dls manual-8-17-2010
TRANSCRIPT
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(Malvern Nano ZS)
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Start-up
Turn on the e ui ment ower
Open the software Zetasizer Wait for up to 2-5 min. The light on the top button will
turn red into green
Create your measurement data file: open File
New,
or open your existing data file: open File open
Measurement File, and select your data file
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Loading Sample
Size Measurement: add the sample solution
n o ce w a e g e ween mm
and 15mm (refer to the diagram on the
backside of e ui ment lid , and insert the
cuvette into sample holder
Zeta Potential Measurement: use a s rin e to
inject the sample solution into DTS1060C cell
(refer to the instruction right) and put on the two
.assembly panel of the cell as the front side.Fill the 1st half Fill the 2nd half
Front panel
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Creating Method
Open File New SOP
Click on Measurement type to select the rightmeasurement type: size, zeta potential, etc.
ame e samp e
Click on Material and define material type
Click on temperature and set up measurement temperature
Click on Cell and define sam le cell select DTS0012 for size
measurement; DTS1060C for zeta potential)
Click on Export and set up data export file (select Frequency Distribution
emp a e, an e ne expor ename an pa
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Running Measurement
Run SOP: open Measure Start SOP, select your SOP,
Press Start and wait until finished
a n w n ow
Multi-view
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Viewing Data
Size Measurement (under size category):
e ec n ens y , o ume , ze
quality report and Expert Advice to view the
data and evaluate the data ualit . For bi-
model samples, Z-Average is not useful
information.
category): Select Zeta Potential, Zeta
quality report and Expert Advice to view the
data and evaluate the data quality
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Viewing Data
Size Measurement (under size category):
Make sure the unit of Z-Ave is d.nm (diameter) rather than r.nm(radius). To change it, click on the Z-Ave tab, and select d.nm.
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To change the material, dispersant and data processing
Editing Data
setting after collecting data, highlight data in RecordsView, right click and select Edit Results.
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xpor ng a Option 1: raw data
o Highlight data that will be exported in Record View
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xpor ng a Option 1: raw data
o Open Edit Copy Size Statistics Table to copy the raw datao Paste the raw data to EXCEL or ORIGIN to plot a curve
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xpor ng a Get number-based PSD data
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o Right click on the tableo Select Number for number-based PSD
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xpor ng a
Option 2: graphic
Open another application such as Excel, drag and drop a graph
or table into the application by holding the Ctrl key
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Shut-down
Close the software Zetasizer Take off the sample, and clean the cells with DI water
Turn off the power of equipment