summary and tables, copies of the validated laboratoryreports and data supporting documentation.

The following table provides the sampling information for the samples that were validated in accordance with theUSEPA Region I Functional Guidelines:

MONITORING WELLS

Sample IDW5S997W5D997MW2997W11997MW8997

MW8FD1*MW9997W10997BP4997OP5997RP1997105997

C5A997OP2397

Notes:

Sample Date9/4/979/4/979/4/979/4/979/4/979/4/979/5/979/5/979/5/979/5/979/8/979/9/979/9/979/23/97

* - Sample collected is a field duplicate ofMW8997.

MatrixWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWaterWater

VolatilesXXXXXXXXXXXXXX

MetalsXXXXXXXXXXXXXX

Data validation was conducted in accordance with the Region I Functional Guidelines and the Quality AssuranceProject Plan (QAPjP) dated February 1992. All sample results (Volatiles and Metals) were verified andvalidated.

November 1997 2 963-6813

2.0 VOLATILE ORGANICS

Data Quality Objectives

Precision: Goals for precision were met.

Accuracy: Goals for accuracy were met.

Sample Results Verification: All sample results were verified.

Completeness: The laboratory submitted five data packages containing VOC results. Fourteen (14) watersamples were validated in this data set. A total of 1036 results were reported in which 1006 weredeemed valid. This results in a completeness of 97% for the monitoring wells. The completenessobjective of 90% specified in the QAPjP was achieved.

Major Deficiencies

Identified below are the major deficiencies that required rejection of data. Refer to Table 1 for the specificsamples affected by each deficiency.

All SDGs (M2204. M2182. M2183, M2362. M2216)The initial and/or continuing calibrations had response factors (RRF) which were less than the minimum of 0.05for Acetone and 2-Butanone. In the case where a calibration had an RRF below 0.05, the associated samplesrequired qualification as estimated value (J) for positive results and rejected (R) for non-detected results.

During the data validation process, the qualitative identification of compounds is evaluated. The evaluations arebased on mass spectra, retention time, peak shape and intensity. The laboratories typically report a compound aspresent even if all spectral criteria are not met. For the compound Chloroethane in various samples, the massspectra did not meet the required criteria identified in the functional guidelines. There is no indication to thepresence of the compound based on mass spectra in these samples. Since the compound cannot be presumed tobe present in these samples, the results for this compound in the specified sample was qualified unusable (R ).

MINOR DEFICIENCIES

Identified below are the minor deficiencies that required qualification of the data. Refer to Table 1 for the specificsamples affected by each deficiency.

AM SDGs (M2204. M2182. M2183. M2362. M2216)Laboratory preparation blanks, rinsate blanks and trip blanks are evaluated for target compound contamination.Methylene chloride and Carbon disulfide were found as contaminants in various blanks for these SDGs. Samplesassociated with these blanks required qualification. For the compound Methylene chloride, an action limit of 10times the concentration found in the associated blank was calculated. For the compound Carbon disulfide, anaction limit of 5 times the concentration found in the associated blank was calculated. For samples where any ofthese compounds were detected as a positive result between the reporting limit (RL) and the action limit, the resultwas flagged as undetected (U). For samples where any of these compounds were detected below the RL, the

November 1997 3 963-6813

result was changed to the RL and qualified as undetected (U). There were no positive detects for either of thesecompounds above the action level.

During the data validation process, the qualitative identification of compounds is evaluated. The evaluations arebased on mass spectra, retention time, peak shape and intensity. For various compounds in various samples, themass spectra indicate that there is presumptive evidence of the presence of the compound, however, all criteria arenot met. Since the compounds are only presumed to be present in the samples, the results for those compounds inthe specific samples were qualified with the "N" flag.

The functional guidelines require the percent differences (%D) for the response factors between the initialand continuing daily calibration be less than + 25%. This criterion was not achieved for the compoundMethylene chloride in the continuing calibration analyzed on September 16, 1997. The functional guidelinesrequire compounds that have %Ds greater than 25% be qualified as estimated value (J). The functionalguidelines also require compounds that have %Ds greater than 50% be qualified as estimated reporting limit (UJ).Since non-of the continuing calibrations had compounds with %Ds greater than 50%, no qualification for non-detects was necessary.

November 1997 4 963-6813

3.0 TARGET ANALYTE LIST INORGANIC PARAMETERS

DATA QUALITY OBJECTIVES

Precision: Goals for laboratory and field precision were generally met, except where noted below.

Accuracy: Goals for accuracy were generally met, except where noted below.

Sample Result Verification: All sample results were supported in the raw data.

Detection Limits: The detection limit goals were achieved for all analyses.

Completeness: The data packages were complete for all requested analyses. Fourteen (14) samples werevalidated in this data set. A total of 336 results were reported in which 336 were deemed valid. This results in acompleteness of 100%. which meet the work plan objective of 90%.

MAJOR DEFICIENCIES

There were no major deficiencies identified with this data set.

MINOR DEFICIENCIES

Identified below are the minor deficiencies that required qualification of the data. Refer to Table 2 for the specificsamples affected by each deficiency.

All SDGs (M2204. M2182. M2183. M2362. M2216)The matrix spike recoveries for Aluminum, Calcium, Magnesium and Manganese were greater than thecriteria (75% - 125%) specified by the functional guidelines. For the affected samples, positive results

were qualified as estimated values (J).

The relative percent difference between the primary sample and the laboratory duplicate was greaterthan 20% when both the sample and the duplicate results for Aluminum, Arsenic, Calcium, Chromium,Iron, Magnesium, Manganese and Sodium were greater than 5 times the CRDL. Failure to meet this

criterion required qualification of these elements in these SDGs. For the affected samples, the resultswere qualified as estimated values (J) for positive detects.

SPG M2182The laboratory is required by the analytical method and the functional guidelines to analyze Mercury within 28days of sample collection. The laboratory failed to meet this requirement for the samples reported in this SDG.As a result, the results for Mercury were qualified as estimated values (J) for positive results and estimatedreporting limit (UJ) for nondetects.

November 1997 5 963-6813

4.0 SUMMARY

Validation of the data collected for the Remedial Design Program from the Coakley Landfill Site was performedin accordance with USEPA Region I data validation guidelines, as applicable, and the criteria specified by thespecific methods and the QAPjP.

Overall, the data required qualification due to some quality control criteria that were not achieved, but themajority of the data may be deemed usable in terms of objectives of the Remedial Design Work Plan. Although apositive result was qualified as estimated, the analyte should be considered present. Similarly, a non-detectedresult, which was qualified as an estimated quantitation/reporting limit, should be considered not present for thepurposes of this study, although the limit itself may not be precise. Rejected (unusable) data that are assigned the"R" qualifier should not be used.

REFERENCES

Golder, 1993, Quality Assurance Project Plan, Coakley Landfill She, North Hampton, New Hampshire,February 1992.

USEPA Region I, 1988, Region I Laboratory Data Validation Functional Guidelines for Evaluating OrganicsAnalyses, EPA Region I, November 1988.

USEPA Region I, 1988, Region I Laboratory Data Validation Functional Guidelines for Evaluating Inorganicsanalyses, EPA Region I, November 1988.

G:\963-6813\3rdq97\3ql97.doc

TABLE 1

DATE: November, 1997PROJECT NAME: Coakley LandfillANALYSIS: Volatile Organic Compounds by SW-846 Method 8260SAMPLE DELIVERY GROUP NUMBER: ALLREVIEWER: Jeffrey Hendel

PROJECT NO.: 963-6813

DEFICIENCY COMPOUND(S) QUALIFIER SAMPLES AFFECTED

Blank contamination

RRF less than 0 05 forinitial calibration

RRF less than 0 05 for thecontinuing calibrations

% difference between the mrtaland continuing RRFs exceeds25%

Methytene Chlonde U RP1997. W5S997,W5D997. MW2997,MW8997, MW8FD1 ,MW9997, BP4997,OP2397, 105997,C5A997, W10997,

OP5997Carbon disulfide U W5S997. W50997,

MW2997, MW8FD1,MW9997, W10997,BP4997, OP5997,OP2397, 105997,

C5A997

Acetone R All samples except sampleIDW11907

Acetone, R All samples except sample2-Butanone ID W1 1907

Methylene chlonde J for positive W5S997, W5D997,results MW8997, MW8FD1,

W11997, MW2997,MW9997, W10997,OP5997, BP4997

G \projects\963-6813\3rdq97\Table1 xls Colder Associates 1 of 2

TABLE 1

DATE: November, 1997PROJECT NAME: Coakley LandfillANALYSIS: Volatile Organic Compounds by SW-846 Method 8260SAMPLE DELIVERY GROUP NUMBER: ALLREVIEWER: Jeffrey Hendel


DEFICIENCY COMPOUND(S)

Presumptive evidence of thepresence of a compound

1,1-Dichloroethane,Toluene

Chloroethane

Chloroethane

Ethyl benzene,m+p-Xylenes,o-Xylene

Toluene

QUALIFIER SAMPLES AFFECTED

N RP1997

N MW8FD1, 105997,

C5A997

R W5S997, W5D997,

MW2997, MW8997.MW9997, OP2397

N W11997

N MW8FD1 . MW9997,BP4997

Notes

RL = Reporting Limit.

