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Journal of AOAC INTERNATIONAL, Vol. 91, Iss. 1

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Journal of AOAC INTERNATIONAL

Volume: 91 | Issue: 1

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Agricultural Materials

An Updated Liquid Chromatographic Assay for the Determination of Glyphosate in Technical Material and FormulationsAuthors: Walter K. Gavlick and David F. Tomkins Page start: 1

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http://www.atypon-link.com/AOAC/doi/abs/10.5555/jaoi.91.1.1

http://www.atypon-link.com/AOAC/doi/pdf/10.5555/jaoi.91.1.1


Determination of Hydrazine in Maleic Hydrazide Technical and Pesticide Formulations by Gas Chromatography: Collaborative StudyAuthors: Anthony S. Riggs, David M. Borth, David G. Tutty and Wan S. Yu Page start: 5


Dietary Supplements

Validation of High-Performance Thin-Layer Chromatographic Methods for the Identification of Botanicals in a cGMP EnvironmentAuthors: Eike Reich, Anne Schibli and Alison DeBatt Page start: 13


Supplemental Information for: Validation of High-Performance Thin-Layer Chromatographic Methods for the Identification of Botanicals in a cGMP EnvironmentAuthors: Eike Reich, Anne Schibli and Alison DeBatt Page start: 1Supp


1b-Green Tea Validation ProtocolPage start: 5Supp


1c-Green Tea Validated MethodPage start: 32Supp






http://www.atypon-link.com/AOAC/doi/abs/10.5555/jaoi.91.1.1Supp

http://www.atypon-link.com/AOAC/doi/pdf/10.5555/jaoi.91.1.1Supp





2a-Ginseng Method EvaluationPage start: 39Supp


2b-Ginseng Validation ProtocolPage start: 48Supp


2c-Ginseng Validated MethodPage start: 71Supp


3a-Eleuthero Method EvaluationPage start: 76Supp


3b-Eleuthero Validation ProtocolPage start: 87Supp


3c-Eleuthero Validated MethodPage start: 114Supp
















4a-Echinacea Method EvaluationPage start: 119Supp


4b-Echinacea Validation ProtocolPage start: 120Supp


4c-Echinacea Validated MethodPage start: 150Supp


5a-Black Cohosh Method EvaluationPage start: 158Supp


5b-Black Cohosh Validation ProtocolPage start: 164Supp


5c-Black Cohosh Validated MethodPage start: 189Supp
















6a-Licorice Method EvaluationPage start: 196Supp


6b-Licorice Validation ProtocolPage start: 211Supp


6c-Licorice Validated MethodPage start: 234Supp


7a-Kava Method EvaluationPage start: 239Supp


7b-Kava Validation ProtocolPage start: 242Supp


7c-Kava Validated MethodPage start: 266Supp
















7d-Kava Method DevelopmentPage start: 270Supp


8a-Milk Thistle Method EvaluationPage start: 278Supp


8b-Milk Thistle Validation ProtocolPage start: 287Supp


8c-Milk Thistle Validated MethodPage start: 311Supp


9a-Feverfew Method EvaluationPage start: 316Supp


9b-Feverfew Validation ProtocolPage start: 325Supp
















9c-Feverfew Validated MethodPage start: 348Supp


10a-Ginger Method EvaluationPage start: 352Supp


10b-Ginger Validation ProtocolPage start: 363Supp


10c-Ginger Validated MethodPage start: 384Supp


Alkaloids and Saponins in Dietary Supplements of Blue Cohosh (Caulophyllum thalictroides)Authors: Subramaniam Satchithanandam, Erich Grundel, John Roach, Kevin D. White, Eugene Mazzola, Markus Ganzera and Jeanne I. Rader Page start: 21


Drug Formulations and Clinical Methods















Spectrophotometric and Reversed-Phase High-Performance Liquid Chromatographic Methods for Simultaneous Determination of Escitalopram Oxalate and Clonazepam in Combined Tablet Dosage FormAuthors: Santosh Vilashchand Gandhi, Nilesh Dnyandev Dhavale, Vijay Yeshawantrao Jadhav and Shweta Sadanand Sabnis Page start: 33


