dls manual-8-17-2010

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    (Malvern Nano ZS)

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    Start-up

    Turn on the e ui ment ower

    Open the software Zetasizer Wait for up to 2-5 min. The light on the top button will

    turn red into green

    Create your measurement data file: open File

    New,

    or open your existing data file: open File open

    Measurement File, and select your data file

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    Loading Sample

    Size Measurement: add the sample solution

    n o ce w a e g e ween mm

    and 15mm (refer to the diagram on the

    backside of e ui ment lid , and insert the

    cuvette into sample holder

    Zeta Potential Measurement: use a s rin e to

    inject the sample solution into DTS1060C cell

    (refer to the instruction right) and put on the two

    .assembly panel of the cell as the front side.Fill the 1st half Fill the 2nd half

    Front panel

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    Creating Method

    Open File New SOP

    Click on Measurement type to select the rightmeasurement type: size, zeta potential, etc.

    ame e samp e

    Click on Material and define material type

    Click on temperature and set up measurement temperature

    Click on Cell and define sam le cell select DTS0012 for size

    measurement; DTS1060C for zeta potential)

    Click on Export and set up data export file (select Frequency Distribution

    emp a e, an e ne expor ename an pa

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    Running Measurement

    Run SOP: open Measure Start SOP, select your SOP,

    Press Start and wait until finished

    a n w n ow

    Multi-view

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    Viewing Data

    Size Measurement (under size category):

    e ec n ens y , o ume , ze

    quality report and Expert Advice to view the

    data and evaluate the data ualit . For bi-

    model samples, Z-Average is not useful

    information.

    category): Select Zeta Potential, Zeta

    quality report and Expert Advice to view the

    data and evaluate the data quality

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    Viewing Data

    Size Measurement (under size category):

    Make sure the unit of Z-Ave is d.nm (diameter) rather than r.nm(radius). To change it, click on the Z-Ave tab, and select d.nm.

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    To change the material, dispersant and data processing

    Editing Data

    setting after collecting data, highlight data in RecordsView, right click and select Edit Results.

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    xpor ng a Option 1: raw data

    o Highlight data that will be exported in Record View

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    xpor ng a Option 1: raw data

    o Open Edit Copy Size Statistics Table to copy the raw datao Paste the raw data to EXCEL or ORIGIN to plot a curve

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    xpor ng a Get number-based PSD data

    -

    o Right click on the tableo Select Number for number-based PSD

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    xpor ng a

    Option 2: graphic

    Open another application such as Excel, drag and drop a graph

    or table into the application by holding the Ctrl key

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    Shut-down

    Close the software Zetasizer Take off the sample, and clean the cells with DI water

    Turn off the power of equipment