G\pro|ects\963-6813\3rdq97\Table1 xls Colder Associates 2 of 2

TABLE 2

DATE: November, 1997PROJECT NAME: Coakley LandfillANALYSIS: TAL Metals - 200 Series MethodologiesSAMPLE DELIVERY GROUP NUMBER: ALLREVIEWER: Jeffrey R. Hendel


DEFICIENCY ANALYTE(S)

Matrix spike recovery outside control limits

RPD between pnmary and lab

duplicate out of control

Aluminum,

Calcium,

Magnesium,

Manganese

Aluminum,

Arsenic,

Calcium,

Chromium,

Iron,

Magnesium,

Manganese,

Sodium

QUALIFIER SAMPLES AFFECTED

J for positive results ALL

J for positive results ALL

DATE: November, 1997SAMPLE DELIVERY GROUP NUMBER: M2182REVIEWER: Jeffrey R. Hendel

DEFICIENCY ANALYTE(S) QUALIFIER

Missed holding times ALL J for positive results

UJ for non-

detected results

SAMPLES AFFECTED

W5S997, W5D997,

MW2997, W11997.

MW8997, MW8FD1

Metals xls Colder Associates 1 of 1

November 1997 963-6813

Data Qualifiers

A - The data is acceptable; identification is confirmed.

U - The analyte was tested for but was not detected. The associated numerical value iseither the sample quantitation limit (organics) or the sample detection limit (inorganics).

R - Reject data due to quality control criteria. The data are unusable (analyte may or maynot be present in the sample).

N - Tentative identification; consider analyte present.

J - The analyte is present. The associated numerical value is an estimated quantity andmay not be accurate or precise.

UJ - The analyte was tested for but not detected. The sample quantitation limit or thesample detection limit is estimated and may be inaccurate or imprecise.

ziqual.def Page 1 of 1

SACCUTESTReport of Analysis Page 1 of 2

Client Sample DD:Lab Sample ID:Matrix:Method:Project:

Run#lRun #2

File IDD0597.

RP1997M2204-1AQ - GroundSWS46 8260Coakley Env.

DFD 2

Water

Monitoring, 480

Analyzed09/17/97

Breakfast Hill

ByDRY

Date Sampled: 09/08/97Date Received: 09/09/97Percent Solids: n/a

Rd., Greenland, NH

Prep Date Prep Batch Analytical Batchn/a n/a MSD23

VGA 8260 List

CAS No. Compound Result RDL Units Q

67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124^8-175-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Buty [benzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachlonde1,1-Dichloroe thane1 , 1-Dichloroethylene1 , 1 -D ichlo rop ropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibromochloromethaneDichlorodifluoromethanecis-1 ,2-Dichloroethylenecis- 1 ,3-Dichloropropenem-Dichlorobenzeneo-Dichlorobenzenep-D ichlorobenzenetrans- 1 ,2-D ichloroe thy lenetrans- 1 , 3-DichIoropropeneEthylbenzene2-Hexanone

ND K 2.015.1 ft 0.80ND Lf 2.0NDNDNDNDND

2.00.800.802.02.0

ND " 2.024.4 ^ 0.8090.2 * 2.0ND U 0.80ND 1 2.0ND 2.0ND 1 2.0ND *• 0.801.2 ^ 0.80ND C' 0.40NDNDNDNDNDNDNDNDNDNDNDNDND*

2.02.00.800.800.802.02.00.800.800.800.20

' 0.80^ 0.80

9.6 A 0.80ND o 0.80ND <-' 0.2062.0 A 0.80ND o 2,0

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAugAugAug/1ugAugAug/1

ND = Not detectedRDL = Reported Detection LimitE = Indicates value exceeds calibration range

J = Indicates an estimated valueB = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compound

000007


Client Sample ED:Lab Sample ID:Matrix:Method:Project:

File EDRun #1 D0597.Run #2

RP1997M2204-1AQ - GroundSW846 8260Coakley Env.

DFD 2

Water

Monitoring, 480 Breakfast

Analyzed By09/17/97 DRY


Hill Rd., Greenland, NH


VGA 8260 List


87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00^

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Methyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1, 1-Trichloroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichloroethane1 ,2,3-Trichlorobenzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethylbenzene1 J ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoromethaneVinyl chlorideXylene (total)

Surrogate Recoveries

DibromofluoromedianeToluene-DS4-Bromofluorobenzene

ND v 2.02.

ND <•NDNDNDND3.9 U

-" z.2.

000

0.8U2.2.0

0080

ND ft 2.023.4 A 2.0^ rt -» A3.2 r

ND iNDNDNDNDNDNDND J30.710.7

•* z.uJ 2.0

2.00.800.800.802.02.02.0

A 2.0A 2

ND <•> 0t

1.6 A* 0NDNDND <98.2

J 0J 0

.0

.80

.80

.80

.80•f 0.80A 0.80

Run# 1 Run# 2

955696%

« ••

10096

ug/1ug/t

f\ug/1ug/1ug/1ug/1ug/1

It TVug/l yug/1ug/1

ftug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

Limits

86-1189688-1109680-120%


J = Indicates an estimated valueB = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compopnd\ n A n Q

QACCUTESTReport of Analysis Page 1 of 2

Client Sample ED:Lab Sample ED:Matrix:Method:Project:

Run #2

File EDD0603.

105997M2216-1AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast

ByDRY


HillRd., Greenland, NH


VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenrenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1 , l-Dichloroethane1 , 1 -Dichloroethylene1 , 1-Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1,2-Dichloroethane1 ,2-Dichloropropane1 , 3 -Dichloropropane2 , 2-D ichloropropaneDibromochloromethaneDichlorodifluorome thanecis-1 ,2-Dichloroethylenecis-1 ,3-Dichloropropenem-Dichlorobenzeneo-Dichlorobenzenep-Dichlorobenzenetrans-1 ,2-Dichloroethylenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

ND & 1.010 /» 0.40ND t; l.oNDNDNDNDNDND

1.00.400.401.01.0

* 1.03.5 A . 0.4012.6^ 1.0ND '̂ 0.40ND ^ 1.0ND I/ 1.01.2 <•> 1.0ND <-' 0.401.9 A 0.40ND U 0.20NDNDNDNDNDNDNDNDNDND'NDND

1.01.00.400.400.401.01.00.400.400.400.100.40

ND * ~ 0.402.8 A 0.40NDt/ 0.40ND" 0.1013.8 A 0.40ND U 1.0

ug/1ug/1ugAug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ugAug/1ug/1ugAug/1ugAug/1ug/1ugAugAugAugAugAugAugAugAugA



000007


Client Sample ID:Lab Sample ED:Matrix:Method:Project:

File EDRun#l D0603.Run #2

105997M2216-1AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast Hill

ByDRY


Rd.. Greenland, NH

Prep Date Prep Batchn/a n/a

Analytical BatchMSD23

VGA 8260 List

CAS No. Compound

87-68-3 Hexachlorobutadiene98-82-8 Isopropylbenzene99-87-6 p-Isopropyltoluene108-10-1 4-Methyl-2-pentanone74-83-9 Methyl bromide74-87-3 Methyl chloride74-95-3 Methylene bromide75-09-2 Methylene chloride78-93-3 Methyl ethyl ketone91-20-3 Naphthalene103-65-1 n-Propylbenzene100-42-5 Styrene630-20-6 1,1,1,2-Tetrachloroethane71-55-6 1,1,1-Tnchloroethane79-34-5 1,1,2,2-Tetrachloroethane79-00-5 1,1,2-Tnchlorocthane87-61-6 1,2,3-Trichlorobenzene96-18-4 1,2,3-Trichloropropane120-82-1 1,2,4-Tnchlorobenzene95-63-6 1,2.4-Trimethylbenzene108-67-8 1,3,5-Trimethylbeozene127-18-4 Tetrachloroethylene108-88-3 Toluene79-01-6 Trichloroethylene75-69-4 Trichlorofluoromethane75-01-4 Vinyl chloride1330-20-7 Xylene (total)

CAS No. Surrogate Recoveries

1868-53-7 Dibromofluoromethane2037-26-5 Toluene-D8460-00-4 4-Bromofluorobenzene

Result

9936-97%107*

RDL Units Q

ND V 1.04.5 A 1.0ND ̂ 1.0NDNDNDND °

1.00.401.01.0

3.1 o' 0.40ND £ 1.02.6 ft 1.0ND O 1.0NDNDNDNDNDNDNDND

1.01.00.400.400.401.01.01.0

3.9 A 1.01.3 A 1.0ND u 0.40ND [ 0.40ND ) 0.40ND 1 0.40ND 0.4025.8 * 0.40

ug/lug/1ug/lugAug/tug/lugAug/lug/lugAug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lugAug/lug/lug/lug/lug/l

Run# 1 Run# 2 Limits

86-118%88-110%80-120%

in hi!.'/'*/„ 7


I = Indicates an estimated valueB = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compound



Run#lRun #2

C5A997M2216-2AQ - GroundSW846 8260Coakley Env.

File ID DFD0604.D 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast

ByDRY




VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106^3-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBroraochloromethaneBromodichlorome thaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachlonde1,1-Dichloroe thane1 , 1-Dichloroethylene1 , 1-Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibromochloromethaneDichlorodifluoromethanecis-1 ,2-Dichloroethylenecis- 1 , 3-Dichloropropenem-Dichlorobenzeneo-Dichloro benzenep-Dichlorobenzenetrans-1 ,2-Dichloroethylenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

ND &• 1.09.3 A 0.40ND ^ 1.0NDNDNDNDNDND

1.00.400.401.01.01.0

22.5 * 0.4019.7^ 1.0ND "' 0.40ND J 1.0ND ^ 1.01.4 *•' 1.0ND v.' 0.401.7 A- 0.40ND U 0.20NDNDNDNDNDNDNDNDNDNDND

1.01.00.400.400.401.01.00.400.400.40

* 0.10ND * ,0.402.0 3, >Vo.405.4 A " 0.40ND O 0.40ND i 0.10ND / 0.40ND L 1.0

ug/1ug/1ugAug/1ug/1ugAugAug/1ug/1ug/1ugAug/1ug/1ug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/IugAugAugAugAugAugAugAugAug/1ug/1ugA



0 0 0 0 1 f


Client Sample CD:Lab Sample ED:Matrix:Method:Project:

Run 01Run #2

File IDD0604.