New Validated Liquid Chromatographic and Chemometrics-Assisted UV Spectroscopic Methods for the Determination of Two Multicomponent Cough Mixtures in SyrupAuthors: Ghada M. Hadad, Alaa El-Gindy and Waleed M.M. Mahmoud Page start: 39


Development and Validation of Column High-Performance Liquid Chromatographic and Ultraviolet Spectrophotometric Methods for Citalopram in TabletsAuthors: Júlia Menegola, Martin Steppe and Elfrides E.S. Schapoval Page start: 52


Development and Validation of an Agar Diffusion Assay for Determination of Ceftazidime in Pharmaceutical PreparationsAuthors: Cleber A. Schmidt, Marcelly Carazzo, Luciane V. Laporta, Celso F. Bittencourt, Marcos R. Santos and Milene Friedrich Page start: 59












New High-Performance Liquid Chromatographic Method for Determination of Clopidogrel in Coated TabletsAuthors: Juliana Sippel, Letícia L. Sfair, Elfrides E.S. Schapoval and Martin Steppe Page start: 67


Validated Stability-Indicating Methods for the Determination of Nizatidine in the Presence of Its Sulfoxide DerivativeAuthors: Rasha M. Youssef Page start: 73


Food Biological Contaminants

The Effect of Preenrichment and Selective Enrichment Media on Recovery of Salmonella Typhi from the Tropical Fruit MameyAuthors: Thomas S. Hammack, Andrew P. Jacobson and Wallace H. Andrews Page start: 83


Food Chemical Contaminants

Proposed Modifications to AOAC 996.06, Optimizing the Determination of Trans Fatty Acids: Presentation of DataAuthors: Brent Rozema, Barbara Mitchell, Doug Winters, Andrew Kohn, Darryl Sullivan and Erin Meinholz Page start: 92


Food Composition and Additives











Determination of Free and Reversibly-Bound Sulfite in Selected Foods by High-Performance Liquid Chromatography with Fluorometric DetectionAuthors: Stephen Wai Cheung Chung, Benny T.P. Chan and Andy C.M. Chan Page start: 98


Real-Time PCR for Quantitative Detection of Chamois (Rupicapra rupicapra) and Pyrenean Ibex (Capra pyrenaica) in MeatMixturesAuthors: Violeta Fajardo, Isabel González, Irene Martín, María Rojas, Pablo E. Hernández, Teresa García and Rosario Martín Page start: 103


Use of Physical and Chemical Properties of Commercial Tomato (Lycopersicon esculentum Mill.) Products forMonitoring Their QualityAuthors: Luis Eduardo Ordóñez-Santos, Enrique Arbones, Lourdes Vázquez-Oderiz, Angeles Romero-Rodríguez, Julio Gómez and Miguel López Page start: 112


Interlaboratory Evaluation of Two Enzyme-Linked Immunosorbent Assay Kits for the Determination of Crustacean Protein in Processed FoodsAuthors: Shinobu Sakai, Rieko Matsuda, Reiko Adachi, Hiroshi Akiyama, Tamio Maitani, Yasuo Ohno, Michihiro Oka, Akihisa Abe, Kohsuke Seiki, Hiroshi Oda, Kazuo Shiomi and Atsuo Urisu Page start: 123












Single-Laboratory Validation of a Liquid Chromatographic/Tandem Mass Spectrometric Method for the Determination of Free and Total Carnitine in Infant Formula and Raw IngredientsAuthors: Dustin E. Starkey, James E. Denison, C. Thomas Seipelt and Wesley A. Jacobs Page start: 130


Event-Specific Qualitative and Quantitative Polymerase Chain Reaction Methods for Detection of Genetically Modified Rapeseed Ms8×Rf3 Based on the Right Border JunctionsAuthors: Gang Wu, Yuhua Wu, Ling Xiao and Changming Lu Page start: 143


