distillation/evaporation processes: limit of … distillation.pdf• distillation/evaporation...
TRANSCRIPT
![Page 1: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/1.jpg)
Distillation and evaporation in general
• Distillation/evaporation processes:
– Separate or undilute solutions (mixtures) based on the different volatilities of the components
• Limit of atmospheric operation:
– thermal sensitivity, decomposition under boiling temperature
• Solution:
– different kinds of vacuum distillation
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„Evolution steps” of vacuum distillers, evaporators
Batch vacuum distillation Falling film evaporator Wiped film evaporators
• Distillation below 1 mbar
• Low temperature: gentle handling (max. 250 °C)
• No thermal decomposition
• Vertical, polished evaporator surface
• Internal cooler
• Roller wiper
• Expensive technique
![Page 3: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/3.jpg)
Batch vacuum distillation
![Page 4: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/4.jpg)
„Evolution steps” of vacuum distillers, evaporators
Batch vacuum distillation Falling film evaporator Wiped film evaporators
• Distillation below 1 mbar
• Low temperature: gentle handling (max. 250 °C)
• No thermal decomposition
• Vertical, polished evaporator surface
• Internal cooler
• Roller wiper
• Expensive technique
![Page 5: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/5.jpg)
Falling film evaporator
![Page 6: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/6.jpg)
„Evolution steps” of vacuum distillers, evaporators
Batch vacuum distillation Falling film evaporator Wiped film evaporators
• Distillation below 1 mbar
• Low temperature: gentle handling (max. 250 °C)
• No thermal decomposition
• Vertical, polished evaporator surface
• Internal cooler
• Roller wiper
• Expensive technique
![Page 7: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/7.jpg)
Wiped film evaporators
![Page 8: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/8.jpg)
„Evolution steps” of vacuum distillers, evaporators
Batch vacuum distillation Falling film evaporator Wiped film evaporators
• Distillation below 1 mbar
• Low temperature: gentle handling (max. 250 °C)
• No thermal decomposition
• Vertical, polished evaporator surface
• Internal cooler
• Roller wiper
• Expensive technique
![Page 9: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/9.jpg)
![Page 10: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/10.jpg)
Roller-wiper system • Vertical and horizontal mixing
• Very thin film (<1 mm)
• Optimal heat transfer
• Low mechanical gear (lightweight)
• Material
• Fiber-glass reinforced PTFE
• Graphite
• Self-cleaning ability
Heating, cooling • Use of preheater
• Heat recovery?
• External steam-heated coat (Thermal
sheet)
• Heated pumps and product outlets
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• Main part of vacuum formation (regulation)
• Condensation just above melting temperature
• Theoretical optimum not feasible
• Problem of freezing product: multiple parallel evaporators
• Leakage
The condenser Vacuum system
• Only to evacuate non
condensable gases
• Generally consists of
Roots-blowers and
diffusion pumps
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Scale up process steps:
Laboratory • After computer
simulation
• Borosilicate glass
• Visual observation
• Feasibility studies
• 0,02 m2 evaporator
surface
• 0,1-0,8 kg/h feed rate
• Computer aided
Pilot
• Stainless steel
• 0,06 m2 evaporator
surface
• Feed rate: 3-9 kg/h
• Often took over by
manufacturer
Industrial: • Residence time:
maximum 20 s
• Evaporator surface: 50 m2
• 11,6 m high 2 m diameter
• 5000 kg/h capacity
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Scale up - Laboratory
• After computer
simulation
• Borosilicate glass
• Visual observation
• Feasibility studies
• 0,02 m2 evaporator
surface
• 0,1-0,8 kg/h feed
rate
• Computer aided
![Page 14: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/14.jpg)
Scale up process steps:
Laboratory • After computer
simulation
• Borosilicate glass
• Visual observation
• Feasibility studies
• 0,02 m2 evaporator
surface
• 0,1-0,8 kg/h feed rate
• Computer aided
Pilot
• Stainless steel
• 0,06 m2 evaporator
surface
• Feed rate: 3-9 kg/h
• Often took over by
manufacturer
Industrial: • Residence time:
maximum 20 s
• Evaporator surface: 50 m2
• 11,6 m high 2 m diameter
• 5000 kg/h capacity
![Page 15: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/15.jpg)
Scale up - Pilot
• Stainless steel
• 0,06 m2 evaporator
surface
• Feed rate: 3-9 kg/h
• Often took over by
manufacturer
![Page 16: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/16.jpg)
Scale up process steps:
Laboratory • After computer
simulation
• Borosilicate glass
• Visual observation
• Feasibility studies
• 0,02 m2 evaporator
surface
• 0,1-0,8 kg/h feed rate
• Computer aided
Pilot
• Stainless steel
• 0,06 m2 evaporator
surface
• Feed rate: 3-9 kg/h
• Often took over by
manufacturer
Industrial: • Residence time:
maximum 20 s
• Evaporator surface: 50 m2
• 11,6 m high 2 m diameter
• 5000 kg/h capacity
![Page 17: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/17.jpg)
Scale up – big industrial
• Residence time: maximum 20 s
• Evaporator surface: 0,3-50 m2
• 11,6 m high 2 m diameter
• 30-5000 kg/h capacity
![Page 18: Distillation/evaporation processes: Limit of … distillation.pdf• Distillation/evaporation processes: –Separate or undilute solutions (mixtures) ... distillation Film evaporator](https://reader031.vdocuments.mx/reader031/viewer/2022021417/5aa9352e7f8b9a72188c92a9/html5/thumbnails/18.jpg)
Operation
Atm
distillation
Vacuum
distillation
Film
evaporator
Short-path
distillation
Molecular
distillation
Pressure
(Pa) 10 5 10 3 10 2 0,1 10 -2
Residence
time (s) 4000 3000 25 10 1
Use cases
Petroleum
industry
Petroleum
industry
Pharmaceutical
Industry
Lanolin
cleaning
Plastic
softeners
Laboratory Laboratory Oil production Fish oil Vacuum oil
Industry Industry Food industry Butter
Separation of
fatty acids
Heat sensitive
materials
Chemical
industry Pepper oil
Separation of
dyes
Vitamins
Silicone oils
Alcohols
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Bibliography:
• UIC Short path vacuum distillaion from laboratory to
production
• Buss-SMS GmbH Feinvakuum Verdampfungsanlagen -
Fragen und Antworten
• Verfahrenstechnische Anlagen GmbH - Kurzweg-
Destillation
• UIC - Computer-gesteuerte Kurzweg-Destillationsanlage für
das Labor
• UIC - Competence in Vacuum distillation, thin film
distillation, short path distillation
• UIC-News Kurzweg-Destillation 1996.
• UIC News 1997 december, april; 2001 december