C5A997M2216-2AQ - GroundSW846 8260Coakley Env.

DFD i

Water

Monitoring, 480

Analyzed09/17/97

Breakfast Hill

ByDRY

Date Sampled: 09/09/97Date Received: 09/10/97Percent Solids: a/a

Rd., Greenland. NH


VGA 8260 List

CAS No.

87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

Compound

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Mediyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1,1 -Tnchloroethane1 , 1 ,2.2-Tetrachloroethane1 , 1 ,2-Tnchloroethane1 ,2,3-Trichlorobenzene1 ,2,3-Tnchloropropane1 ,2,4-Tnchlorobenzene1 ,2,4-Trimethylbenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoro methaneVinyl chlorideXylene (total)


DibromofluoromethaneToluene-DS4-Bromofluorobenzene

Result RDL

ND ^ 1.03.8 A 1.0NDu 1.0ND 1.0ND 0.40ND 1.0ND I 1.01.9 ^ 0.40ND/< 1.02.6 A i.oND V 1.0ND 1.0ND 1.0ND 0.40ND 0.40ND 0.40ND 1.0ND 1.0ND 1.0ND 1.0ND 1.0ND 0.40ND 0.40ND 0.40ND 0.40ND , 0.40ND V 0.40

Run# 1 Run* 2

98%" ~97%101%

Units

ug/1ug/1ugAug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/lug/1ug/1ug/1ug/1ug/1ug/1ugAugAug/1ug/1ug/1

Q

B

Limits

86-118%88-110%80-120%



000012

QACCUTESTReport of Analysis Page I o f 2

Client Sample ED: OP2397 (WELL OP2)Lab Sample ID: M2362-1Matrix:Method:Project:

Run#lRun #2

AQ - GroundSW346 8260Coakley Env.

File ID DFD0887.D 1

Water

Monitoring, 480 Breakfast Hill



Rd., Greenland, NH

Prep Date Prep Batcha/a a/a


VGA 8260 List


67-64-1 Acetone71-43-2 Benzene108-86-1 Bromobenzene74-97-5 Bromochloromediane75-27-4 Bromodichloromethane75-25-2 Bromoform1 04-5 1 -8 n-Buty Ibenzene135-98-8 sec-Butylbenzene98-06-6 tert-Butylbenzene108-90-7 Chlorobenzene75-00-3 Chloroethane67-66-3 Chloroform95-49-8 o-Chlorotoluene106-43-4 p-Chlorotoluene75-15-0 Carbon disulfide56-23-5 Carbon tetrachloride75-34-3 1,1-Dichloroethane75-35-4 1,1-Dichloroethylene563-58-6 1,1-Dichloropropene96-12-8 1 ,2-Dibromo-3-chloropropane106-93-4 1,2-Dibromoethane107-06-2 1,2-Dichloroethane78-87-5 1,2-Dichloropropane142-28-9 1,3-Dichloropropane594-20-7 2,2-Dichloropropane124-48-1 Dibromochloromethane75-71-8 Dichlorodifluoromethane156-69-4 cis-l,2-Dichloroethylene10061-01-5 cis-1.3-Dichloropropene541-73-1 m-Dichlorobenzene95-50-1 o-Dichlorobenzeoe106-46-7 p-Dichlorobenzene156-60-5 trans- 1 , 2-Dichloroethy lene10061-02-6 trans-l,3-Dichloropropene100-41-4 Ediylbenzene591-78-6 2-Hexanone

ND = Not detectedRDL = Reported Detection Limit

NDjE/C i.o13.5 A 0.40ND <J 1.0ND 1.0ND 0.40ND 0.40ND 1.0ND 1.0ND * 1.025.8 ^ 0.406.7 £ 1.0ND w 0.40ND 1 1.0ND * 1.02.9 V 1.0ND U 0.40ND 0.40ND 0.20ND 1.0ND 1.0ND 0.40ND 0.40ND 0.40ND 1.0ND 1.0ND 0.40ND 0.40ND 0.40ND, ! 0.10NBt* % , * 0.400.99^"* 0.407.4-4 0.40ND t/ 0.40ND i/ 0.103.3 A 0.40ND ^ 1.0

ugAug/1ugAugAug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ugAugAug/1ug/1ug/1ug/1ugAug/1ug/1ugAug/1ugAugAugAug/1ugAugAugAug/1ug/1ugAug/1

J = Indicates an estimated valueB = Indicates that analyte is found in associated method blank

E = Indicates value exceeds calibration range N = Indicates presumptive evidence of a compound

000007



Run#lRun #2

File EDD0887.

OP2397 (WELL OP2)M2362-1AQ - Ground WaterSW846 8260Coakley Env. Monitoring, 480

DF AnalyzedD 1 10/04/97

Breakfast Hill

ByDRY


Rd., Greenland, NH


VGA 8260 List


87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Mediyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1.1,1 ,2-Tetrachloroethane1,1,1 -Tnchloroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichloroethane1 ,2,3-Trichlorobenzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Tnmethy Ibenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTnchloroethyleneTrichlorofluoromedianeVinyl chlorideXylene (total)


Dibromofluoro me thaneToIuene-D84-Bromofluorobenzene

ND U4.7^ND UNDNDNDND«'0.58 VND Z22.1 A1.4 A

ND <-;ND |ND INDNDND 1NDJND*12.9 44.8 4ND u1.6 AND oND vND ^23.2 *

Run#l

102 %-;-97%105%

1.01.01.01.00.401.01.00.401.01.01.01.01.00.400.400.401.01.01.01.01.00.400.400.400.400.400.40

Run* 2

>

^

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1 Bug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

Limits

86-118%88-110%80-120%



000008


Qient Sample ED:Lab Sample ED:Matrix:Method:Project:

File EDRun#l DOS 77.Run #2

W5S997M2 182-1AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480 Breakfast Hill



Rd., Greenland, NH


VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106^6-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotoIueneCarbon disulfideCarbon tetrachloride1,1-Dichloroethane1 , 1-Dichloroethylene1 , 1 -Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibrornochloromethaneDichlorodifluoro methanecis-1 ,2-Dichloroethylenecis- 1 , 3 -Dichloropropenem-Dichlorobenzeneo-Dichlorobenzenep-Dichlorobenzenetrans- 1 ,2-Dichloroethylenetrans- 1 , 3-DichloropropeneEthylbenzene2-Hexanone

ND « 1.012.7 ^ 0.40NDNDNDNDND0.61ND28.59.6NDNDND2.7ND

C-̂ 1

i1

1oo1

A 1-J 1A 0

.0

.0

.40

.40

.0

.0

.0

.40R i.ou 0.40

1 L0

* 1.0t/ 1.0i>' 0.40

1.7 A 0.40ND <^ 0.20NDNDNDNDNDNDNDNDNDNDNDND

1.01.00.400.400.401.01.0.0.0.0.0.0.

1.2 * 0.8.9 <* 0.

40404010404040

ND u 0.40ND<-t 0.107.2 A 0.40ND i/ 1.0

ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1 Jug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/lug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1



000007



File IDRun#l D0577.Run #2

W5S997M2182-1AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/16/97

Breakfast Hill

ByDRY


Rd., Greenland, NH


VGA 8260 List


87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Mediyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1, 1-Trichloroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichtoroethane1 ,2,3-TrichIorobenzene1 ,2,3-Tnchloropropane1 ,2,4-Trichlorobenzene1 ,2.4-Trimethylbenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoromethaneVinyl chlorideXylene (total)


DibromofluoromethaneToluene-DS4-B romo fluorobe nzene

ND2.6NDNDNDNDND1.0ND10 '0.35NDNDNDNDNDNDNDND1

0.53

t> 1.0^ 1.0•> 1.0

1.00.401.01.0

w 0.40^ 1.01 1.0A 1.0v 1.0

1.00.400.400.401.01.01.0

* 1.02.0 A i.oND vNDNDND ,ND JND*

J 0.400.400.400.400.400.40

Run? 1 Run? 2

94%

ug/1ug/1ug/1ug/Iug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

B

J

J

Limits

86-118%100%98%

88-110%80-120%



000008



Run#lRun #2

File EDD0578.

W5D997M2 182-2AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/16/97

Breakfast Hill

ByDRY


Rd., Greenland, NH


VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106^3-475-15-056-23-575-34-375-35^563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroe thaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1,1-Dichloroe thane1 , 1-Dichloroethylene1, 1-Dichloropropene1 ,2-Dibromo-3-chIoropropane1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneD ib romochloro methaneDichlorodifluoromethanecis-1 ,2-Dichloroethylenecis- 1 , 3-D ichloropropenem-D ichlorobenzeneo-Dichlorobenzenep-Dichlorobenzenetrans- 1 ,2-Dichloroethylenetrans-l,3-DichloropropeneEthylbenzene2-Hexanone

ND K 1.05.4 A 0.40ND ^ 1.0NDNDNDND

1.00.400.401.0

ND 1.0ND * 1.08.1 * 0.4012.4 /? 1.0ND V 0.40ND 1 1.0ND * 1.04.5 </ 1.0ND <-' 0.401.3 A 0.40ND U 0.20NDNDNDNDNDNDNDNDNDNDNDND

1.01.00.400.400.401.01.00.400.400.400.10

'0.40ND* 0.402.3 A 0.40ND u 0.40ND | 0.10ND 0.40ND v 1.0

ug/1ug/1ug/1ug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ug/1ugAug/1ugAug/1ug/1ugAugAugA

' ugAugAugAugAug/1ug/1ug/1



nnnni1



Run£lRun #2

File EDD0578.