Microbiological Methods

Modifications to the AOAC Use-Dilution Test for Quaternary Ammonium Compound-Based Disinfectants That Significantly Improve Method ReliabilityAuthors: Crystal Arlea, Sharon King, Barbara Bennie, Kere Kemp, Erin Mertz and Richard Staub Page start: 152


Validation Study to Demonstrate the Equivalence of a Minor Modification of Assurance® Enzyme Immunoassay Method, Official Method 996.14, for Detection of Listeria in Foods and Environmental Surfaces to the Reference Culture MethodsAuthors: Philip T. Feldsine, David E. Kerr and Andrew H. Lienau Page start: 159












Evaluation of the VIDAS® Staph Enterotoxin II (SET 2) Immunoassay Method for the Detection of Staphylococcal Enterotoxins in Selected Foods: Collaborative StudyAuthors: Robert P. Jechorek and Ronald L. Johnson Page start: 164


Residues and Trace Elements

Pressurized Liquid Extraction and Microwave-Assisted Extraction in the Determination of Organochlorine Pesticides in Fish Muscle SamplesAuthors: Mercedes Barriada-Pereira, Ivén Iglesias-García, María J. González-Castro, Soledad Muniategui-Lorenzo, Purificación López-Mahía and Darío Prada-Rodríguez Page start: 174


Determination of Low-Level Pesticide Residues in Soft Drinks and Sports Drinks by Liquid Chromatography with Tandem Mass Spectrometry: Collaborative StudyAuthors: Kathleen D. Miller and Paul Milne Page start: 181


Determination of Pesticide Residues (>0.5 μg/L) in Soft Drinks and Sports Drinks by Gas Chromatography with Mass Spectrometry: Collaborative StudyAuthors: Kathleen D. Miller and Paul Milne Page start: 202












Development and Statistical Validation of a Quantitative Method for the Determination of Steroid Hormones in Environmental Water by Column Liquid Chromatography/Tandem Mass SpectrometryAuthors: Christophe Stavrakakis, Ronan Colin, Valérie Héquet, Catherine Faur and Pierre Le Cloirec Page start: 237


Statistical Analysis

Interlaboratory System to Ensure and Improve the Quality of Glassware Calibration and Use in a Large LaboratoryAuthors: Laura Flores, Claudia Santo and Mónica Trías Page start: 247


Veterinary Drug Residues

Application of Matrix Solid-Phase Dispersion and High-Performance Liquid Chromatography for Determination of Sulfonamides in HoneyAuthors: Qiong-Hui Zou, Jin Wang, Xiang-Feng Wang, Yuan Liu, Jie Han, Feier Hou and Meng-Xia Xie Page start: 252


General Referee Reports

Committee on Natural Toxins and Food AllergensAuthors: Gordon S. Shephard Page start: 1B









http://www.atypon-link.com/AOAC/doi/abs/10.5555/jaoi.91.1.1B

http://www.atypon-link.com/AOAC/doi/pdf/10.5555/jaoi.91.1.1B


Committee on Residues and Related TopicsAuthors: Jon W. Wong Page start: 17B


Committee on Microbiology and Extraneous MethodsAuthors: Thomas S. Hammack Page start: 23B


Committee on Biological Threat AgentsAuthors: Tony Hitchins Page start: 32B


Methods Committee Reports

Committee on Pesticide and Disinfectant FormulationsAuthors: Adrian W. Burns, Diane M. Rains, Warren Robert Bontoyan, Doug Marsh, Christopher L. Ritland, Earlene Erbe, Rose Nelson, Qirong Wu, Rodney Noel and Jung K. Lee Page start: 34B












Methods Committee on Additives, Beverages, and Food Process-Related Analytes and Filth and Extraneous Materials in Food and DrugsAuthors: Janice I. Byington, M. Sarita Cardozo, Sneh D. Bhandari, Nathalie Boivin, Charles Eckermann, Steve A. Kupina, Kris Paterson, Anne P. Reid, Lars M. Reimann and Janet Scalese Page start: 36B


