cryogen-free magnets for solid state nmr · cryogen-free magnets for solid state nmr ... z2, x, y,...
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www.cryogenic.co.uk
CRYOGEN-FREE NMR PRODUCTS
CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR
500 MHz and 600 MHz wide bore products
Special bore sizes available on request
Variable temperature inserts down to 2 K
Superconducting sweep coils
Custom magnets tailored to DNP
CF 600 MHz wide bore installed in Université Paris-Sud XI 2009 (*)
17O-NMR spectrum of Cu3Zn(OH)6Cl2 collected by sweeping main magnetic field over 6000 G about 12.9 T (*)
As-NMR spectrum of Sr2VO3FeAs pnictide at room temperature in magnetic field of 13 T. (*)
(*)courtesy Prof. P. Mendels and Dr. H. Alloul, Université Paris-Sud XI
CRYOGEN-FREE NMR PRODUCTS
CRYOGEN-FREE MAGNETS FOR SOLID STATE NMR
(*) Homogeneity measured by plotting field over 1 cm long x 1 cm diameter cylinder and specified assuming cryo-shims and room temperature shim settings have been optimized.
Technical Specifications
Product CF 600/89 AS CF 500/89 AS
Field strength 600 MHz (14.1T) 500 MHz (11.7T)
Homogeneity (*)
<0.1 ppm <0.1 ppm
Cryo-shims Z1, Z2, X, Y, C2, S2, ZX, ZY Z1, Z2, X, Y, C2, S2, ZX, ZY
Drift 0.1 ppm/hr 0.1 ppm/hr
Room Temperature bore
89 mm 89 mm
Field sweep -14.1 to 14.1 T - 11.7 to 11.7 T
Cryocooler 1.5 W pulse tube 1.5 W pulse tube
Compressor Water cooled, 3 phase power
Water cooled, 3 phase power
Cooldown time 48 hours 36 hours
www.cryogenic.co.uk
Cryogenic Limited
Unit 30
Acton Park Industrial Estate
London W3 7QE
United Kingdom
Tel: +44 (0)20 8743 6049
Email: [email protected]
www.cryogenic.co.uk
No cryogenic experience required
Turn-key operation
Overnight cool-down
Low cost of ownership
Minimal maintenance
Minimal quench hazards
Key Benefits of Cryogen-Free Technology
Leaving you to focus on the science
www.cryogenic.co.uk
CRYOGEN-FREE NMR PRODUCTS
CRYOGEN-FREE DESK-TOP NMR SYSTEMS
300 MHz and 400 MHz desk-top products
Variable temperature inserts
Superconducting sweep coils
Cryo-coolers with air-cooled compressors which run off single phase mains
Product features
Compact 7 T and 9.4 T cryogen-free magnets
NMR-grade homogeneity provided by cryo-shims and room temperature shims
NMR-grade drift
LabVIEW® based temperature diagnostics
Magritek Kea2 spectrometer with direct digital transmission & detection
Optional high stability oven-controlled oscillator for spectrometer
ProspaNMRsoftwarewithuser-configurable pulse programmer
The photograph shows an early prototype while the drawing illustrates our new product design
www.cryogenic.co.uk
CRYOGEN-FREE NMR PRODUCTS
CRYOGEN-FREE DESK-TOP NMR SYSTEMS
(*) Homogeneity measured by plottingfieldover1 cmlongx1cmdiametercylinderandspecifiedassuming cryo-shims and room temperature shim settings have been optimized.
Technical Specifications
Product CF 300/52 CF 400/52
Field strength 300 MHz (7T) 400 MHz (9.4T)
Homogeneity (*)
<0.1ppm <0.1ppm
Cryo-shims Z1,Z2,X,Y,C2,S2,ZX,ZY Z1,Z2,X,Y,C2,S2,ZX,ZY
Drift 0.1ppm/hr 0.1ppm/hr
Room Temperature Bore
52 mm 52 mm
Field sweep -7 to +7 T -9.4 to +9.4 T
Cryocooler 100mWGM 250 mW pulse tube
Compressor Air-cooled,singlephase Air-cooled,singlephase
Cooldown time Overnight Overnight
Cryogenic Limited
Unit 30
Acton Park Industrial Estate
London W3 7QE
United Kingdom
Tel: +44 (0)20 8743 6049
Email: [email protected]
www.cryogenic.co.uk
No cryogenic experience required
Turn-key operation
Overnight cool-down
Low cost of ownership
Minimal maintenance
Minimal quench hazards
Key Benefits of Cryogen-Free Technology
Leaving you to focus on the science