W5D997M2 182-2AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/16/97

Breakfast

ByDRY


Hill Rd.. Greenland, NH



VGA 8260 List


87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18^120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Methyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylberueneStyrene1.1,1 ,2-Tetrachloroethane1,1, 1-Trichloroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichloroethane1 ,2,3-Trichlorobenzene1 ,2,3-Tnchloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethy Ibenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoromethaneVinyl chlorideXylene (total)


DibromofluoromeduneToluene-DS4-Bromofluorobenzene

ND U 1.0NDNDNDNDND

1.01.01.00.401.0

ND v 1.01.1 U 0.40ND A 1.03.2 A 1.0ND o' i.ONDNDNDNDNDNDNDND

1.01.00.400.400.401.01.01.0

ND * 1.00.64 (^ 1.0ND A 0.40NDNDNDND

0.400.400.400.40

ND * 0.40

Run? 1 Rurrf 2

98% ' "99%104%

(

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1 Bug/lug/1ug/lug/1ug/lug/lug/lug/lug/lug/lug/lug/lug/l Jug/lug/lug/lug/lug/lugA

Limits

86-118%88-110%80-120%

•V-'Ir'/n


I = Indicates an estimated valueB = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compoundmpoun

000012

QACCUTESTReport of Analysis Page I of 2

Client Sample ED: MW2997Lab Sample ID : M2 1 82-3Matrix:Method:Project:

Run#lRun 07.

VGA 8260

CAS No.

67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-357-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-6J6-12-8106-93-4107-06-278-87-5142-28-9594-20-724-48-1'5-71-856-69-40061-01-541-73-15-50-106-46-756-60-50061-02-600-41-491-78-6

AQ - Ground WaterSW846 8260Coakley Env. Monitoring, 480 Breakfast

File ED DFD0596.D 1

List

Compound

AcetoneBenzeneBromobenzeneB romochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-ChlorotoIuenep-ChlorotolueneCarbon disulfideCarbon tetrachlonde1 , 1 -Dichloroethane1 , 1-Dichloroethylene1 , 1-Dichloropropene


Result RDL

ND £ 1.04.6 A 0.40ND / 1.0NDNDNDNDND

1.00.400.401.01.0

ND 1.015.6 A o 403.4 * 1.0ND v 0.40ND *-' 1.0ND u' 1.02.5 ^ 1.0ND ̂ 0.40NDNDND

l,2-Dibromo-3-chloropropane ND1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibromochloromethaneDichlorodifiuoromethanecis-1 ,2-DichloroethyIenecis-1 ,3-Dichloropropenem-Dichlorobenzeneo-D ichlorobenzenep-Dichlorobenzenetrans-1 ,2-Dichloroethylenetrans-1 ,3-DichIoropropeneEthylbenzene2-Hexanone

NDNDNDNDNDNDNDNDNDNDND-*

0.400.201.01.00.400.400.401.01.00.400.400.400.10

. ,0.40- 0.40

2.7 * 0.40ND U 0.40ND 1 0.10ND 0.40ND ¥ 1.0




Units Q

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/Iug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/Iug/1



000015


Client SamLab SampliMatrix:Method:Project:

'•'—

Run#lRun #2

VGA 8260

CAS No.

87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18^108-88-379-01-675-69^75-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

.pie ED: MW2997» ID: M2 182-3

AQ - Ground WaterSW846 8260Coakley Env. Monitoring, 480 Breakfast Hill

File CO DFD0596.D 1

List

Compound

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Methyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1,1-TrichIoroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichloroethane1 ,2,3-Tnchlorobenzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethylbenzene1 ,3,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoromethaneVinyl chlorideXylene (total)


DibromofluoromethaneToluene-D84-B ro mo fluorobenrene


Result RDL

ND ^ 1.0NDNDNDNDND

1.01.01.00.401.0

ND ' 1.01.8 (J 0.40ND ^ 1.0ND ^' 1.0NDNDNDNDNDNDNDNDNDNDNDNDNDND

l.U

1.01.00.400.400.401.01.01.01.01.00.400.400.40

ND 0.40ND 0.40ND * 0.40

Run# 1 Run* 2

96 £ -V ,96%104%

•?>/*


Rd., Greenland, NH


Units Q

ug/1ugAug/1ug/1

/*ug/111ug/1(1

ug/1ug/1 B

iiug/1/«ug/111ug/1/Iug/1

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAugAug/1ug/1ug/1ugAugA

Limits

86-118%88-110%80-120%

;


J = lHULt.<llco ail twin-.—

B = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compound

000016

SACCUTESTReport of Analysis Page I of 2


Run t f lRun tn.

File IDD0612.

W11997M2 182-4AQ - GroundSW846 8260Coakley Env.

DFD 200

Water

Monitoring, 480

Analyzed09/18/97


Breakfast Hill Rd., Greenland, NH

By Prep Date Prep BatchDRY n/a n/a


VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35^1563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41^591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1,1-DtchIoroethane1 , 1-Dichloroethylene1 , 1-Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-DichIoropropane2,2-DichloropropaneDibromochloromethaneDichlorodifluoromethanecis-1 ,2-Dichloroethylenecis-1 ,3-Dichloropropenem-Dichlorobenzeneo-Dichlorobenzenep-D ichlorobenzenetrans-1 ,2-DicbJoroethylenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

6140 -J 200ND O 80NDNDNDNDNDNDNDNDNDNDNDNDNDND

2002008080200200200802008020020020080

ND 80NDNDNDNDNDNDNDNDNDNDNIXNJ> ,"ND: *

ND 'NDND j

402002008080802002008080

; 80

' 20- 80.80

8080

ND tf 2062.5 X 80ND (j 200

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ug/1ugAugAug/1ugAug/1 Jug/1



r\ n r\ r\ ^ r\


Client Sample ED: W11997Lab Sample ID : M2 1 82-4Matrix:Method:Project:

Run#lRun #2

AQ - GroundSW846 8260Coakley Env.

File ID DFD0612.D 200

Water






VGA 8260 List


87-68-398-82-899-87-6108-10-174-83-974-87-374-88-474-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-4108-05-41330-20-7

CAS No.

1868-53-72037-26-5460-00^

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Methyl-2-pentanoneMethyl bromideMethyl chlorideMethyl iodideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1, 1-Trichloroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichloroethane1 ,2,3-Trichlorobenzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethylbenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluorome thaneVinyl chlorideVinyl AcetateXylene (total)


DibromofluoromethaneToluene-DS4-BromofIuorobenzene

ND L/ 200NDNDNDNDNDNDND ;

20020020080200200200

364 0 8061103" 200ND U 200NDNDNDNDNDNDNDNDNDNDNDND

200200200808080200200200200200

1 808950 « 80ND U 80ND | 80ND 80ND * 200160 // . 80

Run# 1 Run// 2

92%96%98%

/'4

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1 Bug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/lug/1ug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/l

Limits

86-118%88-110%80-120%

^ ••/*/* 7


J = Indicates an estimated valueB = Indicates that analyte is found in associated mediod blankN = Indicates presumptive evidence of a compound

nnnrm



Run if IRun #2

File IDD0600.

MW8997M2 182-5AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast Hill

ByDRY


Rd., Greenland, NH



VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-1*TC T 1 a75-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneB ro mochlo ro methaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1,1-Dichloroe thane1 , 1-Dichloroethylene1, 1-Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibromochloro me thaneDichlorodifluoro me thanecis- 1 ,2-Dichloroethylenecis-1 ,3-Dichloropropenem-Dichlorobenzeneo-Dichloro benzenep-Dichlorobenzenetrans-1 ,2-Dichloroethylenetrans- 1 ,3-DichloropropeneEthylbenzene2-Hexanone

ND K i.o6.3 A 0.40ND U 1.0NDNDNDNDND

1.00.400.401.01.0

ND *• 1.02.1 * o.4011.1 K. 1.0ND <-> 0.40NDNDND

1.01.01.0

ND * 0.402.2 * 0.40ND ^ 0.20NDNDNDNDNDNDNDNDNDNDNDND/

1.01.00.400.400.401.01.00.400.400.40

* . 0.100.40

ND * 0.401.7 A 0.40ND u 0.40ND " 0.1012.3 A 0.40ND ^ 1.0

ugAug/1ug/1ugAugAug/Iug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/Iug/1ug/lug/1ug/1ugAugAug/1ug/1ug/1ug/1ug/1ug/1 "•ugAugAugAugAugAugAug/1ugAugA




Client Sample ID:Lab Sample ID:Matrix:Method:Project:

File EDRun#l D0600.Run #2


DFD 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast

ByDRY




VGA 8260 List


87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69^75-01-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Methyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1,1-Trichloroethane1 , 1 ,2,2-Tetrachloroethane1,1,2-Trichloroethane1 ,2,3-Trichlorobenzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethylbenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoromethaneVinyl chlorideXylene (total)


DibromofluoromedianeToluene-DS4-B romo fluorobenzene

ND3.2 'ND v

NDNDNDND '

J 1.0*• i.oJ 1.0

1.00.401.01.0

2.7 <-' 0.40rt

ND "2.7 f

^ 1.0*• 1.0

ND t/ 1.0NDNDNDNDNDNDNDND3.8 fND iND i1.1 -NDNDND13.4

1.01000111

* 1> 1/ 01 0u 0U 0u 0A 0

040.40.40.0.0.0.0.0.40.40.40.40.40.40

RunPl Run#2

92%95%100%

Qf,,l

ug/1ug/lugAugAugAug/1ug/1ug/1 Bug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAugA

Limits

86-118%88-110%80-120%

*//*/



000024



Run#lRun #2

File IDD0601.