Committee on Natural Toxins and Food AllergensAuthors: Tetsuhisa Goto, Chris M. Maragos, Jean-Marc Fremy, Robert A. Labudde, Tom W. Nowicki, Seth H. Pincus, Joerg Stroka, Mary W. Trucksess, Hans P. van Egmond, Argentina G. Vindiola and Kristina M. Williams Page start: 38B


Committee on Food NutritionAuthors: Katherine E. Sharpless, John Szpylka, Dirk D. Shoemaker, G. Sarwar Gilani, Wayne R. Wolf, Jeanne Rader, Shang-Jing Pan, Marina Torres, David C. Woollard, John G. Phillips and Sara M. Williams Page start: 42B


Commodity Foods and Commodity ProductsAuthors: George W. Latimer, Jr, Prabhakar Kasturi, Julie Henderson, John G. Phillips, P. Christopher Ellis, Quian Graves, Joseph Hillebrandt, I-Pin Ho, Joanna M. Lynch, John M. Tennyson and Kendra C. Pfeifer Page start: 44B












Committee on Residues and Related TopicsAuthors: Stephen G. Capar, Jo Marie Cook, James Bell, Heidi Hickes, Alexander J. Krynitsky, Steven J. Lehotay, Christopher L. Ritland, Frank J. Schenck, David Soderberg and John G. Phillips Page start: 46B


Committee on Microbiology and Extraneous MaterialsAuthors: Wayne A. Ziemer, Melissa C. Newman, Todd Marrow, James R. Agin, Michael H. Brodsky, James E. Brown, Joseph L. Ferreira, Yvonne M. Hale, Walter E. Hill, Charles E. Pixley, Daniel Rice, Roxanne Shively, Kevin J. Vought, Robert A. LaBudde, Robert W. Phillips and Paul Wehling Page start: 49B


Committee on Feeds Fertilizers and Related Agricultural TopicsAuthors: Nancy Thiex, Luann Wetzler, Sara Williams, John G. Phillips, Michael P. Carlson, John Dennis McCurdy, James MacNeil, Dave Mertens and Rodney J. Noel Page start: 59B


Methods Committee on Dietary SupplementsAuthors: Richard Myers, Argentina Vindiola, John G. Phillips, Randall Smith, James Neal-Kababick, Martha Gay, David Ji, Dean Gray, Mark L. Anderson, Ikhlas Khan, George E. Porter and Klaus Reif Page start: 63B












Biological Threat AgentsAuthors: Deborah A. Loveys, Mary McBride, Cheryl Gauthier, Helen Spencer, Patrick J. Treado, Christina Egan, Patrick Eugene Williams, Seth H. Pincus, Robert A. LaBudde, Daryl S. Paulson, Christina Z. Thompson, Mark R. Coleman, Anthony Hitchins, Mark Poli and Brad Stawick Page start: 65B


Committee on Antimicrobial Efficacy TestingAuthors: James Agin, Daniel Klein, Donna B. Suchmann, Lynne M. Sehulster, Candace McManus, Jafrul Hasan, Tajah Lynette Blackburn, Allison Rodriguez, Gayle Mulberry, Vipin K. Rastogi, Eduardo Gomez and Daryl S. Paulson Page start: 68B


Technical Committee Reports

Safety CommitteeAuthors: Argentina G. Vindiola, Eugene Chechik, Sara M. Williams, Julie Henderson, Paul W. McCormack, Robert W. Phillips, Dermont Hayes, David N. Clark, Christina Z. Thompson and Eduardo Gomez Page start: 73B


Statistics CommitteeAuthors: Paul Wehling, Foster D. McClure, Qian F. Graves, Robert A. LaBudde, Jung K. Lee, Zichao Lin, Daryl S. Paulson, John G. Phillips and Stephen Sherken Page start: 74B


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