MW8FD1M2 182-6AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast

ByDRY

Date Sampled: 09/04/97Date Recei ved : 09/05 191Percent Solids: n/a




VGA 8260 List


67-64-1 Acetone71-43-2 Benzene108-86-1 Bromobenzene74-97-5 Bromochloromethane75-27-4 Bromodichloromethane75-25-2 Bromoform104-51-8 n-Butylbenzene135-98-8 sec-Butylbenzene98-06-6 tert-Butylbenzene108-90-7 Chlorobenzene75-00-3 Chloroethane67-66-3 Chloroform95-49-8 o-Chlorotoluene106-43-4 p-Chlorotoluene75-15-0 Carbon disulfide56-23-5 Carbon tetrachloride75-34-3 1,1-Dichloroethane75-35-4 1,1-Dichloroethylene563-58-6 1,1-Dichloropropene96-12-8 l,2-Dibromo-3-chloropropane106-93-4 1 ,2-Dibromoethane107-06-2 1,2-Dichloroethane78-87-5 1,2-Dichloropropane142-28-9 1,3-Dichloropropane594-20-7 2,2-Dichloropropane124-48-1 Dibromochloromethane75-71-8 Dichlorodifluoromethane156-69-4 cis-l,2-Dichloroethylene10061-01-5 cis-l,3-Dichloropropene541-73-1 m-Dichlorobenzene95-50-1 o-Dichlorobenzene106-46-7 p-Dichlorobenzene156-60-5 trans-l,2-Dichloroeuaylene10061-02-6 trans- 1 ,3-Dichloropropene100^1-4 Ethylbenzene591-78-6 2-Hexanone


ND K.6.9 AND ^NDNDNDNDND !ND*-2.4 A12.0 dND UND wND «/1.2 UND ->2.4 AND UNDNDNDNDNDNDNDNDNDNDNDNDND * "1.8 ftND uND U12.6 AND v

1.0 ug/10.40 ug/11.0 ug/11.0 ug/10.40 ug/10.40 ug/11.0 ug/11.0 ug/11.0 ug/10.40 ug/11.0 ug/10.40 ug/11.0 ug/11.0 ug/11.0 ug/10.40 ug/10.40 ug/10.20 ug/I1.0 ug/11.0 ug/10.40 ug/10.40 ug/10.40 ug/11.0 ug/11.0 ug/10.40 ug/10.40 ug/10.40 ug/10. 10 ug/10.40 ug/I0.40 ug/10.40 ugA0.40 ug/10. 10 ug/10.40 ug/11.0 ug/1


000027



Run#lRun #2

File DOD0601.

MW8FD1M2 182-6AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/17/97

Breakfast

ByDRY




VOA 8260 List

CAS No. Compound

87-68-3 Hexachlorobutadiene98-82-8 Isopropylbenzene99-87-6 p-Isopropyltoluene108-10-1 4-Mediyl-2-pentanone74-83-9 Methyl bromide74-87-3 Methyl chloride74-95-3 Methylene bromide75-09-2 Methylene chloride78-93-3 Methyl ethyl ketone91-20-3 Naphthalene103-65-1 n-Propylbenzene100-42-5 Styrene630-20-6 1,1,1 ,2-Tetrachloroethane71-55-6 1,1,1-Tnchloroethane79-34-5 1,1,2,2-Tetrachloroethane79-00-5 1 , 1 ,2-Tnchloroethane87-61-6 1,2,3-Tnchlorobenzene96-18-4 1,2,3-Tnchloropropane120-82-1 1,2,4-Tnchlorobenzene95-63-6 1 ,2,4-Tnmethylbenzene108-67-8 1,3,5-Trimethylbenzene127-18-4 Tetrachloroethylene108-88-3 Toluene79-01-6 Tnchloroethylene75-69-4 Tnchlorofluoromethane75-01-4 Vinyl chloride1330-20-7 Xylene (total)


1868-53-7 Dibromofluorometbane2037-26-5 Toluene-DS460-00-4 4-Bromofluorobenzene


Result

ND tr3.1/1ND L>NDNDNDND V1.9 fND *3.7 AND ^NDNDNDNDNDNDNDND *3.9 A1.3 AND tf1.2 /tND uND *ND«^13,7 A-

Run* I

99%98%106%

RDL Units Q

1.0 ug/11.0 ug/11.0 ug/1l.O ug/10.40 ugA1.0 ug/11.0 ug/10.40 ug/1 Bl.O ug/11.0 ug/11.0 ug/11.0 ug/11.0 ug/10.40 ugA0.40 ugA0.40 ug/11.0 ug/11.0 ug/11.0 ug/11.0 ug/11.0 ug/10.40 ug/10.40 ugA0.40 ugA0.40 ug/10.40 ugA0.40 ug/1

Run* 2 Limits

86-118%88-110%80-120%


000028

QACCUTESTReport of Analysis Page I of 2

Client Sample ED: MW9997Lab Sample ED: M2183-1Matrix:Method:Project:

Run ttlRun #2

VGA 8260

CAS No.

67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-357-66-335-49-8106-43^75-15-056-23-575-34-375-35-4563-58-676-12-8106-93-4L07-06-278-87-5142-28-9•94-20-724^8-1'5-71-856-69-40061-01-541-73-15-50-106-46-756-60-50061-02-600-41-491-78-6

AQ - Ground WaterSW846 8260Coakley Env. Monitoring, 480 Breakfast

File ED DFD0613.D 2

List

Compound

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1 , 1-Dichloroethane1 , 1-Dichloroethylene1 , 1-Dichloropropene





Result RDL Units Q

ND &. 2.012.6 /V 0.80ND (J 2.0NDNDNDNDND

2.00.800.802.02.0

ND * 2.081.9* 0.806.5 £ 2.0ND u 0.80ND j 2.0ND V 2.016.2 U 2.0ND ^ 0.80NDNDND

l,2-Dibromo-3-chloropropane ND1 ,2-Dibromoethane1 ,2-Dichloroediane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibromochloromethaneDichlorodifluoromethanecis- 1 ,2-Dichloroethylenecis-l,3-Dichloropropenem-D ichlorobenzeneo-Dichlorobenzenep-Dichlorobenzenetrans- 1 ,2-Dichloroethylenetrans-1 ,3-DichloropropenfiEthylbenzene2-Hexanone

NDNDNDNDNDNDNDNDNDNDND /•

0.800.402.02.00.800.800.802.02.00.800.800.800.20

'0.80'-'0.80

21.8 A- 0.80ND v 0.80ND * 0.2022.4 * 0.80ND ^ 2.0

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1


J = Indicates an estimated valueB = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compTJtfooo?

EJACCUTESTReport of Analysis Page 2 of 2




DFD 2

Water

Monitoring, 480

Analyzed09/18/97

Date SampledDate ReceivedPercent Solids

Breakfast Hill Rd. , Greenland,

By Prep DateDRY n/a

: 09/05/97: 09/06/97: n/aNH

Prep Batch Analytical Batchn/a MSD23

VOA 8260 List

CAS No. Compound Result

87-68-398-82-899-87-6108-10-174-83-974-87-374-88-474-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69-475-01-4108-05-41330-20-7

CAS No.

1868-53-72037-26-5460-00-4

HexachlorobutadieneIsopropylbenzenep-Isopropyltoluene4-Mediyl-2-pentanoneMethyl bromideMethyl chlorideMethyl iodideMethylene bromideMethylene chlorideMethyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1,1-Trichloroethane1 , 1 ,2,2-Tetrachloroethane1 , 1 .2-Trichloroethane1,2,3 -Trichlorobenzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethylbenzene1 ,3,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichlorofluoromethaneVinyl chlorideVinyl AcetateXylene (total)


DibromofluoromethaneToluene-D84-B romo fluorobenzene

N D L3.3 'ND iNDNDNDNDND '

'L

1

)

2.4 (Js\

ND /12.40.81ND<-NDNDNDNDNDNDND'6.5 '3.5 '

<*.

,\

A1

\,I

ND VI c. A!.6 A>

NDNDNDND9.1

a

*

Run#l

97%98%93%


RDL Units Q

Run# 2 Limits

86-118%88-110%80-120%


009(T-8



Run#lRun//2

File IDDOS 85.

W 10997M2 183-2AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/16/97

Breakfast

ByDRY





VGA 8260 List


67-64-171-43-2108-86-174-97-575-27^75-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93^1107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106-46-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneB romodichloromethaneBromoforrnn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1 , 1 -Dichloroethane1, 1-Dichloroethylene1 , 1-Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1 ,2-Dichloroethane1 ,2-Dichloropropane1 , 3 -D ichloropropane2,2-DichloropropaneDibromochloromethaneDichlorodifluoromethanecis-1 ,2-Dichloroethylenecis-1 ,3-Dichloropropenem-Dichlorobenzeneo-Dichlorobenzenep-D ichlorobenzenetrans- 1 ,2-Dichloroethylenetrans-1 ,3-DichloropropeneEthylbenzene2-Hexanone

ND K. i.o2.6 /*• 0.40ND t/ i.oNDNDNDNDND

1.00.400.401.01.0

ND ' 1.02.0 '* 0.40ND v/' 1.0ND ( 0.40ND 1.0ND *• 1.02.1 U 1.0ND ^ 0.40NDNDNDNDNDNDNDNDNDNDNDNDNDNDNDNDND

0.400.201.01.00.400.400.401.01.00.400.400.400.100.400.400.400.40

ND 0.10ND 1 0.40ND 5 1.0

ug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/Iug/lug/lug/lug/lug/l



00001


Client Sample ID: W10997Lab Sample ED: M2 183-2Matrix: AQ - Ground WaterMethod: SW8468260Project; Coakley Env. Monitoring, 480 Breakfast Hill

.~

Run#lRun #2

File ID DF Analyzed ByD0585.D 1 09/16/97 DRY


Rd., Greenland, NH


VGA 8260 List

CAS No.

87-68-398-82-899-87-6108-10-174-83-974-87-374-95-375-09-278-93-391-20-3103-65-1100-42-5630-20-671-55-679-34-579-00-587-61-696-18-4120-82-195-63-6108-67-8127-18-4108-88-379-01-675-69^75-01^1330-20-7

CAS No.

1868-53-72037-26-5460-00-4

Compound

HexachlorobutadieneIsopropy Ibenzenep-Isopropyltoluene4-Methyl-2-pentanoneMethyl bromideMethyl chlorideMethylene bromideMethylene chloride '• 2

Methyl ethyl ketoneNaphthalenen-PropylbenzeneStyrene1,1,1 ,2-Tetrachloroethane1,1,1-Tnchloroe thane1 , 1 ,2,2-Tetrachloroethane1 , 1 ,2-Trichloroethane1 ,2, 3-Trichloro benzene1 ,2,3-Trichloropropane1 ,2,4-Trichlorobenzene1 ,2,4-Trimethylbenzene1 ,3 ,5-TrimethylbenzeneTetrachloroethyleneTolueneTrichloroethyleneTrichloro fluoromethaneVinyl chlorideXylene (total)


DibromofluoromethaneToluene-D84-B ro mo fluorobenzene

Result

ND VNDNDNDNDNDND *

-.UiSW?1-'>5

ND &5.4 ft

ND ^NDNDNDNDNDNDND •ND {ND ]ND jND fND jND 1ND !ND |ND of

Run#l

97% .97%104%

RDL

1.01.01.01.00.401.01.00.401.01.01.01.01.00.400.400.401.01.01.01.01.00.400.400.400.400.400.40

Run* 2

Units Q

ug/1ug/1ug/1"ug/1ug/1ug/1ug/1

/I "Dug/1 B/Iug/1

ug/1/Iug/1/Iug/1J«

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/lug/1ug/1ug/1ug/1

Limits

86-118%88-110%80-120%



nnnmr

SACCUTESTReport of Analysis Page I o f 2


Run#lRun #2

File EDD0614.

BP4997M2 183-3AQ - GroundSW846 8260Coakley Env.

DFD 2

Water

Monitoring, 480

Analyzed09/18/97

Breakfast

ByDRY




VGA 8260 List


67-64-171-43-2108-86-174-97-575-27^75-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35^1563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106^6-7156-60-510061-02-6100-41^591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichlorome thaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1 , l-Dichloroethane1 , 1 -Dichloroethylene1 , 1 -Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1 ,2-DichIoroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2 , 2-D ichloropropaneDibromochJoromethaneDichlorodifluoromethanecis-1 ,2-Dichloroethylenecis- 1 ,3-Dichloropropenem-D ichlorobenzeneo-Dichlorobenzenep-Dichlorobenzenetrans- 1 ,2-Dichloroethylenetrans-1 ,3-DichloropropeneEthylbenzene2-Hexanone

ND K 2.012.1 A 0.80ND u 2.0NDNDNDND

2.00.800.802.0

0.65 A 2.0ND (J 2.028.3 .4 0.8033.3 A 2.0ND u 0.80ND | 2.0ND I 2.06.8 U 2.0ND U 0.8080.2 A- 0.80ND u 0.40NDNDNDNDNDNDNDNDNDNDNDND

2.02.00.800.800.802.02.00.800.800.800.20

;' ' ^0.80ND - 0.8010 A 0.80ND u 0.80ND U 0.2013.7 A 0.80ND \j 2.0

ug/1ug/1ugAugAug/1ug/1ug/1ug/1 Jug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ugAug/IugAugAugAugAugAugAugAug/1ug/1ug/1



0 0 0 0 1 5




BP4997M2 183-3AQ - GroundSW846 8260Coakley Env.

DFD 2

Water






VGA 8260 List

CAS No. Compound

87-68-3 Hexachlorobutadiene98-82-8 Isopropylbenzene99-87-6 p-Isopropyltoluene108-10-1 4-Methyl-2-pentanone74-83-9 Methyl bromide74-87-3 Methyl chloride74-88-4 Methyl iodide74-95-3 Methylene bromide75-09-2 Methylene chloride78-93-3 Methyl ethyl ketone91-20-3 Naphthalene103-65-1 n-Propylbenzene100-42-5 Styrene630-20-6 1,1,1,2-Tetrachloroethane71-55-6 1,1,1-Tnchloroethane79-34-5 1,1,2,2-Tetrachloroethane79-00-5 1,1,2-Trichloroethane87-61-6 1,2,3-Tnchlorobenzene96-18-4 1,2,3-Trichloropropane120-82-1 1,2,4-Trichlorobenzene95-63-6 1,2,4-Trimethylbenzene108-67-8 1,3,5-Tnmethylbenzene127-18-4 Tetrachloroethylene108-88-3 Toluene79-01 -6 Trichloroethylene75-69-4 Trichlorofluoromethane75-01-4 Vinyl chloride108-05-4 Vinyl Acetate1330-20-7 Xylene (total)


1868-53-72037-26-5460-00-4

D ibromofluoromethaneToluene-D84-B ro mo fluorobenzene

Result


RDL Units Q

ND <•<2.8 *ND UNDNDNDNDND '2.4 tND &

2.02.02.02.00.802.02.02.0

> 0.80: 2.0

12.6 A 2.0ND v.ND u

t 2.02.0

ND "-' 2.019.8ND vNDNDNDND ;

1.9 eND *ND l

1.4 A

A 0.80J 0.80

0.802.02.0

* 2.0^ 2.0t 2.01 0.80F 0.80

ND U 0.80NDNDND 1

0.800.802.0

4.7 A 0.80

Rucrf I Run? 2

98%96%96%

ug/1ugAugAug/1ug/1ug/1ug/1ug/tug/1ug/1ugAug/1ug/1ug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAugAugAug/1ugAugA

B

J

Limits

86-118%88-110%80-120%


000016


Client Sample ID:Lab Sample ID:Matrix:Method:Project:

Run#lRun #2

File EDD0586.

OP5997M2183-4AQ - GroundSW846 8260Coakley Env.

DFD 1

Water

Monitoring, 480

Analyzed09/16/97

Breakfast Hill

ByDRY


Rd., Greenland, NH


VGA 8260 List


67-64-171-43-2108-86-174-97-575-27-475-25-2104-51-8135-98-898-06-6108-90-775-00-367-66-395-49-8106-43-475-15-056-23-575-34-375-35-4563-58-696-12-8106-93-4107-06-278-87-5142-28-9594-20-7124-48-175-71-8156-69-410061-01-5541-73-195-50-1106^6-7156-60-510061-02-6100-41-4591-78-6

AcetoneBenzeneBromobenzeneBromochloromethaneBromodichloromethaneBromoformn-Butylbenzenesec-Butylbenzenetert-ButylbenzeneChlorobenzeneChloroethaneChloroformo-Chlorotoluenep-ChlorotolueneCarbon disulfideCarbon tetrachloride1,1-Dichloroe thane1 , 1-Dichloroethylene1 , 1-Dichloropropene1 ,2-Dibromo-3-chloropropane1 ,2-Dibromoethane1,2-DichIoroethane1 ,2-Dichloropropane1 ,3-Dichloropropane2,2-DichloropropaneDibromochloromethaneDichlorodifluorome thanecis-1 ,2-Dichloroethylenecis-1 ,3-Dichloropropenem-D ichloro benzeneo-D ichlorobenzenep-Dichlorobenzenetrans- 1 ,2-Dichloroethylenetrans- 1 , 3-DichloropropeneEthylbenzene2-Hexanone

ND f£~ 1.0ND I/ 0.40NDNDNDNDNDNDNDNDNDND

1.01.00.400.401.01.01.00.401.00.40

ND 1.0ND * 1.06.8 <J 1.0ND '̂ 0.40NDNDNDNDNDNDNDNDNDNDNDNDND-NDNDNDNDND

0.400.201.01.00.400.400.401.01.00.400.400.40

; 0.100.40

f 0.400.400.400.10

ND ' 0.40ND ./ 1.0

ug/1ug/1ug/1ugAug/1ugAugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/lug/Iug/1ug/1ug/1ugAug/1ugAug/1ug/1ug/1ugAugAugAugAugAugAugAug/1ug/1



oooovo



File IDRun#l D0586.Run n

OP5997M2183-4AQ - GroundSW846 8260Coakley Env.

DFD 1

Water






VOA 8260 List

CAS No. Compound

87-68-3 Hexachlorobutadiene98-82-8 Isopropylbenzene99-87-6 p-Isopropyltoluene108-10-1 4-Methyl-2-pentanone74-83-9 Methyl bromide74-87-3 Methyl chloride74-95-3 Methylene bromide75-09-2 Methylene chloride78-93-3 Methyl ethyl ketone91-20-3 Naphthalene103-65-1 n-Propylbenzene100-42-5 Styrene630-20-6 1,1,1,2-Tetrachloroethane71-55-6 1,1,1-Tnchloroethane79-34-5 1,1,2,2-Tetrachloroethane79-00-5 1,1,2-Tnchloroethane87-61-6 1,2,3-Tnchlorobenzene96-18-4 1,2,3-Trichloropropane120-82-1 1,2,4-Trichlorobenzene95-63-6 1,2,4-Tnmethylbenrene108-67-8 1,3,5-Trimethylbenzene127-18-4 Tetrachloroethylene108-88-3 Toluene79-01-6 Tnchloroethylene75-69-4 Tnchlorofluoromethane75-01-4 Vinyl chloride1330-20-7 Xylene (total)


1868-53-72037-26-5460-00-4

DibromofluoromethaneToIuene-D84-Bromofluorobenzene

Result RDL Units Q

ND o1 1.0NDNDNDNDNDND <

1.01.01.00.401.01.0

1.4 (J 0.40ND/2. 1.0ND u 1.0NDND

ne NDND

ne NDNDND

1.01.01.00.400.400.401.0

ND j 1.0ND } 1.0NDNDNDNDNDND

1.01.00.400.400.400.40

ND j 0.40ND / 0.40

Run#l Run? 2

9796 "989610496

ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1 Bug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/tug/1ug/1ugAug/1ug/1ug/lugAugA

Limits

86-118%88-1109680-12096


J = Indicates an estimated valueB = Indicates that analyte is found in associated method blankN = Indicates presumptive evidence of a compound pv n ^ ->

BACCUTESTReport of Analysis Page 1 of 1

Client Sample ID:Lab Sample ID:Matrix:

Project:

W5S997M2182-1AQ - Ground Water


Coakley Env. Monitoring, 480 Breakfast Hill Rd., Greenland, NH

Metals Analysis

Analyte Result RDL Units DF Prep Analyzed By Method

AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

<100 ^*<5.0 <••*"11.4 T274 *>A<4.0 u*<4.0 o1

68700 r"<20 <V<50 U<25 031700 J"<10 I/48200 :T4190 J~<0.50 yJ"<40 U63500 A< 10 u<7.0 U167000-7"<15 o<50 L/<40 u»

' 1005.05.01004.04.0500020502510010500015

"0.504010000107.050000155040

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

1111111111111111101110111

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBM

HBM

HBM

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

HBM

HBM

HBM

HBMHBM

HBM

HBMHBM

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 245.1EPA 200.7

EPA 258.1EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

RDL = Reported Detection Limit

000006


Client Sample ED:Lab Sample ED:Matrix:

Project:

W5D997M2182-2AQ - Ground Water



Metals Analysis



<100 L><5.0 <*'<5.0 \J188 /»<4.0 u<4.0 «->59000 T<20 a<50 ^<25 ^22300 r< 10 L'

47800 r1340 3"<0.50uJ"<40 ^42000 A<10 u

<7.0 ^1 82000 J~<15 O<50 ^<40 ^

1005.05.01004.04.0500020502510010500015

'0.504010000107.050000155040

ugAug/1ugAug/1ug/1ug/1ugAugAugAug/1ug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

1111111111111111101110111

09/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.710/03/97 10/03/97 HBM EPA 245.109/17/97 09/17/97 HBM EPA 200.709/17/97 09/29/97 HBM EPA 258.109/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.7

'I (/«•/* 7


n o n o i o


Client Sample ID: MW2997Lab Sample ID: M2182-3 Date Sampled: 09/04/97Matrix: AQ - Ground Water Date Received: 09/05/97

Percent Solids: n/aProject: Coakley Env. Monitoring, 480 Breakfast Hill Rd., Greenland, NH

Metals Analysis

Analyte


Result

<100 u

<5.0 ^9.3 r112 A<4.0 <J<4.0 <-•'82700 T<20 v<50 ^<25 u

38600 J"<10 l:29000 r11800 r

<0.50 ur<40 ^8840 flt< 10 ̂<7.0 °'73200 T<15 ^<50 vj<40 \J

RDL

1005.05.01004.04.05000205025100105000300.50401000107.010000155040

Units

ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

DF

111111111111121I1112111

Prep Analyzed By Method

09/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.710/03/97 10/03/97 HBM EPA 245.109/17/97 09/17/97 HBM EPA 200.709/17/97 09/29/97 HBM EPA 258.109/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.7

•^7


000014



Project:

W11997Date Sampled: 09/04/97Date Received: 09/05/97Percent Solids: n/a


AQ - Ground Water

Metals Analysis


AluminumAntimonyArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThallium a

VanadiumZinc

<100 V<5.0 •-'27.1 J"425 A<4.0 u<4.0 *-'280000 r<20 u<50 ^<25 U86100 3-<10 0197000 T2520 T<0.50 UJ~<40 o1

13100-3<10 (J<7.0 ^428000 T"<30 ^<50 ^<40 J

1005.05.01004.04.0500002050251001050000150.50402000107.050000305040

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ug/1ug/lug/1ug/1ug/1

1111111011111101112111021I

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17 79709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

HBMHBMHBM

HBM

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 245.1EPA 200.7

EPA 258. 1

EPA 200.7EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

(a) Elevated detection limit due to dilution required for matrix interference.


000018

BACCUTESTReport of Analysis Page 1 of 1

Client Sample ID: MW8997Lab Sample ID: M2 182-5 Date Sampled: 09/04/97Matrix: AQ - Ground Water Date Received: 09/05/97

Percent Solids: n/aProject: Coakley Env. Monitoring, 480 Breakfast Hill Rd., Greenland, NH

Metals Analysis

Analyte


Result

<100 v<5.0 i-'7.1 T240 A<4.0 v<4.0 ^86500 J~<20 w<50 ^<25 V7410 f<10 <*'74200 r8360 r<0.50 "-'-•"<40 U15000 A<10 v<7.0 w195000 J"< 15 u<50 ^<40 ^

RDL

1005.05.01004.04.050002050251001050001500.50402000107.050000155040

Units

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

DF

1111I11111111101121110111

Prep Analyzed By Method

09/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HUM EPA 200.709/17/97 09/17/97 HBM EPA 200.710/03/97 10/03/97 HBM EPA 245.109/17/97 09/17/97 HBM EPA 200.709/17/97 09/29/97 HBM EPA 258.109/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.709/17/97 09/17/97 HBM EPA 200.7


000022

HQQACCUTEST

Report of Analysis Page 1 of 1

Client Sample ED: MW8FD1Lab Sample ED: M2182-6Matrix:

Project:



AQ - Ground Water

Metals Analysis



<100 ^<5.0 u'6.0 J~225 A<4.0 ^<4.0 "82400 J~<20 is<50 »<25 L>6890 7-<10 <J70800 f7030 1"<0.50 u-~<40 ^'15200 A<10 u<7.0 *164000 f<15 J<50 -<40 ^

1005.05.01004.04.050002050251001050001500.50402000107.050000155040

ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

1111111111111101121110111

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709 / 17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBM

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

HBMHBM

HBMHBM

HBM

HBM

HBM

HBM

HBM

HBMHBM

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7EPA 200.7

EPA 200. 7

EPA 200.7EPA 200.7

EPA 245.1EPA 200.7

EPA 258.1EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200. 7

EPA 200.7


000026


Client Sample ID:Lab Sample ED:Matrix:

Project:

MW9997M2183-1AQ - Ground Water



Metals Analysis


AluminumAntimony *ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

<100 ^< 10 '̂128 T179 /*<4.0 V<4.0 U91900 y<20 U<50 "<25 J

105000^"<10 ^32800 f1790 3"<0.50 ^<40 vJ39000 -^<10 ^<7.0 w127000 J~<30 c,-<50 u-<40 ^

100105.01004.04.010000205025200105000150.504010000107.050000305040

ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

1211112.111211111101110211

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

HBMHBM

HBMHBMHBMHBMHBMHBMHBMHBM

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 245.1

EPA 200.7

EPA 258.1

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7


RDL = Reported Detection Limit000006

SACCUTESTReport of Analysis Page 1 of I

Client Sample ID: W 10997Lab Sample ID: M2183-2Matrix: AQ - Ground Water

Project: Coakley Env. Monitoring. 480 Breakfast


Hill Rd.. Greenland. NH

Metals Analysis

Analyte


VanadiumZinc

Result

. < 100 u<5.0 V29.2 r110 A<4.0 u<4.0 i>95200 J"<20 u

<50 u

<25 u

20600 f< 10 ^33300 r2850 ?"<0.50 <J<40 o>56000 A<10 v<7.0 ^195000 J"<75 w<50 f<40 ^

RDL

1005.05.01004.04.050000205025100105000150.504010000107.050000755040

Units

ug/lug/lug/lug/lug/lug/lug/lugAug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/l

DF

111111101111111I1101110111

Prep

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

Analyzed

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

By

HBM

HBM

HBM

HBM

HBM

HBM

HBMHBMHBMHBMHBM

HBMHBM

HBMHBMHBMHBMHBMHBMHBM

HBMHBMHBM

Method

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 245.1

EPA 200.7

EPA 258. 1EPA 200.7EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7



000010


Client Sample ID: BP4997Lab Sample ED: M2183-3Matrix:

Project:

Date Sampled: 09/05/97Date Received: 09/06/97Percent Solids: a/a.


AQ - Ground Water

Metals Analysis



<100 U<5.0 <-'52.9 3~147 ft<4.0"<4.0 ^125000 J~<20 U<50 <J<25 <J55500 f<10 i>60300 f

1640 T<0.50 i/44.1 /I60200 A<10 U<7.0u>266000 J~<15 ^<50 w<40 ^

1005.05.01004.04.050000205025100105000150.504010000107.050000155040

ug/Iug/1ug/1ug/lug/1ug/lug/lug/lug/lug/lug/lug/Iug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/l

I1111110111111111101110111

09/17/9709 117 19109/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709 717 79709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709 / [7/9709/17/9709/17/9709/17/9709/17/97

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

HBM

HBMHBM

HBM

HBM

HBM

HBM

HBMHBM

HBM

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 245.1EPA 200.7

EPA 258.1EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7


000014



Project:

OP5997Date Sampled: 09/05/97Date Received: 09/06/97Percent Solids: n/a


AQ - Ground Water

Metals Analysis



<100 v<5.0 V45.1 f<100 U<4.0 <J<4.0 U27600 3~<20 t/<50 U<25 it28600 3"< 10 l/5790 3"7600 f<0.50 (J<40 \J2930 -A<10 ^<7.0 V1 1400 J~< 15 J<50 V<40 0

1005.05.01004.04.05000205025100105000300.50401000107.05000155040

ug/1ug/1ug/tug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1

111111r1111112111111111

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

HBMHBM

HBMHBM

HBMHBM

HBM

HBM

HBM

HBMHBM

HBM

HBM

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 245.1EPA 200.7

EPA 258.1EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7EPA 200.7


000018



Project:

RP1997M2204-1AQ - Ground Water



Metals Analysis



2990 J<5.0 V46.6 f266 A<4.0 U<4.0 "94000 T

28.3 f<50 U<25 u'59200 r10.5 A47300 r1200 r<0.50 C58.2 A107000 *<10 f<7.0 V204000 r<15 <J<50 u>41.4 #

1005.05.01004.04.050000205025100105000150.504020000107.050000155040

ug/1ug/Iug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1

11111110111111111201110111

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709 '/1 7 79710/03/9709/17/9709 717/9709/17/9709/17/9709/17/9709 / IT 79709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709 / [7/9709/17/9709/17/9709/17/9709/17/9709/17/9709 / [7/9709 / [7/9709/17/9709 / [7/9710/03/9709/17/9709/29/9709 / 17/9709 / [7/9709/17/9709 / [7/9709 / [7/9709 / [7/97

HBMHBMHBMHBM

HBMHBMHBMHBMHBMHBMHBMHBMHBM

HBMHBMHBMHBMHBMHBMHBMHBMHBM

HBM

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 245.1EPA 200.7

EPA 258.1EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7


000006



Project:

105997M2216-1AQ - Ground Water


Coakley Env. Monitoring, 480 Breakfast Hill Rd.. Greenland, NH

Metals Analysis


AluminumAntimony.ArsenicBariumBerylliumCadmiumCalciumChromiumCobaltCopperIronLeadMagnesiumManganeseMercuryNickelPotassiumSeleniumSilverSodiumThalliumVanadiumZinc

<100 ^<5.0 t.'6.1 J"<100 (J<4.0 o'<4.0 U133000 J"<20 d<50 U<25 "7390 jT<10 \J46900 J"889 J"<0.50 e.'<40 u'7100 A<10 U<7.0 o'164000 J"<15 «-'<50 u<40 "'

1005.05.01004.04.025000205025100105000150.50401000107.025000155040

ug/1ug/1ug/1ug/1ug/1ug/1ug/lug/1ug/1ug/1ug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/lug/l

I1I11151111111111115111

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBMHBM

HBM

HBM

HBM

HBM

HBMHBMHBMHBMHBM

HBM

HBMHBM

HBMHBM

HBM

HBMHBMHBM

HBMHBMHBM

EPA 200.7EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 245.1EPA 200.7

EPA 258. 1EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7


O O O O O G


Client Sample ED:Lab Sample ID:Matrix:

Project:

C5A997M2216-2AQ - Ground Water



Metals Analysis



<100 V<5.0 ^36.7 f373 A<4.0 u<4.0 u135000 *"<20 ^<50 0<25 V22300 T*<10 (J64400 "f294 -J<0.50 "<40 L»47500 A<10 v<7.0 J322000 J"<15 U<50 v/<40 J

1005.05.01004.04.050000205025100105000150.504010000107.050000155040

ug/1ug/1ug/1ug/1ug/1ug/1ugAugAug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/lug/1ug/1ug/1ug/1ug/1

11111110111111111101110111

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

09/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/9710/03/9709/17/9709/29/9709/17/9709/17/9709/17/9709/17/9709/17/9709/17/97

HBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBMHBM

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7

EPA 245. 1EPA 200.7

EPA 258.1EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7

EPA 200.7


000010


Client Sample ED: OP2397 (WELL OP2)Lab Sample ID: M2362-1Matrix: AQ - Ground Water

Project: Coakley Env. Monitoring, 480 Breakfast



Metals Analysis

Analyte


VanadiumZinc

Result

114^ f<5.0 ^286 J-129 ft<4.0 <-'<4.0 *-'146000 J"<20 U<50 tr<25 V107000 r<10 U24400 ->"1010 '<0.50 U<40 <J48500 A<10 U<7.0 u

85000 ~<20 ^<50 "<40 ^

RDL

1005.05.01004.04.010000205025200105000150.504010000107.025000205040

Units

ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1ugAug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ug/1ugAug/1

DF

1111112111211I1110115211

Prep

10/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/03/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/97

Analyzed

10/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/15/9710/03/9710/15/9710/16/9710/15/9710/15/9710/16/9710/15/9710/15/9710/15/97

By

HBMHBMHBMHBMHBMHBM

HBMHBMHBM

HBM

HBMHBMHBM

HBM

HBM

HBM

HBM

HBM

HBMHBMHBMHBMHBM

Method

EPA 200.7

EPA 200.7EPA 200.7

EPA 200

EPA 200

EPA 200

.7

.7

.7EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7

EPA 200.7EPA 200.7

EPA 200.7EPA 200.7

EPA 245.1EPA 200.7

EPA 258.1

EPA 200.7

EPA 200 7EPA 273.1

EPA 200EPA 200EPA 200.

77

7



000006

QACCUTESTReport of Analysis Page l Qf

Client Sample ID: W5S997Lab Sample ID: M2 182-1Matrix:

Project:

AQ - Ground Water

Coakley Env. Monitoring,


480 Breakfast Hill Rd.. Greenland. NH

General Chemistry

Analyte Result RDL Units DF Analyzed By Method

Cyanide, Total <0.020 (J 0.020 mg/1 1 09/18/97 HBM EPA335.2

RDL = Reported Detection Limit 00000^

L-JLJSACCUTEST

Report of Analysis

Client Sample DD: W5D997Lab Sample ED: M2182-2Matrix: AQ - Ground Water

Project:


Coakley Env. Monitoring, 480 Breakfast Hill Rd., Greenland. NH

General Chemistry

Analyte

Cyanide, Total

Page 1 of 1

Result RDL Units

< 0.020 U 0.020 mg/1

DF Analyzed By Method

I 09/18/97 HBM EPA 335.2


000009

BACCUTESTReport of Analysis page {of l

Client Sample DD:Lab Sample ID:Matrix:

Project:

MW2997M2 182-3AQ - Ground Water



480 Breakfast Hill Rd., Greenland, NH

General Chemistry


Cyanide, Total <0.020 U 0.020 mg/1 1 09/18/97 HBM EPA335.2


000013

QACCUTESTReport of Analysis page i Of


Project:

W11997M2182-4AQ - Ground Water



480 Breakfast Hill Rd., Greenland. NH

General Chemistry


Cyanide, Total <0.020 U 0.020 mg/1 1 09/18/97 HBM EPA 335.2


000017

QACCUTESTReport of Analysis Page i of


Project:

MW8997M2 182-5AQ - Ground Water



480 Breakfast Hill Rd.. Greenland, NH

General Chemistry


Cyanide, Total < 0.020 U 0.020 mg/1 1 09/18/97 HBM EPA 335.2


SACCUTESTReport of Analysis Page i of i

Client Sample CD:Lab Sample ED:Matrix:

Project:

MW8FD1M2 182-6AQ - Ground Water

Coakley Env. Monitoring.



General Chemistry


Cyanide, Total <0.020 ^ 0.020 mg/1 1 09/18/97 HBM EPA335.2


000025

QACCUTESTReport of Analysis Page {of


Project:

MW9997M2183-1AQ - Ground Water




General Chemistry


Cyanide, Total <0.020 (J 0.020 mg/1 1 09/18/97 HBM EPA 335.2


000005

QACCUTESTReport of Analysis page i of


Project:

W 10997M2 183-2AQ - Ground Water

Coakley Env. Monitoring, 480


Breakfast Hill Rd., Greenland, NH

General Chemistry


Cyanide, Total <0.020 U 0.020 rag/1 1 09/18/97 HBM EPA335.2


ooocnn

SACCUTESTReport of Analysis Page l of


Project:

BP4997M2183-3AQ - Ground Water




General Chemistry


Cyanide, Total <0.020 C/ Q.020 mg/1 I 09/18/97 HBM EPA 335.2


000013

QACCUTESTReport of Analysis page i of i


Project:

OP5997M2 183-4AQ - Ground Water




General Chemistry


Cyanide, Total <0.020 O 0.020 mg/1 1 09/18/97 HBM EPA335.2

RDL = Reported Detection Limit ^

U U U U J /

QACCUTESTReport of Analysis P a g e l o f l


Project:

RP1997M2204-1AQ - Ground Water


Date Sampled: 09/08/97Date Receired: 09/09/97Percent Solids: n/a


General Chemistry


Cyanide, Total <0.020 (J 0.020 mg/1 1 09/18/97 HUM EPA 335.2

000005RDL = Reported Detection Limit

QACCUTESTReport of Analysis Page i of i

Client Sample ID: 105997Lab Sample ED: M2216-1 Date Sampled: 09/09/97Matrix: AQ - Ground Water Date Received: 09/10/97

Percent Solids: n/a

Project: Coakley Env. Monitoring, 480 Breakfast Hill Rd., Greenland, NH

General Chemistry

Anal ^ Result RDL Units DF Analyzed By Method

Cyanide, Total <0.020l/ 0.020 mg/1 1 09/18/97 HBM EPA 335.2

RDL = Reported Detection Limit 000005

Report of Analysis Page, of


Project:

C5A997M2216-2AQ - Ground Water




General Chemistry


Cyanide, Total < 0.020 U 0.020 mg/1 1 09/18/97 HBM EPA 335.2


n n n n n n

SACCUTESTReport of Analysis Page i of i

Client Sample ED:Lab Sample £0:Matrix:

Project:

OP2397 (WELL OP2)M2362-1AQ - Ground Water




General Chemistry


Cyanide, Total <0.020 U 0.020 mgA 1 10/07/97 SG EPA 335.2

RDL = Reported Detection Limit 000005

Download - Golder Associates Inc. , Golder Associates - · PDF fileMEMORANDUM TO: Coakley Landfill Site Project QA Record FR: Jeffrey R. Hendel, Golder Associates Inc. Cq RE: Data Validation

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